WQ0032855_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0032855
Applicant/Permittee Town of Rutherfordton
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Zach Key
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3367776909
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0032855
Has Current Existing permit number
Applicant/Permittee Address*
129 N Main St. Rutherfordton, NC 28139
Facility Name*
Town of Rutherfordton Class B Residuals Program
Please provide comments/notes on your current submittal below.
Land Application Annual Report for the Town of Rutherfordton Permit No. WQ0032855
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Annual Report WQ0032855.pdf 5.28MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/28/2023

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0032855
County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
US Biosolids, Inc.
Year: 2022
Town of Rutherfordton
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
A Yes LJ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number ofapplication fields in the peri-nit:1
16
Total number of fields utilized for land application during the year:
4
Total amount of dry tons applied during the year for all application sites:1
19.31
Total number of acres utilizes for land application during the year:1
29.3
rart ts - Annual C:ompiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. H Yes .,] No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pFl was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pl-I of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached,
6) The facility did not exceed any ofthe Pollutant Concentration 1-units in I SA NCAC 021' .1 105(a) or the Pollutant
Loading Rates in I5A NCAC 021' .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 021' .l 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. 1 am aware that there are significant penalties for submitting false information, including the
possibility of tines and imprisonment for knowing violations."
roux
Perrrtittee Name and Title (type or print)
Signature of Permittee Date
Signature orPreparer* Date Signature of Laril Applier Date
(il'different from Permitice) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 5039 (r) and I5A NCAC 02T.1102 (26) QENR FORM ACF (1212006)

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ANNUAL, METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Rutherfordton Total Dry Tons Applied (Annual): 11.38
Permit #: WQ0032855 Cation Exchange Capacity (non 503 only):
Operator: Stuart Beam Owner: Stuart Beam Predominant Soil Series: ApB
Acres Used: 14.9 Acres Permitted: 14.9 Site #: HE Field #: 7
Residual Analvsis Data (Heavv Metals and Total Phncnhorus nu- ma/lco 0/. !Znlidc nen qan Pn.•nn..r mil.
Com-
posite
Date
Total
Phos-
-4311U. X ■acarr c►trtaN rtreu t_ uau1n1As 1% aHWHIaren in mcf5trrpt-
Total
�.
2i
_._..
31
4v
51
6I
7;
_...
$
9
_ .
10
1! j
12'
DT/Ac.!
App-
Event
0.76
Arsenic
0.096
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Cadmium
0.019
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Copper
1.067
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
1.067
Chromium
0.048
0,000
0.000
0-000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Lead
0.057
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.057
Mercury
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Molybdenurn
denum
0.048
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
[0.048
Nickel
0.048
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.048
Selenium
0.096
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Zinc
1.803
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.803
Total
Phos-
26.740
0.000
0.000
0.000
0,000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
26.740
horus
--- ---,r------ �•--•-.-•.J .•. ..a ..t auwa a,a,J uv4Yuacut v- prrpttw ru unucr my uirectton or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1-7
VO4-, - -
Signaof Land Apptier
DENR FORM MFLSF (12/2006)

ANNUAL, METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field I.,oading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Rutherfordton Total Dry Tons Applied (Annual):
WQ0032855
Stuart Beam Owner:
7? Acres Permitted:
Cation Exchange Capacity (non 503 only):
Stuart Beam Predominant Soil Series:
7.2 Site #: 11E Field #:
1.02
ApB
8
Residual Analysis Data (Neavv Metals and 'rntad Phncnhnr..c *led- mall.- O/.. C.,.I:A, .- tCf-- o...._- u',_
Com-
posite
Date
rotal
Phos-
vhorus
q.12
DT/Ac./
_
-q
App.
m
Event
0.14
Arsenic
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.018
Cadmium
0,004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.197
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4A00
0.000
4.000
0.000
0.197
Chromium0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Lead
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Mercury
0,005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.005
denum0.009
denum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Nickel
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.000
0.009
Selenium
0.418
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Zinc
0.333
0.000
0.000
4.400
0.000
0A00
0.000
0.000
0.000
0.000
0.000
0.000
0.333
Total
Phos-
4.935
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.935
horns
« . - -• - ••••�++���•••�... ++�aa Incl.a.cu u5suct [fey wrccuvn ursupervision in accoroance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
SignIt ure of [..and APP tier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Rutherfordton Total Dry Tons Applied (Annual): 1.22
Permit #: WQ0032855 Cation Exchange Capacity (non 503 only):
Operator: Stuart Beam Owner: Stuart Beam Predominant Soil Series: PbB2
Acres Used: 1.6 Acres Permitted: 1.6 Site #: HE Field #: 10A
Residual Analysis Data (Heavv Metals and TntnI Phncnhnrne neP me/Ley 0/,. Cni.a..... o-.., u,k.
Com-
posite
Date
'Non
-■■auaa we%-nvy ivaviat rivAu uunutnt±J it_d1Ctimi-e1t to tnunerpr
Total_
z;
s;
4~
5
6
7
8
9
_
10
11 :`
12
DT/Ac./
_.
_ _..
o
App.
co
Event
0.76
y
Arsenic
0.095
0.000
o.aoa
0.000
0.000
0.000
0.000
0.000
0.00o
0.000
0.000
0.000
0.095
Cadmium
0.019
0.000
0.000
0,000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.-000
0.019
Copper
1.064
0.000
0.000
0.00a
0.000
0.000
0.000
1 0.000
0,000
0.000
0.000
0.00a
1.064
Chromium0.048
O'000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.048
Lead
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.057
Mercury
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Molyb-
d n m
0.048
0.000
0.000
0.000
0.000
0,00a
0.000
0.000
0.000
0.000
0.000
0.000
0048
Nickel
0.048
0.000 10.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.048
Selenium
0.095
0.000
0.000
0.000
0,000
0.000
o.000
0.000
0.000
0.000
0.0 00
0.000
0.095
Zinc
1.798
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
1,798
Total
Phos-
26.670
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
26.670
horus
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-
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r . _
- --.,I - t•-.•-..� .,..«.•, ...a.....a a,ILMUMcu. vraa tlrctia1ru uuucr my uirectlon or supervision In accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sig na of 1 and Ap lier
P Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Rutherfordton Total Dry Tons Applied (Annual): 5.69
Permit #: WQ0032855 Cation Exchange Capacity (non 503 only):
Operator: Stuart Beam Owner: Stuart Beam Predominant Soil Series: PsC2
Acres Used: 5.6 Acres Permitted: 5.6 Site #: HE Field #: 12
Residual Analysis Data (Heavv Metals and Total Phncnhoruc uce malka- 0/ cnlidc tics+ Dow Poreont 141.
Corn-
posite
Date
Total
Phos-
phorusMENNEEMENEEN
t%unuai rieavv ivietat rietu t,oautnQs it_aictimrert in inciaerPi!
Total
�
?s
_3
a
5
6
71
8�
9
10J
11 ;
12
DT/AC.;
-�
0
App.
is
l=vent
1.02
Arsenic
0.127
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.127
Cadmium
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.040
0.040
4.044
0.425
Copper
1.418
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.418
Chromium
0.064
0.000
0.000
4.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Lead
0.076
1 0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
Mercury
0.037
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
0.037
0 064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
denum
-denum
Nickel
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Selenium
0.127
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.127
Zinc
2.398
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.398
'rota i
Phos-
35.560
0.000
0.000
0.000
0.000
0.000
0.000
0.400
0.000
0.000
0.000
0.000
35.560
horus
• L« 9 A.V, uuucl pcttaty in law, tuat tilts uucument was prepareu under my airection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signs�Llreof Land �, lier
pp Date
DENR FORM MFISF (12/2006)

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Z
u
<
LJJUON
JO awa
I
u
CL
0
C',
U-
V)
LL.
0
LL
w
Z
LU
0

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Rutherfordton
W WTP Name: Mown of Rutherfordton W W-I-P
Monitoring Period: From 1/1/2022 To
WQ Permit Number: WQ0032855
NPDF.S Number: NCO25909
12/31 /2022
Pathogen Reduction 05A NCAC f12T 11ni�►- PipaLo;nfl;,.f.. 11-1 . h:-.—A —A -[.____. _._
Class A:
Al(. A (time'tenip) ❑
Alt B (Alk Treatnient)❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative performed (Class A only) indicate "Process to Furtlier Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatnient ❑
Thermophilic ❑
Beta Ray ❑
Gamma Kay ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density 21
All. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantiv Reduce Pathogens":
Lime Stabilization ❑
All -Drying ❑
Composting .1
jAerobic Digestion ❑
Anaerobic Digestior ❑
If applicable to alternative performed (Class A or Class B) complete the foliowin monitoring data:
Parameter
Allowable bevel
in Slud-e
h
Pathogen Density
Number ot
Excee-
Frequency
9 y
of Analysis
Sam le
p
Type
na ytica
fech-
Minima
Geo. MeanMaximu
Units
Fecal Colilorm
2 x 0 to the
wer
per gram of
total solids
MPN
839.94
1088
1964.5
MPN/g
0
7
grab
sm9221e
CFU
1000 mpn per gram
oftotal solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Y1i\�l_!•.l\. r_\ILf LIl INE\\KI I I I%■II I1ELSE 1 WAN fs J r• XWOMI iTa fT ll TitALT.T.S�.TiT I'i�1.7T.I�Sf1+1+A!!
Alt.1 (VS reduction) Lj
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) WAIL
4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) L1
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
l�T,h T.r•
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
■.\� ■ ar a�.n i 114 o [ elk 1 nivtr r4 1 (please cnCCK the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met "
J "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
A_N �� WWCh 0'R.C. Dennis Key US 131osolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and "Title (if applicable)(type or print)
1
Signature of reparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM PVRF 02T (12/2006)

Waypoint,
ANALYTICAL
46381
US Rosolids Inc
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number:22-227-0002
Lab No : 58911
Sample ID: Rutherfordton
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypointanalytical.com
Project Rutherfordton
Information :
REPORT OFANAL YSI.S
Report Date : 08/23/2022
Received : 08/15/2022
Taw,& Mt (i,owr
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8111/2022 9:00
Test
Results
Units
MOL
DF
Oate I Time
Analyzed
By
Analytical
Method
Moisture
99.2
%
0.010
1
08/17/2215:42
FMM
SM-254OG
Sulfur
13100
mg/Kg - dry
1250
1
08/19/22 16:13
EAL
6010D
Calcium
15400
mg/Kg - dry
6250
1
08/19/22 16:13
EAL
6010D
Aluminum
16SOO
mg/Kg - dry
625
1
08/19/22 16:13
EAL
6010D
Manganese
439
mg/Kg - dry
62.5
1
08/19/22 16:13
EAL
6010D
Organic N
121800
mg/Kg - dry
31250
1
08/22/22 11:20
CALCULATION
Nickel
<31.3
mg/K9 - dry
31.3
1
08/19/22 16:13
EAL
6010D
Lead
<37.5
mg/Kg - dry
37.5
1
08/19/22 16:13
EAL
6010D
Arsenic
<62.5
mg/Kg - dry
62.5
1
08/19/22 16:13
EAL
6010D
Selenium
<62.5
mg/Kg - dry
62.5
1
08/19/22 16:13
EAL
6010D
Test
Results
Units
MOL
DF
Date i Time
By
Analytical
Analyzed
Method
Total Solids 0.750 % 0.010 1 08/17/22 15:42 FMM SM-254OG
Phosphorus 17500 mg/Kg - dry 625 1 08/19/22 16:13 EAL 6010D
Copper 698 mg/Kg - dry 62.5 1 08/19/22 16:13 EAL 6010D
Total Kjeldaht Nitrogen 122000 mg/Kg - dry 31300 1 08/22/22 11:20 )P) iM-4500-NH3C-TKP
Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit
Page 3 of 8

•
Waypoint.
ANALYTICAL
46381
US Biosolids Inc
Dennis Key
958 Moots Road
Roaring River , NC 28669
Report Number: 22-227-0002
Lab No : 58911
Sample ID : Rutherfordton
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 fax [phone]
www.waypointanalytical.com
Project Rutherfordton
Information :
REPORT OFANAd YSIS
Report Date : O8/23/2022
{q
Received : 08/15/2022
T'Wit Mt Gfvgw t
,
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/11/2022 9:00
Potassium
5060
mg/Kg - dry
1250
1
08/19/22 16:13
EAL
6010D
Magnesium
3550
mg/Kg - dry
625
1
08/19/22 16:13
EAL
6010D
Sodium
4500
mg/Kg - dry
3130
1
08/19/22 16:13
EAL
6010D
Iron
20900
mg/Kg - dry
1250
1
08/19/22 16:13
EAL
6010D
Zinc
1180
mg/Kg - dry
156
1
08/19/22 16:13
EAL
6010D
Ammonia Nitrogen
<12500
mg/Kg - dry
12500
1
08122/22 12.30
3P3
SM-4500-NH3C
Nitrate+Nitrite-N
704
mg/Kg - dry
606
1
08/22/22 15:53
ZBD
4500NO3F-2011
Cadmium
<12.5
mg/Kg - dry
12.5
1
08/19/22 16:13
EAL
6010D
Chromium
<31.3
mg/Kg - dry
31.3
1
08/19/22 16:13
EAL
60100
Mercury
<18.0
mg/Kg - dry
1810
1
08/18/22 11:59
i3S
SW-74718
pH
6.4
s.u.
1
08/22/22 09:42
SAR
9045D
Molybdenum
<31.3
m9/Kg - dry
31.3
1
08/19/22 16:13
EAL
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

—0
X
C14
cn
C14
0
z
0
z
z
�5
W
U)
z
CL
0
C14
CD
9
x
0
z
0
z
z
z
F—
z
z
C*)
c
00
fa

SAR
Sodium Absorption Ratio
Na: Sodium (Mg/L) Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L I Equivalent weight
Na(MgIL) Qpj.MgIQ M jMg/L)
I
M�iMEI
875
SAR= Na Milli EquivalenV[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.733982 (From Mg/L entered above)
J_ SAR= 035 (From ME entered below)
Q I Ca (ME) I Mg (ME)
1.5 5.8 2.2
The amour
amount of i
Permitting!

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 11/16/2022
Reported: 12/27/2022
For: Rutherfordton
Comments:
Sample Number Parameter Sample ID Result
221116-30-01 30 Day Benchscale Rutherfordton 20.0
Respectfully submitted,
X�- � � " �-' J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
STATESVILLE
ANALYTICAL
Unit Method Analyzed Analyst
EPA625-R-92/0 11/16/2022 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

30 Day Bench Worksheet
Sample 1D # 2201116-30-01
WEEK 1 Date: 11/16/22 16:00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.88
0.66
2
0.85
0.64
3
0.88
0.65
Average:
0.87
0.65
0.7471
WEEK 2 Date: 11/23/22 16:00
Samples
Total Solids
Volatile Solids
'% Volatile Fraction
1
0.89
0.66
2
0.87
0.64
3
0.86
0.63
Average:
0.87
0.64
0.73.56
WEEK 3 Date: 11/29/22 16:00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.85
0.62
2
0.86
0.63
3
0.89
0.65
Average:
0.87
0.63
0.7241
WF'F'K d Datet 12/5/22 10:110
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.81
0.58
2
0.80
0.57
3
0.80
0.58
Average:
0.80
0.58
0.7250
WRIPM S nAte- 12/12/22 16.00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.76
0.53
2
0.75
0.53
3
0.77
0.54
Average:
0.76
0.53
0.6974
WEEK 6 Date: 12/20/22 15:00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.71
0.49
2
0.75
0.53
3
0.76
0.54
Average:
0.74
0.52
0.7027
Van Kleeck Reduction: 0.7471 - 0.7027 X 100 = 20.0 %
0.7471 - ( 0.7471 X 0.7027)
Final Result: 20.0%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

p A &AMk FZ
0 R A (7, (3 VI P A TF - r, r: t,, s t- r., I ABORATORIES, INC,
%% kM.11,NRL.%BS.C(Al
PFP,D,7-7" -:1 ANALYSES
X
Nrl:
C"A I
.Ph. SAMP

� AWA
P"R
PIRO SIPT• ACC UPATe- PC � I AM I-C
I A.BORA'I'ORIES, INC
2217 Graham Park Drive
PO Box 411483
Charlotte. NC 28241-1483
NC Cert # 20, SC Cert # 99003001
CLEW NAME: �U.SBIOSOLIDS, INC.
SAMPLE ID- RUTHERFORDTON
SAMPLE DATE: W)1105�
ANALYSIS: E 2 W-1 mrsTelaigrol-.iy, 100ROWT, 061grow, NEI
ANALYSIS METHODMAMOWW8
0 j
146108
fecal C011form
Geometric Mean=
1
509
39.81%
1,278.64
2
431
50.34%
856.74
-7
3
328
39.07%
839.94
4
722
36.77%
1,964.50
5
425
52,75%
805.97
6
450
1 38,08%
1,18194
7
432
1 41-15%
1,050,511

PA&F;Z
F ROMPT-ACCL,1r4ArE.Pf'.4.IA.SLF.'
L:�BORATORIES, INC
WNN'1V.PARl.ABS.0O3Nl
Page 2 of 2
CONTINUATION OF DATA FOR SAMPLE NUMBER 145107
ANALYSIS
ANALYSIS METHOD DATE T114E BY RESULT UNITS
CHLORDANE
TCLP
08/23/22
1619
JC
HEPTACHLOR (AND ITS EPDXIDE)
TCLP
08/23/22
1619
JC
TCLP HERBICIDES
TCLP
08/29/22
1731
VC
2,4-D
TCLP
08/29/22
1731
VC
2,4,5-TP(SIL,VFX)
TCLP
08/29/22
1731
VC
TCLP ORGANICS
TCLP
08/26/22
1337
JV
BENZENE
TCLP
08/26/22
1337
JV
CARBON TETRACHLORIDE
TCLP
08/426122
1337
JV
CHLOROBENZENE
TCLP
08/26/22
1337
JV
CHLOROFORM
TCLP
08/26/22
1337
JV
o-CRES011
TCLP
08/26/22
1337
JV
p.-CRESOL
TCLP
08/26/22
1337
IV
m-CRESOL
TCLP
08/26/22
1337
JV
1, 4-DICHLOROBEINZENE
TCLP
08/26/22
1337
JV
1, 2-DICHLOROETHANE
TCLP
08/26/22
1337
JV
1,1-DICHLOROETHYLENE
TC11?
08/26/22
13 37
JV
2, 4 - D I N I TROT LU EN E
TCLP
08/26/22
1337
JV
HEXACHL0R0REN?LNF
TcLp
08/26/22
1337
JV
H EXACH LOROB UT11 D ,I NE
IT,
I CL P
08/26/22
1337
JV
HEXACHLOROETHANE
Ircilp
0 8 / 2 6/2 2
1, 3 3?
JV
METHYL ETHYL KETONE
TCLP
08/26/22
1331
JV
NITROBENZENE
TCLP
08/26/22
1337
JV
PENTACHLOROPHENOL
TCLP
08/26/22
1337
JV
PYRITE NE
11C, I I p
08/26/22
1337
iv
TETRAC,'Hl.,0RETHYLF,NE
TCLP
08/26/22
1337
JV
TRICHLOROETHYLENE
TCLP
08/26/22
1337
JV
2,4,5-TRICHLOROPHENOL
TCLP
08/26/22
1337
JV
2,4,6-TRICHLORPHEN(,)L
TCLP
08/26/22
1337
JV
VINYL CHLORIDE
TCLP
08/26/22
1337
JV
< 0.003 ppm
< 0.0008 ppm
< I ppm
< 0.1 ppm
< 0.05 ppm
< 0.05 ppm
< 10 ppm
< 0.6 ppm
< 20 ppm
< 20 ppm
< 20 ppm
< 0. 75 ppin
< 0,05 ppul
< 0.07 ppm
< O.013 ppm
<, 0.01.3 PEATI
< 0.05 ppm
0.3 ppm
< 20 F.)p-.n
* 0.2 ppm
.1.0 ppir
* 0.5 F)PITI
< 0.07 ppm
< 0.05 ppm
< 40 ppm
* 0.2 ppm
< 0.02 ppm
LABORATORY DIRECTOR l
a'l. 4z.7
2217 Graham Park Drive • Charlotte. NC28273
Phone: [phone] • Fax: (704) i88-8335

PLLF;Z
PROM PT-ACCU RATE- RELIABLE
LABORATORIES, INC
WWWRARLABS.CONI
REPORT OF ANALYSES
Attn: ZACH KEY
U.S. BIOSOLIDS, INC.
PO BOX 146
RONDA, NC 28670-
PROJECT NAME: AUG 22
DATE: 09/23/22
SAMPLE NUMBER-
145107
SAMPLE ID- RUTHERFORDTON
SAMPLE MATRIX- WW
DATE SAMPLED-
08/1-6/22
TIME SAMPLED- 1030
DATE RECEIVED-
08/16/22
SAMPLER- ZK
RECEIVED BY- DJ
TIME RECEIVED-
1410
DELIVERED BY- ZK
TYPE SAMPLE- Grab
Page 1 of 2
ANALYSIS
ANALYSIS
METHOD DATE TIME BY
RESULT UNITS
TCLP CHARACTERISTICS
TCLP
08/27/22
0952
AV
pH VALUE
TCLP
08/27/22
0952
AV
CORROSIVITY
TCLP
08/27/22
0952
AV
REACTIVITY
TCLP
08/27/22
0952
AV
FLASH POINT
TCLP
08/27/22
0952
AV
IGNITABILITY
TCLP
08/27/22
0952
AV
PAINT FILTER TEST
TCLP
08/23/22
0951
AV
TCLP METALS
TCLP
08/19/22
1434
EV
ARSENIC
TCLP
08/19/22
1434
EV
BARIUM
TCLP
08/19/22
1434
EV
CADMIUM
TCLP
08/19/22
1434
EV
CHROMIUM
TCLP
08/19/22
1434
EV
LEAD
TCLP
08/19/22
1434
EV
MERCURY
TCLP
08/19/22
1434
EV
SELENIUM
TCLP
08/19/22
1434
EV
SILVER
TCLP
08/19/22
1434
EV
TCLP PESTICIDES
TCLP
08/23/22
161.9
JC
ENDRIN
TCLP
08/23/22
1619
JC
LINDANE
TCLP
08/23/22
1619
JC
METHOXYCHLOR
TCLP
08/23/22
1619
JC
TOXAPHENE
TCLP
08/23/22
1619
JC
2217 Graham Park Drive « Charlotte, NC28273
Phone: [phone] • Fax: [phone]
6.7 S. U.
NON
NON
> 200 degrees F
NON
FL
< 0.5 ppm
< 10 ppm
< 0.1 ppm
< 0.5 ppm
< 0.5 ppm
< 0.02 ppm
< 0.1 ppm
< 0.5 ppm
< 0.002 ppm
* 0.04 ppm
< 1 ppm
* 0.05 ppm

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