WQ0032618_2022 Residual Annual Report_20230224 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0032618
Applicant/Permittee Ajinomoto Health & Nutrition North America, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Drew Matthews
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2528839301
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0032618
Has Current Existing permit number
Applicant/Permittee Address*
4020 Ajinomoto Drive Raleigh, NC 27610
Facility Name*
Ajinomoto Health & Nutrition North America Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Ajinomoto Annual Report.pdf 5.21 MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
01f1 i �4e*A~
Submission Date 2/24/2023

Ajinomoto Health & Nutrition
North America, Inc.
2022 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS A RESIDUALS PROGRAM
WQ0032618
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
February 24, 2023
SOIL PLUS

SOIL PLUS
February 24, 2023
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2022 LAND APPLICATION ANNUAL REPORT
Ajinomoto Health & Nutrition North America, Inc. DCAR Program
NC Permit No: WQ0032618
Soil Plus Project No. 200902.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for Ajinomoto Health & Nutrition North
America, Inc. (Ajinomoto). Soil Plus compiled this report using data gathered during the
compliance year. This data includes (1) a certification form, (2) distribution & marketing
summary form, & (3) residual sampling summary.
Ajinomoto prepared and land applied approximately 1,143,965 gallons or 415.01 dry tons
of Class A residual biosolids "Cell Cream" during 2022. The residual biosolids were
distributed to farms in Edgecombe and Nash Counties for agricultural uses. Approximately
6,839 wet tons or 990.98 dry tons of residual biosolids produced from Ajinomoto's
Wastewater Treatment System were taken to a private composting facility for further
processing during 2022.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or Ajinomoto (919-723-2155) for further assistance.
Respectfully,
.-R,-e40
Drew Matthews, Soil Plus
cc: Ryan Faw, Ajinomoto
Jason Smith, Granville Farms
PO Box 1396
Oxford, NC 27565
[phone]
dmatthewsgsoilplus. ne t
www.soilplusuc.com

ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Ajinomoto Health
& Nutrition North
America, Inc. CELL CREAM
ANNUAL RESIDUAL
2022 Annual SAMPLING SUMMARY
Class A Residuals FORM
Nutrients
Management 503 Metals
Report
WASTEWATER
WQ00 32618 TREATMENT SYSTEM
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Nutrients
Raleigh, NC 503 Metals
DISTRIBUTION AND
�AQ�d MARKETING SUMMARY
FORM

Ajinomoto Health & Nutrition North America, Inc.
2022 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT
CLASS A RESIDUALS PROGRAM
WQ0032618
Annual Certification Form
Source Summary Form

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0032618 Ajinomoto Health & Nutrition Ryan Faw Wake [phone]
North America, Inc.
Year: 2022
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Yes No
Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how C
the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: NIA
Total number of fields utilized for land application during the year: NIA
Total amount of dry tons applied during the year for all application sites: 415.01
Total number of acres utilizes for land application during the year: NIA
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality �: E
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6. fhe facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 `were complied with (applicable to 40 CFR Part 503 regulated
facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
R w Sie;h IiY4 101', G-e,,&^ / Ra iadver
Permittee Name and Title (type or print):
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Signature of Permittee Date
1 ,4, 1 /31 /2023
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
WWTP Volume Annlied I Total Dry Tons
Ajinomoto Cell Cream 1,143,965 Gallons 415.01
Total 415.01

Ajinomoto Health & Nutrition North America, Inc.
2022 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT
CLASS A RESIDUALS PROGRAM
WQ0032618
Cell Cream Residual Sami2ling SummaLy Form
Field Loading Calculations
Nutrient Analysis

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&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 2/2/2022
Solids 16.9
Mineralization Rate 0.3
Gallons per DT 1,418.98
pH 3.1
Sodium Absorpotion 1.06 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 83,400 lbs./1,000 gal 117.55
Ammonia Nitrogen (mg/Kg) 2,070.00 lbs./1,000 gal 2.92
Nitrate -Nitrite (mg/Kg) 34.40 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 25,468 lbs./1,000 gal 35.90
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 26,503 lbs./1,000 gal 37.36
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20 lbs./1,000 gal
1.62
P205 lbs./1,000 gal
35.50
Calcium lbs./1,000 gal
0.42
Magnesium lbs./1,000 gal
0.16
Manganese lbs./1,000 gal
0.01
Sulfur lbs./1,000 gal
9.01
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
2.96
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.59
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
2.96
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
1.78
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.08
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
1.48
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
2.96
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
7.40
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
83,400
25,468 50.94
57,932
83,400
26,503 53.01
56,897
57,932
8,690 17.38
49,242
56,897
8,534 17.07
48,362
49,242
3,693 7.39
45,549
48,362
3,627 7.25
44,735
45,549
1,708 3.42
43,841
44,735
1,678 3.36
43,057
43,841
822 1.64
43,019
43,057
807 1.61
42,250
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 40,381 80.76
Total 41,150 82.30

Waypointo
ANALYTICAL
46974
Ajinomoto North America Inc.
Project
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ajinomoto North America Inc.
Report Number : 22-034-0006 REPORT OFANALYSIS
Lab No : 56490
Sample ID : Cell Cream
Report Date : 02/14/2022
Received : 02/03/2022
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 2/2/2022 8:15
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
83.1
%
0.010
1
02/08/2217:16
FMM
SM-2540G
Potassium
959
mg/Kg -
dry
59.2
1
02/11/22 02:24
EAL
6010D
Sulfur
6390
mg/Kg -
dry
59.2
1
02/11/22 02:24
EAL
6010D
Calcium
<296
mg/Kg -
dry
296
1
02/11/22 02:24
EAL
6010D
Magnesium
114
mg/Kg -
dry
29.6
1
02/11/22 02:24
EAL
6010D
Sodium
207
mg/Kg -
dry
148
1
02/11/22 02:24
EAL
6010D
Iron
<59.2
mg/Kg -
dry
59.2
1
02/11/22 02:24
EAL
6010D
Aluminum
<29.6
mg/Kg -
dry
29.6
1
02/11/22 02:24
EAL
6010D
Manganese
4.73
mg/Kg -
dry
2.96
1
02/11/22 02:24
EAL
6010D
Copper
<2.96
mg/Kg -
dry
2.96
1
02/11/22 02:24
EAL
6010D
Zinc
<7.40
mg/Kg -
dry
7.40
1
02/11/22 02:24
EAL
6010D
Cadmium
<0.592
mg/Kg -
dry
0.592
1
02/11/22 02:24
EAL
6010D
Chromium
<1.48
mg/Kg -
dry
1.48
1
02/11/22 02:24
EAL
6010D
Nickel
<1.48
mg/Kg -
dry
1.48
1
02/11/22 02:24
EAL
6010D
Lead
<1.78
mg/Kg -
dry
1.78
1
02/11/22 02:24
EAL
6010D
Arsenic
<2.96
mg/Kg -
dry
2.96
1
02/11/22 02:24
EAL
6010D
Mercury
<0.0834
mg/Kg -
dry
0.0834
1
02/09/22 15:36
JW2
SW-7471B
Selenium
<2.96
mg/Kg -
dry
2.96
1
02/11/22 02:24
EAL
6010D
Molybdenum
<1.48
mg/Kg -
dry
1.48
1
02/11/22 02:24
EAL
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 11

•
0
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Ajinomoto North America Inc.
A/P Cindy
Report Date : 02/14/2022
4020 Ajinomoto Dr
Information :
Received : 02/03/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-034-0006
REPORT OFANALYSIS
Agronomist
Lab No : 56490
Matrix: Solids
Sample ID : Cell Cream
Sampled: 2/2/2022 8:15
Test
Results
Units
MQL DF
Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
2070
mg/Kg - dry
592 1
02/10/22 13:45 JPJ SM-4500-NH3C
Nitrate+Nitrite-N
34.4
mg/Kg - dry
28.6 1
02/09/22 15:07 ZBD 4500NO3F-2011
Organic N
81360
mg/Kg - dry
1479 1
02/10/22 09:00 CALCULATION
pH
3.1
S.U.
1
02/10/2213:37 DRS 9045D
Total Solids
16.9
%
0.010 1
02/08/22 17:16 FMM SM-2540G
Total Kjeldahl Nitrogen
83400
mg/Kg - dry
1480 1
02/10/22 09:00 JPJ ;M-4500-NH3C-TKI`
Phosphorus
11000
mg/Kg - dry
29.6 1
02/11/22 02:24 EAL 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 11

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-034-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 02/03/2022 13:49:39
Page 9 of 11

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&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 5/20/2022
Solids 7.48
Mineralization Rate 0.3
Gallons per DT 3,205.99
pH 5.56
Sodium Absorpotion 0.98 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 113,000 lbs./1,000 gal 70.49
Ammonia Nitrogen (mg/Kg) 1,330.00 lbs./1,000 gal 0.83
Nitrate -Nitrite (mg/Kg) 66.80 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 34,233 lbs./1,000 gal 21.36
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 34,898 lbs./1,000 gal 21.77
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20 lbs./1,000 gal
2.30
P205 lbs./1,000 gal
13.44
Calcium lbs./1,000 gal
0.42
Magnesium lbs./1,000 gal
0.08
Manganese lbs./1,000 gal
0.01
Sulfur lbs./1,000 gal
12.98
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
6.67
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.33
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
6.67
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
4.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
2.01
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
3.33
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
6.67
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
16.70
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
113,000
34,233 68.47
78,767
113,000
34,898 69.80
78,102
78,767
11,815 23.63
66,952
78,102
11,715 23.43
66,387
66,952
5,021 10.04
61,931
66,387
4,979 9.96
61,408
61,931
2,322 4.64
59,608
61,408
2,303 4.61
59,105
59,608
1,118 2.24
58,491
59,105
1,108 2.22
57,997
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 54,509 109.02
Total 55,003 110.01

•
0
Waypoint
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Ajinomoto North America
A/P Cindy
Report
Date : 06/03/2022
4020 Ajinomoto Dr
Information :
Received : 05/24/2022
Raleigh , NC 27610
�oau�
�� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-144-0002
REPORT OFANALYSIS
Agronomist
Lab No : 57962
Matrix:
Solids
Sample ID : Hystadene Cell Cream
Sampled:
5/20/2022
0:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
92.5
%
0.010
1
05/25/2216:33
FMM
SM-2540G
Phosphorus
9410
mg/Kg -
dry
66.7
1
05/31/22 22:18
TJS
6010D
Potassium
3070
mg/Kg -
dry
133
1
05/31/22 22:18
TJS
6010D
Calcium
<667
mg/Kg -
dry
667
1
05/31/22 22:18
TJS
6010D
Aluminum
<66.7
mg/Kg -
dry
66.7
1
05/31/22 22:18
TJS
6010D
Manganese
11.1
mg/Kg -
dry
6.67
1
05/31/22 22:18
TJS
6010D
Copper
<6.67
mg/Kg -
dry
6.67
1
05/31/22 22:18
TJS
6010D
Ammonia Nitrogen
<1330
mg/Kg -
dry
1330
1
06/01/22 14:45
JPJ
SM-4500-NH3C
Nickel
<3.33
mg/Kg -
dry
3.33
1
05/31/22 22:18
TJS
6010D
Lead
<4.00
mg/Kg -
dry
4.00
1
05/31/22 22:18
TJS
6010D
Arsenic
<6.67
mg/Kg -
dry
6.67
1
05/31/22 22:18
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Organic N
112700
mg/Kg -
dry
3333
1
06/01/22 10:00
CALCULATION
Total Solids
7.48
%
0.010
1
05/25/22 16:33
FMM
SM-2540G
Cadmium
<1.33
mg/Kg -
dry
1.33
1
05/31/22 22:18
TJS
6010D
Chromium
<3.33
mg/Kg -
dry
3.33
1
05/31/22 22:18
TJS
6010D
Iron
<133
mg/Kg -
dry
133
1
05/31/22 22:18
TJS
6010D
Magnesium
122
mg/Kg -
dry
66.7
1
05/31/22 22:18
TJS
6010D
Mercury
<2.01
mg/Kg -
dry
2.01
1
06/02/22 11:27
JTR
SW-7471B
Qualifiers/
DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 11

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46974
Ajinomoto North America Inc. Project Ajinomoto North America
A/P Cindy
Report Date : 06/03/2022
4020 Ajinomoto Dr
Information
:
Received : 05/24/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-144-0002
REPORT OFANALYSIS
Agronomist
Lab No : 57962
Matrix:
Solids
Sample ID : Hystadene Cell Cream
Sampled:
5/20/2022 0:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Selenium
<6.67
mg/Kg
- dry
6.67
1
05/31/22 22:18
TJS 6010D
Sulfur
20800
mg/Kg
- dry
133
1
05/31/22 22:18
TJS 6010D
Total Kjeldahl Nitrogen
113000
mg/Kg
- dry
3330
1
06/01/22 10:00
JPJ ;M-4500-NH3C-TKI`
Sodium
383
mg/Kg
- dry
333
1
05/31/22 22:18
TJS 6010D
Zinc
<16.7
mg/Kg
- dry
16.7
1
05/31/22 22:18
TJS 6010D
Nitrate+Nitrite-N
66.8
mg/Kg
- dry
64.9
1
05/27/22 11:03
ZBD 4500NO3F-2011
Molybdenum
<3.33
mg/Kg
- dry
3.33
1
05/31/22 22:18
TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 11

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-144-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 05/24/2022 12:24:23
Page 10 of 11

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Ajinomoto North America
4020 Ajinomoto Dr.
Raleigh, NC 27610
Product: Cell Cream
TKN
NH3
Soilds
Pan (Surface)
PAN (Inj. / Inco
dJJINOMOTO
HIS
15,988 ppm
616 ppm
8.42% % dry
53.85 Ibs / 1000 g
56.42 Ibs / 1000 g
N'sQ—\e cell U?km �A - `J.5%
< JJ"j)' e0 - 1.yZ
Application Information:
Application of this residual other than the recommended rates as related to the values on this specification sheet are prohibited.
* Application must be in accordance with the permit held by the user.
* These residuals are not to be applied to land that is flooded, frozen or snow covered.
* Adequate procedures shall be provided to prevent surface runoff from carrying any residuals into
surface waters.
* The minumum setbacks must be adhered to:
Private or public water sources
100 feet
Surface waters (Streams, Intermittent and perennial, waterbodies and wetlands)
100 feet
Surface water diversions (Ephemeral streams, waterways, ditches)
25 feet
Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT)
25 feet
Wells with exception of monitoring wells.
100 feet
Bedrock outcrops
25 feet
Signed
Date 5/20/2022

&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 8/31/2022
Solids 7.6
Mineralization Rate 0.3
Gallons per DT 3,155.37
pH 3.04
Sodium Absorpotion 1.22 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 108,000 lbs./1,000 gal 68.45
Ammonia Nitrogen (mg/Kg) 2,570.00 lbs./1,000 gal 1.63
Nitrate -Nitrite (mg/Kg) 78.60 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 32,993 lbs./1,000 gal 20.91
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 34,278 lbs./1,000 gal 21.73
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20 lbs./1,000 gal
1.00
P205 lbs./1,000 gal
11.67
Calcium lbs./1,000 gal
0.42
Magnesium lbs./1,000 gal
0.12
Manganese lbs./1,000 gal
0.02
Sulfur lbs./1,000 gal
8.81
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
6.58
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.32
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
6.58
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
3.95
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
2.01
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
3.29
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
6.58
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
16.40
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
108,000
32,993
65.99
75,007
108,000
34,278 68.56
73,722
75,007
11,251
22.50
63,756
73,722
11,058 22.12
62,664
63,756
4,782
9.56
58,975
62,664
4,700 9.40
57,964
58,975
2,212
4.42
56,763
57,964
2,174 4.35
55,791
56,763
1,064
2.13
55,699
55,791
1,046 2.09
54,745
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 52,301 104.60
Total 53,255 106.51

Waypointo
ANALYTICAL
46974
Ajinomoto North America Inc.
Project Sludges
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 22-249-0003 REPORT OFANALYSIS
Lab No : 59270
Sample ID : Ser Cell Cream
Report Date : 09/14/2022
Received : 09/06/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/31/2022 13:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
92.4
%
0.010
Phosphorus
8040
mg/Kg -
dry
65.8
Potassium
1310
mg/Kg -
dry
132
Calcium
<658
mg/Kg -
dry
658
Aluminum
<65.8
mg/Kg -
dry
65.8
Manganese
38.7
mg/Kg -
dry
6.58
Copper
<6.58
mg/Kg -
dry
6.58
Ammonia Nitrogen
2570
mg/Kg -
dry
1320
Nickel
<3.29
mg/Kg -
dry
3.29
Lead
<3.95
mg/Kg -
dry
3.95
Arsenic
<6.58
mg/Kg -
dry
6.58
Test
Results
Units
MQL
1 09/07/2215:40 FMM SM-2540G
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/13/22
13:50
JPJ
SM-4500-NH3C
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
1
09/09/22
18:38
TJS
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
Organic N
105600
mg/Kg -
dry
3289
1
09/13/22 09:50
CALCULATION
Total Solids
7.60
%
0.010
1
09/07/22 15:40
FMM
SM-2540G
Cadmium
<1.32
mg/Kg -
dry
1.32
1
09/09/22 18:38
TJS
6010D
Chromium
<3.29
mg/Kg -
dry
3.29
1
09/09/22 18:38
TJS
6010D
Iron
183
mg/Kg -
dry
132
1
09/09/22 18:38
TJS
6010D
Magnesium
184
mg/Kg -
dry
65.8
1
09/09/22 18:38
TJS
6010D
Mercury
<2.01
mg/Kg -
dry
2.01
1
09/12/22 11:09
TJS
SW-7471B
Qualifiers/
DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 12

•
0
Waypoint
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Sludges
A/P Cindy
Report Date : 09/14/2022
4020 Ajinomoto Dr
Information :
Received : 09/06/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-249-0003
REPORT OFANALYSIS
Agronomist
Lab No : 59270
Matrix: Solids
Sample ID : Ser Cell Cream
Sampled: 8/31/2022 13:00
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Selenium
<6.58
mg/Kg
- dry
6.58
1 09/09/22 18:38 TJS 6010D
Sulfur
13900
mg/Kg
- dry
132
1 09/09/22 18:38 TJS 6010D
Total Kjeldahl Nitrogen 108000
mg/Kg
- dry
3290
1 09/13/22 09:50 JPJ ;M-4500-NH3C-TKI`
Sodium
501
mg/Kg
- dry
329
1 09/09/22 18:38 TJS 6010D
Zinc
<16.4
mg/Kg
- dry
16.4
1 09/09/22 18:38 TJS 6010D
Nitrate+Nitrite-N
78.6
mg/Kg
- dry
63.8
1 09/13/22 15:55 ZBD 4500NO3F-2011
Molybdenum
<3.29
mg/Kg
- dry
3.29
1 09/09/22 18:38 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 12

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-249-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 09/06/2022 07:45:46
Page 9 of 12

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Page 10 of 12

Ajinomoto North America
4020 Ajinomoto Dr.
Raleigh, NC 27610
Product: Cell Cream
TKN
NH3
Soilds
Pan (Surface)
PAN (Inj. / Inco
o4JINOMOTO
SER/TRP
25,943 ppm
2,283 ppm
10.50% % dry
88.45 Ibs / 1000 g
97.97 Ibs / 1000 g
5c";Ae (A coerwN Ail ' �'Oj
�1 d )' P4 - -).1\
Application Information:
Application of this residual other than the recommended rates as related to the values on this specification sheet are prohibited.
* Application must be in accordance with the permit held by the user.
* These residuals are not to be applied to land that is flooded, frozen or snow covered.
* Adequate procedures shall be provided to prevent surface runoff from carrying any residuals into
surface waters.
* The minumum setbacks must be adhered to:
Private or public water sources
100 feet
Surface waters (Streams, Intermittent and perennial, waterbodies and wetlands)
100 feet
Surface water diversions (Ephemeral streams, waterways, ditches)
25 feet
Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT)
25 feet
Wells with exception of monitoring wells.
100 feet
Bedrock outcrops
25 feet
Signed
Date 8/31/2023

&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 12/22/2022
Solids 2.22
Mineralization Rate 0.3
Gallons per DT 10,802.17
pH 3.5
Sodium Absorpotion 0.89 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 150,000 lbs./1,000 gal 27.77
Ammonia Nitrogen (mg/Kg) 5,320.00 lbs./1,000 gal 0.98
Nitrate -Nitrite (mg/Kg) 220.00 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 46,284 lbs./1,000 gal 8.57
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 48,944 lbs./1,000 gal 9.06
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20 lbs./1,000 gal
2.24
P205 lbs./1,000 gal
3.49
Calcium lbs./1,000 gal
0.42
Magnesium lbs./1,000 gal
0.06
Manganese lbs./1,000 gal
0.01
Sulfur lbs./1,000 gal
7.11
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
22.70
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
4.55
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
22.70
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
13.60
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
6.73
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
11.40
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
22.70
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
56.80
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
150,000
46,284 92.57
103,716
150,000
48,944 97.89
101,056
103,716
15,557 31.11
88,159
101,056
15,158 30.32
85,898
88,159
6,612 13.22
81,547
85,898
6,442 12.88
79,455
81,547
3,058 6.12
78,489
79,455
2,980 5.96
76,476
78,489
1,472 2.94
77,017
76,476
1,434 2.87
75,042
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 72,983 145.97
Total 74,958 149.92

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46974
Ajinomoto North America Inc. Project Ronald Pearce Jr.
A/P Cindy Report Date : 01/06/2023
4020 Ajinomoto Dr Information : Received : 12/28/2022
Raleigh , NC 27610
Brandi Watson
Report Number : 22-362-0009 REPORT OFANALYSIS
Lab No : 60282 Matrix: Solids
Sample ID : HIS Cell Cream Sampled: 12/22/2022 13:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
97.8
%
0.010
1
12/29/2216:04
FMM
SM-2540G
Sulfur
38400
mg/Kg -
dry
455
1
01/03/23 22:10
JTR
6010D
Calcium
<2270
mg/Kg -
dry
2270
1
01/03/23 22:10
JTR
6010D
Aluminum
<227
mg/Kg -
dry
227
1
01/03/23 22:10
JTR
6010D
Manganese
29.7
mg/Kg -
dry
22.7
1
01/03/23 22:10
TJS
6010D
Organic N
144700
mg/Kg -
dry
11360
1
01/05/23 10:30
CALCULATION
Nickel
<11.4
mg/Kg -
dry
11.4
1
01/03/23 22:10
JTR
6010D
Lead
<13.6
mg/Kg -
dry
13.6
1
01/03/23 22:10
JTR
6010D
Arsenic
<22.7
mg/Kg -
dry
22.7
1
01/03/23 22:10
JTR
6010D
Selenium
<22.7
mg/Kg -
dry
22.7
1
01/03/23 22:10
JTR
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
2.22
%
0.010
1
12/29/22 16:04
FMM
SM-2540G
Phosphorus
8230
mg/Kg -
dry
227
1
01/03/23 22:10
JTR
6010D
Copper
<22.7
mg/Kg -
dry
22.7
1
01/03/23 22:10
JTR
6010D
Total Kjeldahl Nitrogen
Qualifiers/ DF Dilution Factor
Definitions
150000 mg/Kg - dry 11400 1 01/05/23 10:30 JPJ ;M-4500-NH3C-TKI`
MQL Method Quantitation Limit
Page 3 of 8

waypANALYTICAL
46974
Ajinomoto North America Inc.
Project
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
Report Number : 22-362-0009
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ronald Pearce Jr.
REPORT OFANALYSIS
Report Date : 01/06/2023
Received : 12/28/2022
Brandi Watson
Lab No : 60282
Sample ID : HIS Cell Cream
Matrix: Solids
Sampled: 12/22/2022 13:00
Potassium
10100
mg/Kg -
dry
455
1
01/03/23 22:10
JTR
6010D
Magnesium
320
mg/Kg -
dry
227
1
01/03/23 22:10
JTR
6010D
Sodium
1150
mg/Kg -
dry
1140
1
01/03/23 22:10
JTR
6010D
Iron
<455
mg/Kg -
dry
455
1
01/03/23 22:10
TJS
6010D
Zinc
<56.8
mg/Kg -
dry
56.8
1
01/03/23 22:10
JTR
6010D
Ammonia Nitrogen
5320
mg/Kg -
dry
4550
1
01/05/23 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<220
mg/Kg -
dry
220
1
01/03/23 16:00
CLP
4500NO3F-2011
Cadmium
<4.55
mg/Kg -
dry
4.55
1
01/03/23 22:10
JTR
6010D
Chromium
<11.4
mg/Kg -
dry
11.4
1
01/03/23 22:10
JTR
6010D
Mercury
<6.73
mg/Kg -
dry
6.73
1
01/04/23 13:57
JTR
SW-7471B
pH
3.5
S.U.
1
01/05/2316:00
DRS
9045D
Molybdenum
<11.4
mg/Kg -
dry
11.4
1
01/03/23 22:10
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-362-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 12/28/2022 09:30:33
Page 7 of 8

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Page 8of8

Ajinomoto Health & Nutrition North America, Inc.
2022 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT
CLASS A RESIDUALS PROGRAM
WQ0032618
Wastewater Treatment System Residual Sami2ling Summary Form
Field Loading Calculations
Nutrient Analysis

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&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 2/2/2022
Solids 13.1
Mineralization Rate 0.3
Wet Tons per DT 7.63
pH 7.7
Sodium Absorpotion 21.69 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 87,800
lbs./WT 23.00
Ammonia Nitrogen (mg/Kg) 3,310.00
lbs./WT 0.87
Nitrate -Nitrite (mg/Kg) 38.20
lbs./WT 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 27,040
lbs./WT 7.08
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 28,695
lbs./WT 7.52
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20lbs./WT
2.66
P205lbs./WT
7.44
Calcium lbs./WT
0.63
Magnesium lbs./WT
0.47
Manganese lbs./WT
0.01
Sulfur lbs./WT
2.91
Molybdenum lbs./WT
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
3.82
Cadmium (mg/Kg)
0.76
Copper (mg/Kg)
6.62
Lead (mg/Kg)
2.29
Mercury (mg/Kg)
0.12
Nickel (mg/Kg)
3.24
Selenium (mg/Kg)
3.82
Zinc (mg/Kg)
63.10
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
87,800
27,040
54.08
60,760
87,800
28,695 57.39
59,105
60,760
9,114
18.23
51,646
59,105
8,866 17.73
50,239
51,646
3,873
7.75
47,772
50,239
3,768 7.54
46,471
47,772
1,791
3.58
45,981
46,471
1,743 3.49
44,728
45,981
862
1.72
45,119
44,728
839 1.68
43,890
Arsenic lbs./WT
0.00
Cadmium lbs./WT
0.00
Copper lbs./WT
0.00
Lead lbs./WT
0.00
Mercury lbs./WT
0.00
Nickel lbs./WT
0.00
Selenium lbs./WT
0.00
Zinc lbs./WT
0.02
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 42,681 85.36
Total 43,910 87.82

Waypointo
ANALYTICAL
46974
Ajinomoto North America Inc.
Project
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ajinomoto North America Inc.
Report Number : 22-034-0006 REPORT OFANALYSIS
Lab No : 56491
Sample ID : Sludge Cake
Report Date : 02/14/2022
Received : 02/03/2022
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 2/2/2022 8:30
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
86.9
%
0.010
1
02/08/2217:16
FMM
SM-2540G
Potassium
8470
mg/Kg -
dry
382
5
02/11/22 19:03
EAL
6010D
Sulfur
11100
mg/Kg -
dry
76.3
1
02/11/22 02:39
EAL
6010D
Calcium
2390
mg/Kg -
dry
382
1
02/11/22 02:39
EAL
6010D
Magnesium
1800
mg/Kg -
dry
38.2
1
02/11/22 02:39
EAL
6010D
Sodium
16000
mg/Kg -
dry
191
1
02/11/22 02:39
EAL
6010D
Iron
366
mg/Kg -
dry
76.3
1
02/11/22 02:39
EAL
6010D
Aluminum
152
mg/Kg -
dry
38.2
1
02/11/22 02:39
EAL
6010D
Manganese
52.9
mg/Kg -
dry
3.82
1
02/11/22 02:39
EAL
6010D
Copper
6.62
mg/Kg -
dry
3.82
1
02/11/22 02:39
EAL
6010D
Zinc
63.1
mg/Kg -
dry
9.54
1
02/11/22 02:39
EAL
6010D
Cadmium
<0.763
mg/Kg -
dry
0.763
1
02/11/22 02:39
EAL
6010D
Chromium
6.23
mg/Kg -
dry
1.91
1
02/11/22 02:39
EAL
6010D
Nickel
3.24
mg/Kg -
dry
1.91
1
02/11/22 02:39
EAL
6010D
Lead
<2.29
mg/Kg -
dry
2.29
1
02/11/22 02:39
EAL
6010D
Arsenic
<3.82
mg/Kg -
dry
3.82
1
02/11/22 02:39
EAL
6010D
Mercury
<0.121
mg/Kg -
dry
0.121
1
02/09/22 15:37
JW2
SW-7471B
Selenium
<3.82
mg/Kg -
dry
3.82
1
02/11/22 02:39
EAL
6010D
Molybdenum
<1.91
mg/Kg -
dry
1.91
1
02/11/22 02:39
EAL
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 5 of 11

•
0
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Ajinomoto North America Inc.
A/P Cindy
Report Date : 02/14/2022
4020 Ajinomoto Dr
Information :
Received : 02/03/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-034-0006
REPORT OFANALYSIS
Agronomist
Lab No : 56491
Matrix: Solids
Sample ID : Sludge Cake
Sampled: 2/2/2022 8:30
Test
Results
Units
MQL DF
Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
3310
mg/Kg - dry
763 1
02/10/22 13:45 JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<38.2
mg/Kg - dry
38.2 1
02/09/22 15:07 ZBD 4500NO3F-2011
Organic N
84500
mg/Kg - dry
1908 1
02/10/22 09:00 CALCULATION
pH
7.7
S.U.
1
02/10/2213:37 DRS 9045D
Total Solids
13.1
%
0.010 1
02/08/22 17:16 FMM SM-2540G
Total Kjeldahl Nitrogen
87800
mg/Kg - dry
1910 1
02/10/22 09:00 JPJ ;M-4500-NH3C-TKI`
Phosphorus
12400
mg/Kg - dry
38.2 1
02/11/22 02:39 EAL 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 11

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-034-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 02/03/2022 13:49:39
Page 9 of 11

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&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 5/20/2022
Solids 14.8
Mineralization Rate 0.3
Wet Tons per DT 6.76
pH 7.42
Sodium Absorpotion 22.42 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 82,400
lbs./WT 24.39
Ammonia Nitrogen (mg/Kg) 676.00
lbs./WT 0.20
Nitrate -Nitrite (mg/Kg) 34.90
lbs./WT 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 24,890
lbs./WT 7.37
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 25,228
lbs./WT 7.47
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20lbs./WT
2.64
P205lbs./WT
6.68
Calcium lbs./WT
0.75
Magnesium lbs./WT
0.48
Manganese lbs./WT
0.01
Sulfur lbs./WT
4.03
Molybdenum lbs./WT
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
3.38
Cadmium (mg/Kg)
0.68
Copper (mg/Kg)
7.97
Lead (mg/Kg)
2.03
Mercury (mg/Kg)
1.07
Nickel (mg/Kg)
3.59
Selenium (mg/Kg)
3.38
Zinc (mg/Kg)
48.60
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
82,400
24,890 49.78
57,510
82,400
25,228 50.46
57,172
57,510
8,626 17.25
48,883
57,172
8,576 17.15
48,596
48,883
3,666 7.33
45,217
48,596
3,645 7.29
44,951
45,217
1,696 3.39
43,522
44,951
1,686 337
43,266
43,522
816 1.63
42,705
43,266
811 1.62
42,454
Arsenic lbs./WT
0.00
Cadmium lbs./WT
0.00
Copper lbs./WT
0.00
Lead lbs./WT
0.00
Mercury lbs./WT
0.00
Nickel lbs./WT
0.00
Selenium lbs./WT
0.00
Zinc lbs./WT
0.01
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 39,695 79.39
Total 39,946 79.89

•
0
Waypoint
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Ajinomoto North America
A/P Cindy
Report Date : 06/03/2022
4020 Ajinomoto Dr
Information :
Received : 05/24/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-144-0002
REPORT OFANALYSIS
Agronomist
Lab No : 57963
Matrix: Solids
Sample ID : Sludge Cake
Sampled: 5/20/2022 0:00
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Moisture
85.2
%
0.010
1 05/25/2216:33 FMM SM-2540G
Calcium
2530
mg/Kg - dry
338
1 05/31/22 22:23 TJS 6010D
Manganese
50.1
mg/Kg - dry
3.38
1 05/31/22 22:23 TJS 6010D
Copper
7.97
mg/Kg - dry
3.38
1 05/31/22 22:23 TJS 6010D
Organic N
82430
mg/Kg - dry
1689
1 06/01/22 10:00 CALCULATION
Lead
<2.03
mg/Kg - dry
2.03
1 05/31/22 22:23 TJS 6010D
Arsenic
<3.38
mg/Kg - dry
3.38
1 05/31/22 22:23 TJS 6010D
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
<676
mg/Kg
- dry
676
1
06/01/22 14:45
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
34.9
mg/Kg
- dry
32.7
1
05/27/22 11:03
ZBD
4500NO3F-2011
Total Kjeldahl Nitrogen
82400
mg/Kg
- dry
1690
1
06/01/22 10:00
JPJ
;M-4500-NH3C-TKI`
Phosphorus
9860
mg/Kg
- dry
33.8
1
05/31/22 22:23
TJS
6010D
Aluminum
171
mg/Kg
- dry
33.8
1
05/31/22 22:23
TJS
6010D
Cadmium
<0.676
mg/Kg
- dry
0.676
1
05/31/22 22:23
TJS
6010D
Chromium
6.82
mg/Kg
- dry
1.69
1
05/31/22 22:23
TJS
6010D
Iron
557
mg/Kg
- dry
67.6
1
05/31/22 22:23
TJS
6010D
Molybdenum
<1.69
mg/Kg
- dry
1.69
1
05/31/22 22:23
TJS
6010D
Potassium
7430
mg/Kg
- dry
338
5
06/01/22 14:03
EAL
6010D
Sodium
15300
mg/Kg
- dry
169
1
05/31/22 22:23
TJS
6010D
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 5 of 11

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46974
Ajinomoto North America Inc. Project Ajinomoto North America
A/P Cindy Report Date : 06/03/2022
4020 Ajinomoto Dr Information : Received : 05/24/2022
Raleigh , NC 27610
�oau� �� Grow
Report Number : 22-144-0002 REPORT OFANALYSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 57963 Matrix: Solids
Sample ID : Sludge Cake Sampled: 5/20/2022 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Zinc
48.6 mg/Kg - dry 8.45 1 05/31/22 22:23 TJS 6010D
Total Solids
14.8
%
0.010
1
05/25/22 16:33
FMM
SM-2540G
Sulfur
13600
mg/Kg -
dry
67.6
1
05/31/22 22:23
TJS
6010D
Magnesium
1610
mg/Kg -
dry
33.8
1
05/31/22 22:23
TJS
6010D
Nickel
3.59
mg/Kg -
dry
1.69
1
05/31/22 22:23
TJS
6010D
Mercury
<1.07
mg/Kg -
dry
1.07
1
06/02/22 11:28
JTR
SW-7471B
Selenium
<3.38
mg/Kg -
dry
3.38
1
05/31/22 22:23
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 11

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-144-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 05/24/2022 12:24:23
Page 10 of 11

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Ajinomoto North America
4020 Ajinomoto Dr.
Raleigh, NC 27610
Product: Cell Cream
TKN
NH3
Soilds
Pan (Surface)
PAN (Inj. / Inco
dJJINOMOTO
HIS
15,988 ppm
616 ppm
8.42% % dry
53.85 Ibs / 1000 g
56.42 Ibs / 1000 g
N'sQ—\e cell U?km �A - `J.5%
< JJ"j)' e0 - 1.yZ
Application Information:
Application of this residual other than the recommended rates as related to the values on this specification sheet are prohibited.
* Application must be in accordance with the permit held by the user.
* These residuals are not to be applied to land that is flooded, frozen or snow covered.
* Adequate procedures shall be provided to prevent surface runoff from carrying any residuals into
surface waters.
* The minumum setbacks must be adhered to:
Private or public water sources
100 feet
Surface waters (Streams, Intermittent and perennial, waterbodies and wetlands)
100 feet
Surface water diversions (Ephemeral streams, waterways, ditches)
25 feet
Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT)
25 feet
Wells with exception of monitoring wells.
100 feet
Bedrock outcrops
25 feet
Signed
Date 5/20/2022

&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 8/31/2022
Solids 15
Mineralization Rate 0.3
Wet Tons per DT 6.67
pH 7.11
Sodium Absorpotion 18.36 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 88,000
lbs./WT 26.40
Ammonia Nitrogen (mg/Kg) 1,850.00
lbs./WT 0.56
Nitrate -Nitrite (mg/Kg) 30.60
lbs./WT 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 26,801
lbs./WT 8.04
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 27,726
lbs./WT 8.32
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20lbs./WT
2.59
P205lbs./WT
6.94
Calcium lbs./WT
0.85
Magnesium lbs./WT
0.52
Manganese lbs./WT
0.02
Sulfur lbs./WT
2.86
Molybdenum lbs./WT
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
3.33
Cadmium (mg/Kg)
0.67
Copper (mg/Kg)
6.80
Lead (mg/Kg)
2.00
Mercury (mg/Kg)
0.99
Nickel (mg/Kg)
3.49
Selenium (mg/Kg)
3.33
Zinc (mg/Kg)
38.30
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
88,000
26,801 53.60
61,199
88,000
27,726 55.45
60,274
61,199
9,180 18.36
52,019
60,274
9,041 18.08
51,233
52,019
3,901 7.80
48,118
51,233
3,842 7.68
47,391
48,118
1,804 3.61
46,314
47,391
1,777 3.55
45,614
46,314
868 1.74
45,445
45,614
855 1.71
44,758
Arsenic lbs./WT
0.00
Cadmium lbs./WT
0.00
Copper lbs./WT
0.00
Lead lbs./WT
0.00
Mercury lbs./WT
0.00
Nickel lbs./WT
0.00
Selenium lbs./WT
0.00
Zinc lbs./WT
0.01
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 42,555 85.11
Total 43,242 86.48

•
0
Waypoint
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46974
Ajinomoto North America Inc.
Project
Sludges
A/P Cindy
Report Date : 09/14/2022
4020 Ajinomoto Dr
Information :
Received : 09/06/2022
Raleigh , NC 27610
�oau� �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number : 22-249-0003
REPORT OFANALYSIS
Agronomist
Lab No : 59271
Matrix: Solids
Sample ID : Sludge Cake
Sampled: 8/31/2022 13:30
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Moisture
85.0
%
0.010
1 09/07/2215:40 FMM SM-2540G
Calcium
2820
mg/Kg - dry
333
1 09/09/22 18:43 TJS 6010D
Manganese
68.7
mg/Kg - dry
3.33
1 09/09/22 18:43 TJS 6010D
Copper
6.80
mg/Kg - dry
3.33
1 09/09/22 18:43 TJS 6010D
Organic N
86130
mg/Kg - dry
1667
1 09/13/22 09:50 CALCULATION
Lead
<2.00
mg/Kg - dry
2.00
1 09/09/22 18:43 TJS 6010D
Arsenic
<3.33
mg/Kg - dry
3.33
1 09/09/22 18:43 TJS 6010D
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
1850
mg/Kg
- dry
667
1
09/13/22 13:50
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<30.6
mg/Kg
- dry
30.6
1
09/13/22 15:56
ZBD
4500NO3F-2011
Total Kjeldahl Nitrogen
88000
mg/Kg
- dry
1670
1
09/13/22 09:50
JPJ
;M-4500-NH3C-TKI`
Phosphorus
10100
mg/Kg
- dry
33.3
1
09/09/22 18:43
TJS
6010D
Aluminum
133
mg/Kg
- dry
33.3
1
09/09/22 18:43
TJS
6010D
Cadmium
<0.667
mg/Kg
- dry
0.667
1
09/09/22 18:43
TJS
6010D
Chromium
6.93
mg/Kg
- dry
1.67
1
09/09/22 18:43
TJS
6010D
Iron
424
mg/Kg
- dry
66.7
1
09/09/22 18:43
TJS
6010D
Molybdenum
<1.67
mg/Kg
- dry
1.67
1
09/09/22 18:43
TJS
6010D
Potassium
7200
mg/Kg
- dry
333
5
09/12/22 12:25
TJS
6010D
Sodium
13000
mg/Kg
- dry
167
1
09/09/22 18:43
TJS
6010D
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 5 of 12

Waypointo
ANALYTICAL
46974
Ajinomoto North America Inc.
Project Sludges
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
Report Number : 22-249-0003
Lab No : 59271
Sample ID : Sludge Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 09/14/2022
Received : 09/06/2022
0Awl[ � Grow
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/31/2022 13:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Zinc
38.3 mg/Kg - dry 8.33 1 09/09/22 18:43 TJS 6010D
Total Solids
15.0
%
0.010
1
09/07/22 15:40
FMM
SM-2540G
Sulfur
9530
mg/Kg -
dry
66.7
1
09/09/22 18:43
TJS
6010D
Magnesium
1720
mg/Kg -
dry
33.3
1
09/09/22 18:43
TJS
6010D
Nickel
3.49
mg/Kg -
dry
1.67
1
09/09/22 18:43
TJS
6010D
Mercury
<0.987
mg/Kg -
dry
0.987
1
09/12/22 11:11
TJS
SW-7471B
Selenium
<3.33
mg/Kg -
dry
3.33
1
09/09/22 18:43
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 12

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-249-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 09/06/2022 07:45:46
Page 9 of 12

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Page 10 of 12

Ajinomoto North America
4020 Ajinomoto Dr.
Raleigh, NC 27610
Product: Cell Cream
TKN
NH3
Soilds
Pan (Surface)
PAN (Inj. / Inco
o4JINOMOTO
SER/TRP
25,943 ppm
2,283 ppm
10.50% % dry
88.45 Ibs / 1000 g
97.97 Ibs / 1000 g
5c";Ae (A coerwN Ail ' �'Oj
�1 d )' P4 - -).1\
Application Information:
Application of this residual other than the recommended rates as related to the values on this specification sheet are prohibited.
* Application must be in accordance with the permit held by the user.
* These residuals are not to be applied to land that is flooded, frozen or snow covered.
* Adequate procedures shall be provided to prevent surface runoff from carrying any residuals into
surface waters.
* The minumum setbacks must be adhered to:
Private or public water sources
100 feet
Surface waters (Streams, Intermittent and perennial, waterbodies and wetlands)
100 feet
Surface water diversions (Ephemeral streams, waterways, ditches)
25 feet
Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT)
25 feet
Wells with exception of monitoring wells.
100 feet
Bedrock outcrops
25 feet
Signed
Date 8/31/2023

&AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 12/21/2022
Solids 15.3
Mineralization Rate 0.3
Wet Tons per DT 6.54
pH 7
Sodium Absorpotion 21.85 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 84,300
lbs./WT 25.80
Ammonia Nitrogen (mg/Kg) 4,840.00
lbs./WT 1.48
Nitrate -Nitrite (mg/Kg) 32.70
lbs./WT 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 26,291
lbs./WT 8.04
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 28,711
lbs./WT 8.79
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
K20lbs./WT
2.93
P205lbs./WT
6.96
Calcium lbs./WT
0.57
Magnesium lbs./WT
0.48
Manganese lbs./WT
0.02
Sulfur lbs./WT
2.90
Molybdenum lbs./WT
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
3.27
Cadmium (mg/Kg)
0.65
Copper (mg/Kg)
6.60
Lead (mg/Kg)
1.96
Mercury (mg/Kg)
0.98
Nickel (mg/Kg)
3.29
Selenium (mg/Kg)
3.27
Zinc (mg/Kg)
32.50
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
84,300
26,291 52.58
58,009
84,300
28,711 57.42
55,589
58,009
8,701 17.40
49,308
55,589
8,338 16.68
47,251
49,308
3,698 7.40
45,610
47,251
3,544 7.09
43,707
45,610
1,710 3.42
43,899
43,707
1,639 3.28
42,068
43,899
823 1.65
43,076
42,068
789 1.58
41,279
Arsenic lbs./WT
0.00
Cadmium lbs./WT
0.00
Copper lbs./WT
0.00
Lead lbs./WT
0.00
Mercury lbs./WT
0.00
Nickel lbs./WT
0.00
Selenium lbs./WT
0.00
Zinc lbs./WT
0.01
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 41,224 82.45
Total 43,021 86.04

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46974
Ajinomoto North America Inc. Project Ronald Pierce Jr.
A/P Cindy Report Date : 01/05/2023
4020 Ajinomoto Dr Information : Received : 12/22/2022
Raleigh , NC 27610
Brandi Watson
Report Number : 22-356-0007 REPORT OFANALYSIS
Lab No : 60260 Matrix: Solids
Sample ID : Sludge Cake Sampled: 12/21/2022 10:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
84.7
%
0.010
1
12/28/2215:37
FMM
SM-2540G
Sulfur
9480
mg/Kg -
dry
65.4
1
12/30/22 21:44
BKN
6010D
Calcium
1850
mg/Kg -
dry
327
1
12/30/22 21:44
JTR
6010D
Aluminum
130
mg/Kg -
dry
32.7
1
12/30/22 21:44
BKN
6010D
Manganese
59.2
mg/Kg -
dry
3.27
1
12/30/22 21:44
BKN
6010D
Organic N
79480
mg/Kg -
dry
1634
1
01/04/23 10:00
CALCULATION
Nickel
3.29
mg/Kg -
dry
1.63
1
12/30/22 21:44
BKN
6010D
Lead
<1.96
mg/Kg -
dry
1.96
1
12/30/22 21:44
BKN
6010D
Arsenic
<3.27
mg/Kg -
dry
3.27
1
12/30/22 21:44
BKN
6010D
Selenium
<3.27
mg/Kg -
dry
3.27
1
12/30/22 21:44
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
15.3
%
0.010
1
12/28/22 15:37
FMM
SM-2540G
Phosphorus
9930
mg/Kg -
dry
32.7
1
12/30/22 21:44
BKN
6010D
Copper
6.60
mg/Kg -
dry
3.27
1
12/30/22 21:44
BKN
6010D
Total Kjeldahl Nitrogen
Qualifiers/ DF Dilution Factor
Definitions
84300 mg/Kg - dry 1630 1 01/04/23 10:00 JPJ ;M-4500-NH3C-TKI`
MQL Method Quantitation Limit
Page 3 of 10

waypANALYTICAL
46974
Ajinomoto North America Inc.
Project
A/P Cindy
4020 Ajinomoto Dr
Information
Raleigh , NC 27610
Report Number : 22-356-0007
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ronald Pierce Jr.
REPORT OFANALYSIS
Report Date : 01/05/2023
Received : 12/22/2022
Brandi Watson
Lab No : 60260
Sample ID : Sludge Cake
Matrix: Solids
Sampled: 12/21/2022 10:45
Potassium
7970
mg/Kg -
dry
327
5
01/03/23 17:28
JTR
6010D
Magnesium
1580
mg/Kg -
dry
32.7
1
12/30/22 21:44
BKN
6010D
Sodium
13600
mg/Kg -
dry
163
1
12/30/22 21:44
BKN
6010D
Iron
337
mg/Kg -
dry
65.4
1
12/30/22 21:44
TJS
6010D
Zinc
32.5
mg/Kg -
dry
8.17
1
12/30/22 21:44
BKN
6010D
Ammonia Nitrogen
4840
mg/Kg -
dry
654
1
01/04/23 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<32.7
mg/Kg -
dry
32.7
1
12/30/22 11:36
ZBD
4500NO3F-2011
Cadmium
<0.654
mg/Kg -
dry
0.654
1
12/30/22 21:44
BKN
6010D
Chromium
7.06
mg/Kg -
dry
1.63
1
12/30/22 21:44
BKN
6010D
Mercury
<0.980
mg/Kg -
dry
0.980
1
12/30/22 15:05
TJS
SW-7471B
pH
7.0
S.U.
1
01/03/2315:55
DRS
9045D
Molybdenum
<1.63
mg/Kg -
dry
1.63
1
12/30/22 21:44
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 10

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46974
Customer Name: Ajinomoto North America Inc.
Report Number: 22-356-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 12/22/2022 12:28:02
Page 7 of 10

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2022 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT
CLASS A RESIDUALS PROGRAM
WQ0032618
Annual Distribution & Marketing/Surface Disj2osal Certification and Summary Form

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