WQ0034688_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0034688
Applicant/Permittee Neuse Regional Water and Sewer Authority
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0034688
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name* Neuse Regional WASA Class A Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for Neuse Regional Water and Sewer Authority, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
NeUse NC 2022 Annual Report FINAL.pdf 5.63MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tt,
Submission Date 2/28/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 28, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0034688
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of Neuse
Regional Water and Sewer Authority, NC.
If you have any questions or need additional information, please do not hesitate to contact
Charlie Colie at [phone] or Matthew Carter at 336-705-9886.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Charlie Colie, Neuse Regional Water and Sewer Authority
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

NEUSE REGIONAL WATER AND SEWER
AUTHORITY
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0034688
2022 ANNUAL REPORT

Neuse Regional Water and Sewer Authority, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

SYNAGRO
February 23, 2023
REFERENCE: EXPLANATION OF NON -COMPLIANT ANNUAL REPORT OF
PERMIT # WQ0034688 NEUSE REGHIONAL WASA
On behalf of the Neuse Regional WASA, Synagro is submitting an explanation of why the
2022 annual report is marked non -compliant.
In this annual report you will find that 341.91 Dry Tons were land applied, but there are
not enough sampling results for dry tonnage applied. Since we applied more than 319 dry
tons, there should have been 4 sample results for the year, but only a single sample was taken.
That sample was taken during the same quarter the material was land applied. Historically
depending on the percent solids, the dry tonnage will vary drastically. In 2022 when we
proj ected the amount material, we were going to land apply we proj ected under the 319 mark.
After hauling we also double check the amount, we haul to know the dry tonnage amount, but
in 2022 we double checked the amount hauled before all the tickets we inputted into our
system which led to this oversight. Going forward, to prevent this issue again, we are going to
take quarterly samples. Over the past few years, the dry tonnage amount has been increasing
so we are now going to do quarterly sampling.
If you have any further questions, please contact me at (704)-650-4341 or
abrigmang synagro. com
Sincerely,
Adam Brigman
Technical Services Manager
Synagro
284 Boger Road, Mocksville, NC 27028 • Phone: [phone] • Fax: [phone]

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00034688 County Lenoir Year 2022
Facility Larne (as shown on permit) Neuse Regional Water Treatment Plant NPDES No. NC0088111
Land Application Operator, Synagro _ Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. IFNO, skip PartA, and Part B and proceed to PartC. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary
Total number of application Fields in the permit: NIA
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 349,91
Total number of acres utilized for land application during the year: 115.50
Part B --- Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityYES _—X_ _,NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
L Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in I SA NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T ,1 11 I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10, No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
It. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13, All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." el _, i/11
Harold Herring, Executive Director
Permittee Name and Title (type or print)
Signattre of Preparer* Date
(if different from Permittee)
7;
Signature of Permittee v 15ate I
02/01 /2023
S of La Applier Date
(if different om Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503,9(r) and ISA NCAC 02T . 1102 (26) DE1NR FORM ACIt (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
NEUSE REGIONAL WASA, NC
NEUSE REGIONAL WASA, NC WTP LIQUID
MONTH/YEAR
October 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/14/2023 4:29:24 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
2,507,400.00
G
341.91
D
310.11
2,507,400.00
G
341.91
D
310.11

SECTION 2

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: NRWASA
Lot Number:XG27053
Date Completed:08/19/2022
NIM�� Mr�
08/19/2022 1:32 PM
Approved and released by:
Project Manager II: Lucas Odom
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XG27053
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Non -Metals
The method blank (MB) and continuing calibration blanks (CCB's) for prep batch 49397 contained the
analyte total phosphate greater than the method acceptance criteria. The MB and CCB's recovered less
than the limit of quantitation (LOQ) but not less than the minimum detection limit (MDL), as required by
the method. The affected samples contained detections for the analyte at concentrations greater than
1 OX the value found in the MB and CCB's; therefore sample results are not impacted.
Inorganic Metals
Due to the matrix and low percent solids, the following samples have an initial volume is that 3x greater
than standard procedure: XG27053-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:XG27053-001
Description: NRWASA Matrix: Solid
Date Sampled:07/26/2022 1015 % Solids: 3.27 08/08/2022 2247
Date Received:07/27/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
2
(% Solids) SM 2540G
1 08/08/2022 2247 MJS2
50448
1 350.1
(Ammonia - N ) 350.1
1 08/03/2022 1254 CMM
49861
1
(Nitrate - N ) 353.2
1 07/29/2022 1357 KKP
49563
1
(Nitrite - N ) 353.2
1 07/29/2022 1357 KKP
49565
1
(Phosphorus) 365.1
2 07/29/2022 1128 DMA
07/28/2022 1345 49397
1
(Soil pH meas) 9045D
1 07/28/2022 1910 KKP
49586
1 351.4
(TKN) 351.2
1 07/28/2022 1835 DMA
07/28/2022 1152
49368
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.27
%
2
Ammonia - N (gas diffusion)
350.1
710
31
16
mg/kg
1
Nitrate - N (soluble)
353.2
62
6.1
0.82
mg/kg
1
Nitrite - N (soluble)
353.2
2.3 J
6.1
0.80
mg/kg
1
Phosphorus
7723-14-0 365.1
3000
310
61
mg/kg
1
Soil pH measured in water @
24.2 ° C
9045D
6.6
su
1
TKN
351.2
11000
1500
770
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/28/2022 1624 MRW2
07/28/2022 1449 49353
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
0.080
0.019
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 08/01/2022 1445 JMH
08/01/2022 0046 49486
2 3050B
601OD
1 08/02/2022 0240 JMH
08/01/2022 0046 49486
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
120000
160
61
mg/kg
1
Arsenic
7440-38-2 6010D
10
6.1
2.0
mg/kg
1
Cadmium
7440-43-9 6010D
ND
2.0
0.51
mg/kg
1
Calcium
7440-70-2 6010D
2000
2000
260
mg/kg
1
Chromium
7440-47-3 6010D
21
4.1
1.0
mg/kg
1
Copper
7440-50-8 6010D
150
4.1
1.8
mg/kg
1
Iron
7439-89-6 6010D
32000
41
19
mg/kg
1
Lead
7439-92-1 6010D
17
4.1
1.8
mg/kg
1
Magnesium
7439-95-4 6010D
1300 J
2000
260
mg/kg
1
Manganese
7439-96-5 6010D
1900
6.1
2.4
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
16
4.1
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:XG27053-001
Description: NRWASA Matrix: Solid
Date Sampled:07/26/2022 1015 % Solids: 3.27 08/08/2022 2247
Date Received:07/27/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 08/01/2022 1445 JMH
08/01/2022 0046 49486
2 3050B
6010D 1 08/02/2022 0240 JMH
08/01/2022 0046 49486
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
13 J 16
4.3
mg/kg
1
Potassium
7440-09-7 6010D
1300 J 2000
260
mg/kg
1
Selenium
7782-49-2 6010D
7.4 J 8.2
3.3
mg/kg
1
Sodium
7440-23-5 6010D
970 J 2000
260
mg/kg
2
Zinc
7440-66-6 6010D
77 20
5.1
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Page 6 of 7

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
August 05, 2022
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: NRWASA
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22071543
Summit Environmental Technologies, Inc. received 1 sample(s) on 7/27/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 34

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22071543
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 8/5/2022
CLIENT: Synagro
Project: NRWASA
WorkOrder Narrative:
22071543: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Original
Page 2 of 34

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 22071543
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 8/5/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 34

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO ijULES. JNG, Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: NRWASA
Lab SampleID Client Sample ID
22071543-001 NRWASA
Tag No Date Collected
7/26/2022 10:00:00 AM
Workorder
Sample Summary
WO#: 22071543
05 Aug-22
Date Received Matrix
7/27/2022 10:20:00 AM Sludge
Page 4 of 34

A
Or
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Ni p V O O O O O O O p p O O
p ul C C O C C C O p p O O
M M 01 \O �O 01 00 V1 M M p p O N
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N N N N N N N N N N N N N N
O N O O O O O O O O p p O O
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0o N o0 0o O M O O O, O, O, G,
r N r r r r r r r r r r
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SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22071543
Date Reported: 8/5/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/26/2022 10:00:00 AM
Lab ID: 22071543-OOIA
Project: NRWASA
Client Sample ID NRWASA
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: ICA
1 8/3/2022 1:38:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
SW301OA Analyst: MSK
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
7/28/2022 4:05:00 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
7/28/2022 4:05:00 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
7/28/2022 4:05:00 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
7/28/2022 4:05:00 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
7/28/2022 4:05:00 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
7/28/2022 4:05:00 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
7/28/2022 4:05:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: CSS
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2
7/29/2022 5:10:00 PM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
7/29/2022 5:10:00 PM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2
7/29/2022 5:10:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
7/29/2022 5:10:00 PM
Cresols, Total
ND
10.0
mg/L
2
7/29/2022 5:10:00 PM
Hexachloro-1,3-butadiene
ND
0.0400
mg/L
2
7/29/2022 5:10:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
7/29/2022 5:10:00 PM
Hexachloroethane
ND
0.200
mg/L
2
7/29/2022 5:10:00 PM
Nitrobenzene
ND
0.200
mg/L
2
7/29/2022 5:10:00 PM
Pentachlorophenol
ND
0.500
mg/L
2
7/29/2022 5:10:00 PM
Pyridine
ND
0.500
mg/L
2
7/29/2022 5:10:00 PM
Surr: 2-Fluorophenol
101
10 - 157
m %Rec
2
7/29/2022 5:10:00 PM
Surr: Phenol-d6
99.4
10 - 169
m %Rec
2
7/29/2022 5:10:00 PM
Surr: Nitrobenzene-d5
92.5
32.1 - 130
%Rec
2
7/29/2022 5:10:00 PM
Surr: 2,4,6-Tribromophenol
110
45.4 - 166
%Rec
2
7/29/2022 5:10:00 PM
Surr: 2-Fluorobiphenyl
89.0
35.7 - 130
%Rec
2
7/29/2022 5:10:00 PM
Surr: p-Terphenyl-d14
88.3
70 - 145
%Rec
2
7/29/2022 5:10:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration used to
determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 6 of 34

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22071543
Date Reported: 8/5/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/26/2022 10:00:00 AM
Lab ID: 22071543-OOIA
Project: NRWASA
Client Sample ID NRWASA
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
63.2
Surr: TCMX
60.6
Surr: DCB
62.4
Surr: DCB
55.0
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 105
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
106
Surr: Di brom ofl uorom ethane
102
SW8081 SW351OC Analyst: PGP
0.0250
mg/L
10
7/29/2022 9:30:00 AM
0.0500
mg/L
10
7/29/2022 9:30:00 AM
0.0100
d
mg/L
20
7/30/2022 9:43:00 PM
0.00500
d
mg/L
10
7/29/2022 9:30:00 AM
0.00500
d
mg/L
10
7/29/2022 9:30:00 AM
0.00500
d
mg/L
10
7/29/2022 9:30:00 AM
0.00500
d
mg/L
10
7/29/2022 9:30:00 AM
10 - 119
%Rec
10
7/29/2022 9:30:00 AM
10 - 119
%Rec
20
7/30/2022 9:43:00 PM
10 - 119
%Rec
10
7/29/2022 9:30:00 AM
10 - 119
m
%Rec
20
7/30/2022 9:43:00 PM
S W 8321
Analyst: PGP
0.500
mg/L
50
7/30/2022 6:29:00
PM
0.500
mg/L
50
7/30/2022 6:29:00
PM
70 - 130
%Rec
50
7/30/2022 6:29:00
PM
SW8260
SW1311M Analyst: EMB
0.250
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
5.00
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
2.50
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
0.250
mg/L
50
7/29/2022 2:42:00
PM
0.100
mg/L
50
7/29/2022 2:42:00
PM
70 - 130
%Rec
50
7/29/2022 2:42:00
PM
70 - 130
%Rec
50
7/29/2022 2:42:00
PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 34

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone] WO#: 22071543
Website: http://www.settek.com Date Reported: 8/5/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/26/2022 10:00:00 AM
Lab ID: 22071543-OOIA
Project: NRWASA
Client Sample ID NRWASA
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: EMB
TCLP VOLATILES ANALYSIS
Surr: Toluene-d8
100
70 - 130
%Rec
50
7/29/2022 2:42:00 PM
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.490
mg/Kg
1
7/28/2022 1:06:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: SMZ
Ignitability Non -Flammable
mm/sec
1
7/28/2022 1:43:12 PM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: SMZ
Percent Solids
3.22
%
1
7/28/2022 11:43:00 AM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH
6.7
s.u.@20.5C
1
8/1/2022 3:49:54 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
7/28/2022 1:06:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
fr
3310 Win St.
SUMMIEF
Analv n tes Report
ENOROMMEWAL IrECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
22071543
Wehsite: http://www.settek.com
05 Aug-22
Client: Synagro
State: NW
Project: NRWASA
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22071543-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Key
Key
Key
NC WW SCM A Accredited
NC WW SCM N Not Accredited
NC WW SCM U
Unavailabl
Original #1
Page 9 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
ENVIROMMEWAL IrECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
22071543
Wehsite: http://www.settek.com
05 Aug-22
Client: Synagro
State: NW
Project: NRWASA
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22071543-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl
Original #1
Page 10 of 34

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Page 33 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 22071543 RcptNo: 1
Logged by: Tegan A. Richards 7/27/2022 10:20:00 AM 41 n qE;-
Completed By: Tegan A. Richards 7/27/2022 12:24:32 PM 4n qE;-
Reviewed By: Jennifer Woolf 7/27/2022 3:51:29 PM )V'of'�
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition?
Yes
d❑
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present V
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
11.0
Goodl
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neese Regional Water and Sewer Authority WQ Permit Number: WQ0034688
WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NC0088111
Monitoring Period: From 01/01/2022 To 12/31/2022
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed;
Class A:
Alt. I/A (time/temp) Alt. 21B (A1k Treatment) Alt. 3/C (Prior Testing)
lt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens";
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitorin data:
parametel pie
PERMIT DOES NOT REQUIRE e
Fecal
Coliform MONITORING FOR PATHOGEN
& VECTOR ATTRACTION
REDUCTION
bacteria (i€fir
lieu of fecal
conform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Analytical
Technique
0 tion/Alt. I
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt, 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying --- Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/1 SA NCAC 02T. 1106 and the vector attraction
X reduction requirement in 40 CFR 503,33/15A i`ICAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/1 SA NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503,33115A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Haroid Herring, LLxecutive DirectosNRWASA
Preparcr Na and T' pe ring Land Applier Name and Title (if applicable) (type or print)
S€21 of Preparcr* ate l Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

SECTION 6

Agricultural Lime Application Log
Year 2022
Project Neuse Regional AWASA
Fields
(state -county -site -field)
Soil Lime Requirements
PH (from soil analysis)
Tons/Acre Date
Ip ied Ip ied
LN-X5-3
5.6
0.4T
N/A
LN-X6-1
5.8
0.4T
N/A
LN-X6-2
5.8
0.3T
N/A
LN-X6-3
5.8
0.3T
N/A
LN-X6-4
1 5.81
103T
I N/A
N/A
N/A
N/A- Did not apply in 2022
*Lime will be applied when field conditions/cropping pattern permits

SECTION 7

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