WQ0003035_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0003035
Applicant/Permittee City of Eden
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0003035
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name* City of Eden Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for City of Eden, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Eden NC 2022 Annual Report FINAL.pdf 25.34MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 27, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0003035
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Eden, NC.
If you have any questions or need additional information, please do not hesitate to contact
Melinda Ward at [phone] ext. 130 or Ryan Copeland at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Melinda Ward — City of Eden
Ryan Copeland — Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF EDEN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003035
2022 ANNUAL REPORT

City of Eden, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms & Metals Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00003035 County Rockingham Year 2022
Facility Name (as shown on permit) Mebane Bridge WWTP NPDES No. NCO023841
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 52
Total number of fields utilized for land application during the year: 14
Total amount of dry tons applied during the year for all application sites: 529.19
Total number of acres utilized for land application during the year: 160.70
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit ( including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
II. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Melinda Ward, WWTP Superintendent
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
-2 - i �3
Signature of a ittee Date
02/01/2023
S nature of LaU Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
EDEN, NC
EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
January 2022
504.00
W
85.18
D
77.25
February 2022
480.00
W
81.12
D
73.58
March 2022
204.00
W
34.48
D
31.27
April2022
408.00
W
68.95
D
62.54
May 2022
132.00
W
21.78
D
19.75
June 2022
528.00
W
87.12
D
79.02
August 2022
300.00
W
56.10
D
50.88
December 2022
576.00
W
94.46
D
85.68
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/4/2023 9:00:32 PM
3,132.00 W 529.19 D 479.97

SECTION 2

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Waypointo
ANALYTICAL
1 /28/2022
Synagro Central LLC/ Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 22-020-0001
Project Description: Eden
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/20/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
�aw,'c MC G19"./
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 22-020-0001
Client Project Description: Eden
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
56332
Eden
Solids
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
O1/19/2022
13:32
01/20/2022
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypointo
ANALYTICAL
46452
Synagro Central LLC/ Eden
Project Eden
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 01/28/2022
Received : 01/20/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D.. CPA
Report Number : 22-020-0001 REPORT OFANALYSIS
Agronomist
Lab No : 56332 Matrix: Solids
Sample ID : Eden Sampled: 1/19/2022 13:32
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
83.1
%
0.010
1
01/21/2216:10
FMM
SM-2540G
Sulfur
8930
mg/Kg -
dry
59.2
1
01/26/22 02:23
EAL
6010D
Calcium
8820
mg/Kg -
dry
296
1
01/26/22 02:23
EAL
6010D
Aluminum
48600
mg/Kg -
dry
29.6
1
01/26/22 02:23
EAL
6010D
Manganese
675
mg/Kg -
dry
2.96
1
01/26/22 02:23
EAL
6010D
Organic N
43360
mg/Kg -
dry
1479
1
01/27/22 12:07
CALCULATION
Nickel
21.8
mg/Kg -
dry
1.48
1
01/26/22 02:23
EAL
6010D
Lead
44.3
mg/Kg -
dry
1.78
1
01/26/22 02:23
EAL
6010D
Arsenic
7.99
mg/Kg -
dry
2.96
1
01/26/22 02:23
EAL
6010D
Selenium
6.86
mg/Kg -
dry
2.96
1
01/26/22 02:23
EAL
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
16.9
%
0.010
1
01/21/22 16:10
FMM
SM-2540G
Phosphorus
22200
mg/Kg -
dry
29.6
1
01/26/22 02:23
EAL
6010D
Copper
2060
mg/Kg -
dry
2.96
1
01/26/22 02:23
EAL
6010D
Total Kjeldahl Nitrogen
Qualifiers/ DF Dilution Factor
Definitions
47300 mg/Kg - dry 1480 1 01/27/22 12:07 JPJ ;M-4500-NH3C-TKI`
MQL Method Quantitation Limit
Page 3 of 7

Waypointo
ANALYTICAL
46452
Synagro Central LLC/ Eden
Project Eden
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
Report Number : 22-020-0001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 01/28/2022
Received : 01/20/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 56332
Sample ID : Eden
Matrix: Solids
Sampled: 1/19/2022 13:32
Potassium
1840
mg/Kg -
dry
59.2
1
01/26/22 02:23
EAL
6010D
Magnesium
2140
mg/Kg -
dry
29.6
1
01/26/22 02:23
EAL
6010D
Sodium
651
mg/Kg -
dry
148
1
01/26/22 02:23
EAL
6010D
Iron
26700
mg/Kg -
dry
59.2
1
01/26/22 02:23
EAL
6010D
Zinc
1700
mg/Kg -
dry
7.40
1
01/26/22 02:23
EAL
6010D
Ammonia Nitrogen
3920
mg/Kg -
dry
592
1
01/27/22 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<28.1
mg/Kg -
dry
28.1
1
01/25/22 16:36
ZBD
4500NO3F-2011
Cadmium
2.17
mg/Kg -
dry
0.592
1
01/26/22 02:23
EAL
6010D
Chromium
37.8
mg/Kg -
dry
1.48
1
01/26/22 02:23
EAL
6010D
Mercury
0.822
mg/Kg -
dry
0.0828
1
01/24/22 13:59
TJS
SW-7471B
pH
7.1
S.U.
1
01/26/2216:05
DRS
9045D
Molybdenum
11.3
mg/Kg -
dry
1.48
1
01/26/22 02:23
EAL
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Eden
Project: Eden
Lab Report Number: 22-020-0001
Date: 1 /27/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 96710
Analyte: Aluminum
QC Batch No: 1-596317/1-596005
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96710
Analyte: Iron
QC Batch No: 1-596317/1-596005
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96710
Analyte: Manganese
QC Batch No: 1-596317/1-596005
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 56356
Analyte: Mercury
QC Batch No: 1-595981/1-595746
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLC/ Eden
Report Number: 22-020-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 01/20/2022 10:09:28
Page 6 of 7

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Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Eden
Lot Number:XD22053
Date Completed:06/14/2022
NIM�� Mr�
06/14/2022 1:33 PM
Approved and released by:
Project Manager II: Lucas Odom
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XD22053
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as biosolids therefore in order to maintain proper digestion they
were weighed out between 3.0-4.0 grams: XD22053-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The run 1 Nitrate analysis contained an associated LCS that was prepared incorrectly. As such, the LCS
exceeded the low limit. Reanalysis was performed out of hold; however, the associated LOQ exceeded
the low limit and did not recover. Results confirm the original analysis. The in hold analysis is reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: XD22053
Sample Number Sample ID Matrix Date Sampled Date Received
001 EDEN Solid 04/21/20221215 04/22/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:XD22053-001
Description: EDEN Matrix: Solid
Date Sampled:04/21/2022 1215 % Solids: 16.5 04/24/2022 2023
Date Received:04/22/2022
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date
Batch
3 350.1
(Ammonia - N ) 350.1
50
05/12/2022 1922 CMM
41046
1
(Nitrate - N ) 9056A
1
05/12/2022 1640 CAW
41645
1
(Nitrite - N ) 9056A
1
05/12/2022 1640 CAW
41644
1
(Phosphorus) 365.1
100
05/03/2022 1633 DMA
05/03/2022 1154
40174
1
(Soil pH meas) 9045D
1
05/13/2022 2015 KKP
41893
1 351.4
(TKN) 351.2
10
05/03/2022 1856 DMA
05/03/2022 1057
40172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Ammonia - N (gas diffusion)
350.1
13000
300
160
mg/kg
3
Nitrate - N (soluble)
9056A
ND L
3.0
0.61
mg/kg
1
Nitrite - N (soluble)
9056A
ND L
1.2
0.61
mg/kg
1
Phosphorus
7723-14-0 365.1
19000
3000
610
mg/kg
1
Soil pH measured in water @
25 ° C
9045D
5.5
su
1
TKN
351.2
44000
3000
1500
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:XD22053-001
Description: EDEN Matrix: Solid
Date Sampled:04/21/2022 1215 % Solids: 16.5 04/24/2022 2023
Date Received:04/22/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 04/27/2022 0733 JAB2 04/27/2022 0236 39271
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.43 J 0.49 0.12 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:XD22053-001
Description: EDEN Matrix: Solid
Date Sampled:04/21/2022 1215 % Solids: 16.5 04/24/2022 2023
Date Received:04/22/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/29/2022 0952 JMH 04/27/2022 1528 39358
2 3050B 6010D 5 04/29/2022 1858 JMH 04/27/2022 1528 39358
Parameter
CAS
Number
Analytical
Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5
6010D
36000
200
74
mg/kg
2
Arsenic
7440-38-2
6010D
6.6
1.5
0.49
mg/kg
1
Cadmium
7440-43-9
6010D
1.4
0.49
0.12
mg/kg
1
Calcium
7440-70-2
6010D
8800
490
61
mg/kg
1
Chromium
7440-47-3
6010D
36
0.98
0.25
mg/kg
1
Copper
7440-50-8
6010D
1700
4.9
2.2
mg/kg
2
Iron
7439-89-6
6010D
25000
9.8
4.5
mg/kg
1
Lead
7439-92-1
6010D
44
4.9
2.2
mg/kg
2
Magnesium
7439-95-4
6010D
2300
490
61
mg/kg
1
Manganese
7439-96-5
6010D
720
1.5
0.58
mg/kg
1
Molybdenum
7439-98-7
6010D
11
3.9
0.98
mg/kg
1
Nickel
7440-02-0
6010D
20
3.9
1.0
mg/kg
1
Potassium
7440-09-7
6010D
1900
490
61
mg/kg
1
Selenium
7782-49-2
6010D
6.7
2.0
0.80
mg/kg
1
Sodium
7440-23-5
6010D
530
490
61
mg/kg
1
Zinc
7440-66-6
6010D
1200
25
6.1
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive
West Columbia,
SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9
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PACE ANALYTICAL SERVICES, LLC
Sampkes Receipt Checklist (SRC) (MEODIEC,15 Rev'.sed:9/29M20
Is suingAutharity: Face LMV-'JVCDL pate 1 or 1
Sample Receipt Checklist (SRQ
-Cw1•_r IntipLcLcd by/date: TFf 1 M.=2M Lat �' XIC2053
Metric of
Kcipt: Pace I I ICIent 1411 UPs Fvdl Other;00_
Ye�S
No
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HNU
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❑1 wet!Ice ❑Icl'.Rxh- © Dry Ice ❑ Nonc1Y
Method;
vletio:loi�iC0013w;
Yes
No
EN
3, if temperature of any cooler exoeerW 6.0 , was Project hunag r Notili�d?
k1 was Notified hy- phone I omail / Face-ro-face (cu+cle ate)_
Ycs
ND
,/ NA
14, Is tlio cornmeiviat courier's p0c kiTkg slip attached to this form"
d Yus
I . No
S. Wimc proper custody procedum;(rclinipil-dbed/receivegfollowed?
Yes
No
6_ Wwr sump le IN Listed on the COC?
'� es
Na
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7, %--m sumplc IUs listcd on all sample Cnatairiers?
YeSFEN13
8_ Was callc­�tion date &. timo lifted or the C f]C?
Yes
N_ 0
9_ Was oollection d9te & lime l'Sted or. all Samp]v containers'?
Yes,
lea
1p„I3i�l a[i con�ir,L:r label inYormatinn (ID, d8te, tune) agre3 with t1,-2: OOC7
yes
Ti LI
11 _j Wr-xs tests to be perfarmec l inted cm ti,4 0_1C7 —
12,;Did 3115mnplQ�s az- iVQ in tho proper containers tfor tach MSt andfai' in gOW WR7 id[Al
(unitroken. lids on, etc_)?
L3.': Wa, vikg4u{s; mmple volume availa'rle?
Yfia
© ha
Lj NON —
Yes
J Ycs
LTNO1
} 14.I WYro all 6aznples received lail}tirt �4 E$C holding time or48 hau.q whicheVCr comes flmt7
Ycs
Y c s
115.iWalewly
sorinple fcirole one) samples Nor listed ❑n €'O[:7
tCYx VOAand RST4-175 .5ani Ics wQ-e bubbles resent=•" a size' 'W'or 6mLn ill {1]2LL1]GtCr
arw ethe VOA vials? p ' P 1 ( �
ere 4111DRCVmcWVnutrieo- sa_•n Ies received at a pH of < 2?
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'es
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1 $. YLf}y ti ull Cvae ido cam pies mcei vr.d art 8 pH > 12 and sul ride ;um pica received at a
] 9. j1�L'ere Al applicable Nli.VTKNUcyanidG�*nDU625.1.60B.3 (e 0.5ueL) €amp to Fitt: of
res:duaJ chlorine?
client rcmarl mgtLcsts (i.e_ requomn &r.ricnis, MSiMSI) designations, etc—)
oarrectly f>rarl50TjbGd from the {.:C)C into the commer_t seLti0u in [,1M5?
2I_ 4' LILI-L3IrntLmberlis7ed0?l 1h1: container label? Tf yuWc iF
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NA
Yes?0.:were
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. . CGI
L6 Nei
Sampler[ Servstirin (fVtls . be completxd for Any sample(g) ituornet_y preserved or with hcadspacc.)
5ampletsj+NA tiwGte rcccivcd inci mauly prescrvod and -were adjaaccordinl;ly
La s3ntiple y Cdiving with NA j rOLOF6-1c one; H2SO43 %NO3, HCl, NaOTI using STD iq N.{_
Time 4t PIF scrvL nn NA If orc than air prtwrvalive is needed, rlestte nwe in the cQMl:nenlr h-1o;°v
SamPle.(s)
�^ �vcrc received with rubbles>6 inm in diameter'.
WA _ - - wore received with TRC s 0,5 ingJLl (If-� 19 ix u++l and were
dimly in samO; ='Mng wr Lhl $ociurn thiosnlf= wlIli Shealy ID.
Samplesk.
a4just1 J
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l abels applied by. rrrC I bc: +h9 ry+2822
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-220-0006
Client Project Description: Eden
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
58879
Storage Pad
Solids
08/04/2022
08/08/2022
58879
Storage Pad
Solids
08/04/2022
08/08/2022
SM-4500-NH3C
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
9045D
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
4500NO3F-2011
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
6010D
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
SW-7471B
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
SM-4500-NH3C-TKN
WP MTN
58879
Storage Pad
Solids
08/04/2022
08/08/2022
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 1 of 6

Waypointo
ANALYTICAL
46452
Synagro Central LLC/ Eden
Project Eden
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 08/16/2022
Received : 08/08/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D.. CPA
Report Number : 22-220-0006 REPORT OFANALYSIS
Agronomist
Lab No : 58879
Sample ID : Storage Pad
Matrix: Solids
Sampled: 8/4/2022 0:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
81.3
%
0.010
1
08/10/2215:49
FMM
SM-2540G
Sulfur
9140
mg/Kg -
dry
53.5
1
08/11/22 23:46
EAL
6010D
Calcium
9200
mg/Kg -
dry
267
1
08/11/22 23:46
EAL
6010D
Aluminum
39500
mg/Kg -
dry
26.7
1
08/11/22 23:46
EAL
6010D
Manganese
754
mg/Kg -
dry
2.67
1
08/11/22 23:46
EAL
6010D
Organic N
36070
mg/Kg -
dry
1337
1
08/15/22 10:00
CALCULATION
Nickel
20.3
mg/Kg -
dry
1.34
1
08/11/22 23:46
EAL
6010D
Lead
36.4
mg/Kg -
dry
1.60
1
08/11/22 23:46
EAL
6010D
Arsenic
7.49
mg/Kg -
dry
2.67
1
08/11/22 23:46
EAL
6010D
Selenium
5.72
mg/Kg -
dry
2.67
1
08/11/22 23:46
EAL
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
18.7
%
0.010
1
08/10/22 15:49
FMM
SM-2540G
Phosphorus
21000
mg/Kg -
dry
26.7
1
08/11/22 23:46
EAL
6010D
Copper
1960
mg/Kg -
dry
2.67
1
08/11/22 23:46
EAL
6010D
Total Kjeldahl Nitrogen 38700 mg/Kg - dry 1340 1 08/15/22 10:00 JPJ ;M-4500-NH3C-TKI`
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 2 of 6

Waypointo
ANALYTICAL
46452
Synagro Central LLC/ Eden
Project Eden
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
Report Number : 22-220-0006
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 08/16/2022
Received : 08/08/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 58879
Sample ID : Storage Pad
Matrix: Solids
Sampled: 8/4/2022 0:00
Potassium
1620
mg/Kg -
dry
53.5
1
08/11/22 23:46
EAL
6010D
Magnesium
2430
mg/Kg -
dry
26.7
1
08/11/22 23:46
EAL
6010D
Sodium
526
mg/Kg -
dry
134
1
08/11/22 23:46
EAL
6010D
Iron
24500
mg/Kg -
dry
53.5
1
08/11/22 23:46
EAL
6010D
Zinc
1100
mg/Kg -
dry
6.68
1
08/11/22 23:46
EAL
6010D
Ammonia Nitrogen
2590
mg/Kg -
dry
535
1
08/16/22 09:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
62.6
mg/Kg -
dry
25.7
1
08/12/22 15:08
ZBD
4500NO3F-2011
Cadmium
1.26
mg/Kg -
dry
0.535
1
08/11/22 23:46
EAL
6010D
Chromium
34.1
mg/Kg -
dry
1.34
1
08/11/22 23:46
EAL
6010D
Mercury
<0.850
mg/Kg -
dry
0.850
1
08/10/22 11:40
TJS
SW-7471B
pH
6.8
S.U.
1
08/15/2215:07
DRS
9045D
Molybdenum
10.9
mg/Kg -
dry
1.34
1
08/11/22 23:46
EAL
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 6

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Eden
Project: Eden
Lab Report Number: 22-220-0006
Date: 8/16/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 96289 (Stat - Q422)
Analyte: Aluminum
QC Batch No: 1-631773/1-631375
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96289 (Stat - Q422)
Analyte: Arsenic
QC Batch No: 1-631773/1-631375
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96289 (Stat - Q422)
Analyte: Calcium
QC Batch No: 1-631773/1-631375
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96289 (Stat - Q422)
Analyte: Copper
QC Batch No: 1-631773/1-631375
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLC/ Eden
Report Number: 22-220-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 08/08/2022 09:32:18
Page 5 of 6

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Waypointo
ANALYTICAL
10/19/2022
Synagro Central LLC/ Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 22-283-0006
Project Description: Eden WW rP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/10/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
�aw,'c MC G19"./
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-283-0006
Client Project Description: Eden WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
59613
Storage
PAO
Solids
10/05/2022
12:05
10/10/2022
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypointo
ANALYTICAL
46452
Synagro Central LLC/ Eden
Project
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Eden WWTP
Report Number : 22-283-0006 REPORT OFANALYSIS
Lab No : 59613
Sample ID : Storage PAO
Report Date : 10/19/2022
Received : 10/10/2022
0Awl[ Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10/ 5/ 2022 12:05
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
83.6
%
0.010
1
10/11/2215:58
FMM
SM-2540G
Potassium
1850
mg/Kg -
dry
61.0
1
10/14/22 04:28
TJS
6010D
Sulfur
9940
mg/Kg -
dry
61.0
1
10/17/22 23:06
EAL
6010D
Calcium
11000
mg/Kg -
dry
305
1
10/14/22 04:28
TJS
6010D
Magnesium
2550
mg/Kg -
dry
30.5
1
10/14/22 04:28
TJS
6010D
Sodium
582
mg/Kg -
dry
152
1
10/14/22 04:28
TJS
6010D
Iron
30900
mg/Kg -
dry
61.0
1
10/14/22 04:28
TJS
6010D
Aluminum
47900
mg/Kg -
dry
30.5
1
10/14/22 04:28
TJS
6010D
Manganese
890
mg/Kg -
dry
3.05
1
10/14/22 04:28
TJS
6010D
Copper
2230
mg/Kg -
dry
3.05
1
10/14/22 04:28
TJS
6010D
Zinc
1230
mg/Kg -
dry
7.62
1
10/14/22 04:28
TJS
6010D
Cadmium
0.762
mg/Kg -
dry
0.610
1
10/14/22 04:28
TJS
6010D
Chromium
40.7
mg/Kg -
dry
1.52
1
10/14/22 04:28
TJS
6010D
Nickel
23.5
mg/Kg -
dry
1.52
1
10/14/22 04:28
TJS
6010D
Lead
42.1
mg/Kg -
dry
1.83
1
10/14/22 04:28
TJS
6010D
Arsenic
6.95
mg/Kg -
dry
3.05
1
10/14/22 17:23
EAL
6010D
Mercury
<0.890
mg/Kg -
dry
0.890
1
10/13/22 13:00
TJS
SW-7471B
Selenium
7.87
mg/Kg -
dry
3.05
1
10/14/22 17:23
EAL
6010D
Molybdenum
10.7
mg/Kg -
dry
1.52
1
10/14/22 04:28
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

•
0
Waypoint
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46452
Synagro Central LLC/ Eden
Project
Eden WWTP
Mary Brewer
Report Date : 10/19/2022
284 Boger Road
Information :
Received : 10/10/2022
Mocksville , NC 27028
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-283-0006
REPORT OFANALYSIS
Agronomist
Lab No : 59613
Matrix: Solids
Sample ID : Storage PAO
Sampled: 10/5/2022 12:05
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
1590
mg/Kg - dry
610
1 10/18/22 15:20 JPJ SM-4500-NH3C
Nitrate+Nitrite-N
40.7
mg/Kg - dry
30.4
1 10/17/22 15:21 CLP 4500NO3F-2011
Organic N
35300
mg/Kg - dry
1524
1 10/18/22 10:30 CALCULATION
pH
6.7
S.U.
1 10/14/2215:03 SAR 9045D
Total Solids
16.4
%
0.010
1 10/11/22 15:58 FMM SM-2540G
Total Kjeldahl Nitrogen
36900
mg/Kg - dry
1520
1 10/18/22 10:30 JPJ ;M-4500-NH3C-TKI`
Phosphorus
23500
mg/Kg - dry
30.5
1 10/14/22 04:28 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Eden
Project: Eden WWTP
Lab Report Number: 22-283-0006
Date: 10/18/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 94251 (SW Cake)
Analyte: Aluminum
QC Batch No: 1-643164/1-642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Iron
QC Batch No: 1-643299/1-642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Potassium
QC Batch No: 1-643164/1-642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94251 (SW Cake)
Analyte: Sulfur
QC Batch No: 1-643566/1-642701
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLC/ Eden
Report Number: 22-283-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
0 Yes
* No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 10/10/2022 09:31:01
Page 6 of 7

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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
December 30, 2020
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Eden - REVISED
Dear Ryan Copeland:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 20121120
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/18/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 37

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20121120
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 12/30/2020
CLIENT: Synagro
Project: Eden - REVISED
WorkOrder Narrative:
20121120: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20121120-001a TCLP-SVOC-CPEST(808 I B): Possible low bias for Methoxychlor due to poor
recovery in ending CCV. Other ending CCV's, including on confirmation column (R121734) exhibit
similar results. Compound demonstrates adequate sensitivity in RLC.
Analytical Sequence QC Notes:
20121120-001AMS/1\4SD TCLP-SVOC-CPEST(8081B): Possible low bias for Methoxychlor due to
poor recovery in ending CCV. Other ending CCVs, including on confirmation column (R121734)
exhibit similar results. Compound demonstrates adequate sensitivity in RLC.
MB/LCS-46981 TCLP-SVOC-CPEST(8081B): Possible low bias for Methoxychlor due to poor
recovery in ending CCV. Other ending CCVs, including on confirmation column (R121734) exhibit
Revision vI
Page 2 of 37

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 Wo#: 20121120
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 12/30/2020
CLIENT: Synagro
Project: Eden - REVISED
similar results. Compound demonstrates adequate sensitivity in RLC.
REVISED REPORT 12/30/20: Includes QC Summary Report pages for TCLP Herbicices.
Revision vI
Page 3 of 37

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� Wo#: 20121120
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 12/30/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 37

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO ijULES. JNG, Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Eden - REVISED
Lab SampleID Client Sample ID
20121120-001 Eden TCLP
Tag No Date Collected
12/17/2020 9:52:00 AM
Workorder
Sample Summary
WO#: 20121120
30 Dec-20
Date Received Matrix
12/18/2020 10:20:00 AM Sludge
Page 5 of 37

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SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20121120
Date Reported: 12/30/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/17/2020 9:52:00 AM
Lab ID: 20121120-OOIA
Project: Eden - REVISED
Client Sample ID Eden TCLP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00500 mg/L
SW7470A SW7470A Analyst: ERA
1 12/23/2020 4:29:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
12/23/2020 12:19:38 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
12/23/2020 12:19:38 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
12/23/2020 12:19:38 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
12/23/2020 12:19:38 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
12/23/2020 12:19:38 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
12/23/2020 12:19:38 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
12/23/2020 12:19:38 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2
12/22/2020 8:33:00 PM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
12/22/2020 8:33:00 PM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2
12/22/2020 8:33:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
12/22/2020 8:33:00 PM
Cresols, Total
ND
10.0
mg/L
2
12/22/2020 8:33:00 PM
Hexachloro-1,3-butadiene
ND
0.0400
mg/L
2
12/22/2020 8:33:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
12/22/2020 8:33:00 PM
Hexachloroethane
ND
0.200
mg/L
2
12/22/2020 8:33:00 PM
Nitrobenzene
ND
0.200
mg/L
2
12/22/2020 8:33:00 PM
Pentachlorophenol
ND
0.500
mg/L
2
12/22/2020 8:33:00 PM
Pyridine
ND
0.500
mg/L
2
12/22/2020 8:33:00 PM
Surr: 2-Fluorophenol
78.4
10 - 157
%Rec
2
12/22/2020 8:33:00 PM
Surr: Phenol-d6
88.2
10 - 169
%Rec
2
12/22/2020 8:33:00 PM
Surr: Nitrobenzene-d5
80.0
32.1 - 130
%Rec
2
12/22/2020 8:33:00 PM
Surr: 2,4,6-Tribromophenol
95.0
45.4 - 166
%Rec
2
12/22/2020 8:33:00 PM
Surr: 2-Fluorobiphenyl
91.2
35.7 - 130
%Rec
2
12/22/2020 8:33:00 PM
Surr: p-Terphenyl-d14
125
74.7 - 145
%Rec
2
12/22/2020 8:33:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation
exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Revision v1
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 7 of 37

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20121120
Date Reported: 12/30/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/17/2020 9:52:00 AM
Lab ID: 20121120-OOIA
Project: Eden - REVISED
Client Sample ID Eden TCLP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: CSS
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
1
12/22/2020 8:10:00 PM
Toxaphene
ND
0.0500
mg/L
1
12/22/2020 8:10:00 PM
Endrin
ND
0.00250
mg/L
1
12/22/2020 8:10:00 PM
gamma-BHC
ND
0.00250
mg/L
1
12/22/2020 8:10:00 PM
Heptachlor
ND
0.00250
mg/L
1
12/22/2020 8:10:00 PM
Heptachlor epoxide
ND
0.00250
mg/L
1
12/22/2020 8:10:00 PM
Methoxychlor
ND
0.00250
mg/L
1
12/22/2020 8:10:00 PM
Surr: TCMX
68.0
10 - 119
%Rec
1
12/22/2020 8:10:00 PM
Surr: DCB
85.2
10 - 119
%Rec
1
12/22/2020 8:10:00 PM
TCLP HERBICIDES BY EPA 8321B
SW8321A
Analyst: TM
2,4-D
ND
1.00
mg/L
100 12/24/2020 10:42:00 AM
2,4,5-TP
ND
1.00
mg/L
100 12/24/2020 10:42:00 AM
Surr: 2,4-Dichlorophenylacetic aci
107
70 - 130
%Rec
100 12/24/2020 10:42:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
1,2-Dichloroethane
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
MEK
ND
5.00
mg/L
50 12/24/2020 3:28:00 AM
Benzene
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
Carbon tetrachloride
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
Chlorobenzene
ND
2.50
mg/L
50 12/24/2020 3:28:00 AM
Chloroform
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
Tetrachloroethene
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
Trichloroethene
ND
0.250
mg/L
50 12/24/2020 3:28:00 AM
Vinyl chloride
ND
0.100
mg/L
50 12/24/2020 3:28:00 AM
Surr: 4-Bromofluorobenzene
96.7
70 - 130
%Rec
50 12/24/2020 3:28:00 AM
Surr: Di brom ofl uorom ethane
102
70 - 130
%Rec
50 12/24/2020 3:28:00 AM
Surr: Toluene-d8
99.4
70 - 130
%Rec
50 12/24/2020 3:28:00 AM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Revision v1
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 8 of 37

Summit Environmental Technologies, Inc.
SU3310 Win St.
MMIT
Analytical Report
ENVIRONMENTAL TECHNOLOGIE-3, IRC
Cuyahoga Falls, Ohio 44223
(base report)
Arralyt9cal Laboralorfas TEL: (330)
253-8211 FAX.- [phone]
WO#: 20121120
Website: http://www.settek.com
Date Reported: 12/30/2020
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
12/17/2020 9:52:00 AM
Lab ID: 20121120-OOIA
Project: Eden - REVISED
Client Sample ID Eden TCLP
Analyses Result
RL Qual Units
DF Date Analyzed
RCISOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.490 mg/Kg
1 12/21/2020 2:38:00 PM
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095)
SW9095
Analyst: DHC
Free Liquid pass
1 12/24/2020 9:10:00 AM
RCISOLID-W/ IGNITABILITY1030
SW1030
Analyst: CXS
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability nonflammable
mm/sec
1 12/29/2020 3:03:57 PM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: VVK
PH (SW9045D)
pH 7.0
s.u.@20.3C
1 12/22/2020 11:31:06 AM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1 12/21/2020 2:38:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision v1
U Samples with CaleVal < MDL
Page 9 of 37

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
ENOROMMEWAL YECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20121120
Wehsite: http://www.settek.com
30 Dec-20
Client: Synagro
State: NW
Project: Eden - REVISED
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20121120-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Paint Filter Free Liquids Test (SW-846: 9095)
Free Liquid
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
N
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
N
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Key
Key
NC WW SCM A Accredited
NC WW SCM N Not Accredited
Version #2
Page 10 of 37

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20121120
Wehsite: http://www.settek.com
30 Dec-20
Client: Synagro
State: NW
Project: Eden - REVISED
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20121120-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited
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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOQH�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 20121120 RcptNo: 1
Logged by: Christina N. Jager 12/18/2020 10:20:00 AMr'
Completed By: Christina N. Jager 12/18/2020 1:16:17 PMdrx
Reviewed By: Jennifer Woolf 12/18/2020 1:24:30 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition?
Yes
d❑
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present V
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑d
No
❑ NA ❑
Person Notified: IRvan Copeland Date: 1 12/18/2020
By Whom: JJennifer Woolf Via: 0 eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: Istate
Client Instructions: I NC
18. Additional remarks:
NC
project address not included
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.6
Goodl
Not Present
Page 37 of 37

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 01/01/22 To 03/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61s
MPN
CFU/g
Coliform
power per gram of
total solids
1 156
7504
18557
CFU/g
0
4/yr
Grah
9222 D
CFI;
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt.2
(40-day bench)
Option/Alt.3
(30-day bench)
Option/Alt.4
(Spec. 02 uptake) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 8
(Drying — Unstable)
Option/Alt. 9
(Infection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the ppathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward Utilities Manager
Pr arer Name And Tit ( e r print)
i /La-
Signa a of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date

Meritech, Inc.
Environmental Laboratory
„,.. Laboratory Certification No. 165
LL
Contact: Ryan Copeland Page 1Report Date: 1/21/2022
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 1/12/2022
Meritech Work Order # 01122275 Sample: Eden E1 Grab 1/12/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 18.2 % 1/13/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 6,494 col/g dry wt 1/12/22 739 col/g dry wt SM 9222D
Meritech Work Order # 01122276 Sample: Eden E2 Grab 1/12/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
18.7 %
1/13/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
15,508 col/g dry wt
1/12/22
745 col/g dry wt
SM 9222D
Meritech Work Order #
01122277 Sample: Eden E3 Grab
1/12/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
23.6 %
1/13/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,971 cal/g dry wt
1/12/22
130 col/g dry wt
SM 9222D
Meritech Work Order #
01122278 Sample: Eden E4 Grab
1/12/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
17.6 %
1/13/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
11,364 col/g dry wt
1/12/22
130 col/g dry wt
SM 9222D
Meritech Work Order #
01122279 Sample: Eden ES Grab
1/12/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
19.4 %
1/13/22
0-100 %
SM 2540E
Fecal Coliform (Sludge)
18,557 col/g dry wt
1/12/22
716 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
O
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 01122280 Sample: Eden E6 Grab
Parameters Results Analysis Date
% Total Solids 17.8 % 1/13/22
Fecal Coliform (Sludge) 9,142 col/g dry wt 1/12/22
Page 2
Report Date: 1/21/2022
Project: Eden
Date Sample Rcvd: 1/12/2022
1/12/22
Reporting Limit Method
0-100 % SM 2540B
466 col/g dry wt SM 9222D
Meritech Work Order # 01122281 Sample: Eden E7 Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 17.3 % 1/13/22 0-100 %
Fecal Coliform (Sludge) 1,156 col/g dry wt 1/12/22 727 col/g dry wt
1/12/22
Method
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result
Log
6494
3.81
Min 1156
15508
4.19
Max 18557
5971
3.78
Geometric Mean 7504
11,364
4.06
18557
4.27
9142
3.96
1156
3.06
Average
3.88

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
8.49
8.5
8.39
8.2
8.07
7.92
7.84
7.64
7.5
7.34
7.18
6.8
6.6
64
6_3
Mebane Bridge
WQ0003035
1 /27/2022
1 /27/22 1435
M. Tuttle
1 /27/22 1438
M. Tuttle
1.4
11.7
12.9
Slope: 0.15
1 ntercept: 8.7
Correlation Coefficient: 1.00
Dry Solids
iegrees Celsius
iegrees Celsius
Oxygen Uptake Rate: 9.02 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.64 mg Oxygen/hr/g
Average Temperature: 12 degrees Celsius
Temperature Correction Factor: 1.72
Temperature Corrected Specific Oxygen Uptake Rate: 1 .1 1mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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(1/6w) U06AXO panlossid

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 4/01/22 To 06/30/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If a licable to alternative erformed Winss A or Class 131 complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6l
MPN
CFU/g
Coliform
power per gram of
total solids
568
1110
2895
CFU/g
0
4/yr
Grah
9222 D
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt. 3
(30-day bench)
Option/Alt.4
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward, Utilities Manager
P�reparerr Name And Title I(typ or prru l
�C�
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
s
Page 1
Contact: Ryan Copeland Report Date: 5/4/2022
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 4/27/2022
Meritech Work Order # 04272282 Sample: E 1 Grab 4/27/22
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 15.4 % 4/28/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,361 col/g dry wt 4/27/22 130 col/g dry wt SM 9222D
Meritech Work Order # 04272283 Sample: E 2 Grab 4/27/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 15.9 % 4/28/22 0-100 % SM 2540B
Fecal Coliform (Sludge) <572 col/g dry wt 4/27/22 572 col/g dry wt SM 9222D
Meritech Work Order #
04272284 Sample: E 3 Grab
4/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
13.2 % 4/28/22
0-100 %
SM 2540E
Fecal Coliform (Sludge)
<689 col/g dry wt 4/27/22
689 col/g dry wt
SM 9222D
Meritech Work Order #
04272285 Sample: E 4 Grab
4/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
16.0 % 4/28/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<568 col/g dry wt 4/27/22
568 col/g dry wt
SM 9222D
Meritech Work Order # 04272286 Sample: E 5 Grab 4/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 15.5 % 4/28/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,346 col/g dry wt 4/27/22 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
MocksvilIe, NC 27028
Meritech Work Order 4 04272287 Sample: E 6 Grab
Parameters Results Analysis Date
% Total Solids 15.7 % 4/28/22
Fecal Coliform (Sludge) 579 col/g dry wt 4/27/22
Meritech Work Order # 04272288 Sample: E 7 Grab
Parameters Results Analysis Date
% Total Solids 15.7 % 4/28/22
Fecal Coliform (Sludge) 2,895 col/g drywt 4/27/22
Page 2
Report Date: 5/4/2022
Project: Eden
Date Sample Rcvd: 4/27/2022
4/6/22
Reporting Limit Method
0-100 % SM 2540B
130 col/g dry wt SM 9222D
4/6/22
Reporting Limit Method
0-100 % SM 2540B
130 col/gdry wt SM9222D
I hereby certify that have reviewed and approve these data. �Oanc OCAL"
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Lab result
2361
572
689
568
2346
579
2895
Average
Log
3.37
2.76
2.84
2.75
3.37
2.76
3.46
3.05
FECAL DATA SHEET
Min 568
Max 2895
Geometric Mean 1110

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
7.89
7.41
7.13
6.8
6.49
6.15
5.88
5.52
5.22
4.9
4.59
3.69
3.39
3.1
Mebane Bridge
WQ0003035
5/18/2022
5/18/22 1442
M. Tuttle
5/18/22 1443
M. Tuttle
1.3
21.5
21.8
Slope: 0.31
1 ntercept: 7.8
Correlation Coefficient: 1.00
Dry Solids
iegrees Celsius
iegrees Celsius
Oxygen Uptake Rate: 18.84 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.45 mg Oxygen/hr/g
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.91
Temperature Corrected Specific Oxygen Uptake Rate: 1.31 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 002507 1
From
Monitoring Period: 7/1/22 To 09/30/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
11 Y pPl ICHVIC LU HIM IIYILIVC VC1 WE IIICU %.lilt
- H Ul I Rbb Dy CUM ICLC LIIC IUIIUWIIIK IIIUIIILUE 111Y,Until;
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6`h
MPN
CFU/g
Coliform
power per gram of
total solids
CFU
2054
2724
5556
CFU/g
0
4/yr
Grab
9222 D
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying— Stable)
(Drying— Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward, Utilities Manager
Pr arer Name pd Title (type or pri t)
14-5 aQ
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102 (26)
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 8/2/2022
Project: Eden
Date Sample Rcvd: 7/21/2022
Meritech Work Order # 07212250 Sample: E 1 Grab 7/21/22
Parameters Results Analysis Date, Reporting Limit Method
% Total Solids 17.7 % 7/22/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,054 CFU/g dry wt 7/21/22 130 CFU/g dry wt SM 9222D
Meritech Work Order #
07212251 Sample: E 2 Grab
7/21/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
17.7 % 7/22/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
3,082 CFU/g drywt 7/21/22
130 CFU/gdrywt
SM 9222D
Meritech Work Order #
07212252 Sample: E 3 Grab
7/21/22
Parameters
Results Analysis Date
Reporting Limit
Method
% TotaI Solids
18.0 % 7/22/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,556 CFU/g drywt 7/21/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 07212253 Sample: E 4 Grab 7/21/22
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 16.8 % 7/22/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,706 CFU/g dry wt 7/21/22 130 CFU/g dry wt SM 9222D
Meritech Work Order # 07212254 Sample: E 5 Grab 7/21/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 17.7 % 7/22/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,054 CFU/g dry wt 7/21/22 130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
MocksviIle, NC 27028
Page 2
Report Date: 8/2/2022
Project: Eden
Date Sample Rcvd: 7/21/2022
Meritech Work Order #
07212255 Sample: E 6 Grab
7/21/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
17.3 %
7/22/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,102 CFU/g dry wt
7/21/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
07212256 Sample:
E 7 Grab
7/21/22
Parameters
Results
Analysis Date
Reporting Limit
Method
Total Solids
16.8 %
7/22/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,706 CFU/g dry wt
7/21/22
130 CFU/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. WMCxft-b
.Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Lab result
2054
3082
5556
2,706
2054
2102
2706
Average
Log
3.31
3.49
3.74
3.43
3.31
3.32
3.43
3.44
FECAL DATA SHEET
Min 2054
Max 5556
Geometric Mean 2724

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
7.52
7.43
7.39
7.35
7.29
7.23
7.18
7.03
6.99
6.94
6.88
6.79
6.73
6.68
6.65
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Mebane Bridge
WQ0003035
8/15/2022
8/15/22 1315
M Tuttle
8/15/22 1317
M Tuttle
0.5 %Dry Solids
24.3 degrees Celsius
24.5 degrees Celsius
0.06
7.5
1.00
3.60 mg Oxygen/hr
0.72 mg Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate: 0.59 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 10/01/22 To 12/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahla to altarnativa Dorf ....aa ire .tee ♦ ..- di..-- n. -
-.-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61h
MPN
CFU/g
Coliform
power per gram of
total solids
CFU
6952
11949
15205
CFU/g
0
4/yr
Grab
9222 D
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
- Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt. 3
(30-day bench)
Option/Alt. 4
(Spec. 02 uptake) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 8
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward, Utilities Manager
Preparer Name And Title (type_or print) f,
��J� 1-1- 23
Signadure of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 1.65
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 10/13/2022
Project: Eden
Date Sample Rcvd: 10/5/2022
Meritech Work Order #
10OS2250 Sample: E 1 Grab
10/5/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
17.1 % 10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
14,035 CFU/g dry wt 10/5/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
10052251 Sample: E 2 Grab
10/5/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
17.0 % 10/6/22
0-100 %
SM 2540B
Fecal Coliform (SIudge)
11,765 CFU/g dry wt 10/5/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
10052252 Sample: E 3 Grab
10/5/22
Parameters
Results Analysis Date
Reporting limit
Method
% Total Solids
17.3 % 10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
12,139 CFU/g dry wt 10/5/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
10OS2253 Sample: E 4 Grab
10/5/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
17.0 % 10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
6,952 CFU/g drywt 10/5/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
10052254 Sample: E 5 Grab
10/5/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
17.2 % 10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
11,099 CFU/g dry wt 10/5/22
130 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
Page 2
Report Date: 10/13/2022
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 10/5/2022
Meritech Work Order # 10052255
Parameters
Sample: E 6 Grab
Results Analysis Date
10/5/22
Reporting Limit Method
% Total Solids
17.1 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
15,205 CFU/g dry wt
10/5/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 10052256 Sample: E 7 Grab 10/5/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 16.9 % 10/6/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 14,793 CFU/g dry wt 10/5/22 130 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.iY1C�C0�� OLL
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result
Log
14035
4.15
Min 6952
11765
4.07
Max 15205
12139
4.08
Geometric Mean 11949
6,952
3.84
11099
4.05
15205
4.18
14793
4.17
Average
4.08

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
8.42
8.52
8.4
8.2
8.13
7.98
7.83
7.7
7.55
7.42
7.28
M.
Mebane Bridge
WQ0003035
12/13/2022
12-13-22 1430
M. Tuttle
12-13-22 1430
M. Tuttle
1.1
14.5
15
Slope: 0.13
1 ntercept: 8.6
Correlation Coefficient: 1.00
Dry Solids
iegrees Celsius
iegrees Celsius
Oxygen Uptake Rate: 7.88 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.72 mg Oxygen/hr/g
Average Temperature: 15 degrees Celsius
Temperature Correction Factor: 1.40
Temperature Corrected Specific Oxygen Uptake Rate: 1.00 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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SECTION 6

Agricultural Lime Application Log
Year: 2022
Project: EDEN
Field Soil Lime Requirement Tons/Acre Date Applied
(state -county -site -field) pH (from soil analysis) Applied
NC-RC-5-1
5.7
0.0 tons/ac.
NC-RC-5-2
5.7
0.0 tons/ac.
NC-RC-5-11
6.0
0.0 tons/ac.
NC-RC-11-1
6.1
0.0 tons/ac.
NC-RC-1 1-2
6.1
0.0 tons/ac.
NC-RC-1 1-3
6.0
0.0 tons/ac.
NC-RC-1 1-4
5.8
0.0 tons/ac.
NC-RC-26-1 B
5.9
0.0 tons/ac.
NC-RC-26-2A
6.1
0.0 tons/ac.
NC-RC-26-2B
6.1
0.0 tons/ac.
NC-RC-26-3
6.1
0.0 tons/ac.
NC-RC-26-4
5.9
0.0 tons/ac.
NC-RC-26-5
5.9
0.0 tons/ac.
NC-RC-27-1
5.8
0.0 tons/ac.
NC-RC-27-2
5.6
0.0 tons/ac.
* Ag lime will be applied once field and crop conditions are suitable

SECTION 7

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