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HomeMy WebLinkAboutWQ0036561_2022 Residual Annual Report_20230228 (2)Initial Review Reviewer Nathaniel.Thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR) * WQ0036561 Applicant/Permittee City of Danville Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 336-399-3646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0036561 Has Current Existing permit number Applicant/Permittee Address* 279 Park Avenue, Danville, VA 24541 Facility Name* City of Danville Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2022 Danville Annual Report - WQ0036561.pdf 15.95MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/28/2023 February 3, 2023 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2022 Annual Report — City of Danville, VA Treatment and Land Application of Residuals Permit No. WQ0036561 Dear Sir or Madam: Enclosed is one copy of the 2022 Annual Report for the above referenced land application permit During 2022 EMA Resources, Inc. land applied 472.12 dry tons of wastewater residuals to 172.15 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Z�z 4;2W - Brent Collins Director of Technical Services brent.collinskemaresourcesinc.com Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 --Resources, Inc. City of Danville 2022 Annual Report Residuals Land Application Permit No. WQ0036561 Prepared By: EMA Resources, Inc. Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0036561 County: Pittsylvania County, VA Year: 2022 Facility Name (as shown on permit): Land Application Operator: City of Danville, Northside WWTP EMA Resources Inc. Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? El Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 33 Total number of fields utilized for land application during the year: 7 Total amount of dry tons applied during the year for all application sites: 472.12 Total number of acres utilizes for land application during the year: 172.15 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes 0 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." d&. Feb 3 2023 ,gran Johnson - Division Director of water & wastewater Treatment Alan Johnson (Feb 3, 2023 09:17 EST) 7 Permittee Name and Title (type or print) Signature of Permittee Date &9� 0 61ul l Feb 1 2023 ALan D. Gould (Feb 1, 202314:13 EST) Z�fz 2/6/2022 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data WQ0036561 City of Danville VA0060593 Northside WWTP Laboratory: 1) 2) 3) 4) 5) Waypoint Analytical Parameter (mg/kg) Conc. Limit (mg/kg a Sample or Composite Date 4/12/22 4/26/22 5/3/22 5/17/22 Average Percent Solids (%) NA 4.71 4.29 4.66 5.21 4.72 Arsenic 75 13.2 11.6 10.6 10.2 11.40 Cadmium 85 2.13 22.9 2.13 1.92 7.27 Copper 4,300 449 456 398 431 433.50 Chromium NA 59.4 85.8 63 1 60 67.05 Lead 840 54.5 108 48.9 61.9 68.33 Mercury 57 1.88 1 3.19 2.85 3 2.73 Molybdenum 75 11.3 9.77 9.19 9.23 9.87 Nickel 420 61.9 76.7 63 60.2 65.45 Selenium 100 10.6 11.6 10.6 9.62 10.61 Zinc 7,500 2260 2420 2050 2350 2270.0 Total Phosphorus NA 21500 22900 20300 22900 21900 TKN NA 48500 60200 39800 49000 49375 Ammonia -Nitrogen NA 11400 10000 11300 10300 10750 Nitrate and Nitrite NA 104 112 104 113 108.25 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Feb 1, 2023 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0036561 Facility Name: City of Danville Residual Source NPDES # or WQ#: WWTP Name: Residual Analysis Data VA0060593 Northside WWTP Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter Sample or Composite Date •:11 •11 111 � 11 :1 1 ------- 11 11 11 •11 �------- - • � 1 � 1 1 • 1 � 1 1 •11 ------- •� 1 11 11 1111 • •1 �------- ------------ ------------ ------------ ------------ ------------ ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." AL- D. Gourd fFd 1. 2o2314:13 ESrI Signature of Preparer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Feb 1, 2023 Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville Total Dry Tons Applied (Annual): 30.71 WQ0036561 Cation Exchange Capacity (non 503 only): James Blackwell Owner: James Blackwell Predominant Soil Series: CgB2 19.6 Acres Permitted: 19.6 Site #: CS07 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 21 3 4 5j 6j 7j 81 9 10 ill 12 DT/Ac./ App. .fir Event 1.57 Arsenic 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Cadmium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Copper 1.359 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.359 Chromium 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210 Lead 0.214 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.214 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 denum Nickel 0.205 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.205 Selenium 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 Zinc 7.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.114 Total Phos- 68.635 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.635 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- 1/30/2023 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville James Blackwell Operator: James Blackwell Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 30.71 Site #: Predominant Soil Series: CgB2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: CS07 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 19.6 19.6 0 Q Volume applied enter one Solids/ Liquid Cu. Yds Gallons o /o Solids Volume A lied er pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a c� w *o• o ,•d � # w , * N *� TKN mg/kg Z ; o oa o �• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/29 65000 4.72 0.653 Northside WWTP Dry <.5" S 0.5 1 0.3 49375 10750 108.25 22.285 NA Fescue 6/30 91000 4.72 0.914 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 31.199 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF so pp to this form): TOTALS: 01 156000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 53.485 0.000 Lime Applied Annuallbs/acre 0.036 0.023 1.359 0.210 0.214 0.009 0.031 0.205 0.033 7.114 68.635 Date lbs/ac Prior Years Cumulative lbs/ac 0.717 0.226 109.325 6.56 4.957 0.091 0.94 4.264 0.362 120.024 Current Cumulative lbs/ac 0.753 0.249 110.684 6.770 5.171 0.100 0.971 4.469 0.395 127.138 Permitted C. P. L. R.**** 36 1 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit lst/2nd Crop 156 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 103.62 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series: RnB Acres Used: 30 Acres Permitted: 65 Site #: CS09 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 2 1 3 4 5j 6j 7j 81 9 10 11 1 12 DT/Ac./ App. .fir Event 3.45 Arsenic 0.079 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.079 Cadmium 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Copper 2.995 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.995 Chromium 0.463 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.463 Lead 0.472 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.472 Mercury 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Molyb- 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.068 denum Nickel 0.452 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.452 Selenium 0.073 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.073 Zinc 15.681 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.681 Total Phos- 151.285 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 151.285 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- 1/30/2023 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville Glenn Hodges Operator: Glenn Hodges Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 103.62 Site #: Predominant Soil Series: RnB Crop 1 Max. PAN: 125 Crop 2 Name: Acres Utilized: CS09 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 30 65 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/30 84500 4.72 0.554 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 18.928 NA Fescue 7/1 130000 4.72 0.853 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 29.119 NA Fescue 7/5 136500 4.72 0.896 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 30.575 NA Fescue 7/6 110500 4.72 0.725 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 24.752 NA Fescue 7/7 65000 4.72 0.426 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 14.560 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 526500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 117.9741 o.000 Lime Applied Annuallbs/acre 0.079 0.050 2.995 0.463 0.472 0.019 0.068 0.452 0.073 15.681 151.285 Date lbs/ac Prior Years Cumulative lbs/ac 0.218 0.058 9.206 1.425 1.211 0.028 0.283 1.504 0.195 47.095 Current Cumulative lbs/ac 0.297 1 0.108 12.201 1.888 1.683 0.047 0.351 1.956 0.268 62.776 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 125 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 25.59 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Marc Thomas Owner: Marc Thomas Predominant Soil Series: CfB Acres Used: 9.8 Acres Permitted: 9.8 Site #: CS 10 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 11 2 1 3 4 5j 6j 7j 81 9 10 11 1 12 DT/Ac./ App. .fir Event 2.61 Arsenic 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Cadmium 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Copper 2.264 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.264 Chromium 0.350 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.350 Lead 0.357 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.357 Mercury 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Molyb- 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 denum Nickel 0.342 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.342 Selenium 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Zinc 11.854 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.854 Total Phos- 114.362 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 114.362 horus "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- Signature of Land Applier 1/30/2023 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville Marc Thomas Operator: Marc Thomas Crop 1 Name: Fescue -Hay WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 25.59 Site #: Predominant Soil Series: C1B Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: CS 10 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 9.8 9.8 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/7 130000 4.72 2.611 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 89.141 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 130000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 89, 14 iT o.000 Lime Applied Annuallbs/acre 0.060 0.038 2.264 0.350 0.357 0.014 0.052 0.342 0.055 11.854 114.362 Date lbs/ac Prior Years Cumulative lbs/ac 0.431 0.116 19.679 4.002 2.629 0.054 0.584 2.775 0.346 68.4 Current Cumulative lbs/ac 0.491 1 0.154 21.943 4.352 2.986 0.068 0.636 3.117 0.401 80.254 Permitted C. P. L. R.**** 1 36 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 1 1 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 61.41 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Marc Thomas Owner: Marc Thomas Predominant Soil Series: Clifford Acres Used: 38.5 Acres Permitted: 38.5 Site #: CS10 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 11 21 3 4 5j 6j 7j 81 9 10 ill 12 DT/Ac./ App. .fir Event 1.60 Arsenic 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Cadmium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Copper 1.383 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.383 Chromium 0.214 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.214 Lead 0.218 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.218 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 denum Nickel 0.209 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.209 Selenium 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Zinc 7.241 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.241 Total Phos- 69.861 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 69.861 horus "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- Signature of Land Applier 1/30/2023 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville Marc Thomas Operator: Marc Thomas Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 61.41 Site #: Predominant Soil Series: Clifford Crop 1 Max. PAN: 162 Crop 2 Name: Acres Utilized: CS 10 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 38.5 38.5 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/7 52000 4.72 0.266 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 9.076 NA Fescue 7/8 117000 4.72 0.598 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 20.421 NA Fescue 7/11 143000 4.72 0.731 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 24.960 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4-0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 312000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 54,4577 0.000 Lime Applied Annuallbs/acre 0.036 0.023 1.383 0.214 0.218 0.009 0.031 0.209 0.034 7.241 69.861 Date lbs/ac Prior Years Cumulative lbs/ac 0.409 0.116 20.516 4.014 2.726 0.055 0.556 2.887 0.354 69.723 Current Cumulative lbs/ac 0.445 0.139 21.899 4.228 2.944 0.064 0.587 3.096 0.388 76.964 Permitted C. P. L. R.****1 36 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 235.42 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: ToB Acres Used: 51 Acres Permitted: 61.4 Site #: CS 14 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 11 2 1 3 4 5j 6j 7j 81 9 10 11 1 12 DT/Ac./ App. .fir Event 4.62 Arsenic 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.105 Cadmium 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Copper 4.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.002 Chromium 0.619 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.619 Lead 0.631 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.631 Mercury 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Molyb- 0.091 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.091 denum Nickel 0.604 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.604 Selenium 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.098 Zinc 20.957 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.957 Total Phos- 202.181 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 202.181 horus "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- Signature of Land Applier 1/30/2023 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville David Sartin Operator: David Sartin Crop 1 Name: Bermuda -Pasture WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 235.42 Site #: Predominant Soil Series: ToB Crop 1 Max. PAN: 162 Crop 2 Name: Acres Utilized: CS 14 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 51 61.4 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/16 188500 4.72 0.727 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 24.837 NA Fescue 6/17 175500 4.72 0.677 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 23.124 NA Fescue 6/20 39000 4.72 0.151 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 5.139 NA Fescue 6/21 182000 4.72 0.702 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 23.981 NA Fescue 6/22 253500 4.72 0.978 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 33.402 NA Fescue 6/23 221000 4.72 0.853 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 29.119 NA Fescue 6/24 117000 4.72 0.452 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 15.416 NA Fescue 6/29 19500 4.72 0.075 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 2.569 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 1196000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P i57,587T o.000 Lime Applied Annuallbs/acre 0.105 0.067 4.002 0.619 0.631 0.025 0.091 0.604 0.098 20.957 202.181 Date lbs/ac Prior Years Cumulative lbs/ac 0.43 0.096 15.8 2.6 2.302 0.048 0.465 2.416 0.324 65.342 Current Cumulative lbs/ac 0.535 1 0.163 19.802 3.219 2.933 0.073 0.556 3.020 0.422 86.299 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4- *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 39.66 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: Toast Acres Used: 18.25 Acres Permitted: 24.3 Site #: CS 14 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date OEM MEMO Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 11 2 1 3 4 5j 6j 7 8 9 10 11 12 DT/Ac./ App. Event 2.17 Arsenic 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Cadmium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Copper 1.884 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.884 Chromium 0.291 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.291 Lead 0.297 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.297 Mercury 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Molyb- 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043 denum Nickel 0.284 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.284 Selenium 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.046 Zinc 9.865 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.865 Total Phos- 95.177 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 95.177 horus "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- Signature of Land Applier 1/30/2023 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville David Sartin Operator: David Sartin Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 39.66 Site #: Predominant Soil Series: Toast Crop 1 Max. PAN: 96 Crop 2 Name: 2 CS14 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 18.25 24.3 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/15 201500 4.72 2.173 Northside WWTP Dry <.5" S 0.5 0.3 49375 10750 108.25 74.195 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 201500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 74.195 0.000 Lime Applied Annuallbs/acre 0.050 0.032 1.884 0.291 0.297 0.012 0.043 0.284 0.046 9.865 95.177 Date lbs/ac Prior Years Cumulative lbs/ac 0.245 0.056 7.524 1.191 0.988 0.025 0.243 1.127 0.169 35.226 Current Cumulative lbs/ac 0.295 0.088 9.408 1.482 1.285 0.037 0.286 1.411 0.215 45.091 Permitted C. P. L. R.**** 36 34 1 1338 1 267 15 374 1 89 2498 Permit PAN Limit lst/2nd Crop 96 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 30.71 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: CmB Acres Used: 5 Acres Permitted: 5 Site #: CS 14 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date OEM MEMO Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 11 2 1 3 4 5j 6j 7 8 9 10 11 12 DT/Ac./ App. .fir Event 6.14 Arsenic 0.140 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.140 Cadmium 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Copper 5.324 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.324 Chromium 0.824 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.824 Lead 0.839 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.839 Mercury 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Molyb- 0.121 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.121 denum Nickel 0.804 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.804 Selenium 0.130 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.130 Zinc 27.880 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 27.880 Total Phos- 268.976 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 268.976 horus 1 1 1 1 1 "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z: f z 4; 5 1 114- Signature of Land Applier 1/30/2023 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Danville David Sartin Operator: David Sartin Crop 1 Name: Fescue -Hay WQ Permit #: WQ0036561 Field #: Annual Dry Tons Applied: 30.71 Site #: Predominant Soil Series: CmB Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: CS 14 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Q Volume applied enter one Solids/ Liquid Cu. Yds Gallons o /o Solids Volume A lied er pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a 4 � c� w *o• o ,•d 2 � # 4 w , * N *� TKN mg/kg Z ; o oa o �• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/13 156000 4.72 6.141 Northside WWTP Dry <.5" S 0.5 1 0.3 49375 10750 108.25 209.660 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 1560001 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 209.6601 0.000 Lime Applied Annuallbs/acre 0.140 0.089 5.324 0.824 0.839 0.034 0.121 0.804 0.130 27.880 268.976 Date lbs/ac Prior Years Cumulative lbs/ac 0.184 0.052 5.607 0.691 0.726 0.018 0.188 0.85 0.21 29.636 Current Cumulative lbs/ac 0.324 0.141 10.931 1.515 1.565 0.052 0.309 1.654 0.340 57.516 Permitted C. P. L. R.**** 36 1 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit lst/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation vv''t���'^�-- 1/30/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Waypointo ANALYTICAL 5/2/2022 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 22-104-0001 Project Description: VPDES PERMIT# VA0060593 LTS B-Basin 22 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/14/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, � aw, c M ( G.'o w y/ Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 15 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-104-0001 Client Project Description: VPDES PERMIT# VAOO6O593 LTS B-Basin 22 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 SM-2540G WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 9045D WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 SW-7471B WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 6010D WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 4500NO3F-2011 WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 SM-4500-NH3C WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 SM-2320 B WP MTN 57531 LTS B-Basin 22-A Solids 04/12/2022 08:05 04/14/2022 SM-4500-NH3C-TKN WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 8081A WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 7470A WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 6010D WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 SW-1311 (ZHE) WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 8151A WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 SW-1311 WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 8270C WP MTN 57532 LTS B-Basin 22-B TCLP 04/12/2022 08:05 04/14/2022 8260B WP MTN 57533 LTS B-Basin 22-C Solids 04/12/2022 08:05 04/14/2022 SW-9045C WP MTN 57533 LTS B-Basin 22-C Solids 04/12/2022 08:05 04/14/2022 SW-7.3.4 WP MTN 57533 LTS B-Basin 22-C Solids 04/12/2022 08:05 04/14/2022 SW-7.3.3 WP MTN 57533 LTS B-Basin 22-C Solids 04/12/2022 08:05 04/14/2022 ASTM D93-80 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 15 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERMIT# VA0060593 A/P Report Date : 05/02/2022 Northside WWTP Information : LTS B-Basin 22 Received : 04/14/2022 229 Northside Drive Danville, VA 24540 Pauric Mc Groary Ph.D., CPA Report Number : 22-104-0001 REPORT OFANALYSIS Agronomist Lab No : 57531 Matrix: Solids Sample ID : LTS B-Basin 22-A Sampled: 4/12/2022 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Potassium 4110 mg/Kg - dry 213 1 04/23/22 02:21 EAL 6010D Sulfur 11900 mg/Kg - dry 213 1 04/23/22 02:21 EAL 6010D Magnesium 3940 mg/Kg - dry 106 1 04/23/22 02:21 EAL 6010D Sodium 10700 mg/Kg - dry 532 1 04/23/22 02:21 EAL 6010D Iron 35100 mg/Kg - dry 213 1 04/23/22 02:21 EAL 6010D Zinc 2260 mg/Kg - dry 26.6 1 04/23/22 02:21 EAL 6010D Ammonia Nitrogen 11400 mg/Kg - dry 2130 1 05/02/22 13:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N <104 mg/Kg - dry 104 1 04/20/22 15:07 ZBD 4500NO3F-2011 Cadmium <2.13 mg/Kg - dry 2.13 1 04/23/22 02:21 EAL 6010D Chromium 59.4 mg/Kg - dry 5.32 1 04/23/22 02:21 EAL 6010D Mercury 1.88 mg/Kg - dry 0.334 1 04/22/22 17:39 JTR SW-7471B pH 7.4 S.U. 1 04/25/2215:54 DRS 9045D Molybdenum 11.3 mg/Kg - dry 5.32 1 04/23/22 02:21 EAL 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 57400 mg/Kg - dry 2130 1 04/15/22 09:50 NNL SM-2320 B Total Solids 4.71 % 0.010 1 04/14/22 16:18 FMM SM-2540G Copper 449 mg/Kg - dry 10.6 1 04/23/22 02:21 EAL 6010D Lead 54.5 mg/Kg - dry 6.38 1 04/23/22 02:21 EAL 6010D Manganese 1110 mg/Kg - dry 10.6 1 04/23/22 02:21 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Q RPD >40% dual column results Page 3 of 15 �' WayP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERMIT# VA0060593 A/P Report Date : 05/02/2022 Northside WWTP Information : LTS B-Basin 22 Received : 04/14/2022 229 Northside Drive Danville, VA 24540 Pauric Mc Groary Ph.D., CPA Report Number : 22-104-0001 REPORT OFANALYSIS Agronomist Lab No : 57531 Matrix: Solids Sample ID : LTS B-Basin 22-A Sampled: 4/12/2022 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Nickel 61.9 mg/Kg - dry 5.32 1 04/23/22 02:21 EAL 6010D Selenium <10.6 mg/Kg - dry 10.6 1 04/23/22 02:21 EAL 6010D Analytical Method: SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Batch Moisture 95.3 % 0.010 1 04/14/2216:18 FMM L610924 Total Kjeldahl Nitrogen 48500 mg/Kg - dry 5320 1 05/01/22 12:30 JPJ ;M-4500-NH3C-TKI` Phosphorus 21500 mg/Kg - dry 106 1 04/23/22 02:21 EAL 6010D Calcium 13500 mg/Kg - dry 1060 1 04/23/22 02:21 EAL 6010D Aluminum 39800 mg/Kg - dry 106 1 04/23/22 02:21 6010D Organic N 37150 mg/Kg - dry 5319 1 05/01/22 12:30 CALCULATION Arsenic 13.2 mg/Kg - dry 10.6 1 04/23/22 02:21 EAL 6010D Total Volatile Solids 46.5 % 0.010 1 04/14/22 16:18 FMM SM-2540G Qualifiers/ DF Dilution Factor Definitions Q RPD >40% dual column results MQL Method Quantitation Limit Page 4 of 15 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 22-104-0001 Lab No : 57532 Sample ID : LTS B-Basin 22-B Project VPDES PERMIT# VA0060593 Report Date : 05/02/2022 Information : LTS B-Basin 22 Received : 04/14/2022 REPORT OFANALYSIS 0Iwl[ M� Grow Pauric Mc Groary Ph.D., CPA Agronomist Matrix: TCLP Sampled: 4/12/2022 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Combined 1 04/21/22 14:00 KBL SW-1311 TCLP Metals Extraction Combined 1 04/21/22 14:00 KBL SW-1311 TCLP Pesticide Extraction Combined 1 04/21/22 14:00 KBL SW-1311 TCLP SVOC Extraction Combined 1 04/21/22 14:00 KBL SW-1311 TCLP VOC ZHE Extraction Combined 1 04/21/22 14:00 KBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L612765 04/26/22 11:17 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/26/22 17:18 EAL L612943 TCLP Barium <0.250 mg/L 0.250 1 04/26/22 17:18 EAL L612943 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/26/22 17:18 EAL L612943 TCLP Chromium <0.100 mg/L 0.100 1 04/26/22 17:18 EAL L612943 TCLP Lead <0.100 mg/L 0.100 1 04/26/22 17:18 EAL L612943 TCLP Selenium <0.500 mg/L 0.500 1 04/26/22 17:18 EAL L612943 TCLP Silver <0.0500 mg/L 0.0500 1 04/26/22 17:18 EAL L612943 Qualifiers/ DF Dilution Factor Definitions Q RPD >40% dual column results MQL Method Quantitation Limit Page 5 of 15 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERMIT# VA0060593 A/P Report Date : 05/02/2022 Northside WWTP Information : LTS B-Basin 22 Received : 04/14/2022 229 Northside Drive Danville , VA 24540 1 Pauric Mc Groary Ph.D., CPA Report Number : 22-104-0001 REPORT OFANALYSIS Agronomist Lab No : 57532 Matrix: TCLP Sample ID : LTS B-Basin 22-B Sampled: 4/12/2022 8:05 Analytical Method: 7470A Prep Batch(es): L612735 04/26/22 13:00 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/26/22 14:47 ZMT L612953 Analytical Method: 8081A Prep Batch(es): L612328 04/22/22 12:31 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.004000 mg/L 0.004000 10 04/23/22 12:29 VIC L612571 TCLP gamma-BHC <0.004000 mg/L 0.004000 10 04/23/22 12:29 VIC L612571 TCLP Methoxychlor <0.004000 mg/L 0.004000 10 04/23/22 12:29 VIC L612571 TCLP Toxaphene <0.03000 mg/L 0.03000 10 04/23/22 12:29 VIC L612571 TCLP Chlordane <0.02000 mg/L 0.02000 10 04/23/22 12:29 VIC L612571 TCLP Heptachlor Epoxide <0.004000 mg/L 0.004000 10 04/23/22 12:29 VIC L612571 TCLP Heptachlor <0.004000 mg/L 0.004000 10 04/23/22 12:29 VIC L612571 Surrogate: Decachlorobiphenyl 77.97 Limits: 34-116% 10 04/23/22 12:29 VIC L612571 Surrogate: Tetrachloro-m-xylene 59.27 Limits: 25-123% 10 04/23/22 12:29 VIC L612571 Analytical Method: 8151A Prep Batch(es): L612387 04/22/22 15:45 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 04/26/22 00:13 VIC L612783 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 04/26/22 00:13 VIC L612783 Surrogate: DCAA 86.60 Limits: 20-120% 1 04/26/22 00:13 VIC L612783 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Q RPD >40% dual column results Page 6 of 15 �' WayP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERMIT# VA0060593 A/P Report Date : 05/02/2022 Northside WWTP Information : LTS B-Basin 22 Received : 04/14/2022 229 Northside Drive Danville, VA 24540 Pauric Mc Groary Ph.D., CPA Report Number : 22-104-0001 REPORT OFANALYSIS Agronomist Lab No : 57532 Matrix: TCLP Sample ID : LTS B-Basin 22-B Sampled: 4/12/2022 8:05 Analytical Method: 8260B Prep Batch(es): L612329 04/22/22 08:05 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Carbon Tetrachloride <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Chlorobenzene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Chloroform <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP 1,4-Dichlorobenzene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP 1,2-Dichloroethane <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP 1,1-Dichloroethene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Methyl Ethyl Ketone (MEK) <0.200 mg/L 0.200 1 04/22/22 14:51 ELM L612330 TCLP Tetrachloroethene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Trichloroethene <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 TCLP Vinyl Chloride <0.0100 mg/L 0.0100 1 04/22/22 14:51 ELM L612330 Surrogate:4-Bromofluorobenzene 137 Limits:71-137% 1 04/22/22 14:51 ELM L612330 Surrogate: Dibromofluoromethane 113 Limits: 70-128% 1 04/22/22 14:51 ELM L612330 Surrogate: 1,2-Dichloroethane - d4 113 Limits: 63-136% 1 04/22/22 14:51 ELM L612330 Surrogate: Toluene-d8 111 Limits: 70-130% 1 04/22/22 14:51 ELM L612330 Analytical Method: 8270C Prep Batch(es): L612282 04/22/22 10:07 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP 3&4 Methylphenol <0.100 mg/L 0.100 1 04/22/22 20:56 VBW L612455 TCLP 2,4-Dinitrotoluene <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Q RPD >40% dual column results Page 7 of 15 waypANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 22-104-0001 Lab No : 57532 Sample ID : LTS B-Basin 22-B 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Project VPDES PERMIT# VA0060593 Information : LTS B-Basin 22 REPORT OFANALYSIS Report Date : 05/02/2022 Received : 04/14/2022 �oau� �� Grow Pauric Mc Groary Ph.D., CPA Agronomist Matrix: TCLP Sampled: 4/12/2022 8:05 Analytical Method: 8270C Prep Method: 3510C Test Results Prep Batch(es): Units L612282 04/22/22 10:07 MQL DF Date / Time By Analyzed Analytical Batch TCLP Hexachlorobenzene <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP Hexachlorobutadiene <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP Hexachloroethane <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP Nitrobenzene <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP Pentachlorophenol <0.100 mg/L 0.100 1 04/22/22 20:56 VBW L612455 TCLP Pyridine <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP 2,4,5-Trichlorophenol <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 TCLP 2,4,6-Trichlorophenol <0.0500 mg/L 0.0500 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP 2,4,6-Tribromophenol 79.4 Limits: 42-102% 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP 2-Fluorobiphenyl 48.5 Limits: 24-86% 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP 2-Fluorophenol 23.0 Limits: 13-37% 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP 4-Terphenyl-d14 83.2 Limits: 30-122% 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP Nitrobenzene-d5 62.2 Limits: 25-78% 1 04/22/22 20:56 VBW L612455 Surrogate: TCLP Phenol-d6 18.6 Limits: 9-27% 1 04/22/22 20:56 VBW L612455 Qualifiers/ DF Definitions Q Dilution Factor RPD >40% dual column results MQL Method Quantitation Limit Page 8 of 15 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 22-104-0001 Lab No : 57533 Sample ID : LTS B-Basin 22-C Project VPDES PERMIT# VA0060593 Report Date : 05/02/2022 Information : LTS B-Basin 22 Received : 04/14/2022 REPORT OFANALYSIS 0Iwl[ M� Grow Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 4/12/2022 8:05 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Sulfide (Reactivity) <25.0 mg/Kg 25.0 1 04/25/22 10:19 FMM SW-7.3.4 Cyanide (Reactivity) <0.125 mg/Kg 0.125 1 04/25/22 10:19 FMM SW-7.3.3 Ignitability >96 degrees C 1 04/26/22 08:41 ANV ASTM D93-80 pH 7.4 S.U. 1 04/22/2213:24 DRS SW-9045C Qualifiers/ DF Dilution Factor Definitions Q RPD >40% dual column results MQL Method Quantitation Limit Page 9 of 15 Waypointo ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES PERMIT# VA0060593 Lab Report Number: 22-104-0001 Date: 5/2/2022 Flashpoint Method ASTM D93-80 QC Batch No: L612867 The sample analysis was performed using a modified version of the reference method. Due to the sample matrix, the continual stirring required by the method had to be omitted. Separatory Funnel Extraction 8081 Method 3510C Sample 57532 (LTS B-Basin 22-B) QC Batch No: L612328/L612328 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction Method 3510C Sample 57532 (LTS B-Basin 22-B) QC Batch No: L612282/L612282 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Limited sample Metals Analysis Method 601 OD Sample 94742 QC Batch No: L612503/L611792 One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are required. Sample 94742 Analyte: Aluminum QC Batch No: L612753/L611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Arsenic QC Batch No: L612753/L611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Chromium QC Batch No: L612753/L611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Iron Page 10 of 15 Waypointo ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Potassium QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Magnesium QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Manganese QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Molybdenum QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Phosphorus QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Lead QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Sulfur QC Batch No: 1-612753/1-611792 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94742 Analyte: Zinc QC Batch No: 1-612753/1-611792 Page 11 of 15 Waypoint".0 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 12 of 15 WayPAoInt.. NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 22-104-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: lBrandi Watson Date & Time: 04/14/2022 09:33:41 Page 13 of 15 ST 30 bT abud C% y cn m m 0 7 7 r E E E n ro ❑ c l� CU t O i W} N ❑ a 4 Q O Z ui n n r�\ ►�Lj 7 �' n ry '� ^� z `a m Q N vi 0 x' .. ry u E U] En m ae nn= a .n �'E c LV °u=Z===*uOL N 3 o a ❑ J E E E n « J J 0 CD Q 7 a a ~ L2 L7 wa E 0 r a u c 0. 7) U > tt a W" v 0 d E u E 5 a a c a fY r r ya 0 D L 0. � N T R a ❑ Z ❑ a E O y U P a A w E L � � V a o o a L+ E �= d 0) d��l C N W W isil payoel4e aag E w 7 o Y r a Q O _` N C 3 a— z z cv E z S o n O cr] d r ❑7 o a V C [V m_ r i ❑ n O a3!sodwo{}J jo qej{qJ V U U x A .� a -� U C [AaM of ia�ay�j ■�i1ey� Fa) IL E ❑ � d C � siau�eluo� ya iagwnN r r r- � � `•, � � a 157 J q Cf) � v 9 E r at QCnU LO o ~ 6m n µ CV N N G � °7 3 s C 4 N C\J it v N— cc v t[° E j[ a Q a N tI3 f17 0 T �° J m m m m _ C V J J �7�M _J N b V mx L 7 O E 0 c Z 6& E Z5 w d d❑ O t Q N rn Gp y [ I n O � ry N a Y Q s NCla` >> d 1 Required Biosolids Tests for Inframark Danville, VA WWTP (Waypoint VA Account 79434) Sample: LTS B Basin 22 - I o�7 T1 PO: j34 q q -j %TS %TVs pH Alkalinity TKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen Fz ; o=� Ln + Organic Nitrogen (calculation) -q x Phosphorus � r Potassium_ Sulfur W Calcium Magnesium r ¢ Sodium f Iron N N W Aluminum N M11 Manganese Copper Zinc Cadmium Chromium Nickel Lead Arsenic Mercury Selenium Molybdenum Page 15 of 15 4/12/2022 mg/kg mg/L Equiv Weight Milli Equiv Sodium 10700 503.97 23 21.91174 Calcium 13500 635.85 20 31.7925 Magnesium 3940 185.574 12 15.4645 Percent Solids 4.71 SAR 4.51 SAR = Na+ a (Ca2+ + M;42+ ) 21.91174 0.5( 31.793 2 + 15.46450 2 ) Waypointo ANALYTICAL 5/6/2022 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 22-117-0017 Project Description: VPDES PERMIT#VA0060593 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/27/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-117-0017 Client Project Description: VPDES PERMIT#VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 57690 LTS B-BASIN 22-1300 Solids 04/26/2022 08:25 04/27/2022 SM-2540G WP MTN SW-7471B WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SM-4500-NH3C WP MTN 9045D WP MTN SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 �' WayP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERM IT#VA0060593 A/P Report Date : 05/06/2022 Northside WWTP Information : Received : 04/27/2022 229 Northside Drive Danville, VA 24540 Pauric Mc Groary Ph.D., CPA Report Number : 22-117-0017 REPORT OFANALYSIS Agronomist Lab No : 57690 Matrix: Solids Sample ID : LTS B-BASIN 22-1300 Sampled: 4/26/2022 8:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 95.7 % 0.010 1 04/29/2215:53 FMM SM-2540G Sulfur 12700 mg/Kg - dry 233 1 04/30/22 01:01 EAL 6010D Calcium 13500 mg/Kg - dry 1160 1 05/02/22 21:36 EAL 6010D Manganese 1080 mg/Kg - dry 11.6 1 04/30/22 01:01 TJS 6010D Zinc 2420 mg/Kg - dry 29.1 1 04/30/22 01:01 EAL 6010D Nickel 76.7 mg/Kg - dry 5.81 1 04/30/22 01:01 EAL 6010D Lead 108 mg/Kg - dry 6.98 1 04/30/22 01:01 EAL 6010D Arsenic <11.6 mg/Kg - dry 11.6 1 04/30/22 01:01 EAL 6010D Selenium <11.6 mg/Kg - dry 11.6 1 04/30/22 01:01 TJS 6010D pH 7.3 S.U. 1 05/04/2212:24 DRS 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 52300 mg/Kg - dry 2330 1 04/29/22 09:55 NNL SM-2320 B Organic N 50230 mg/Kg - dry 5814 1 05/05/22 13:00 CALCULATION Total Solids 4.29 % 0.010 1 04/29/22 15:53 FMM SM-2540G Phosphorus 22900 mg/Kg - dry 116 1 04/30/22 01:01 EAL 6010D Copper 456 mg/Kg - dry 11.6 1 04/30/22 01:01 EAL 6010D Magnesium 4020 mg/Kg - dry 116 1 04/30/22 01:01 EAL 6010D Molybdenum 9.77 mg/Kg - dry 5.81 1 04/30/22 01:01 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 8 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES PERM IT#VA0060593 A/P Report Date : 05/06/2022 Northside WWTP Information : Received : 04/27/2022 229 Northside Drive Danville, VA 24540 Report Number : 22-117-0017 REPORT OFANALYSIS Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 57690 Matrix: Solids Sample ID : LTS B-BASIN 22-1300 Sampled: 4/26/2022 8:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 11500 mg/Kg - dry 581 1 04/30/22 01:01 EAL 6010D Total Kjeldahl Nitrogen 60200 mg/Kg - dry 5810 1 05/05/22 13:00 JPJ ;M-4500-NH3C-TKI` Potassium 4280 mg/Kg - dry 233 1 04/30/22 01:01 EAL 6010D Iron 35600 mg/Kg - dry 233 1 04/30/22 01:01 TJS 6010D Aluminum 37900 mg/Kg - dry 116 1 04/30/22 01:01 EAL 6010D Ammonia Nitrogen 10000 mg/Kg - dry 2330 1 05/05/22 13:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <112 mg/Kg - dry 112 1 05/02/22 14:41 ZBD 4500NO3F-2011 Cadmium 22.9 mg/Kg - dry 2.33 1 04/30/22 01:01 EAL 6010D Chromium 85.8 mg/Kg - dry 5.81 1 04/30/22 01:01 EAL 6010D Mercury <3.19 mg/Kg - dry 3.19 1 04/29/22 12:03 ZMT SW-7471B Total Volatile Solids 47.4 % 0.010 1 04/29/22 15:53 FMM SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 8 Waypointo ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES PERMIT#VA0060593 Lab Report Number: 22-117-0017 Date: 5/5/2022 Metals Analysis Method 601 OD Sample 99343 Analyte: Aluminum QC Batch No: 1-613745/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Calcium QC Batch No: 1-613861/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Iron QC Batch No: 1-613861/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Potassium QC Batch No: 1-613745/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Magnesium QC Batch No: 1-613745/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Manganese QC Batch No: 1-613861/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99343 Analyte: Selenium QC Batch No: 1-613861/1-613349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 8 WayPAoInt.. NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 22-117-0017 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: lBrandi Watson Date & Time: 04/27/2022 13:08:14 Page 6 of 8 d �y m F d U) Q} Y b n C m D CCS p (� V �Qg7n N a ry O O ry 4 .o q n j (A Q = 3� i a {f] y "Dana V" $SmZZx D c4 U i8 N 3 oa IL r > ae�0 W wQr_ p f� ., _ Qj or is a x a x a 2 U) a x IX E uiw e5 v j cu E w a V E M r^0)' E W m T yr x C s a. CC t yp p C Ix � L ti LJ 6 L f�— � O C� � r• � b a d V J T R -k � G m m a E n :E:� �" � v Ll A _ � @ l � 0 [J ��y- m o ❑Car 2 iii 19 Q payaeue aa5 �j m >N a z z z m E Z u� 0 aylsodwo[]) �0 4ui�1 U m cNv p a o z a a a' V C ;Aa)l oy jayaa} xpl ew H E A E @ saau�e7uo3 ja jagwnH LL a ` u �i c � cg U3 T— v 8�LO O E >Qj p � '> li c A _ _0 - crr Y a cc a _ C -D N o d E ���ryry a Cr7 Off] W t m � a ~ 3 2 Q1 Q TF r--i L) [] d V L I w T 9 R ace v d N a©� ¢ d1 coC 7 na 1Lf7 a+ �y z ^ i.i¢ E x 4 1 x > R� o N a �W � � 0 a N �' � N r o u zE� s �© C) ��� CID m4 ?ro Page 7 of 8 8 30 8 a6Pd Required Biosolids Tests for Infrarnark Danville, VA VVVVTP (Waypoint VA Account 79434) Sample: LTS B Basin 22 - I3 Db PO: 3 7 x l / %TS %TVs pH Alkalinity TKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen Organic Nitrogen (calculation) Phosphorus Potassium Sulfur calcium Magnesium Sodium Iron o m N d Aluminum m Manganese n 0 Copper o = 0 cn � m Zinc w _ Cadmium Chromium Nickel V Lead � N N "' $ N � Arsenic V Mercury Selenium Molybdenum 4/26/2022 mg/kg mg/L Equiv Weight Milli Equiv Sodium 11500 493.35 23 21.45 Calcium 13500 579.15 20 28.9575 Magnesium 4020 172.458 12 14.3715 Percent Solids 4.29 SAR 4.61 SAR = Na+ a (Ca2+ + M;42+ ) 21.45000 0.5( 28.958 2 + 14.37150 2 ) Waypoint.(D ANALYTICAL 5/14/2022 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 22-125-0001 Project Description: VPDES permit# VA0060593 7621 White pine Road, Richmond, VA 23237 Main a04-743-Ml ° Fax 804-271-6446 www.waypointanalytical.com Dear AIP: Waypoint Analytical Virginia, Inc. received sample(s) on 5/5/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Tawil Mt (rare Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 10 Waypoint-(D ANALYTICAL 7621 Whitepine Road, RichMond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalocal.com Sample Summary Table Report Number: 22-125-0001 Client Project Description: VPDES permit# VA0060593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 SM-254OG WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 SW-74713 WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 SM-4500-NH3C-TKN WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 4500Na3F-2011 WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 6010D WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 SM-4500-NH3C WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 9045D WP MTN 57747 LTS B-Basin 22-1316 Solids 05/03/2022 08:15 05/05/2022 SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 10 Waypointo ANALYTICAL 79434 Inframark Project A/P Northside iNWTP Information 229 Northside Drive Danville, VA 24540 7621 Whitepine Road, Richmond, VA 23237 Main 804-743.9401 ° Fax 804-271-6446 www.waypointanalytical.com VPDES permit# VA0060593 Report Number: 22-125-0001 REPORT OF ANALYSIS Lab No : 57747 Sample ID : LTS B-Basin 22-1316 Report Date : 05/14/2022 Received : 05/05/2022 Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 5/3/2022 8:15 Test Results Units MQL DF Date 1 Time By Analytical Analyzed Method Moisture 95.3 % 0.010 1 05/06/2216:11 FMM SM-2540G Sulfur 11100 mg/Kg - dry 213 1 05/12/22 22:38 EAL 6010D Calcium 13300 mg/Kg - dry 1060 1 05/12/22 22:38 EAL 6010D Manganese 932 mg/Kg - dry 10.6 1 05/12/22 22:38 EAL 6010D Zinc 2050 mg/Kg - dry 26.6 1 05/12/22 22:38 EAL 6010D Nickel 63.0 mg/Kg - dry 5.32 1 05/12/22 22:38 EAL 6010D Lead 48.9 mg/Kg - dry 6.38 1 05/12/22 22:38 EAL 6010D Arsenic <10.6 mg/Kg - dry 10.6 1 05/12/22 22:38 EAL 6010D Selenium <10.6 mg/Kg - dry 10.6 1 05/12/22 22:38 EAL 6010D pH 7.2 S.U. 1 05/12/2215:54 DRS 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 53000 mg/Kg - dry 2130 1 05/10/22 09:40 DAS SM-2320 6 Organic N 2SS30 mg/Kg - dry 5319 1 05/12/22 11:00 CALCULATION Total Solids 4.66 % 0.010 1 05/06/22 16:11 FMM SM-254OG Phosphorus 20300 mg/Kg - dry 106 1 05/12/22 22:38 FAL 6010D Copper 398 mg/Kg - dry 10.6 1 05/12/22 22:38 EAL 6010D Magnesium 3620 mg/Kg - dry 106 1 05/12/22 22:38 EAL 6010D Molybdenum 9.19 mg/Kg - dry 5.32 1 05/12/22 22:38 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 20 0 Waypoint, 7621 Whltepine Rudd, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 Inframark Project VPDES permit# VA0060593 A/P Report Date : 05/14/2022 Northside WWTP Information : Received : 05/05/2022 229 Northside Drive Danville , VA 24540 T $Wll t iriaa. Report Number : 22-12$-0001 REPORTOFANALYSIS Pau ric Mc Groary Ph.D., CPA Agronomist Lab No : 57747 Matrix: Solids Sample ID : LTS B-Basin 22-1316 Sampled: 5/3/2022 8:15 Test Results Units MOL DF Date 1 Time By Analytical Analyzed Method Sodium 10000 mg/Kg - dry 532 1 05/12/22 22:38 EAL 6010D Total Kjeldahl Nitrogen 39800 mg/Kg - dry 5320 1 05/12/22 11:00 JPJ M-4500-NH3C-TKP Potassium 3640 mg/Kg - dry 213 1 05/12/22 22:38 FAL 6010D Iron 31300 mg/Kg - dry 213 1 05/12/22 22:38 FAL 601UD Aluminum 33000 mg/Kg - dry 106 1 05/12/22 22:38 EAL 6010D Ammonia Nitrogen 11300 mg/Kg - dry 2130 1 05/13/22 13:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <104 mg/Kg - dry 104 1 05/11/22 14:28 ZBD 45DONO3F-2011 Cadmium <2.13 mg/Kg - dry 2.13 1 05/12/22 22:38 EAL 6010D Chromium 63.0 mg/Kg - dry 5.32 1 05/12/22 22:38 EAL 6010D Mercury <2.85 mg/Kg - dry 2.85 1 05/11/22 11:36 JTR SW-7471B Total Volatile Solids 47.6 % 0.010 1 05/06/22 16:11 FMM SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitatiun Limit Page 4 of 10 Waypoint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES permit# VA0060593 Lab Report Number: 22-125-0001 Date: 5/13/2022 Metals Analysis Method 6010D Sample 86253 (MCCOTP21050322D) Analyte: Aluminum QC Batch No: L615844/L615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Arsenic QC Batch No. 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Calcium QC Batch No: L615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Cadmium QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Copper QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Iron QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Potassium QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 20 Waypoint-(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-749-9401 ° Fax 804-271-6446 www.waypointanalytital.com Sample 86253 (MCCOTP21050322D) Analyte: Magnesium QC Batch No: L615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Manganese QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Molybdenum QC Batch No: L615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Sodium QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Nickel QC Batch No: 1-6158441615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Phosphorus QC Batch No: L6158441L615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Lead QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Sulfur QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 6 of 10 Waypoint,(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypoin to nalytica l.com Sample 86253 (MCCOTP21050322D) Analyte: Selenium QC Batch No: 1-615844/1-615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86253 (MCCOTP21050322D) Analyte: Zinc QC Batch No: L6158441L615225 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 57762 (Strasburg) Analyte: Mercury QC Batch No: 1-615983/1-615093 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 7 of 10 ANALYTICAL Waypoint(D 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Y Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 22-125-0001 Shipping Method Fed ExCJ US Postal 0 Lab UPS (D Client () Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? # Yes No Number of coolers/boxes received 01 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes C) No Not Present Chain of Custody (COC) present? 0 Yes (D No COC agrees with sample label(s)? 0 Yes C) No COG properly completed # Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved Yes No 0 NIA Water -VOA vials free of headspace Yes 0 No (J NIA Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 NIA High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) ! Low concentration Encore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: F_ Signature: Brandi Watson Date & Time: 05/05/2022 09:22:16 Page 8 of 10 fJ: to i goo Mini LU irarL }CL l �. Its co r co 4 � ro to C3 � 22CNY f I � � � � �► � _ � ':� � Q � ��li pe�e#3e egg � ° Q d) i ME Et }}} ^' rm L / Ln- N UJ -, M - M O a s _ Li [ % , P i Page 9 of 10 Y Ia OT 30 OT 06ed Required Biosoilds Tess for lnframark Danvi ft YAK (iA "Int VA A=urrt 79434) Sample: !T5 a Basin 22 - PD: ZITS r %TVs r pN /'TKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen / Organic Nitrogen (calculation) Phosphorus Potassium f Sulfur fCalcit," Zkfagneslurn r Sodium Iron / Aluminum Manganese /Copper ,/Zinc / Cadmium •Chromium -/Nickel ✓Lead / Arsenic +/Mercury '/Selenium v/Molybdenum 5/3/2022 mg/kg mg/L Equiv Weight Milli Equiv Sodium 10000 466 23 20.26087 Calcium 13300 619.78 20 30.989 Magnesium 3620 168.692 12 14.05767 Percent Solids 4.66 SAR 4.27 SAR = Na+ a (Ca2+ + M;42+ ) 20.26087 0.5( 30.989 2 + 14.05767 2 ) Waypointo ANALYTICAL 6/1 /2022 'Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 22-139-0001 Project Description: VPDES Permit# VA0060593 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/19/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-139-0001 Client Project Description: VPDES Permit# VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 57924 LTS B-Basin 22-1353 Solids 05/17/2022 08:05 05/19/2022 SM-2540G WP MTN SW-7471B WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SM-4500-NH3C WP MTN 9045D WP MTN SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 9 �' WayP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 'Inframark Project VPDES Permit# VA0060593 A/P Report Date : 06/01/2022 Northside WWTP Information : Received : 05/19/2022 229 Northside Drive Danville, VA 24540 Pauric Mc Groary Ph.D., CPA Report Number : 22-139-0001 REPORT OFANALYSIS Agronomist Lab No : 57924 Matrix: Solids Sample ID : LTS B-Basin 22-1353 Sampled: 5/17/2022 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 94.8 % 0.010 1 05/24/2215:27 FMM SM-2540G Sulfur 12000 mg/Kg - dry 192 1 05/25/22 22:16 TJS 6010D Calcium 13900 mg/Kg - dry 962 1 05/25/22 22:16 TJS 6010D Manganese 1110 mg/Kg - dry 9.62 1 05/25/22 22:16 TJS 6010D Zinc 2350 mg/Kg - dry 24.0 1 05/25/22 22:16 TJS 6010D Nickel 60.2 mg/Kg - dry 4.81 1 05/25/22 22:16 TJS 6010D Lead 61.9 mg/Kg - dry 5.77 1 05/25/22 22:16 TJS 6010D Arsenic 10.2 mg/Kg - dry 9.62 1 05/25/22 22:16 TJS 6010D Selenium <9.62 mg/Kg - dry 9.62 1 05/25/22 22:16 TJS 6010D pH 7.2 S.U. 1 06/01/2214:19 ADM 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 31300 mg/Kg - dry 1920 1 05/25/22 09:20 DAS SM-2320 B Organic N 38690 mg/Kg - dry 4808 1 05/25/22 14:00 CALCULATION Total Solids 5.21 % 0.010 1 05/24/22 15:27 FMM SM-2540G Phosphorus 22900 mg/Kg - dry 96.2 1 05/25/22 22:16 TJS 6010D Copper 431 mg/Kg - dry 9.62 1 05/25/22 22:16 TJS 6010D Magnesium 4020 mg/Kg - dry 96.2 1 05/25/22 22:16 TJS 6010D Molybdenum 9.23 mg/Kg - dry 4.81 1 05/25/22 22:16 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 9 WayP �' 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 79434 'Inframark Project VPDES Permit# VA0060593 A/P Report Date : 06/01/2022 Northside WWTP Information : Received : 05/19/2022 229 Northside Drive Danville, VA 24540 Report Number : 22-139-0001 REPORT OFANALYSIS Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 57924 Matrix: Solids Sample ID : LTS B-Basin 22-1353 Sampled: 5/17/2022 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 9290 mg/Kg - dry 481 1 05/25/22 22:16 TJS 6010D Total Kjeldahl Nitrogen 49000 mg/Kg - dry 4810 1 05/25/22 14:00 JPJ ;M-4500-NH3C-TKI` Potassium 4000 mg/Kg - dry 192 1 05/25/22 22:16 TJS 6010D Iron 35000 mg/Kg - dry 192 1 05/25/22 22:16 TJS 6010D Aluminum 41500 mg/Kg - dry 96.2 1 05/25/22 22:16 TJS 6010D Ammonia Nitrogen 10300 mg/Kg - dry 1920 1 05/27/22 13:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 113 mg/Kg - dry 89.4 1 05/25/22 14:37 ZBD 4500NO3F-2011 Cadmium <1.92 mg/Kg - dry 1.92 1 05/25/22 22:16 TJS 6010D Chromium 60.0 mg/Kg - dry 4.81 1 05/25/22 22:16 TJS 6010D Mercury <3.00 mg/Kg - dry 3.00 1 05/26/22 16:26 JTR SW-7471B Total Volatile Solids 46.9 % 0.010 1 05/24/22 15:27 FMM SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 9 Waypointo ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Client: 'Inframark CASE NARRATIVE Project: VPDES Permit# VA0060593 Lab Report Number: 22-139-0001 Date: 6/1 /2022 Metals Analysis Method 601 OD Sample 95262 Analyte: Aluminum QC Batch No: 1-618303/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95262 Analyte: Iron QC Batch No: 1-618303/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95262 Analyte: Potassium QC Batch No: 1-618453/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95262 Analyte: Magnesium QC Batch No: 1-618303/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95262 Analyte: Manganese QC Batch No: 1-618303/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95262 Analyte: Lead QC Batch No: 1-618303/1-617886 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 95654 (SB-6-1) Analyte: Mercury QC Batch No: 1-618609/1-618266 Page 5 of 9 Waypoint".0 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 6 of 9 WayPAoInt.. NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 79434 Customer Name: 'Inframark Report Number: 22-139-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 05/19/2022 07:44:53 Page 7 of 9 cr) m 25 LO v raj 13 ° O Gi Y� D W a r�+ 3 t 1.7 N i d CLOtdj C41 [[3 y•}�� y IL G U in v i. • O Zj "�YaS mix V a�Nw \ Y (�� L C- N �p to LLi ❑ 12 J a W E LO ❑ 0 ❑ 4�A `^ i o n .8 m Em E U) E a N d E W r o r x{ CO d E c & 5 9 E R� fq a 8& V 5 _ r d Ii 0. G V ti M gg f7f��1 R a7 Y E � n n � m � tr awe G E c m N + i 04 c It N y C W jIJ 4 o a � y (s{j papoepe Gas � y3 m Z c^ n p m �^ m e p O aIjS*du-(]) jo 4ej(91 U n 3 3 (Aail w jQ&a) xple N r a E pdy F � a ;jauia3uo7 M AgwnH r LL ac cc I c N S V] m x r c (� IVJ 4 C LO D V c N ri D w Q d N O — > Y _ 'S ~ C04 T � = �D I J c 9 p E G o LO r = C r1 u E aC 4 i nU) n F a E ��� mot � m rop� ni I= all- Q m ~ F% c N 3 E L4] NLO �..+ g= -K oe a ty E y C� E ° a ~ U rryv m E Z o W x pp Egn �' u 5 N a 45 Page 8 of 9 wnuapgAjo"-� wnlualas� ?IuasjvA peal la)PINX wnlwoay3A. wnlwpe:)- G •- aul2 ? 7 T aaddo) asaueSueyy wnulwnlV uoas - wnlpoS Q _ wnlsau`deVy - _ wnl3leo _ p - JnjlnS - a wn'Sselad snjoydsoyd (uoljelmleo) uaROJ;IN 31ueft ua$oa}IN Se a;IJIIN + aMI N uaBOJ;IN-eluowwV NNl ►4lulieMIV — Hd SA-L% -- S1.% j 2 _ 1 -Od S - zZ u1se8 9 Sll .ajdweS (VEV61 3unomV VA 3ueodAeM) d1MM VA `alpAuep i1aeweipI iio4 s=sal spiposoi8 pailr&*ji Page 9 of 9 5/17/2022 mg/kg mg/L Equiv Weight Milli Equiv Sodium 9290 484.009 23 21.04387 Calcium 13900 724.19 20 36.2095 Magnesium 4020 209.442 12 17.4535 Percent Solids 5.21 SAR 4.06 SAR = Na+ a (Ca2+ + M;42+ ) 21.04387 0.5( 36.21 2 + 17.45350 2 ) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Danville WQ Permit Number: WQ0036561 WWTP Name: Northside WWTP NPDES Number: VA0060593 Monitoring Period: From l/l/2022 To 12/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ 1 Gamma Ray ❑ 1 Pasteurization ❑ Class B: I Alt. (1) Fecal Density 0 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o 1;xcee- ences 1'�requency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NWN CFU 152 207 294 col/ g 0 l Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 NWN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑,► Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑`' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Alan Gould - Project Manager Preparer Name and Title (type or print) AyI0 (51ul,/Feb 1, 2023 ALan D. Gould (Feb 1. 2023 14:13 EST) Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) 1/30/2023 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 May 03, 2022 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on April 12, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Stacy Heasley stacy.heasley@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Lab ID Sample ID Matrix Date Collected Date Received 30481039001 CATWALK 131 #1 Solid 04/12/22 07:10 04/12/22 12:02 30481039002 CATWALK 132 #2 Solid 04/12/22 07:50 04/12/22 12:02 30481039003 CATWALK 133 #3 Solid 04/12/22 07:15 04/12/22 12:02 30481039004 CATWALK 134 #4 Solid 04/12/22 07:55 04/12/22 12:02 30481039005 CATWALK 135 #5 Solid 04/12/22 07:20 04/12/22 12:02 30481039006 CATWALK 136 #6 Solid 04/12/22 08:00 04/12/22 12:02 30481039007 CATWALK 136 #7 Solid 04/12/22 08:05 04/12/22 12:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: INFRAMARK-DANVILLE 30481039 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30481039001 CATWALK 131 #1 SM 2540G-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039002 CATWALK 132 #2 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039003 CATWALK 133 #3 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039004 CATWALK 134 #4 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039005 CATWALK 135 #5 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039006 CATWALK 136 #6 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30481039007 CATWALK 136 #7 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Sample: CATWALK B1 #1 Lab ID: 30481039001 Collected: 04/12/22 07:10 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.0 % 0.10 1 04/19/22 16:17 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <250 CFU/g 250 0.25 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B2 #2 Lab ID: 30481039002 Collected: 04/12/22 07:50 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.6 % 0.10 1 04/19/22 16:19 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <294 CFU/g 295 0.295 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B3 #3 Lab ID: 30481039003 Collected: 04/12/22 07:15 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.9 % 0.10 1 04/19/22 16:20 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <196 CFU/g 197 0.197 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B4 #4 Lab ID: 30481039004 Collected: 04/12/22 07:55 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Percent Moisture Date: 05/03/2022 01:07 PM Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver 95.7 % 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/19/22 16:22 N2 Page 5 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Sample: CATWALK B4 #4 Lab ID: 30481039004 Collected: 04/12/22 07:55 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <233 CFU/g 233 0.233 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B5 #5 Lab ID: 30481039005 Collected: 04/12/22 07:20 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.0 % 0.10 1 04/19/22 16:27 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <167 CFU/g 167 0.167 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B6 #6 Lab ID: 30481039006 Collected: 04/12/22 08:00 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 93.4 % 0.10 1 04/19/22 16:30 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <152 CFU/g 152 0.152 04/12/22 19:07 04/13/22 17:45 Sample: CATWALK B6 #7 Lab ID: 30481039007 Collected: 04/12/22 08:05 Received: 04/12/22 12:02 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.7 % 0.10 1 04/19/22 16:34 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <189 CFU/g 189 0.189 04/12/22 19:07 04/13/22 17:45 Date: 05/03/2022 01:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/03/2022 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK-DANVILLE Pace Project No.: 30481039 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30481039001 CATWALK B1 #1 SM 2540G-11 498382 30481039002 CATWALK B2 #2 SM 2540G-11 498382 30481039003 CATWALK B3 #3 SM 2540G-11 498382 30481039004 CATWALK B4 #4 SM 2540G-11 498382 30481039005 CATWALK B5 #5 SM 2540G-11 498382 30481039006 CATWALK B6 #6 SM 2540G-11 498382 30481039007 CATWALK B6 #7 SM 2540G-11 498382 30481039001 CATWALK B1 #1 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039002 CATWALK B2 #2 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039003 CATWALK B3 #3 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039004 CATWALK B4 #4 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039005 CATWALK B5 #5 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039006 CATWALK B6 #6 SM 9222D-2006 498361 SM 9222D-2006 498364 30481039007 CATWALK B6 #7 SM 9222D-2006 498361 SM 9222D-2006 498364 Date: 05/03/2022 01:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 CHAIN -OF -CUSTODY Analytical Request Document LasU$ a)ulx A.M' fllarkaraar/�igin�akte[IH;ereor�tsfPac-VorkarderNumber aceAnal `_ytrcal' Chain -of -Custody is a LEGAL DOC(JMFNT- Complete all relevent fields ; WO# • 30481039 Company: Inframark-Danville Billing Information: Inframark-Danville WWTP ! ALL SHADE Address: 229 Northslde Dr., Danville, VA 24540 229 Northside Drive Danville, VA 24540 Container Preservative Type 30481039 U. Report To: Robert.Clifton@lnframark.com Email To: Stephanie.Mosko@lnframark.com ••Preservative Types: (Tnitric acid, 2 sulfuricauo, i6f n.,.-,,»,1-,-, (6) methanol, (7) sodium bisulfate, (a) sodium thiosutfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, Copy TO. Kimberly.Wickemeyer@Inframark.cam Site Collection Info/Address: (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (of other Danville VA WWTP 229 Nonhside, Dr., Danvife, VA24540 Analyses Lab Prnf[le/Line; Customer Project Name/Number: State: County/City: Time Zone Collected: yob Samgle Rece Pt CheCk71"s Inframark-Danville (client #: 92-618203) VA /Danville [ ] PT [ ] MT [ ] CT V IET —t Phone: 434-799-5137 Site Facilit ID #; / Y Compliance Monitoring? P g• ' _ CUs�9dy Sa819 iPFd BRRt/�tltaG Custgtiy Sig3�atvres present..:; Email: kimberiy.ivickemeyer@inrramark.com Danville, VA WWTP permit VA0060593 [ jVYes [ ] No' Collector Signature"Psesen# Collected By (print): �%., rV Purchase Order #; DW PWS ID #: Q} $noes Sntact Corzec Hottls Rober# Clifton (, Quote #: 0 ) t tj C� "f g ❑W Location Code: Sut'#iGent WoTume ; Cn ¢cted B (si nature): urnaround Date Re aired: Immediate) Pace on Ice; Y Samples iioceived nn Ice WOA [teadspace acceptable Its by 04/30/2022 [ Yes [ ] Na USDAt;egttlated Soils Sample Disposal: 111� Dispose as appropriate [ ] Return [ ) Archive: [ ) Hold: Rush: [ ] Same Day [ ] Next Day [ ] 2 Day [ ] 3 Day [ ] 4 pay [ ] 5 Day (Expedite Charges Apply) Field Filtered (if applicable): [ ] Yes `/] No Analysis: * Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Sail/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix ` Comp / Grab Collected (or Composite Start) Composite End Res CI # of Ctns Date Time Date Time a wa SL* Grab o4r12r2o22 07:10 - - - - - - - - No 1 Catwalk SL* Grab 0411212022 07:50 - - - - - - - - No 1 Catwalk SL* Grab 0411212022 07:15 - - - - - - - - No 1 Catwalk B4 #�4 SL* Grab 0411212022 07:55 _ _ _ _ _ No 1 atwa 5 SL* Grab 04112f2022 07:20 - - - - - - - - No 1 Catwalk SL* Grab 0411212022 08:00 - - - - - - - - No 1 a wa SL* Grab 04112f2022 08:05 - - - - - - - - No 1 Customer Remarks / Special Conditions / Possible Hazards: *Biosolids for Fecal Coliform Relinquished by/Company: (Signature) Kid" Date/Time: Received by/Company: (Signature) Date/Time: Relinquished by/Company: (Signature) Date/Time: Rec ived by/Company: ($ignature) Date/Time: it ® fy A/ -. �! r 1 V Prclogln. (Signature) j Date/Time: r cei ed by/Company: (Signature) r y Date/Ti PM; Non Conformanc@(s} Page: Page 9 of 1 of: 0 LIMS73 Lab Sample Condition Upon Receipt (West Virgin" 40# : 3048103g Client Name: �r�l AM: SDH Due Date: 04/27/22 CLIENT: TNFRAMRl2K Courier: ElFed Ex ❑ UPS ❑ USPS lent ElCommercial ❑ Pace [ Tracking #: Custody Seal on Cooler/BoxlContainers Present: ❑ yes ❑ no Seals intact: ❑ yes ❑ no Thermometer Used (_ 7-*4 Type of lee: oetBlue Done Cooler Temperature Observed Temp 5 ° C Correction Factor: ' C Final Temp: T. A— * C Comments pH gaper Lat# =contents: ate and Initials of person examining Yes NIA Chain of Custody Present: 1. Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COC: 4. Sample Labels match COC: -Includes dateltime/ID Matrix: 5. Samples Arrived within Hold Time: 6. Short Hold Time Analysis (<72hr remaining): 7. Push Turn Around Time Requested: g. Sufficient Volume: 9. Correct Containers Used: -Pace Containers Used: 10. Containers Intact 11. Orthophosphate field filtered: 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) 13. Filtered volume received for Dissolved tests: 14. All containers have been checked for preservation: exceptions: VOA', coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: 15. Initial when complete Dateltime samples provided to lab . Tests not preserved: Headspace in VOA Vials: 16. Trip Blank Present: Trip Blank Custody Seals Present: 17. Initial when completed: ate:Ly- Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date£fime: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. *Pitt review is documented electronically in LIM$, when the Project Manager closes the SRF Review schedule in LIM$. The status may be reviewed in the Status section of the Workorder Edit Screen. $Cttt? WV - rev.082219 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 6/8/2022 Date Sample Rcvd: 5/5/2022 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 05OS2217 Sample: Danville Composite 5/5/22 Total Solids Volatile Solids o Volatile Solids Week 1 1.20 0.580 0.488 Week 2 1.22 0.660 0.539 Week 3 1.14 0.540 0.475 Week 4 0.990 0.460 0.469 Week 5 1.01 0.490 0.487 Van Kleek Reduction (%): 0.39 I hereby certify that I have reviewed and approve these data. .Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 ca d d A 9 R O 0 o w Q� O; V O v O ev G m u � 11J/mil A b � a C C -G •C �'+ c G •G C 1 = C C E Yen r�.i C: �e L a C y R ry L C y R cp v C y A A A co ] W U A U' U F54 N 0 P. Q E c N U o O 0 0 0 T�1 x 0 vvi U U U a o n U U C ❑v 00 r— o wr ° a ra •21, w H 3�� o ZD0 r� �•� G o a 60 x1 VO D ICI U U .D y1 w 'V7'1 'V7-1 C cn V) 3 a 1� h C �jL Or oa A ry W N VI � s 3 Q M U -• R- z w� ro, a O p• 0. n � i � - - � L y � x o '.G � c U� .n cn a � a .� m a a 'N Ucn � u Ct - z QQ W P-4 C"l En t� C Ch rn r I 1 1 1 I 1 cn F. LIE. I O0 � e O cn C) rl Q J o p _ II o p, a 0 li 7f •--� N A � _ O O O +n vn v� v1 W � C a a y N Q S o. a � O p FD O O !-� G & n U O kp A W zo0 W � � c 7 W z rr- 7; s� IT a Unl u Q p O :. O T v� E, a CO HG 3 " LX� O b �a v N[ _1 3 0 n n vz ,n A L d C � ij eC a •G d a L .cL u .v m = `f Y Seo e❑ O O 2 = « a N n V Q a m El ti 13 (9 a)Z V7 ` Gi uJ A. ;M m E E 00 bA ~ ~ v U tw Lf) Ln = x Y m m v o m m �+ N w a t O so > E z a LL LL� a h• C E C Cl) N o 1 n C1 '0 a) E r1 u coO a U a � i U Y a Ul c 7 •> C •� d' OcutA a ? c a y -le O a v v Q c> O Q1 2 7 Ln c E ui n C CII +-� ra aj G K N O V7 O L m # U 1 V u ai c c a h. — ❑ +� cu O a ° rn 0 Q U Q C a o v E E E aCj L H F G � 000 N `N • L V W h 0r4�� Zn m d 0 } o d a o m E L 0 OT `n ° CI i m u uO txo O E o x "O J d ti i Q� 4 CL O LU H E M V Z @J E V] - I O W O a)V N Z N O ' � O U ra N h �` ` U z E w Q} a a�i p W F- a > } N L O � l4 (Y U m E cr cr c c c E O �J z a••+ t 0 J i (Ij NI LU J CL LL O 0 Ln ❑ ❑ ❑ ❑ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Danville WQ Permit Number: WQ0036561 WWTP Name: Northside WWTP NPDES Number: VA0060593 Monitoring Period: From l/l/2022 To 12/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ 1 Gamma Ray ❑ 1 Pasteurization ❑ Class B: I Alt. (1) Fecal Density 0 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o 1;xcee- ences 1'�requency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NWN CFU 192 239 270 col/ g 0 l Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 NWN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑,► Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑`' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Alan Gould - Project Manager Preparer Name and Title (type or print) AyI0 (51ul,/Feb 1, 2023 ALan D. Gould (Feb 1. 2023 14:13 EST) Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) 1/30/2023 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 May 16, 2022 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cynthia Walker cynthia.walker@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Lab ID Sample ID Matrix Date Collected Date Received 30484084001 CATWALK 131 #1 Solid 04/26/22 07:45 04/26/22 12:20 30484084002 CATWALK 132 #2 Solid 04/26/22 08:20 04/26/22 12:20 30484084003 CATWALK 133 #3 Solid 04/26/22 08:00 04/26/22 12:20 30484084004 CATWALK 134 #4 Solid 04/26/22 08:15 04/26/22 12:20 30484084005 CATWALK 135 #5 Solid 04/26/22 08:05 04/26/22 12:20 30484084006 CATWALK 136 #6 Solid 04/26/22 08:10 04/26/22 12:20 30484084007 CATWALK 132 #7 Solid 04/26/22 08:25 04/26/22 12:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: INFRAMARK- DANVILLE 30484084 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30484084001 CATWALK 131 #1 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084002 CATWALK 132 #2 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084003 CATWALK 133 #3 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084004 CATWALK 134 #4 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084005 CATWALK 135 #5 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084006 CATWALK 136 #6 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30484084007 CATWALK 132 #7 SM 2540G-11 NEM 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Sample: CATWALK B1 #1 Lab ID: 30484084001 Collected: 04/26/22 07:45 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.3 % 0.10 1 05/10/22 16:54 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <270 CFU/g 271 0.271 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B2 #2 Lab ID: 30484084002 Collected: 04/26/22 08:20 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.0 % 0.10 1 05/10/22 16:56 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <250 CFU/g 250 0.25 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B3 #3 Lab ID: 30484084003 Collected: 04/26/22 08:00 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.8 % 0.10 1 05/10/22 16:57 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <238 CFU/g 239 0.239 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B4 #4 Lab ID: 30484084004 Collected: 04/26/22 08:15 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Percent Moisture Date: 05/16/2022 07:51 AM Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver 96.2 % 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/10/22 16:59 H1,N2 Page 5 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Sample: CATWALK B4 #4 Lab ID: 30484084004 Collected: 04/26/22 08:15 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <263 CFU/g 264 0.264 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B5 #5 Lab ID: 30484084005 Collected: 04/26/22 08:05 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.8 % 0.10 1 05/10/22 17:00 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <192 CFU/g 193 0.193 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B6 #6 Lab ID: 30484084006 Collected: 04/26/22 08:10 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.3 % 0.10 1 05/10/22 17:01 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <213 CFU/g 213 0.213 04/26/22 19:40 04/27/22 18:40 Sample: CATWALK B2 #7 Lab ID: 30484084007 Collected: 04/26/22 08:25 Received: 04/26/22 12:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.1 % 0.10 1 05/10/22 17:02 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <256 CFU/g 257 0.257 04/26/22 19:40 04/27/22 18:40 Date: 05/16/2022 07:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/16/2022 07:51 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK- DANVILLE Pace Project No.: 30484084 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30484084001 CATWALK B1 #1 SM 2540G-11 503484 30484084002 CATWALK B2 #2 SM 2540G-11 503484 30484084003 CATWALK B3 #3 SM 2540G-11 503484 30484084004 CATWALK B4 #4 SM 2540G-11 503484 30484084005 CATWALK B5 #5 SM 2540G-11 503484 30484084006 CATWALK B6 #6 SM 2540G-11 503484 30484084007 CATWALK B2 #7 SM 2540G-11 503484 30484084001 CATWALK B1 #1 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084002 CATWALK B2 #2 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084003 CATWALK B3 #3 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084004 CATWALK B4 #4 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084005 CATWALK B5 #5 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084006 CATWALK B6 #6 SM 9222D-2006 504046 SM 9222D-2006 504047 30484084007 CATWALK B2 #7 SM 9222D-2006 504046 SM 9222D-2006 504047 Date: 05/16/2022 07:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 aceAnalytical CHAIN -OF -CUSTODY Analytical Request Document Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields LAB Use entt „- Am—`--' - 4 Workorder Number or WO# : 3048408 ONLY U 30484084 ger: - PreservaLive iypm: 11) nitric acid, (21 sulfuric acid, (3) hydrochloric acid, (9) sodium hydroxide, (5) zinc acetate, (6) methanol, (71 sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other Company: Inframark-Danville Billing Information: 229 North a Drive WTP Danville, VA zasao Address: 229 Northside Dr., Danville, VA 24540 Report To: Robert.Clifton@lnframark.com Email To: alieia.erumpton@inframark.eom Copy To: Kimberly.Wickemeyer@lnframark.com Site Collection Info/Address: Danville VA WWfP 229 Northaide, Dr., Danville, VA, 4q- Analyses Lab Profile/Line: Customer Project Name/Number: Inframark-Danville (client #: 92-618203) State: County/City: Time Zone Collected: VA /Danville ( ] PT [ ] MT [ ] CT VIET u� Lab Sample Receipt Checklist: Custody Seals Present/Intact Y N NA Custody Si natvras Present Y N NA ComplianceMonitoring7 Email: kim4edy.wickemeyer�inframark.com Danville, VA WWTP permit VA0060693 P [ Wes [ ] No CL v 6. (D rn J E L0 y �-0 0 U N LL Collector Signature Present Y N NA Bottles Intact Y N NA correct Bottles Y N NA Sufficient Volume Y N NA Samples Received on Ice Y N NA VOA - Headspace Acceptable Y N NA USDA Regulated Soils Y N NA Samples in Holding Time Y N NA Residual Chlorine Present Y N NA Cl Strips: Sample p]R Acceptable Y N NA pH Strips: Sulfide Present Y N NA Lead Acetate Strips: LAB USE ONLY: Lab Sample # ! Comments: Collected By (print): Robert Clifton Purchase Order#: 17 (�r7 Quote #: 00109788 1 i DW PWS ID #: DW Location Code: Coll ted By (signature): �- Turnaround Date Re wired: results by b5115/2022 Immediately Pace on Ice: [V Ies [ ] No Sample Disposal: L., Dispose as appropriate [ ] Return [ ] Archive: [ ]Hold: Rush: [ ] Same Day [ ) Next Day [ ] 2 Day [ ] 3 Day [ ] a Day [ ] 5 Day (Expedite Charges A ply] p Field Filtered (If applicable]: [ ] Yes No Analysis: * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Sail/Solid {SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix' Comp/ Grab Collected (or Composite Start) Composite End Res Cl #of Ctns Date Time Date Time Catwalk SL' Grab !i -7a ---- ---- No 1 a Wa SL* Grab 01 - - - - - - - - No 1 Catwalk SL' Grab ,t - - - - - - - - No 1 Catwalk B4 #4 SL" Grab /1 j - - - - - - - - No 1 Catwalk 5 #5 SL* Grab 1, - - - - - - - - No 1 Catwalk SL' Grab if 080--- ---- INO 1 Catwalk SL* Grab , # r - - - - - - No 1 Customer Remarks / Special Conditions / Possible Hazards: 'Mosollds for Fecal Coliform Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT {<72 hours]: Y N N/A Lab Sample Temperature Info: Temp Blank Receivedd Y/� A Therm ID#: i r ' Cooler 1 Temp Upon Recelp , oC Cooler 1 Therm Corr. Factor_, ,pC Cooler 1 Corrected Tem oC P� Comments: Packing Material Us d: Lab Tracking #: Radchem sample(s) screened (<500 cpm}; Y N NA Samples received via: FEDEX UPS Cllent Courier Pace Courier Relinquished by/Company: Pignature) Y Date/Time: Received by/Com (Signature) Date/Tjm@ ((1�rr MTJL LAB USE ONLY Table #: Acctnum: Template: Prelogln: pM. PB: Relinquished by omp y: [Sin r Date/Time:yA�C ff y l r" 1C.Y Received by/C mpany: (Signature) Date/Tlme: Trip Blank Received: Y N NA HCL McOH TSP Other Rel]n wished by/ omp�[Signature[ ff�c —_ JJI` Date/Time: eceiv y/Com any; (SI hat re] �f 'q � r Date Me: on Conformance{s): YES / NO page: Rage 9 of 10 of: u• 4 / LIMS73 Lab Sample Condition Upon Receipt (West Virc wO# ; 30 FaceArlalylical PM! SDH Client Name: ` , ra n+w� L- CLIENT: INFRAM Courier: ❑ Fed Ex ❑ UPS ❑ USPS lient ❑ Commercial ❑ Pace L_I Utner: Tracking #: Custody Seal on Cooler/Box/Containers Present: ❑ yes ❑ no Seals intact: ❑ Thermometer Used Type of Ice: 10 Blue None Cooler Temperature Observed Temp �• �) C CorrectionFactor`t—i7• C Fi Comments: pH paper Lot# Date contents: Yes No NIA $084, Due Date- 05/06/22 RK Yes ❑ no ial Tempe C nd Initials of person examining Chain of Custody Present: 1. Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COO: 4. Sample Labels match COC: -Includes dateltime/ID Matrix: 5. Samples Arrived within Hold Time: 6. Short Hold Time Analysis (<72hr remaining): 7. Rush Turn Around Time Requested: 8. Sufficient Volume: 9. Correct Containers Used: -Pace Containers Used: 10. Containers Intact: 11. Orthophosphate field filtered: 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) 33. Filtered volume received for Dissolved tests: 4. All containers have been checked for preservation: exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: 5. itial when completed Dateltime provided I samples D lab 7 Z� Tests not preserved: Headspace in VOA Vials: 16. Trip Blank Present: Trip Blank Custody Seals Present: 17. I--,- Inital when completed: Client Notification! Resolution: Person Contacted: Date/Time: Contacted Comments/ Resolution: By. ❑ A check in this box indicates that additional information has been stored in ereports. m *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status ay be reviewed in the Status section m of the Workorder Edit Screen. rl $CUR WV-rev.082219 AAUMI Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 6/15/2022 Date Sample Rcvd: 5/10/2022 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 05102208 Sample: Danville Composite 5/10/22 Total Solids Volatile Solids Jo Volatile Solids Week 1 1.37 0.640 0.468 Week 2 1.28 0.630 0.493 Week 3 1.05 0.510 0.487 Week 4 0.960 0.480 0.500 Week 5 0.960 0.500 0.519 Van Kleek Reduction (%): -22.89 I hereby certify that I have reviewed and approve these data. ryla Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 q.o 0 "Chti9. 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A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ 1 Gamma Ray ❑ 1 Pasteurization ❑ Class B: I Alt. (1) Fecal Density 0 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o 1;xcee- ences 1'�requency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NWN CFU 167 209 244 col/ g 0 l Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 NWN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑,► Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑`' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Alan Gould -Project Manager Preparer Name and Title (type or print) AyI0 (51ul,/Feb 1, 2023 ALan D. Gould (Feb 1. 2023 14:13 EST) Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) 1/30/2023 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 May 25, 2022 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cynthia Walker cynthia.walker@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Lab ID Sample ID Matrix Date Collected Date Received 30485744001 CATWALK 131 #1 Solid 05/03/22 07:30 05/03/22 13:00 30485744002 CATWALK 132 #2 Solid 05/03/22 08:10 05/03/22 13:00 30485744003 CATWALK 133 #3 Solid 05/03/22 07:35 05/03/22 13:00 30485744004 CATWALK 134 #4 Solid 05/03/22 08:05 05/03/22 13:00 30485744005 CATWALK 135 #5 Solid 05/03/22 07:40 05/03/22 13:00 30485744006 CATWALK 136 #6 Solid 05/03/22 08:00 05/03/22 13:00 30485744007 CATWALK 132 #7 Solid 05/03/22 08:15 05/03/22 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: INFRAMARK- DANVILLE 30485744 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30485744001 CATWALK 131 #1 SM 2540G-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744002 CATWALK 132 #2 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744003 CATWALK 133 #3 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744004 CATWALK 134 #4 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744005 CATWALK 135 #5 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744006 CATWALK 136 #6 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30485744007 CATWALK 132 #7 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Sample: CATWALK B1 #1 Lab ID: 30485744001 Collected: 05/03/22 07:30 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.8 % 0.10 1 05/19/22 16:32 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <238 CFU/g 238 0.238 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B2 #2 Lab ID: 30485744002 Collected: 05/03/22 08:10 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.9 % 0.10 1 05/19/22 16:34 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <196 CFU/g 196 0.196 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B3 #3 Lab ID: 30485744003 Collected: 05/03/22 07:35 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.1 % 0.10 1 05/19/22 16:36 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <204 CFU/g 204 0.204 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B4 #4 Lab ID: 30485744004 Collected: 05/03/22 08:05 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Percent Moisture Date: 05/25/2022 08:22 AM Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver 95.4 % 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/19/22 16:38 H1,N2 Page 5 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Sample: CATWALK B4 #4 Lab ID: 30485744004 Collected: 05/03/22 08:05 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <217 CFU/g 217 0.217 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B5 #5 Lab ID: 30485744005 Collected: 05/03/22 07:40 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.0 % 0.10 1 05/19/22 16:40 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <167 CFU/g 167 0.167 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B6 #6 Lab ID: 30485744006 Collected: 05/03/22 08:00 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.9 % 0.10 1 05/19/22 16:42 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <244 CFU/g 244 0.244 05/03/22 20:30 05/04/22 20:05 Sample: CATWALK B2 #7 Lab ID: 30485744007 Collected: 05/03/22 08:15 Received: 05/03/22 13:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.2 % 0.10 1 05/19/22 16:44 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <208 CFU/g 208 0.208 05/03/22 20:30 05/04/22 20:05 Date: 05/25/2022 08:22 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/25/2022 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK- DANVILLE Pace Project No.: 30485744 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30485744001 CATWALK B1 #1 SM 2540G-11 504867 30485744002 CATWALK B2 #2 SM 2540G-11 504867 30485744003 CATWALK B3 #3 SM 2540G-11 504867 30485744004 CATWALK B4 #4 SM 2540G-11 504867 30485744005 CATWALK B5 #5 SM 2540G-11 504867 30485744006 CATWALK B6 #6 SM 2540G-11 504867 30485744007 CATWALK B2 #7 SM 2540G-11 504867 30485744001 CATWALK B1 #1 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744002 CATWALK B2 #2 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744003 CATWALK B3 #3 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744004 CATWALK B4 #4 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744005 CATWALK B5 #5 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744006 CATWALK B6 #6 SM 9222D-2006 504013 SM 9222D-2006 504015 30485744007 CATWALK B2 #7 SM 9222D-2006 504013 SM 9222D-2006 504015 Date: 05/25/2022 08:22 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 CHAIN -OF -CUSTODY Analytical Request Document ;a'-- e A n'a lXica ` Chain -of -Custody is il LEGAL DOCUMENT -Complete all reievent fields LAB USE Of WO# : 30485744 beror i Container 3011 5744 __ Company: Inframark-Danville Billing Information: Inframark-Danville WWTP 229 Northside Drive Danville, VA 24540 Address: 229 Northside Dr., Danville, VA 24540 Report To: Robert.Clifton@lnframark.eom Email To: alieia.erumpton@inframark.eom "Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, {6) methanol, (7) sodium bisulfate, (8) sodium thlosulfate, {9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (o) TSP, (U) Unpreserved, (0) other copy To: Kimberly.Wiekemeyer@Inframark-cam Site Collection Info/Address: Danville VAWWTP 229 Nodhside, Dr., Danville, VA 24540 Analyses Lab Profile/Line: Customer Project Name/Number: Inframark-Danville (client #: 92-618293) State: County/City: Time Zone Collected: VA /Danville [ ] PT [ ] MT [ ] CT ET V N •7 ,2 to tQ v ••L- O (� 0 LL Lab Sample Receipt Checklist: Custody Seals Present/Intact Y N NA Custody signatures Present: Y N NA Collector Signature Present Y N NA Bottles Intact Y N NA Correct Bottles Y N NA Sufficient Volume Y N NA Samples Received on ice Y N NA VOA - Headspace Acceptable Y N NA USDA Regulated Sells Y N NA Samples in Holding Time Y N NA Residual Chlorine Present Y N NA Cl Strips: Sample pH Acceptable Y N NA pH Strips: Sulfide Present Y N NA Lead Acetate Strips: LAB USE ONLY: Lab Sample # / Comments: Phone:434-799-51137 Small: himbedy.wckemeyer�lnframark.com Site/Facility ID 9-1 Danville, VA WWTP permit VA0060593 Compliance Monitoring? [ Yes [ ] No Collected By (print): Robert Clifton Purchase Order d: 137975 Quote#; 00109788 DW PWS ID M DW Location Code: Co (�gnature): Turnaround Date Required: results by 05/18/2022 Imme late y Pac a on Ice: *ti Yes [ ]No Sample Disposal: IVI Dispose as appropriate [ ] Return [ I Archive: [ ]Hold: Rush: [ ] Same Day [ ] Next Day I ] 2 Day [ ] 3 Day [ ] 4 Day [ ) 5 Day {ExpedlteChargesApply) Field Filtered (if applicable): [ )Yes No Analysis: * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid {SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix * Comp / Grab Collected (or Composite Start) Composite End Res Cl p of Ctns Date I Time Date Time Catwalk SL* Grab 05/03/22 075V - - - - - - - - No 1 X_ Catwalk SL* Grab 05/03/22 0 - - - - - - - - No 1 CatwalkSL* Grab 05/03/22 fl 735- - - - - - - - No 1 Catwalk B4 #4 SL* Grab 05/03/22 flQjD - - - - - - - - No 1 Catwalk 5 SL* Grab 05/03/22 O7 - - -- - - -- No 1 Catwalk SL* Grab 05/03/22 Q - - - - - - - - NO 1 Catwalk SL* Grab 05/03/22 - - - - - - - - No 1 Customer Remarks / Special Conditions / Possible Hazards: 'Blosolids for Fecal Coliform Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (02 hours); Y N N/A Lab Sample Temperature Info: Temp Blank e e d N NA Therm IDN: Cooler 1 Temp Upon Receipt; C Cooker 1 Therm Corr. Factort o''S o Cooler 1 Corrected Temp, Comments: Packing Material Used: Lab Tracking M Radchern sample(s) screened (c500 cpm): Y N NA Samples received vl FEDEX UPS Client Courier Pace Courier Relinquished by/company: Si nature q// (Signature) ) ����/'� ,� G Date/Time: Date �/,�� � ! �` - Received by/Company: [Signature) ' 3 • G17 � Date/Time: �7 � ✓ 0 `�% MTJLLAB USE ONLY Table Ac Relin ' hed by/C mpan : (SigUnatu�ree))�) Datt.re//TTiim�e:/ Received bye/Co pa y; (Signature[ Date/Tlme: Template: Prelogin: Trip Blank Received: Y N NA HCL McOH TSP Other Relinquished by/Comp, y: Z�{Sig!natOure) DateTme: c ived Co pan ignatuvre,v 4 Date�yV® b� PM: IRB: Non Canfarmance(s); YES / NO Page: Re 9 of 10b of: o LIMS73 Lab Sample Condition Upon Receipt (West Virgi O# . 304g574 3/22 0 Due Date: 05/1 piaceArrarytical PM : SDH '�v� Client Name: — a CLIENT : INFRAI�ARK Courier: ❑ Fed Ex ❑ UPS ❑ US PS fient ❑ Commercial ❑ Pace [1 Tracking #: Custody Seal on Cooler/BoxlContainers Present: ❑ yes o Seals intact: ❑ yes ❑ no Thermometer Used lr� E�- - T e of Ice: Wet Blue None Cooler Temperature C 'C C Observed Temp Correction Factor+C)p5 Final Temp: Comments pH paper Lot# Date and Initials of person contents' 9, a Yes I No NIA Chain of Custody Present: 1. Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COC: 4. Sample Labels match COC: -Includes dateltimellD Matrix: 5. Samples Arrived within Hold Time: 6. Short Hold Time Analysis (a72hr remaining): 7. Rush Turn Around Time Requested: 8. Sufficient Volume: g. Correct Containers Used: -Pace Containers Used: 10. Containers Intact: 11. Orthophosphate field filtered: 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) 13. Filtered volume received for Dissolved tests: 14, All containers have been checked for preservation: exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: 5. Initial when completed._ E �F} Dateltime samples provided to lab V Tests not preserved: Headspace in VOA Vials: 6. Trip Blank Present: Trip Blank Custody Seals Present- 17. Inifiat when completed: r Date: Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Contacted ❑ A check in this box indicates that additional information has been stored in ereports. `PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. SCUR WV - rev.682219 AMP - Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 6/20/2022 Date Sample Rcvd: 5/17/2022 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 05172204 Sample: Danville Composite 5/17/22 Total Solids Volatile Solids % Volatile Solids Week 1 1.30 0.660 0.506 Week 2 1.19 0.580 0.485 Week 3 1.01 0.470 0.471 Week 4 1.04 0.600 0.577 Week 5 0.900 0.450 0.505 Van HIeek Reduction (%): 0.38 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 P2 V ca p ACOD �f a w a a O r C n/ N W O 7r t ` � N A � a con D a z w U W a i ;41 U 0 C 0 >C QI U C� j a n O v7 h u v U A A Ca � � U C CO 63 ca N- n. o v❑ O O J CL O = u o m ry cl _ ❑ •� C to m O o - -0 C• c u - m .. w` a O a =1 E ui ECL ai v 0 v `^ '� O v E cj E 0 ~ ~ _ ~ d� r4 E Q C m } 7 4 C rl ri 3 O 0 N /► U•1 III O n n VI ❑ uo D l0 c6 m m ar * ❑ Ln u Q} C X zO w O L •� N O a Li a a n• C L a cu cu Cs a O � a v aJ Q w m H a co I u N q v +1 Ln (N aJ N U Y W v tlJ Z Ln O p o q � ro V Y —_ q 'a L) C- Q } C: 3 v ! J E W a > v ? a 7 �Ln n O C LLiCP m N CL O O C .S i-Qf Y U rst ~ U Z El aj d rv' E C o U Q Q a U o vY Z i E E E Q3 E v CS rCt } ■ N V i ? u S tn O An 0 N N tV z CL E ] ID m [6 a� 4 U 0 m m u 0 o C �+ o O-A ai ra o .. q7 IV/� f�� C Ln 6 to o Z +- L @� W orN to h o rl O aC U �O Ul Uj b z L cu U ' Lu �- u Z ro _ C U E �' R tB o � U a°1c z a O �-- � } 1 a- - •r J -0 O V7 LU j . Q N a a - O` 6 0) -0 L U ro O Z> V) `^ ❑ ❑ ❑ ❑ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Danville WQ Permit Number: WQ0036561 WWTP Name: Northside WWTP NPDES Number: VA0060593 Monitoring Period: From l/l/2022 To 12/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ 1 Gamma Ray ❑ 1 Pasteurization ❑ Class B: I Alt. (1) Fecal Density 0 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o 1;xcee- ences 1'�requency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NWN CFU 147 202 263 col/ g 0 l Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 NWN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑,► Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑`' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Alan Gould - Project Manager Preparer Name and Title (type or print) Ayalv 0 (o9/W Feb 1, 2023 ALan D. Gould (Feb 1.2023 14:13 EST) Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) 1/3 0/2023 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 June 03, 2022 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on May 17, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cynthia Walker cynthia.walker@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Lab ID Sample ID Matrix Date Collected Date Received 30490043001 CATWALK 131 #1 Solid 05/17/22 07:30 05/17/22 12:33 30490043002 CATWALK 132 #2 Solid 05/17/22 08:00 05/17/22 12:33 30490043003 CATWALK 133 #3 Solid 05/17/22 07:35 05/17/22 12:33 30490043004 CATWALK 134 #4 Solid 05/17/22 07:50 05/17/22 12:33 30490043005 CATWALK 135 #5 Solid 05/17/22 07:40 05/17/22 12:33 30490043006 CATWALK 136 #6 Solid 05/17/22 07:55 05/17/22 12:33 30490043007 CATWALK 132 #7 Solid 05/17/22 08:05 05/17/22 12:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: INFRAMARK-DANVILLE 5/17/22 30490043 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30490043001 CATWALK 131 #1 SM 2540G-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043002 CATWALK 132 #2 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043003 CATWALK 133 #3 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043004 CATWALK 134 #4 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043005 CATWALK 135 #5 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043006 CATWALK 136 #6 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE 30490043007 CATWALK 132 #7 SM 254OG-11 LPO 1 PASI-BV SM 9222D-2006 JCD 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Sample: CATWALK B1 #1 Lab ID: 30490043001 Collected: 05/17/22 07:30 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 95.3 % 0.10 1 05/25/22 13:30 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <213 CFU/g 213 0.213 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B2 #2 Lab ID: 30490043002 Collected: 05/17/22 08:00 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.1 % 0.10 1 05/25/22 13:31 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <256 CFU/g 257 0.257 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B3 #3 Lab ID: 30490043003 Collected: 05/17/22 07:35 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.6 % 0.10 1 05/25/22 13:33 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <185 CFU/g 186 0.186 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B4 #4 Lab ID: 30490043004 Collected: 05/17/22 07:50 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Percent Moisture Date: 06/03/2022 03:58 PM Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver 95.1 % 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/25/22 13:34 H1,N2 Page 5 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Sample: CATWALK B4 #4 Lab ID: 30490043004 Collected: 05/17/22 07:50 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <204 CFU/g 205 0.205 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B5 #5 Lab ID: 30490043005 Collected: 05/17/22 07:40 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 93.2 % 0.10 1 05/25/22 13:36 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <147 CFU/g 148 0.148 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B6 #6 Lab ID: 30490043006 Collected: 05/17/22 07:55 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 94.2 % 0.10 1 05/25/22 13:38 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <172 CFU/g 173 0.173 05/17/22 17:30 05/18/22 17:27 Sample: CATWALK B2 #7 Lab ID: 30490043007 Collected: 05/17/22 08:05 Received: 05/17/22 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-11 Pace Analytical Services - Beaver Percent Moisture 96.2 % 0.10 1 05/25/22 13:41 H1,N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Lexington Fecal Coliform <263 CFU/g 264 0.264 05/17/22 17:30 05/18/22 17:27 Date: 06/03/2022 03:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2022 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK-DANVILLE 5/17/22 Pace Project No.: 30490043 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30490043001 CATWALK B1 #1 SM 2540G-11 506620 30490043002 CATWALK B2 #2 SM 2540G-11 506620 30490043003 CATWALK B3 #3 SM 2540G-11 506620 30490043004 CATWALK B4 #4 SM 2540G-11 506620 30490043005 CATWALK B5 #5 SM 2540G-11 506620 30490043006 CATWALK B6 #6 SM 2540G-11 506620 30490043007 CATWALK B2 #7 SM 2540G-11 506620 30490043001 CATWALK B1 #1 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043002 CATWALK B2 #2 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043003 CATWALK B3 #3 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043004 CATWALK B4 #4 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043005 CATWALK B5 #5 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043006 CATWALK B6 #6 SM 9222D-2006 508983 SM 9222D-2006 508986 30490043007 CATWALK B2 #7 SM 9222D-2006 508983 SM 9222D-2006 508986 Date: 06/03/2022 03:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 F�CF1VFi ��. Robert.Clifton@lnframark.com rmau io: allcia.crf. mpion(C_UInTramarK,coM ** Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosul€ate, (9) hexane (A) ascorbic acid, (B) ammonium sulfate, Copy To: Kimberly.Wickemeyer@lnfrarnark.com Site Collection Info/Address: (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (D) Other Danville VA WWTP 229 Northslde, Dr., Danville, VA 24540 Analvses Lah Prnfiirall Customer Project Name/Number: State: County/City: Time Zone Collected: Inframark-Danville (client #: 92-618203) VA /Danville [ }PT( ]MT[ ]CT VET Phone: 434-799-5137 Site/Facility ID #: Compliance Monitoring? Email: kimbetly.wickemeyer@inframark.com Danville, VA WWTP permit VA0060593 [ oes [ ] No Collected By (print): Purchase order #:137975 DW PWS ID #: Robert Clifton Quote #: 00109788 DW Location Code: Coll cted By (signatu 0: Turnaround Date Required: Immediately Packed on Ice: o-L- results by 06/01 /2022 [b�Yes [ IN. Sample Disposal: Rush: Field Filtered (if applicable): M Dispose as appropriate (j Return [ ] Same Day [ ] Next Day ( } Yes 6,1 No t 1 Archive: [ 1 Z Day [ ] 3 Day [ ] 4 Day [ ] S Day Analysis:' Samp7 i?H Acceptable ': Y N NA ( )Hold: {Expedite Charges Apply) pH-Stz�ps; * Matrix Codes (Insert in Matrix box below): Drinking Water [DW], Ground Water (GW), Wastewater (WW), Su3.fide PrOsent .X W Nil Lead, Acei#te Strips; Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay {B), Vapor (V), Other (OT) 0 Customer Sample ID P Matrix * Comp / Grab Collected (or Composite Start) Composite End Res CI # of Ctns N Lab Ssmpl e / comments Date Time Date Time a Wa SL* Grab �� D7 0 ---- ---- N o 1 a Wa SL* Grab r, b8 )o - - - - - - - - No 1 atwa SL* Grab � p�35 - - - - - - - - No 1 Catwalk B4 #4 SL• Grab y ©-7 - - - - - - - - No 1 walk5 SL* Grab 4� - - - - _ - - No 1 a Wa SL' Grab fi755 - - -- - - -- No 1 a Wa SL* Grab L, ff'F - - - - - - - - Nn 114 . ... .. Customer Remarks / Special Conditions / Possible Hazards: 'Eliosolids for Fecal Coliform Relinquished by/Company: (Signature) Date/Time: Relinquished by/Company: (Signature) Date/Time: 06"gz'� 5 - / 9 - as //121?.r) Received by/Company: (Signature) Date/Time: Received by/Cpmp�ny: (Signature) Date/Time: (Signature) Date/Tlme:iVontonforrhance(S} Page: PA.. YP§ I i110 . -: of: r 0 LIMS73 Lab Sample Condition Upon Receipt (West Virginia) WO# : 30490043 ° 0 ' f'aceAr lyhia! PM: CEW Due Date: 05/27/92 Client Name:OG CLIENT: INFRAMARK o Courier: ❑ Fed Ex ❑ UPS ❑ USPS D:Client ❑ Commercial ❑ Pace ❑ Other: Tracking #: Custody Seal on Cooler]Box/Containers Present: ❑ yes ❑ no Seals intact: ❑ yes ❑ no Thermometer used LXTAd U Type of Ice: Wet Blue None Cooler Temperature Observed Temp �' �Q C Correction Factor: 0'S C Final Temp: . a C_T pH paper Lot# Date and Initials of person examining Comments: contents: Yes I No NIA Chain of Custody Present: 1. Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COO: 4. Sample Labels match COC: -Includes dateltimellD Matrix: 5. Samples Arrived within Hold Time: 6. Short Hold Time Analysis (a72hr remaining): 7. Rush Turn Around Time Requested: 8. Sufficient Volume: l 9. Correct Containers Used: -Pace Containers Used: 10. Containers Intact: 11. Orthophosphate field filtered: 12, Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) 13. r Filtered volume received for Dissolved tests: 14. All containers have been checked for preservation: i exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: / 15. Initial when completed02L Date/time samples provided to tab - f - as Tests not preserved: Headspace in VOA Vials: 16. Trip Blank Present: Trip Blank Custody Seals Present: 17. LL Initial when completed: Date: r r Client Notification/ Resolution: Person Contacted: Comments/ Resolution: DateMme: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. SCUR WV - rev.082219 T AWO M1 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, IBC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: 6/22/2022 Date Sample Rcvd: 5/19/2022 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 05192213 Sample: Danville Composite 5/19/22 Total Solids Volatile Solids a Volatile Solids Week 1 1.65 0.770 0.466 Week 2 1.01 0.460 0.458 Week 3 0.960 0.440 0A53 Week 4 1.07 0.520 0.481 Week 5 0.910 0.450 0.498 Van Kleek Reduction (%): -13.55 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 rn q 0 0 a cn A o 0 o S a � a z s� QL W ea 3 � v c � o p.0 c-. 0 0 0 .QA a0 i..i h0 b0 r K Q +� C ca � cc ev v ON V'i O1 r1l ul o 0 GO e a O O O n ,n F 1O r 0 O II e N a n. c o it 13 v yfi � N o U U a o O O V1 kn Y'Y Vl a Nb o O tn W kn kn W PI O U U a Ln o 0 FO a U O4 u O O � N � O�•+, C � V)cf� -O h 4 •--� U 0 ZO O vUM3 cl N cco � a remit y 6! 'C U C C3 ❑ W Cd A a 3 L 0 0 0 � � H o � o > 0 0 0 0 Ln 4] '� knN c tn 4l n 'n u�j t o t" C = x a � R A A L c. w p• __ � v ;C u a � � o U a H 0 0 o L" e O � F• � O O u u ?- c II N o ao 0 0 o kn W � � � � d O or^ U O a a U v �v A C �F+ n ? Y E ? o of O c J _ `m E E o C 43 [Q — a D. C rl N io m Q c c „ m } u c� rl 3 O H Vx1 O LO u] c a o o o rr1 m a ✓� h TZ �r ' L�•J 'LU c: '� u ai Xt (��'� C o Q aCL X a o a Oa- ` ( v ♦ r Q m Z Ui w c X t LL- n II_ -a L V / L OO -6 � N u `� C y w G1 L L .ar L 4-J II O � N >^ V) °1 ' v aJ ,Le - aj E v Q v Z r o uQ s n } u Q O a o s > In W E a Q a v J O PO N as E \ I c a c Q 0 vi O rYa xt U vi y CJ Y � O Q � Y7 u ¢ a a N c vi (U + E E a) v� re r f N V LU U 3 W N Vl ON m V1 M1 N II O II fV I--m m . qy O E N -a, a cr.m CL IN 0 m m M Tco O ❑ o o 00 i Q Q n�Ui � E_ M o- m •Q H Q U 5 a L.L N L + Lq CD U CU a W ca � v z U� — o m r m C LM cu 0 ,u�1 N W = LAO N O —_ �� 0 cf U re O t y > E w w N Z m Lu _ V Ol �J Q II Q Q; m N s 7 Q�J N '0 r 'j N ':5 C cr Q � C U s O C: w m .Z; cu UO ii O to ❑ El El ❑ V NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY23-SL008054 k5i I"14'4+; 4 L Client: James Y Blackwell Advisor: Brent Collins Predictive 7402 NC Hwy 158 W EMA Resources Inc °± f' Yanceyville, NC 27379 755 Yadkinville Rd �- Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Caswell _1 Links to Helpful Information Sampled: 10/05/2022 Received: 10/10/2022 Completed: 10/20/2022 Farm: CS07 Client ID: 242509 Advisor ID: 405413 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 1.0 120-200 0 30 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.76 1.09 6.8 67 2.2 5.5 126 57 48 14 83 1573 961 633 633 1353 0.1 1 North Carolina Tcbwiv Truk f and Ct wmisskm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY23-SL008053 kSi l"14'4+;4, Client: Glenn Hodges Advisor: Brent Collins Predictive 2388 Allison Rd EMA Resources Inc °± f' Pelham, NC 27311 755 Yadkinville Rd �- Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Caswell _1 Links to Helpful Information Sampled: 10/05/2022 Received: 10/10/2022 Completed: 10/20/2022 Farm: CS09 Client ID: 535611 Advisor ID: 405413 Sample ID: 00003 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.92 1.17 8.3 82 1.5 6.1 129 49 70 9 57 410 262 337 337 108 0.2 2 North Carolina Tai wLv Truk f and Ctwinlsskm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY23-SL003059 k5i I"14'4+; 4 L Client: Marc Thomas Advisor: Brent Collins Predictive 730 Old Satterfield Rd. EMA Resources Inc °± f' Milton, NC 27305 755 Yadkinville Rd �- Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Caswell _1 Links to Helpful Information Sampled: Received: 08/24/2022 Completed: 09/01/2022 Farm: CS10 Client ID: 523433 Advisor ID: 405413 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 pH$ 0 0 0 Note: 12 Note: $ 2 - Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 pH$ 0 0 0 Note: 12 Note: $ Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.98 11.5 91 1.0 6.6 290 28 61 28 38 340 212 212 981 981 507 0.1 1 Sample ID: 00005 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 pH$ 0 0 0 Note: 12 Note: $ 2 - Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 pH$ 0 0 0 Note: 12 Note: $ Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 1.05 9.4 91 0.8 6.7 174 24 60 30 32 147 95 95 612 612 328 0.1 1 North Carolina Tai wLv Truk f and Ctwinlsskm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY23-SL000905 k5i I"14'4+;4, Client: David / Sledge Sartin Advisor: Brent Collins Predictive 3404 Park Springs Rd EMA Resources Inc °± f' Providence, NC 27315 755 Yadkinville Rd �- Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Caswell _1 Links to Helpful Information Sampled: Received: 07/18/2022 Completed: 07/26/2022 Farm: CS14 Client ID: 347847 Advisor ID: 405413 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 90 50 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 90 50 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 1.11 5.7 81 1.1 6.2 22 43 50 27 26 175 120 120 108 108 97 0.1 2 Sample ID: 00002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.8 120-200 40 40 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 40 40 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.08 6.4 71 1.8 5.5 43 48 48 19 41 352 228 228 168 168 113 0.1 2 North Carolina Tai wLv Truk f and Ctwinlsskm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL036094 k5i I"14'4+;4, Client: David / Sledge Sartin Advisor: Brent Collins Predictive 3404 Park Springs Rd EMA Resources Inc °± f' Providence, NC 27315 755 Yadkinville Rd �- Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Caswell _1 Links to Helpful Information Sampled: Received: 06/24/2022 Completed: 07/01/2022 Farm: CS14 Client ID: 347847 Advisor ID: 405413 Sample ID: 00003 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.3 120-200 60 80 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 60 80 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 0.98 8.8 85 1.3 5.8 35 29 53 30 31 103 79 79 319 319 173 0.1 1 North Carolina Tcbwiv Truk f and Ctwinlsskm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Signature Pages Final Audit Report Created: 2023-02-01 By: Brent Collins (brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAAS9_Y16lk7yUvN361-KRZEi_VtbZ_MyMb "Signature Pages" History Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2023-02-01 - 6:52:29 PM GMT- IP address: 206.85.202.26 P-► Document emailed to alan.gould@inframark.com for signature 2023-02-01 - 6:57:57 PM GMT Email viewed by alan.gould@inframark.com 2023-02-01 - 7:12:36 PM GMT- IP address: 65.254.177.125 dp Signer alan.gould@inframark.com entered name at signing as Al -an D. Gould 2023-02-01 - 7:13:38 PM GMT- IP address: 65.254.177.125 2023-02-01 Gip Document e-signed by Al -an D. Gould (alan.gould@inframark.com) Signature Date: 2023-02-01 - 7:13:40 PM GMT - Time Source: server- IP address: 65.254.177.125 Q Agreement completed. 2023-02-01 - 7:13:40 PM GMT 0 Adobe Acrobat Sign Danville Signature Page Final Audit Report 2023-02-03 Created: 2023-02-03 By: Brent Collins (brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAAPAt8oDuT_oOAJLNogS214ei3cl66AKAq "Danville Signature Page" History Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2023-02-03 - 2:14:09 PM GMT- IP address: 206.85.202.26 P-► Document emailed to johnsra@danvilleva.gov for signature 2023-02-03 - 2:14:39 PM GMT Email viewed by johnsra@danvilleva.gov 2023-02-03 - 2:15:47 PM GMT- IP address: 216.146.48.10 dp Signer johnsra@danvilleva.gov entered name at signing as Alan Johnson 2023-02-03 - 2:17:21 PM GMT- IP address: 216.146.48.10 Gip Document e-signed by Alan Johnson (johnsra@danvilleva.gov) Signature Date: 2023-02-03 - 2:17:23 PM GMT - Time Source: server- IP address: 216.146.48.10 Q Agreement completed. 2023-02-03 - 2:17:23 PM GMT 0 Adobe Acrobat Sign