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HomeMy WebLinkAboutWQ0036723_Application_20230323NC DIVISION OF WATER RESOURCES Check Number: 001 R8544 Invoice Date Invoice Number P.O. Number Voucher Invoice Description Net Invoice Amount 02/2312023 022323 CLASS A PERMIT RENEWAL - 810.00 #W00036723 Vendor No. Vendor Name Check No. Check Date Check Amount 5681 NC DIVISION OF WATER RESOURCES 00188544 03/03/2023 810.00 Town of Mooresville Finance Department P.O. Box 878 Mooresville, NC 28115 (704) 663-3800 Fax (704) 663-7386 aectspayable@mooresvillenc.gov 'AY Eight Hundred Ten Dollars and 00 Cents* To the NC DIVISION OF WATER RESOURCES Order Of ATTN: ANIMAL/DISCHARGE/NON-DISCHARGE BILLING 1617 MAIL SERVICE CENTER RALEIGH, NC 27699-1617 VELLS FARGO BANK, N.A. Check Check Date Number 11-24 03/03/2023 00188544 1210 VOID IF NOT PRESENTED FOR PAYMENT WITHIN 180 DAYS $810.00 Provisions for the payment of Ws warrant has been made by an appropriation duly made or a bond or note duly authorized, as required by the Local Govemment Budget and Fiscal Control Act. Authorized Signature MP Interim Finance Officer 1111100 18854411' I: 1 2 L000 2481: 2000000447 26311■ State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Agolicant shall submit one original and two copies of the ai2vlication and sun1aortin2 documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b1. ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). I � Facility Classification New Permit Major Modification' Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 i $395 I Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3 D. Program Information (All Application Packages) ® Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. ® How the residuals will be processed/treated (attach process flow diagram). ® How leachate collection will be handled. ® Where the residuals will be stored until processed. ® How the final product will be distributed (packaging, bulk, etc.) ® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ® Name and address of the person who prepared the residual that is sold or given away. ® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ® Information on all applicable setbacks in accordance with 15A NCAC 02T .I 108(b). ® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104 a . Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1104t2 iI B 1, including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). G. Environmental Assessments (Maybe Required— See 15A NCAC 1C .0300) ❑' Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .I 110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted,_ the Applicant shall submit one original and two conies of the application and sugnorting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR I1-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC I 1-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Maya Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 To: NCDWQ/AQUIFER PROTECTION SECTION/LAND APPLICATION UNIT Re: Renewal for Class A Distribution Permit - Permit# WQ0036723 The Town of Mooresville wishes to Renew our Distribution of Class A residuals permit. In this application package, we believe that all the requested information has been provided. If additional information is needed, please see contact info at the bottom of this letter. Please see the attached documents referenced in the application, one original and two copies. ➢ A check in the amount of $810.00 made payable to NCDEQ. ➢ Completed Distribution of Class A Residuals (DCAR 06-16) form. ➢ Attachment 1 - Program information and flow diagram ➢ Attachment 2 - Marketability Statement ➢ Attachment 3 — Product label/information sheet. ➢ Attachment 4 — Operation and Maintenance Plan. ➢ Completed Residuals Source Certification (RSC 06-16) form ➢ Attachment 5 — Vicinity Map. ➢ Attachment 6 — Quantitative justification statement. ➢ Attachment 7 — Sampling Plan. ➢ Attachment 8 — Laboratory analytical data. Thank you for your time and consideration. Allison Kraft, Utilities Director Phone 704-799-4066 akraft ci mooresvillenc. ,ov Jamie Levis, WWTP Plant Manager Phone 704-662-8341 tlevis c mooresvillenc.gov Larry Hendren, WWTP Biosolids Coordinator Phone 704-799-4063 lhendrenLd)mooresvillenc.g ov DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 —DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Town of Mooresville Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Jamie Levis Title: Plant Manager Applicant's mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115- Telephone number: (704) 662-8341 Email Address:,ilevis[?mooresvillenc.gov 2. Consultant's name: License Number (for P.E.): Affiliation: ❑ On Staff ❑ Retained (Firm: ) Consultant's mailing address: City: State: Zip: Telephone number: (`) Email Address: 3. Fee submitted: $810.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00036723 Date of most -recently issued permit: August 30, 2018 Date of most -recently certified Attachment A (if different than the permit): December 9. 2021 III. FACILITY INFORMATION: 1. Name of residuals processing facility: Rocky River Wastewater Treatment Facility City: Mooresville State: NC Zip: 28115- Coordinates: Latitude: 35' 3 F 33" Longitude: 80' 46' 56" Datum: Level of accuracy: Method of measurement: GPS County where facility is located: Iredell 2. Facility contact (person familiar with residuals preparation): Name: Larry Hendren Title: Biosolids Coordinator Mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115- Telephone number: (704) 799-4063 E-mail address: lhendren@mooresvillenc.gov FORM: DCAR 06-16 Pagel of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 180 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); Bulk residuals given to local farmers Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials I Amounts to be added per 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 1600 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 1100 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Storage is on a covered and_ paved pad with dimensions I I P x 79'. Average storage time is 60 days. Maximum storage time 180 day 6. Does the facility have a stormwater management plan? ® Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Storage area is under permanent steel erected roof. Pad is also sloped in the event of water intrusion so that the runoff would be directed to a drainage line that goes back to the head of the_plant. V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. RSC 06-16.doc FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) , attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ❑ Yes KNo, Explain; — —P "'1A^ (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for (Facility Name) C Da (-/� ? 13' has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,OO)(per violation. 3 � 3 2oZ Signatur ,. Date: 3 .00" FORM: DCAR 06-16 Page 3 of 3 4800�pS` 4. !a� P not ap Attachment1' 1 1 1 1 Processed residual pellets are transported from dryer to covered facility where they are stored from 30 — 180 days until recipients/end users are ready for delivery. Recipients coordinate bulk hauling of residuals to their final destination through correspondence with the Biosolids Coordinator. Suggested nutrient limiting factors could be nitrogen, phosphorus, calcium and aluminum. Leachate is not a concern due to cover storage pad. However, pad is sloped to drainage line as an extra safety precaution. Process flow is explained below: Waste activated sludge is pumped from WAS basin to one of two aerobic digesters. Sludge is held in digesters before being pumped to a belt press. The sludge is dewatered and pressed to achieve an approximate 14-16% cake which is conveyed to a storage hopper. The cake is then conveyed to the belt dryer system where it is heated for 4 hours at —20OF to achieve 90% - 98% dry Class A pellet. Dry pellets are conveyed to a dump truck. Dump truck transfers product to the covered storage facility until ready for final bulk shipping. Loaded trucks leaving the facility contain 4 — 8 tons of residuals depending on the vehicle. of F400r�.S, la�eR\NVolcfia�Attachment 2 — Marketability Statement All Class A residuals are distributed to local farmers who land apply in accordance with the Town of Mooresville Utilization Agreement. Residuals were applied at predetermined agronomic rates by their own equipment. A total of 1093.02 dry tons left the facility in 2022. For 2021 we completed a permit modification to raise our distribution rate to 1600 dry tons per year. Attachment 3 — Product Label/Information Sheet No product label — Current Class A Utilization Agreement Included TOWN OF MOORESVILLE CLASS A BIOSOLID PELLETS UTILIZATION AGREEMENT DISTRIBUTED UNDER NC DWQ PERMIT # WQ0036723 I. CONTACT INFORMATION THIRD PARTY INFORMATION Name Mailing Address Phone Number Email TOWN OF MOORESVILE INFORMATION Larry Hendren (Permittee Designee) P.O. Box 878, Mooresville NC 28115 704-799-4063 lhendren@mooresvillenc.gov II . DESCRIPTION This is pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A biosolid product according to the EPA's 40 CFR Part 503 regulations. III. RESTRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agreement: 1. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat 2. If the application causes prolonged nuisance conditions 3. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards 4. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year flood elevation, unless the bulk residuals are injected or incorporated within a 24- hour period following a residuals land application event 6. During a measurable precipitation event (i.e. greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period 7. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop 8. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event 9. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot 10. If the vertical separation of bedrock and the depth of residuals application is less than one foot 11. Biological Residuals shall not be stockpiled for more than 30 days prior to distribution 12. The Third Party accepting the residuals shall provide the Permittee with all other nutrient applications (i.e. organic and/or inorganic fertilizers) 13. A copy of this Utilization Agreement shall be maintained at the site when bulk residuals are being applied 14. The residuals shall be prevented from entering any public or private water supply source (including wells) and any surface waters (e.g. streams, lake, river, wetland) 15. Residuals should be land applied at agronomic rates 0 2021 Town of Mooresville 16. Submission of Soil Samples prior to distribution of product 17. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement IV. SETBACKS Applicable setbacks in accordance with 15A NCAC 02T .1108(b): Description of Setback Setback by type of application (feet) Cake Residuals Private or public water supply 100 Surface Waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 25 Surface water diversions (ephemeral streams, waterways, ditches 0 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT) 0 Wells with exception to monitor' wells 100 Bedrock outcrops 0 V. APPLICATION RATES Application Rates should not exceed the calculated nitrogen requirements based on the Realistic Yield Expectation for a particular crop and the predominant soil series within the application area. This product has a North Carolina Fertilizer label of 5% Nitrogen — 1% Phosphorus — 0% Potassium ratio, but given that it is generated from aerobically digested residual biosolids it is assumed that a 30% mineralization rate (Organic Nitrogen to Plant Available Nitrogen) is used to calculated the Plant Available Nitrogen (PAN). The PAN listed below should be used along with other nutrient application to determine agronomic rates. NUTRIENT RANGES Percent Solids: 94-98% Total Nitrogen: 22-100 lbs_ ton Ammonia Nitrogen: 0.4-61bs/ton Nitrate/Nitrite Nitrogen: 0 - 0.01 lbs/ ton PAN: 7-40 lbs/ton Total Phosphorus: 20-38 lbs1 ton (as P-O;) Total Potassium: V. AGREEMENT 0-10 lbs/ton (as K 0) Larry Hendren, Town of Mooresville Date Approximate Density:15 - 20 lbs ft3 Third Party (Printed Name) Third Party (Signature) Date 0 2021 Town of Mooresville 1 1 Attachment 4 — Operations and Maintenance Plan Operations and Maintenance The Town of Mooresville's Rocky River WWTP is permitted to discharge 7.5mgd. The current average flow is 4.Omgd. The incoming waste stream is protected from excessive fats, oils, and grease by our FOG program though a system of monitoring and permitting local dischargers. The incoming waste stream is further protected from heavy metals and other toxins through our industrial Pretreatment program system of permitting and monitoring. The plant's extended air activated sludge is managed by our Operations Supervisor and Biosolids Coordinator. This sludge is pumped to one of two digesters. We operate the digesters on a rotational basis filling and digesting one while removing sludge from the other via our belt press. We rotate the digester functions approximately every 30 days. The belt press solids are then transferred to the belt dryer system where we achieve an average dryness of 95%. All maintenance and calibration schedules are based on manufacturer's recommendations. Safety protocols are based on OHSA requirements. All wet processes are either contained or directed to an internal drainage system that leads back to the head of the plant. Inspection Plan Daily inspections are performed by the Biosolids Coordinator of all equipment, safety, and records. Any problems are reported to the Operations Supervisor. Weekly inspections are performed by the Operations Supervisor of all equipment, safety, and records. Any problems are reported to the Plant Manager. Monthly inspections are performed by the Plant Manager of all equipment, safety, and records. Any problems are reported to the Utilities Director. Annual review performed by the Utilities Director. Annual safety inspection performed by the Town's Safety Committee. During operational inspections if any noncompliant solids are observed they will be reintroduced to the system of disposed of in a lined landfill. All safety issues will be corrected in house as soon as noted. All records will be verified monthly by at least three people. Sampling Plan In house percent solids testing will be done by the Biosolids Coordinator and verified by our Laboratory Analyst. Samples will be sent to a certified commercial lab for TCLP analyses. Ignitability, corrosivity and reactivity will be conducted annually. Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted quarterly. Heat drying will be used to meet pathogen reduction. Drying of stabilized residuals will be used to meet vector attraction reduction. Sample location will be at the exit of the dryer. Sample type will be grab. F 0 R y O � O L � H C L A E •CK a C � O O � L L � �+ M N G l� M O O � 3 Q, 7 � U a c R 3 3 CJ 0 GTy U L b O x �> � o o � O w �W C � V� U w ti oq a State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Rock. River Wastewater Treatment Facility 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Larry Hendren Complete mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115- Telephone number: (704) 799-4063 E-mail address: lhendrennmooresvillencgov 4. Facility physical address: 369 Johnson Dairy Rd City: Mooresville State: NC Zip: 28115- Coordinates: Latitude: 35' 3 F 33" Longitude: 80' 46' 56" Datum: Level of accuracy: Method of measurement: GPS 5. Purpose of the facility: ® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ® Yes ❑ No 7. Facility permitted/design flow: 75 MGD and facility average daily flow: 4 MGD 8. Average amount of residuals being generated at this facility 1100 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 1.1MG aerobic digestion, belt press to 14%-16% solids, heat dry to above 90% solids Type and volume of residuals storage (i.e., outside of residuals treatment units): 111' x 79' covered Rad II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257, 2. Specify if residuals are defined under 15A NCAC 02T.1102; 6) as: ® Biological ❑ Non -Biological FORM: RSC 06-16 Page 1 of 61 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: WWOint Analytical and Date of analysis: 1-9-23 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: 204.8 OF (> 140°F) Passed reactivity test: ®yes ❑no. HCN: <0.125 mg/kg (<250) & H2S: <25 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (m9/1) TCLP Parameter Limit (mg/1) Result (m9/1) Arsenic 5.0 <0.250 Hexachlorobenzene 0.13 <0.100 Barium 100.0 <0.250 Hexachloro-1,3-Butadiene 0.5 N/A Benzene 0.5 <0.0050 Hexachloroethane 3.0 <0.100 Cadmium 1.0 <0.0500 Lead 5.0 <0.100 Carbon Tetrachloride 0.5 <0.0200 Lindane 0.4 N/A Chlordane 0.03 <0.02000 Mercury 0.2 <0.0200 Chlorobenzene 100.0 <0,.0050 Methoxychlor 10.0 <0.004000 Chloroform 6.0 <0.0050 Methyl Ethyl Ketone 200.0 0.209 Chromium 5.0 <0.100 Nitrobenzene 2.0 <0.100 m-Cresol 200.0 N/A Pentachlorophenol 100.0 <0.200 o-Cresol 200.0 N/A Pyridine 5.0 <0.100 p-Cresol 200.0 N/A Selenium 1.0 <0.500 Cresol 200.0 N/A Silver 5.0 <0.0500 2,4-D 10.0 <0.0200 Tetrachloroethylene 0.7 N/A 1,4-Dichlorobenzene 7.5 <0.0050 Toxaphene 0.5 <0.03000 1,2-Dichloroethane 0.5 <0.0050 Trichloroethylene 0.5 N/A 1, 1 -Dichloroethylene 0.7 <0.0050 2,4,5-Trichlorophenol 400.0 <0.100 2,4-Dinitrotoluene 0.13 <0.100 2,4,6-Trichlorophenol 2.0 <0.100 Endrin 0.02 <0.004000 2,4,5-TP (Silvex) 1.0 <0.0020 Heptachlor and its Hydroxide 0.008 N/A Vinyl Chloride 0.2 <0.0050 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For DistributionlLand Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 1-9-23 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 3.59 Cadmium 85 39 0.582 Copper 4,300 1,500 176 Lead 840 300 8.77 Mercury 57 17 <0.196 Molybdenum 75 n/a 12.8 Nickel 420 420 10.2 Selenium 100 100 2.81 Zinc 7,500 2,800 370 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of FORM: RSC 06-16 Page 4 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 1-9-23 Parameter Result (mg/kg) Aluminum 15000 Ammonia -Nitrogen 3120 Calcium 13100 Magnesium 2530 Nitrate -Nitrite Nitrogen <10.4 pH (Standard Unit) 6.5 Phosphorus 16900 Potassium 2970 Sodium 795 Total Kjeldahl Nitrogen 53100 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.13 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (11t) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 9,640 Injection/Incorporation 10,490 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 5 of 7. Pathoeen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application OL Class A or E uivalent: ® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ® Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ® heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal. ® Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II.7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization. ® Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 6 of 5 �o� Pf1Unr�s� t she Nunn�o Attachment 5 — Vicinity Map The attached Vicinity Map was obtained from Iredell County GIS Website and includes an overview of the entirety of the plant. ireaeu uounry, i%jorEn tarouna Tax Map Information • PIN 4675025684.000 • Address 369 JOHNSON DAIRY RD •Account# Acct 47807000 • Tax Owner TOWN OF MOORESVILLE • Mailing PO BOX 878 Address • MOORESVILLE, NC 28115 • GIS Owner TOWN OF MOORESVILLE • Deed Info 10011213 - WD - 19961009 • Tax Acres 244.065 AC Lot # • Description TOWN OF MOORESVILLE SR1146 ANNEX PB43-3 • Zoning RLS • Old Parcel# 0301E000OOA017 • Bldg Value $51.450 • OBXF Value $0 • Land Value $1,903,710 • Total Value $1,955,160 • Defer Value $0 •Tax MOORESVILLE--- Districts Rocky River VWIWTP MAP FOR REFERENCE ONLY NOT A LEGAL DOCUM ENT Iredell County, North Carolina makes no claims and no warranties, expressed or implied, concerning the validity or accuracy of the GIS data presented on this map. Geometry updated 0211612023 Data updated 02/16/2023 r f—CUIUdIy LIJ, GVLJ 1" = 271.44626735956274 ft �.,Joliris 1 Print map scale is approximate. Critical layout or measurement activities should not be done using this resource. Attachment 6 — Quantitative Justification Statement The figure presented in Section 1.8. was based upon the 2022 Class A Annual Sludge Report. We are currently permitted to produce 1600 dry tons. Records state that a total of 1093.02 dry tons left the facility in 2022. We are currently running the dryer at the maximum capacity and operate on a 24/7 basis except during periods of maintenance or malfunction. Residuals production greater than the permitted 1600 dry tons would be unlikely without major dryer modifications and are not forecasted for the upcoming permit term. `rho NormalAttachment 7 — Sampling Plan Sampling Plan In house percent solids testing will be done by the Biosolids Coordinator and verified by our Laboratory Analyst. Samples will be sent to Waypoint Analytical, a certified commercial lab for TCLP analyses. Ignitability, corrosivity and reactivity will be conducted annually. Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted quarterly. Heat drying will be used to meet pathogen reduction. Drying of stabilized residuals will be used to meet vector attraction reduction. Sample location will be at the exit of the dryer. Sample type will be grab. "off PAonr�sG l,�k� Norota� Attachment 8 — Laboratory Data The attached laboratory data was used to complete Residuals Source Certification (RSC 06-16). 0 Waypoint ANALYTICAL 2/14/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Revised Lab Report Number: 23-009-0011 Client Project Description: Class A Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/9/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerell�y,,� /)f Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 20 Waypoint, ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Protiram Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/23-009-0011 Page 2 of 20 s (2)Charlotte, NC 28217 Waypo�nt ' 449 Springbrook Rd, Ch Main 704.529.6364 VA LYT I CAL www.waypointanalytical.com Sample Summary Table Report Number: 23-009-0011 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 7470A WP MTN 97038 Class A Sludge O1/09/2023 08:27 01/09/2023 11:31 8270C WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 SW-1311 WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 6010D WP MTN 97038 Class A Sludge O1/09/2023 08:27 01/09/2023 11:31 8151A WP MTN 97038 Class A Sludge O1/09/2023 08:27 01/09/2023 11:31 8081E WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 350.1 AES 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 9045D WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 7471A WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 6010D WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 4500NORGD-2011 WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 SW-DRYWT WP MTN 97039 Class A Solids O1/09/2023 08:47 01/09/2023 11:31 2540G-2011 WP MTN 97079 Class A SAR Solids O1/09/2023 08:47 01/09/2023 11:31 SW-DRYWT WP MTN 97079 Class A SAR Solids O1/09/2023 08:47 01/09/2023 11:31 Saturate Paste WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 20 Waypointo ANALYTICAL Client: Town of Mooresville/RR VWVfP Project: Class A Lab Report Number: 23-009-0011 Date: 2/14/2023 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE This is a revised report and supersedes the original laboratory report dated 2/3123. Calcium, magnesium, and sodium have been added to the metals list (mg/Kg). Report Comments Ammonia was subcontracted to Analytical Environmental Services. Block Digestion and FIA Method 4500NORGD-2011 QC Batch No: L658309 Matrix spike recovery is outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Separatory Funnel Extraction 8081 Method 3510C Sample 97038 (Class A) QC Batch No: 1-659760/1-659760 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 97038 (Class A) QC Batch No: 1-659728/1-659728 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 6010D Sample 97039 (Class A) Analyte: Aluminum QC Batch No: 1-658928/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Calcium QC Batch No: 1-658928/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Copper QC Batch No: 1-658650/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Potassium QC Batch No: 1-658928/1-658311 Page 4 of 20 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Potassium QC Batch No: L659032IL658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Magnesium QC Batch No: 1-658650/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Phosphorus QC Batch No: L658928/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Zinc QC Batch No: 1-658650/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D Sample 97038 (Class A) QC Batch No: L659895/L659728 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. SAR=[Na]/SQRT{([Ca]+[Mg])/2} SAR=[7.59]/SQRT{([14.4]+[11.0])/2} SAR=[7.59]/SQRT{([25.4])/2} SAR=[7.59]/SQRT{12.7} SAR = 2.13 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN —Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (53100-3120) + 0.5 * (3120) + (10) PAN = 16559 Page 5 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 Report Number: 23-009-0011 REPOR T OF A NA L YSIS Lab No : 97038 Sample ID : Class A Matrix: Sludge Sampled: 1/9/2023 8:27 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP Metals Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP Pesticide Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP SVOC Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP VOC ZHE Extraction Leachate 1 01/12/23 12:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L658666 01/16/23 11:20 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 01/16/23 17:41 TJS L658925 TCLP Barium <0.250 mg/L 0.250 1 01/16/23 17:41 TJS L658925 TCLP Cadmium <0.0500 mg/L 0.0500 1 01/16/23 17:41 TJS L658925 TCLP Chromium <0.100 mg/L 0.100 1 01/16/23 17:41 TJS L658925 TCLP Lead <0.100 mg/L 0.100 1 01/16/23 17:41 TJS L658925 TCLP Selenium <0.500 mg/L 0.500 1 01/16/23 17:41 TJS L658925 TCLP Silver <0.0500 mg/L 0.0500 1 01/16/23 17:41 TJS L658925 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit H Beyond holding time Page 6 of 20 Waypoint.0 ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 Report Number : 23-009-0011 REPORT OPANALYSIS Lab No : 97038 Matrix: Sludge Sample ID : Class A Sampled: 1/9/2023 8:27 Analytical Method: 7470A Prep Batch(es): L660377 01/25/23 10:56 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 01/25/23 15:44 JTR L660548 Analytical Method: 8081B Prep Batch(es): L659760 01/20/23 16:20 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 TCLP gamma-BHC <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 TCLP Methoxychlor <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 TCLP Toxaphene <0.03000 mg/L 0.03000 10 01/20/23 23:34 NFP L659894 TCLP Chlordane <0.02000 mg/L 0.02000 10 01/20/23 23:34 NFP L659894 TCLP Heptachlor Epoxide <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 TCLP Heptachlor <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 Surrogate: Decachlorobiphenyl 75.83 Limits: 36-116% 10 01/20/23 23:34 NFP L659894 Surrogate: Tetrachloro-m-xylene 58.50 Limits: 25-123% 10 01/20/23 23:34 NFP L659894 Analytical Method: 8151A Prep Batch(es): L659539 01/19/23 17:20 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 01/20/23 20:26 NFP L659908 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 01/20/23 20:26 NFP L659908 Surrogate: DCAA 58.40 Limits: 20-120% 1 01/20/23 20:26 NFP L659908 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 7 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number: 23-009-0011 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OFANALYSIS Lab No : 97038 Matrix: Sludge Sample ID : Class A Sampled: 1/9/2023 8:27 Analytical Method: 8260D Prep Batch(es): V29271 01/27/23 09:00 Prep Method: 5030E Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 01/27/23 17:14 MSA V29272 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Chloroform <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Methyl Ethyl Ketone (MEK) 0.209 mg/L 0.0500 10 01/27/23 17:14 MSA V29272 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 Surrogate:4-Bromofluorobenzene 105 Limits: 80-124% 10 01/27/23 17:14 MSA V29272 Surrogate: Dibromofluoromethane 102 Limits: 75-129% 10 01/27/23 17:14 MSA V29272 Surrogate: Toluene-d8 110 Limits: 77-123% 10 01/27/23 17:14 MSA V29272 Analytical Method: 8270C Prep Batch(es): L659728 01/20/23 14:30 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 3&4 Methylphenol <0.200 mg/L 0.200 2 01/21/23 02:09 VBW L659895 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Hexachlorobenzene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 8 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number: 23-009-0011 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OFANAL PSIS Lab No : 97038 Sample ID : Class A Analytical Method: 8270C Prep Method: 3510C Test Results Prep Batch(es): Units Matrix: Sludge Sampled: 1/9/2023 8:27 L659728 01/20/23 14:30 MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Hexachloroethane <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Nitrobenzene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Pentachlorophenol <0.200 mg/L 0.200 2 01/21/23 02:09 VBW L659895 TCLP Pyridine <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 2,4,6-Trichlorophenol <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 2,4,6-Tribromophenol 50.1 Limits: 42-102% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 2-Fluorobiphenyl 43.7 Limits: 24-86% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 2-Fluorophenol 16.7 Limits: 13-37% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 4-Terphenyl-d14 57.2 Limits: 30-122% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP Nitrobenzene-d5 43.9 Limits: 25-78% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP Phenol-d6 11.0 Limits: 9-27% 2 01/21/23 02:09 VBW L659895 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit H Beyond holding time Page 9 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number:23-009-0011 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OFANALYBIS Lab No : 97039 Matrix: Solids Sample ID : Class A Sampled: 1/9/2023 8:47 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Fecal Coliform MPN/g <2.5 MPN/g - dry 2.5 1 01/09/23 12:03 SMW 9221E-2011 Moisture 20.9 % 1 01/17/2316:06 FMM SW-DRYWT Ammonia Nitrogen 3120 mg/Kg AR 1 350.1 pH 6.5 H s.u. 1 01/23/23 14:00 SAR 9045D Total Solids 79.1 H % 0.010 1 01/17/23 16:06 FMM 2540G-2011 Total Kjeldahl Nitrogen 53100 mg/Kg - dry 1260 20 01/16/23 11:53 ANH 4500NORGD-2011 Phosphorus 16900 mg/Kg - dry 31.6 5 01/16/23 20:15 TJS 6010D Aluminum 15000 mg/Kg - dry 31.6 5 01/16/23 20:15 TJS 6010D Arsenic 3.59 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 6010D Cadmium 0.582 mg/Kg - dry 0.126 1 01/14/23 03:08 TJS 6010D Calcium 13100 mg/Kg - dry 316 5 01/16/23 20:15 TJS 6010D Copper 176 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 6010D Lead 8.77 mg/Kg - dry 0.379 1 01/14/23 03:08 TJS 6010D Magnesium 2530 mg/Kg - dry 6.32 1 01/14/23 03:08 TJS 6010D Mercury (Total) <0.196 mg/Kg - dry 0.196 1 01/19/23 16:12 JTR 7471A Molybdenum 12.8 mg/Kg - dry 0.316 1 01/14/23 03:08 TJS 6010D Nickel 10.2 mg/Kg - dry 0.316 1 01/14/23 03:08 TIS 6010D Potassium 2970 mg/Kg - dry 63.2 5 01/17/23 14:04 TJS 6010D Selenium 2.81 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 6010D Sodium 795 mg/Kg - dry 31.6 1 01/14/23 03:08 TJS 6010D Zinc 370 mg/Kg - dry 1.58 1 01/14/23 03:08 TJS 6010D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 10 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number:23-009-0011 Lab No : 97079 Sample ID : Class A SAR 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytFcal.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OF ANALYSIS Test Results Units Matrix: Solids Sampled: 1/9/2023 8:47 MQL DF Date / Time By Analytical Analyzed Method Calcium (saturated paste) 14.4 meq/L 0.005 1 01/17/23 14:16 SWL Saturate Paste Magnesium (saturated paste) 11.0 meq/L 0.008 1 01/17/23 14:16 SWL Saturate Paste Sodium (saturated paste) 7.59 meq/L 0.004 1 01/17/23 14:16 SWL Saturate Paste Sodium Absorption Ratio 2.13 1 01/17/23 14:16 SWL Saturate Paste Moisture 3.51 % 1 01/23/2316:46 FMM SW-DRYWT Qualifiers/ DF Dilution Factor Definitions H Beyond holding time Page 11 of 20 0 Access c ANALYTICAL. INC. ANALYTICAL REPORT CLIENT Waypoint Analytical, LLC (Charlotte) 449 Springbrook Road Charlotte NC 28217 ATTENTION Terri W Cole PROJECT ID 23-009-0011 LABORATORY REPORT NUMBER 2301B68 DATE January 17, 2023 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 12 of 20 Page 1 of 6 cu a " $ E Co 4Z of � o � m C G a m C C C w v a K, Q r�i C le a E Ti z c vi m 0 N N w 0 M m c c i�n a Analytical Environmental Services, Inc Date: 17-Jan-23 Client: Waypoint Analytical, LLC (Charlotte) Client Sample ID: 97039 Lab Order 2301 B68 Tag Number: Class A Project Name: 23-009-0011 Collection Date: 1/9/2023 8:47:00 AM Lab ID: 2301B68-OOIA Matrix: Solid ReportingUnits Analyses Result Qual MDL BatchID DF Date Analyzed Analyst Limit Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 3120 104 212 mg/Kg-dry 349327 20 01/17/2023 11:23 TL PERCENT MOISTURE D2216 Percent Moisture 8.35 0 0 wt°/ R506077 1 01/13/2023 00:00 JW Qualifiers: . Value exceeds maximum contaminant level BRL Not Detected at MDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated value above quantitation range S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit < Less than Result value Page 14 of 20 Page 3 of 6 LJ a z 0 z a v L O ❑ N U ❑ V G i Lu V In u ❑ _� (1 � U N s�� Q Z w x dW[A u a E i Q z . C � d 'i V U C D a 0 U E `w d d u O- \ Q Gl ~ a CL E 6 ❑ N C m L o ❑ u v o > c L 3 v d d C Y (D — d o u 0 O. d ❑ � d N 0 cc F o y E o v c m -0 O u a •' • O :)C3CC w > u � a �y 17 C v C � a r. C O N m � E d Y � 3 D- C Al.! c Ou r d V c d 3 M1• E a d D C d d M1. bo C m C •G OO E O CD 0 o c 0E ^„' o d c c 5- •CL Y• C v d H C Q r C a,N L 3 y N a 0 C y > .0 M1• U o m V OV O O it � C)�\6 C `' Y C d d O >• >• C d C c, m a v 0 o d E E N a o ' E u u c— vd v°1 i Y N 0 C a a d D O d d E C. n O o k E W p_ o E C 76 c '�o CL E d G vLi U U H U d V V vi ~ U U � 3 is m v C E E F H v 00 v v 00 00 U U i o V V c v v 0 0 m m CL CL cu N LD d d O 0 U U 0 0 N ,4 Q) aj y a c. sn c d u d E O O E U U U Ln a z O z ❑ ❑ ❑ U V O ❑ ❑ O V p V C C (Uo > a d m d CC,u W L N_ - = 0 a O c o c ❑❑ � u -0U a c o > O vu v s= N N 4 0 Ou Q a a C C E E 0 c Q4GE) Q •: Q SOOCC N d T f6 c M1• d Z L � -0 m a � O d > 0 U 0 r V ^ N r u � M1• c d c u (0 n a v V OUo v R c - Ou c E v s C C t4 C d d D R CL o L o 0 E o o L 3 U N CL_d U V N io CD lu d CL p a ' � m E a E u v v E C a ^' E N N d a a,D c D m v v a v y C C C N N C a H U > u L o c O 7 6 d d a �[ 0,o u y G E > ' a N (co E Yd (uC)> 0 Y° N L E a Q S1 — 0 0 E d D o 3 u u ' 0 a 1 3 3 0 3 3 3 (n e-I u U _N A a '•O 0 M 00 N C �0 u d a d 2 w a CL t E co u a O r O � J N L 00 i 0 z N C L U U N � d 1 CL ! d C 0 1 N i L 3 fC � M1• N H N ( N d a C j E -dD a I y u o p o'o c u aEi I N L d N N .-Err u v n 1 E C ( E C SZ C o� 6 l s d O E C C d a t 0 d N E mY a a N N 0 t d >a 0 f m i L U U 2 U lD n o6 D1 6 e4 N m d' (n l0 (-� 00 (T O �l c l c IH N N N N N" N 14 N N m (D N cm CO a (N 0 LY) li N M ro a a a A A zz zz 0 0 O O O O N N N N N h N h 00 oo hi A A ci A A0. 0 :N •N a x � x en r t6 r Y S 06 0 e rn � rn w w o0 o0 w � z z A a Y S A w .. O N c D➢ c OVA z 'z v v O 00 °O O N U c U o U F U F ;a a Q' W eq GWC M O M V1 U .a o M o Oq bA d d DO m z v, v) z M a O N tn N O N z o m co z a A 00 00 - M M a a O O O d x A o w N c) d A A - v E c Y m a, A Y a- o a on x b en r �ON Cl o .a rn 00 o e c s N g P W vo O c $ W DD '. U o U b N Ou > ¢ c (� W a � v T d R � � � a w � z ca � V1 ¢ c L� m i vo A al c 44 a Ca d F� z a End of Report Page 17 of 20 Page 6 of 6 0 (2) Waypoint ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waVpointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-009-0011 Shipping Method 0 Fed Ex 0 US Postal !. Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IIRT153.3C Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F1 Custody seals intact on shipping container/cooler? 0 Yes 0 No !: Not Present Custody seals intact on sample bottles? 0 Yes 0 No ;1W Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? • Yes 0 No COC properly completed • Yes 0 No Samples in proper containers? • Yes No Sample containers intact? • Yes 0 No Sufficient sample volume for indicated test(s)? • Yes 0 No All samples received within holding time? • Yes 0 No Cooler temperature in compliance? i Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ■ Yes 0 No Water - Sample containers properly preserved %: Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No .0 N/A Trip Blanks received with VOAs 0 Yes 0 No /, N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: Signature: Angelo Norvell Date & Time: 01/09/2023 14:18:50 Page 18 of 20 CjLLZL Oi Z o 8 L y? 21 N L m' c - ILLGC,� Ti a -+IL mi n '�� 01 L m` I yLLID D z " nc D L 4 0! A1F n miv N 101. eLLOhi ;I nZ1. O. l L,,. r � 0>v y L L r >i Zz 0 Oi N I L� Z. r =LLO1 L �n»mom 0 0 `� A 0 3 N - Of -n YI eo 03 K A a a U o x zz N Z -1 CO 17 10 A 3 c c 3 moi' y � mT to " m a r ;mpti a a m m 0 z';m L L 0 r iDmpo 04_0 m m D n m p n Fazi�c a L mm s M(m{ ' O o p�� Rm -am O .t >s ami a o L 0 +op Ljat 2 m 1 4W A FA N 4,0 D,mm M +� N O � A •!1 s ■ , ra p' r 6 a 7 Q 2 c. Q A A ei 10 o Z i-# m 3 Z .p ii 3 O' X m 9 v rn r I� T o m ��f O 4 2 O r � � n 0 0 0 0 4 O.03 p) a v,a z m 3 mow' , o� � m ° D o Qr- iC m PC) S -- N ON p` E r v w C a o m a01a p = m Me p� � 1 to -1 � w r A� p rn» m C I Page 19 of 20 Cj L L Z 4 `` Qi z a D L Mm f11' n c M - m �L L C + Z CA 2 m Si v � L y L L Q Di n� ZI LZp m Ow An" � � rn o u 0 6 L L 0 n �' o Q L 0 ps m K v r m- L tn; A Q m n u L �I >'. L L Mi° z 0: 0i nl' v, L i O° n �LLe� I o� Yam; m L Mp mi NCf y A uni LL� D •, z z w 0 D M Lr �1 �r m A =LLO m [Z9 m al m L 7a �m 0 m iLT � 7c -M m m x ;m un Cam n m G - d� gr(84J r - D �� 3 r-rv°'' o a {yA� oxmm a mo° O ea z mIc m 4 Q �+� }� -Aim w 0 1 x .�:„'�,��■ tl+j a A — vA I ',¢ z C O r- CIO IOU I yA_ m g m to m J S C y A Om a v o a � d o¢ 01 cpO �'°1 T A� Z AT�tic v 1 Q W m Z 1 0 01cr Lm q m �tpC W 10 v /I/q� mm na o o mL/ a m 4 a _ zA�C �n0• 61 r$ <9 M Ln ` m a � 0 m 3 p0 m OCA��°i `� as O 3 �•1 S N C~Om .0 A 4 o p P N �I Z raiZM'i Ord jI tn0D O m A 1m y -_1 M � IN Z ,_' CA � 0 n En J 1° m � > ! rA IQ a a a A\ i m � � . Z a a z fv �I 61 p o Page 20 of 20 Waypoint ANALYTICAL 1 /24/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 23-009-0005 Client Project Description: Class A TCLP Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waVpointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/9/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 6fflA-6 LO Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WI? CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID E�xiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/23-009-0005 Page 2 of 8 Waypointo ANALYTICAL Report Number: 23-009-0005 Client Project Description: Class A TCLP 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 97027 Class A Sludge 01/09/2023 08:47 O1/09/2023 11:31 SW-1311 WP MTN 97027 Class A Sludge 01/09/2023 08:47 01/09/2023 11:31 8270C WP MTN 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 SW-7.3.3 WP MTN 97028 Class A Solids O1/09/2023 08:47 01/09/2023 11:31 2540G-2011 WP MTN 97028 Class A Solids O1/09/2023 08:47 01/09/2023 11:31 SW-7.3.4 WP MTN 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 9045D WP MTN 97028 Class A Solids O1/09/2023 08:47 01/09/2023 11:31 ASTM D93-80 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 8 0 Waypoint ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A TCLP Lab Report Number: 23-009-0005 Date: 1 /23/2023 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalyfical.com CASE NARRATIVE Flashpoint Method ASTM D93-80 QC Batch No: L659394 The sample analysis was performed using a modified version of the reference method. Due to the sample matrix, the continual stirring required by the method had to be omitted. Separatory Funnel Extraction 8270 Method 3510C Sample 97027 (Class A) QC Batch No: 1-659728/1-659728 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D Sample 97027 (Class A) QC Batch No: 1-659895/1-659728 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Page 4 of 8 Wayp i ,, 01205 ANALYTICAL Town of Mooresville/RR WWTp Whitney Munroe 369 Joh Project nson Dairy Rd. MOOrese,ille , NC 28115 Information : Report Number:23_00g_0005 Lab No : 97027 Sample ID : Class A Test TCLP SVOC Extraction Analytical Method: 8270C Prep Method; 3510C Test TCLP 2-Methylphenol TCLP 3&4 Methylphenol TCLP 2,4-DinitrOtOluene TCLP Hexachlorobenzene TCLP Hexachlorobutadiene TCLP Hexachloroethane TCLP Nitrobenzene TCLP Pentachlorophenol TCLP Pyridine TCLP 2 4 S_Trichlorophenol TCLP 2,4,6-Trichlorophenol Surrogate: TCLP 2,4,6-Tribromophenol Surrogate: TCLP 2-Fluorobi Surrogate: TCLP 2-Flphenyl uorophenol Surrogate: TCLP 4-Terphenyl-d14 Surrogate: TCLP Nitrobenzene-d5 Surrogate: TCLP Phen1l-d6 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 �^+Ww.waYPointanalyt1Cal.Com Class A TCLP 10?EPpR7-0FANA1 ySIS Results-y----------� Units MQL Leachate Prep Batch(es): Results Units <0.100 rng/L <0.200 m9/L <0.100 m9/L <0.100 m9/L <0.100 m9/L <0.100 m9/L <0.100 m9/L <0.200 m9/L <0.100 m9/L <0.100 m9/L <0.100 m9/L Qualifiers/ Definitions DF Dilution F actor MQL Method Quantitation Limit 44.2 46.3 15.2 47.2 47.8 9.60 Report Date : 01124/2023 Received : O11O912023 J1W Terri W Cole Laboratory ProJect Manager Matrix: Sludge Sampled: 1/9/2023 8:47 DF Date / Time Analyzed ey Analytical Method 1 01/12/23 14:00 PHE L65972g 0112012314:30 SW-1311 MQL DF Date / Time By ' nalYzed Analytical Batch 0.100 0.200 2 01/21/23 01:03 VBW 0.100 2 01/21/23 01:03 VBW L659895 0.100 L659895 2 01/21/23 01:03 VBW 0.100 2 01/21/23 01:03 VBW L659895 0.100 2 01/21/23 01:03 VBW L659895 0.1002 01/21/23 01;03 VBW L659895 0.200 2 01/21/23 01:03 VBW L659895 0.100 2 01/21/23 01:03 VBW L659895 0.1002 01/21/23 01:03 VBW L659895 0.100 2 01/21/23 01:03 VBW L659895 Limits: 42-102% 2 01/21/23 01:03 VBW L659895 L659895 Limits: 24-86% 2 01/21/23 p1:03 VBW Limits: 13-37% 2 01/21/23 01:03 VBW L6598g5 Limits; 30-122% 2 01/21/23 01:03 VBW L659895 Limits; 25-78% 2 01/21/23 01:03 VBW L659895 Limits: 9-27010 2 01/21/23 01:03 VBW L659895 2 Ol121/23 01.03 VBW L6598g5 H L659895 Beyond holding time Page 5 of 8 ont. 01205 Wa Y PA Town of Mooresville/RR WWTp Whitney Munroe Project 369 Johnson Dairy Rd. Mooreseville , NC 28115 Information : Report Number:23-Oog_0005 Lab No : 97028 Sample ID : Class A Test Sulfide (Reactivity) Moisture Cyanide, Reactive Ignitability PH Total Solids 449 Springbrook Rd. Charlotte, NC 28217 Main 71)4.529.6364 www. wa ypo i n to na lyti CaI, co m Class A TCLP REPORT pFANALYSIS Report Date : 01/24/2023 Received : 01/09/2023 jo wo�' Terri W Cole Laboratory Project Manager Matrix: Solids Results y -�---- Sampled: 1/9/2023 8:47 =-_- Units MQL DF Date / Time g -- - - _ Analyzed Analytical ------- - _ Method <25.o m9/Kg l-4 3.68 % 25.0 1 0112312310:30 <0.125 m9/Kg F MM SW-7.3.4 1 0111212315:03 >96 0.125 degrees C AMB SW-pRyWT 1 01/23/23 10:30 6.4li S.U. FMM SW-7.3.3 1 01/18/23 08:40 45.9 W % OR ASTM D93-8o 1 01/23/23 14:00 O.O1D SAR 9045D 1 01/17/2316:06 FMM 254OG-2011 Qualifiers/ DF Definitions Dilution Factor MQL Method Quantitation Limit H � Beyond holding time Page 6 of 8 WaYp,ogintYTICAL 449 Sprin�tyrook Rd, Charlotte Ivc 28217 Main 704.529 6364 Customer Shipment wuv�y waVpointana! Number: 01205 ent Receipt �'t'CaLco Customer pt FOm Namrm e: Town of M oresville/RR WWTp Report Number: o 23-009-0005 0 Fed Ex Shipping Method Client UPS 0 US Postal G Lab Shi 0 Courier Aping container/cooler uncom Number of coolepromised? rs/boxes received T-�.yes. Custody seals intact on Custod1 shipping container/cooler? 1 y seals intact on sample bottles? Yes Chain of Custody (COC Present? 0 Yes COC agrees with sample label(s)? *) Yes COC properly completed A Yes Samples in proper containers. Yes Sample containers intact? 1 Yes Sufficient sample volume for Indic _ �.' Yes within All samples received ated test(s)? holding(*I Yes Cooler temperature time? in com Yes Cooler/S pliance? SamplesamPles arrived at the laboratory Yes were considered acceptable °n ice. Process had begun. Yes as cooling Water - Sample containers Water - VOA properly present-4 0 Other: Thermometer ID: IRT15 1.2C 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No Not Present Not Present vials free of heads r Yes Trip Blanks received pace � No With VOAs 0 Yes 0 No 0 N/A Soil VOA method 0 Yes N/A 5035 — Compliance � No High concentration container criteria N/A met 0 Yes I^ High concentration (48 hr) 0 No pre-wei Low concentration EnCore i \ N/A SpeC1al precautions ghed (methanol -14 d or instructions included? ) Low conc samplers (48 hr) pre -weighed No vials (Sod Bis -14 d Comments: -- _ _ _ � 0 Yes ) ~ f Signature: Belo Now - Date &Time:1/09/2023 12:25:15�1 f ~� - Page 7 of 8 — A a c Page 8 of 8 P ® a C ' n n O �� a as moo L WAWS pmAmcaam� i m a A m `' m C O CM, m m r + OD m > m to m sa�o:A ? ; 'fn h �m r GO 6n �Arxi n a L yfi1�Y Q . CO y 9 - L L G�b:i m n Y m a.s F Q �� Oe �O A m m C ] VXe n