WQ0003351_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0003351
Applicant/Permittee Town of Mocksville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0003351
Has Current Existing permit number
Applicant/Permittee Address*
171 Clement Street, Mocksville, NC 27028
Facility Name*
Town of Mocksville Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Mocksville Annual Report - WQ0003351.pdf 14.63MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/28/2023

February 3, 2023
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report — Town of Mocksville
Treatment and Land Application of Residuals
Permit No. WQ0003351
Dear Sir or Madam:
Enclosed is one copy of the 2022 Annual Report for the above referenced land
application permit.
During 2022 EMA Resources, Inc. land applied 166.64 dry tons of wastewater residuals
to 79.75 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Z�z 4;2W -
Brent Collins
Director of Technical Services
brent.collinskemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

--Resources, Inc.
Town of Mocksville
2022 Annual Report
Residuals Land Application
Permit No. WQ0003 3 51
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0003351 County: Davie Year:
2022
Facility Name (as shown on permit):
Land Application Operator:
EMA Resources Inc.
Town of Mocksville
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
10
Total number of fields utilized for land application during the year:
7
Total amount of dry tons applied during the year for all application sites:
166.64
Total number of acres utilizes for land application during the year:
79.75
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Ken Gamble - Town Manager
/Km Ga)WbGe
Ken Gamble (Feb 3, 2023 16:15 EST)
Feb 3, 2023
Permittee Name and Title (type or print) Signature of Permittee Date
T�fcfsobi3rf� y Feb 3, 2023 2i2i2023
Todd Robinson (Feb 3, 202311:56 EST)
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WQ0003351 Laboratory:
Town of Mocksville
NCO021491
WWTP Name: Dutchman's Creek WWTP
Recidnal Analvcic Data
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/kg a
Sample or Composite Date
1/24/22
4/6/22
8/3/22
10/6/22
Percent Solids (%)
NA
1.77
1.89
1.05
1.09
Arsenic
75
13.3
26.3
24
21.8
Cadmium
85
1.11
5.26
2
1.82
Copper
4,300
187
161
188
380
Chromium
NA
23.9
23.4
23.6
1 31.1
Lead
840
17
21.1
18
22.8
Mercury
57
0.346
0.335
0.68
0.606
Molybdenum
75
7.5
13.2
13.5
12.3
Nickel
420
11.9
13.2
12.1
21.2
Selenium
100
17.8
26.3
32
29.1
Zinc
7,500
594
437
461
819
Total Phosphorus
NA
19500
24400
32700
28900
TKN
NA
78900
75800
87500
85600
Ammonia -Nitrogen
NA
6170
6160
7230
6080
Nitrate and Nitrite
NA
405
254
4780
7920
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
TWd Dbi�roy Feb 3, 2023
Todd Robinson (Feb 3, 2023 11:56 EST)
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0003351
Facility Name: Town of Mocksville
Residual Source NCO021491
NPDES # or WQ#:
WWTP Name: Dutchman's Creek WWTP
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
ParameterSample
•
or Composite Date
MMMMMMMMMMMM
1.11
11
11
• 11
--------
••11
11
11
:11
--------
'•
•111
1
111
•1 1
--------
------------
------------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
%OG�G� kMl, ,f,y
Todd Robinson (Feb 3, 2023 11:56 EST)
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Feb 3, 2023
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied (Annual): 67.36
Permit #: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series: CeB2
Acres Used: 21.8 Acres Permitted: 21.8 Site #: NC-DV08 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
1/24/22
2 1
4/6/22
3
4
5
6
7
8
9
10
11
12
% Solids
1.77
1.89
Arsenic
13.3
26.3
Cadmium
1.11
5.26
Copper
187
161
Chromiurn
23.9
23.4
Lead
17
21.1
Mercury
0.346
0.335
Molyb-
denum
7.5
13.2
Nickel
11.9
13.2
Selenium
17.8
26.3
Zinc
594
437
Total
Phos-
horns
19500
24400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
D
mammon
NOOSE
Event
1 1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 1
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
��
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •m
••
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized: 21.8
Land Owner: Roger Spillman Annual Dry Tons Applied: 67.36 Site #: NC-DV08 Acres Permitted: 21.8
Operator: Roger Spillman Predominant Soil Series: CeB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
met'
Moist)
Precip.
Past 24
Hrs.
inches,
a
co S
0 w
* °�
o
-
N
o
7
w
N
o
TKN
mg/kg
Z a
;
o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/15/22
22500
1.77
0.076
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
3.856
NA
Fescue
2/16/22
36000
1.77
0.122
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
6.170
NA
Fescue
2/17/22
45000
1.77
0.152
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
7.712
NA
Fescue
2/19/22
22500
1.77
0.076
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
3.856
NA
Fescue
2/21/22
45000
1.77
0.152
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
7.712
NA
Fescue
2/22/22
36000
1.77
0.122
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
6.170
NA
Fescue
3A/22
40500
1.77
0.137
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
6.941
NA
Fescue
3/5/22
45000
1.77
0.152
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
7.712
NA
Fescue
3/7/22
40500
1.77
0.137
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
6.941
NA
Fescue
4A/22
1
36000
1.89
1 0.130
Dutchman's Creek
Dry
<.5"
S
1 0.5
1 0.3
1 75800
6160
1 254
6.306
NA
Fescue
4/5/22
31500
1.89
0.114
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
5.518
NA
Fescue
4/11/22
36000
1.89
0.130
Dutchman's Creek
Dr
<.5"
S
0.5
0.3
75800
6160
254
6.306
NA
Fescue
0
439500
1.589
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
76.986
0.000
TOTALS:
01
876000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
152.1851
o.000
Lime Applied
Annuallbs/acre
0.1332
0.0232
1.0536
0.1457
0.1212
0.0021
0.0687
0.0786
0.1434
3.0545
139.747
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.0511
0.0041
0.1970
0.2735
0.0995
0.0008
0.0152
0.1321
0.0468
0.6421
Current Cumulative lbs/ac
0.1843
0.0273
1.25061
.4192
0.2207
0.0029
0.0839
0.2107
0.1902
3.6966
Permitted C. P. L. R. * * * *
36
34
1338
267
1 15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 1 156
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
L•�'� 2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized:
Roger Spillman Annual Dry Tons Applied: 67.36 Site #: NC-DV08 Acres Permitted:
Roger Spillman
Crop 1 Name:
Fescue -Pasture
Predominant Soil Series: CeB2
Crop 1 Max. PAN:
156
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max PAN:
21.8
21.8
o
r./o
o
Volume applied (enter
one)
Cu. Yds Gallons
o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, W #,
Fert., Animal
Waste, etc)
Soil
Cond.
(D
We '
Moist)
Precip.
Past 24
Hrs.
inches
y
a
°o w
°�
o
7� w
N'
o'
7� ?_
CD N•
o,
TKN
mg/kg
Z
o
ua o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/12
40500
1.89
0.146
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
7.094
NA
Fescue
4/13
40500
1.89
0.146
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
7.094
NA
Fescue
4/14
40500
1.89
0.146
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
7.094
NA
Fescue
4/15
31500
1.89
0.114
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
5.518
NA
Fescue
4/21
31500
1.89
0.114
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
1 5.518
NA
Fescue
4/22
36000
1.89
0.130
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
6.306
NA
Fescue
4/24
36000
1.89
0.130
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
6.306
NA
Fescue
4/25
36000
1.89
0.130
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
6.306
NA
Fescue
4/26
36000
1.89
0.130
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
6.306
NA
Fescue
4/27
13500
1.89
0.049
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
2.365
NA
Fescue
5/19
97500
1.89
0.352
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
17.079
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
01
439500
1.5891
1
1
1
76.986
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied (Annual): 13.21
Permit #: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series: MrB2
Acres Used: 17.09 Acres Permitted: 17.09 Site #: NC-DV08 Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Solon
0
Total
Phos-
phomsMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEW
ao
0
o
o
•D
--
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
ro
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
Total
' •
• •
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
• •
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 8 Acres Utilized: 17.09
Land Owner: Roger Spillman Annual Dry Tons Applied: 13.21 Site #: NC-DV08 Acres Permitted: 17.09
Operator: Roger Spillman Predominant Soil Series: MrB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
met'
Moist)
Precip.
Past 24
Hrs.
inches,
a
co S
0 w
* °�
o
-
N
o
7
w
N
o
TKN
mg/kg
Z a
;
o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/18/22
143000
1.09
0.380
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
26.483
NA
Fescue
10/19/22
84500
1.09
0.225
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
15.649
NA
Fescue
12/28/23
18000
1.09
0.048
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
3.334
NA
Fescue
12/29/23
45000
1.09
0.120
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
8.334
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
29050o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
53.799T
0.000
Lime Applied
Annuallbs/acre
0.0337
0.0028
0.5875
0.0481
0.0352
0.0009
0.0190
0.0328
0.0450
1.2662
44.679
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.4620
0.1810
18.1950
5.0050
4.2100
0.0930
0.6870
2.3620
0.4720
72.5300
Current Cumulative lbs/ac
0.4957
0.1838
18.7825
5.0531
4.2452
0.0939
0.7060
2.3948
0.5170
73.7962
Permitted C. P. L. R. * * * *
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 141
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
L•�'� 2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
Total Dry Tons Applied (Annual):
WQ0003351 Cation Exchange Capacity (non 503 only):
Greg Dooley Owner: Greg Dooley Predominant Soil Series:
9.7 Acres Permitted: 9.7 Site #: NC -DV 11 Field #:
16.28
CfB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phomsMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
�
mammon
NOOS
E
Event
1 1::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1::
ro
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1::
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
:: •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:: •
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z. I z 4; �; �e_
2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:
Land Owner:
Operator:
Town of Mocksville
Greg Dooley
Greg Dooley
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0003351 Field #:
Annual Dry Tons Applied: 16.28 Site #:
Predominant Soil Series: CfB2
Crop 1 Max. PAN:
209
Crop 2 Name:
Acres Utilized:
NC-DV11 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
9.7
9.7
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
Wet'
Moist)
Precip.
Past 24
Hrs.
inches,
a
4 -z:;
co S
0 w
* °�
o
-
N
o
7 �
w
N
o
TKN
mg/kg
Z a
.;
o o
CD �
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/6/22
36000
1.89
0.293
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
14.172
NA
Fescue
6/7/22
13500
1.89
0.110
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
5.315
NA
Fescue
6/13/22
13000
1.89
0.106
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
5.118
NA
Fescue
6/14/22
27000
1.89
0.219
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
10.629
NA
Fescue
6/15/22
49500
1.89
0.402
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
19.487
NA
Fescue
6/16/22
40500
1.89
0.329
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
15.944
NA
Fescue
6/17/22
27000
1.89
0.219
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
10.629
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
206500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
81.294
0.000
Lime Applied
Annuallbs/acre
0.088
0.018
0.540
0.079
0.071
0.001
0.044
0.044
0.088
1.467
81.886
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.035
0.004
0.114
0.024
0.013
0.001
0.011
0.024
0.041
0.468
Current Cumulative lbs/ac
0.123
0.022
0.654
0.103
0.084
0.002
0.055
0.068
0.129
1.935
Permitted C. P. L. R. * * * *
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 209
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
;d-e j *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
Total Dry Tons Applied (Annual):
WQ0003351 Cation Exchange Capacity (non 503 only):
Greg Dooley Owner: Greg Dooley Predominant Soil Series:
10.4 Acres Permitted: 10.4 Site #: NC -DV 11 Field #:
12.05
FcC2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phomsMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
D
mammon
NOOSE
Event
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
• •
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
• •
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z. I z 4; �; �e_
2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 2 Acres Utilized: 10.4
Land Owner: Greg Dooley Annual Dry Tons Applied: 12.05 Site #: NC-DV11 Acres Permitted: 10.4
Operator: Greg Dooley Predominant Soil Series: CfB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 118 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
Wet'
Moist)
Precip.
Past 24
Hrs.
inches,
a
4 -z:;
co S
0 w
* °�
o
-
N
o
7 �
w
N
o
TKN
mg/kg
Z a
.;
o o
CD �
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/20/22
22500
1.89
0.171
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
8.261
NA
Fescue
6/21/22
36000
1.89
0.273
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
13.218
NA
Fescue
6/22/22
31500
1.89
0.239
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
11.566
NA
Fescue
6/23/22
27000
1.89
0.205
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
9.914
NA
Fescue
6/28/22
36000
1.89
0.273
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
13.218
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
0
1530001
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
56.178
0.000
Lime Applied
Annuallbs/acre
0.061
0.012
0.373
0.054
0.049
0.001
0.031
0.031
0.061
1.013
56.559
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.061
0.012
0.373
0.054
0.049
0.001
0.031
0.031
0.061
1.013
Permitted C. P. L. R. * * * *
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 118
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
;d-e j *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied (Annual): 24.55
Permit #:
Operator:
Acres Used:
WQ0003351 Cation Exchange Capacity (non 503 only):
Arthur Rupard Owner: CB Rupard Heirs Predominant Soil Series: MsB - Mocksville
12.04 Acres Permitted: 12.04 Site #: NC-MKO1 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
4/6/22
2 1
8/3/22
3
4
5
6
7
8
9
10
11
12
% Solids
1.89
1.05
Arsenic
26.3
24
Cadmium
5.26
2
Copper
161
188
Chromimn
23.4
23.6
Lead
21.1
18
Mercury
0.335
0.68
Molyb-
denum
13.2
13.5
Nickel
13.2
12.1
Selenium
26.3
32
Zinc
437
461
Total
Phos-
horns
24400
32700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
D
mammon
NOOSE
Event
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
ro
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 •:
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®
1:
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
•1 ••
1111
1 111
1111
1111
1 111
1 111
1111
1111
1 111
1111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/2/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 2 Acres Utilized: 12.04
Land Owner: CB Rupard Heirs Annual Dry Tons Applied: 24.55 Site #: NC-MKO1 Acres Permitted: 12.04
Operator: Arthur Rupard Predominant Soil Series: MsB - Mocksville Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 167 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
met'
Moist)
Precip.
Past 24
Hrs.
inches,
a
co S
0 w
* °�
o
-
N
o
7
w
N
o
TKN
mg/kg
Z a
;
o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/31/22
36000
1.89
0.236
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
11.418
NA
Fescue
6/l/22
54000
1.89
0.353
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
17.127
NA
Fescue
6/2/22
54000
1.89
0.353
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
17.127
NA
Fescue
6/3/22
45000
1.89
0.295
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
14.272
NA
Fescue
8/26/22
49500
1.05
0.180
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
11.692
NA
Fescue
8/29/22
63000
1.05
0.229
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
14.881
NA
Fescue
8/30/22
63000
1.05
0.229
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
14.881
NA
Fescue
8/31/22
4500
1.05
0.016
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
1.063
NA
Fescue
9/l/22
40500
1.05
0.147
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
9.566
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
40950o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
i i2.o27T
0.000
Lime Applied
Annuallbs/acre
0.1036
0.0162
0.6999
0.0957
0.0811
0.0019
0.0543
0.0521
0.1164
1.8206
112.816
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.2800
0.1616
12.0997
0.9960
2.3033
0.0543
0.6962
1.1581
0.3538
44.1340
Current Cumulative lbs/ac
0.3836
0.1778
12.7996
1.0917
2.3844
0.0562
0.7505
1.2102
0.4702
45.9546
Permitted C. P. L. R. * * * *
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 167
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
L•�'� 2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
WQ0003351
Jeff Smith Owner:
4.12 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Town of Mocksville Predominant Soil Series:
4.12 Site #: NC-MK05 Field #:
17.22
CeB2 - Cecil
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
1/24/22
2 1
4/6/22
3
4
5
6
7
8
9
10
11
12
% Solids
1.77
1.89
Arsenic
13.3
26.3
Cadmium
1.11
5.26
Copper
187
161
Chromiurn
23.9
23.4
Lead
17
21.1
Mercury
0.346
0.335
Molyb-
denum
7.5
13.2
Nickel
11.9
13.2
Selenium
17.8
26.3
Zinc
594
437
Total
Phos-
horns
19500
24400
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
D
mammon
NOOSE
Event
1 1
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
ro
1 11
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1•
1 :1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 1••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
��
1 1 1
1 1••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1.1
�
1111
1 111
1111
1111
1 111
1 111
1111
1111
1 111
1111
1 •
®�®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
•• 1
••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z.lz 2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized: 4.12
Land Owner: Town of Mocksville Annual Dry Tons Applied: 17.22 Site #: NC-MK05 Acres Permitted: 4.12
Operator: Jeff Smith Predominant Soil Series: CeB2 - Cecil Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
Wet'
Moist)
Precip.
Past 24
Hrs.
inches,
a
co
w
* °�
o
-
N
o
7
w
N
o
TKN
mg/kg
Z a
.;
o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/28/22
4500
1.77
0.081
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
1 78900
6170
1 405
4.081
NA
Fescue
1/31/22
22500
1.77
0.403
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
20.403
NA
Fescue
2/l/22
27000
1.77
0.484
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
24.484
NA
Fescue
2/2/22
40500
1.77
0.726
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
36.726
NA
Fescue
5/17/22
71500
1.89
1.368
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
75800
6160
254
66.270
NA
Fescue
5/18/22
58500
1.89
1.119
Dutchman's Creek
Dry
<.5"
S
0.5
1 0.3
75800
1 6160
254
54.221
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
224500
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
2o6.185
0.00o
Lime A lied
Annuallbs/acre
0.176
0.030
1.434
0.197
0.163
0.003
0.091
0.106
0.191
4.185
187.393
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.54
0.117
11.567
1.996
1.59
0.055
0.425
1.438
0.618
36.955
Current Cumulative lbs/ac
0.716
0.147
13.001
2.193
1.753
0.058
0.516
1.544
0.809
41.140
Permitted C. P. L. R. * * * *
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 209
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
j *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
WQ0003351
Jeff Smith Owner:
4.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Town of Mocksville Predominant Soil Series:
4.6 Site #: NC-MK05 Field #:
15.97
CfB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phomsmMENEEMENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
TotalNEW
a
D
mammon
NOOSE
Event
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
ro
1 11 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 •
1 •
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
11
��
Isfi'iiL'yiii�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1••
1 1•
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
��
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 1•:
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
• 1
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
1 1 •
•
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z.lz 2/2/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 2 Acres Utilized: 4.6
Land Owner: Town of Mocksville Annual Dry Tons Applied: 15.97 Site #: NC-MK05 Acres Permitted: 4.6
Operator: Jeff Smith Predominant Soil Series: CfB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
Soil
Cond.
D
Wet'
Moist)
Precip.
Past 24
Hrs.
inches,
a
co
w
* °�
o
-
N
o
7
w
N
o
TKN
mg/kg
Z a
.;
o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/26/22
36000
1.77
0.578
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
1 78900
6170
1 405
29.239
NA
Fescue
1/27/22
31500
1.77
0.505
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
25.584
NA
Fescue
1/28/22
27000
1.77
0.433
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
21.929
NA
Fescue
3/2/22
36000
1.77
0.578
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
29.239
NA
Fescue
3/3/22
40500
1.77
0.650
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
78900
6170
405
32.894
NA
Fescue
8/24/22
40500
1.05
0.385
Dutchman's Creek
Dry
<.5"
S
0.5
1 0.3
87500
1 7230
4780
25.039
NA
Fescue
8/25/22
36000
1.05
0.343
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
87500
7230
4780
22.257
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
0
2475001
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
186.180
o.000
Lime Applied
Annuallbs/acre
0.108
0.009
1.300
0.166
0.120
0.003
0.061
0.083
0.144
3.931
154.627
Date
lbs/ac
Prior Years Cumulative lbs/ac
1.956
0.254
3.645
12.355
12.113
0.41
0.202
3.825
1.614
11.829
Current Cumulative lbs/ac
2.064
0.263
4.945
12.521
12.233
0.413
0.263
3.908
1.758
15.760
Permitted C. P. L. R. * * * *
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 1 209
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
j *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/2/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
2/2/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-025-0021
Client Project Description: Dutchman's Creek
Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1 /25/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-025-0021
Page 2 of 9

Waypoint 27(2) 90 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypoin ta nalytical. cam
Sample Summary Table
Report Number: 22-025-0021
Client Project Description: Dutchman's Creek
Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
9IS81 Dutchman's Creek Solids 01/24/2022 08:00 01/2S/2022
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Dutchman's Creek
Lab Report Number: 22-025-0021
Date: 2/1 /2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99187
Analyte: Aluminum
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Calcium
QC Batch No: L597088/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Copper
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Iron
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Potassium
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99187
Analyte: Magnesium
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Manganese
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Analyte: Phosphorus
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Lead
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Sulfur
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Zinc
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

s
•
2790 Whitten Road, Memphis, TN 38133
Waypoint
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Dutchman's Creek
Mr. Brent Collins Report Date : 02/02/2022
755 Yadkinville Rd Information : Mocksville, NC Received : 01/25/2022
Mocksville , NC 27028 0
�' `�'-C7•'t� Qk3�
Report Number :22-025-0021 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 91581
Matrix: Solids
Sample ID : Dutchman's Creek
Sampled:
1/24/2022
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.2
%
0.010
1
01/26/22 16:41
FMM
SW-DRYWT
Ammonia Nitrogen
6170
mg/Kg - dry
889
5560
1
02/01/22 14:00
]P]
4500NH3C-2011
Nitrate+Nitrite-N
405
mg/Kg - dry
263
263
1
02/01/22 14:47
ZBD
4500NO3F-2011
Organic N
72720
mg/Kg - dry
888.9
5556
1
01/31/22 10:00
CALCULATION
pH
6.4
S.U.
1
01/31/2215:39
DRS
9045D
Total Solids
1.77
%
0.010
0.010
1
01/26/22 16:41
FMM
2540G-2011
Total Volatile Solids
72.9
%
0.010
0.010
1
01/26/22 16:41
FMM
2540G-2011
Total Kjeldahl Nitrogen
78900
mg/Kg - dry
556
13900
1
01/31/22 10:00
]P] iM-4500-NH3C-TKP
Phosphorus
19500
mg/Kg - dry
153
278
1
01/28/22 05:40
EAL
6010D
Aluminum
10600
mg/Kg - dry
257
278
1
01/28/22 05:40
EAL
6010D
Arsenic
<13.3
mg/Kg - dry
13.3
27.8
1
01/28/22 05:40
EAL
6010D
Cadmium
<1.11
mg/Kg - dry
1.11
5.56
1
01/28/22 05:40
EAL
6010D
Calcium
19600
mg/Kg - dry
2150
2780
1
01/28/22 05:40
EAL
6010D
Chromium
23.9
mg/Kg - dry
13.1
13.9
1
01/28/22 05:40
EAL
6010D
Copper
187
mg/Kg - dry
17.2
27.8
1
01/28/22 05:40
EAL
6010D
Iron
17600
mg/Kg - dry
473
556
1
01/28/22 05:40
EAL
6010D
Lead
17.0
mg/Kg - dry
10.0
16.7
1
01/28/22 05:40
EAL
6010D
Magnesium
3770
mg/Kg - dry
143
278
1
01/28/22 05:40
EAL
6010D
Manganese
989
mg/Kg - dry
18.1
27.8
1
01/28/22 05:40
EAL
6010D
Mercury
<0.346
mg/Kg - dry
0.346
0.794
1
01/26/22 17:16
]W2
7471A
Molybdenum
<7.50
mg/Kg - dry
7.50
13.9
1
01/28/22 05:40
EAL
6010D
Nickel
11.93
mg/Kg - dry
6.67
13.9
1
01/28/22 05:40
EAL
6010D
Potassium
6000
mg/Kg - dry
343
556
1
01/28/22 22:03
EAL
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 6 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 22-025-0021
Lab No : 91581
Sample ID : Dutchman's Creek
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Dutchman's Creek
Information : Mocksville, NC
REPORT OFANALYSIS
Report Date : 02/02/2022
Received, (: 01/25/2022
�' `�'-C7•'t� Qk3�
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/24/2022 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<17.8
mg/Kg - dry
17.8
27.8
1
01/28/22 22:03
EAL
6010D
Sodium
9780
mg/Kg - dry
722
1390
1
01/28/22 05:40
EAL
6010D
Zinc
594
mg/Kg - dry
45.0
69.4
1
01/28/22 05:40
EAL
6010D
Sulfur
9830
mg/Kg - dry
288
556
1
01/28/22 05:40
EAL
6010D
Sodium Absorption Ratio
2.24
Ratio
0.01
0.01
1
01/28/22 05:40
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

poi ��"' 2790 Whiten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT (CAL www.waypoiritanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-025-0021
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T137
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes # No
Comments:
Signature: Imakayla Weaver Date & Time: 01 /25/2022 09:04:46
Page 8 of 9

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1 /24/2022
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
9780
173.106
23 7.526348
Calcium
19600
346.92
20 17.346
Magnesium
3770
66.729
12 5.56075
Percent Solids
1.77
SAR
2.22
SAR =
Na+
2 (Ca2+ + Mg2+)
7.52635
0.5( 17.346 2 + 5.56075 2 )

Waypointo
ANALYTICAL
4/15/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-097-0045
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/7/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-097-0045
Page 2 of 9

Waypoint 27(2) 90 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypoin ta nalytical. cam
Report Number: 22-097-0045
Client Project Description: Mocksville, NC
Lab No Client Sample ID
89653 Mocksville
Sample Summary Table
Matrix Date Collected
Solids 04/06/2022 09:15
Date Received
04/07/2022
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 22-097-0045
Date: 4/15/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99495 (SS-1)
Analyte: Arsenic
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99495 (SS-1)
Analyte: Calcium
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Iron
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Potassium
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Magnesium
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Manganese
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Phosphorus
QC Batch No: L610642/L609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Analyte: Lead
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Mocksville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 04/15/2022
Received : 04/07/2022
Connie Cook
Report Number :22-097-0045
REPORT OFANAL YSIS
Project
Manager
Lab No : 89653
Matrix:
Solids
Sample ID : Mocksville
Sampled:
4/6/2022
9:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.1
%
1
04/07/22 16:58
FMM
SW-DRYWT
Ammonia Nitrogen
6160
mg/Kg - dry
842
5260
1
04/14/22 14:30
]P]
4500NH3C-2011
Nitrate+Nitrite-N
<254
mg/Kg - dry
254
254
1
04/14/22 15:34
ZBD
4500NO3F-2016
Organic N
69630
mg/Kg - dry
842.1
5263
1
04/14/22 09:30
CALCULATION
pH
7.1
S.U.
1
04/14/2216:03
DRS
9045D
Total Solids
1.89
%
0.010
0.010
1
04/07/22 16:58
FMM
2540G-2011
Total Volatile Solids
76.3
%
0.010
0.010
1
04/07/22 16:58
FMM
2540G-2011
Total Kjeldahl Nitrogen
75800
mg/Kg - dry
526
13200
1
04/14/22 09:30
]P] iM-4500-NH3C-TKP
Phosphorus
24400
mg/Kg - dry
145
263
1
04/12/22 23:32
TJS
6010D
Aluminum
12400
mg/Kg - dry
243
263
1
04/13/22 13:40
T]S
6010D
Arsenic
<26.3
mg/Kg - dry
12.6
26.3
1
04/12/22 23:32
TJS
6010D
Cadmium
<5.26
mg/Kg - dry
1.05
5.26
1
04/12/22 23:32
T]S
6010D
Calcium
13700
mg/Kg - dry
2040
2630
1
04/12/22 23:32
TJS
6010D
Chromium
23.4
mg/Kg - dry
12.4
13.2
1
04/12/22 23:32
T]S
6010D
Copper
161
mg/Kg - dry
16.3
26.3
1
04/12/22 23:32
TJS
6010D
Iron
16900
mg/Kg - dry
448
526
1
04/12/22 23:32
T]S
6010D
Lead
21.1
mg/Kg - dry
9.47
15.8
1
04/12/22 23:32
TJS
6010D
Magnesium
4460
mg/Kg - dry
136
263
1
04/12/22 23:32
T]S
6010D
Manganese
905
mg/Kg - dry
17.1
26.3
1
04/12/22 23:32
TJS
6010D
Mercury
<0.335
mg/Kg - dry
0.335
0.768
1
04/14/22 14:33
ZMT
7471A
Molybdenum
<13.2
mg/Kg - dry
7.11
13.2
1
04/12/22 23:32
TJS
6010D
Nickel
<13.2
mg/Kg - dry
6.32
13.2
1
04/12/22 23:32
T]S
6010D
Potassium
7740
mg/Kg - dry
325
526
1
04/12/22 23:32
TJS
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions I
Estimated value
MQL
Method Quantitation
Limit
Page 6 of 9

s
•
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main
901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 04/15/2022
755 Yadkinville Rd
Information :
Received : 04/07/2022
Mocksville , NC 27028
Connie Cook
Report Number :22-097-0045
REPORT OFANAL
YSIS
Project Manager
Lab No : 89653
Matrix: Solids
Sample ID : Mocksville
Sampled: 4/6/2022 9:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<26.3
mg/Kg - dry
16.8
26.3 1 04/12/22 23:32 TJS 6010D
Sodium
8950
mg/Kg - dry
684
1320 1 04/12/22 23:32 T]S 6010D
Zinc
437
mg/Kg - dry
42.6
65.8 1 04/12/22 23:32 TJS 6010D
Sulfur
10800
mg/Kg - dry
273
526 1 04/13/22 13:40 T]S 6010D
Sodium Absorption Ratio
2.33
Ratio
0.01
0.01 1 04/12/22 23:32 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 7 of 9

poi ��"' 2790 Whiten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT (CAL www.waypoiritanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-097-0045
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T102
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes # No
Comments:
Signature: Imakayla Weaver Date & Time: 04/07/2022 10:49:04
Page 8 of 9

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Page 9 of 9

4/6/2022
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
8950
169.155
23 7.354565
Calcium
13700
258.93
20 12.9465
Magnesium
4460
84.294
12 7.0245
Percent Solids
1.89
SAR
2.33
SAR =
Na+
2 (Ca2+ + Mg2+)
7.35457
0.5( 12.947 2 + 7.02450 2 )

Waypointo
ANALYTICAL
8/11 /2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-216-0027
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/4/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-216-0027
Page 2 of 8

Waypoint 27(2) 90 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypoin ta nalytical. cam
Report Number: 22-216-0027
Client Project Description: Mocksville, NC
Lab No Client Sample ID
94983 Mocksville
Sample Summary Table
Matrix Date Collected
Solids 08/03/2022 06:40
Date Received
O8/04/2022
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 22-216-0027
Date: 8/11 /2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99623 (Sludge Vector 1 Dup.)
Analyte: Aluminum
QC Batch No: L630653/L630360
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99623 (Sludge Vector 1 Dup.)
Analyte: Potassium
QC Batch No: L630653/L630360
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99623 (Sludge Vector 1 Dup.)
Analyte: Sulfur
QC Batch No: L630653/L630360
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 94983 (Mocksville)
Analyte: Mercury
QC Batch No: L630902/L630456
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Mocksville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 08/11/2022
Received : 08/04/2022
Connie Cook
Report Number :22-216-0027
REPORT OFANAL YSIS
Project
Manager
Lab No : 94983
Matrix:
Solids
Sample ID : Mocksville
Sampled:
8/3/2022
6:40
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
99.0
%
1
08/08/22 16:08
FMM
SW-DRYWT
Ammonia Nitrogen
72303
mg/Kg - dry
1600
10000
1
08/11/22 12:30
]P]
4500NH3C-2011
Nitrate+Nitrite-N
4780
mg/Kg - dry
495
495
1
08/09/22 14:33
ZBD
4500NO3F-2016
Organic N
802703
mg/Kg - dry
1600
10000
1
08/11/22 09:00
CALCULATION
pH
5.7
S.U.
1
08/11/2215:11
DRS
9045D
Total Solids
1.05
%
0.010
0.010
1
08/08/22 16:08
FMM
2540G-2011
Total Volatile Solids
68.9
%
0.010
0.010
1
08/08/22 16:08
FMM
2540G-2011
Total Kjeldahl Nitrogen
87500
mg/Kg - dry
1000
25000
1
08/11/22 09:00
]P] iM-4500-NH3C-TKP
Phosphorus
32700
mg/Kg - dry
276
500
1
08/05/22 20:04
EAL
6010D
Aluminum
11300
mg/Kg - dry
462
500
1
08/05/22 20:04
EAL
6010D
Arsenic
<24.0
mg/Kg - dry
24.0
50.0
1
08/05/22 20:04
EAL
6010D
Cadmium
<2.00
mg/Kg - dry
2.00
10.0
1
08/05/22 20:04
EAL
6010D
Calcium
13700
mg/Kg - dry
3870
5000
1
08/05/22 20:04
EAL
6010D
Chromium
<23.6
mg/Kg - dry
23.6
25.0
1
08/05/22 20:04
EAL
6010D
Copper
188
mg/Kg - dry
31.0
50.0
1
08/05/22 20:04
EAL
6010D
Iron
16800
mg/Kg - dry
852
1000
1
08/05/22 20:04
EAL
6010D
Lead
<18.0
mg/Kg - dry
18.0
30.0
1
08/05/22 20:04
EAL
6010D
Magnesium
7300
mg/Kg - dry
258
500
1
08/05/22 20:04
EAL
6010D
Manganese
816
mg/Kg - dry
32.5
50.0
1
08/05/22 20:04
EAL
6010D
Mercury
<0.680
mg/Kg - dry
0.680
15.6
1
08/08/22 12:14
T]S
7471A
Molybdenum
<13.5
mg/Kg - dry
13.5
25.0
1
08/05/22 20:04
EAL
6010D
Nickel
12.13
mg/Kg - dry
12.0
25.0
1
08/05/22 20:04
EAL
6010D
Potassium
12000
mg/Kg - dry
618
1000
1
08/05/22 20:04
EAL
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

s
•
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main
901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 08/11/2022
755 Yadkinville Rd
Information :
Received : 08/04/2022
Mocksville , NC 27028
Connie Cook
Report Number :22-216-0027
REPORT OFANAL
YSIS
Project Manager
Lab No : 94983
Matrix: Solids
Sample ID : Mocksville
Sampled: 8/3/2022 6:40
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<32.0
mg/Kg - dry
32.0
50.0 1 08/05/22 20:04 EAL 6010D
Sodium
17000
mg/Kg - dry
1300
2500 1 08/05/22 20:04 EAL 6010D
Zinc
461
mg/Kg - dry
81.0
125 1 08/05/22 20:04 EAL 6010D
Sulfur
12900
mg/Kg - dry
518
1000 1 08/05/22 20:04 EAL 6010D
Sodium Absorption Ratio
2.91
Ratio
0.01
0.01 1 08/05/22 20:04 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

poi ��"' 2790 Whiten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT (CAL www.waypoiritanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-216-0027
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T102
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes # No
Comments:
Signature: Imakayla Weaver Date & Time: 08/04/2022 09:52:53
Page 7 of 8

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Page 8 of 8

8/3/2022
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 17000 178.5 23 7.76087
Calcium 13700 143.85 20 7.1925
Magnesium 7300 76.65 12 6.3875
Percent Solids 1.05
SAR 2.98
SAR =
Na+
2 (Ca2+ + Mg2+)
7.76087
0.5( 7.1925 2 + 6.38750 2 )

Waypointo
ANALYTICAL
10/18/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-280-0047
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/7/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

ANALYTICAL
Waypointo
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/22-280-0047
Page 2 of 8

Waypoint,(D
ANALYTICAL
Report Number: 22-280-0047
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received
94062 Mocksville
Solids 10/06/202211:45 10/07/2022
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 22-280-0047
Date: 10/18/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 94251 (SW Cake)
Analyte: Aluminum
QC Batch No: L643164/L642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Iron
QC Batch No: L643299/L642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Potassium
QC Batch No: L643164/L642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Sulfur
QC Batch No: L643566/L642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Mocksville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 10/18/2022
Received : 10/07/2022
Connie Cook
Report Number : 22-280-0047
REPORT OFANALY .15
Project
Manager
Lab No : 94062
Matrix:
Solids
Sample ID : Mocksville
Sampled:
10/6/2022
11:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.9
%
1
10/12/22 15:33
FMM
SW-DRYWT
Ammonia Nitrogen
6080 ]
mg/Kg - dry
1450
9090
1
10/17/22 15:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
7920
mg/Kg - dry
450
450
1
10/08/22 11:32
ZBD
4500NO3F-2016
Organic N
79550 ]
mg/Kg - dry
1455
9091
1
10/17/22 10:00
CALCULATION
pH
5.6
S.U.
1
10/14/2215:03
SAR
9045D
Total Solids
1.09
%
0.010
0.010
1
10/12/22 15:33
FMM
2540G-2011
Total Volatile Solids
68.0
%
0.010
0.010
1
10/12/22 15:33
FMM
2540G-2011
Total Kjeldahl Nitrogen
85600
mg/Kg - dry
909
22700
1
10/17/22 10:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
28900
mg/Kg - dry
251
455
1
10/14/22 03:14
TJS
6010D
Aluminum
16200
mg/Kg - dry
420
455
1
10/14/22 03:14
TJS
6010D
Arsenic
<21.8
mg/Kg - dry
21.8
45.5
1
10/14/22 18:00
EAL
6010D
Cadmium
<1.82
mg/Kg - dry
1.82
9.09
1
10/14/22 03:14
TJS
6010D
Calcium
27800
mg/Kg - dry
3520
4550
1
10/14/22 03:14
TJS
6010D
Chromium
31.1
mg/Kg - dry
21.5
22.7
1
10/14/22 03:14
TJS
6010D
Copper
380
mg/Kg - dry
28.2
45.5
1
10/14/22 03:14
TJS
6010D
Iron
23500
mg/Kg - dry
775
909
1
10/14/22 03:14
TJS
6010D
Lead
22.8]
mg/Kg - dry
16.4
27.3
1
10/14/22 03:14
TJS
6010D
Magnesium
6350
mg/Kg - dry
235
455
1
10/14/22 03:14
TJS
6010D
Manganese
973
mg/Kg - dry
29.5
45.5
1
10/14/22 03:14
TJS
6010D
Mercury
<0.606
mg/Kg - dry
0.606
13.9
1
10/11/22 12:45
TJS
7471A
Molybdenum
<12.3
mg/Kg - dry
12.3
22.7
1
10/14/22 03:14
TJS
6010D
Nickel
21.2]
mg/Kg - dry
10.9
22.7
1
10/14/22 03:14
TJS
6010D
Potassium
9050
mg/Kg - dry
562
909
1
10/14/22 03:14
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

■
Waypoint
2790 Whitten Road, Memphis, TN 38133
Main
901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville,
NC
Mr. Brent Collins
Report Date : 10/18/2022
755 Yadkinville Rd
Information :
Received : 10/07/2022
Mocksville , NC 27028
Connie Cook
Report Number : 22-280-0047
REPORT OFANALY .15
Project Manager
Lab No : 94062
Matrix: Solids
Sample ID : Mocksville
Sampled: 10/6/2022 11:45
Test
Results
Units
MDL
MOL DF Date / Time By Analytical
Analyzed Method
Selenium
<29.1
mg/Kg - dry
29.1
45.5 1 10/14/22 18:00 EAL 6010D
Sodium
14700
mg/Kg - dry
1180
2270 1 10/14/22 03:14 TJS 6010D
Zinc
819
mg/Kg - dry
73.6
114 1 10/14/22 03:14 TJS 6010D
Sulfur
14500
mg/Kg - dry
471
909 1 10/17/22 23:42 EAL 6010D
Sodium Absorption Ratio
2.17
Ratio
0.01
0.01 1 10/14/22 03:14 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

poi ��"' 2790 Whiten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT (CAL www.waypoiritanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-280-0047
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T102
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes # No
Comments:
Signature: Imakayla Weaver Date & Time: 10/07/2022 11:01:55
Page 7 of 8

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Page 8 of 8

10/6/2022
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
14700
160.23
23 6.966522
Calcium
27800
303.02
20 15.151
Magnesium
6350
69.215
12 5.767917
Percent Solids
1.09
SAR
2.15
SAR =
Na+
2 (Ca2+ + Mg2+)
6.96652
0.5( 15.151 2 + 5.76792 2 )

aceRnalj4ical
i
V
4
N l"'ffi'
ANALYTICAL REPORT
February 07, 2022
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1454549
01/25/2022
Sludge
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accwacy of the information provided,
and as the samples are received.
-
Ilk
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
rMA Resources L1454549 02/07/22 16:05 1 of 21

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
DUTCHMAN'S CREEK L1454549-01
5
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
Wet Chemistry by Method D93/1010A
10
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: S DG:
DATE/TIME: PAGE:
EMA Resources L1454549
02/07/22 16:05 2 of 21

DUTCHMAN'S CREEK L1454549-01 Waste
Collected by
Brent Collins
Collected date/time
01/24/2208:00
Received date/time
01/25/2209:15
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1808840
1 01/27/2210:39
01/27/2210:39
JWS
Mt. Juliet, TN
Preparation by Method 1311
WG1809554
1 01/28/2212:49
01/28/2212:49
CJW
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1808566
1 01/30/2211:27
02/01/2214:38
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1809680
1 01/31/2216:00
02/01/22 22:00
SAC
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1808419
1 01/26/2214:00
01/27/22 09:00
GI
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1812928
1 02/04/22 01:08
02/04/22 01:08
WOS
Mt. Juliet, TN
Mercury by Method 7470A
WG1810317
1 01/30/22 09:32
01/31/22 09:35
MRW
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1810384
1 02/01/22 00:24
02/01/22 23:48
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1810127
1 01/29/2216:06
01/29/2216:06
JAH
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1811223
1 02/02/22 08:09
02/03/2211:44
AO
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1809205
1 02/03/22 06:33
02/03/2215:47
AO
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1809535
1 01/30/2216:30
01/31/22 05:50
JNJ
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
LMA Resources L1454549 02/07/2216:05 3 of21

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the [—CP]
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples 17C
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my ISS]
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
I
Sr
5
_QC]
GI
Justin Carr CAI
Project Manager Project Narrative I _SC
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
rMA Resources L1454549 02/07/2216:05 4 of21

SAMPLE RESULTS - 01
L1454549
DUTCHMAN'S CREEK
Collected date/time: 01/24/22 08:00
Preparation by Method 1311
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
1/27/202210:39:54 AM
WG1208840
TCLP ZHE Extraction
- 1/28/202212:49:36 PM
WG1209554
Fluid
1 1/27/202210:39:54 AM
WG1208840
Initial pH
7.01 1/27/202210:39:54 AM
WG1208840
Final pH
4.99 1/27/202210:39:54 AM
WG1208840
Wet Chemistry by Method 9012 B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.250
Wet Chemistry by Method 9034-9030B
Dilution Analysis Batch
date / time
1 02/01/202214:38 WG1808566
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Sulfide ND 25.0 1 02/01/2022 22:00 WG1809680
Wet Chemistry by Method 9045D
Result Qualifier Dilution Analysis
Analyte so date / time
Corrosivity by pH 7.19 T8 1 01/27/2022 09:00
Sample Narrative:
L1454549-01 WG1808419: 7.19 at 18C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at 200
Mercury by Method 7470A
Batch
WG1808419
Qualifier Dilution Analysis Batch
date/time
1 02/04/2022 01:08 WG1812928
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
LMA Resources
Dilution Analysis
date / time
1 01/31/2022 09:35
Batch
WG1810317
Dilution Analysis
Batch
date / time
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
1 02/01/2022 23:48
WG1810384
Dilution Analysis
Batch
date / time
1 01/29/202216:06
WG1810127
1 01/29/202216:06
WG1810127
1 01/29/202216:06
WG1810127
1 01/29/202216:06
WG1810127
SDG:
DATE/TIME: PAGE:
L1454549
02/07/22 16:05 5 of 21

DUTCHMAN'S CREEK
SAMPLE RESULTS
- 01
Collected date/time: 01/24/22 08:00
L1454549
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1
01/29/202216:06
WG1810127
1,1-Dichloroethene
ND
0.0500
0.70
1
01/29/202216:06
WG1810127
2-Butanone (MEK)
ND
0.500
200
1
01/29/202216:06
WG1810127
Tetrachloroethene
ND
0.0500
0.70
1
01/29/202216:06
WG1810127
Trichloroethene
ND
0.0500
0.50
1
01/29/2022 16:06
WG1810127
Vinyl chloride
ND
0.0500
0.20
1
01/29/202216:06
WG1810127
(S) Toluene-d8
90.9
80.0-120
011291202216:06
WG1810127
(S)4-Bromofluorobenzene
94.5
77.0-126
011291202216:06
WG1810127
(S)1,2-Dichloroethane-d4
89.5
70.0-130
011291202216:06
WG1810127
Chlorinated Acid Herbicides (GC) by
Method 8151A
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1
02/03/202211:44
WG1811223
2,4-D
ND
0.00200
10
1
02/03/202211:44
WG1811223
(S) 2,4-Dichlorophenyl Acetic Acid
71.2
14.0-158
021031202211:44
WG1811223
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1
02/03/202215:47
WG1809205
Endrin
ND
0.00500
0.02
1
02/03/202215:47
WG1809205
Heptachlor
ND
0.00500
0.0080
1
02/03/202215:47
WG1809205
Heptachlor epoxide
ND
0.00500
0.0080
1
02/03/202215:47
WG1809205
Lindane
ND
0.00500
0.40
1
02/03/202215:47
WG1809205
Methoxychlor
ND
0.00500
10
1
02/03/202215:47
WG1809205
Toxaphene
ND
0.0100
0.50
1
02/03/202215:47
WG1809205
(S) Decochlorobiphenyl
93.6
10.0-128
021031202215:47
WG1809205
(S) Tetrochloro-m-xylene
93.3
10.0-127
021031202215:47
WG1809205
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
01/31/2022 0550
WG1809535
2,4-Dinitrotoluene
ND
0.100
0.13
1
01/31/2022 0550
WG1809535
Hexachlorobenzene
ND
0.100
0.13
1
01/31/2022 0550
WG1809535
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
01/31/2022 0550
WG1809535
Hexachloroethane
ND
0.100
3
1
01/31/2022 0550
WG1809535
Nitrobenzene
ND
0.100
2
1
01/31/2022 0550
WG1809535
Pyridine
ND
0.100
5
1
01/31/2022 0550
WG1809535
3&4-Methyl Phenol
ND
0.100
400
1
01/31/2022 0550
WG1809535
2-Methylphenol
ND
0.100
200
1
01/31/2022 0550
WG1809535
Pentachlorophenol
ND
0.100
100
1
01/31/2022 0550
WG1809535
2,4,5-Trichlorophenol
ND
0.100
400
1
01/31/2022 0550
WG1809535
2,4,6-Trichlorophenol
ND
0.100
2
1
01/31/2022 0550
WG1809535
(S) 2-Fluorophenol
51.5
10.0-120
0113112022 05:50
WG1809535
(S) Phenol-d5
33.3
10.0-120
0113112022 05:50
WG1809535
(S) Nitrobenzene-d5
80.0
10.0-127
0113112022 05:50
WG1809535
(S) 2-Fluorobiphenyl
75.9
10.0430
0113112022 05:50
WG1809535
(S) 2,4,6-Tribromophenol
69.0
10.0-155
0113112022 05:50
WG1809535
(S) p-Terphenyl-d14
82.1
10.0-128
0113112022 05:50
WG1809535
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
LIMA Resources
L1454549
02/07/22 16:05 6 of 21

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
u
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix Interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix Interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1454549 02/07/22 16:05 19 of 21

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
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17-026
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TN000032021-1
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AZ0612
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2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932�
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky's
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006 _
Michigan
9958
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110033
Minnesota
047-999-305
Washington _
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
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998093910
Montana
CERT0086
Wyoming
A2LA
A21-A-15017025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025'
1461.02
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1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks ' Aquatic Toxicity 4 Chemical/Microbiological ' Mold ' Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1454549 02/07/2216:05
PAGE:
20 of 21

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Mocksville WQ Permit Number: WQ0003351
WWTP Name: Dutchman's Creek WWTP
PWS Number: NCO021491
Monitoring Period: From l/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
I Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimud
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
514286
554472
593220
col/ g
0
Annually
y
Grab
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) El
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Todd Robinson - Area Manager
Preparer Name and Title (type or print)
T,,W koh,/,f,w
Todd Robinson (Feb 3, 202311:56 EST)
Brent Collins - Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
Feb 3, 2023 v���/-
2/2/2023
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
•
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, A 27028
Page 1
Report Date: 1/31/2022
Date Sample Rcvd: 1/24/2022
Meritech Work Order #
Parameters
%Total Solids
Fecal Coliform (Sludge)
01242204 Sample: Dutchman's Creek 1 Grab
Result Analysis Date Reporting Limit
1.80 % 1/25/22 0-100 %
555,556 col/gdrywt 1/24/22 130 col/gdry wt
1/24/22
Method
SM 2540B
SM 9222D
Meritech Work Order #
01242205 Sample: Dutchman's Creek 2 Grab
1/24/22
Parameters
Result Analysis Date Reporting
Lirnj
Method
% Total Solids
1.77 % 1/25/22 0-100 %
SM 2540B
Fecal Coliform (Sludge)
519,774 col/g dry wt 1/24/22
130 col/g dry wt
SM 9222D
Meritech Work Order #
01242206 Sample: Dutchman's Creek 3 Grab
1/24/22
Parameters
Result Analysis Date Reporting
Limit
Method
% Total Solids
1.75 % 1/25/22 0-100 %
SM 2540E
Fecal Coliform (Sludge)
548,571 col/gdrywt 1/24/22
130 col/gdry wt
SM 9222D
Meritech Work Order # 01242207 Sample: Dutchman's Creek 4 Grab 1/24/22
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.77 % 1/25/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 593,220 col/g dry wt 1/24/22 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
•
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Page 2
Report Date: 1/31/2022
Mocksville, NC 27028 Date Sample Revd: 1/24/2022
Meritech Work Order # 01242208 Sample: Dutchman's Creek 5 Grab 1/24/22
Parameters Result Analysis Date Reporting Limit Method.
% Total Solids 1.75 % 1/25/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 514,286 col/g dry wt 1/24/22 130 col/g drywt SM 9222D
Meritech Work Order # 01242209 Sample: Dutchman's Creek 6 Grab
Parameters Result Analysis Date Reporting Limit
% Total Solids 1.74 % 1/25/22 0-100 %
Fecal Coliform CSludge) 574,713 col/g dry wt 1/24/22 130 col/g dry wt
Meritech Work Order # 01242210 Sample: Dutchman's Creek 7 Grab
Parameters Result Analvsis Date Reporting Limit
% Total Solids 1.81 % 1/25/22 0-100 %
Fecal Coliform (Sludge) 580,110 col/g dry wt 1/24/22 130 col/g dry wt
1/24/22
Method
SM 2540B
SM 9222D
1/24/22
Method
SM 2540B
SM 9222D
a�
1 hereby certify that d have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date: 5/18/2022
Date Sample Rcvd: 4/6/2022
Vector Attraction Reduction
Aerobically Digested Sludge
30 Day Test
Meritech
Work Order # 04062223
Sample: Mocksville Composite
4/6/22
Total Solids
Volatile Solids
@ Volatile Solids
Week 1
1.24
0.930
0.751
Week 2
1.24
0.930
0.752
Week 3
1.18
0.890
0.757
Week 4
1.12
0.840
0.749
Week 5
1.00
0.730
0.733
Van Kleek Reduction (%): 8.67
I hereby certify that I have reviewed and approve these data.
Pass or Fail
Pass
� doA
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Chain of Custody Record (COC)
NPDES#:
ME R I TE C H, INC.
Client: EMA Resources Inc. Phone:— 336-751-1441
Address: 755 Yadkinville Rd Fax: [phone]
ENVIRONMENTAL LABORATORIES
Mocksville iVC 27028 Email:` Brent,
coil ins @ ern aresourcesinccom
642 Tamco Rd. Prone; 336-342-4748
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Brent Collins Turn Around Time*
www.meritechlabs.com
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: 5td 10da s) 3_5 Davs ors
��{ referred) , Fax, Mail
Sampling Dates &Times
Person Taking Sample (Sign/Print):
��,'7t Lab Use Only
Sample Location
and/or ID 0Start
End Comp? Hof Test(s) Required
Date Time Date Time
Yes es CROOK?
Grab? Cont. No
i octcs,;i(
wI" 9'/S
C I 30 )"Q reek lD,' C4'U-, a
Temperature Upon
Method of
Receipt: t l~
*** Dechlorination <0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior preservation. C 4
Shipment:
Comments:
-to
Compositor #
p
❑ UPS
Plepre frAA� [�ar�C✓l��iisq ✓�nrf{� 4./ /YFr
❑ Fed Ex
Are these results for regulatory purposes? Yes
Jug #
L4�No ❑ Report results in: mg/L ❑ mg/kg 0 ug/C ❑
❑
Hand Delivery
Relinquished by; Date: y
Time: JD ors Received by: Date: Time:
❑ Other
Relinquished by: Date:
Time: Received by: Date: Time;
Relinquished by: Date:
Time: Re ed la _-
{
f
�

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SLO36093
In-,
Client: Roger Spillman
Advisor: Brent Collins
{r r Predictive
PO Box 378
EMA Resources Inc
Cooleemee, NC 27014
755 Yadkinville Rd
r -3 Extraction
Soil Report Mehlich
Mocksville, NC
! Links to Helpful Information
Sampled: Received: 06/24/2022 Completed: 07/01/2022 Farm: DV08
Sampled County: Davie
Client ID: 411288
Advisor ID: 405413
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 1.1 120-200 130
100 0 20
0 0
0 0
Note: 12
2-Fescue/OGrass/Tim, M 0.0 120-200 130
100 0 20
0 0
0 0
Note: 12
Test Results [units - W/V in g/crrf3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-AI1 Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.51 1.26 5.7 65 2.0 5.2 8 22 44 18
23 644 403 403
104 104
27 0.1 2
North Carolina
Art'fiattit� +iu31 r wki C�wnul�SshslM
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

Page 1 of 1
Report No: 22-356-0770
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypoeinto
ANALYTICAL
Client: Roger Spillman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm:DV08
Date Received: 12/22/2022
Date of Report: 12/29/2022
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-1 Mn-Ali Mn-Al2 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
21263 08 MIN 1.6 5.8 2.2 3 36 48 1338 0 0 63 63 60 11.7 81 48 32 0.4 0
Comment
Test result units = CEC and Na in meq/100cm3, NO3 N in mg/dm3, W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 22-356-0763
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypoeinto
ANALYTICAL
Client: Greg Dooley
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: DV11
Date Received: 12/22/2022
Date of Report: 12/29/2022
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K-1
S-1
Mn-1
Mn-Ali
Mn-Al2
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na
21248
01
MIN
2.2
6.3
1.2
45
22
17
413
0
0
433
433
420
11.0
90
60
28
0.6
0.1
21249
02
MIN
2.3
6.1
1.3
36
43
15
688
0
0
410
410
315
9.2
86
57
26
0.5
0
Comment:
Test result units = CEC and Na in meq/100cm3, NO3 N in mg/dm3, W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 22-356-0771
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypoeinto
ANALYTICAL
Client: Arthur Rupard
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: MK01
Date Received: 12/22/2022
Date of Report: 12/29/2022
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-1 Mn-Ali Mn-Al2 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
21264 02 MIN 1.8 5.8 2.1 94 80 25 925 0 0 325 325 255 11.0 81 63 14 0.6 0.1
Comment
Test result units = CEC and Na in meq/100cm3, NO3 N in mg/dm3, W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 22-356-0765
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypoei nt
ANALYTICAL
Client: Town of Mocksville
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: MK05
Date Received: 12/22/2022
Date of Report: 12/29/2022
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K-1
S-1
Mn-1
Mn-Ali
Mn-Al2
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na
21251
01
MIN
1.3
7.0
0.0
3
39
62
756
0
0
38
38
35
7.9
100
76
20
1.3
0.1
21252
02
MIN
1.3
6.5
0.5
8
28
48
900
0
0
50
50
70
7.2
93
72
17
1.4
0.1
Comment:
Test result units = CEC and Na in meq/100cm3, NO3 N in mg/dm3, W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

2022 Mocksville Annual Report - WQ0003351
Final Audit Report 2023-02-03
Created: 2023-02-03
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAebmRPt_uR9pmP9cpFl7FIIIjM8eSupCc
"2022 Mocksville Annual Report - WQ0003351" History
tJ Document created by Brent Collins ([e-mail])
2023-02-03 - 3:22:30 PM GMT- IP address: 206.85.202.26
D--P. Document emailed to [e-mail] for signature
2023-02-03 - 3:24:02 PM GMT
Email viewed by [e-mail]
2023-02-03 - 3:28:39 PM GMT- IP address: 71.76.192.62
clp Signer [e-mail] entered name at signing as Todd Robinson
2023-02-03 - 4:56:49 PM GMT- IP address: 99.173.169.21
&p Document e-signed by Todd Robinson ([e-mail])
Signature Date: 2023-02-03 - 4:56:51 PM GMT - Time Source: server- IP address: 99.173.169.21
Q Agreement completed.
2023-02-03 - 4:56:51 PM GMT
a Adobe Acrobat Sign

Pages from 2022 Mocksville Annual Report -
WQ0003351
Final Audit Report 2023-02-03
Created: 2023-02-03
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAABti3kgxbzjnOErXEXS2jZRlcjZ025MBQ
"Pages from 2022 Mocksville Annual Report - WQ0003351" Hist
ory
Document created by Brent Collins ([e-mail])
2023-02-03 - 8:59:42 PM GMT- IP address: 206.85.202.26
E—�!, Document emailed to [e-mail] for signature
2023-02-03 - 9:00:07 PM GMT
Email viewed by [e-mail]
2023-02-03 - 9:15:24 PM GMT- IP address: 67.213.52.2
r-iq, Signer [e-mail] entered name at signing as Ken Gamble
2023-02-03 - 9:15:48 PM GMT- IP address: 67.213.52.2
C5 Document e-signed by Ken Gamble ([e-mail])
Signature Date: 2023-02-03 - 9:15:50 PM GMT - Time Source: server- IP address: 67.213.52.2
Q Agreement completed.
2023-02-03 - 9:15:50 PM GMT
0 Adobe Acrobat Sign