WQ0004609_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * W00004609
Applicant/Permittee Wayne Farms LLC
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0004609
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
Wayne Farms Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for Wayne Farms, LLC - Dobson, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Wayne Farms NC 2022 Annual Report FINAL.pdf 8.24MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 27, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0004609
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of
Wayne Farms, L.L.C.-Dobson, NC.
If you have any questions or need additional information, please do not hesitate to contact
Matthew Wooten at [phone] or Alex Fox at [phone].
Sincerely,
01171 Y--
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Matthew Wooten, Wayne Farms, L.L.C.-Dobson
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

WAYNE FARMS, L.L.C. , NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0004609
2022 ANNUAL REPORT

Wayne Farms, L.L.C. - Dobson, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form & Annual Operations Summary
2. Annual Residual Sampling Summary Forms
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Control of Possible Nuisance Conditions
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W0004609 County Surry Year 2022
Facility Name (as shown on permit) Wayne Farms NPDES No. NC0006548
Land Application Operator S na o Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A— Residuals A licationSumm
Total number of application fields in the permit: 26
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 94_57
Total number of acres utilized for land application during the year: 50.90
Part B —Annual Cons fiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken,
I . Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
T All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All .monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities),
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
H. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specked
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specked on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, jnclud' g the possibility of fines and imprisonment for
knowing violations." /
Matthew Wooten Cornplex Mane er G (� 7IZ2
Permittee Name and Title (type or print) Signature of P muttee Date
02/01/2023
Signature of Preparer* Date tare of d Applier Date
(if different from. Permittee) (if A= from Permit and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (I2/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
WAYNE FARMS, L.L.C., NC
WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
MONTH/YEAR
April 2022
May 2022
November 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/14/2023 4:30:48 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
347,200.00
G
38.66
D
35.06
124,000.00
G
13.81
D
12.52
378,200.00
G
42.11
D
38.19
849,400.00
G
94.57
D
85.78

SECTION 2

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Wayne Farms
Lot Number:XA28089
Date Completed:02/20/2022
NIM�� Mr�
02/21/2022 3:01 PM
Approved and released by:
Project Manager II: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA28089
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to the matrix, the initial sample amount used for sample -001 was approximately 3X greater than the
standard procedure. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:XA28089-001
Description: Wayne Farms Matrix: Solid
Date Sampled:01/26/2022 0900 % Solids: 2.67 02/02/2022 0244
Date Received:01/28/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 02/02/2022 0244 NBW
30433
1 350.1
(Ammonia - N ) 350.1
5 02/10/2022 1906 DRD
31097
3
(Nitrate - N ) 9056A
10 02/17/2022 0935 AAB
32346
1
(Nitrite - N ) 9056A
1 02/02/2022 1932 SUH
30794
1
(Phosphorus) 365.1
10 01/31/2022 1647 DMA
01/31/2022 1327
30217
1
(Soil pH meas) 9045D
1 02/08/2022 0206 NBW
30888
1 351.4
(TKN) 351.2
2 02/08/2022 1615 DMA
02/08/2022 1024
31009
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
2.67
%
1
Ammonia - N (gas diffusion)
350.1
4300
190
97
mg/kg
1
Nitrate - N (soluble)
9056A
170 J
190
37
mg/kg
3
Nitrite - N (soluble)
9056A
4.4 J
7.5
3.7
mg/kg
1
Phosphorus
7723-14-0 365.1
16000
1900
370
mg/kg
1
Soil pH measured in water @
19.8 ° C
9045D
6.8
su
1
TKN
351.2
73000
3700
1900
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 02/01/2022 1016 JAB2
02/01/2022 0255
30167
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
3.0
0.72
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 02/01/2022 1817 KSH2
02/01/2022 0827
30046
3 3050B
601OD
1 02/04/2022 1610 KSH2
02/01/2022 0827
30046
4 3050B
6010D
1 02/05/2022 1610 KSH2
02/01/2022 0827
30046
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
5400
250
93
mg/kg
1
Arsenic
7440-38-2 6010D
4.5 J
9.3
3.1
mg/kg
1
Cadmium
7440-43-9 6010D
ND
3.1
0.78
mg/kg
1
Calcium
7440-70-2 6010D
23000
3100
390
mg/kg
1
Chromium
7440-47-3 6010D
11
6.2
1.5
mg/kg
1
Copper
7440-50-8 6010D
290
6.2
2.8
mg/kg
3
Iron
7439-89-6 6010D
8400
62
28
mg/kg
1
Lead
7439-92-1 6010D
8.4
6.2
2.8
mg/kg
1
Magnesium
7439-95-4 6010D
12000
3100
390
mg/kg
1
Manganese
7439-96-5 6010D
470
9.3
3.7
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:XA28089-001
Description: Wayne Farms Matrix: Solid
Date Sampled:01/26/2022 0900 % Solids: 2.67 02/02/2022 0244
Date Received:01/28/2022
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D
1 02/01/2022 1817 KSH2
02/01/2022 0827 30046
3 3050B
601OD
1 02/04/2022 1610 KSH2
02/01/2022 0827 30046
4 3050B
601OD
1 02/05/2022 1610 KSH2
02/01/2022 0827 30046
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Molybdenum
7439-98-7 6010D
10 J 25
6.2
mg/kg
4
Nickel
7440-02-0 6010D
16 J 25
6.5
mg/kg
1
Potassium
7440-09-7 6010D
7400 3100
390
mg/kg
1
Selenium
7782-49-2 601OD
ND 12
5.0
mg/kg
1
Sodium
7440-23-5 6010D
4800 3100
390
mg/kg
1
Zinc
7440-66-6 6010D
450 31
7.7
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
SaenpJes Receipt -Ch,=klist (SHO {MF0418C-15) Eiff0lsedAP9,r2020
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Yrs No 7+A I Ercurtmr v €eels iewc E.-sent, ware til irttuut and unbroker?
PI -I Strip ID. NA _ C]fIon[rc S[rip In- fest'd by, M"
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PM was Notified by: phone f ems,i] I face-i-face (ciMle. one) -
Yes No V NA 4, Is the cummercuil uuuril7'shacking Slip alLMhcd to this fdm77
Yas NO 5, lVene ,oiler c[Istady' procMules (rc.linqui Eledr„ oivr l) Callawe�?
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i"t s No 9- Was cial lec[inn data a 6ruc listed nn all €aErpla containers?
ayes i M N0 ] b. Tiirl all C 3nikGinCr laL�e] itJf�maaocn (IJl}, dy tiirio}agree with t �e COC7
Z Yes No 11. Wore tests to be peeffmmcd listed on the MC.?
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(Unbrokon, ]i& On' &L.-)?
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14- ory ail sampiles rexivExi wid]itt �4 the 'rtahlirrgtiMeOr4$ htiurs, whkchf,Yer eramvs firS;?
15. Wenp any "rririlm containers nussingjaxtess Orf.Js one) rrnoJes No4 listed on C0C7
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Were cltertt renIarE;s,ftcccue€is rki,e, Tee]treykd dilutions, MS %iSDU rksignhtiuns, etc
sctly t anscri6ed kurr -lie �-'CIC into the Comment scWokt i:r LIMS?
W2q, the quotonumbar iistpd on the rE3ntairer label? If yes, ()E.ote
Sample Preser-4^ntiorr he Contpieted Tor arjy %,.rrp]c(s) it1curNotly 1+xG5erved or with headslaaEc .)
fiample(sj Nn wee receivea incormr-11Y pr'esffvEd rand were adju,"d aoeonJingly
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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SECTION 4

SUMM111
ENVIRONMENTAL TECHNOLOMZ3. INC
Arraly0ca1 Laboralorfas
August 21, 2019
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Wayne Farms
Dear Nate Roth:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Order No.: 19071834
Summit Environmental Technologies, Inc. received 1 sample(s) on 7/26/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 36

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 19071834
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 8/21/2019
CLIENT: Synagro
Project: Wayne Farms
WorkOrder Narrative:
19071834: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19071834-OOIA TCLP-SVOC_8270E: Surrogate recovery was outside of the laboratory established
acceptance criteria for: p-Terphenyl-d14. All other surrogates exhibited recoveries within the
acceptance criteria.
Original
Page 2 of 36

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� WO#: 19071834
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co, Date: 8/21/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
EkiV1RONM@NtaL YECHHQ WGhES, INQ Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Wayne Farms
Lab SampleID Client Sample ID
19071834-001 Wayne Farms
Tag No Date Collected
7/25/2019 9:00:00 AM
Workorder
Sample Summary
WO#: 19071834
2l Aug-l9
Date Received Matrix
7/26/2019 9:50:00 AM Sludge
Page 4 of 36

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Summit Environmental Technologies, Inc.
PESUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.com
Analytical Report
(base report)
WO#: 19071834
Date Reported: 8/21/2019
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID:
19071834-OOIA
Project:
Wayne Farms
Client Sample ID Wayne Farms
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
20.7
Surr: Phenol-d6
26.9
Surr: Nitrobenzene-d5
24.2
SW7470A SW7470A Analyst: DNS
0.00500 mg/L 1 8/2/2019 5:29:00 PM
SW6010D SW3010A Analyst: EAM
0.500
mg/L
1
8/5/2019 6:03:12 PM
5.00
mg/L
1
8/5/2019 6:03:12 PM
0.100
mg/L
1
8/5/2019 6:03:12 PM
0.200
mg/L
1
8/5/2019 6:03:12 PM
0.500
mg/L
1
8/5/2019 6:03:12 PM
0.0500
mg/L
1
8/5/2019 6:03:12 PM
0.500
mg/L
1
8/5/2019 6:03:12 PM
SW1010
Analyst: TAH
°F
1
7/31/2019 12:01:41 PM
SW8270 SW3510C Analyst: BJH
0.200
mg/L
2
8/6/2019 6:13:00 PM
0.500
mg/L
2
8/6/2019 6:13:00 PM
0.500
mg/L
2
8/6/2019 6:13:00 PM
0.100
mg/L
2
8/6/2019 6:13:00 PM
10.0
mg/L
2
8/6/2019 6:13:00 PM
0.0400
mg/L
2
8/6/2019 6:13:00 PM
0.100
mg/L
2
8/6/2019 6:13:00 PM
0.200
mg/L
2
8/6/2019 6:13:00 PM
0.200
mg/L
2
8/6/2019 6:13:00 PM
0.500
mg/L
2
8/6/2019 6:13:00 PM
0.500
mg/L
2
8/6/2019 6:13:00 PM
10 - 109
%Rec
2
8/6/2019 6:13:00 PM
10 - 109
%Rec
2
8/6/2019 6:13:00 PM
19 - 120
%Rec
2
8/6/2019 6:13:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 6 of 36

Summit Environmental Technologies, Inc.
PESUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.com
Analytical Report
(base report)
WO#: 19071834
Date Reported: 8/21/2019
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID:
19071834-OOIA
Project:
Wayne Farms
Client Sample ID Wayne Farms
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: 2,4,6-Tribromophenol 27.0 10 - 120 %Rec
Surr: 2-Fluorobiphenyl 24.7 22 - 117 %Rec
Surr: p-Terphenyl-d14 25.9 34 - 116 S %Rec
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
47.1
Surr: DCB
50.1
SW8270 SW3510C Analyst: BJH
2 8/6/2019 6:13:00 PM
2 8/6/2019 6:13:00 PM
2 8/6/2019 6:13:00 PM
SW8081 SW3510C Analyst: MES
0.0250
mg/L
10
8/6/2019 4:13:00 PM
0.0500
mg/L
10
8/6/2019 4:13:00 PM
0.00500
mg/L
10
8/6/2019 4:13:00 PM
0.00500
mg/L
10
8/6/2019 4:13:00 PM
0.00500
mg/L
10
8/6/2019 4:13:00 PM
0.00500
d mg/L
10
8/6/2019 4:13:00 PM
0.00500
d mg/L
10
8/6/2019 4:13:00 PM
10 - 119
%Rec
10
8/6/2019 4:13:00 PM
10 - 119
%Rec
10
8/6/2019 4:13:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)-SOLID
2,4-D ND 0.0100
2,4,5-TP ND 0.00500
Surr: DCAA 99.9 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
SW8151A SW8151A Analyst: MES
d mg/L 1 8/13/2019 5:34:00 PM
mg/L 1 8/13/2019 5:34:00 PM
%Rec 1 8/13/2019 5:34:00 PM
SW8260
Analyst: CTB
0.250
mg/L
50
8/5/2019 2:00:00 PM
0.250
mg/L
50
8/5/2019 2:00:00 PM
5.00
mg/L
50
8/5/2019 2:00:00 PM
0.250
mg/L
50
8/5/2019 2:00:00 PM
0.250
mg/L
50
8/5/2019 2:00:00 PM
2.50
mg/L
50
8/5/2019 2:00:00 PM
0.250
mg/L
50
8/5/2019 2:00:00 PM
0.250
mg/L
50
8/5/2019 2:00:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 7 of 36

MMIT
Summit Environmental Technologies, Inc. Analytical Report
PESU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone] WO#: 19071834
Website: http://www.settek.com Date Reported: 8/21/2019
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID:
19071834-OOIA
Project:
Wayne Farms
Client Sample ID Wayne Farms
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
Analyst: CTB
TCLP VOLATILES ANALYSIS
Trichloroethene
ND
0.250
mg/L
50
8/5/2019 2:00:00 PM
Vinyl chloride
ND
0.100
mg/L
50
8/5/2019 2:00:00 PM
Surr: 4-Bromofluorobenzene
93.9
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
Surr: Dibromofluoromethane
97.3
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
Surr: Toluene-d8
97.0
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.490
mg/Kg
1
7/31/2019 12:26:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: VVK
PH (SW9045D)
pH
6.7
s.u.@20.00
1
7/29/2019 3:21:02 PM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
7/31/2019 12:26:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 8 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
fr
3310 Win St.
summlmr
Analv n tes Report
ENOROMMEWAL YECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
19071834
Wehsite: http://www.settek.com
21Aug-l9
Client: Synagro
State: NW
Project: Wayne Farms
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19071834-OOIA Sludge
Flashpoint Determination (1010)
Flashpoint (1407)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW1311/8151)-solid
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)-solid
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Version #2
Page 9 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
19071834
Wehsite: http://www.settek.com
21Aug-l9
Client: Synagro
State: NW
Project: Wayne Farms
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19071834-OOIA Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Version #2
Page 10 of 36

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Page 35 of 36

�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTALTECHNOLOGiES.lftC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafyacal Laboralnrlas TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19071834 RcptNo: 1
Logged by: John A.Semenik
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
7/26/2019 9:50:00 AM
7/26/2019 11:18:05 PM
7/29/2019 2:54:58 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4.
Shipping container/cooler in good condition?
Yes
d❑
No ❑
Custody seals intact on shipping container/cooler?
Yes
❑
No ❑
Not Present V
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
❑d
No ❑
NA ❑
6.
Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No ❑
NA ❑
7.
Sample(s) in proper container(s)?
Yes
❑d
No ❑
8.
Sufficient sample volume for indicated test(s)?
Yes
❑d
No ❑
9.
Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No ❑
10.
Was preservative added to bottles?
Yes
❑
No ❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
14.5
Goodl
Not Present
Page 36 of 36

SECTION 5

Wayne Farms Land Application Program
Permit #WQ0004609
Calendar Year 2022
Animal processing wastewater residuals were land applied in
two events in the year 2022. The biosolids were sampled in the
start of the year to cover the entire year since we hauled less
than 300 dry tons per year.
The biosolids land applied in 2022 had sufficient lime added to
raise the pH of the uniform mixture to a pH of 10 for thirty
minutes prior to being surface land applied. This was
performed to control possible nuisance conditions (see Section
II, Item 7 in permit #WQ0004609).

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SECTION 6

Agricultural Lime Application Log
Year: 2022
Project: Wayne farms
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
Lime is in the sludge

SECTION 7

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