WQ0036706_2022 Residual Annual Report_20230213 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0036706
Applicant/Permittee Town of Ahoskie
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name" Town of Ahoskie
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2528839301
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0036706
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 767 Ahoskie, NC 27910
Facility Name*
Town of Ahoskie Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Ahoskie Annual Report.pdf 4.25MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
01f1 i �4e*A~
Submission Date 2/13/2023

TOWN OF AHOSKIE
2022 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0036706
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
February 9, 2023
SOIL PLUS

SOIL PLUS
February 9, 2023
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2022 LAND APPLICATION ANNUAL REPORT
Town of Ahoskie "Class B" Program
NC Permit No.: WQ0036706
Soil Plus Project No. 201201.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Ahoskie on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The Town of Ahoskie conducted application events on permitted fields in Hertford
County during 2022. A total of 99.53 Dry Tons or 663,000 Gallons of permitted residual
biosolids were land applied to the Town of Ahoskie's permitted fields.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Town of Ahoskie (252-332-3840) for further assistance.
Respectfully,
-pe') NAk alzn
Drew Matthews, Soil Plus
cc: Jonathan Hoggard, Town of Ahoskie
Jason Smith, Granville Farms
PO Box 1396
Oxford, NC 27565
[phone]
dmatthewsgsoilplus. ne t
www.soilplusuc.com

Town of Ahoskie
2022 Annual Land
Application of
Residual Biosolids
Report
WQ0036706
Ahoskie, NC
ANNUAL
CERTIFICATION FORM
Source Summary-
Field Loading Summary
RESIDUAL SAMPLING
SUMMARY FORM
Annual Analytical Data
FIELD SUMMARY FORMS
Town of Ahoskie Farm
PATHOGEN & VECTOR
REDUCTION FORM
Fecal Coliform Data
30-Day Bench Scale Test
SOIL SAMPLES
Town of Ahoskie Farm

Town of Ahoskie
2022 Class B Annual Report
WQ Permit# WQ0036706
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0036706 Town of Ahoskie Granville Farms, Inc. Hertford [phone]
Year: 2022
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the FV� ❑E
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 4
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 99.53
Total number of acres utilizes for land application during the year: 28.75
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑d ❑o
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities)
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities)
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Jennifer Bracy, Town Clerk
Permittee Name and Title (type or rint):
a� 3
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
�. q a
gibAmanlv-�-
nature of ittee U Date
ck. 1 /25/23
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
WWTP VolumeApplied Total
Ahoskie WWTP 663,000 99.53
Total 663,000 99.53

Site# TA
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 10.24 240,500
36.10
84.11
Fescue Hay
194
43.4%
2 4.5 104,000
15.61
82. - -
Fescue Hay
194
42.7%
3 4.69 84,500
12.69
64.52
Fescue Hay
184
35.1%
4 9.32 234,000
35.13
89.91
Fescue Hay
154
58.4%
Total 663,000 99.53

Town of Ahoskie
2022 Class B Annual Report
WQ Permit# WQ0036706
Residual Sampling Summary Form
Field Loading Calculations
2022 Analytical
2022 TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0036706 Facility Name Town of Ahoskie Source Permit No. NCO088561 Source Name Ahoskie WWTP
Laboratory 1 Meritech, Inc.
.'Laboratory 2
Sample or CompositeDate 8/18/2022
Parameter (mg/Kg) Class A Class B
Aluminum
N/A
N/A
3.47
Ammonia Nitrogen
N/A
N/A
589
Arsenic
41
75
1.72
Cadmium
39
85
2.32
Calcium
N/A
N/A
222,250
Copper
1,500
4,300
20.4
Lead
300
840
3.64
Magnesium
N/A
N/A
5,056
Mercury
17
57
0.208
Molybdenum
N/A
75
10.8
Nickel
420
420
1.61
Nitrate -Nitrite Nitrogen
N/A
N/A
6,140
Percent Solids
N/A
N/A
3.60
pH (no units)
N/A
N/A
4.50
Phosphorus
N/A
N/A
511
Potassium
N/A
N/A
4,972
PAN (Inj./Inc.)
N/A
N/A
12 111
PAN (Surface)
N/A
N/A
11,928
Selenium
100
100
3.17
Sodium
N/A
N/A
7,611
SAR
N/A
N/A
2.27
TKN
N/A
N/A
18,900
Zinc
2,800
7,500
1633
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the passibility of fines and imprisonment for knowing violations."
of Preparer *
-7--q-23
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

&,,AGMAN FIELD LOADING ESTIMATES
Facility Ahoskie WWTP
Sampling Date 8/18/2022
Solids 3.6
Mineralization Rate 0.30
Gallons per DT 6,661.34
pH 4.5
Sodium Absorpotion 2.27 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 18,900 lbs./1,000 gal 5.67
Ammonia Nitrogen (mg/Kg) 589.00 lbs./1,000 gal 0.18
Nitrate -Nitrite (mg/Kg) 6,140.00 lbs./1,000 gal 1.84
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 11,928 lbs./1,000 gal 3.58
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 12,222 lbs./1,000 gal 3.67
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.49
Phosphorus lbs./1,000 gal 0.15
Calcium lbs./1,000 gal 6.68
Calcium lbs./1,000 gal 1.52
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
1.72
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.32
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
20.40
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
3.64
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.21
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
1.61
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
3.17
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1633.00
Zinc lbs./1,000 gal
0.49
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
18,900
11,928 23.86
6,972
18,900
12,222 24.44
6,678
6,972
1,046 2.09
5,926
6,678
1,002 2.00
5,676
5,926
444 0.89
5,482
5,676
426 0.85
5,250
5,482
206 0.41
5,276
5,250
197 0.39
5,053
5,276
99 0.20
5,177
5,053
95 0.19
4,959
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 13,723 27.45
Total 13,941 27.88

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
9/27/2022
Ahoskie
8/18/2022
Meritech Work Order # 081822122 Sample: AH 081822 Grab
8/18/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.60 %
0-100 %
SM 2540B
Ammonia, Nitrogen
589 mg/kg
10 mg/kg
EPA 350.1
TKN
18,900 mg/kg
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
6,140 mg/kg
10.0 mg/kg
EPA 353.2
Aluminum, total
Attached -
-
-
Arsenic, total
Attached -
-
-
Cadmium, total
Attached -
-
-
Calcium, total
Attached -
-
-
Copper, total
Attached -
-
-
Lead, total
Attached -
-
-
Magnesium, total
Attached -
-
-
Mercury, total
0.208 mg/kg
0.064 mg/kg
EPA 245.1
Molybdenum, total
Attached -
-
-
NickeI, total
Attached -
-
-
Phosphorus, total
Attached -
-
-
Potassium, total
Attached -
-
-
Selenium, total
Attached -
-
-
Sodium, total
Attached -
-
-
Zinc, total
Attached -
-
-
pH
4.5 S.U. 8/23/22
1.0 - 14.0 S.U.
SM 4500-HB
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

u, Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
E14li(JR014&1ENTALTE0I4M1tQLOGIE-S, INC. Cuyahoga Falls, Ohio 44223 (consolidated)
Anafyrficaf Laboratorws TEL: [phone] FAX.- [phone] WO#: 22090248
Website: http://www.settekcom Date Reported: 9127/2022
CLIENT: Meritech Environmental Laboratories Collection Date: 8/18/2022 9:30.00 AM
Project:
Lab ID: 22090248-009 Matrix: NON -POTABLE WATER
Client Sample ID: 081822-122
Analyses Result PQL Qua] Units DF Date Analyzed
METALS (EPA 200.7)
E200.7
E200.7
Analyst: MSK
Calcium(Ca)
22250
174
mg/kg-dry
10
9/8/2022 10:47:00 AM
Magnesium(Mg)
5056
55.6
mg/kg-dry
20
9/12/2022 11 AT00 AM
Potassium(K)
4972
347
mg/kg-dry
10
9/8/2022 10:47:00 AM
Sodium(Na)
7611
347
mg/kg-dry
10
9/8/2022 10:47:00 AM
Zinc(Zn)
1633
6,94
mg/kg-dry
10
9/8/2022 10:47:00 AM
METALS ANALYSIS BY ICPlMS (EPA200.8)
E200.8
E200.8
Analyst: RJE
Aluminum(AI)
ND
3.47
mg/kg-dry
5
9/9/2022 9:34:04 PM
Arsenic(As)
1.72
0.694
mg/kg-dry
5
9/9/2022 9:34:04 PM
Cadmium(Cd)
2.32
0.694
mg/kg-dry
5
9/8/2022 10:03:32 PM
Copper(Cu)
20A
0.694
mglkg-dry
5
9/8/2022 10.03:32 PM
Lead(Pb)
3.64
0.694
mg/kg-dry
5
9/8/2022 10:03:32 PM
Molybdenum(Mo)
10.8
0.694
mg/kg-dry
5
9/812022 10:03:32 PM
Nickel(Ni)
1.61
0.139
mg/kg-dry
1
9/12/2022 2:55:57 PM
Selenium(Se)
3.17
0.694
mglkg-dry
5
9/8/2022 10:03:32 PM
PHOSPHORUS (SM4500-PE) 2011
SM 4500-P-E
Analyst: MS
Phosphorus(P)
511
11.1 Z
mg/kg-dry
20
9/12/2022 7:31:00 PM
NOTES:
Z: Method Deviation - Sample was preserved with the wrong
preservative, HNO3 instead of H2SO4.
Qualifiers: B Analyte detected in the associated Method Blank
II Holding times for preparation or analysis czcccdcd
ND Not Dctcctcd
R RPD outside accepted recovery limits
W Sample container tcmpequurc is out of limit m specified at tegeode
E Value above quaadtation range
M Manua: Integration used to determine arcs response
PL Permit Limit
RL Reporting Detection Limit
Original
Page 14 of 64

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
s
Contact: Drew Matthews
Client: Soil Plus
Page 1
Report Date: 9/15/2022
P.O. Box 1396 Project: Ahoskie
Oxford, NC 27565 Date Sample Rcvd: 8/18/2022
Meritech Work Order 4 081822124 Sample: AH 081822 Grab 8/18/2022
1311-
TCLP Metals
Parameter
Results
Analysis Date
Det. Limit
Reg, Limit
Method
Arsenic
<0.100 mg/L
8/25/2022
0.100
5.0
EPA 200.7
Barium
0.138 mg/L
8/25/2022
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/25/2022
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/25/2022
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/25/2022
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/23/2022
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/25/2022
0.100
1.0
EPA 200.7
Silver
<0.050 mg/L
8/25/2022
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
Reporting Limit
Method
Volatiles 8260
Attached
8/24/2022
-
8260
Semi Vol. 8270
Attached
9/1/2022
-
8270
Other Tests
Parameter
Results
Analysis Date
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
8/19/2022
0.500 mg/kg
EPA 335.4
Sulfide
<10.0 mg/kg
8/19/2022
10.0 mg/kg
SM4500S2D
Flash Point
>140 OF
8/19/2022
-
EPA 1020C
Corrositivity (pH)
5.5 S.U.
8/23/2022
1.0 -14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
aP
Page 2
Contact: Drew Matthews Report Date: 9/15/2022
Client: Soil Plus
P.O. Box 1396 Project: Ahoskie
Oxford, NC 27565 Date Sample Rcvd: 8/18/2022
Meritech Work Order # 081822124 Sample: AH 081822 Grab 8/18/2022
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - -
Chlordane
Attached - - -
Toxaphene
Attached - - -
Methoxychlor
Attached - - -
Heptachlor
Attached - - -
Lindane
Attached - - -
Herbicides - SW-846 8151A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
2,4-D Attached - - -
2,4,5-TP (Silvex) Attached - - -
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
,�. Environmental Laboratories
�.s Laboratory Certificate #>~165
CIient: Soil Plus
Project: Ahoskie
Client Sample ID: AH08I 822
Sample Collection: 08/18/22
Meritech Sample ID. 081822124
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 08/24/22
Extraction:
08/22/22
Analyst: V WV
Report Date:
08/25/22
Parameter
Result
Units
Det. Limit
Rea. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
<0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 09/01/22
Extraction:
08/22/22
Analyst: PM
Report Date:
09/02/22
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. .Sdmcff)ow�1
Laboratory Representative
642 Tameo Road * Reidsville, NC 27320
[phone] * [e-mail]

IT Stanmit Environmental Technologies, Inc. Analytical Report
r:;3r.ovq SUMM3310 Win SL
..EKV40NMEN-rAL EC"U0W--1,S, mC Cuyahoga Falls. Ohio 44223 (consolidated)
Anafyflcv'r Laboratories TEL: [phone] FAX- [phone] WO#: 22081656
Website: httD:llwww.settekcom Date Reported: 9/14/2022
Lab ID: 22081656-003 Collection Date: 8/18/2022 9:18:00 AM
Client Sample ID . 081822-124 Matrix: NON -POTABLE WATER
Analysis
Result
MDL
PQL
Qual
Units
Dilution Batch
Date Analyzed
TCLP PESTICIDES ANALYSIS (SW131118081)
EPA 8081 B
EPA 3610 Analyst: PGP
Chlordane, total
ND
0.380
25.0
U
µg/L
10
59219
9/3l2022 3:59:00 AM
Toxaphene
ND
1.60
50.0
U
µg/L.
10
59219
9/3/2022 3:59:00 AM
Endrin
ND
0.0634
5.00
U
µg/L
10
59219
9/3/2022 3:59:00 AM
gamma-BHC
ND
0.0429
5.00
U
µg/1.
10
59219
9/3/2022 3:59:00 AM
Heptachlor
ND
0.0336
5.00
U
µg/
10
59219
9/3/2022 3:59:00 AM
Heptachlor epoxide
ND
0.0676
5.00
U
µg/L
10
59219
9/3/2022 3:59:00 AM
Methoxychlor
ND
0.0509
5.00
U
µgq-
10
59219
9/3/2022 3:59,00 AM
TCLP HERBICIDES BY EPA 8321A EPA 8321 A EPA 1311 Analyst: PGP
2,4-D ND 0,500 0.500 U mg/L 50 59222 9/2/2022 2:29:00 AM
2,4,5-TP ND 0,500 0.500 U mg/L 50 59222 9/2/2022 2:29:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E
H Holding times for preparation or analysis exceeded M
MC Value is below Minimum Compound Limit. N
ND Not Detected OG1
P Second column confirmation exceeds PL
Page 6 of 15
Value above quantitation range
Manual Integration used to determine area response
Tentatively identified compounds
Permit Limit

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Town of Ahoskie
2022 Class B Annual Report
WQ Permit# WQ0036706
Land Application Field Summary Forms

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706 Site# TA County Hertford Crop 1 Fescue Hay
Facility Name Town of Ahoskie Field Name 1 SoilSeries Rams Crop 1 Pan 194
LandOwner Town ofAhoskie Acres Permited 10.24 SoilAbbrevation: Ra Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization
TKN Ammonia Nitrite
PAN
PAN Crop
03/29/2022 Gallons
19,500 3.60
10.24
0.29 2.93
Ahoskie WWTP
Dry < 0.5"
Surface
0.29
0.50
0.3
18,900
589.00 6,140.00
6.82
Crop 1
03/30/2022 Gallons
71,500 3.60
10.24
1.05 10.73
Ahoskie WWTP
Dry < 0.5"
Surface
1.07
0.50
0.3
18,900
589.00 6,140.00
25.01
Crop 1
03/31/2022 Gallons
65,000 3.60
10.24
0.95 9.76
Ahoskie WWTP
Dry < 0.5"
Surface
0.97
0.50
0.3
18,900
589.00 6,140.00
22.73
Crop 1
04/04/2022 Gallons
32,500 3.60
10.24
0.48 4.88
Ahoskie WWTP
Dry < 0.5"
Surface
0.49
0.50
0.3
18,900
589.00 6,140.00
11.37
Crop 1
12/07/2022 Gallons
52,000 3.60
10.24
0.76 7.81
Ahoskie WWTP
Moist < 0.5"
Surface
0.78
0.50
0.3
18,900
589.00 6,140.00
18.19
Crop 1
Total Volume Applied
240,500
Total Dry Tons 36.10
Sum Total P
3.60
Total
84.11
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.012 0.016
0.144
0.026 0.001
0.076
0.011
0.022
11.515
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
6.154 4.095
34.222
11.102
21.777 0.820
10.413
10.838
10.172
82.838
N/A
Cumulative Total
6.166 4.111
34.366
21.803 0.821
10.489
10.849
10.195
94.354
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
01-25-2023 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706 Site# TA County Hertford Crop 1 Fescue Hay
Facility Name Town of Ahoskie Field Name 2 SoilSeries Lynchburg Crop 1 Pan 194
LandOwner Town of Ahoskie Acres Permited 4.50 Soil Abbrevation: Ly Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement Applied
%Solids
Used DT/Ac.
Tons
Source
Condition Precip
Method
P
Volatilization Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
03/15/2022
Gallons 26,000
3.60
4.50 0.87
3.90
Ahoskie WWTP
Dry < 0.5"
Surface
0.89
0.50 0.3
18,900
589.00 6,140.00
20.69
Crop 1
03/16/2022
Gallons 39,000
3.60
4.50 1.30
5.85
Ahoskie WWTP
Dry < 0.5"
Surface
1.33
0.50 0.3
18,900
589.00 6,140.00
31.04
Crop 1
12/09/2022
Gallons 39,000
3.60
4.50 1.30
5.85
Ahoskie WWTP
Moist < 0.5"
Surface
1.33
0.50 0.3
18,900
589.00 6,140.00
31.04
Crop 1
Total Volume Applied
104,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.012
0.016
Prior Year
6.179
4.106
Cumulative Total
6.191
4.122
Permitted CPLR
36
34
Total Dry Tons 15.61
Copper Chromium
Lead
0.142
0.025
36.799 11.264
16.026
36.941
16.051
1338
267
Mercury Molybdenum
0.001 0.075
0.822 10.475
0.823 10.550
15
Sum Total P 3.55
Nickel
Selenium
Zinc
0.011
0.022
11.331
10.950
10.198
75.728
10.962
10.220
87.059
374
89
2498
Total 82.77 Total
Crop 1 Crop 2
PAN PAN
Lime (T/Ac.)
(lbs./Ac.) (lbs./Ac.)
Date
N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
n9 7r 7M2 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706
Site# TA County Hertford Crop 1 Fescue Hay
Facility Name Town of Ahoskie
Field Name 3 SoilSeries Goldsboro Crop 1 Pan 184
LandOwner Town of Ahoskie
Acres Permited 4.69 Soil Abbrevation: GoA Crop 2
Operator
Crop 2 Pan
Volume
Acres Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite
PAN
PAN Crop
03/17/2022 Gallons
32,500 3.60
4.69 1.04 4.88
Ahoskie WWTP
Dry < 0.5"
Surface
1.06
0.50
0.3 18,900
589.00 6,140.00
24.82
Crop 1
03/21/2022 Gallons
52,000 3.60
4.69 1.66 7.81
Ahoskie WWTP
Dry < 0.5"
Surface
1.70
0.50
0.3 18,900
589.00 6,140.00
39.71
Crop 1
Total Volume Applied
84,500
Total Dry Tons 12.69
Sum Total P
2.76
Total
64.52
Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.009 0.013
0.110
0.020
0.001
0.058
0.009
0.017
8.834
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
6.192 4.112
39.125 11.327
18.156
0.824
10.499
10.997
10.211
83.892
Cumulative Total
6.201 4.124
39.235
18.175
0.825
10.557
11.006
10.229
92.726
N/A
Permitted CPLR
36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
y 01-25-2023 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706
Site# TA County Hertford Crop 1 Fescue Hay
Facility Name Town of Ahoskie
Field Name 4 SoilSeries Caroline Crop 1 Pan 154
LandOwner Town of Ahoskie
Acres Permited 9.32 Soil Abbrevation: CaA Crop 2
Operator
Crop 2 Pan
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied %Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization
TKN Ammonia Nitrite
PAN
PAN Crop
03/22/2022 Gallons
52,000 3.60
9.32
0.84 7.81
Ahoskie WWTP
Dry < 0.5"
Surface
0.86
0.50
0.3
18,900
589.00 6,140.00
19.98
Crop 1
03/23/2022 Gallons
65,000 3.60
9.32
1.05 9.76
Ahoskie WWTP
Dry < 0.5"
Surface
1.07
0.50
0.3
18,900
589.00 6,140.00
24.98
Crop 1
03/28/2022 Gallons
58,500 3.60
9.32
0.94 8.78
Ahoskie WWTP
Dry < 0.5"
Surface
0.96
0.50
0.3
18,900
589.00 6,140.00
22.48
Crop 1
12/08/2022 Gallons
58,500 3.60
9.32
0.94 8.78
Ahoskie WWTP
Moist < 0.5"
Surface
0.96
0.50
0.3
18,900
589.00 6,140.00
22.48
Crop 1
Total Volume Applied
234,000
Total Dry Tons 35.13
Sum Total P
3.85
Total
89.91
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.013 0.017
0.154
0.027 0.002
0.081
0.012
0.024
12.310
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
6.185 4.108
37.429
11.285
22.017 0.822
10.475
10.964
10.203
77.669
Cumulative Total
6.198 4.125
37.582
22.045 0.824
10.556
10.976
10.227
89.979
N/A
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
S"�Z,4 4�;M�c ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

Town of Ahoskie
2022 Class B Annual Report
WQ Permit# WQ0036706
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Geometric Mean
30-Day Bench Scale Test

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Ahoskie WQ Permit Number: WQ0036706
WWTP Name: Ahoskie WWTP NPDES Number: NCO088561
Monitoring Period: 01/01/2022 to 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform CFU Minimum Geo. Mean
(Dry Weight)
253 262
Analytical Technique SM 9222 D
Maximum # of Exceedences Frequency
283 0 Annually
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
Sample Type
Grab Samplcs
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Jonathan Iloggard, ORC
Preparer Name and Title (type or print)
5�x� 2- ?-23
Signature of Preparer* Date
Jason Smith, VP
Land Applier Name and Title (if applicable)(type or print)
-,� S�� 1 /25/23
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Amp
Page 1
Contact: Drew Matthews Report Date: 8/30/2022
Client: Soil Plus
P.O. Box 1396 Project: Ahoskie
Oxford, NC 27565 Date Sample Rcvd: 8/18/2022
Meritech Work Order # 081822115 Sample: AH 081822 (001) Grab
Parameters
Results Analysis Date
8/18/22
Reporting Limit Method
% Total Solids
3.56 %
8/23/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<255 CFU/g drywt
8/18/22
255 CFU/g dry wt
SM 9222D
Meritech Work Order # 081822116 Sample: AH 081822 (002) Grab
Parameters
Results Analysis Date
8/18/22
Reporting Limit Method
% Total Solids
3.83 %
8/23/22
0-100 %
SM 2540E
Fecal Conform (Sludge)
<283 CFU/g dry wt
8/18/22
283 CFU/g dry wt
SM 9222D
Meritech Work Order # 081822117 Sample: AH 081822 (003) Grab
Parameters
Results Analysis Date
8/18/22
Reporting Limit Method
% Total Solids
3.51 %
8/23/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<259 CFU/g dry wt
8/18/22
259 CFU/g dry wt
SM 9222D
Meritech Work Order # 081822118 Sample: AH 081822 (004) Grab 8/18/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.50 % 8/23/22 0-100 % SM 2540B
Fecal Coliform (Sludge) <260 CFU/gdry wt 8/18/22 260 CFU/gdry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

F�
Contact; Drew Matthews
Client: Soil Plus
PO B 1
Meritech, .Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 8/30/2022
ox 396 Project: Ahoskie
Oxford, NC 27565 Date Sample Rcvd: 8/18/2022
Meritech Work Order # 081822119 Sample: AH 081822 (005) Grab 8/18/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.59 % 8/23/22 0-100 % SM 2540B
Fecal Coliform (Sludge) <253 CFU/g dry wt 8/18/22 253 CFU/g dry wt SM 9222D
Meritech Work Order # 081822120 Sample: AH 081822 (006) Grab 8/18/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.54 % 8/23/22 0-100 % SM 2540B
Fecal Coliform (Sludge) <257 CFU/g drywt 8/18/22 257 CFU/g dry wt SM 9222D
Meritech Work Order # 081822121 Sample: AH 081822 (007) Grab 8/18/22
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 3.41 % 8/23/22 0-100 % SM 2540B
Fecal Coliform (Sludge) <267 CFU/g dry wt 8/18/22 267 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date: 9/23/2022
Project: Ahoskie
Date Sample Rcvd: 8/18/2022
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 0122123 22 Sample: AH 081822 Grab 8 18
p / /
Total Solids Volatile Solids % Volatile Solids
Week 1
Week 2
Week 3
Week 4
Week 5
1.29
1.24
1.13
0.970
Mass Balance Equation = 5.
I hereby certify that I have
1 :1
0.750
0.570
0.550
0.607
0.616
,1 : •
0.571
Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
and approve these data.
.Laboratory Representative
Tamca Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Town of Ahoskie
2022 Class B Annual Report
WQ Permit# WQ0036706
Soil Samples

Page 1 of 1
Report No: 22-327-0509
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypo'10 t
ANALYTICAL
Client: Granville Farms Inc
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: TA
Date Received: 11/23/2022
Date of Report: 11 /28/2022
Lab No Field ID
Sample ID
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
CEC BS %
Ca %
Mg %
ESP
Na
15180
1
MIN 0.6
6.3
1.2
440
21
46
56
46
0
883
883
465
11.3 89
67
20
1.4
0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K2
97
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
15181
2
MIN 0.5
6.2
1.2
479
25
46
44
40
0
1075
1075
545
11.9 89
67
20
1.5
0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K2
89
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
15182
3
MIN 0.5
6.3
1.1
447
21
42
50
42
0
913
913
475
10.2 89
67
20
1.4
0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K2
97
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
15183
4
MIN 0.3
6.0
1.3
467
19
42
50
47
0
870
870
490
9.0 85
64
19
1.2
0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
102
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.