WQ0028653_2022 Residual Annual Report_20230215 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0028653
Applicant/Permittee Pilgrim's Pride Corporation
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0028653
Has Current Existing permit number
Applicant/Permittee Address*
484 Zimmerman Road Sanford NC 27331
Facility Name*
Pilgrim's Pride - Sanford Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
PP_SAN_2022_AR_final.pdf 1.68MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/15/2023

2022 ANNUAL REPORT
PILGRIM'S PRIDE CORPORATION
WATER TREATMENT PLANT
SANFORD, NORTH CAROLINA
PERMIT #WQ0028653
Prepared For:
Pilgrim's Pride Corporation
484 Zimmerman Road
Sanford, N.C. 27331-3668
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill SC, 29732
February 2023

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 16, 2023
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2022 LAND APPLICATION ANNUAL REPORT
Pilgrim's Pride Corporation.
Sanford, North Carolina
Permit No. WQ0028653
BR&S Project No. 2007-66
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in
the referenced permit on behalf of Pilgrim's Pride Corporation for their facility in Sanford, North
Carolina. This report includes: 1) Distribution and Marketing Certification and Summary Forms,
2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP
Lab Sheets, 7) Pathogen & Vector Attraction Form, 8) Pathogen and Vector Attraction
Reduction Documentation, 9) Soils Lab Data 10) 2022 Application Summary Table, and 11)
2022 Application Condition Summaries.
A total of 1,107,800 gallons (53.12 dry tons) of alum residuals were distributed to sites on the
Pilgrim's Pride Facility at Sanford, NC in September of 2022.
If any further information is required regarding this land application program, please do not
hesitate to contact me at [phone].
Sincerely,
r
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures

TABLE OF CONTENTS
SECTION NO. TITLE
I Distribution and Marketing Certification and Summary
Forms
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Form
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Report
X 2022 Application Summary Table
XI 2022 Application Condition Summaries

DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM

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ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation Total Dry Tons Applied (Annual):
WQ0028653 Cation Exchange Capacity (non 503 only):
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series
7.14 Acres Permitted: 7.14 Site #: 1 Field #:
n/a
StA
16.69
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
22-196-0073
' •
1:1
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
..
hrusIMENNEENEENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
infor nw9on submi . I am aware that there are significant penalties for submitting false information,
inc g t ,p i f fines and imprisonment for knowing violations"
Z114 /z T
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation Total Dry Tons Applied (Annual):
WQ0028653 Cation Exchange Capacity (non 503 only):
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series
0.74 Acres Permitted: 0.74 Site #:
Field #:
1.11
n/a
ToB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
22-196-0073
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incl the pos ' i of fines and imprisonment for knowing violations"
r
Signature of Land Applier Date
Author Darvl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation Total Dry Tons Applied (Annual):
WQ0028653 Cation Exchange Capacity (non 503 only):
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series
16.01 Acres Permitted: 16.01 Site #: 1 Field #:
35.32
n/a
StA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
22-196-0073
®
1 M
®
1' 11
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inc l 1 thej!!OXibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Darvl D. Merritt DENR FORM MFLSF (7/20021

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd —
Cadmium
Cr —
Chromium
Cu —
Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

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RESIDUAL ANALYSIS LAB SHEETS

waypoint
ANALYTICAL
7/25/2022
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 22-196-0073
Client Project Description: Sludge Testing
Pilgrim's WTP
Sanford, NC
Project #2007-66
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 7/15/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
��Wzzfflel
Randy Thomas
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 16

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
_ Program
Lab ID
_ Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program - NELAP
LA037
12/31/2022
Louisiana
State Program - NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program - NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program - NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
460181
09/14/2022
Page 1 of 1 00001/22-196-0073
Page 2 of 16

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint,
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-196-0073
Client Project Description: Sludge Testing
Pilgrim's WTP
Sanford, NC
Project #2007-66
Lab No Client Sample ID Matrix Date Collected Date Received
99811 PPS Solids 07/14/2022 11:30 07/15/2022
Page 3 of 16

Waypoint
ANALYTICAL
Client: Branch Residuals and Soils LLC
Project: Sludge Testing
Lab Report Number: 22-196-0073
Date: 7/25/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 98867 (Biosolids)
Analyte: Molybdenum
QC Batch No: 1-628257/1-627918
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98867 (Biosolids)
Analyte: Lead
QC Batch No: 1-628257/1-627918
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 98867 (Biosolids)
Analyte: Lead
QC Batch No: 1-628257/1-627918
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 98867 (Biosolids)
Analyte: Zinc
QC Batch No: 1-628257/1-627918
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 98867 (Biosolids)
Analyte: Zinc
QC Batch No: 1-628257/1-627918
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 99109 (Sludge (March))
Analyte: Mercury
QC Batch No: 1-628259/1-628048
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 16

Waypointo
ANALYTICAL
22972
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Branch Residuals and Soils LLC Project Sludge Testing
Mr. Bob Branch
1735 Heckle Blvd Information : Pilgrim's V TP
Suite 103-291 Sanford, NC
Rock Hill , SC 29732
Report Number:22-196-0073
REPORT OFANAL YSIS
Report Date : 07/25/2022
Received : 07/15/2022
Lab No : 99811
Matrix: Solids
Sample ID: PPS
Sampled:
7/14/2022 11:30
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.8
%
0.010
1
07/20/2216:09
FMM
254OG-2011
Ammonia Nitrogen
<8330
mg/Kg - dry
8330
1
07/25/22 12:30
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<83.3
mg/Kg - dry
83.3
1
07/19/22 15:37
JCA
9056A
Nitrite (NO2-N)
<83.3
mg/Kg - dry
83.3
1
07/19/22 15:37
JCA
9056A
Nitrate+Nitrite-N
<83.3
mg/Kg - dry
83.3
1
07/19/22 15:37
9056A
pH
6.9
S.U.
1
07/22/22 13:20
SAR
9045D
Total Solids
1.15
%
0.010
1
07/20/22 16:09
FMM
2540G-2011
Total Kjeldahl Nitrogen
<17000
mg/Kg - dry
17000
1
07/19/22 12:39
CLP 4500NORGD-2011
Phosphorus
1080
mg/Kg - dry
417
1
07/22/22 12:06
TJS
6010D
Aluminum
93300
mg/Kg - dry
417
1
07/22/22 12:06
TJS
6010D
Arsenic
<41.7
mg/Kg - dry
41.7
1
07/22/22 12:06
TJS
6010D
Cadmium
<8.33
mg/Kg - dry
8.33
1
07/22/22 12:06
TJS
6010D
Calcium
<4170
mg/Kg - dry
4170
1
07/22/22 12:06
TJS
6010D
Copper
50.9
mg/Kg - dry
41.7
1
07/22/22 12:06
TJS
6010D
Lead
<25.0
mg/Kg - dry
25.0
1
07/22/22 12:06
TJS
6010D
Magnesium
825
mg/Kg - dry
417
1
07/22/22 12:06
TJS
6010D
Mercury
<13.3
mg/Kg - dry
13.3
1
07/22/22 14:09
JTR
7471A
Molybdenum
<20.8
mg/Kg - dry
20.8
1
07/22/22 12:06
TJS
6010D
Nickel
<20.8
mg/Kg - dry
20.8
1
07/22/22 12:06
TJS
6010D
Potassium
<833
mg/Kg - dry
833
1
07/22/22 12:06
TJS
6010D
Selenium
<41.7
mg/Kg - dry
41.7
1
07/22/22 12:06
TJS
6010D
Sodium
2680
mg/Kg - dry
2080
1
07/22/22 12:06
TJS
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 5 of 16

Waypointo
ANALYTICAL
22972
Branch Residuals and Soils LLC Project Sludge Testing
Mr. Bob Branch
1735 Heckle Blvd Information : Pilgrim's WTP
Suite 103-291 Sanford, NC
Rock Hill , SC 29732
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 07/25/2022
Received : 07/15/2022
Report Number: 22-196-0073 REPORTOFANALYSIS
Lab No : 99811 Matrix: Solids
Sample ID : PPS Sampled: 7/14/2022 11:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Zinc
Qualifiers/ DF Dilution Factor
Definitions
<104 mg/Kg - dry 104 1 07/22/22 12:06 TJS 6010D
MQL Method Quantitation Limit
Page 6 of 16

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.24001 Fax [phone]
www.waypointanalytical.com
Quality Control Data
Client ID:
Branch Residuals and Soils LLC
Project Description:
Sludge Testing
Report No:
22-196-0073
QC Analytical Batch:
L627806
Analysis Method:
254OG-2011
Analysis Description:
Total, Fixed, and Volatile Solids
Duplicate L 81935-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 98.6 98.6 0.0 20.0 07/20/2216:09
Total Solids % 1.38 1.37 0.7 20.0 07/20/22 16:09
Date: 07/25/2022 05:32 PM Page 1 of 8
Page 7 of 16

Waypoint
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Quality Control Data
Client ID:
Branch Residuals and Soils LLC
Project Description:
Sludge Testing
Report No:
22-196-0073
QC Analytical Batch:
L628467
Analysis Method:
4500NH3C-2011
Analysis Description:
Ammonia Nitrogen
Lab Reagent Blank
LRB
Matrix: SOL
Associated Lab Samples:
99811
Blank
MQL
Analyzed
Parameter
Units
Result
Ammonia Nitrogen
mg/Kg
< 100
100
07/25/22 12:30
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
Ammonia Nitrogen
mg/Kg
1000
952
95.0 85-115
Matrix Spike & Matrix Spike Duplicate
L 98409-MS L 98409-MSD
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Ammonia Nitrogen
mg/Kg
5570 4640
10100
10000 98.0 0.9 70-130 0.9 20.0
Date: 07/25/2022 05:32 PM Page 2 of 8
Page 8 of 16

0
2790 Whitten Road, Memphis,
Waypoint,
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL www.waypointanalytical.com
Quality Control Data
Client ID: Branch Residuals and Soils LLC
Project Description: Sludge Testing
Report No: 22-196-0073
QC Prep: L627279
QC Analytical Batch(es): L627312
QC Prep Batch Method: TKN/TKP
Digestion
Analysis Method:
4500NORGD-2011
Analysis Description:
Block Digestion and FIA
Lab Reagent Blank
LRB-1-627279
Matrix: SOL
Associated Lab Samples: 99811
Blank
MQL
Analyzed
Parameter
Units
Result
Total Kjeldahl Nitrogen
mg/Kg
< 50.0
50.0
07/19/22 12:20
Laboratory Control Sample
LCS-1-627279
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
Total Kjeldahl Nitrogen
mg/Kg
500
458
92.0 90-110
Duplicate
L 98481-DUP-L627279
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
Total Kjeldahl Nitrogen
mg/Kg
9200 9230
0.3 20.0
07/19/22 12:23
Matrix Spike
L 98481-MS-L627279
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
Total Kjeldahl Nitrogen
mg/Kg
9200 2450
11700
102 70-130
Date: 07/25/2022 05:32 PM Page 3 of 8
Page 9 of 16

Waypoint.0
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Quality Control Data
Client ID: Branch Residuals and Soils LLC
Project Description: Sludge Testing
Report No: 22-196-0073
QC Prep: L627918 QC Analytical Batch(es): L628257
QC Prep Batch Method: 3050E Analysis Method: 6010D
Analysis Description: Metals Analysis
Lab Reagent Blank LRB-1-627918 Matrix: SOL
Associated Lab Samples: 99811
Blank MQL Analyzed
Parameter Units Result
Phosphorus
mg/Kg
< 2.76
5.00
07/22/22 11:39
Aluminum
mg/Kg
< 4.62
5.00
07/22/22 11:39
Arsenic
mg/Kg
< 0.240
0.500
07/22/22 11:39
Cadmium
mg/Kg
< 0.0200
0.100
07/22/22 11:39
Calcium
mg/Kg
< 38.7
50.0
07/22/22 11:39
Copper
mg/Kg
< 0.310
0.500
07/22/22 11:39
Lead
mg/Kg
< 0.180
0.300
07/22/22 11:39
Magnesium
mg/Kg
< 2.58
5.00
07/22/22 11:39
Molybdenum
mg/Kg
< 0.135
0.250
07/22/22 11:39
Nickel
mg/Kg
< 0.120
0.250
07/22/22 11:39
Potassium
mg/Kg
< 6.18
10.0
07/22/22 11:39
Selenium
mg/Kg
< 0.320
0.500
07/22/22 11:39
Sodium
mg/Kg
< 13.0
25.0
07/22/22 11:39
Zinc
mg/Kg
< 0.810
1.25
07/22/22 11:39
Laboratory Control Sample LCS-1-627918
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Phosphorus
mg/Kg
500
497
99.0
80-120
Aluminum
mg/Kg
500
524
105
80-120
Arsenic
mg/Kg
5.00
5.04
101
80-120
Cadmium
mg/Kg
5.00
5.15
103
80-120
Calcium
mg/Kg
500
524
105
80-120
Copper
mg/Kg
50.0
50.8
102
80-120
Lead
mg/Kg
5.00
5.19
104
80-120
Magnesium
mg/Kg
500
503
101
80-120
Molybdenum
mg/Kg
50.0
50.3
101
80-120
Date: 07/25/2022 05:32 PM
Page 10 of 16
Page 4 of 8

0
Waypoint
2790 Whitten
Road,
Memphis,
TN 38133
Main 901.213.24001 Fax
901.213.2440
ANALYTICAL
www.waypointanaiytical.com
Quality
Control Data
Client ID:
Branch Residuals and Soils LLC
Project Description:
Sludge Testing
Report No:
22-196-0073
QC Prep:
L627918
QC Analytical Batch(es): L628257
QC Prep Batch Method:
3050E
Analysis Method:
6010D
Analysis Description:
Metals Analysis
Laboratory Control Sample
LCS-1-627918
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Nickel
mg/Kg
50.0
52.2
104
80-120
Potassium
mg/Kg
50.0
53.7
107
80-120
Selenium
mg/Kg
5.00
4.76
95.0
80-120
Sodium
mg/Kg
500
473
95.0
80-120
Zinc
mg/Kg
50.0
51.9
104
80-120
Matrix Spike & Matrix Spike Duplicate
Q 98867-MS-L627918
Q 98867-MSD-L627918
MS Spike
MSD MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Phosphorus
mg/Kg
1410 455
470 1860
1820
99.0
87.0
75-125
2.1
20.0
Arsenic
mg/Kg
32.0 4.55
4.70 36.7
36.9
103
104
75-125
0.5
20.0
Cadmium
mg/Kg
0.270 4.55
4.70 3.84
3.84
78.0
76.0
75-125
0.0
20.0
Copper
mg/Kg
23.8 45.5
47.0 61.0
61.3
82.0
80.0
75-125
0.4
20.0
Lead
mg/Kg
15.1 4.55
4.70 18.4
18.1
72.0*
64.0*
75-125
1.6
20.0
Molybdenum
mg/Kg
4.37 45.5
47.0 39.2
39.3
76.0
74.0*
75-125
0.2
20.0
Nickel
mg/Kg
12.2 45.5
47.0 47.3
47.9
77.0
76.0
75-125
1.2
20.0
Selenium
mg/Kg
3.09 4.55
4.70 7.34
7.12
93.0
86.0
75-125
3.0
20.0
Sodium
mg/Kg
427 455
470 822
819
87.0
83.0
75-125
0.3
20.0
Zinc
mg/Kg
61.9 45.5
47.0 92.8
91.9
68.0*
64.0*
75-125
0.9
20.0
* QC Fail
Date: 07/25/2022 05:32 PM
Page 5 of 8
Page 11 of 16

0
Waypoint.
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL
www.waypointanalytical.com
Quality
Control Data
Client ID:
Branch Residuals and Soils LLC
Project Description:
Sludge Testing
Report No:
22-196-0073
QC Prep:
L628048
QC Analytical Batch(es): L628259
QC Prep Batch Method:
7471A
Analysis Method: 7471A
Analysis Description: Solids Total Mercury Analysis - CVAA
Lab Reagent Blank
1-1113-1-628048
Matrix: SOL
Associated Lab Samples:
99811
Blank
MQL Analyzed
Parameter
Units
Result
Mercury
mg/Kg
< 0.160
0.160 07/22/22 13:48
Laboratory Control Sample
LCS-1-628048
Spike
LCS LCS %Rec % Rec
Parameter
Units
Conc.
Result Limits
Mercury
mg/Kg
0.400
0.323 81.0 80-120
Matrix Spike
L 99109-MS-1-628048
MS Spike
MSD MS Result MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike Result %Rec Limits RPD
Conc.
Mercury
mg/Kg
< 0.137 0.342
0.311 91.0 80-120
Date: 07/25/2022 05:32 PM Page 6 of 8
Page 12 of 16

Waypoint.
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Quality Control Data
Client ID: Branch Residuals and Soils LLC
Project Description: Sludge Testing
Report No: 22-196-0073
QC Analytical Batch: L628231
Analysis Method: 9045D
Analysis Description: pH in Solids
Duplicate L 98322-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
pH
S.U. 7.9 7.9 0.0 10.0 07/22/2213:20
Date: 07/25/2022 05:32 PM Page 7 of 8
Page 13 of 16

0
Waypoint
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Quality Control Data
Client ID:
Branch Residuals and
Soils LLC
Project Description:
Sludge Testing
Report No:
22-196-0073
QC Prep:
L627455
QC AnalyticalBatch(es): L627637
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method: 9056A
Analysis Description: Anions by Ion Chromatography
Lab Reagent Blank
LRB-L627455
Matrix: SOL
Associated Lab Samples: 99811
Blank
MQL
Analyzed
Parameter
Units
Result
Nitrate (NO3-N)
mg/Kg
< 1.00
1.00
07/19/22 13:41
Nitrite (NO2-N)
mg/Kg
< 1.00
1.00
07/19/22 13:41
Laboratory Control Sample & LCSD
LCS-1-627455
LCSD-L627455
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec % Rec
Limits
RPD Max
RPD
Nitrate (NO3-N)
mg/Kg
113
118
118
105 105
80-120
0.0 20.0
Nitrite (NO2-N)
mg/Kg
76.1
73.1
73.3
96.0 96.0
80-120
0.2 20.0
Date: 07/25/2022 05:32 PM Page 8 of 8
Page 14 of 16

•
(2) 2790 Whitten Road, Memphis,
Waypoint
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 22-196-0073
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
* UPS () Client 0 Courier
0 Other:
Thermometer ID:
r102
Shipping container/cooler uncompromised?
C Yes
0 No
Number of coolers/boxes received
f '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
G Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
C Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
Q Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Q Yes
❑ No
Water - Sample containers properly preserved
0 Yes
C No
00 N/A
Water - VOA vials free of headspace
0 Yes
0 No
* N/A
Trip Blanks received with VOAs
0 Yes
0 No
i• N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
IW N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes
G, No
Signature: IMakayla Weaver Date & Time: 7/15/2022 12:10:10
Page 15 of 16

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Page 16 of 16

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT
TCLP analyses are required once every permit cycle.

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORM

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. The form is marked to reflect these requirements.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Pilgrim's Pride Corporation
WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP
Monitoring Period: From l/l/2022 To
WQ Permit Number: WQ0028653
NPDES Number: PWS 03-53-130
12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A timeltem) ❑ 1
Alt B (Alk Treatment) ❑
Alt. C Prior Testin) E
A1t.D o Prior Test) ❑
Process to Further Reduce Patho en s O
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying D
Heat Treatment ❑
Ilienno hilic [i
Beta Ray ❑
Gamtna Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Densi ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Dryin ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion D
If applicable to alternative performed
(Class A or Class B) complete the ollowing
monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Number o
Excee-
Frequency
of Analysis
y
Sample
Type
a ,ca
Tech -
Minimum
Geo. Mean
aximu
Units
Fecal Colifonn
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
146
163
200
MPN/
Gram
0
Annually
Grab
SMl8
9221 C,E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. 0,2 uptake) p
Alt. 5 (14-Day Aerobic) O
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed Cj
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Tina Pedley, WTP Lagoons ORC
Preparer Name and Title (type or print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
n�KID Gnane nsncnr t4w,2nnni

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. Documentation is attached to reflect these requirements.

WQ0028653
July, 2022
Data Analyzed 7/14/2022
I1a . € . € € €
....................................................................................................g..:.......:...:.:.:.:.:
Lo'
...............................................
���`er.
.......................
22-32239
166
2.220
22-322240
163
2.212
22-322241
175
2.243
22-322242
200
2.301
22-322243
149
2.173
22-322244
146
2.164
22-322245
147
2.167
Mean Colonies 1 Gram
Total €i€1#$1
Average €€2X2
Fecal Coliformlgram
Fecal Coliform values are less than 1,000 and meets the Class A pathogen
reduction requirement

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoCt-environmentalchemists.corn
Branch Residuals/Bob Branch
Date of Report:
Jul 28, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill
SC 29732
Customer ID:
15060009
Attention:
Bob Branch
Report #:
2022-13271
Project ID: Pilgrim's
- Sanford
Lab ID
Sample ID:
Collect Date/Time Matrix
Sampled by
22-32239
Site: Sludge 1
7/14/2022 11:10 AM Solid/Sludge
Bob Branch
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.09 % 07/15/2022
Fecal Density SM 9221C E-2014 <166 MPN/g 07/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32240 Site: Sludge 2 7/14/2022 11:14 AM Solid/Sludge Bob Branch
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.11 % 07/15/2022
Fecal Density SM 9221C E-2014 <163 MPN/g 07/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32241 Site: Sludge 3 7/14/2022 11:18 AM Solid/Sludge Bob Branch
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.03 % 07/15/2022
Fecal Density SM 9221C E-2014 <175 MPN/g 07/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32242 Site: Sludge 4 7/14/2022 11:22 AM Solid/Sludge Bob Branch
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 0.90 % 07/15/2022
Fecal Density SM 9221C E-2014 <200 MPN/g 07/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32243 Site: Sludge 5 7/14/2022 11:26 AM Solid/Sludge Bob Branch
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.21 % 07/15/2022
Fecal Density SM 9221C E-2014 <149 MPN/g 07/14/2022
Report #. 2022-13271
Page 1 of 2

:enviroehemn]
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Lab ID Sample ID:
22-32244 Site: Sludge 6
Test
Total Solids (%)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
info denvironmentalchemists.com
Date of Report: Jul 28, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-13271
Project ID: Pilgrim's - Sanford
Collect Date/Time Matrix Sampled by
7/14/2022 11:29 AM Solid/Sludge Bob Branch
Method Results Date Analyzed
SM 2540 B
1.24 % 07/15/2022
Fecal Density SM 9221C E-2014 <146 MPN/g 07/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32245 Site: Sludge 7 7/14/2022 11:32 AM Solid/Sludge Bob Branch
Test
Total Solids (%)
Method
SM 2540 B
Results Date Analyzed
1.23 % 07/15/2022
Fecal Density SM 9221C E-2014 <147 MPN/g 07/14/2022
Comment: Results reported on a dry weight basis.
Reviewed by:
c./
Report #.; 2022-13271 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: DZN(-4 LE IsDAkS Date:) h4](Q3k ReportNumber: o- a -- �
Receipt of sample
ECHEM Pickup 1A Client Delivery ❑
UPS ❑ FeclEx ❑ Other ❑
❑ YES ❑ NO
N/A
1. Were custody seals present on the cooler?
O YES J ❑ NO
N/A 12.
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt "C Corrected temperature upon receipt _ eC
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
0 YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
�] YES
❑ NO
5. Were sample ID's listed an the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
JIQ YES
PQ YES
10 NO
Cl NO
10. Did samples arrive in good condition for each test?
_..... .................---- _. __. _
11. Was adequate sample volume available?'
M YES
❑ NO
12. Were samples received within proper holding time for requested tests? i
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* "TOC:/Volatiles are pl-i checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new samp a or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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SOIL ANALYSIS REPORT

SOIL ANALYSIS REPORT
Soil samples are not required to be included in this annual report, according to the current permit.
Pilgrim's Pride will have these samples available for review if desired by the NCDEQ Regional
office.

2022 APPLICATION SUMMARY TABLE

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2022 APPLICATION CONDITION SUMMARIES

Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2022
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 7.14
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids : 1.15
Residual Report No.: 22-196-0073
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/21 /22
1
75,400.0
Dry
warn, Partly Cloud
0.00
9/21 /22
1
104,400.0
Dry
warn, Sunny
0.00
9/22/22
1
11,600.0
Dry
warn, Partly Cloudy
0.00
9/23/22
1
17,400.0
Dry
warn, Sunny
0.00
9/24/22
1
139,200.0
Dry
warm, Cloudy
0.00
Total Gallons
348,000.0

Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2022
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 0.74
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids : 1.15
Residual Report No.: 22-196-0073
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/20/22
2
11,600.0
Dry
Wann, Partly Cloudy0.00
9/22/22
2
11,600.0
Dry
Wann, Partly Cloudy
0.00
Total -Gallons
23,200.0

Pilgrim's Pride WTP
Samford, North Carolina
Denali Water Solutions
W Q0028653
Annual 2022
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 16.01
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids : 1.15
Residual Report No.: 22-196-0073
Crop: Fescue
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
............................................................................................................................
...........................................................................................................................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/20/22
3
52,200.0
Dry
warm, Partly Cloudy
0.00
9/21/22
3
150,800.0
Dry
warm, sunny
0.00
9/22/22
3
214,600.0
Dry
warm, Partly Cloud
0.00
9/23/22
3
87,000.0
Dry
wann, Sunny
0.00
9/24/22
3
92,800.0
Dry
warm, Cloudy
0.00
9/25/22
3
139,200.0
Dry
warm, Cloudy
0.00
.>::.:::.:::::
: 736 60.0.0