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HomeMy WebLinkAboutWQ0036723_2022 Residual Annual Report_20230208 (2)Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR) * WQ0036723 Applicant/Permittee Town of Mooresville Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Mooresville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Matthew Herman Email Address* mherman@mooresvillenc.gov Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 7046632460 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0036723 Has Current Existing permit number Applicant/Permittee Address* 369 Johnson Dairy Rd, Mooresville, NC 28115 Facility Name* Town of Mooresville Class A Residuals Program Please provide comments/notes on your current submittal below. Subject: 2022 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone:704-663-2840 2) Responsible official and facility contact— Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone:704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # W00036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2022 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total = 991.6 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs as well as copies of utilization agreements for new users this year. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Class A Annual Report 2022 Complete Scan.pdf 3.81 MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/8/2023 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 Town. of Mooresville FAX (704) 662-8473 NORTH CAROLINA POST OFFICE BOX 878 MOORESVILLE, NC 28115 2022 Annual Class A Report, WQ0036723 Rocky River Wastewater Treatment Facility Mooresville, N.C. 28115 Town of Mooresville NORTH CAROLINA NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 2/8/23 Subject: 2022 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2022 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total � 991.6 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs as well as copies of utilization agreements for new users this year. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Matthew Herman Biosolids Operator Reviewed by: Jamie Levis, WWTP Plant Manager Signature: yb4a,- Date Signatur . 27 d-,�-3 Date Town of Mooresville NORTH CAROLINA U.S. EPA Region 7 ATTN: BIOSOLIDS CENTER W WPD/WENF 11201 Renner Boulevard Lenexa, Kansas 66219 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 218123 Subject: 2022 Annual Sludge Report, WQ0036723 Distributions of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. BOX 878 Mooresville, NC 28115 Phone: 704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2022 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total = 991.6 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs as well as copies of utilization agreements for new users this year. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Matthew Herman Biosolids Operator Signature: Date Reviewed by: Jamic Levis WWTP Plant Manager Signat e• D c Town of Mooresville 2022 Class A Hauling Summary Sheet DATE TONS- TRANSPORTER DESTINATION COMMENTS , 1/25/2022 6.1 Town of Mooresville Boyd Randy Bo 1 Load Mt Ulla 2/1/2022 41.6 Town of Mooresville Randy Boyd 6 Loads Mt.11lla 2/2/2022 35.8 Town of Mooresville Doug Carrigan5 Loads Mooresville 2/7/2022 6.8 Town of Mooresville Doug Carrigan1 Load Mooresville 2/15/2022 35.3 Town of Mooresville Doug Carrigan Loads Mooresville 2/17/2022 20.4 Town of Mooresville Doug Carrigan . 3 Loads Mooresville 3/2/2022 14.7 Town of Mooresville Atwell Farms2 loads Mooresville 3/2/2022 21.6 Town of Mooresville Randy Boyd 3 Loads Mt Lllla 3/7/2022 19.6 Mike Bowers Mike Bowers 3 Loads Troutman 3/15/2022 14.1 Town of Mooresville Atwell Farms2 loads Mooresville 3/22/2022 19.4 Town of Mooresville Randy Boyd 3 loads Mt Ulla 3/22/2022 13.3 Town of Mooresville Doug Carrigan2 loads Mooresville 3/28/2022 29.4 Town of Mooresville AFH Sod Farm5 Loads Mooresville 4/11/2022 18.1 Town of Mooresville AFH Sod Farm3 Loads Mooresville 4/12/2022 12.3 Town of Mooresville Doug Carrigan 2 loads Mooresville 4/12/2022 19.4 Town of Mooresville Boyd Randy Bo 3 Loads Mt.Uila 4/13/2022 12.9 Town of Mooresville AFH Sod Farm 2 loads Mooresville 4/19/2022 19.9 Mike Bowers Mike Bowers 3 Loads Troutman 4/25/2022 13.5 Town of Mooresville Doug Carrigan2 loads Mooresville 4/26/2022 6.5 Town of Mooresville Doug Carrigan 1 Load Mooresville 4/26/2022 13.1 Town of Mooresville Atwell Farms 2 loadsMooresville 4/28/2022 6.5 Town of Mooresville Atwell Farms Load Mooresville 5/3/2022 12.3 Town of Mooresville Doug Carrigan 2 LoadsMooresville 5/3/2022 6.5 Town of Mooresville Boyd Randy Bo 1 Load Mt.Ulla 5/16/2022 12.4 Town of Mooresville Atwell Farms 2 loadsMooresville 5/17/2022 19.3 Town of Mooresville Atwell Farms3 Loads Mooresville 5/18/2022 20.0 Town of Mooresville Doug Carrigan 3 LoadsMooresville 6/2/2022 13.2 Town of Mooresville Atwell Farms 2 loads Mooresville 6/3/2022 15.8 Scott Atwell Atwell Farms 1 load Mooresville 6/3/2022 6.7 Town of Mooresville Randy Boyd1 load Mt.Ulla 6/6/2022 16.2 Scott Atwell Atwell Farms 1 loadMooresville 6/9/2022 12.8 Town of Mooresville Randy Boyd 2 loadsMt.Ulla 6/21/2022 37.0 Town of Mooresville Doug Carrigan 4 LoadsMooresville 6/22/2022 7.8 Town of Mooresville Doug Carrigan 1 LoadMooresville 6/28/2022 14.5 Town of Mooresville Doug Carrigan 2 loadsMooresville 7/5/2022 20.2 Town of Mooresville Doug Carrigan3 Loads Mooresville 7/6/2022 12,2 Town of Mooresville Doug Carrigan2 loads Mooresville 7/13/2022 12.7 Town of Mooresville Doug Carrigan 2 loadsMooresville 7/25/2022 18.5 Town of Mooresville Doug Carrigan 3 Loads Mooresville 7/27/2022 19.0 1 Town of Mooresville Doug CarriganMooresville 3 Loads 8/4/2022 21.2 Mike Bowers Mike Bowers 4 LoadsTroutman $/5/2022 11.7 Mike Bowers Mike Bowers 2 Loads Troutman 8/10/2022 15.8 Scott Atwell Atwell Farms 1 Load Mooresville 8/23/2022 26.7 Town of Mooresville Doug Carrigan 4 Loads Mooresville 8/25/2022 6.3 Town of Mooresville AFM Sod Farm 1 Load Mooresville 9/12/2022 6.7 Town of Mooresville Doug Carrigan 1 Load Mooresville 9/12/2022 6.5 Town of Mooresville Atwell Farms 1 Load Mooresville 9/12/2022 16.1 Scott Atwell Atwell Farms Load Mooresville 9/12/2022 18.4 Scott Atwell Atwell Farms 1 Load Mooresville 9/20/2022 21.4 Town of Mooresville Doug Carrigan 3 Loads Mooresville 9/24/2022 14.2 Town of Mooresville Atwell Farms 2 Loads Mooresville 10/4/2022 21.1 Town of Mooresville Atwell Farms 3 Loads Mooresville 10/12/2022 15.0 Town of Mooresville Randy Boyd 2 loads Mt.Ulla 10/24/2022 7.2 Town of Mooresville Randy Boyd 1 Load Mt.Ulla 10/24/2022 18.1 Scott Atwell Atwell Farms 1 Load Mooresville 10/25/2022 17.9 Scott Atwell Atwell Farms 1 Load Mooresville 11/2/2022 29.3 Town of Mooresville Doug Carrigan 4 Loads Mooresville 11/3/2022 6.1 town of Mooresville Randy Boyd 1 Load Mt.Ulla 11/8/2022 7.4 Town of Mooresville Randy Boyd 1 Load Mt.Ulla 11/9/2022 14.7 Town of Mooresville Boyd Randy Bo 2 loads Mt.Ulla 11/17/2022 7.5 Town of Mooresville Atwell Farms 1 Load Mooresville 11/17/2022 34.1 Scott Atwell Atwell Farms 2 loads Mooresville 11/21/2022 7.6 Town of Mooresville Atwell Farms 1 Load Mooresville 11/29/2022 22.6 Town of Mooresville Atwell Farms 3 Loads Mooresville 12/14/2022 45.8 Town of Mooresville Atwell Farms Mooresville 6 Loads Randy Boyd 12/20/2022 14.9 Town of Mooresville 2 loads Mt.Ulla Atwell Farms 12/20/2022 29.6 Town of Mooresville 4 Loads Mooresville Total tons 1141.30 Avg. % solids 0.96 Dry tons 1093.02 Conversion factor 0.907184 Metric tons 1035.4 Dry metric tons 991.6 Calculation: Dry metric tons= total tons * avg.% solids* conversion factor Waypoin.(Dt ANALYTICAL 1 /2012022 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-010-0012 Client Project Description: Class A TCLP Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/10/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 6fflA6 W&YJL..' Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shalt be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID North Carolina State Program 37735 North Carolina State Program 402 South Carolina State Program 99012 South Carolina State Program 99012 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Alabama State Program 40750 Arkansas State Program 88-0650 California State Program 2904 Florida State Program - NELAP E871157 Georgia State Program C044 Georgia State Program 04015 Illinois State Program - NELAP 200078 Kentucky State Program 80215 Kentucky State Program KY90047 Louisiana State Program - NELAP LA037 Louisiana State Program - NELAP 04015 Mississippi State Program MS North Carolina State Program 415 Pennsylvania State Program - NELAP 68-03195 South Carolina State Program 84002 South Carolina State Program 84002 Tennessee State Program 02027 Texas State Program - NELAP T104704180 Virginia State Program 00106 Virginia State Program - NELAP 460181 Expiration Date 07/31 /2022 12/31 /2022 07/31 /2022 12/31/2021 Expiration Date 02/28/2022 02/07/2022 06/30/2022 06/30/2022 02/18/2023 06/30/2022 10/10/2022 06/30/2022 12/31 /2022 12/31 /2022 06/30/2022 02/11/2023 12/31 /2022 05131 /2022 06/30/2022 06/30/2022 02/11 /2023 09/30/2022 06/30/2022 09/14/2022 Page 1 of 1 00016122-010-0012 Page 2 of 8 a Waypoint,. ANALYTICAL Report Number: 22-010-0012 Client Project Description: Class A TCLP 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytica Isom Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 91913 Class A Sludge 01/10/2022 07:53 01/10/2022 12:25 8270C WP MTN 91913 Class A Sludge 01/10/2022 07:53 01/10/2022 12:25 SW-1311 WP MTN 91914 Class Solids 01/10/2022 07:53 01/10/2022 12:25 91914 Class A Solids 01/10/2022 07:53 01/10/2022 12:25 SW-7.3.4 WP MTN 91914 Class Solids 01/10/2022 07:53 01/10/2022 12:25 SW-7.3.3 WP MTN 91914 Class A Solids 01/10/2022 07:53 01/10/2022 12:25 ASTM D93-80 WP MTN WP MTN - Memphis, TN: Waypolnt Analytical - TN, Memphis, TN Page 3 of 8 Waypoelnt(D ANALYTICAL Client: Town of Mooresville/RR WVVfP Project: Class A TCLP Lab Report Number: 22-010-0012 Date: 1 /20/2022 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Flashpoint Method ASTM D93-80 QC Batch No: L594898 The sample analysis was performed using a modified version of the reference method. Due to the sample matrix, the continual stirring required by the method had to be omitted. Separatory Funnel Extraction Method 3510C Sample 91913 (Class A) QC Batch No: L595182/L595182 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D QC Batch No: L595459/L595182 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non -target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Page 4 of 8 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-010-0012 449 Springbrook lid, Charlotte, NC 23217 Main 704.529,6964 www.waypointanalyti caLcom Class A TCLP REPORT OFANALYSIS Report Date : 01/20/2022 Received : 01/10/2022 Terri W Cole Laboratory Project Manager Lab No : 91913 Sample ID : Class A Matrix: Sludge Sampled: 1/10/2022 7:53 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP SVOC 5draction Leachate 1 01/17/22 14:00 PHE SW-1311 Analytical Method: 8270C Prep Batch(es): L595182 01/19/22 09:15 Prep Method: 3510C Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP 3&4 Methylphenol <0.100 mg/L 0.100 1 01/19/22 18:50 VBW L595459 TCLP 2,4-Dinitrotoluene <0.0500 mglL 0.0500 1 01/19/22 18:50 VBW L595459 TCLP Hexachlorobenzene <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP Hexachlorobutadiene <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP Hexachloroethane <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP Nitrobenzene <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP Pentachlorophenol <0.100 mg/L 0.100 1 01/19/22 18:50 VBW L595459 TCLP Pyridine <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP 2,4,5 Trichlorophenol <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 TCLP 2,4,6Trichlorophenol <0.0500 mg/L 0.0500 1 01/19/22 18:50 VBW L595459 Surrogate: TCLP 2,4,6-Tribromophenol 58.1 Limits: 42-102% 1 01/19/22 18:50 L595459 Surrogate: TCLP 2-Fluorobiphenyl 36.3 Limits: 24-86% 1 01/19/22 18:50 L595459 Surrogate; TCLP 2-Fluorophenol 12.8 * Limits: 13-37% 1 01/19/22 18:50 L595459 Surrogate: TCLP 4 Terphenyl-d14 63.7 Limits: 30-122% 1 01/19/22 18:50 L595459 Surrogate: TCLP Nitrobenzene-d5 41.9 Limits: 25-78% 1 01/19/22 18:50 L595459 Surrogate: TCLP Phenol-d6 9.70 Limits: 9-27% 1 01/19/22 18:50 L595459 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 5 of 8 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-010-0012 Lab No : 91914 Sample ID : Class A Test 449 Springbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanslytical.com Class A TCLP REPORT OFAIVAIYSIS Report Date; 01/20/2022 Received : 01/10/2022 fUk& Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 1/10/2022 7:53 Results Units MQL DF Date 1 Time By Analytical Analyzed Method Flashpoint >96 degrees C 1 01/17/22 08:05 MAR ASTM D93-80 Sulfide (Reactivity) <25.0 mg/Kg 25.0 1 01/13/22 13:47 FMM SW-7.3.4 Moisture 3.99 % 1 01/11/2214:13 TJW SW-DRYWT Cyanide, Reactive <0.125 mg/Kg 0.125 1 01/13/22 13:47 FMM SW-7.3.3 pH 6.27 s.u. 1 01/18/2210:03 SMW 9045D Qualifiers/ Outside QC Limit DF Dilution Factor Definitions Page 6 of 8 Waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.cwm Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-010-0012 Shipping Method 0 Fed Ex 0 US Postal Lab 0 LIPS 0 Client 0 Courier 0 Other: Thermometer ID: IRT-15 1.5 C Shipping container/cooler uncompromised? # Yes 0 No Number of coolers/boxes received I Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? * Yes 0 No COG agrees with sample label(s)? # Yes 0 No COC properly completed . Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 NIA High concentration container (48 hr) Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: oe S. Vigilant Date & Time: 1110/2022 13:04:24 Page 7 of 8 T zn z. nm L to a Z. l7 ❑c m z 0 N n �0LC 0 C Z �.-... nb S7 R Yi +� 'L {i fl M. rr n Cl `< a � n r 0 U C E tv _ a 0 0 G z C7 0 r« m 0 � C L f m C m a T G _4 x m 0 t O 3 3 xco a I3 to w m m V �92I m o v®� '0 CD O O•C D� .0 0. :Z6a a CL o CL �g CL Q 5'8 i d perp„' i .. a m d bG ro axCL a iSi4 > &' 1f m v � pr or a r m jR cm ► -4 CP x m p .� m G� m' 0 m-0 3 n 3LL Fm[1 Gm HN mbaca a m $ m- , Z T � m l7 Am _.. CL ❑ m A m "W m -� t1 O z to C. 0) m m Z -C ;L ° z < � =0,` o- ao G i m. ZZ-+n'a co dam OWN OL -Ym i°c a NC A �p1a-� m y Colo GL zm�`pym,.,ORQ Qm y i' DDew n� mm a� r n m m w m -. m 6 G \" � CL m m Ib y m m ' z a a m 4 0 r y y � m..� m �� rn a mXoc� :vm m m 8 m m m m 3 ?� �=rmninttn a�nr`zm .a to m 5zpzir GCA Q m m m 2 "�' y WaypointoANALYTICAL. 112812022 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-010-0013 Client Project Description: Class A Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical-com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/10/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the LISEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 6fflAe Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 12 Waypointo ANALYTICAL 449 Springbrook Rd,. Charlotte, NC 28217 Main 704.529.6364 www.waypointana lyti cal.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Ex iration Date North Carolina State Program 37735 07/31/2022 North Carolina State Program 402 12/31/2022 South Carolina State Program 99012 07/31/2022 South Carolina State Program 99012 12/31/2021 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2022 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00016122-010-0013 Page 2 of 12 Waypoint.0 ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lytica l-com sample Summary Table Report Number: 22-010-0013 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 6010D WP MTN 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 SW-1311 WP MTN 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 8081B WP MTN 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 8151A WP MTN 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 8270C WP MTN 91919 Class A Sludge 01/10/2022 07:48 01/10/2022 12:25 7470A WP MTN 91920 Class Solids 01/10/2022 07:48 01/10/2022 12:25 91920 Class A Solids 01/10/2022 07:48 01/10/2022 12:25 350.1 AES 91920 Class A Solids 01/10/2022 07:48 01/10/2022 12:25 6010D WP MTN 91920 Class A Solids 01/10/2022 07:48 01/10/2022 12:25 4500NORGD-2011 WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 12 Waypoint'.(D ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Lab Report Number: 22-010-0013 Date: 1 /24/2022 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypdintanalytical.com CASE NARRATIVE Separatory Funnel Extraction 8081 Method 3610C Sample 91919 (Class A) QC Batch No: L5949991L594999 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction Method 3510C QC Batch No: L5949611L594961 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis (TCLP) Method 6010D Sample 70025 Analyte: Selenium QC Batch No: L595452/L595216 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected; Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D Sample 91919 (Class A) QC Batch No: 1-59529711-594961 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non -target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Analysis note for PAN PAN Equation = 0.3 * (TKN —Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (25000 — 2290) + 0.5 * (2290) + 2.0 PAN = 7960 mglKg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Page 4 of 12 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number:22-010-0013 Lab No : 91919 Sample ID : Class A 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com REPORT OFANAL PSIS Report Date : 01/28/2022 Received : 01/10/2022 6xgw J- Jp LQI/ Terri W Cale Laboratory Project Manager Matrix: Sludge Sampled: 1/10/2022 7:48 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 01/17/22 14:00 PHI: SW-1311 TCLP Metals Extraction Leachate 1 01/17/22 14:00 PHE SW-1311 TCLP Pesticide Extraction Leachate 1 01/17/22 14:00 PHE SW-1311 TCLP SVOC Extraction Leachate 1 01/17/22 14:00 PHE SW-1311 TCLP VOC ZHE Extraction Leachate 1 01/12/22 14:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L595216 01/19/22 10:00 Prep Method: 3015A Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 01/19/22 17:29 TJS. L595452 TCLP Barium <0.250 mg/L 0.250 1 01/19/22 17:29 TJS L595452 TCLP Cadmium <0.0500 mg/L 0.0500 1 01/19/22 17:29 EAL L595452 TCLP Chromium <0.100 mg/L 0.100 1 01/19/22 17:29 TJS L595452 TCLP Lead <0.100 mg/L 0.100 1 01/19/22 17:29 TJS L595452 TCLP Selenium <0.500 mg/L 0.500 1 01/19/22 17:29 EAL L595452 TCLP Silver <0.0500 mg/L 0.0500 1 01/19/22 17:29 TJS L595452 Qualifiers/ Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 5 of 12 Waypoint.0 ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Report Number :22-010-0013 REPORTOFANALYSiS Lab No : 91919 Sample ID : Class A Report Date : 01/28/2022 Received : 01/10/2022 60W Terri W Cale Laboratory Project Manager Matrix: Sludge Sampled: 1110/2022 7:48 Analytical Method: 7470A Prep Batch(es): L595156 01/19/22 08:30 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 01/19/22 14:38 3W2 L595320 Analytical Method: 8081B Prep Batch(es): L594999 01/18/22 12:30 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.004000 mg/L 0.004000 10 01/19/22 23:46 VIC L595465 TCLP gamma-BHC <0.004000 mg/L 0.004000 10 01/19/22 23:46 VIC L595465 TCLP Methoxychlor <0.004000 mg/L 0.004000 10 01/19/22 23:46 VIC L595465 TCLP Toxaphene <0.03000 mg/L 0.03000 10 01/19/22 23:46 VIC L595465 TCLP Chlordane <0.02000 mg/L 0.02000 10 01/19/22 23:46 VIC L595465 TCLP Heptachlor Epoxide <0.004000 mg/L 0.004000 10 01/19/22 23:46 VIC L595465 TCLP Heptachlor <0.004000 mg/L 0.004000 10 01/19/22 23:46 VIC L595465 Surrogate: Decachlorobiphenyl 58.47 Limits: 36-116% 10 01/19/22 23:46 L595465 Surrogate: Tetrachloro-m-xylene 47.82 Limits: 25-123% 10 01/19/22 23:46 L595465 Analytical Method: 8151A Prep Batch(es): L595078 01/18/22 16:20 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 01/19/22 19:12 VIC L595487 TCLP 2,4,5 TP (Silvex) <0.0020 mg/L 0.0020 1 01/19/22 19:12 VIC L595487 Surrogate: DCAA 44.40 Limits: 20-120% 1 01/19/22 19:12 L595487 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 6 of 12 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC.28217 Main 704.529.6364 www.waypointanalytical.com Report Number : 22-010-0013 REPORT OFANAL YSIS Lab No : 91919 Sample ID : Class A Report Date : 01/28/2022 Received : 01/10/2022 6m Terri W Cale Laboratory Project Manager Matrix: Sludge Sampled: 1/10/2022 7:48 Analytical Method: 8260D Prep Batch(es): V13914 01/17/22 09:00 Prep Method: 5030B Test Results Units MOL DF Date I Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 01/17/22 21:13 JLB V13915 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Chloroform <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 01/17/22 21:13 ]LB V13915 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Methyl Ethyl Ketone (MEK) 0.194 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 01/17/22 21:13 JLB V13915 Surrogate: 4-Bromofluorobenzene 96.0 Limits: 80-124% 10 01/17/22 21:13 JLB V13915 Surrogate: Dibromofluoromethane 102 Limits: 75-129% 10 01/17/22 21:13 JLB V13915 Surrogate: Toluene-d8 85.4 Limits: 77-123% 10 01/17/22 21:13 JLB V13915 Analytical Method: 8270C Prep Batch(es): L594961 01/18/22 09:00 Prep Method: 3510C Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP 3&4 Methylphenol <0.200 mg/L 0.200 2 01/18/22 21:39 VBW L595297 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP Hexachlorobenzene <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 7 of 12 Waypoint 0 449 Springl7rook Rd, Charlotte, NC 28217 Main 704.529.6864 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 01/28/2022 369 Johnson Dairy Rd. Information : Received : 01/10/2022 Mooreseville, NC 28115 Terri W Cole Report Number :22-010-0013 REPORiOFAIVALYSIS Laboratory Project Manager Lab No : 91919 Matrix: Sludge Sample ID : Class Sampled: 1/10/20227:48 Analytical Method: 8270C Prep Batch(es): 1-594961 01/18/22 09:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP Hexachloroethane <0.100 mg1L 0.100 2 01/18/22 21:39 VBW L595297 TCLP Nitrobenzene <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP Pentachlorophenol <0.200 mg1L 0.200 2 01/18/22 21:39 VBW L595297 TCLP Pyridine <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP 2,4,5 Trichlorophenol <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 TCLP 2,4,6 Trichlorophenol <0.100 mg/L 0.100 2 01/18/22 21:39 VBW L595297 Surrogate: TCLP 2,4,6 Tribromophenol 49.6 Limits: 42-102% 2 01/18/22 21:39 L595297 Surrogate: TCLP 2-Fluorobiphenyl 28.4 Limits: 24-86% 2 01/18/22 21:39 L595297 Surrogate: TCLP 2-Fluorophenol 10.1 * Limits: 13-37% 2 01/18/22 21:39 L595297 Surrogate: TCLP 4-Terphenyl-d14 43.9 Limits: 30-122% 2 01/18/22 21:39 L595297 Surrogate: TCLP Nitrobenzene-d5 32.5 Limits: 25-78% 2 01/18/22 21:39 L595297 Surrogate: TCLP Phenol-d6 7.30 * Limits: 9-27% 2 01/18/22 21:39 L595297 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 8 of 12 0 Waypol . to . ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Report Number :22-010-0013 REFORTOFANALYSIS Lab No: 91920 Sample ID : Class A Report Date : 01/28/2022 Received : 01/10/2022 60 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 1/10/2022 7:48 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Fecal Coliform MPN/g <2.0 MPN/g - dry 2.0 1 01/10/22 14:20 SMW 9221E-2011 Moisture 3.92 % 1 01/11/2214:13 TJW SW-DRYWT Ammonia Nitrogen 2380 mg/Kg - dry 104 1 01/20/22 09:23 350.1 Nitrate+Nitrite-N <2.08 mg/Kg - dry 2.08 1 01/18/22 14:46 9056A pH 6.26 s.u. 1 01/18/2210:03 SMW 9045D Total Kjeldahl Nitrogen 26000 mg/Kg - dry 1640 10 01/14/22 14:44 CLP 4500NORGD-2011 Phosphorus 16200 mg/Kg - dry 52.0 10 01/17/22 19:49 TJS 6010D Aluminum 8650 mg/Kg - dry 26.0 10 01/18/22 20:44 EDV 6020B Arsenic 1.30 mg/Kg - dry 1.04 10 01/18/22 20:44 EDV 6020B Cadmium <0.520 mg/Kg - dry 0.520 10 01/18/22 20:44 EDV 6020B Copper 104 mg/Kg - dry 2.60 10 01/18/22 20:44 EDV 6020E Lead 3.96 mg/Kg - dry 1.04 10 01/18/22 20:44 EDV 60205 Mercury (Total) 0.0961 mg/Kg - dry 0.0312 1 01/14/22 11:35 EDV 7471E Molybdenum 11.4 mg/Kg - dry 1.04 10 01/18/22 20:44 EDV 6020B Nickel 5.60 mg/Kg - dry 1.04 10 01/18/22 20:44 EDV 6020E Potassium 1960 mg/Kg - dry 104 10 01/18/22 20:44 EDV 6020B Selenium <2.08 mg/Kg - dry 2.08 10 01/18/22 20:44 EDV 6020B Zinc 271 mg/Kg - dry 10.4 10 01/18/22 20:44 EDV 6020B Qualifiers/ * Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 9 of 12 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTR Report Number: 22-010-0013 Shipping Method 0 Fed Ex 0 US Postal Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: 11RT-15 1.5 C Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COG agrees with sample label(s)? Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? (0) Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) (� High concentration pre -weighed (methanol -14 d) [_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: Voe S. Vigilant Date & Time: 01/10/2022 13:09:42 Page 10 of 12 A L� L K L U) u T M A _ G ❑ C M L Z 0 cn H m n a °10 n _�� 0 ff n rn z a 0 h m a L7G0aom G? 7G a v,N n Lz 9 o coolb z i 0 0 w M m w ss Zr z 0 m 0 � yr O ro C1 > � r bz WeLM nO o. AnA b Y K & L zs n m Z. GLLta � 0 a z O Lfn r o 3 U L. C D Z zu m � T f"l N L: p b qa N r" u Q h n yLL0 R n M � G 7Ik n 0 VI I IL.) D n Q 0 w 0 m rim M rn V► r mFT to nz22 z N V1 M M = o 9 oa��� a t� ...�—. C` 7 7 h M 0x a a — a m 91 anQ 0 mCD M r•M m X a W a m m z4M=g o °m - k W - a Cc:) A O aCoo G M motor m 2 MM . N i.w C £ K7 01 = N n zO'v— N 0 EL m h a Al _am Cm rm=� u h�nm O n 0 C, r G1 <3 g �mm���Q n cMIDr tYlt uth �« th cF Q Z O r M 0 N "" 0 0 p C �. CL 7 . w z lu o �. 6 sR O x Z, M0 x D �+n I C N a.s °o ° rL ° 4 m m N 0 N Q I! D � m � K N in N C # N .� m ° M/ 13 13 en V UP maCCS� ..�. m c wi M of K01 wm 041 fA 0>Y F a H N ❑ f7 O C i A Y" 2 CL W n 0 Z 7 rnC U, M 3 z� Dmty(q) N v 5f o D z _ = -+ amm-� O q c 0 )> ry w a • m 2 ti7 fr�l�# E D Page 11 of 12 Op— C;L t ZL Q Z'U rn M Cy - �L6.c`� M i n n w 3 I G L m � m N n a m y Z -i ii - ZO 3 L: K m cr 0 C3 m v 0m 11 0. 0 Z ry O X D 13 LZ� n to 0g 0 N n 'sy " m 1 maLLW � Z m � L •• 0 ; U L Im b Z Z7 0 L.' C 3 �GLr A Z Z L m Chi r m MILL© CL tS m f!1 L CD 0 X r rr $ �' v 3 m a = to e v] m !E F oai r :33 _ m �n ro m C, m Cam] K) I I C� n i3. c a d m m N m m,v Om O m m N n z m D 33 h f!J a .O F d @ ° w Ina p1 x �� � D a m m m z O m tm��'� �m@,C a CS b m � 3 a , � W Q O L L C z m10 � a CL R' m mn m H z 0 N CL m,mc'�� a L 1G �n �W pam v OE r Z @ W. N L L bs M v N¢ or bx In Y =�tO a Dga o 0 a G m o ID 2 m W /" _ a_ �¢ C.n�� G m m m � � n y. A N z c C M* �. o 4 {` C m m .v A tin "G 40. IM Page 12 of 12 Waypoint(D ANALYTICAL 2/15/2022 Town of Mooresville/RR VWVf P Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-034-0023 Client Project Description: Class A Dried Sludge Dear Whitney Munroe: 449 Springbrook lid, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/3/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, CoJaVLOW '0- --&�) Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses ,performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 Waypoint..(D ANALYTICAL 449 Springbrook Rd,. Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State North Carolina North Carolina South Carolina South Carolina Program State Program State Program State Program State Program Lab ID Expiration Date 37735 07/31 /2022 402 12/31 /2022 99012 07/31 /2022 99012 12/31 /2021 Page 1 of 1 00016/22-034-0023 Page 2 of 7 0. a Waypoint, ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.064 www.waypointana"cai.Com Sample Summary Table Report Number: 22-034-0023 Client Project Description; Class A Dried Sludge Lab No Client Sample ID Matrix Date Collected Date Received 93376 Class A Solids 02/01/2022 08:35 02/03/2022 11:10 Page 3 of 7 waypointANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Dried Sludge Lab Report Number: 22-034-0023 Date: 2115/2022 SAR = [ 2.36 ] 1 SQRT { ( [2.37] + [2.00] )12 } = 1.60 SAR =[2.36]/SQRT {(4.37)12}=1.60 SAR = [ 2.36 ] 1 SQRT { 2,185) = 1.60 SAR = [ 2.36 ] 11.478 = 1.60 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. Page 4 of 7 0 Waypoint, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364. ANALYTICAL www.waypointanalytii;al.com 01205 Town of Mooresville/RR WWTP Project Class A Dried Sludge Whitney Munroe Report Date : 02/15/2022 369 Johnson Dairy Rd. Information : Received : 02/03/2022 Mooreseville, NC 28115 + 1l� Terri W Cole Report Number :22-034-0023 REPORT OFANALYSiS Laboratory Project Manager Lab No: 93376 Matrix: Solids Sample ID : Class Sampled: 2/1/2022 8:35 Test Results Units MQL DF Date 1 Time By Analytical Analyzed Method Calcium (saturated paste) 2.37 meq/L 0.250 1 02/12/22 16:05 1V/Mr Saturate Paste Magnesium (saturated paste) 2.00 meq/L 0.417 1 02/12/22 16:05 )V/Mr Saturate Paste Sodium (saturated paste) 2.36 meq/L 0.217 1 02/12/22 16:05 IV/MP Saturate Paste Sodium Absorption Ratio 1.60 1 02/12/22 16:05 M/Mr Saturate Paste Moisture 78.1 % 1 02/1012214:26 EDV SW-DRYWT Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 5 of 7 waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www waypointanalytical-corn Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-034-0023 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IRT-15 5.5 C Shipping container/cooler uncompromised? # Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample Iabel(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace - 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA F_ High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (0) No Comments: Signature: oe S. Vigilant I Date & Time: 2/03/2022 11:38:23 Page 6 of 7 hGGzL 'a Z C.) $ G a mY y aN 4 � e Z A'{ no m m m O L G mb a M. fi p my 9 D Z �m IV oy H A m°^� ZO tt ,,il, �'. { C . L:isG im I z a . LK C:G z m ' a t*G) xT N C MR II �4i N o Z r It G i M � � m E: qN ULM€ z I b C.. z I3 m o zml 'n p mo Li o (A G 7 I N GAP'• b Z ACA r p �i m 0 �LL0 x z.i am � m L � 0 Rj � e1 � 4) m N "zr M m„ Im i 9° m o 0 zflm ZZ N 00 A •d G3D� rn A • �— oma_ mpX r 3. m m 3 7 i m o 0 C vs 3 71 m m C m' @ m M tbFL mg"r m O O mOmm Z ,c m L L L z m *-1 CL m -< 76 7 v Q - f K a p, a. Li tD m Zz Nv L :u 6 m � D q H q ° a -L' i9 - n me nc, m mm�v� g aCrL m w R N � m v Z 0 Q U C ,. A IL R W n °— m m � �C ea m 3 Z a CA NC\ z \ M jz E 0 z z m r p r- rot km d w� D CL -1 rL Q Z K � w ID N C Ad ,ech.� _+) 5 0 � ^ c. F 10 �z s► �b r o � Q Page 7 of 7 Waypoint(D ANALYTICAL 5f212022 Town of Mooresville/RR W VrP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-101-0005 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.5213.6364 www waypointanalytica l.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/1112022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported. on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 6AA�) Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 20 Waypoint,,(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2022 North Carolina State Program 402 12/31/2022 South Carolina State Program 99012 07/31/2022 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2022 Florida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2022 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/202.2 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00016/22-101-0005 Page 2 of 20 a 449 Springbrook Rd, Charlotte, NC 28217 WaypointMain 704.529.6364 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-101-0005 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 98193 Class A Sludge 04/11/2022 08:40 04/11/2022 12:45 98193 Class Sludge 04/11/2022 08:40 04/11/2022 12:45 6010D WP MTN 98193 Class A Sludge 04/11/2022 08:40 04/11/2022 12:45 SW-1311 WP MTN 98193 Class A Sludge 04/11/2022 08:40 04/11/2022 12:45 8081A WP MTN 98193 Class Sludge 04/11/2022 08:40 04/11/2022 12:45 8151A WP MTN 98193 Class A Sludge 04/11/2022 08:40 04/11/2022 12:45 8270C WP MTN 98193 Class A Sludge 04/11/2022 08:40 04/11/2022 12:45 7470A WP MTN 98194 Class A Solids 04/11/2022 08:40 04/11/2022 12:45 98194 Class Solids 04/11/2022 08:40 04/11/2022 12:45 350.1 AES 98194 Class Solids 04/11/2022 08:40 04/11/2022 12:45 6010D WP MTN 98194 Class Solids 04/11/2022 08:40 04/11/2022 12:45 4500NORGD-2011 WP MTN 98305 Class SAR Solids 04/11/2022 08:40 04/11/2022 12:45 AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 20 (D Wayp * nt.. At 449 Springbrook Rd, Charlotte, NC 28217 Main 704.S29.6364 www.waVpointanalytical.com Client: Town of Mooresville/RR VWVTP CASE NARRATIVE Project: Class A Lab Report Number: 22-101-0005 Date: 5/2/2022 Ammonia was subcontracted to Analytical Environmental Services. PAN Equation = 0.3 * (61100 — 2540) + 0.5 * (2540) + 20.4 Pan = 30370 Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Analysis note for SAR SAR =[2.54 ]1SQRT t([1.68]+[1.74])12}=1.94 SAR =[2.54 ]ISQRT(3.42)12)= 1.94 SAR =[2.54 ]1SQRT{ 1.711= 1.94 SAR =[ 2.54 ] / 1.31 = 1.60 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. Concentrations for Na, Ca, and Mg are expressed in milli -equivalents per liter, and SQRT designates taking the square root of the operand in parentheses. Separatory Funnel Extraction 8081 Method 3510C Sample 98193 (Class A) QC Batch No: 1-612097/1-612097 The weightivolume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction Method 3510C Sample 98193 (Class A) QC Batch No: L6115361L611536 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 6010D Sample 98194 (Class A) QC Batch No: V176551V17465 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 98194 (Class A) QC Batch No: V 1 77731V1 7465 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 98194 (Class A) QC Batch No: V179681V17465 Page 4 of 20 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalydcal.com The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Solids Total Mercury Analysis - CVAA Method 7471 B Sample 98194 (Class A) QC Batch No: V1 7538/V1 7511 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Semivolatile Organic Compounds - GC/MS (TCLP) Method 82700 Sample 98193 (Class A) QC Batch No: L611851 /L611536 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non4arget analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Page 5 of 20 a aypoInt, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.corn 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 05/02/2022 369 Johnson Dairy Rd. Information: Received : 04/11/2022 Mooreseville , NC 28115 Terri W Cole Report Number :22-101-0005 REPORT OFANALVSIS Laboratory Project Manager Lab No : 98193 Matrix: Sludge Sample ID : Class A Sampled: 4/11/2022 8:40 Test Results Units MQL DF Date I Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 04/12/22 12:00 PHE SW-1311 TCLP Metals Extraction Leachate 1 04/12/22 12:00 PHE SW-1311 TCLP Pesticide Extraction Leachate 1 04/12/22 12:00 PHE SW-1311 TCLP SVOC Extraction Leachate 1 04/12/22 12:00 PHE SW-1311 TCLP VOC ZHE Extraction Leachate 1 04/13/22 13:30 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Satch(es): L611628 04/19/22 13:40 Prep Method: 3015A Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/20/22 16:27 EAL L611990 TCLP Barium <0.250 mg/L 0.250 1 04/20/22 16:27 EAL L611990 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/20/22 16:27 EAL L611990 TCLP Chromium <0.100 mg/L 0.100 1 04/20/22 16:27 EAL L611990 TCLP Lead <0.100 mg/L 0.100 1 04/20/22 16:27 EAL L611990 TCLP Selenium <0.500 mg/L 0.500 1 04/20/22 16:27 EAL L611990 TCLP Silver <0.0500 mg/L 0.0500 1 04/20/22 16:27 EAL L611990 Qualifiers/ * Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 6 of 20 a Waypoint 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalyVcal.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 05/02/2022 369 Johnson Dairy Rd. Information : Received: 04/11/2022 Mooreseville , NC 28115 60 W4 Terri W Cole Report Number :22-101-0005 REPORT OF ANALYSIS Laboratory Project Manager Lab No : 98193 Matrix: Sludge Sample ID : Class A Sampled: 4/11/2022 8.40 Analytical Method: 7470A Prep Batch(es): L612345 04/22/22 12:30 Prep Method. 7470A Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/22/22 16:29 JTR L612414 Analytical Method: 8081A Prep Batch(es): L612097 04/21/22 12A3 Prep Method: 3510C Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Endrin <0.004000 mg/L 0.004000 10 04/21/22 23:02 VIC L612354 TCLP gamma-BHC <0.004000 mg/L 0.004000 10 04/21/22 23:02 VIC L612354 TCLP Methoxychlor <0.004000 mg/L 0.004000 10 04/21/22 23:02 VIC L612354 TCLP Toxaphene <0.03000 mg/L 0.03000 10 04/21/22 23:02 VIC L612354 TCLP Chlordane <0.02000 mg/L 0.02000 10 04/21/22 23:02 VIC L612354 TCLP Heptachlor Epoxide <0.004000 mg/L 0.004000 10 04/21/22 23:02 VIC L612354 TCLP Heptachlor <0.004000 mg/L 0.004000 10 04/21/22 23:02 VIC L612354 Surrogate: Decachlarobiphenyl 67.50 Limits: 34-116% 10 04/21/22 23:02 L612354 Surrogate: Tetrachloro-m-xylene 49.83 Limits: 25-1230/0 10 04/21/22 23:02 L612354 Analytical Method: 8151A Prep Batch(es): L611664 04/16/22 16:15 Prep Method, 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 04/19/22 13:22 VIC L611668 TCLP 2,4,5 TP (Silvex) <0.0020 mg/L 0.0020 1 04/19/22 13:22 VIC L611668 Surrogate: DCAA 73.80 Limits: 20-120% 1 04/19/22 13:22 L611668 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 7 of 20 Waypoel. t ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number . 22-101-0005 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com REPORT OTANALYSIS Report Date: 05/02/2022 Received : 04/11/2022 0 U) 11 1P r .. V Terri W Cole Laboratory Project Manager Lab No : 98193 Matrix: Sludge Sample ID : Class A Sampled: 4/11/2022 8:40 Analytical Method: 8260D Prep Batch(es): V17873 04/21/22 09:00 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 04/21/22 23:23 ]LB V17874 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP Chloroform <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP 1,2-Dichloroethane <0,0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP i,i-Dichloroethene <0.0050 mg/L 0.0050 10 04/21/22 2323 JLB V17874 TCLP Methyl Ethyl Ketone (MEK) 0.170 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 04/21/22 23:23 JLB V17874 Surrogate: 4-Bromofluorobenzene 100 Limits: 80-124% 10 04/21/22 23:23 JLB V17874 Surrogate: Dibromofluoromethane 99.6 Limits: 75-129% 10 04/21/22 23:23 JLB V17874 Surrogate: Toluene-d8 99.2 Limits: 77-123% 10 04/21/22 23:23 JLB V17874 Analytical Method: 8270C Prep Batch(es): L611536 04/19/22 09:45 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP 3&4 Methylphenol <0.200 mg/L 0.200 2 04/19/22 20:06 VBW L611851 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP Nexachlorobenzene <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 8 of 20 Wayoi to ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-101-0005 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6264 www,waypointana lytica I Corn REPORT OFANALYSIS Report Date : 05/02/2022 Received : 04/11/2022 Terri W Cole Laboratory Project Manager Lab No : 98193 Matrix: Sludge Sample ID : Class A Sampled: 4/11/2022 8:40 Analytical Method. 8270C Prep Batch(es): L611536 04/19/22 09:45 Prep Method: 3510C Test Results Units MOL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP Hexachloroethane <0.100 m9/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP Nitrobenzene <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP Pentachlorophenol <0.200 m9/L 0.200 2 04/19/22 20:06 VBW L611851 TCLP Pyridine <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 TCLP 2r4,6-Trichlorophenol <0.100 mg/L 0.100 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP 2,4,6-Tribromophenol 36.8 * Limits: 42-102% 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP 2-Fluorobiphenyl 28.3 Limits: 24-86% 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP 2-Fluorophenol 12.5 * Limits: 13-370/a 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP 4-Terphenyl-d14 47.3 Limits: 30-122% 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP Nitrobenzene-6 37.5 Limits: 25-78% 2 04/19/22 20:06 VBW L611851 Surrogate: TCLP Phenol-d6 9.30 Limits: 9-27% 2 04/19/22 20:06 VBW L611851 Qualifiers/ Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 9 of 20 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytica Isom Report Number : 22-101-0005 REPOR7rOFANALYSIS Lab No: 98194 Sample ID : Class A Report Date: 05/02/2022 Received : 04/11/2022 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 4/11/2022 8:40 Test Results Units MQL DF Date I Time Analyzed By Analytical Method Fecal Coliform MPN/g 2.0 MPN/g - dry 2.0 1 04/11/22 13:13 SMW 9221E-2011 Moisture 1.80 % 1 04/1912212:36 ZSV SW-DRYWT Ammonia Nitrogen 2540 mg/Kg AR 1 04/19/22 14:45 350.1 Nitrate+ Nitrite-N <20.4 mg/Kg - dry 20.4 10 04/26/22 16:01 9056A pH 6.25 S.U. 1 04/18/2212:15 CLB 9045D Total Solids 95.6 % 0.010 1 04/18/22 12:30 ZSV 2540G-2011 Total Kjeldahl Nitrogen 61100 mg/Kg - dry 1640 10 04/20/22 16:29 CLP 4500NORGD-2011 Phosphorus 18000 mg/Kg - dry 25.5 5 04/21/22 20:15 TJS 6010D Aluminum 10700 mg/Kg - dry 25.5 5 04/20/22 15:56 EDV 6010D Arsenic <2.55 mg/Kg - dry 2.55 5 04/20/22 15:56 EDV 6010D Cadmium <0.509 mg/Kg - dry 0.509 5 04/18/22 17:42 EDV 60101) Copper 177 mg/Kg - dry 1.27 5 04/18/22 17:42 EDV 6010D Lead 6.46 mg/Kg - dry 1.53 5 04/18/22 17:42 EDV 6010D Mercury (Total) <0.153 mg/Kg - dry 0.153 5 04/15/22 11:27 EDV 7471E Molybdenum 13.3 mg/Kg - dry 2.55 5 04/25/22 14:12 EDV 6010D Nickel 9.62 mg/Kg - dry 1.27 5 04/18/22 17:42 EDV 6010D Potassium 3550 mg/Kg - dry 127 5 04/20/22 15:56 EDV 6010D Selenium 2.64 mg/Kg - dry 2.55 5 04/20/22 15:56 EDV 6010❑ Zinc 350 mg/Kg - dry 2.55 5 04/18/22 17:42 EDV 6010D Qualifiers/ * Outside QC limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 10 of 20 Waointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-101-0005 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lytica I.corn REPORT OFANALYSIS Report Date: 05/02/2022 Received : 04/11/2022 W4V. Terri W Cole Laboratory Project Manager Lab No: 98305 Sample ID : Class A SAR Matrix: Solids Sampled: 4/11/2022 8:40 Test Results Units MC1L DF Date / Time By Analytical Analyzed Method Calcium (saturated paste) 1.68 meq/L 0.050 1 04/12/22 15:00 JMC Saturate Paste Magnesium (saturated paste) 1.74 meq/L 0.083 1 04/12/22 15:00 JMC Saturate Paste Sodium (saturated paste) 2.54 meq/L 0.043 1 04/12/22 15:00 JMC Saturate Paste Sodium Absorption Ratio 1.94 1 04/12/22 15:00 JMC Saturate Paste Moisture 74.8 % 1 04/13/22.15:33 EDV SW-DRYWT Qualifiers/ * Outside QC Limit Definitions DF Dilution Factor Page 11 of 20 ACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W Cole PROJECT ID 22-101-0005 LABORATORY REPORT NUMBER 2204C05 DATE April 20, 2022 Primary Data Review By Secondary Data Review By a Chris Pafford Project Manager, AES PLEASE NOTE: Ashley Amick Project Manager, Access Analytical aamick@axs-inc.com - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - AMA-LAP,LLC (laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 12 of 20 Page 1 of 6 � 4 \ & l� a � � � f� § $ k�U 5kk cc -<3= ■� D g 7 ■ . Q 4 q d 5 k 2 � i 2 gymLn O z � j § a . ut \ . � e A � � d ■ £ 9 & k � � \ 0 § 2 0 9 a. f, a k 27 o\ ZY � a / 2 � e _ - com e � � \ x § CD§k & c o it u z � � � . � . � \ ® : n \� S / c £ I k & § k k E & _ a J 2 to \ / 0 \ \ Analytical Environmental Services, Inc Date: 20-Apr-22 Client: Waypoint Analytical Client Sample ID: 98194 Lab Order 2204C05 Tag Number: Class A Project Name: 22-101-0005 Collection Date: 4/11/2022 8:40:00 AM Lab lD: 2204C05-001A Matrix: Solid Analyses Result Qual MDL ReportinLimit fDatlyzlkdttchID DF Analyst Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 2540 106 215 mg/Kg-dry 334688 20 04/19/2022 14:45 TL PERCENT MOISTURE D2216 Percent Moisture 6.78 0 0 Wti/. R483181 1 04/15/2022 00:00 7W Qualifiers: " Value exceeds maximum contaminant level E Estimated value above quantitation range BRL Not Detected at MDL S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded > Greater thau Result value N Analyte not NELAC certified 3 Estimated value detected below Reporting Limit B Analyte detected in the associated method blank ¢ Less than Result value Page 14 of 20 Page 3of6 i•N+ N E 0 u N v CL y U O 0 W u p � on F 71 °1 � v O � � c m A -p v u a U C Z O Z .. � M w r 14 r1iiW�1 o w w a a � al N cp m K 0 m 0 ai 0 'a cv O v v c ai `w nL a c a, d n. nFn o E U a b c ° a r a8 C M1 (0 W L di CL L y a F L i [V m 'O a7 n a bFD U e-I nl O FO = a 0 u M_ N o a 0 ° m v a `0 v y c a 7 T C w" v m O• O Q O 0 w N E y p R f0 D_ 7 R Y F• �--' UF— ,� 'a -o v 0 o a Cc o E o 0 a o 7 W m 0, c c 77� u E L t E V o U 0 vn U U F- 7 Fa-• U a+ U U Lm m N 0 Q J w ai Ln a�tn N M r4 m M N M N _ Intl' 7 zz q rn cc CD� N � y a M 4 c N N N N c O K U a �� �� 00C� O, y bV5 'f OLfj U CX ®' Cd•y A �a 7 Q ?, x ti R a to a z o a oy a o a Q oy M a a C) N_ T O -IR b _ O CL O O A! k9e O tn N N as N h LO gyp• ° 0.1 N N W4 C v'i v trxj W cn Gs7 W z z z z O m O r ❑ ,n O o O e i-1 O a pray� 'z ot z a z z .� C? o aN a 7 A R - e o e n W War W W o Z o Z o N N a°Oo a M � ¢ O m U ",I CAC Uv A d C ° aai n R6 bo tc 2 G C O 0 O W w 3 ¢ z ¢ z < z V)� ¢ z a QD O LO 0 N w 0 N M a End of Report Page 17 of 20 Page 6 of 6 Waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-101-0005 Shipping Method 0 Fed Ex 0 US Postal +! Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: 11RT-15 5.6 C Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received I ' Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? Yes 0 No CDC agrees with sample Iabel(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 NIA F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (# No Comments: Signature: oe S. Vigilant Date & Time: 04/11/2022 13:26:07 Page 18 of 20 ci r EI � �G#C7t N N a N a a O m 0 y m im z Q 91 0 0 m m f » 0 3 ID a '0 d r .r rC > rmw, -a a S z tR N � I en K � n a � a to O s m x- a m N IR m 3 m m7 �Q� Ma c 1 m o mom z y -rv;t^rn©m - Zir-; rA ICH v 'r 17 al galN 0 t. 4 m� 'pg❑ QCL O m � m to a 3 CL m� W � to W N�O V , sOL yo«�° a m RCL- CL C m o pr a U Iz Page 19 of 20 ID. L Z z. c 3 DM L(a s i to m�[ n5 4 m L x� S 0 rom 931 m nr z �' 9r Op m N . C-) .y N emiLL22 �m 67 Z,_ m ..� 'pro G z N � sy iCC I w . 4 �•1 y Im O ro m� L© �.w m A 4 -� 11 ❑ o 0 rn r- az. m L Ll ;a n L a 0 L L 6F7 m o Z c 0� O Z o rcn v 0. unf GG � n .ZZ A 0 L.L z w z x a m N a - y L . a N m A c .. z F- m Fn fj• m = lc �L 0 S � 0 m �m a A� =30 C mg CAp m CID a o O x V1 .m �{ m-C d 3 vy?b. 1m7k N •gyp O cR._ n ELa ,vim_„_ N m t• iii mtn .03 go 'j ' Z at 0 Z ova zx I r z a m m m Z w O Y fA n�� N O "O •- v c _ -- a m m Eei Y� Q m m �axaa m Z e. �.�. # n s CL acl e I a + m r�z, 0g�gg 3 [] p, . 1 (A 7 OW o o, V,••,4 �N M. L to = G G �.' \ 7 co � D . H C. mKO�rro Off' 3 �tl t Y a * m m n In � m 0 m'm t -Z * m m z m w m c, v !Kn\ t a d Z 5 vn.a�zrn i cn 7 4K qn� D m i r /l° a ZO (mA < � � a m o Z n 0 ga 0 Y a m 3 CL. IA. \ 1�11< c 1 I I o r in ���11II Page 20 of 20 Waypointo ANALYTICAL 8/12/2022 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-199-0003 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Chartotte, NC 28217 Main 704.529.6364 www.waypointanalytieal.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/18/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 24 o Waoint ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.520.6364 www.waypointanalyflcal.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State North Carolina North Carolina South Carolina South Carolina Program Lab ID State Program 37735 State Program 402 State Program 99012 State Program 99012 Laboratory 1D: WP MTN: Waypoint Analytical, LLC., Memphis, TN Expiration Date 07/31 /2023 12131 /2022 07/31 /2022 12/31/2022 State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00016/22-199-0003 Page 2 of 24 0 (2) Waypoint, ANALYTICAL Report Number: 22-199-0003 Client Project Description: Class A 449 Springbroak Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanaiytica l.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 94547 Class A Sludge 07/18/2022 08:15 07/18/2022 11:54 94548 Class A Solids 07/18/2022 08:15 07/18/2022 11:54 94548 Class Solids 07/18/202206:15 07/18/2022 11:54 350.1 AES 94548 Class A Solids 07/18/2022 08:15 07/18/2022 11:54 6010D WP MTN 94548 Class Solids 07/18/2022 08:15 07/18/2022 11:54 4500NORGD-2011 WP MTN 94571 Class A SAR Solids 07/18/2022 11:54 AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 24 Waypoint(D ANALYTICAL Client: Town of Mooresville/RR WVVTP Project: Class A Lab Report Number: 22-199-0003 Date: 8/8/2022 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE This is a revised report and supersedes the original laboratory report dated 8110/22. The SAR calculation has been added to the case narrative. TCLP Herbicides was not completed due to laboratory error. The client will resample. Ammonia was subcontracted to Analytical Environmental Services. Block Digestion and FIA Method 4500NORGD-2011 QC Batch No: L628501 Percent recovery for the matrix spike analysis was outside of the allowable QC limits. QC Batch No: L628501 The MS recovery is outside QC acceptance limits. Metals Analysis Method 601 OD Sample 84141 QC Batch No: L628813/L628403 One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are required. Sample 84141 QC Batch No: L628985/L628403 One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are required. Sample 84141 Analyte: Aluminum QC Batch No: L6292951L628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Arsenic QC Batch No: L6292951L628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Calcium QC Batch No: L6292951L628403 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 4 of 24 0 Waypoint 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com Sample 84141 Analyte: Potassium QC Batch No: L6288131L628403 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Sample 84141 Analyte: Potassium QC Batch No: L6292951L628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Magnesium QC Batch No: 1-629295/1-628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Phosphorus QC Batch No: 1-629295/1-628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Lead QC Batch No: 1-629295/1-628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Selenium QC Batch No: 1-629295/1-628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 84141 Analyte: Zinc QC Batch No: L629295/1-628403 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94648 (Class A) QC Batch No: V217621V21654 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 94826 QC Batch No: V21762/V21654 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Page 5 of 24 Waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Sample 94826 Analyte: Calcium QC Batch No: V21762N21654 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 94826 Analyte: Calcium QC Batch No: V21762N21654 The MSIMSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Sample 94826 Analyte: Cadmium QC Batch No: V21762N21654 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: V21762N21654 LLC failed high. Result 1 OX concentration. Result not affected. Sample 94826 Analyte: Potassium QC Batch No: V21762N21654 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94826 Analyte: Lead QC Batch No: V21762N21654 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94826 Analyte: Selenium QC Batch No: V21696/V21654 LLC failed high. Sample concentration BRL. Result not affected. Sample 94826 Analyte: Zinc QC Batch No: V21762IV21654 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94826 Analyte: Zinc QC Batch No: V21762/V21654 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Metals Analysis (TCLP) Method 601 OD Analyte: Barium QC Batch No: V21935N21913 Page 6 of 24 Waypointo ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704,529.6364 www.waypointana lytical.com CCB failed high. Samples BRL or 1 Ox concentration. Results not affected. Analyte: Chromium QC Batch No: V21935N21913 LLC failed high. Sample concentration BRL. Results not affected. Mercury Method 7470A Sample 94547 (Class A) QC Batch No: V216941V21694 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Solids Total Mercury Analysis - CVAA Method 7471E Sample 94548 (Class A) QC Batch No: V21661IV21642 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Organochlorine Pesticides by GC (TCLP) Method 8081 B Analyte: gamma-BHC QC Batch No: V22153N22009 Analyte above range in CCV. Not detected in samples No further action taken. Analyte: Heptachlor epoxide QC Batch No: V22153N22009 Analyte above range in CCV. Not detected in samples No further action taken. Sample 94547 (Class A) Analyte: Tetrachloro-m-xylene QC Batch No: V22153N22009 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270E Sample 94547 (Class A) QC Batch No: V22096N22095 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. SAR =[4.60]ISQRT{([12.5]+[5.18])12} SAR =[4.6011SQRT{( 17.68 )12} SAR =[4.60]ISQRT{8.84} SAR = [ 4.60112.97 SAR =1.54 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 + (59900-3720) + 0.5 x 3720 + 10.5 PAN =16854 + 1865.25 Page 7 of 24 waypointo ANALYTICAL PAN = 18719.25 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalyVcal.com Page 8 of 24 0 Waypoint, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6164 ANALYTICAL www,waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 08/12/2022 369 Johnson Dairy Rd. Information : Received: 07/18/2022 Mooreseville , NC 28115 60 Terri W Cole Report Number :22-199-0003 REPORT OF ANALYSIS Laboratory Project Manager Lab No : 94547 Matrix: Sludge Sample ID : Class Sampled: 7/18/20228:15 Test Results Units MQL DF Date I Time By Analytical Analyzed Method TCLP Metals Extraction Leachate 1 07/20/22 15:23 LMZ SW-1311 TCLP Pesticide Extraction Leachate 1 07/20/22 15:23 LMZ SW-1311 TCLP SVOC Extraction Leachate 1 07/20/22 15:23 LMZ SW-1311 TCLP VOC ZHE Extraction Leachate 1 07/20/22 13:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): V21913 07/27/22 10:32 Prep Method: SW-3010A Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Arsenic <0.050 m91L 0.050 1 07/27/22 14:09 EDV V21935 TCLP Barium <0.050 mg/L 0.050 1 07/28/22 14:28 EDV V21935 TCLP Cadmium <0.0150 mg/L 0.0150 1 07/27/22 14:09 EDV V21935 TCLP Chromium <0.025 mg/L 0.025 1 07/27/22 14:09 EDV V21935 TCLP Lead <0.030 mg/L 0.030 1 07/27/22 14:09 EDV V21935 TCLP Selenium <0.100 mg/L 0.100 1 07/27/22 14:09 EDV V21935 TCLP Silver <0.025 mg/L 0.025 1 07/27/22 14:09 EDV V21935 Analytical Method: 7470A Prep Batch(es): V21694 07/22/22 12:48 Prep Method: 7470A Test Results Units MQL DF Bate / Time By Analytical Analyzed Batch TCLP Mercury <0.0008 mg/L 0.0008 1 07/22/22 17:14 EDV V21745 Qualifiers/ Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 9 of 24 0 Waypoint 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date ; 08/12/2022 369 Johnson Dairy Rd. Information : Received : 07/18/2022 Mooreseville, NC 28115 60LO U-4 Terri W Cole Report Number : 22-199-0003 REPORTOFANALYSIS Laboratory Project Manager Lab No: 94547 Matrix: Sludge Sample ID : Class A Sampled: 7/18/2022 8:15 Analytical Method: 8081B Prep Batch(es): V22009 07/29/22 09:17 Prep Method: 3510C Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Endrin <0.000250 mg/L 0.000250 1 08/02/22 15:30 3C1 V22153 TCLP gamma-BHC <0.000250 mg/L 0.000250 1 08/02/22 15:30 JCS V22153 TCLP Methoxychlor <0.000500 mg/L 0.000500 1 08/02/22 15:30 JC1 V22153 TCLP Toxaphene <0.005000 mg/L 0.005000 1 08/02/22 15:30 JC1 V22153 TCLP Chlordane <0.002500 mg/L 0.002500 1 08/02/22 15:30 JC1 V22153 TCLP Heptachlor Epoxide <0.000500 mg/L 0.000500 1 08/02/22 15:30 JC1 V22153 TCLP Heptachlor <0.000250 mg/L 0.000250 1 08/02/22 15:30 JC1 V22153 Surrogate: Decachlorobiphenyl 48.00 Limits: 13-186% 1 08/02/22 15:30 JC1 V22153 Surrogate: Tetrachloro-m-xylene 32.00 * Limits: 40-134% 1 08/02/22 15:30 JC1 V22153 Analytical Method: 8260D Prep Batch(es): V22041 07/28/22 09:00 Prep Method: 5030E Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 07/28/22 14:01 JLB V22042 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP Chloroform <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP Methyl Ethyl Ketone (MEK) 0.110 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP Tetrachloroethene <0,0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 10 of 24 Waypointo. ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytica l.corn Report Number :22-199-0003 REPORTOFANALYSIS Lab No : 94547 Sample ID : Class A Report Date : 08/12/2022 Received : 07/18/2022 Terri W Cale Laboratory Project Manager Matrix: Sludge Sampled: 7/18/2022 8:15 Analytical Method: 8260D Prep Batch(es): V22041 07/28/22 09:00 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Trichloroethene <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 07/28/22 14:01 JLB V22042 Surrogate; 4-Bromofluorobenzene 97.8 Limits: 80-124% 10 07/28/22 14:01 JLB V22042 Surrogate: Dibromofluoromethane 100 Limits: 75-129% 10 07/28/22 14:01 31-13 V22042 Surrogate: Toluene-d8 95.0 Limits: 77-123% 10 07/28/22 14:01 JLB V22042 Analytical Method: 8270E Prep Satch(es): V22095 07/26/22 08:56 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP 3&4 Methylphenol <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP 2,4-Dinitrotoluene <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP Hexachlorobenzene <0.100 mg/L 0.100 1 07/26/22 21:30 JMV V22096 TCLP Hexachlorobutadiene <0.100 mg/L 0.100 1 07/26/22 21:30 JMV V22096 TCLP Hexachloroethane <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP Nitrobenzene <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP Pentachlorophenol <0.250 mg/L 0.250 1 07/26/22 21:30 JMV V22096 TCLP Pyridine <0.050 mg/L 0.050 1 07/26/22 21:30 JMV V22096 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 1 07/26/22 21:30 JMV V22096 Qualifiers/ Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 11 of 24 Wayoint ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 23217 Main 704.529.6864 www.waypointanalytica i.corn Report Number :22-199-0003 REPORT OFANAL YSIS Lab No : 94547 Sample ID : Class A Report Date: 08/12/2022 Received : 07/18/2022 Terri W Cale Laboratory Project Manager Matrix: Sludge Sampled: 7/18/2022 8:15 Analytical Method: 8270E Prep Batch(es): V22095 07/26/22 08:56 Prep Method: 3510C Test Results Units 14 OL DF Date / Time By Analytical Analyzed Batch TCLP 2,4,6-Trichlorophenol <0.100 mg/L 0.100 1 07/26/22 21:30 3MV V22096 Surrogate: TCLP Phenol-d5 8.20 * Limits: 11-100% 1 07/26/22 21:30 3MV 8270E Surrogate: TCLP 2,4,6-Tribromophenol 24.2 * Limits: 43-140% 1 07/26/22 21:30 JMV V22096 Surrogate: TCLP 2-Fluorobiphenyl 15.6 * Limits: 44-119% 1 07/26/22 21:30 JMV V22096 Surrogate: TCLP 2-Fluorophenol 11.2 * Limits: 20-119% 1 07/26/22 21:30 JMV V22096 Surrogate: TCLP 4 Terphenyl-d14 25.2 * Limits: 44-120% 1 07/26/22 21:30 JMV V22096 Surrogate: TCLP Nitrobenzene-d5 12.8 * Limits: 44-120% 1 07/26/22 21:30 3MV V22096 Qualifiers/ * outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 12 of 24 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 3ohnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-199-0003 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6164 www.waypointanalytica Isom REPORT OF ANALYSIS Report Date : 08/12/2022 Received : 07/18/2022 Ld CQJ-� Terri W Cole Laboratory Project Manager Lab No: 94548 Sample ID : Class Matrix: Solids Sampled: 7/18/2022 8:15 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Fecal Coliform MPN/g <2.1 MPN/g - dry 2.1 1 07/18/22 12:53 SMW 9221E-2011 Plant Available Nitrogen 18719.25 1 CALCULATION Moisture 4.80 11/0 1 07/26/2210:58 ADC SW-DRYWT Ammonia Nitrogen 3720 mg/Kg AR 1 07/28/22 13:03 350.1 Nitrate+Nitrite-N <10.5 mg/Kg - dry 10.5 10 07/21/22.17:43 CEG 9056A PH 6.22 S.U. 1 07/19/2213:00 CLB 9045D Total Solids 95.1 °/a 0.010 1 07/26/2210:58 ADC 2540G-2011 Total Kjeldahl Nitrogen 59900 mg/Kg - dry 3130 10 07/25/22 15:56 ANH 4500NORGD-2011 Phosphorus 17500 mg/Kg - dry 26.3 5 07/27/22 14:14 EAL 6010D Aluminum 16000 mg/Kg - dry 26.3 5 07/22/22 18:42 EDV 6010D Arsenic <2.63 mg/Kg - dry 2.63 5 07/22/22 18:42 EDV 6010D Cadmium 0.588 mg/Kg - dry 0.525 5 07/22/22 18:42 EDV 6010D Calcium 18000 mg/Kg - dry 26.3 5 07/22/22 18:42 EDV 6010D Copper 291 mg/Kg - dry 1.31 5 07/22/22 18:42 EDV 6010D Lead 11.3 mg/Kg - dry 1.58 5 07/22/22 18:42 EDV 6010D Magnesium 2250 mg/Kg - dry 26.3 5 07/22/22 18:42 EDV 6010D Mercury (Total) 0.686 mg/Kg - dry 0.158 5 07/21/22 16:29 EDV 7471B Molybdenum 29.7 mg/Kg - dry 2.63 5 07/22/22 18:42 EDV 6010D Nickel 14.5 mg/Kg - dry 1.31 5 07/22/22 18:42 EDV 6010D Potassium 2420 mg/Kg - dry 131 5 07/22/22 18:42 EDV 6010D Selenium 4.68 mg/Kg - dry 2.63 5 07/22/22 18:42 EDV 6010D Sodium 912 mg/Kg - dry 263 5 07/22/22 18:42 EDV 6010D Qualifiers/ Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 13 of 24 waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-199-0003 Lab No : 94548 Sample ID : Class A Test Zinc 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com REPORT OFANALYSIS Results Units 667 mg/Kg - dry MQL 2.63 Report Date : 08/12/2022 Received : 07/18/2022 6mw '- J!P CQJJ Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 7/18/2022 8:15 DF Date I Time By Analytical Analyzed Method 5 07/22/22 18:42 EDV 6010D Qualifiers/ Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 14 of 24 Waypoint, 449 Sgringbrovtc Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 08/12/2022 369 Johnson Dairy Rd. Information : Received : 07/18/2022 Moareseville , NC 28115 0 W4 V Terri W Cale Report Number : 22-199-0003 REPORTOFANALYSIS Laboratory Project Manager Lab No : 94571 Matrix: Solids Sample ID : Class A SAR Sampled: Test Results Units MOL DF Date / Time By Analytical Analyzed Method Calcium (saturated paste) 12.5 meq/L 0.250 1 07/26/22 15:58 EDV Saturate Paste Magnesium (saturated paste) 5.18 meq/L 0.417 1 07/26/22 15:58 EDV Saturate Paste Sodium (saturated paste) 4.60 meq/L 0.217 1 07/26/22 15:58 EDV Saturate Paste Sodium Absorption Ratio 1.54 1 07/26/22 15:58 EDV Saturate Paste Moisture 4.80 % 1 07/2612210:58 ADC SW-DRYWT Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions Page 15 of 24 Acass ANALYC[CAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical, LLC (Charlotte) 449 Springbrook Road Charlotte NC 28217 ATTENTION 'Perri W Cole PROJECTID 22-199-003 LABORATORY REPORT NUMBER 2207K58 DATE July 29, 2022 Primary Data Review By Secondary Data Review By j� Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory It 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory it E87582 ARIA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803,781.4243 or toll fee at 883.315.4243 Page 16 of 24 Page 1 of 6 -60 _ o � R CLI � 2a$ #§4 z �k aka 0 M cc .| 2 , ■ � � \� q PQ a �.� . / K @ §j £ £ . p « % £ N 'Con / / MewrL ? 2 2 I k�§ 7 2co k® z Q a m c. G. 2 = q . Cr' k U / z § k� U. . . z e. § m ) 3 q e 2 / 0 caG 2 k 2 e = . \ \ A . . 41 2 \ \ \ � \ � � % v v + # a \ C o � ■ a m k © G ^ t t: CD j CL � o c UJ W . § § \ k F- 2� ) �.. / � c cn .To . § \ \ �.. Ln / k .I > ƒ\ & % CL in § - cr. k /. « I J .I � Analytical Environmental Services, Inc Date: 28-Jul-22 Client: Waypoint Analytical, LLC (Charlotte) Client Sample ID: 94548 Lab Order 2207K58 Tag Number: Class A Project Name: 22-199-003 Collection Date: 7/18/2022 8:15:00 AM Lab ID: 2207K58-001A Matrix: Solid Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst Limit Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 3720 106 215 mg/Kg-dry 340417 20 07/28/2022 13:03 T1. PERCENT MOISTURE D2216 Percent Moisture 7.05 0 0 wp/. R491674 1 07/21/2022 00:00 JW Qualifters: . Value exceeds maximum contaminant level E Estimated value above quantilation range BRL Not Detected at MDL S. Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded > Greater than Result value N Analyte notNELAC certified I Estimated value detected below Reporting Limit B Analyte detected in the associated method blank < Less than Result value Page 18 of 24 Page 3 of 6 -4 w to 3 � d m c � � m w m m w a U Q Q F Q m h m a a c 0 0 w U u a z U 0 o c e w = U U =a a c �`• C N w w U 3 u a o O d (u n• C C •C 0 O O t 0u c o Y c 0 : 'y 00 w y 'Q C . N Q m u a to c� o p'w O •-• m i.l w V U w a) V C � O_ y C p c G L) s 7 7 � N u Y �� U •� v y m m w L Y Y O T C w Q' o w Q W a y E o o m E E w y y U U �--� 111 iw+ R 0 E w y y E d O c O 0- Gl @ C 0- 'm "m a' c fl E o E E ¢ °0 U 0 U t=if U U Fa U w U U of ~ U q J a z a z } N ' -0 w G � � V U c � x Q O c 0 N � � Z n• � ` c Q E O_ 4Jy. Q- L4 u w (n O a) to 0 r y m r_ c •- ai V V @ fl. .LD E (D w m cC c o c E o t2 w (U i m c V a w m C ou = x N Y N ¢ E N 7 G m U r4 of m N N N c m O M 00 N 0 a � r a � a '� a N a O _ Y M php M 04 N M Opp N el)00 N R 0 ON ONM Ul z z A zz fa zz A zzca La m a ar Q Q Q 00el p F4 M N N o' N N N N N N � U " N N N N N N N H a r •� W W � ~ ''mil � —�1i � _T Q cl ¢ i 0.'i +-+ cD a a 3 3 3 3 rn C F cq N c c 0 ,y ka en a y w 7 i d > C c a ` .� m v? n a V > h v V cu z R w x O L x O .4 O W v] G] c W cn W e �-7 O aWy O o N eay H Q Q P�yl Q v Q F4 L4 ai W e 00 00 b° 7 4 R o V a+ •z aiS z a eh v a V U NN- y R+ y N p cOCrI 3 R p = v m A e7 00 � k x W W = - g 0 a csN oLn �ra Mco� � j p W p N N N n R ci cu 41 m M o W a 3 Qn z rn cn d G' End of Report Page 21 of 24 Page 6 of 6 Waypoint(D ANALYTICAL 449 Springbrook Itd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-199-0003 Shipping Method 0 Fed Ex 0 US Postal * Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: I IRT-15 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? (0) Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) [_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes # No Comments: Signature: Angelo Norvell bate & Time: 07/18/2022 12:21:26 Page 22 of 24 �. PRO- zL) z. nMm FL y,, 'a 0 Lm_ R rA m ro �az�� Y m ( H Z 0 c °K,.V CS 1�t1� �xa. m aLa m n z D ro G) m e?z 0 m T r o u G :E a ca � m aIn C]Lln't� z m 0 t a AZ z C ❑� 9 Z z n li i a-m =r 0 A: n 0 n 0 3 m 9 m»lam 9 a ar men -ZI 77t O 0 �m Taws a/MoaresvillelRR WWip 0ms 7 M2022 Class A 12:20:19 =30 0 IF m G xr 7a c7 ro m 0 0 m D O a `0 CL C. » MCC - ro � m �. W X > 00 ash v r- N2 _ Ac-. • ' W V ��o m• rmn ?.o a. i a 7 . m * ` z i aIf Ir+:a X � m 0 -- v Page 23 of 24 i Zlpii _ v a y ( u ©� .:J zss: L x rn ❑ as v QF .' P d b Z Q o n �a 31 w i9 > 0Q. Ll ❑ m a Tm �It Gi Z � to C ma m Cl ::E s � c . m A C $ '' .. j. e+Lip 3 � � o _ m a �•m m O tls '1 :cam Cl m �ClE}m and � � n �+e a m �m g 0 m� 3 c Li U ar c zz w 0 rleg loco -- M o a m m Gk ?d G 3 m 111 m n � i A m m 9 m N PD am n c Qm zcn a cn 4� _� M N gppv0 N w Page 24 of 24 0 r �M �m C7 �mwf: �. •� 6 Y1 G 3 R1 Ql m 0 rn m o.0 p FL a O c��; wp�' m z C CL GCL Ll ��. m 0 T Cf 2 N M r n m LL z a o a o ° w CS a � = W. .r -'d m� - OL m � 4 tr uz 0 �m C • :ate D.3aiS'o «k C. 0, m m A t9. m a r H c 0 tt► z xc! "0 O . C� A. C,\ X M WaypointANALYTICAL 8/19/2022 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-217-0041 Client Project Description: Class A TCLP Herbicides Resample Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/5/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 6fflAc Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 Waypoint ANALYTICAL 449 Springbrooh Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2022 South Carofina State Program 99012 07/31/2022 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00016122-217-0041 Page 2 of 7 (D Waypoint�. 44g Springbrook Rd, Charlotte, NC 2$217 Main 704.529.6364 ANALYTICAL www.waypointana"cal.com Sample Summary Table Report Number: 22-217-0041 Client Project Description: Class A TCLP Herbicides Resample Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 96249 Class A Sludge 08/05/2022 08:35 08/05/2022 11:46 8151A WP MTN 96249 Class A Sludge 08/05/2022 08:35 08/05/2022 11:46 SW-1311 WP MTN 0 WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 7 Waypoint(D ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A TCLP Lab Report Number: 22-217-0041 Date: 8/19/2022 449 Springbraok Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE TCLP Herbicides were subcontracted to Waypoint Memphis. Page 4 of 7 Waypointo ANALYTICAL 01205 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointa na lytica I-com Town of Mooresville/RR WWTP Project Class A TCLP Whitney Munroe Report Date : 08/19/2022 369 Johnson Dairy Rd. Information : Herbicides Resample Received : 08/05/2022 Maoreseville , NC 28115 f�I Terri W Cole Report Number : 22-217-0041 REPORT QFANALYSIS Laboratory Project Manager Lab No : 96249 Matrix: Sludge Sample ID : Class A Sampled: 8/5/2022 8:35 Test Results Units MCIL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate Analytical Method: 8151A Prep Method: 8151A Test Results 1 08/10/2213:00 HAW SW-1311 Prep Satch(es): L632212 08/15/22 15:54 Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 TCLP 2,4,5 TP (Silvex) <0.0020 mg/L 0.0020 Surrogate: DCAA 32.80 Limits: 20-120% 1 08/17/22 21:42 VIC L632869 1 08/17/22 21:42 VIC L632869 1 08/17/22 21:42 L632869 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 5 of 7 0 . 0 Waypoint ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number:01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-217-0041 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IRT-15 1.7 C Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received I ' Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No # Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? Q Yes 0 No COG properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No 0 NIA Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 NIA (— High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: erri W Cole Date & Time: 8/05/2022 17:14:20 Page 6 of 7 ty� 'a$ O n�' I LI U wdl x -1 u 0 C ❑ a i r o S; i m ry . iiccl ..a = 0 9 �. 00 3 upw n cr ai i a n M a D) Lu 2D w 0 — G1 � X 2 a u 2 9 . w m 0:* qyy 4 m f1 ip V r F zr r o 0� � m o i m Cf a' L .. Ia � G C Os A z2 ID Fry' Sl E� n ZZ asi 00 r � wr N n Gc0 a Q. m N Lj' Q N mN 3 m to w m f m aA z �, a m po z 1� 0 3 CD Page 7 of 7 h n 0 m m v imll- x m ? M m m m 4m ImoM d C m R7 40 a n c omQ� Wecu m z <am�C;Gc m N yN, ° L 6 az Hb a N 7 p N rwxaOa L7m y an w m n a f N Li mmNN, A �Sc nm Cpv J ❑ c C,M . .� L C o@ V � m 1�I1 x o'ACLW, 0 o a t> > m --z 4, = c i] m 0 ji s n 9 . cm ze - r Q m m i o s° v (D Waoint ANALYTICAL 10/25/2022 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 22-283-0009 Client Project Description: Class A Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointana lytica l-corn Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/10/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis_ Page 1 of 22 Waypoint,.. ANALYTICAL 449 Springbrook Rd,. Charlotte, NC 28217 Main 704.529.6364 www.waypointanalyfical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State North Carolina North Carolina South Carolina South Carolina Program Lab ID State Program 37735 State Program 402 State Program 99012 State Program 99012 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN Exoiration Date 07/31 /2023 12/31/2022 07/31 /2023 12/31/2022 State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016122-283-0009 Page 2 of 22 a WaYPOint ANALYTICAL Report Number: 22-283-0009 Client Project Description: Class A 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalydr,al.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 90311 Class A Sludge 10/10/2022 07:38 10/10/2022 11:42 90311 Class A Sludge 10/10/2022 07:38 10/10/2022 11:42 80818 WP MTN 90311 Class Sludge 10/10/2022 07:38 10/10/2022 11:42 SW-1311 WP MTN 90311 Class Sludge 10/10/2022 07:38 10/10/2022 11:42 8151A WP MTN 90312 Class A Solids 10/10/2022 07:38 10/10/2022 11:42 90312 Class A Solids 10/10/2022 07:38 10/10/2022 11:42 350.1 AES 90312 Class Solids 10/10/2022 07:38 10/10/2022 11:42 4500NORGD-2011 WP MTN 90312 Class Solids 10/10/2022 07:38 10/10/2022 11:42 6010D WP MTN 90314 Class Solids 10/10/2022 07:38 10/10/2022 11:42 90314 Class A Solids 10/10/2022 07:38 10/10/2022 11:42 Saturate Paste WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 22 Waypoi nt.w (l) ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Lab Report Number: 22-263-0009 Date: 10/2112022 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Sample 95726 (Broadwater) Analyte: Calcium QC Batch No: L643695/L642954 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95726 (Broadwater) Analyte: Potassium QC Batch No: L643411/L642954 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95726 (Broadwater) Analyte: Magnesium QC Batch No: L6434111L642954 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95726 (Broadwater) Analyte: Phosphorus QC Batch No: L643411/1-642954 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90312 (Class A) QC Batch No: V25123N24903 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 90361 (1016-10/9 Gypsum Composite) QC Batch No: V251231V24903 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 90361 (10/6-1019 Gypsum Composite) Analyte: Calcium QC Batch No: V25123N24903 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90312 (Class A) Analyte: Copper QC Batch No: V25123N24903 LLC failed high. Result 1 OX concentration. Result not affected. Page 4 of 22 Wayposinto ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 wwwmaypointana lyti cal-com Sample 90361 (1016-10/9 Gypsum Composite) Analyte: Potassium QC Batch No: V24971N24903 Matrix Spike and Post Digestion Spike outside of control limits. Matrix Spike Duplicate and RPD passes. Sample 90361 (10/6-10/9 Gypsum Composite) Analyte: Magnesium QC Batch No: V24971N24903 LLC failed high. Result 1 OX concentration. Result not affected. Sample 90361 (10/6-10/9 Gypsum Composite) Analyte: Lead QC Batch No: V24971N24903 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90361 (10/6-10/9 Gypsum Composite) Analyte: Zinc QC Batch No: V24971IV24903 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Mercury Method 7470A Sample 90311 (Class A) QC Batch No: V251071V25107 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Solids Total Mercury Analysis - CVAA Method 7471B Sample 90312 (Class A) QC Batch No: V24964N24902 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Organochlorine Pesticides by GC (TCLP) Method 8081 B Analyte: Decachlorobiphenyl QC Batch No: L644343 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Semivolatile Organic Compounds - GCIMS (TCLP) Method 8270E Sample 90311 (Class A) Analyte: 2,4,6-Tribromophenol QC Batch No: V25252IV25059 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Sample 90311 (Class A) Analyte: 2-Fluorobiphenyl QC Batch No: V25252N25059 Page 5 of 22 Waypoint.(D ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529,6364 www.waypointanalytical.com Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Sample 90311 (Class A) Analyte: 4-Terphenyl-d14 QC Batch No: V252521V25059 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Analyte: Hexachlorobutadiene QC Batch No: V25252/V25059 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 90311 (Class A) Analyte: Nitrobenzene-d5 QC Batch No: V25252N25059 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. SAR = [Na] 1 SQRT { ( [Ca] + [Mg] )12 } SAR = [4.571 / SQRT { ( [7.58] + [3.65] )12 } SAR = [4.5711 SQRT { 5.615) SAR = [4.57] 12.371 SAR =1.93 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN —Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * 60880 + 0.5 * 2021.04 PAN =18264 + 1010.52 PAN=19274.52 (19300) Page 6 of 22 Waypoint 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6164 ANALYTICAL WWW.Waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 10/25/2022 369 Johnson Dairy Rd. Information : Received : 10/10/2022 Mooreseville , NC 28115 Terri W Cole Report Number :22-283-0009 REPORTOFANALYSIS Laboratory Project Manager Lab No: 90311 Matrix: Sludge Sample ID : Class A Sampled: 10/10/2022 7:38 Test Results Units MQL DF Date I Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 10/10/22 16:33 LMZ SW-1311 TCLP Metals Extraction Leachate 1 10/10/22 16:33 LMZ SW-1311 TCLP Pesticide Extraction Leachate 1 10/10/22 16:33 LMZ SW- 1311 TCLP SVOC Extraction Leachate 1 10/10/22 16:33 LMZ SW- 1311 TCLP VOC ZHE Extraction Leachate 1 10/10/22 14:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): V24955 10/11/22 12:20 Prep Method: SW-3010A Test Results Units MOIL DF Date I Time By Analytical Analyzed Batch TCLP Arsenic <0.050 mg/L 0.050 1 10/11/22 16:05 EDV V24990 TCLP Barium <0.050 m9/L 0.050 1 10/11/22 16:05 EDV V24990 TCLP Cadmium <0.0150 mg/L 0.0150 1 10/11/22 16:05 EDV V24990 TCLP Chromium <0.025 mg/L 0.025 1 10/11/22 16:05 EDV V24990 TCLP Lead <0.030 mg/L 0.030 1 10/11/22 16:05 EDV V24990 TCLP Selenium <0.100 mg/L 0.100 1 10/11/22 16:05 EDV V24990 TCLP Silver <0.025 mg/L 0.025 1 10/11/22 16:05 EDV V24990 Qualifiers/ Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 7 of 22 • • Waypoint, 449 Springbroak Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waVpointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 10/25/2022 369 3ohnson Dairy Rd. Information: Received : 10/10/202.2 Mooreseville , NC 28115 6MLOPIP Terri W Cole Report Number :22-283-0009 REPORT OFANAL YSIS Laboratory Project Manager Lab No : 90311 Matrix: Sludge Sample ID : Class A Sampled: 10/10/2022 7:38 Analytical Method: 7470A Prep Batch(es): V25107 10/14/22 11:40 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0008 mg/L 0.0008 1 10/14/22 17:27 EDV V25178 Analytical Method: 8081E Prep Satch(es): L644114 10/19/22 13:53 Prep Method: 3510C Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Endrin <0.001600 mg/L 0.001600 10 10/20/22 03:32 VIC L644343 TCLP gamma-BHC <0.001600 mg/L 0.001600 10 10/20/22 03:32 VIC L644343 TCLP Methoxychlor <0.001600 mg/L 0.001600 10 10/20/22 03:32 VIC L644343 TCLP Toxaphene <0.01200 mg/L 0.01200 10 10/20/22 03:32 VIC L644343 TCLP Chlordane <0.008000 mg/L 0.008000 10 10/20/22 03:32 VIC L644343 TCLP Heptachlor Epoxide <0.001600 mg/L 0.001600 10 10/20/22 03:32 VIC LW343 TCLP Heptachlor <0.001600 mg/L 0.001600 10 10/20/22 03:32 VIC L644343 Surrogate: Decachlorobiphenyl 51.42 Limits: 36-116% 10 10/20/22 03:32 L644343 Surrogate: Tetrachloro-m-xylene 46.42 Limits: 25-123% 10 10/20/22 03:32 L644343 Analytical Method: 8151A Prep Batch(es): L644185 10/19/22 17:33 Prep Method: 8151A Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 10/21/22 00:57 VIC LW616 TCLP 2,4,5 TP (Silvex) <0.0020 mg/L 0.0020 1 10/21/22 00:57 VIC L644616 Surrogate: DCAA 75.80 Limits: 20-120% 1 10/21/22 00:57 L644616 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation limit Page 8 of 22 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Report Number :22-283-0009 REPORT OFANALYSTS Lab No : 90311 Sample ID : Class A Report Date : 10/25/2022 Received : 10/10/2022 60LO '- . P Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 10/10/2022 7:38 Analytical Method: 8260D Prep Method: 5030B Test Results Prep Batch(es): Units V25007 10/11/22 14:00 MQL DF Date I Time Analyzed By Analytical Batch TCLP Benzene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 10/11/22 17:53 MSA V25008 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Chloroform <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Methyl Ethyl Ketone (MEK) 0.0909 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Tetrachioroethene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 10/11/22 17:53 MSA V25008 Surrogate:4-Bromofluorobenzene 99.0 Limits:80-124% 10 10/11/22 17:53 MSA V25008 Surrogate: Dibromofluoromethane 102 Limits: 75-129% 10 10/11/22 17:53 MSA V25008 Surrogate: Toluene-d8 98.4 Limits: 77-123% 10 10/11/22 17:53 MSA V25008 Analytical Method: 8270E Prep Batch(es): V25059 10/13/22 08:45 Prep Method: 3510C Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP 3&4 Methylphenol <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP 2,4-Dinitrotoluene <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP Hexachlorobenzene <0.100 mg/L 0.100 1 10/17/22 00:37 JMV V25252 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 9 of 22 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 22-283-0009 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lytica l.com REPORT OFAIVAIYSIS Report Date: 10/25/2022 Received : 10/10/2022 Terri W Cole Laboratory Project Manager Lab No: 90311 Matrix: Sludge Sample ID : Class A Sampled: 10/10/2022 7:38 Analytical Method: 8270E Prep Batch(es): V25059 10/13/22 08:45 Prep Method: 3510C Test Results Units MOL DF Date 1 Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.100 mg/L 0.100 1 10/17/22 00:37 JMV V25252 TCLP Hexachloroethane <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP Nitrobenzene <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP Pentachlorophenol <0.250 mg/L 0.250 1 10/17/22 00:37 JMV V25252 TCLP Pyridine <0.050 mg/L 0.050 1 10/17/22 00:37 JMV V25252 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 1 10/17/22 00:37 JMV V25252 TCLP 2,4,6 Trichlorophenol <0.100 mg/L 0.100 1 10/17/22 00:37 JMV V25252 Surrogate: TCLP Phenol-d5 14.8 Limits: 11-100% 1 10/17/22 00:37 JMV 8270E Surrogate: TCLP 2,4,6 Tribromophenol 34.4 * Limits: 43-140% 1 10/17/22 00:37 JMV V25252 Surrogate: TCLP 2-Fluorobiphenyl 23.6 * Limits: 44-11913/o 1 10/17/22 00:37 JMV V25252 Surrogate: TCLP 2-Fluorophenol 20.6 Limits: 20-119% 1 10/17/22 00:37 JMV V25252 Surrogate: TCLP 4-Terphenyl-d14 40.0 * Limits: 44-120% 1 10/17/22 00:37 JMV V25252 Surrogate: TCLP Nitrobenzene-d5 22.4 * Limits: 44-120% 1 10/17/22 00:37 JMV V25252 Qualifiers/ Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 10 of 22 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information ; Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Report Number :22-283-0009 REPORT OFANALY.SIS Lab No: 90312 Sample ID : Class A Report Date : 10/25/2022 Received ; 10/10/2022 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 10/10/2022 7:38 Test Results Units MQL DF Date I Time Analyzed By Analytical Method Fecal Coliform MPN/g 13.5 MPN/g - dry 2.0 1 10/10/22 12:49 SMW 9221E-2011 Plant Available Nitrogen 19300 mg/Kg - dry 1.04 1 10/17/22 15:39 CALCULATION Moisture 4.04 % 1 10114/2211:34 AMB SW-DRYWf Ammonia Nitrogen 2020 mg/Kg AR 1 350.1 Nitrate+Nitrite-N <1.04 mg/Kg - dry 1.04 1 10/20/22 12:09 9056A PH 6.04 s.u. 1 10/13/2213:20 CLB 9045D Total Solids 94.7 % 0.010 1 10/17/22 10:14 AMB 254OG-2011 Total Kjeldahl Nitrogen 62900 mg/Kg - dry 2640 10 10/17/22 15:39 ANH 4500NORGD-2011 Phosphorus 15900 mg/Kg - dry 26A 5 10/18/22 02:28 EAL 6010D Aluminum 13700 mg/Kg - dry 26.1 5 10/19/22 14:10 MMR 6010D Arsenic <2.61 mg/Kg - dry 2.61 5 10/13/22 20:51 EDV 6010D Cadmium 0.729 mg/Kg - dry 0.521 5 10/19/22 14:10 MMR 6010D Calcium 16400 mg/Kg - dry 26.1 5 10/13/22 20:51 EDV 6010D Copper 237 mg/Kg - dry 1.30 5 10/13/22 20:51 EDV 6010D Lead 11.2 mg/Kg - dry 1.56 5 10/13/22 20:51 EDV 6010D Magnesium 2330 mg/Kg - dry 26.1 5 10/13/22 20:51 EDV 6010D Mercury (Total) 0.530 mg/Kg - dry 0.156 5 10/11/22 13:16 EDV 7471B Molybdenum 15.3 mg/Kg - dry 2.61 5 10/13/22 20:51 EDV 6010D Nickel 14.2 mg/Kg - dry 1.30 5 10/13/22 20:51 EDV 6010D Potassium 2820 mg/Kg - dry 130 5 10/13/22 20:51 EDV 6010D Selenium 4.43 mg/Kg - dry 2.61 5 10/19/22 14:10 MMR 6010D Sodium SIB mg/Kg - dry 261 5 10/19/22 14:10 MMR 6010D Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 11 of 22 Waypoint 0 449 Spring6rook Rd, Charlotte, NC 28217 Main 704.529.6964 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date ; 10/25/2022 369 Johnson Dairy Rd. Information : Received : 10/10/2022 Mooreseville , NC 28115 60 LO e 'P Terri W Cole Report Number :22-283-0009 REPORT OFANAL YSTS Laboratory Project Manager Lab No : 90312 Matrix: Solids Sample ID : Class Sampled: 10/10/2022 7:38 Test Results Units MQL Di= Date / Time By Analytical Analyzed Method Zinc 646 mg/Kg - dry 2.61 5 10/13/22 20:51 EDV 6010D Qualifiers/ * Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 12 of 22 { Waypoint, 449 Springbroolc Rd, Charlotte, NC 2$217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 10/25/2022 369 Johnson Dairy Rd. Information : Received : 10/10/2022 Mooreseville , NC 28115 l Terri W Cole Report Number : 22-283-0009 REPORTOFANAL.YSIS Laboratory Project Manager Lab No : 90314 Matrix: Solids Sample ID : Class A Sampled: 10/10/2022 7:38 Test Results Units MQL DF Date 1 Time By Analytical Analyzed Method Calcium (saturated paste) 7.58 meq/L 0.005 1 10/19/22 16:38 JCG Saturate Paste Magnesium (saturated paste) 3.65 meq/L 0.008 1 10/19/22 16:38 JCG Saturate Paste Sodium (saturated paste) 4.57 meq/L 0.004 1 10/19/22 16:38 JCG Saturate Paste Sodium Absorption Ratio 1.93 1 10/19/22 16:38 JCG Saturate Paste Moisture 4.09 014 1 10/14/2211:34 AMB SW-DRYWT Qualifiers/ * Outside QC Limit Definitions DF Dilution Factor Page 13 of 22 t4ceACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical, LLC (Charlotte) 449 Springbrook Road Charlotte NC 28217 ATTENTION Terri W Cole PROJECT ID 22-283-0009 LABORATORY REPORT NUMBER 2210963 DATE October 18, 2022 Primary Data Review By Secondary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: Ashley Amick Project Manager, Access Analytical aamick@axs-inc.com Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified tab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 14 of 22 Page 1 of 6 l IS) - t N \ % � k�t"E � ƒ . 2 ■ .. .. m . CL eLq , z f u 2 E ■ r . h %Ln im %CL : S. � =:f .� 6 \ cn N §. U6 � � � � ��. ■ . u J . / e in . Ln d in ■ . . ■�o 0 0Im k 2 2 ug « _ � � J 2 o c. / k k « o x § z . .� k� k � � � % k EL �E ® E E m j \ Analytical Environmental Services, Inc Date: 18-oct-22 Client: Waypoint Analytical, LLC (Charlotte) Client Sample ID: 90312 Lab Order 2210963 Tag Number: Class A Project Name: 22-283-0009 Collection Date: 10/10/2022 7:38:00 AM Lab ID: 2210963-OOIA Matrix: Soil Analyses Result Qual MDL Reporting Units BatchlD DF Date Analyzed Analyst Limit Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 2020 48.9 99.2 mg/Kg-dry 344754 10 10/18/2022 16:05 TL PERCENT MOISTURE D2216 Percent Moisture 3.02 0 0 Wt% R498617 1 10/12/202200:00 JW Qualifiers: " Value exceeds maximum contaminant level E Estimated value above quantitation range BRL Not Detected at MDL S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded > Ctteater than Result value N Analyte not NELAC certified J Estimated value detected below Repordug Limit B Analyte detected in the associated method blank < Less than Result value Page 16 of 22 Page 3 of 6 W W m O. I 3 i I 4 W-9 CY ly IV IW e IL IL A A ev a a U lu :I Is E i I LIE] ❑ ❑❑ u o e o �u ❑ ❑ ❑ E E G G IIf � r 0 0 •� M1 M1. a � M1• � ���ujj5 �1 E C G_ c E ° e g N E e E e E ��pp %� u1 �p 4 m N 4 N 0 9 N N e I i A s i0 ai 0 a o a o a a Ch �c o Z co Z IL M N N 0 N N o N N c N N \ e C X a � E Cr 0 0 R O C id 0 0 �3 0 0 ao � Q v d Q W¢ m x qz a nn� ooQ ear L titQ q � Qa � oa A GQ as r�.71 C��77 e N v 4i O F co U k °o N O O p' O P O Ri J W T FL kn c in trl v^�i G*� fz] W e Y w 7 d 7 0 R p > M .o > > M z z z z o o e ca e U A m "" y P'r-� W '� aNi fii ON T N G Z n Z Z C Z a E c N [�I D +D A c� v En� L 00 ,n D U D p N O .a N y F N y n rd ^ a °' a Z Z End of Report Page 19 of 22 Page 6 of 6 Waypoint(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanaiytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 22-283-0009 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IRT-15 1.6C . Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received 1 ' Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler ternperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr) 7- High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: 0 Yes 0 No Signature: ngelo Norvell Date & Time: 10/10/2022 11:46:09 Page 20 of 22 m W D D 'O m O Dr C_- G w cy m� rn s m 4 . r ,, o o n i m A a m� 3 ern- a'. c D. � u? m - -a - @ rF Vs i° Nm o '.n 3 ..7 4 -D m m I11 n La y� v O $ pZj m7 n ID c i m a 6 of Z fl' -rlPi � ,D It�. pma D �Qm o^ EI q i3 ci d h .q t H d s D C ' tm agot on m m .rE C Z r y 0 h a C3mCx .�..r It � n '� CR.�.S5iiII �,vmN. k you p • IN -��a In L Z� G1 w 7 zC wo ' i ns a p D M.6 rc. ;'i a X i � r a 4 m �{ G o m to r m� r In p N m M� . fJ FA 0. s z �= m trt b uo n7v ° e� a a O. co m x N m ra mw ui... m a o z m A e m O rEI y Z z a m v m 6 � Z r% m `ra �� rb a w �5 7 n R A EL z.° °'" '" -41 rn m 6 o p z "^gym }� ID rn ° n `t m pc Li 0'0 m U G 11 O o� i a _� y m p om= f m[ D u � 40.5— H G R yn o zCl C 3mz L i a a4�N~� az mom w °arw =i CD ri 0 w W 3� NmN v ��yam o s O m iii tli ... o �m 11r N> q -. x fl.. _ 9 00 { � w C' y IC'� ��. myro U A 'n di m 7 I ` iQED C= Q zi nZ R' 9 PLO R/ v c' �m��, T �N V w fn 1' n f'� m C7 N as 'n 7 U ' u L', O a z E7 m l p ro m D C L x G �� c9dot y W T -�M. Oo. w d" Q � K 9 b Z m .noto r -f li z ' m D z z rn . x a - x c o maw n _ .. .D+ 0 Z to m n m a r II� 'D y W - ti oFL It9l I I I 1l N a 3 _� V 0 o �o01 r o z r jf I n ii f n Page 21 of 22 nGLzC 0v y GMT Z N L mi n 4 L O C m n "4 s a 0 L" N m m n p s� m Z.x� o a 0 C L ZI W o m n �m� o �� 7D m L Z Gf 7G 2 A U z 2' .y t� GI m o a M m® r w f1 Q R v T C C d � n m n 10 L o z;d m s ry co Q 4.r v '71 N % r aULO 0 D f" N M v ism ;u 91(AMm x;wv3 co A v m a a 7 3 � w TZMfA D ° a a A y O � 3ii© a M a Om v' m v to�0 �M mar v O m =1 m n m in A(a CL" H v m z O C, D z C3 M tD m 1 m"p� m m Z {nI O f) G z az5oomq._ M pN�y v K ac cn NN m, aMi iA -r A N L D z N _� Z. a N n N on M L m �Nx $ a m fn -kM�� d � 4[ W U n �� N Z a A�arom C m z x O Z O Vi (A 0. . .04 p m M v n e o '• r OF a 3 CL M c a z M 0 Z z M r A A o a � C) = a 0 b sO 3 a A Arr c ■ ZM x ANr °-i ` x m >= :or 3�'p vim-. a o I a m coal a D y p a � �1 SCm m y pz JD� N C C) m n M° m m A 'o n C .. - } ) ra 0 m` Z o s y p � no m v Page 22 of 22 O Z M N DD 3 Q L CL Q N N O N LL cm 0 J L m 2 N N O N a, LL U Cu 0 U O Q fU N7 OD Q CL Q N N O N N LL As 1 � 1 N CIA Ir k— au 7,r t1i._ al Lo y d � V �m CL '.3 ' '. �;','� i�"•. , �a 'j mil' "1:'"C4'd Ln 4 Lq� qr c V Fri pi 0 CU a:Sli O „� LL ��'f•> F' 0 r-I N Cn "i Ln lO l� 00 O1 O c-1 T-4 c-i N r-I m c-i "i c-i Ll1 c•i LO ri fl- a -I 00 r^I Ol 5-i O N ri N N N M N d N Ln N Ili1" N 00 N O1 N O M ri M u O 41 CL N Ln 3 n a N N � W LL a V N ro {Si C I;t f p a C p A ' - `yw �'Zrl '+ L' o• ®� ® 9 g %yy i P Y A v �7 �Iy ryQ W E k>d U •� Do a fll, o r 'a m A in tA in �A a ©` t1 ;Af Sq t4_ J 4 41 LL lo ri N enLfi tD i� 00 Gl a�1 eN-i rm-I e^i L Ni Lc" N 1C4"" N co N O e� n I u Q O Z u O 40 Q a n� 9�a 0 to Ca �77 a N Q r �r�Pep w s7� 'ir4 Ql Q °r ,per 8/ .� V1 .. ` ` �ry !�- 0"' v✓ Q 4410 %��yp all, d V� P C G � m 1 4 . r co j co Q Q ] y a aeA Its Z�� `ice' .J .� ya.. �i ✓ LL cu lD f� 00 O� O r N r-t %-I M �i elD i "I ci W 61 H r-I N N N NNM N N N W rn O r-I htrH N M M Q U N Q Q Z U r i 0 � � a� A ► a � ,® rs i a� •i •°��.�y�® fb Sd �8 NJ ��°� v Q r i E �.l� �U ads � STJ BPI A�Sr 00 V � ¢1 1� 4� a d+ aD V Q � � J t� Yl :.J 4 T en WC -A tYz r ��� P. h a.� �� �* + O b ® �y s 60 Ill. a Cis t� 6 w f� t j� q; c� 1 �3 Q CL MNIpll� R Ir �iT A 0 4 cj ( O4kr tit 4,4 co e 8 � ��f NO �'� Q L _Q O ICA GJ � � � ,BSI � ,pq r .. � Y.J � � �A ay^��' kV W 1 Y - ■. Oj r-1 eN-3 r-q rr-1 rll rrl r l %H rH ON N N N N N NN N M 19,19 u v 0 z 4+ CL N N N O N fU LL On 0 U Cl) n L CL Q V d lv� lr�_134 n ` > a V� x 9 Y Y zate°. �, Qq , �- +N-i CL kol i a 5 tn ID CD r4 CP la 61a, 7 r ¢ !zip 0. lip FE Q E%� 'm m Cl m a rq 00 N o N � Cl) C co LL E s o _ .. sn �11�r % � s j 4 QN y 9 e cc a 40 C to r ,, moo, � a ® r-- r r't JIr. ' au ra N Kf d to to I.,00 O� o N m 'D �t n co n 00 0) o ri N fn SV � N en co t� co I'm o N N N N N M M U A V O i aj to 3 Q Q Q m 2 3 , Y 9 t � Q CL ID r � fn NR a ct E�� �� ���w � � � co � as 0 LA Ln [G ice-+ Ln Q co r in cc��00 X :a,) r-I N. M Ln [G hOot31O N KSLA'D3�00 c-I -Irl e l r-I Gl r-I O N N N N M NN LA l0 h N N coG1 NNen O co u O CL O EA L Q a L m 5 TOWN OF N100RESVILLE CLASS A B OSOLID PELLETS UT AGREEMENT DISTRIBUTED UNDER NC DWQPERMIT # WQ0036723 I. C0N'TKT--1N—F0RM&TLQN THIRD PARTY TOWN OF MOORESVILE INFORMATION INFORMATION Name € vers Larr• flendren Tesrniee Designtj -M-dling address .-151 e.� f RO. Box S? NlooresviJe " 25115 P'lioae Number - 7€1=4-799-4005 End vier - !I. DE CRIPTION "1"his is padle ized raaat rial produced from the beat treat ent of residuals frcra ttaaasaic pal t��ste',V t. Dais product meets the staadards for a Class A biosolid product according to the EPxVs 40 C FR Part 50:3 regulations. II1. RF-STRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agrel anent: 1. If the residla Ls :ire likely to adversely affect a. threatened or endangered species listed Lander section.4 of to Endangered Species act or its designated critical habitat ?. If the appli don causes prolonged nuisance conditions , If the, Land fads to assirr�late the bulk residuals or the ,Ipplication causes the contravention of surface eater or groundwater standards 4, If the land. is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year. flood elevation, unless the bull- residuals are injected ot` incorporated within a 2 - hour prod following a residuals land application event 6. During a measurable prec-ipitadon event (iae. greaser than 0.01 inch per hour), or withia 24 hours following rai f-M event of 0-5 inches or greater m a ` 4--hour period". 1f the wail pi is not maintained at 6.0 or greater, unless suf cient amounts of lime are applied [a achieve a rEnal, sail pal of at least 6.0, or if an agronomist provides information indicating that the pH of the sc-�E, residuals and lime rxsiKuire is suitable for the Specified crop 8, if the land dog not have an established vegctadve cover unless the residuals are UilcorporAted or injected within a 24--hour period folld)wing a residuals landapplication event 9. If the vertical separation be wren the seasofial hig h cvacer table and the depth of residuals application is lies ran one foot 1{i. if the verdc;d sepaxation of bedrock and the depth of residualsapplication is less thaai one foot IL Biological Residuals shall not bestockpiled, for more than 30 days prior to distrilrudon 1-1. The Third Party accepting tlac; residuals shall provide die. Pemiiaee with all rather nutrient applications (ik, organic and/or inorg-i is fcrdlizera} 13. A Copy of this Utilization .Agteernent shall be maintainedl. it the: site when balk residuals are being applied 14. "flue residuals �,11211 he pre -rented frorn entering any public or private water suppll, source (including wells) axed any starface w,atexs (e.g. str�atns, .lade, river, kv"C tlnaicl) 15. Residaaa.ls should, be,Lund applied at ;a ronomic rates �0, 2021 To%vu t)f %lc accsi-ilk 16. 'Subn-Fission of Soil Samples prior to distti autir-,n, of product 1 f 'the Per it;tee� shall not distriboten bulls residuals to any pion t» entity known �� �� applying xesidr�al� craz1t?�r to the condition of the signed Utilization Agreement I . SE'fRA —S Applicable: setbacks in accordance with 15A NCAC 02T .1 l 8rla); V APPLICATION,RAM Application Rates should tior exceed die calculated nitrogen requirements based ou the 'Realistic Field E aecradon for a particular cusp and the predozni.naut sailseries x%rithin thc: application area.. This product has a North. Carolina Fertilizer label of 5% Nittogen — I% Phosphorus -•- 0% porassiuni ratio, but given that it is generamd from aerobically digested .residual bi<asolidy it is assumed that a 30% mineralization rate: (Organic Nitrogm to Plant .Avalable Nitrogen) is used to calculated the Plant Available Nitrogen (PANN)_ 11e PAN listed below- should be used along with rather nutrient application to determine agronomic rates. NUTRIENT RANGES Percent Solids: 94,r3 -'(_ "otal -Nitrogen" �00 lbs Lton 'Nitrate/lit ite Nitrogen, Q - (ffl"l lbs rcD PAN: 1,-401b5�LOMI Total Phospljorus: 20-3�t lbaltou has 2 .AW Total Poo ssiutn: 010 1t�s toil as 1��� La rz He.. re , Town of !l€aortsvillc Dar€ h ppxwdtnatc. Densit:L5 - 20 lbsIft' M ; ChA A v � ThJxd P-.ury (Panted. Name) J--- t.. Third party ESig iat-ure) llate CG; 2021 Town of MoocePHIC