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HomeMy WebLinkAboutWQ0000461_2022 Residual Annual Report_20230228 (4)Initial Review Reviewer Nathaniel.Thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR) * W00000461 Applicant/Permittee Town of La Grange Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Washington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Lysa Finnerty Email Address* LFinnerty@synagro.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 4105376150 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0010488 Has Current Existing permit number Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220 Facility Name* Town of La Grange Class B Residuals Program Please provide comments/notes on your current submittal below. 2022 Annual Report for Town of LaGrange, NC At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) LaGrange NC 2022 Annual Report FINAL.pdf 4.73MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Alva �Cit'wt%tt, Submission Date 2/28/2023 435 Williams Court, Suite 100 Baltimore, MD 21220 www.synagro.com FEBRUARY 28, 2023 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2022 Annual Report for Permit No. WQ0010488 Dear NCDEQ: SYNAGRO Synagro is submitting one electronic copy of the above referenced report on behalf of the Town of LaGrange, NC. If you have any questions or comments, please contact John Craft at (252) 566-3186 or Matthew Carter at (336) 705-9886. Sincerely, 01171 Y-- Derrick Shivar Environmental Compliance Manager Enclosures cc: John Craft, Town of LaGrange Matthew Carter, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD TOWN OF LAGRANGE, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0010488 2022 ANNUAL REPORT Town of LaGrange, NC Residuals Land Application Program 2022 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms and Residuals Analyses 3. Annual Land Application Field Summary Form 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analysis SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: WO0010488 County Lenoir Year 2022 Facility Name (as shown on permit) LaGrange WWTP NPDCS No. NCO021644 Land Application OperatorSynagro Phone# 336 99) 9 8-7150 Land application of residuals as allowed by the above permit occurred during the past calendaryear? X YES NO. IfNO, skip Part A, and Part Bind proceed to fart C. Also, irresiduals were generated but not land applied, please attach an explanation oil how the residuals were handled. Part A — Residuals Application Suinmarv: Total numberol'applieation fields in the permit: 3 Total number or fields utilized for land application during the year: Total amount of dry Ions applied during the year for all application sites: 8.55 Total nu€nberol acres utilized for land application during theyear: 13.62 Part i3 — Annual Compliance Statement: Facility was compliant during calendar year 2022 with all conditions orthe land application permit (including but not limited to items 1-13 below) issued by the Division orWater Quality X YES NO, If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pId was adjusted us specified in the permit and lime was applied (irneeded) to achieve a soil pH of at least 6.0 or the limit specified in the permit, 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies or laboratory results are attached. 4. Annual TCLP analysis (ifrequired) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies orcertified laboratory results are attached. G. The facility did not exceed any orthe Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .l 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T , I I I I were ewnplied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case ora deviation, prior authorization was received fxorn tile Division or Water Quality. 10. No contravention ol'Cround Water Quality Standards occurred at a monitoring well or explanations orviolations are attached to include appropriate actions and remediations. i 1. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No run€ofTof residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C--Certif€cation: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belier, true, accurate, and complete. 1 a€n aware that there are significant penalties f'or submitting False in ion, including the poss' rty of fines and imprisonment far knowing violations." rJ John Craft, Town Manager 4 !� 2 17, p� Permittee Name and Title (type or print) ignature of.Lemifitei Date Signature of Preparcr* Date g.Wftfe c f La€VApplicr Date (if different from Per€nittce) ordifrereff frorn Permittee and Preparer) *Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 02T .1102 (26) DENR rOR€M ACF (121200G) OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA ALL COUNTIES - ALL SITES DATE RANGE: 1/1/2022 - 12/31/2022 LA GRANGE, NC LA GRANGE, NC AEROBICALLY DIGESTED LIQUID MONTH/YEAR November 2022 TOTAL Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards Report Date: 2/14/2023 4:31:13 PM AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS 117,800.00 G 8.55 D 7.75 117,800.00 G 8.55 D 7.75 SECTION 2 7 } i 0 k \ 2 § @ k 2 � § z OD a u C } j k k \ a 5 _ z § k / E u z K ] / ) ƒ) § 0. ] o . a a z \ a k � c_ _ L)E � f E q)% R»"®q k\§ f k 9 v m m n $ p m / 2 E r)\) z z z z 0 / ] « E \ - z E k E 0 ] \® E [ ƒ + ` e R 2 2 4 E e 7 z E $) 3 G)) k z$ q /ƒ 2 8 m a Z E to a ti a w M Q LOL w i 0 0 0 0 0 0 o m 0 o er) In rn m rr Lq O W .see ;G 3 v 3 '� m ai -o z � (L d L) a a° 0) a vi up <O N O I G 0 0 iL EY ix d w a z W Q 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Chris Wynne Project Name: LaGrange WW-FP Lot Number:XH17019 Date Completed:09/06/2022 NIM�� Mr� 09/07/2022 9:38 AM Approved and released by: Project Manager II: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: XH17019 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Where sampling is conducted by the client, results relate to the accuracy of the information provided, and as the samples are received. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2- dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal Coliform Colilert-18. Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight unless flagged with a "W" qualifier. If you have any questions regarding this report, please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Inorganic Metals Due to the matrix and low percent solids, the initial amount of sample -001 is 3x greater than the standard procedure. The LOQ has been adjusted accordingly. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 7 Client:Synagro Laboratory ID:XH17019-001 Description: La Grange WWTP Matrix: Solid Date Sampled:08/16/2022 1015 % Solids: 1.74 08/20/2022 1458 Date Received:08/17/2022 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 08/20/2022 1458 CVR 51761 1 350.1 (Ammonia - N ) 350.1 1 08/23/2022 1349 CMM 51884 1 (Nitrate - N ) 353.2 10 08/25/2022 1752 KKP 52152 1 (Nitrite - N ) 353.2 10 08/25/2022 1752 KKP 52154 1 (Phosphorus) 365.1 5 08/22/2022 1949 DMA 08/22/2022 1442 51852 2 (Soil pH meas) 9045D 1 08/29/2022 1941 KKP 52578 1 351.4 (TKN) 351.2 1 08/25/2022 1725 DMA 08/25/2022 1159 52188 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 1.74 % 1 Ammonia - N (gas diffusion) 350.1 ND 58 30 mg/kg 1 Nitrate - N (soluble) 353.2 5900 120 15 mg/kg 1 Nitrite - N (soluble) 353.2 ND 120 15 mg/kg 1 Phosphorus 7723-14-0 365.1 8200 1400 290 mg/kg 1 Soil pH measured in water @ 20.9 ° C 9045D 4.0 su 2 TKN 351.2 28000 2900 1400 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471 B 7471 B 1 08/23/2022 1718 MRW2 08/23/2022 1506 51513 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 4.2 1.0 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 08/25/2022 0723 JAB2 08/24/2022 0101 51820 2 3050B 601OD 1 09/02/2022 1330 JMH 08/24/2022 0101 51820 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 41000 S 370 140 mg/kg 1 Arsenic 7440-38-2 6010D 7.1 J 14 4.6 mg/kg 1 Cadmium 7440-43-9 6010D 1.2 J 4.6 1.2 mg/kg 1 Calcium 7440-70-2 6010D 10000 4600 580 mg/kg 1 Chromium 7440-47-3 6010D 27 9.2 2.3 mg/kg 1 Copper 7440-50-8 6010D 430 9.2 4.2 mg/kg 1 Iron 7439-89-6 6010D 29000 92 42 mg/kg 2 Lead 7439-92-1 6010D 57 9.2 4.2 mg/kg 1 Magnesium 7439-95-4 6010D 2500 J 4600 580 mg/kg 1 Manganese 7439-96-5 6010D 150 14 5.5 mg/kg 1 Molybdenum 7439-98-7 6010D ND 37 9.2 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Laboratory ID:XH17019-001 Description: La Grange WWTP Matrix: Solid Date Sampled:08/16/2022 1015 % Solids: 1.74 08/20/2022 1458 Date Received:08/17/2022 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 08/25/2022 0723 JAB2 08/24/2022 0101 51820 2 3050B 6010D 1 09/02/2022 1330 JMH 08/24/2022 0101 51820 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Nickel 7440-02-0 6010D 11 J 37 9.7 mg/kg 1 Potassium 7440-09-7 6010D 3500 J 4600 580 mg/kg 1 Selenium 7782-49-2 6010D ND 18 7.5 mg/kg 1 Sodium 7440-23-5 6010D 1900 J 4600 580 mg/kg 1 Zinc 7440-66-6 6010D 560 46 12 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES, LLC Y O 4h TT y SS _ S - U tlp �ca ae E v ED J g 6 C a $Ye$Y� fiJ:! IIQ � [❑ JEOu IrJr-.d ❑ 04 C E ¢ u a I ¢ iA i sJ aj � ill � � a apl:��q�hH g .e a WMdead d-M— one ix _ jQ7-TT I i G -2 w F ] !CL ry w -j _ c ,L ` ° -2 ep 4 E 9p 49. -A qfto-o �6 ua r A 40 rk U a w S t ' L ll 'Fad ° al 1 $ 6 LL ID Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 PACE ANALYTICAL SERVICES, LLC DOCritle: EW-ARM-WCOL-0285 ►r02_5axnples Re�alipt Checklist 15RC) ENOM! Cates: 8/2/2022 Sample Receipt Cheel,;list (SRC' C']i�atr byiva��a _ Co�31ct'Ll ctcsib}'rtiai�= ?C�.� r 45,'1?,�42.s ��}i#- ��l?'ji9 icar�: oaf a ccxi t: J}�cc lzcpt UP9 FedU Oflie r• Yew No "_ Were i.ustady�cals -esmit oil t1lC Cooler° — Ycs N o V , N.1 2. Ifcu: tod� � seals were mellL u-cre t11ev ilrtect alrrl soaix oleeu? 11 Srxip ID: xn C111oAUC Strilr ID: xn _ �'e�red Ly;xA, On,-,iml Irluper, ran 1lpoas MCC / Duiwed (Con-ecttA) 1-,u CTIIM-c' upo11 receipt % olid S11alx-CUp 1D. 12-1253 1,2 11,2 XA r _A oC NA r'cA oC MeL j A oC - htcthad-OTclnpeltur 81.gilk ea i ng t 13a#ties IR C�tui II]: $ Il t7n'ozl ccnou Facmr- C'( IM&od of cc; ]Ault: N�'et Icr 1—h r PRCU I}1-V It ti MNO.. El NA -3, Were all coollen rcrrive;: u srr t}claw (,.,Y'C:? If 1)0, vria s Project YfutngT. lEauficrl'} TV was Nori&d b - Idione ' :.11ni face-to-facp. (eilclr one). cs l�Ta I, Is Zhu conuwrcial c�lx�licr's paclpit<g slip at,rL:tlyd io 16 fonr.? 1 Yes Ufa �. WvN proper cltsxadyproccciures {re mquiSh-' ` tivcd) fsxllutved9 +f des No 6 -'elc 54m le IDS Tis,tcd ant Aw CDC and all mnpiG l:antaiuerg, Ycs '4 i. V� c'ollection dare & rime listed on the COC mid till Sample caalabl s7 Yes itio IS. Did all containcr labd infonration 90, date, tim) hmrs vL'itLLtfte coc7 +lYesNc3 9 Wcrc tests to Esc pelf0med listed on the € o. Yes �?40 10. Uid a1I swnples arrive ui die pup,7' iojn� qCF for calc�t rrst �11�e'or ingoodctncit�lon (lrublx►�2n, lids oa etc)r _ Yes No 11_ 'as ad:rplatr to ltullr v:lilaLle' Yes IN7G 12_ Were all salnpies received within ;�� tfyt Loidi�l¢ Eii,lc nr �F hc1�s, v�l71CT1cvcr rapes first^ Na 13. Wcrc a!1 s7lples conjaiucfs accourad for? (TO rnissiugr'ca€cess QYes DNo WINA -4 crc VOA. 801 �C alld KSK-175 samples free -of(Albbles (V�Ior 6utm iul ctlailletM) f1 aliny of W VOA Vials,? Yes To ,I A 15_ Wue ail DT 0AuetaWuutriellt sau les lt=A'ed at a 11 of <.27 YCs NO JZ_tMA 16_ W= ai l I > 12 and stjlfir : S9h lcs received a3 a 11 > 9? Yes []TYo �A 17` Wetc #kPPC7i 4 N i3l I < Nr'cytuEl Cp7 E11oFG.Z3.lrr -3 ft= C.t resj&mll cWcuiuO []Yes NO IS. Wah dic quosr umnher listed oil t11e co,tai Ilea labcl? if ws. Qum; Sams I'resei�;�ltiou (N1h1St 11e. tclnlpleted Far any s.�rnlSle (s} iuc;ur�cctly f1r'escd er witjllt,�tdspatc.) SainPir.{3} 'KA were rc�cived itxonecti}' presrrved and �t1�re >;dfusled arccor{Tiehl u1 salrlple rcceiV4 wide M1L Of rirc le Oae: H2SO 1. HNOS, T�CI. NPOI l SjW STZ # _ ii,u= o� 1�resen tFou ? = IE`�t re lll2a4ph'eWwrive is nEx&d, pltau note in the Co117i11C11CR below. nlple(s) -- Wne [eceis�led vdr:3 b bblcs >6 1riI11 ill rlFanlrtcl- Sanlples(sj rya were received wil3 TRC > �?.S n1g {!i#I9 is n) and wen rtJuS€ed wellydiiu&in saulpie receiviag widl sodir» glios111Jatc (I TaAz( j with Cinirlrlc I17: ITA C'j6kllllerlts_ Air bill mo -,vv to calm oii cao2tr_ 7raeJrir� k 1'L 11.79W221M09224 Qualtrax ID: 56360 Pace Analy4ca Sunfic s, RC Rage -r of 1 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 SECTION 3 r N 0) a 0 Z en r O ri O Z a W nWi U n. F W Q Z:) a U N U U Q w Q L x U U u� Z U U O n. 'n O Z W W it - W E o d +n cl ¢ J_ r 0 Ci z Z O O � < k Z ~ Z R W U r 4_ 0 CL a fL 0 U t° Z � W u W J N z -1 N � � W 3 o of w O }z � O z ¢ F O r d CL d U¢ o U n� N a � � c n a ¢ m •v o � M � � U z � N a ,z ❑ U Q Z p cj , a o ! U - Y L Z rn O O o 0 � ui ui a c ❑ m rn o 0 E E r L) O � O E m � N N iu a o c j a a a C Uo 4 �i d N V V V 4_ y o 0 n. ul � ❑ O Q �; d ill W m Of cn U¢ Ca7 J J N m N � � F o 0 � 0 � 0 o 0 w r r N � ❑ U U 7 o O O o ao 4 o� N O O O N O N N a � > 0 O 0 0 m r O F Lq 0 a U) co O .6 N rn a _a O Q N O 0 C U O U) CL cal m b 0 _T U �q G U O w U O M CD cj� U) tl o C C < `n (v U U Q1 O J r. C In m n U Q. j CR ) a n Li l6 C J w crE F C C Ai d `- �e7U= N a�i l6 J U) rnO) W SECTION 4 SUMM111 ENVIRONMENTAL TECHNOLOMZ3. INC Arraly0ca1 Laboralorfas September 07, 2022 Chris Wynne Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: FAX: RE: LaGrange WWTP Dear Chris Wynne: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com Order No.: 22081198 Summit Environmental Technologies, Inc. received 1 sample(s) on 8/17/2022 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-011-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon 0112O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah 011009232020-12, Virginia VELAP 10381, West Virginia 9957C Page 1 of 32 SUMMIY Summit Environmental Technologies, Inc. Case Narrative 3310 Win St. ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22081198 Arralyi9cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com Date: 9/7/2022 CLIENT: Synagro Project: La Grange WWTP WorkOrder Narrative: 22081198: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 22081198-OOIA MTL-TCLP-7(6010D): Bracketing CCV exhibited high recovery for Selenium. Sample exhibits detection < PQL for this analyte. 22081198-OOIA TCLP-SVOC_8270E: MB-59147 exhibited detections for all analytes likely due to contamination during extraction. Associated samples uploaded in this sequence were ND for all compounds. Original Page 2 of 32 MMIT summit Environmental Technologies, In Qualifiers and Acronyms SU3310 Win S EkiwAOMM@NTALTEc„NOLOGir,S,INC Cuyahoga Falls, Ohio442� Wo#: 22081198 Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-446 Wehsite: httn:11www.settek.co Date: 9/7/2022 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time PLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 32 �� 1 � Summit Environmental Technologies, Inc. SU3310 Win St. ENVIRCNMEWAL YECHHOLOGNUS, JNC, Cuyahoga Falls, Ohio 44223 Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com CLIENT: Synagro Project: La Grange WWTP Lab SampleID Client Sample ID 22081198-001 La Grange WWTP Tag No Date Collected 8/16/2022 10:00:00 AM Workorder Sample Summary WO#: 22081198 07-Sep-22 Date Received Matrix 8/17/2022 9:55:00 AM Sludge Page 4 of 32 V A C. V N N cn o ;o V T 'O p U cC .U. ONO iC iC i,. O O U V] y H N co O O cB Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223 Arralyt9cal Laboralorfas TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://�i,-"-m,.settek.coin Analytical Report (base report) WO#: 22081198 Date Reported: 9/7/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 8/16/2022 10:00:00 AM Lab ID: 22081198-OOIA Project: La Grange WWTP Client Sample ID La Grange WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP MERCURY ANALYSIS (SW1311/7470) TCLP Mercury ND 0.00200 mg/L SW7470A SW7470A Analyst: ICA 1 8/31/2022 11:56:00 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010 SW301OA Analyst: MSK TCLP METALS ANALYSIS (SW1311/6010) TCLP Arsenic(As) ND 0.500 mg/L 1 8/30/2022 5:30:19 PM TCLP Badum(Ba) ND 5.00 mg/L 1 8/30/2022 5:30:19 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 8/30/2022 5:30:19 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 8/30/2022 5:30:19 PM TCLP Lead(Pb) ND 0.500 mg/L 1 8/30/2022 5:30:19 PM TCLP Selenium(Se) ND 0.0500 mg/L 1 8/30/2022 5:30:19 PM TCLP Silver(Ag) ND 0.500 mg/L 1 8/30/2022 5:30:19 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW351OC Analyst: SFG TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270) 1,4-Dichlorobenzene ND 0.200 MB+ mg/L 2 8/31/2022 4:35:00 AM 2,4,5-Trichlorophenol ND 0.500 MB+ mg/L 2 8/31/2022 4:35:00 AM 2,4,6-Trichlorophenol ND 0.500 MB+ mg/L 2 8/31/2022 4:35:00 AM 2,4-Dinitrotoluene ND 0.100 MB+ mg/L 2 8/31/2022 4:35:00 AM Cresols, Total ND 10.0 MB+ mg/L 2 8/31/2022 4:35:00 AM Hexachloro-1,3-butadiene ND 0.0400 MB+ mg/L 2 8/31/2022 4:35:00 AM Hexachlorobenzene ND 0.100 MB+ mg/L 2 8/31/2022 4:35:00 AM Hexachloroethane ND 0.200 MB+ mg/L 2 8/31/2022 4:35:00 AM Nitrobenzene ND 0.200 MB+ mg/L 2 8/31/2022 4:35:00 AM Pentachlorophenol ND 0.500 MB+ mg/L 2 8/31/2022 4:35:00 AM Pyridine ND 0.500 mg/L 2 8/31/2022 4:35:00 AM Surr: 2-Fluorophenol 95.7 10 - 157 %Rec 2 8/31/2022 4:35:00 AM Surr: Phenol-d6 103 10 - 169 %Rec 2 8/31/2022 4:35:00 AM Surr: Nitrobenzene-d5 80.0 32.1 - 130 %Rec 2 8/31/2022 4:35:00 AM Surr: 2,4,6-Tribromophenol 121 45.4 - 166 %Rec 2 8/31/2022 4:35:00 AM Surr: 2-Fluorobiphenyl 84.1 35.7 - 130 %Rec 2 8/31/2022 4:35:00 AM Surr: p-Terphenyl-d14 98.1 70 - 145 %Rec 2 8/31/2022 4:35:00 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected OG1 P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 32 Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223 Arrafyt9caf Laboralorfas TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://�i,-"-m,.settek.coin Analytical Report (base report) WO#: 22081198 Date Reported: 9/7/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 8/16/2022 10:00:00 AM Lab ID: 22081198-OOIA Project: La Grange WWTP Client Sample ID La Grange WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND Toxaphene ND Endrin ND gamma-BHC ND Heptachlor ND Heptachlor epoxide ND Methoxychlor ND Surr: TCMX 77.4 Surr: DCB 85.6 TCLP HERBICIDES BY EPA 8321 B 2,4-D ND 2,4,5-TP ND Surr: 2,4-Dichlorophenylacetic aci 96.2 TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 1,2-Dichloroethane ND MEK ND Benzene ND Carbon tetrachloride ND Chlorobenzene ND Chloroform ND Tetrachloroethene ND Trichloroethene ND Vinyl chloride ND Surr: 4-Bromofluorobenzene 104 Surr: Di brom ofl uorom ethane 96.5 Surr: Toluene-d8 100 SW8081 SW351OC Analyst: PGP 0.0250 mg/L 10 9/3/2022 2:46:00 AM 0.0500 mg/L 10 9/3/2022 2:46:00 AM 0.00500 mg/L 10 9/3/2022 2:46:00 AM 0.00500 mg/L 10 9/3/2022 2:46:00 AM 0.00500 mg/L 10 9/3/2022 2:46:00 AM 0.00500 mg/L 10 9/3/2022 2:46:00 AM 0.00500 mg/L 10 9/3/2022 2:46:00 AM 10 - 119 %Rec 10 9/3/2022 2:46:00 AM 10 - 119 %Rec 10 9/3/2022 2:46:00 AM SW8321 Analyst: PGP 0.500 mg/L 50 9/1/2022 9:13:00 PM 0.500 mg/L 50 9/1/2022 9:13:00 PM 70 - 130 %Rec 50 9/1/2022 9:13:00 PM SW8260 SW1311 M Analyst: ZDA 0.500 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 10.0 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 5.00 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 0.500 mg/L 100 8/31/2022 6:36:00 PM 0.200 mg/L 100 8/31/2022 6:36:00 PM 70 - 130 %Rec 100 8/31/2022 6:36:00 PM 70 - 130 %Rec 100 8/31/2022 6:36:00 PM 70 - 130 %Rec 100 8/31/2022 6:36:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds OG 1 PL Permit Limit Original RL Reporting Detection Limit Page 7 of 32 MMIT Summit Environmental Technologies, Inc. Analytical Report SU3310 Win St. ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report) Arralyt9cal Laboralories TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22081198 Website: http://www.settek.com Date Reported: 9/7/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 8/16/2022 10:00:00 AM Lab ID: 22081198-OOIA Project: La Grange WWTP Client Sample ID La Grange WWTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9014 Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2)-SOLID Cyanide, Reactive ND 0.490 mg/Kg 1 8/25/2022 2:39:00 PM IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: SMZ Ignitability Nonflammable mm/sec 1 8/29/2022 11:49:37 AM PERCENT SOLIDS BY SM2540MOD A2540B Analyst: SMZ Percent Solids 1.88 % 1 8/26/2022 11:44:02 AM RCI SW9045D Analyst: ALT PH (SW9045D) pH 3.6 s.u.@18.7C 1 8/18/2022 5:16:00 PM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 8/25/2022 2:39:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds OG 1 PL Permit Limit Original RL Reporting Detection Limit Page 8 of 32 Summit Environmental Technologies, Inc. Accreditation Program frSU 3310 Win St. MM'EF Analv n tes Report ENOROMMEWAL IrECHNOL.OG{r,S, INC Cuyahoga Falls, Ohio 44223 J Y Arralytical Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22081198 Wehsite: http://www.settek.com 07-Sep-22 Client: Synagro State: NW Project: La Grange WWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 22081198-OOIA Sludge Ignitability of Solids (SW-846: 1030) Ignitability A Sludge Percent Solids by SM2540Mod Percent Solids N Sludge pH (SW9045D) Hydrogen Ion (pH) A Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A Sludge TCLP Herbicides by EPA 8321B 2,4-D A Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A Sludge TCLP Metals Analysis (SW1311/6010) Barium A Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A Sludge TCLP Metals Analysis (SW1311/6010) Chromium A Sludge TCLP Metals Analysis (SW1311/6010) Lead A Sludge TCLP Metals Analysis (SW1311/6010) Selenium A Sludge TCLP Metals Analysis (SW1311/6010) Silver A Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Sludge TCLP Pesticides Analysis (SW1311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A Key Key Key NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl Original #1 Page 9 of 32 Summit Environmental Technologies, Inc. Accreditation Program MM'EF frSU3310 Win St. Analv n tes Report ENVIROMMEWAL IrECHHOL.OG{r,S, INC Cuyahoga Falls, Ohio 44223 J Y Arralytical Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22081198 Wehsite: http://www.settek.com 07-Sep-22 Client: Synagro State: NW Project: La Grange WWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 22081198-OOIA Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A Sludge TCLP Volatiles Analysis 1, 1 -Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A Sludge TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzene A Sludge TCLP Volatiles Analysis Chloroform A Sludge TCLP Volatiles Analysis Tetrachloroethene A Sludge TCLP Volatiles Analysis Trichloroethene A Sludge TCLP Volatiles Analysis Vinyl chloride A NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl Original #1 Page 10 of 32 0 M '1 Fi U V a 0 T r) r 00 a_LO M M r) d Z ry z ry ry 0 N O N rn E N J 00 L O) N N = 6 ) Q U) E Q) 'N J d T (6 O � J Q U W 0 J E (0 r > Z M Y IL U) a co co > Y H CO IL � Z 0 U J Ci H a J M m N a a E ca m CO U O M LO m CO � CO Q � � (E6 O co C cn U Q O O O O O O r- r- r- 00 r- o m m U') LO U') 0 0 0 0 0 0 0 0 0 0 N N L6 N N 0 N N N O O O O N O 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 Z Z Z Z Z Z Z Z Z Z LO N M N C C C 0 0 O O O 00 N N O O O 7 co N (06 O O O O O N E N O O 00 Z '00_ CO Q 0 O O N O O 00 O V i H N Q O O (U6 t U O O 7 Y r-O O U T��� N W N co L L O s r 7 A U :C �Q m J N 00 T 0� M d zo zo c � i/) Flo N N N N Q1 E N M 00 00 L _D O) O) 2 (6 (6 cl cl Q N E 2 'N 3 a c J Q U W J tm E O N L > M � N Y a Qi cn z 00 a 23), U ci m N � � z 0 U N J U H a � a le N L a a .V. 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R N m L o o 0- >, co O C U U Q O O N�� O �f7 L�2 �2 N N N O O O O O O O O O o � mo m v) co co m ai ai 1- m O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 O O O O O O 0 0 0 0 0 0 0 cn o 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 �f7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 p p r— m m cn co r,m z z O m 0 0 0 0 0 O O O O O X U o o 2 m C C m O O U H co L L T 'O 0-C E U U X W W O 7 7 o x -o E o o y U U U H W o) 2 2 2 n 75 O N N N E M M 00 m L _D N N cl cl a U) E .N 3 co J LU U J C1 E o � N Lo > C) Cl) Y a U U y00 25 a 00 co U Y H � 00 z U N J U H a Q) a y rn Q) Lc) a a .U. E m co Co 0 Q O 4 U M C7 M O .v. R N m L o o Co co O C U U Q rl N A U :C 75 n a O N N N E M M 00 G1 L _D O) O) 2 (6 (6 cl cl a U) E 2 .N 3 a '• c J Q U u1 J C1 E o � N L > C) C � � � N Y a U U N c a a co co m U Y H N � � Z 0 U N J U H a � a N 0*1 O) if LO a a .U. E m co Co 0 00 O 4 U M C'1 0 t O .v. R N m 0) 0) Co O C U U Q 0 0 0 0 0 0 0 m m m m m m m O O O V uf) V N O O m N I� O O1 V m N m V O O �f7 CO 0 0 0 0 0 0 0 0 0 0 0 O O N� 0 0 �f7 N N N O O O O O O O O O o m N O N of m r- o 0 0 0 0 0 0 0 0 0 0 0 0 0 0�C14 0 0 0 0 0 0 0 0 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 �f7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 O O m O N Uf I, Z Z N N N 0 0 0 0 0 0 0 0 0 0 O) LD X U o o m N L L T -O 0-C E U U X i i W W O 7 7 o x o E a a y U U U H W 0) 2 = 2 N M 4- 0 co O ca 0- �Q m J n a- M d zo zo c 0- in 75 n N N N N o E M MiD 00 00 L _2) O) O) 2 (6 (6 cl cl a U E 2 .N 3 a '• c J Q U w a a a o 5 _ v > � N Y a n U a J p � H� n co 2 CO a- 0 Z U N J U H a (D a m N () L a a .V. E m co Co O O N O O ii i 2 a m J 00 M d zo zo c � [If in 75 n N N N N o E M MiD 00 00 L N N cl cl a U E E .N 3 a '• c J Q U w a a a o 5 _ v > Cl) Y a n U a J p � H� n m 2 CO a- 0 Z U N J U H a (D a U rn o Of J to a a .V. E m co Co O N N am U? co Cl) Cl) J J 0) 0 0) 0- >, m o c U U Q O O 0 0 v rn O m J rn a- to � M d zo zo c 0- � in 75 n N N N N o E M M 00 00 L _D N N cl cl a U E 2 .N 3 a '• c J Q U w a a a o 5 _ v > n Cl) Y a n U a J p � H� I, 2 CO a- 0 Z U Q) J a U Q) a Cl)N Q) L a a .V. E m co Co Q r 4 an U L c t o r R N m L 0) 0) 0- 5% m o c cn U Q O Ut rn O m J a- M d zo zo c � in co N N N N o E M M 00 00 L _2) (6 (6 cl cl a U) E 2 .N 3 a c J Q U w a a a o 5 v > y_ n � N Y a n U a J p H� n m 2 m a- -0 Z 0 U N J U H a � a N N L a a .V. E m co Co a CO Q 4 LO U L c t o r R N m L 0) 0) 0- >, m o c U U Q O N V 26 i 2 a J U w 0 N N Fi U U V a 0 r) to t ry M r) d ry z z 0- 75 0 N N CDO N N O E M M J 00 00 L 0 N N = 6 ) Q U) E d T � J Q U LU 0 N N � N a a E ca m CO 0 co ¢ oco 0 U N N m N � N mm c cn U Q s N co O O N O (B d U V a 0 J L(.) co IL L T ry co Lo M r) IL Ir z z Ir In ry ry 0 N (D N W J 00 L 2) N N = 6 ) Q U) E CL T � J Q U W U v 0 N 7 y > C Y IL 0 U Cie 01 > I Y Q. CO IL �o Z 0 U J IL H a 0175 a v o � � ui a a E ca m CO a Q 4 cm CY co 0 N R N m N � N mm c cn U Q 0 N r— N O K� O N 2 a s N co O N O (B d 0 J co � IL L T ry ao Lo M r) IL Z Ir z In ry ry 0 N O N W � J 00 L N N Q N CL T � J Q U LU U � v N 7 > C Y IL I Y Q. CO IL �o Z 0 U J IL H a LO LO co 3 U U J J N � N m m c cn U Q m In m O O O 2 Q i N co O N N O (B d m J M a- Lf)am L M d zo zo c � i/) 75 O _ N W 00 L _D N N = (6 (6 cl cl Q N E 2 .N 3 a '• c J Q U w U n 6 7 N N N > C D � Y o a LO U v a v Z rn j a CO a- 0 z 0 U N J U H a (D a LO C1 U) Cl)co J � � N a a .V. E m co Co LO e G1 e Cl) Cl) J J 47 N fl >, E o co c/ U Q V O O O rn 0 O O r- O r- m J MLO to � am L M d zo zo c � [If i/) 75 O _ N W E 00 L _2) N N = cl cl a U) E E .N 3 a c J Q U w U L ai 7 y co N > C D � Y o a LO Cl) v a v Z rn co j a CO a- 0 z 0 U N J U H a (D a M e — Im a00Q) o � � N a a .V. E m co m CO a W O 4 U o U, 0 s o r R N m L 47 N E o m Co � U Q m J M COO � M d zo zo C ZT (n n 75 O _ N E N 00 L _D cl cl Q to 2.N 3a > c J Q U u1 J C1 E 75 N > C D � Y a R o a m w 01 > N � � Z 0 U N J U H a (D a N CM Y cn J Im u) a a .V. E m co Co N M M rn m � a E o co Co n a O Ut N cl Z 0 co Q) m J N Im to M COO � M d zo zo C ZT (n n 75 O _ N E N 00 L _2) cl cl Q to .N 3a >• c J Q U u1 J tm E 75 N > C D � Y a Q C/) m � � o o m w 01 > N � � z 0 U N J U H a CD a N M � Cl) N J a a .V. E m co Co N M M U co J J 0) O) E o m c / U Q 00 O 00 v rn O O rn N N O Ut N O N m J a- M COO � M d zo zo C CT a' (n n 75 O _ N E N 00 L _D C6 (6 cl cl Q to 2.N 3a > c J Q U u1 J C1 E 75 N > C ) � Y a t5 CO R o a co w 01 > N � � z 0 U Q) J Q CJ N Cl) Cl) - 01 N 0) a a .V. E m co Co CO Q O 4 U M 0 00 t o r R N m L 0) E o m cl) U Q U') N �f7 r- C6 rn O O rn N N O Ut N O Co N N 0 co Q) m J LO 0 M O CO to M d o zo z C ZT (n n 75 O _ N E N 00 L _D (6 (6 cl cl a U) E 2 .N 3 a > c J Q U u1 J C1 E 75 CD N > C D � Y a t5 C/) R o a m w 01 > N � � z 0 U N J U H a CD a N Cl) Cl) CO CO 0) a a .V. E m co Co a CO Q O � U M C'1 c t o r R N m L 0) E o co Co /) U Q O cam 00 00 O O co N N �f7 N �f7 O rn N N O Ut N O N N 0 co Q) LD CO N M M 7 .-I u Fi U Z3 0 J LO r) M is m to M r) d ry z z tT C� Cl) ry ry 0 N O N E N J 00 L 2) N N = 6 ) Q U) E Q) 'N J d T � J Q U LU 0 J (a _Z6 > C Y v a R U) � � m a o co w CA > a � Z 0 U J IL H a M M75 � � N N a a E ca m CO 0 co CY co 0 � U N N m N � N mm c cn U Q s N co O LO N O (B d m J O � M Cn0 � M d zo zo C � (n n 75 O _ N E N 00 L _D (6 N cl cl Q N 2.N 3a c J Q U W J C1 E 75 N > C D � Y a- m U m Y U Co Cl) 70 z 0 U N J U H a a cn cn Y CM U) J Im N a a .V. E m co Co rn v 0 cl z m J M Cn0 � M d zo zo C � a' (n n 75 O _ N E N 00 L _2) (6 N cl cl Q N .N 3a '• c J Q U W J C1 E 75 CD N > C D � Y a- m Cl) CD Y U Co Cl) 70 z 0 U N J U H a CD a M � Cl) J a a .V. E m co Co CO 00 O N O O m J C') a- M Cn0 � M d zo zo C 0- a' (n n 75 O _ N E N 00 L _D C6 N cl cl Q N 2.N 3a c J Q U W J C1 E 75 N > C ) � Y a- m CO m Y U Co a- � z 0 U Q J Q CJ x U N M Cl) Cl) > U U m d co J J N m 0) 0) cl 6 cl O) O) 0) 0) 0) 0) 'c Q j, 'c C- j, T C>1 co CoE cn = U C QC) Co U = U C Q U co cn �� U C Q O 0 co Q) LD C m J M m to Im to M d o zo z0 C � (n n N O _ N E N 00 L _D co co cl cl a U) E 2 .N 3 a c J Q U W J C1 E 75 N > C D � Y a- m U m Y U N a- (D z 0 U N J U H a � a M M � rn N a Q) a a .V. E m co Co CO Q O � U M C'1 c s o� R N m L 0) 0) Co co Q)C U U Q 0 co Q) C co >, U m J M M to to M d Z Z o C � (n n 75 O _ N E N 00 L _D (6 N cl cl Q N 2.N 3a c J Q U u1 J C1 E 75 N > C D � Y a- m U m Y U Co Cl) 70 Z 0 U N J U) H CJ le M cn rn 0 v 0 a a .V. E m co Co Q O 4 U M 0 co c t O U R N m b 0) 0) fl >, Co C U U Q m J le C*4 O a- a m to to M d Z Z o C � (n n 75 O _ N E N 00 L _D (6 N cl cl a 0 E 2 .N 3 a c J Q U u1 J C1 E 75 CD N > C D � Y a- m U CD Y U Co Cl) 70 Z 0 U N J U H a CD a- le M CM CO 0) of a a .V. E m co Co a CO Q O U M 0 � t co U R N m b 0) 0) E co Co C U U Q O O cam rn O co ai rn O O rn v 0 co m m J 00 M n to M d Z Z o c � (n 75 O _ N E N 00 L _D (6 N cl cl Q U)2.N 3 a c J Q U w e N N > C D � Y a CO = m � �O v co LO Y a � � Z 0 U N J U H a (D a 01 n Y M U) J le U) a a .V. E m co Co G1 n Cl) G1 E co m � a Co C C/) Q O O cl Z U) O m J Im Mim n M d Z Z o c � (n 75 O _ N 4) E N 00 L _2) (6 N cl cl Q N .N 3a '• c J Q U w e N N > C D � Y a Cl)I = m � CO v m Y a LO � � Z 0 U N J U H a (D a 01 n M � Cl) N J a a .V. E m co Co 01 n M co Cl) Cl) J J 0) O) 0- T E co (6 C U U Q O O O O 6 O O O U) O m J a- M n � M d Z Z o c 0- � (n N O _ N E N 00 L _D O) O) 2 (6 N cl cl a U) E 2 .N 3 a c J Q U w e N N > C ) � Y a Cl)I 00 Q) co U) v Y aLO � � Z 0 U Q) J a U Q) a am n M � a o Q) a a .V. E m co Co a O rn c 00 (� N J 0) Co co = C cn U Q U') N Cl? O 00 O O 00 O U V a 0 J r r) C,4 toV O ry M r) d ry z z ry ry 0 N O N rn E N J 00 L 6 ) Q U) E d T � J Q U LU CV! E E _Z6 > C Y IL I U) O � w 0 > s= 3 Y co IL �o Z 0 U J IL H a cm LO co U U J J mm co cn U Q O co O r- LO O O V N r- M M 00 T .1 i N co O O') N O (B d m Cl J a- n N 00 M d o zo z C (n n 75 N N _ O rn � _D ib ib = 6 m cl cl a U 2.N 3a > c J Q U u1 J C1 E 75 N > C D � Y a U U CO N a' CM (6 00 > U Y H N � � z 0 U N J U H a � a cn 01 n J N N a a .U. E m co Co N 2 G1 N 00 O N N Cl)m � a O O fl >, Co O C C/) Q cam C6 0 0 0 0 p cl CO z z 00 O U co U a u m J N n N 00 c') d zo zo C � a' (n n 75 N N _ O rn � _2) co m 0 cl a U) E 2 .N 3 a >• c J Q U u1 J C1 E 75 N > C ) � Y a U U Ct? N =5 d M (6 00 > U Y H N � � z 0 U N J U H a � a M G1 ... n � v J U) U a a .U. E m co Co CO m N 2 G1 N 00 O N N Cl) U J J O � O Co O co = C C/) C) Q � � O 0 rn rn cl Flo J M a- n N 00 M d zo zo C � a' (n n a N N _ O N E rn � _D ib ai = m m cl cl a U) E .N 3a > 5 J Q U u1 J C1 E 75 N > C ) � Y a U U Ct? N =5 d C) 75 00 > U Y H N � Q) z 0 N U J a U Q) a M T C U) v J � N a a .U. E m co Co CO m V 4) 2 G1 N 00 O N N N O Cl) U J J O O co co O C � C) Q U') 0 O CR 00 v Cl? N 0 0 O Un co O m Oco �n o co 0 0 C). rn cl N M O O co � O O c6 O O O) m n CIS N M 4- 0 Tl- O O7 m 0- �� � � Summit Environmental Technologies, Inc. SU3310 Win St. ENVIRONMENTAL TECHNOLOQH�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List Arrafocaf Laboralorias TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://`h,,",m,.settek.com Client Name: SYN-NC-27028 Work Order Number: 22081198 RcptNo: 1 Logged by: Christina N. Jager 8/17/2022 9:55:00 AM C. Completed By: Tegan A. Richards 8/17/2022 1:49:20 PM 41 n qE;- Reviewed By: Jennifer Woolf 8/17/2022 6:08:58 PM )V' Chain of Custody 1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑ 2. How was the sample delivered? UPS Lop In 3. Coolers are present? Yes ❑d No ❑ NA ❑ 4. Shipping container/cooler in good condition? Yes d❑ No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑ 6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑ 7. Sample(s) in proper container(s)? Yes ❑d No ❑ 8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑ 9. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑ 10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑ 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials ❑� 12. Were any sample containers received broken? Yes ❑ No ❑d 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑ 15. Is it clear what analyses were requested? Yes ❑d No ❑ 16. Were all holding times able to be met? Yes No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V Person Notified: Date: By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 18. Additional remarks: Cooler Information Cooler No Temp °C Condition I Seal Intact Seal No Seal Date Signed By 1 15.9 Goodl Not Present Page 32 of 32 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of La WIVTP Name: Town of La Grange WWTP NPDES Number: \4onitoringPeriod: From 01/01/2022 To 12/31/2022 WQ Permit Number: Wp0010488 NCO021664 Pathogen Reduction (40 CFR 503.32115A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. I/A (time/tenip) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) AIL 5/Process to further Reduce Pathogens AIL 6 (Gquivalettl to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Y Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion I£nnnGenhlc to alternative nerfnrmed lCl-m A nr f'lacc tti emmnlefe the fntinwinn ninnitnrinn dnta- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Cxcee- of Type Technique Minimum Gco. Mean Maximum Units deuces Analysis Fecal 2x10to the 611, MPN MPN/g Coli form power per gram of total solids <93400 <139000 <178000 CFU/g 0 Annually Grab SM9222D CPU -M F 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. I Option/Alt. 2 Option/Alt. 3 Option/All, 4 (VTreduction) (40-day bench) (30-day bench) \ (Spec. 02 uptake) Option/Alt. 5 Option/AIt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying -- Stable) (Drying -- Unstable) Option/Alt. 9 Option/Alt. 10 (injection) (incorporation) No vector attraction reduction alternatives were perforated CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalt), of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction Y reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under pcnalt), of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.I 106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been stet. I am aware that there are significant penalties for false certification including tine and imprisonment." John Cr wn NUnager Prrer Name , n ' e p o ty e) Land Applier Name and Title (ifapplicable) (type or print) '100 Z� Signatu f Preparer* Dale Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date Cameron Testing Services, Inc. Laboratory Report NCDENR#654 NC PHHS #37799 US EPA#NC01918 Client: Synag ro CTS Proj. 2208-0039 DW Cert # 37799 Project. LaGrange WWTP Regulatory Yes Sample Information Sampled C. Wynne Date 08/03/22 Received J. Strickland Date 08/03/22 Analyses and Results Lab ID Sample ID F ` E ra Analyte Result c C i r °.3 = Std. Methods c Q Reference a 2208-0039 -01 sludge Gr Fec. Coliform-S <145000 CFUIg 145000 08/04/22 ERP 9222D - MP -02 <162000 CFUIg 162000 -03 <133000 CFUIg 133000 -04 <126000 CFUIg 126000 -05 <93400 CFUIg 93400 -06 <155000 CFUIg 155000 -07 <178000 CFUIg 178000 Geomean <139000 CFUIg 2208-0039 -01 nudge Gr TS (%) 1.90% 0.01 08/04/22 ERP 2540 G -TS -02 1.90% 0.01 -03 1.90% 0.01 -04 1.90% 0.01 -05 1.90% 0.01 -06 1.90% 0.01 -07 1.90% 0.01 Report ' Review Project Manager Date I 4�WA 219 S. Steele Str. 919-2084240 Sanford NC 27330 chris@camerontesting.com O m a. � 1 O 1 � t � S = b n i i N 7 co m Z O b d a 0 Z } d N a a w N a }as VCA O 0 co �, rn Z d 009 ! d OZ£ I�`J ZIP i s ii o (N/M aal a _ .2 xuleW �v E qei� l I dLuoo v 0o s - -- CD m I tiCLOWLL i r� ale(] NII t I 4j o� co ],t 00 UO ❑ •` CL T Lt , E` V �. a U) O 00 co 0 0 I 00 C) CN CN 'o o � NC)c) V N N O N tq Gam! d 7, rr C 4) Q k � N a CD N W C R CM Q to M a e . o CO Cl) r M I� id7 In O j L 7 LL � � N N N y N N N N O OD 01) W 0 a o CO I-- M V lO y(.0 �o n (C) CD CL Y w cn N N o m e o 01 0 CC! 0 Cl 0 C] 0 � o Y cz C7 Cn y LL' it o K L? o � N V' C/) _ o Cl) .+ D w N N �. m O m U o o a0 i-p V E O d d co Q tm N F a v O Lo V N N N IL IR Cl) 6 0 0 N 4- 0 N ca co POO aQ C'] r I I cc L © 0 N .N w y N t1f m N F* U °= m0� ; Q @ z o j CL 0 ? z a- w co CL rn fl Jay3Q MW II r�iIMMl� a W V d hE 0 Cl) O N 47 0 r M ro y. U >• 0 @ In 2 z L31. d OZE 4t V -t� Cs II I U ICJ Z16 = U. a (N/A) ail .Z Z a z - z _ o XIJIEW ws i E gej!D a- �° duaoo 'J Iv 0o .- NI Nawil -=�- Z r) `V N TT, CD ° o v uo c� m N >' CO 50 c C ` w O a CD o o f C 8 f�{ 0 a a O a w cy- 0 3 U) M SECTION 6 Agricultural Lime Application Log Year 2022 Project La Grange Fields Soil Lime Requirements Tons/Acre Date (state -county -site -field) PH (from soil analysis) Applied A lied LN-2-2 1 4.81 11.8T I N/A LN-2-4 1 5.11 11.4T I N/A N/A- Did not apply in 2022 *Lime will be applied when field conditions/cropping pattern permits SECTION 7 cn N -e O M %D . N N N m N N O O j N F 000 a r r E m c E a c 'p O U. C cc .Q o w 00 s N tD n U L U U O0 J N J O C, c N CO oQ a>mz rn O, U 3 N N N V N o O cm') (.0 600 m v ro> Y N p >, O000 O U �E N r O Z o Z •• + fA O3 a V d m Q 70 Q Z r r 0 0 N W ol C � � OR U m v OR y m m m Lo c0 W V W N LO O U o r CO L. 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