WQ0001800_2022 Residual Annual Report_20230223 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0001800
Applicant/Permittee Town of Yadkinville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001800
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste. 100, Baltimore, MD 21220
Facility Name* Town of Yadkinville Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for Town of Yadkinville, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Yadkinville NC 2022 Annual Report FINAL.pdf 8.08MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 23, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0001800
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Yadkinville, NC.
If you have any questions or need additional information, please do not hesitate to contact Jacob
Swaim at [phone] or Alex Fox at [phone].
Sincerely,
Devd& skkc"
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Jacob Swaim — Town of Yadkinville
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF YADKINVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001800
2022 ANNUAL REPORT

Town of Yadkinville, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms & Metal Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001800 County Yadkin Year 2022
Facility Name (as shown on permit) Town of Yadkinville WWTP & WTP NPDES No. NCO020338
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 15
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 64.36
Total number of acres utilized for land application during the year: 32.20
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
l . Only residuals approved for this permit were applied to the permitted sites.
x..: 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
It. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
.�,..... am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Jacob Swaim. Director of Public Works
Permittee Name and Title (type or print) Sig r o e it ee Date
4Signature
� _� S — 2/ 1 /2023
of Preparer* Date Sig r of and plier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
YADKINVILLE, NC
YADKINVILLE, NC WWTP LIQUID
MONTH/YEAR
August 2022
TOTAL
YADKINVILLE, NC WTP LIQUID
AMOUNT UNIT
316,200.00 G
316,200.00 G
DRY TONS UNIT DRY METRIC TONS
27.03 D 24.52
27.03 D
24.52
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
April2022
91,000.00
G
10.55
D
9.57
June 2022
150,500.00
G
17.45
D
15.82
July 2022
31,500.00
G
3.65
D
3.31
September 2022
49,000.00
G
5.68
D
5.15
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/2/2023 1:17:54 PM
322,000.00 G 37.33 D
33.86

SECTION 2

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Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Yadkinville
Lot Number:XA28097
Date Completed:02/20/2022
NIM�� Mr�
02/21/2022 3:06 PM
Approved and released by:
Project Manager II: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA28097
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to the matrix, the initial sample amount used for sample -001 and -002 was approximately 3X greater
than the standard procedure. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix for Nitrate and Nitrite analysis:
XA28097-001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

Client:Synagro Laboratory ID:XA28097-001
Description: Yadkinville WWTP Matrix: Solid
Date Sampled:01/26/2022 1000 % Solids: 2.05 02/02/2022 0244
Date Received:01/28/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 02/02/2022 0244 NBW
30433
1 350.1
(Ammonia - N ) 350.1
5 02/10/2022 1848 DRD
31097
2
(Nitrate - N ) 9056A
10 02/17/2022 0820 AAB
32346
1
(Nitrite - N ) 9056A
10 02/10/2022 0252 AAB
31602
1
(Phosphorus) 365.1
25 02/08/2022 1942 DMA
02/08/2022 1151
31041
1
(Soil pH meas) 9045D
1 02/08/2022 0218 NBW
30888
1 351.4
(TKN) 351.2
1 02/08/2022 1603 DMA
02/08/2022 1024
31009
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
2.05
%
1
Ammonia - N (gas diffusion)
350.1
6900
240
130
mg/kg
1
Nitrate - N (soluble)
9056A
200 J
240
49
mg/kg
2
Nitrite - N (soluble)
9056A
ND
98
49
mg/kg
1
Phosphorus
7723-14-0 365.1
28000 S
6100
1200
mg/kg
1
Soil pH measured in water @
20 ° C
9045D
7.1
su
1
TKN
351.2
51000
2400
1200
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 02/01/2022 1029 JAB2
02/01/2022 0255
30167
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
3.5
0.84
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 02/01/2022 1718 KSH2
02/01/2022 0827
30046
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
60000
320
120
mg/kg
1
Arsenic
7440-38-2 6010D
4.6 J
12
4.1
mg/kg
1
Cadmium
7440-43-9 6010D
ND
4.1
1.0
mg/kg
1
Calcium
7440-70-2 6010D
12000
4100
510
mg/kg
1
Chromium
7440-47-3 6010D
59
8.1
2.0
mg/kg
1
Copper
7440-50-8 6010D
420
8.1
3.7
mg/kg
1
Iron
7439-89-6 6010D
24000
81
37
mg/kg
1
Lead
7439-92-1 6010D
35
8.1
3.7
mg/kg
1
Magnesium
7439-95-4 6010D
3300 J
4100
510
mg/kg
1
Manganese
7439-96-5 6010D
3300
12
4.8
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
32
8.1
mg/kg
1
Nickel
7440-02-0 6010D
48
32
8.5
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Client:Synagro Laboratory ID:XA28097-001
Description: Yadkinville WWTP Matrix: Solid
Date Sampled:01/26/2022 1000 % Solids: 2.05 02/02/2022 0244
Date Received:01/28/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 02/01/2022 1718 KSH2
02/01/2022 0827
30046
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
4600
4100
510
mg/kg
1
Selenium
7782-49-2 6010D
7.1 J
16
6.6
mg/kg
1
Sodium
7440-23-5 6010D
4600
4100
510
mg/kg
1
Zinc
7440-66-6 6010D
1900
41
10
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
Sarnples Receipt Cher:klist(SPQ(PA E0018C-15) Ponhad_ 29/2020
CE4r7alytical IssuingAuthorlty: Pecs ENLI- LVCOL Page 1 of t,
Sample Receipt Cheeldist (SRC)
Client.-yY.iioro Cnolcr]us tWb ?dL[tL: Jk[rz' i 0117,r2-)22 LAP;
cans of receipt: Act Clicait 1 11}S SF7edSx Odicr:
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PH Str`p ID: YA Chlorine Sr;ip ID. ^ 'Fasted .3y_ NA
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El Yes ❑ No hrA 3. JPtcmperatvre Of MY coDler uxc:icd�ci 6-LMC, was Prpjeet ll%6naeer-l-Pli ed?
PM waF, t+odfied by. 1 hone ( tmail 1 Fare-m-face (cirolc one).
Yrai No V NA4 4- Is []ic commercial Wurices paekiug slip attached to this f,,rrrn?
Yesi No 5. Were proper ru=dy proadures (reIineuislrotlhr'oeived) FUJlowLer
J Yes ' Na 6. WaQ Nam !e IP% IiMixi on Jie COC7
J Ye; ❑ N01 7. Were sampie 1Ds listed on al 15amplc tontainm's7
d Yes No S. W2K cplld;cjat date & time Jisred on this COC? - -
0 Yes No 9. 'rV:,s collection dale 8t titnt::istel 01 all samaltieanrain-crs?
q- Did all container lab4-1 informal ion ([D. date, Wam) Eq�with rho COC?
J Yes \,Gl 11 , Wr -s: tcsrs to be perFomicd lis[A im the [` '?
Y�-' ❑ Ne 12. 1Xd zJJ samples Arrive in tine proper otmwiners far e�n each nest arWor in ,ad condition
i(wtLrokcn, Iids ori., ewX
0 3'es Na 13- W2z adoquate swrtple volume avallziblr`; '
Yes No l4- Wvrc ill grmples re-!go-ved wli'khi �the holdinp, time or 48 hours, uhic.'www ;,cures fjmt?
;t'cs 5, Were xtty Sampies izanlainers missiuglexceSs (circl€. one) 5-r-kpla5 Nor listed orr coc?
❑ Yes E]Nn ONAlin
lb, For VDA and RSK-175 €ainplt;, were bubble.; present 6mm -n diarr-OZ
my of&c VOA Vials?
yesi Ll No 1V, 17_ Were FiE DRO}nietalslnturitmt sam bm rcceivec at a pH of
Yes 'N. gr NA 19- W all cyanide Numptcs Nceiv�d ar d pH > ]2 Ltd 9Ldr3dc sane pies recxivL!kl At a pH -a 9?
�l'e Na ' 1, 19. Wert all ar,p.�cable l�1Hj [�, cyarid� P},enalf425.IKM,3 1` .SmgfL) samples Fina of
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❑Yes ❑Nv 0NA 20. 1Wixc client remarksh-eq ms [ix.rcquested dilations, MSiMSDdc�,ignations, etc...)
currcctiv transcrih&: from the OCtC ioD flue eotnmoat section :r 1.rm ?
'es J No 121. Was ilia am numIxe Fisted on the conrai,rer labrl? V!,&r, Qu oto +i
Sample Preservation (Mu3Lbc MMphAr.s" for any srttriplcXs) Jncorrmelypreserved or with hcndspace.)
Sarup:c(s) NA wen, rccciarodircomealypreserWed undwcrcadjiesredArcordingly
'n sampie race.ivh-tZ Fitt NA mL of circle One. H2SC 4, HNO3, I•IC 1, NaOH us`ng SR :p XA
Time of irrL-serv.3don fah 1f m-nre that one prc.sc rvu ivc is needarl, please note is the vorr,nienrs below.
Semp s) � _ were received with bubbles?5 Irinr in dianratw.
Snrrrplcs(al "� were received with TRC'> 0.5 m giL (rf 419 is no) and wcrc
djustcci a: cordiugly of sampie renriviag wg1l sodium fijosulfMe {Na3S,00 witty Slicahr :D,
SCE bar do lnbcls appl iml by- J LW'2 Date: OI r � 322
'arrtnen ts;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

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Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Yadkinville
Lot Number:XA28097
Date Completed:02/20/2022
NIM�� Mr�
02/21/2022 3:06 PM
Approved and released by:
Project Manager II: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA28097
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to the matrix, the initial sample amount used for sample -001 and -002 was approximately 3X greater
than the standard procedure. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix for Nitrate and Nitrite analysis:
XA28097-001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

Client: Synagro Laboratory ID: XA28097-002
Description: Yadkinville WTP Matrix: Solid
Date Sampled:01/26/2022 1030 % Solids: 2.78 02/02/2022 0244
Date Received: 01 /28/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 02/02/2022 0244 NBW
30433
1 350.1
(Ammonia - N ) 350.1
1 02/10/2022 1850 DRD
31097
2
(Nitrate - N ) 9056A
1 02/17/2022 0839 AAB
32346
1
(Nitrite - N ) 9056A
1 02/10/2022 0315 AAB
31602
1
(Phosphorus) 365.1
1 02/08/2022 1809 DMA
02/08/2022 1151
31041
1
(Soil pH meas) 9045D
1 02/08/2022 0219 NBW
30888
1 351.4
(TKN) 351.2
1 02/08/2022 1603 DMA
02/08/2022 1024
31009
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
2.78
%
1
Ammonia - N (gas diffusion)
350.1
98
36
19
mg/kg
1
Nitrate - N (soluble)
9056A
46
18
3.6
mg/kg
2
Nitrite - N (soluble)
9056A
5.6 J
7.2
3.6
mg/kg
1
Phosphorus
7723-14-0 365.1
910 S
180
36
mg/kg
1
Soil pH measured in water C)
20.2 ° C
9045D
6.6
su
1
TKN
351.2
5300
1800
900
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 02/01/2022 1032 JAB2
02/01/2022 0255
30167
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
ND
2.9
0.69
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 02/01/2022 1714 KSH2
02/01/2022 0827
30046
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
110000
230
88
mg/kg
1
Arsenic
7440-38-2 6010D
4.3 J
8.8
2.9
mg/kg
1
Cadmium
7440-43-9 6010D
ND
2.9
0.74
mg/kg
1
Calcium
7440-70-2 6010D
920 J
2900
370
mg/kg
1
Chromium
7440-47-3 6010D
15
5.9
1.5
mg/kg
1
Copper
7440-50-8 6010D
21
5.9
2.6
mg/kg
1
Iron
7439-89-6 6010D
14000
59
27
mg/kg
1
Lead
7439-92-1 6010D
35
5.9
2.6
mg/kg
1
Magnesium
7439-95-4 6010D
620 J
2900
370
mg/kg
1
Manganese
7439-96-5 6010D
4300
8.8
3.5
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
23
5.9
mg/kg
1
Nickel
7440-02-0 6010D
7.5 J
23
6.2
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client: Synagro Laboratory ID: XA28097-002
Description: Yadkinville WTP Matrix: Solid
Date Sampled:01/26/2022 1030 % Solids: 2.78 02/02/2022 0244
Date Received: 01 /28/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 02/01/2022 1714 KSH2
02/01/2022 0827
30046
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
610 J
2900
370
mg/kg
1
Selenium
7782-49-2 6010D
7.4 J
12
4.8
mg/kg
1
Sodium
7440-23-5 6010D
460 J
2900
370
mg/kg
1
Zinc
7440-66-6 6010D
74
29
7.3
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
Sarnples Receipt Cher:klist(SPQ(PA E0018C-15) Ponhad_ 29/2020
CE4r7alytical IssuingAuthorlty: Pecs ENVI- LVCOL Page 1 of t,
Sample Receipt Cheeldist (SRC)
Client.-yY.iioro Cnolcr]us tWb ?dt[tL: J11(r2' i 0117,-2-)22 LAP; 6a3�o�x
cans of receipt: Act Clicait 1 11}S SF7edSx Odicr:
Yeti Na 1. Wei custody seals pmant ooNerF
Ll Yes No • KAJ ][ cu€tadp seals wqc e5e�tt,�YerC rh intactand unhr ktaFt)
PH Str`p ID: YA Chlorine Sr;ip ID. ^ 'Fasted .3y_ NA
Dr;gi:nalLzuLjXrUtUreupon receipt(DeTJved(CDrrmk: )trmpvraaireu} nrxeips, NSAP'idSrap-Cupl L-266:
0.9 10.9 cC NA I NA NA f NA oC L'A 1 .1JA a — —
Meth Pomp 'an�lre Blku,k [ inrtFicr#les iRGurr 1D; IR Gun Con�ecdLm FFacwi-. _A"
Meth C-dofcoo.ant, 0Wn I" ff I"Pttcks ❑ Uryic4 LiNcniv.
El Yes ❑ No hrA 3. JPtcmperatvre Of MY cooler uxc:icd�ci 6-LMC, was Prpjeet ll%6naeer-l-Pli ed?
PM waF, t+odfied by. 1 hone ( email 1 Fare-m-face (cirolc one).
Yrai No V NA4 4- Is []ic commercial Wurices paekiug slip attached to tftls f,,rrrn?
Yesi No 5. Were proper ru=dy proadures CreIineuislrotlh,<oeived) FUJlowLer
J Yes ' Na 6. WaQ Nam !e IP% IiMixi on Jie COC7
J Ye; ❑ N01 7. Were sampie 1Ds listed on al 15amplc tontainm's7
d yes No S. W2K cplld;cjat date & time Jisred on this COC? - -
0 Yes No 9. 'rV:,s collection dale 8t titnt::istel 01 all samaltieanrain-crs?
q- Did al I container lab4-1 informal ion (M. date, W a m) Eq� ,M wi tlt the COC?
J Yes \,Gl 11 , Wr -a: tcsrs to be perFomicd lis[A im the [` '?
Y�-' ❑ Ne 12. 1Xd zJJ samples Arrive in tine proper otmwiners far each nest and�n and/or in ,ad condition
i(wtLraikcn, Iids ori., ewX
0 3'es Na 13- W2z adoquate sample volume avall2;blr`; '
Yes No l4- Wvrc ill grmples re-!go-ved wii'khi �the holdinp, time or 48 hours, uhic.'www ;,cures fjmt?
;t'cs 5, Were xtty Sampies izanlainers mis5i13glexoeS5 (circlr- one) 5-r-kpla5 Nor listed orr coc?
❑ Yes E]Nn ONAlin
lb, For VDA and RSK-175 €ainplt;, were bubble.; present 6mm -n diarr-OZ
my of&c VOA Vials?
yesi Ll No 1V, 17_ Were FiE DRO}nietalslnturitmt sam bm rcceivec at a pH of
Yes 'N. gr NA 19- W all cyanide Nam ptcs Ncaived ar d pH > ]2 Ltd 9Ldr3dc sane pies recxivL!kl At a pH -a 9?
�l'e Na ' 1, 19. Wert all ar,p.�cable l�1Hj [�, cyarid� P},enalf425.IKM,3 1` .SmgfL) samples Fina of
residua] ah=ovine?
❑ Yes ❑ Nv 0NA 20, 1Wi.rc client remarksh-eq ms 6x. rcquested dilations, MSiMSD designations, etc...)
currcctiv transcrih&: from the OCtC ioD flue eotnmoat section :r 1.rm ?
'es J No 121. Was ilia am numIxe Fisted on the conrai,rer labrl? V!,&r, Qu oto +i
Sample Preservation (Musrbc camphAr.s" for any srttriplcXs) incorrmelypreserved or with hcndspace.)
Sarup:c(s) NA wen, rccciarodircomealypreserWed undwcrcadjiesredArcordingly
'n sampie race.ivh-tZ Fitt NA mL of circle One. H2SC 4, HNO3, I•IC 1, NaOH us`ng SR :p XA
Time of irrL-serv.3don fah 1f m-nre that one: prc.sc rvu ivc is needarl, please note is the vorr,nienrs below.
Semp s) � _ were received with bubbles?5 Inru in dianratw.
Snrrrplcs(al "� were received with TRC'> 0.5 m giL (rf 419 is no) and wcrc
djustcci a: cordiugly of sampie renriviog wg1l sodium fijosulfMe {Na3S,00 witty Slicahr :D,
SCE bar do lnbcls appl iml by- J LW'2 Date: OI r � �22
'arrtnen ts;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorhn
February 07, 2022
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Yadkinville
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22011806
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/28/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-011-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 011009232020-1, New
Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon 0112O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah 011009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 35

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22011806
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/7/2022
CLIENT: Synagro
Project: Yadkinville
WorkOrder Narrative:
22011806: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
22011806-OOIA TCLP-VOC-MSTR 8260D: CCV exhibited high recoveries for Chloroform and
Tetrachloroethene. Sample is ND for these analytes. Surrogate outside recovery limits. Minimum
method criterion of one surrogate within established recovery limits was met.
22011806-OOIA TCLP-SVOC_8270E: Surrogate outside recovery limits. Minimum method criterion of
one surrogate within established recovery limits was met.
22011806-OOIA MTL-TCLP-7(6010D): Bracketing CCV and LCS-54696 exhibited high recoveries for
Arsenic, Barium, and SIlver. Sample exhibits detection < PQL for these analytes. MB-54696 exhibited
detection for Selenium > 1/2 PQL. Sample exhibits detection < PQL for this analyte.
Analytical Sequence QC Notes:
Original
Page 2 of 35

SUMMIY Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Yadkinville
Case Narrative
wo#: 22011806
Date: 2/7/2022
CCV VOC-MSTR_NPW(8260): CCV exhibited high recoveries for Chloroform and Tetrachloroethene.
Associated samples are ND for these analytes.
LCS TCLP-VOC-MSTR TCLP(8260): Possible high bias for Chloroform and Tetrachloroethene due to
high recoveries in CCV.
MB-54696 Mtl-TCLP-7(6010): MB-54696 exhibited detection for Selenium > 1/2 PQL. Associated
samples exhibit detections < PQL for this analyte.
LCS-54696 Mtl-TCLP-7(6010): LCS-54696 exhibited high recovery for Silver. Samples were re-
prepped/analyzed multiple times.
LCS-54712 TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater than 40%.
Original
Page 3 of 35

�� Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� Wo#: 22011806
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co Date: 2/7/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 35

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRCNMEWAL YECHHOLOGNUS, JNC, Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Yadkinville
Lab SampleID Client Sample ID
22011806-001 Yadkinville WWTP
Tag No Date Collected
1/26/2022 11:00:00 AM
Workorder
Sample Summary
WO#: 22011806
07-Feb-22
Date Received Matrix
1/28/2022 11:30:00 AM Sludge
Page 5 of 35

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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22011806
Date Reported: 2/7/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/26/2022 11:00:00 AM
Lab ID:
22011806-OOIA
Project:
Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Badum(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4, 5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
27.8
Surr: Phenol-d6
38.4
Surr: Nitrobenzene-d5
77.2
Surr: 2,4,6-Tribromophenol
44.4
Surr: 2-Fluorobiphenyl
73.7
Surr: p-Terphenyl-d14
108
SW7470A SW7470A Analyst: KLC
0.00200 mg/L 1 2/4/2022 3:20:00 PM
SW6010 SW301OA Analyst: MSK
0.500
mg/L
1
2/2/2022 11:07:00 AM
5.00
mg/L
1
2/2/2022 11:07:00 AM
0.100
mg/L
1
2/2/2022 11:07:00 AM
0.200
mg/L
1
2/2/2022 11:07:00 AM
0.500
mg/L
1
2/2/2022 11:07:00 AM
0.0500
MB+ mg/L
1
2/2/2022 11:07:00 AM
0.500
QL+ mg/L
1
2/2/2022 11:07:00 AM
SW8270 SW351OC Analyst: SFG
0.200
mg/L
2
2/2/2022 12:31:00 AM
0.500
mg/L
2
2/2/2022 12:31:00 AM
0.500
mg/L
2
2/2/2022 12:31:00 AM
0.100
mg/L
2
2/2/2022 12:31:00 AM
10.0
mg/L
2
2/2/2022 12:31:00 AM
0.0400
mg/L
2
2/2/2022 12:31:00 AM
0.100
mg/L
2
2/2/2022 12:31:00 AM
0.200
mg/L
2
2/2/2022 12:31:00 AM
0.200
mg/L
2
2/2/2022 12:31:00 AM
0.500
mg/L
2
2/2/2022 12:31:00 AM
0.500
mg/L
2
2/2/2022 12:31:00 AM
10 - 157
m %Rec
2
2/2/2022 12:31:00 AM
10 - 169
%Rec
2
2/2/2022 12:31:00 AM
32.1 - 130
%Rec
2
2/2/2022 12:31:00 AM
45.4 - 166
S %Rec
2
2/2/2022 12:31:00 AM
35.7 - 130
%Rec
2
2/2/2022 12:31:00 AM
70 - 145
%Rec
2
2/2/2022 12:31:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 35

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22011806
Date Reported: 2/7/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/26/2022 11:00:00 AM
Lab ID:
22011806-OOIA
Project:
Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
2/3/2022 1:48:00 PM
Toxaphene
ND
0.0500
mg/L
10
2/3/2022 1:48:00 PM
Endrin
ND
0.00500
mg/L
10
2/3/2022 1:48:00 PM
gamma-BHC
ND
0.00500
mg/L
10
2/3/2022 1:48:00 PM
Heptachlor
ND
0.00500
mg/L
10
2/3/2022 1:48:00 PM
Heptachlor epoxide
ND
0.00500
mg/L
10
2/3/2022 1:48:00 PM
Methoxychlor
ND
0.00500
mg/L
10
2/3/2022 1:48:00 PM
Surr: TCMX
75.0
10 - 119
%Rec
10
2/3/2022 1:48:00 PM
Surr: DCB
93.1
10 - 119
%Rec
10
2/3/2022 1:48:00 PM
TCLP HERBICIDES BY EPA 8321 B
SW8321
Analyst: RIS
2,4-D
ND
0.500
mg/L
50
2/2/2022 12:32:00 PM
2,4,5-TP
ND
0.500
mg/L
50
2/2/2022 12:32:00 PM
Surr: 2,4-Dichlorophenylacetic aci
104
70 - 130
%Rec
50
2/2/2022 12:32:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: NAW
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50
2/1/2022 6:20:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50
2/1/2022 6:20:00 PM
MEK
ND
5.00
mg/L
50
2/1/2022 6:20:00 PM
Benzene
ND
0.250
mg/L
50
2/1/2022 6:20:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50
2/1/2022 6:20:00 PM
Chlorobenzene
ND
2.50
mg/L
50
2/1/2022 6:20:00 PM
Chloroform
ND
0.250
QC+ mg/L
50
2/1/2022 6:20:00 PM
Tetrachloroethene
ND
0.250
QC+ mg/L
50
2/1/2022 6:20:00 PM
Trichloroethene
ND
0.250
mg/L
50
2/1/2022 6:20:00 PM
Vinyl chloride
ND
0.100
mg/L
50
2/1/2022 6:20:00 PM
Surr: 4-Bromofluorobenzene
88.2
70 - 130
%Rec
50
2/1/2022 6:20:00 PM
Surr: Di brom ofl uorom ethane
104
70 - 130
%Rec
50
2/1/2022 6:20:00 PM
Surr: Toluene-d8
131
70 - 130
S %Rec
50
2/1/2022 6:20:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to
determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation
exceeds
PL Permit Limit
Original
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 8 of 35

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralories TEL: [phone] FAX.- [phone] WO#: 22011806
Website: http://www.settek.com Date Reported: 2/7/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/26/2022 11:00:00 AM
Lab ID:
22011806-OOIA
Project:
Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.481 mg/Kg
1
1/31/2022 4:58:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: ALT
Ignitability Nonflammable
mm/sec
1
2/4/2022 3:44:39 PM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH 6.5
s.u.@19.6C
1
2/1/2022 12:12:34 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1
1/31/2022 4:58:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 35

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Analv n tes Report
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
22011806
Website: http://www.settek.com
07-Feb-22
Client: Synagro
State: NW
Project: Yadkinville
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22011806-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original #1
Page 10 of 35

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Analv n tes Report
ENVIROMMEWAL YECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
22011806
Website: http://www.settek.com
07-Feb-22
Client: Synagro
State: NW
Project: Yadkinville
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22011806-001A Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Original #1
Page 11 of 35

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Page 34 of 35

�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTAL TECHNOLOQH�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 22011806 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
1/28/2022 11:30:00 AM
1 /30/2022 9:11:27 PM
2/1/2022 3:43:32 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
9. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
The lid was rec'd cracked, lid replaced in receiving
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.1
Goodl
Not Present
Page 35 of 35

TCLP data is not included in the 2022 Annual Report for Yadkinville WTP. A TCLP sample was
taken in 2019 and is only required to be taken once per permit cycle.

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Yadkinville WQ Permit Number: WQ0001800
WWTP Name: Yadkinville WWTP NPDES Number: NCO020338
Monitoring Period: From 0 1/0 1/ 2022 To 12/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1 /A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
it appiicame
Parameter
to anernauve pei iu, 111vu %—
Allowable Level in Sludge
AbJ es VI t .aoo +� ��••• •"" �••" • •• •• ••• --- -••_ -
Pathogen Density
--_ _
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
MPN
239,234
386,089
546,219
MPN/g
0
Annual
Grab
Sm9221C
Coliform
power per gram
E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. I
Option/Alt. 2
Option/Alt.3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/l5A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
ersonnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
teen met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Grant Trivette Plant Manager
Pr p er Name and Title (type or print)
----
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Town of Yadkinville
PO Box 816
Yadkinville, NC 27055
Receive Date: 03/17/2022
Reported: 03/18/2022
For:
Comments: GEOMETRIC MEAN: 386,089 MPN/g
STATESVILLE
ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
220317-14-01
Fecal Coliforms
1
495496
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-01
Percent Solids
1
2.22
%
SM2540B-2011
03/17/2022
MD
220317-14-02
Fecal Coliforms
2
357143
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-02
Percent Solids
2
2.24
%
SM2540B-2011
03/17/2022
MD
220317-14-03
Fecal Coliforms
3
358744
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-03
Percent Solids
3
2.23
%
SM2540B-2011
03/17/2022
MD
220317-14-04
Fecal Coliforms
4
311111
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-04
Percent Solids
4
2.25
%
SM2540B-2011
03/17/2022
MD
220317-14-05
Fecal Coliforms
5
495496
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-05
Percent Solids
5
2.22
%
SM2540B-2011
03/17/2022
MD
220317-14-06
Fecal Coliforms
6
239234
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-06
Percent Solids
6
2.09
%
SM2540B-2011
03/17/2022
MD
220317-14-07
Fecal Coliforms
7
546219
MPN/g
SM92210E-2006
03/17/2022
MD
220317-14-07
Percent Solids
7
2.38
%
SM2540B-2011
03/17/2022
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 220317-14-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220317-14-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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volatilesolids.xls 2/2/06 % TOTAL SOLIDS % VOLATILE SOLIDS
SM 2540 G
Analyzed By: 5A Calculated By:
Date In 103-105 oven: _ Date In 550 furnace:
Time In 103-105 oven: Time In 550 furnace:�ti��
Time Out 103-105 oven: Time Out 550 furnace:
Sam [le ID
INITIAL
RAS
INITIAL
RAS (dup)
Dry wt.
5 4.
Dish wt.
Sample vol.
^01
TS %
076
' � �A J-7i
Dish #
# 2—
Dry wt.
I
Ash M.
D
VS %
Divide VS% by
a C� h_ I
V '
C`w�n
INITIAL
AVERAGE:
G ;`l U 5
Samp[le ID
FINAL
Holding Tankp-
3
FINAL
Holding Tank (dup) 44
Dry wt.
L ago
Dish wt.Sample
vol.
Ts%
°
�,` '3
-a`
Dish #
Dry wt.
' , c
o`
Ash wt.
Vs%
7
Divide VS% by
b U
% volatile
fraction
% volable
fraction
E
GE:
Calculation for TS% and VS%: Dry wt. - Dish wt. X 100
Sample vol.

USE INITIAL AND FINAL AVERAGES OF YOUR % VOLATILE FRACTION TO CALCULATE THE
PERCENT REDUCTION (USE THE VAN KLEECK FORMULA)
Van Kleeck Reduction:
Initial % vol. frac. - Final % vol. frac. X 100 = % reduction
Initial % vol. frac. - (Initial % voi. frac x Final % vol. frac.)
c, minus o C ) x 100 = �;
9 t ) minus 1 �c times ° ce- 6 �(� A
* Do multiplication inside [( )] before you subtract on bottom of equation.
Gy 11�u�5

SECTION 6

Agricultural Lime Application Log
Year: 2022
Project: Yadkinville WWTP
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
YK-08-1 5.7 0.5 T/AC
YK-33-1 6.0 0.0 T/AC
YK-33-2 6.0 1 O.OT/AC
YK-29-2 1 5.9 1 .5T/AC
YK-29-1 1 6.8 1 0.0 1 O.OT/AC
*Lime will be applied when conditions improve.

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