WQ0001863_2022 Residual Annual Report_20230223 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0001863
Applicant/Permittee City of Mount Holly
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001863
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste100, Baltimore, MD 21220
Facility Name*
City of Mount Holly Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for City of Mount Holly, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Mt Holly NC 2022 Annual Report FINAL.pdf 20.47MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 24, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0001863
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Mount Holly, NC.
If you have any questions or need additional information, please do not hesitate to contact
Danny Jackson at [phone] or Alex Fox at [phone].
Sincerely,
P '�ELY--
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Danny Jackson, City of Mount Holly
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

City of Mount Holly, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001863
2022 ANNUAL REPORT

City of Mount Holly, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W 00018G3 County Gaston Year 2022
Facility Name (as shown on permit) Mount Holly WWTP & WTP - _NPDES No. NC002l l56 & 01-36-020
Land Application Operator S na =ro Phone## [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summa :
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 8
Total amount of dry tons applied during the year for all application sites: 117.94
Total number of acres utilized for land application during the year: 112,70
Part B -- Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X 'YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pl-I was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the pen -nit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached,
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Pennit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9• All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received frorn the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and rennediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, sunder penalty of law, that the above information is, to the bes of my knowledge and belief, true, accurate, and complete, I
am aware that there are significant penalties for submitting false inform io , including the possibility of fines and imprisonment for
knowing violations."
Miles Braswell City Manager
Permittee Name and Title (type or print) 491ge P mittee Date
%2/01/2023
' natur of 4P,,p,,er* Date e of d Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 4/3/2022
MOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
January 2022
March 2022
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2023 9:51:53 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
341,000.00
G
33.13
D
30.05
483,600.00
G
46.99
D
42.62
824,600.00
G
80.12
D
72.67

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 12/14/2022 - 12/31/2022
MOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
December 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2023 9:53:54 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
589,000.00
G
37.82
D
34.31
589,000.00
G
37.82
D
34.31

SECTION 2

C3 CN
J d
fl �
a
J
O
d N
J
O
LU
Q C
LU
ad
m
U
z
J
o O
00 r =
M
r
O Z Z
z
a D
E
Z
O E
: u O
� CLi a z �r
Ci
0
Ca
c..
f � .J
LQ N N Q V M O 00 61 Q 00 O C) N
N It V V T m O O Cl) N
d o rn
O 00 M
hi r co N p V r M Oti M r
V Y 0
{ O O I` M Ln r r% O O O O O
r r r V V to O O c �r
r 9 Co
M { O 0 0 O ^ 0 O CD 0 CD
O O O N
N O M O V
M
V V 10 M
CD CD
Q Lo L(� m Q ti n N i'n Q Q Q Q
Z r+ e0 * Z CO Lf1 r V Ih Z Z Z Z
ul °3
Ln E z
° E E E c° `0 m
m a a o E> se m E
d°' Qchi U7 O ti C
U U U J Z US N I I— � Z
0
ti
L'
LL
d
0)
0
r
N
N
m
c
a

o )
§ 7
< _
o j \q
<
I
j E 0 §
{ z \ f )
# m a
IL
2 L J z k
0 / 0 � § / / 0
/ v ® m o 4 §
o 0 0 0 0 o 0—
) § LO m /
o R 0) o R 0§
§ / / LO A §
a
° § @ ) 8 8 % g
/ G $ ® q J 0 \
N
�
O
N
�
k
a_

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:XA04050
Date Completed:01/18/2022
NIM�� Mr�
01/19/2022 2:30 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA04050
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of these samples was 3 times the standard procedure amount. The
LOQ has been adjusted accordingly.
Inorganic Non -Metals
All samples analyzed with batch 28656 were analyzed using expired ascorbic acid reagent. This run was
a re -analysis of a previous run that was analyzed using a linear calibration range that was slightly greater
than 6 months old, per SOP criteria. The instrument was re -calibrated and the samples were re-
analyzed, using the new calibration, and similar results were obtained. Thus, re-ananlysis is not required
for samples that were within calibration range. All instrumentation check standards and method criteria
were met.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: XA04050
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mt. Holly Solid 01/04/2022 1145 01/04/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:XA04050-001
Description: Mt. Holly Matrix: Solid
Date Sampled:01/04/2022 1145 % Solids: 2.33 01/12/2022 0029
Date Received:01/04/2022
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date
Batch
1 350.1
(Ammonia - N ) 350.1
2
01/12/2022 2103 DAK
28095
1
(Nitrate - N ) 9056A
1
01/05/2022 2258 AAB
27592
1
(Nitrite - N ) 9056A
1
01/05/2022 2258 AAB
27593
2
(Phosphorus) 365.1
10
01/13/2022 1135 DMA
01/06/2022 1459
27588
1
(Soil pH meas) 9045D
1
01/11/2022 2032 NBW
28081
1 351.4
(TKN) 351.2
2
01/05/2022 1749 DMA
01/05/2022 1000
27443
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Ammonia - N (gas diffusion)
350.1
3300
86
45
mg/kg
1
Nitrate - N (soluble)
9056A
100
21
4.3
mg/kg
1
Nitrite - N (soluble)
9056A
22
8.6
4.3
mg/kg
1
Phosphorus
7723-14-0 365.1
13000
2100
430
mg/kg
2
Soil pH measured in water @
19.6 ° C
9045D
7.2
su
1
TKN
351.2
53000
4300
2100
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:XA04050-001
Description: Mt. Holly Matrix: Solid
Date Sampled:01/04/2022 1145 % Solids: 2.33 01/12/2022 0029
Date Received:01/04/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/10/2022 0733 JAB2 01/10/2022 0116 27833
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 3.2 0.76 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:XA04050-001
Description: Mt. Holly Matrix: Solid
Date Sampled:01/04/2022 1145 % Solids: 2.33 01/12/2022 0029
Date Received:01/04/2022
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst
6010D 1 01/06/2022 1050 JMH
Prep Date Batch
01/06/2022 0311 27531
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Aluminum
7429-90-5
6010D
17000
280
110
mg/kg
1
Arsenic
7440-38-2
6010D
13
11
3.5
mg/kg
1
Cadmium
7440-43-9
6010D
ND
3.5
0.89
mg/kg
1
Calcium
7440-70-2
6010D
6300
3500
440
mg/kg
1
Chromium
7440-47-3
6010D
100
7.1
1.8
mg/kg
1
Copper
7440-50-8
6010D
300
7.1
3.2
mg/kg
1
Iron
7439-89-6
6010D
5300
71
32
mg/kg
1
Lead
7439-92-1
6010D
5.3
J
7.1
3.2
mg/kg
1
Magnesium
7439-95-4
6010D
2800
J
3500
440
mg/kg
1
Manganese
7439-96-5
6010D
150
11
4.2
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
28
7.1
mg/kg
1
Nickel
7440-02-0
6010D
7.9
J
28
7.4
mg/kg
1
Potassium
7440-09-7
6010D
3600
3500
440
mg/kg
1
Selenium
7782-49-2
6010D
6.7
J
14
5.7
mg/kg
1
Sodium
7440-23-5
6010D
4400
3500
440
mg/kg
1
Zinc
7440-66-6
6010D
440
35
8.8
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES. LLC
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
�ceAr-ff4—Vcai
Clicnr! S NACRO
Samples Receipt Checklist ISRCf (AAEGOIRC-15) Keviscd;9/29jN20
Issuing Autholty, Pace ENV -'l li:7i}I. Paga 1 of 1
Sample Receipt Cheekl6t (SRC)
CaolerinsDarmi Irrldatc, JAEH I JAaW Lot A: ,Agansn
calls ofreedpa: 0 Pac,a
Client Ll4:T S NAEX tither,
�
yet
, A 0
_ ] , 15�ere
cusCOtiv Seals preSent (in rlm roeleff
Yc
Ztio
RfA 1, 1
austodysealswom resent,w?,rethc • in tc-,aLi l Lin bmAgn.,
pI-I drip 1D_ awn
rigirud louip=ture upon fece
3.3 13.3 �C tiA INA aC
-M'tf od-ElTim-.peraftim. A lank
—thud : Q d of eaoluatwtet i
Clilorise strip li7_ `{ TpMed by,
tpt! Derived (Corrected) temperaWM tirrm receipt %Snlid SnaFr
HA r+NA DC NA jKA AC
❑,4_}�=arest.BOtaleR I GEn ID: iRGun CorrCtition F
-e LI k* picks ❑ Dry Ice ❑ None
—
! up ID: 21-2661
tur: � 11C
0 Ycs
Yes
�] Flo
Q Nn
[DNAM
©NA
3, I
ce rnpamture ofar-y cooler exccedcd 8,U° , was l°-ojoot Mnnagsr No
wasN,,itif3ecl gam, phone,'ema.iI f face-to-face (circle anc),
ified;'
4. l�
Iae oommerdal coin-ier's packing slip attache_i In this Cxjr„?,
7 Yes
Ll No
5,
Were proper cusmdy proced',ims (ralinquished,teceivud) followcd?
,f
Yes
No
6,
. ac sample IDs lio" on the COC?
//
VL%
Tf„
?_
pro santiple IDs lisued on all €iEnple co bwrs?
'e;
No
ti,
w collecti-nn data & time listed on the CDC?
Yes
I Lj No
7. ijJas
cullcxtiu„ clatc & tirria listed on a1I salmi la containers?
, Yes
❑No
10,
Pid all ccmlAiner label infarma:inn (10, date, tinier irith-1he Oor
a7 as
=No
I t,
"ctr t*sts W be T)&FGnna9 IisWrll LM Lha COC?
21Ym
❑ No
12-
(imi
Did all samples zrAve in the proper contant €ar -each test a_i&Dr in
Qkc-n. N-l-; rin, dc.}e
goad o0ndki0n
Y;
No
13.
T'as ads uata sample volum r vailablO
j
y,-s
No
Id.
Mere all samples nweived within ;,�tFe lioldingtimeor4ahours, vrh iiaver vowm first?
!_ yes
Nu
1.5.
Wlorc any samples of itainors missirgfexcass (ciryio ono) sumplcs NO
Ei5W on COC?
Yes
❑lt0
❑ N.A
16.
ir.
or VGA and RSK-175 samples, were bubbles present �"�+�-si21u" ('
ofrhe VOA viaWL
�"ar 6rnm in dialri=)
's
No
HA!
17,
"rrc all T)Ttr'metaly+nutrienl satnple; rGririxl milPN rrC?
Y{
No
91NA i
I �.
Were all cyanide samjJm res4�ived at a pH > 12 wW sulfide 53mple5 r�c4iv
t:d at a pH > 9?
Y
F INo
MNA
resi�uo]
ere all applicable lo609.3 M-g,
Chlorine?
) samples I'riw of
❑ Yas
El No
MNA
20.
crirr.clly
"ereclieiitremarkdfequeRt; (i.e. i%sque.,�ned dilutions, MSIMSO des
I.t;ir14;c7rihed From the MC; inal 1lie cornmer.t 5actinn in 1,IMS?
7rdatio ins, eDc---1
Ll y'!x
Nu
2i,
'aa tiir iiomlulmbcrlis!cd �n tl.o containcr I bt1 If w.-s Quote*
9ampip Prewr ati-un (t*'tt44t
bt mplr•. I fir r nv y,im�I{ � inrnrre,lly rrrtir. 4rc3 err wiih hradtr
;r,.]
Sample(s) n
in nw-r4e receiving with
Time of ptesuvaticfn
were i zdved mcotrectly piTsrytwctand
mL of circle Dn5: H2SO4. HNW, HCI, NaOE using SRpr NA
, If more than one punsDrvativc is :ie�-ed, picasc riot:. in the ram
ztiiusted accorcint;l;
ents.bciaw.
Sfrnple(s) v-i
WUN recuivod with bubbks
r6 min in diami CD r.
3L,irnples(s) Nk
fiustcd aocordingly iri wurupl
were rec.e:ved wib TRC > 0-5 ma/L. (lf >'t
raot�ivirtg Mill sodiuiu thiMilfate (''l+ Z!1aSa03)with Shealy ID_ >gA
i 9 is no) and were
SK borco6e labels aripIM by:
6P Date t1d1 022
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (4400 x 2.3300) = 100 = 102.52
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (6300 x 2.3300) = 100 = 146.79
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2800 x 2.3300) = 100 = 65.24
Na meq = Na mg/I = Molec.Wgt.Na = 102.52 = 23 = 4.45739
Ca meq = Ca mg/I = Molec.Wgt.Ca = 146.79 = 20 = 7.3395
Mg meq = Mg mg/I = Molec.Wgt.Mg = 65.24 = 12 = 5.43667
Sample Date Report Range Ratio
1 /4/2022 1 /1 /2022 - 3/31 /2022 1.7636
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.45739 = SgrRoot[0.5(7.3395+5.43667)] = 1.76358

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:XD07060
Date Completed:04/28/2022
NIM�� Mr�
04/29/2022 11:10 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XD07060
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as a biosolid therefore they were weighed out at around 3.0 grams
to 4.0 grams to ensure proper digestion: XD07060-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following samples were ran in a sequence in which nitrate was not present in the solid LOQ:
XD07060-001. The aqueous LOQ passes along with all other aqueous and solid QC. Since the detections
are greater than the LOQ in runs 1 and 2 and the LCS passed for nitrate in run 2, data will be reported
from run 2.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XD07060-001
Description: MT HOLLY Matrix: Solid
Date Sampled: 04/06/2022 1000 % Solids: 1.41 04/21/2022 2204
Date Received:04/07/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
2
(% Solids) SM 2540G
1 04/21/2022 2204 CVR
39012
1 350.1
(Ammonia - N ) 350.1
2 04/13/2022 1649 CMM
37749
2
(Nitrate - N ) 9056A
1 04/15/2022 1555 CAW
38511
2
(Nitrite - N ) 9056A
1 04/15/2022 1555 CAW
38510
1
(Phosphorus) 365.1
10 04/12/2022 1150 DMA
04/08/2022 1221
37480
1
(Soil pH meas) 9045D
1 04/10/2022 1921 NBW
37674
1 351.4
(TKN) 351.2
1 04/11/2022 1912 DMA
04/08/2022 1143
37479
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
1.41
%
2
Ammonia - N (gas diffusion)
350.1
6000
140
74
mg/kg
1
Nitrate - N (soluble)
9056A
160
35
7.1
mg/kg
2
Nitrite - N (soluble)
9056A
1000
14
7.1
mg/kg
2
Phosphorus
7723-14-0 365.1
17000
3500
710
mg/kg
1
Soil pH measured in water C)
19.5 ° C
9045D
7.2
su
1
TKN
351.2
74000
3500
1800
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 04/13/2022 0740 JAB2
04/13/2022 0139
37586
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
ND
5.3
1.3
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 04/13/2022 0140 KSH2
04/08/2022 1202 37530
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
15000
380
140
mg/kg
1
Arsenic
7440-38-2 6010D
13 J
14
4.7
mg/kg
1
Cadmium
7440-43-9 6010D
1.4 J
4.7
1.2
mg/kg
1
Calcium
7440-70-2 6010D
11000
4700
590
mg/kg
1
Chromium
7440-47-3 6010D
170
9.5
2.4
mg/kg
1
Copper
7440-50-8 6010D
430
9.5
4.3
mg/kg
1
Iron
7439-89-6 6010D
7600
95
43
mg/kg
1
Lead
7439-92-1 6010D
17
9.5
4.3
mg/kg
1
Magnesium
7439-95-4 6010D
5100
4700
590
mg/kg
1
Manganese
7439-96-5 6010D
150
14
5.6
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
38
9.5
mg/kg
1
Nickel
7440-02-0 6010D
15 J
38
9.9
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XD07060-001
Description: MT HOLLY Matrix: Solid
Date Sampled: 04/06/2022 1000 % Solids: 1.41 04/21/2022 2204
Date Received:04/07/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 04/13/2022 0140 KSH2
04/08/2022 1202 37530
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
7200
4700
590
mg/kg
1
Selenium
7782-49-2 6010D
ND
19
7.7
mg/kg
1
Sodium
7440-23-5 6010D
11000
4700
590
mg/kg
1
Zinc
7440-66-6 6010D
670
47
12
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
L
E
i3
z
q>
9
1
u
v
�.
g
C
i
�
hYh R�%14u._tyy4•
F. 6
Er
'
E
.cwalaltll�aS
.�
UOq:611a:i
�
1p
= _ to
c 'i L6
3
of
a'i�-5
Fi
O
a
m
Os
CC
N
O r EN of
� r
�
L
o
0
B
'4
Oz
6
4
o
F
F-
i:-
0
U
el
k
�S
k �
} Q
a
m
LA
CC
C M
6
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Saanples Receipt Checklist ISt7C1 1M17001AC-1 s) RawlsMA/29f2420
G9 + y +#fi Issuing k.sth arity: Paste -':NV - V .0I Page 1 of i
Sample Receipt Cheel€Iist (Sl y'
Sy—ya {NR �#'157 74Z2 XDDTCSC
[-
Client:Cao:ea' lys ected byldate: d,nl ; -
reaus ofreceipt, Face J ]iew 1 1 UPS FedEx C}thc::
Yea1 [ZINOI 1 1.. %yere nistady sea Is pmxrA on the coolar7
rE_]YwlT10DNA 12. 117vvsWal suLls wuro Fr_sLmL, wLrU LFIL inI.=, An6 unbroken'
t I Strip ID- NA Chlorinc Strip 111 �^— - - Tested 1py_ rare
M-633!d Lnrrgl tr4tvry upvc N-"i-j ? Us7ivus (Cormctud) tempermire upon receipt n/rsolid Sna cup TD: 22 3ip
9,1 f+4.7 u rlt rMA %U NA INA -'C M1 ILJ,t sr
Method: ❑f Temperwnim BliiA ail)'tDOLtIM Il,Cultl ID: a IRGun CDrrcction Factor 0 £C
MAW ofuwLard: � Wet Ice El Tee Packr ❑ fDLv ice Munn
❑ Yr
©lo
;l
_
3. ]f t Lrperar-in ofnj)W Cooler exe-, le 6,00C, wus I1rffjcct Man3gcr Notiiit:d'r'
,M was Notified by: phone d mail I fbec-m4acc "ci-cic orro),
Yes
-No
,r NA
J. fib tha cniur_iarciol rOarler'g [11 king blitz ULULuhvd to This IuTm?
{ YL•s
Na
.A. Worn proper rmrodv proredUMS (relingµislre ieL:eived)fulluwk:d?
Ycs
o
6, Wcr: sampJc lily listed on ttte (.IOC?Ye
Es
❑Na
_
7- era sample ]M lisped as all &acuple uonruiadurti?
J 'Yeti
No
8_ Was cuRectior_ date & tbne listed on the Cam?
Yes
,\a
9- u 9 wllcdiur. duL6e dk timc Jistcd an all sample contalr ?
❑ \ n
wi Lh Lhc COC- --
19. DId al l conla finer lslrr] information (ID, Ca , lime) :�
FT -Y2&
LJ Nrjl
1 J . �Vtnt Lust,. Lu htC PC; Ri mrd lislad on the COC?
© Yea
Lj No
1:4. Did all samples arrive Ln the preprr cothtuhral-s fQ each not arKVcjr!,I good uL?lIdiLkm
�utrbrOkcn, lids on, c�a.)'�
-'e.9
LJ Nn
13. Ira% acequale sam f,?e vc,hm,,, a�-LifgbJ&?
'es
No
14. Ww all mnples rucciyod within h the J1utdLng time ot`49 horn, whichever comes CrsL?
i FJYcs
LdNc,
15. lVere any s@E- tes containei—s m i~singiaxcess (ci rele anc) Ku n M_cs; Nnl. lisferi M COO
❑Yes
El[7]-N.A.1fx
�IJL
Frn 1�Q_°► and RSK-I +5 sanLpIts, wrrc bubb]cs pro >upea•tiize" ('f"or {Smrn in d:umaacr
IUMy of Llw VOA vials?
YcsJ
LJ Nal
[Z]14AI
17, %ViBre all DROj nvta s} utricnt samples racEt-ved At �L pH of = V?
Yes
I IN01e
NA
TR-Were all eysdidc svnles receMai ut s►p1T � 17. and su'_fide samples reco;vcd 2Lt
❑ YeS ❑ No QLN " WL:141 uII HIJln19:t UIL: Nrj� r nrv+uyanrue,'pnt!nOvu:D. L0i3Lr&3 k{. U_3MVL) kvnIikm trw of
residual eitlarilu2
20, Wcrc client rernarkslrequects(i.e. rcquesteddLLItiours, MS?NMDdcsWrwdona, etc._,)
[--]Yes No �1 A carrccdy transcribed from tha COC Jnta the c mile:ir sm:Linu iu L]1I 137
Y y NO 21. 13 .--the quore Limberllstad Cm'1^n container lrbel? Tfyes. Quotc f ~J
:�rnQpe l'aesarvr�tio� (phis# be complct d -br any xampie(s) IrcorTcwtly preserved or with hemcispucc.)
Ssimpte(s) wcre receivicl incurruaty preserved aLLd were adju4LL:d a}ca[djF3gly
in sainplu: recoivijig with 'IA unL of r-kirle ogre, HIS04, HNO3, ITC:, NaCNT -.ising 5R. 4 NA
TLrre of presenadon NA� _ If MOt tl;Lld ont preservative is nee-ded, please, nota in the comni erg, tacl�rx
Sauup]c�s) NA _ _. YMrc received wilt bubbtes >6 nun i u d:ar=Teter.
5+3rnp1 (x) NA — we rw roceiyed with TRQ > O.S mgrt (If 419 i,, nr, a-rd
Adjtist€+d aeca)dialgty in simple mcciving with smdiurn lhiosLinte (NaTY.Qa) with uheuly ID. -
SR barecA labels anpdicd by: KNR Dam; od,+n."Mitt
C0111112elits:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (11000 x 1.4100) = 100 = 155.1
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11000 x 1.4100) = 100 = 155.1
Mg mg/I = (mg mg/kg x % Solids) = 100 = (5100 x 1.4100) = 100 = 71.91
Na meq = Na mg/I = Molec.Wgt.Na = 155.1 = 23 = 6.74348
Ca meq = Ca mg/I = Molec.Wgt.Ca = 155.1 = 20 = 7.755
Mg meq = Mg mg/I = Molec.Wgt.Mg = 71.91 = 12 = 5.9925
Sample Date Report Range Ratio
4/6/2022 4/1 /2022 - 6/30/2022 2.5721
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.74348 = SgrRoot[0.5(7.755+5.9925)] = 2.5721

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:XG07088
Date Completed:07/22/2022
NIM�� Mr�
07/24/2022 6:27 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XG07088
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Sample -001 was classified as biosolids therefore it was initially weighed out at around 3.0-4.0 grams to
ensure proper digestion. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The method blank for prep batch 47664 contained the analyte total phosphate greater than the method
acceptance criteria. The associated samples contained detections for this analyte at concentrations
greater than 1 OX the value found in the method blank; therefore sample results are not impacted. The
data has been reported.
The Nitrate and Nitrite method blank, LCS and samples ran in a bracket that contained 11 injections. Per
the SOP, no more than 10 injections shall be analyzed between CCV and CCB pairs. Bracketing QC is
passing and the data is not believed to be adversely affected.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XG07088-001
Description: MT HOLLY Matrix: Solid
Date Sampled: 07/06/2022 1000 % Solids: 2.46 07/10/2022 1650
Date Received:07/07/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 07/10/2022 1650 TAD
47512
1 350.1
(Ammonia - N ) 350.1
10 07/21/2022 1255 CMM
48425
1
(Nitrate - N ) 353.2
1 07/20/2022 1305 KKP
47766
1
(Nitrite - N ) 353.2
1 07/20/2022 1305 KKP
47768
1
(Phosphorus) 365.1
10 07/18/2022 1603 DMA
07/12/2022 1324
47664
1
(Soil pH meas) 9045D
1 07/11/2022 1348 KKP
47566
1 351.4
(TKN) 351.2
2 07/19/2022 2048 DMA
07/16/2022 1320
48198
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
2.46
%
1
Ammonia - N (gas diffusion)
350.1
13000
410
210
mg/kg
1
Nitrate - N (soluble)
353.2
140 S
8.1
1.1
mg/kg
1
Nitrite - N (soluble)
353.2
56 S
8.1
1.1
mg/kg
1
Phosphorus
7723-14-0 365.1
13000
2000
410
mg/kg
1
Soil pH measured in water @
16.7 ° C
9045D
7.6
su
1
TKN
351.2
57000
4100
2000
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/10/2022 1056 MRW2
07/10/2022 0654
47419
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
ND
2.9
0.71
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 07/13/2022 0758 JMH
07/11/2022 1541
47423
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
15000
260
96
mg/kg
1
Arsenic
7440-38-2 6010D
23
9.6
3.2
mg/kg
1
Cadmium
7440-43-9 6010D
1.9 J
3.2
0.80
mg/kg
1
Calcium
7440-70-2 6010D
12000
3200
400
mg/kg
1
Chromium
7440-47-3 6010D
210
6.4
1.6
mg/kg
1
Copper
7440-50-8 6010D
600
6.4
2.9
mg/kg
1
Iron
7439-89-6 6010D
9400
64
29
mg/kg
1
Lead
7439-92-1 6010D
15
6.4
2.9
mg/kg
1
Magnesium
7439-95-4 6010D
4900
3200
400
mg/kg
1
Manganese
7439-96-5 6010D
150
9.6
3.8
mg/kg
1
Molybdenum
7439-98-7 6010D
11 J
26
6.4
mg/kg
1
Nickel
7440-02-0 6010D
19 J
26
6.7
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XG07088-001
Description: MT HOLLY Matrix: Solid
Date Sampled: 07/06/2022 1000 % Solids: 2.46 07/10/2022 1650
Date Received:07/07/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 07/13/2022 0758 JMH
07/11/2022 1541
47423
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
4500
3200
400
mg/kg
1
Selenium
7782-49-2 6010D
ND
13
5.2
mg/kg
1
Sodium
7440-23-5 6010D
5700
3200
400
mg/kg
1
Zinc
7440-66-6 6010D
1100
32
8.0
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
—
u
b
c
eE j
'6
x
O
:J
8
N F
O
-;j O
32
t K E W +`1
g
E n �
E '-' I"
e T ' -
}
L L1 O
tf]
c
m
pz
hL'kPuEaI
n�
�
4 o6
e{�ndwa r3NN
Ir
F
dtn P�
m
•ti
h2
v
w
U
i3
�
C
1}
CL 2 a
M I'!
a
a
r i
i
o"'� ❑
r�i
r�i
7
Ad
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt [hecklist JSRQ (MEO01812-151 Re'iiiised'9 f 2912020
��;rvIrA'
Issuin0Autharity_PaceE`1V ya'CC11. iaageloF1
Sample Receipt Cheeldist (SRQ
Clicut: sM
Cooler Inspected hyrdatc: yDIiW + C71U7.7A2� � �;
-
A4eans ol'receiivi
✓ Paso Uieac UPS FeYIE Ot[1Cr;
Yos Nra
1. 11 cuAody Goals prCBent not the cooler?
Yes No
/ NA
2- if cuswd saal., were rC3Cn4 wera they inT L and unk mken?
II strip IT).- _ C.hltm-ine St:1p ID, _ fc,ted by:!�E�
derived (Co[racted) tt rrperattire upon rt c[Iat 'a$[}lid 5nsp-Cu}a-4
rigina7=empoTatuee upon neoeipt r
3.4 .,O TEA } VJ, ar�N rwn + TaAR+Ielbal;�etnperature
13IJ� oqt7rist BDnjl � IR Gun [Ty: �' Mc;ur:COL -tionrar-rrm
mwa ii>dofersu' It: );let [cc ❑ 1r 1'atilcf ❑ L]r Ice plane
3. if tasmpersturc ❑] iMy C401ee MCCOLied b.11'C, was P rDjta t Mana$Cr Notlficd?
El Yes �No
E�`1A pr;]v hs Notiu u b3: phone eTuail f face to face (�inle one).
`ies No
NA 4. is tit: G7mmerr1a. courier's paot[ingslir attachesito this form'"
jZj
YCS '40
5- Wzro praprraasEodp o"dures (reli3tquksjile aivcd) followed?
Na
6. here Nuinple M9 11;A 0n the CDC?
f
gyres No
17. W Samp[o 0s1iswd an all santpic euutainCtS?
J
'Yes lalo
8- Wam C AGI cdiott tirnri listed an the C(}t:;?
©
Y(m 11,40
9. Was colleden date lima listed 0i all sampl.; roraainerO
Yrs ❑Too
10. Did all container ;abel infnrrnat:on QD, date, time) aagrec will the Cl7C?
[ l
l Yes ?]0
11- Vkfrxe tests to be erfarm lislod on the DG 1
LONo 12. Did ai] samples arrive in the proper ro�raiIrifarcuels best and,nrin gosxlucriditlan
(smbriker., -Lids ¢n, M oe:Na l ;- WaS adcx{u,1[e saMpie vnlnmc a[va=1a1;Ie'}
we yes No 14. Were all Samples retx�ivxl u�i-i�in ! � ih4e holdiTlg-Lime or�lii 11C11 s, tvluci3aver cQr.1�4 tirf.2
Yt (cit
No I5- Were an}' sasnp ks totttainerx f , i��io�+cxccs� �Ie k ris) saouples �]nt list��' as CDC r
VOrI Slid FtSK-175 3ar.]ples, worn 1r.,Ualcs pac_5e�1t �`�caasiae" ('�,"Ot' 6mm in di,�rssaner)
Yex Dtdo - I in any arfthe VOA vials'?
Y N0 NA 17. 14err al: DRiblmela nutrient=11ples received at a pH d<2?
Yes LiNo N1A� 1 S. TeTc id] cyanide Gam les race; 4et1 at a pH > 12 Prtd sulfide samples received at a CIA > 99
19L Wcm all (<0.5 1 +L s,rrples fTL-4 of
Yes [I No ©NA Midual chlorine?
�-1
20. ).°ere client. remaikaftcgwns (i.e. requestrd dilu[lons, M1SiMSD d0ign4tions, Ctc---)
Dyes C] Nu [DNA correct]} uauscrihed firm lha C irtto the cmmult section in (11wim2
1'eS 10 21. '111 the o mjmb„rr• ',ist; on ilia ro:rralner lal di? I f w, 01 a tr
,am ple IP'reservation (MLIS[ be camplet�l for any samples) 1ACarractly primed ar w i 11 Ilea dspucu,)
Sarr[a1e(sj MA were: T--.i od incomelly arose-ved and were adjusIred wcordiugly
inszunpiercori0ri with h�A TrL ofcircic aniiE2304, IM-03, HCI,NaOH usinp�3R 9—
T'imn of presetvalu-ui t` _. If more than onr p gert ice is ne d, p!�se no4d in the rommctTts below,
Smmp]$(s) NA _ 'eCe receiver] witlr h-abbhm >6 n nt in dlaructer,
Samples(s) 't } wcro v Ce iyod with ,RG > -0.5 Tr.PrL (If lr l4 is no) and Were
LSR"hwiod,
lcd ar,rordingly in sample eCENiTL9 will sodium tkilnsulfritc CNaaSjQL) with Shealy 1D: NA
by; KDR'i� drilc: 0-,}0?r2GZ2
Comments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (5700 x 2.4600) = 100 = 140.22
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (12000 x 2.4600) = 100 = 295.2
Mg mg/I = (mg mg/kg x % Solids) = 100 = (4900 x 2.4600) = 100 = 120.54
Na meq = Na mg/I = Molec.Wgt.Na = 140.22 = 23 = 6.09652
Ca meq = Ca mg/I = Molec.Wgt.Ca = 295.2 = 20 = 14.76
Mg meq = Mg mg/I = Molec.Wgt.Mg = 120.54 = 12 = 10.045
Sample Date Report Range Ratio
7/6/2022 7/1 /2022 - 9/30/2022 1.7311
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.09652 = SgrRoot[0.5(14.76+10.045)] = 1.73112

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:XJ04090
Date Completed:10/26/2022
NIM�� Mr�
10/27/2022 11:17 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XJ04090
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solid, sample -001 has an initial weight that is 3x greater than standard
procedure. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XJ04090-001
Description: Mt Holly Matrix: Solid
Date Sampled:10/04/2022 0900 % Solids: 1.54 10/11/2022 2200
Date Received:10/04/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 10/11/2022 2200 MJS2
56709
1 350.1
(Ammonia - N ) 350.1
5 10/19/2022 1638 CMM
57366
1
(Nitrate - N ) 353.2
1 10/19/2022 1522 KKP
57569
1
(Nitrite - N ) 353.2
1 10/19/2022 1522 KKP
57570
1
(Phosphorus) 365.1
5 10/08/2022 1452 DMA
10/07/2022 1400 56358
1
(Soil pH meas) 9045D
1 10/12/2022 1520 KKP
56841
1 351.4
(TKN) 351.2
1 10/07/2022 1751 DMA
10/06/2022 1447
56231
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
1.54
%
1
Ammonia - N (gas diffusion)
350.1
9300 S
320
170
mg/kg
1
Nitrate - N (soluble)
353.2
1200
13
1.7
mg/kg
1
Nitrite - N (soluble)
353.2
12 J
13
1.7
mg/kg
1
Phosphorus
7723-14-0 365.1
14000 S
1600
320
mg/kg
1
Soil pH measured in water @
21.4 ° C
9045D
7.2
su
1
TKN
351.2
70000
3200
1600
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/07/2022 1522 MRW2
10/07/2022 1138
55609
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
5.2
1.3
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 10/18/2022 0112 JMH
10/07/2022 0714
56157
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
14000
410
150
mg/kg
1
Arsenic
7440-38-2 601OD
20
15
5.2
mg/kg
1
Cadmium
7440-43-9 601OD
2.2 J
5.2
1.3
mg/kg
1
Calcium
7440-70-2 601OD
12000
5200
640
mg/kg
1
Chromium
7440-47-3 601OD
210
10
2.6
mg/kg
1
Copper
7440-50-8 601OD
460
10
4.6
mg/kg
1
Iron
7439-89-6 601OD
8400
100
47
mg/kg
1
Lead
7439-92-1 601OD
14
10
4.6
mg/kg
1
Magnesium
7439-95-4 601OD
3600 J
5200
640
mg/kg
1
Manganese
7439-96-5 6010D
200
15
6.1
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
41
10
mg/kg
1
Nickel
7440-02-0 6010D
18 J
41
11
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XJ04090-001
Description: Mt Holly Matrix: Solid
Date Sampled:10/04/2022 0900 % Solids: 1.54 10/11/2022 2200
Date Received:10/04/2022
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/18/2022 0112 JMH 10/07/2022 0714 56157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium
7440-09-7
Selenium
7782-49-2
Sodium
7440-23-5
Zinc
7440-66-6
601OD
3700 J
5200
640
mg/kg 1
601OD
8.9 J
21
8.4
mg/kg 1
601OD
6700
5200
640
mg/kg 1
601OD
900
52
13
mg/kg 1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
M
CO
L
ME OR
r3
f
C
t
I� r —
J
r'
c
a I �FV
day
raw
rCS�f
ti
a
Ifl
4
}
c4
And
'I t
E I a
tl I L V ro
I` �n
•� a
C
f k
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
D[#? Titre; ENV-PRM-WCOL-4286vO2_SamplesReCcip:Checklis PRO
Eifdc#fye Daily: 8f 2 j2o22
aDlPIL- Receipt Choeldist RQ
CIicrr[; Sa"-ti'�ro _ �'u�alcr Tn.S ettcd Gylrlati: �rt��' � ro,�tiu.r�rr�.z Z.sxl �- 7���.00�
res No 1. VV'cl c[�tntT srxlJs eseut.ontlrccoo?et'?
Yes 1-4 , �A n Il -m5lcd srals'ATTt rese% wn 111cl intact and lrnbro n?
rH Stilp ID. NA_ CJ3lvrine Strip JD. KA Testcd b}.
)[9lnill rM raOule ttporr tecOvir ! Denvcd (Cmectvd) rE,rtrperanlc UP-,% receipt #%Solid ud Snal_�-CI17- R--� sas
!"t I I.1 a,� NA f NA c NA fNA oC PA /N. Off.. - —
44-w4-CIFIFF' ueUJULk�cA BOLOOIRGrlD-
Ik C1w retlauract�';sierhod ��
- —
fn��F-(�YC'iN�rd LI1.1�J EI13—�'Wg!leSJIrootrrccult'?
Phi wasNodfTrd ly phortcl gnad f face-ts-fare (eir'c'!e nrjr).
Yes No { NA �" f.� the co""MCLUjal 00tlfifr's paCH919 slip aMfAied to #Ills lbrarp
re prt� eT eu-stodypi-oc ur�cs D-el [IrdslT-d�rccei-d
+' sdr� s listen nn the CSC a��rl al!arnple tis
it s coilechall date & t1fisted on the COC and a]T
Nid rail uwainer Ial)ei infofT Tian {ID, date, tiurc) a'l
Virerc tests to he perfornaetl hblod nil tLe COC?
coivair'f
life. ooc?
+ I cs []ND 19, Did:all samp'r:s arF vr-iu tLte (}foijer cwnjllu�i for cach [csr atad+ur W A0-bd coniliti-on
xMbmkem lids uiL erc,)?
H
110T 1Was adequate lLur.l V11 No J2. Yece all salatpk-5 received'A Ahin �s dic holding tu>ue Ur 4R IMIM, wluc?e€yeT Conley
!w yce QNO 13- Wl "Lr 4 satin LS contliners acccttoacd fX7 (NO it>fssin exc )
EVe5 QNo �1 14' Wzzc LrOA, 8DI5C aW,RSIC-175 sNo[ples Mttc 01 Udihle r' e0 ;zti'a {'•a'•aa" 6lllli[ i�r
disrrj i a[ry ❑thy 4'[4 �+1E�5'?
rrs il4a ,/ @Y:�L 15- VVerc all D1Z(ji tal iauEriegt saL les [ettived r[ a pit of k= ?
des No 4 l6. erc al l c aside s des roccived �t a ]d silIftde a01 Ies rmeive at [i PH ---I-
El E] IZNA 17_ LVere At'P ;� le i�l r cya Qid l enoY A5.1/608.3 (< .S T.) tics ut
esidrzal chlorirrc'?
CYCS LJ Na I ❑T4A 18- W'LS the quote ❑mober tared on tlzc(Mlahier labci? 2ye-S, 577
�xrople Presrr3'tt�orr ,3laa5t17[ Cottijalcle # 'sArnplfi(3] ina3l�rrtl} Qre9erv+ar t1t11llGadslkCe-)
wlac feccivcd iDCOrrk�ct1ypre9erved arul lvu-e ad llsr{ �arc��x i:itiel '
ns�unp�e ircr;iviug'�vi4-A ;a7 -OfCi Vlc Due- M504, HNG3, Ma, Na[}IJ Minh SR 4'. ___
f5uae fafpreser� #ion '' iCincnee tiros wie p�reser4fiti a is tlee[led, lcsfse uO ua tile. ❑otufnenrs be -low-
',om„I.dPI t+L4
_1Vm'1Nei%'cd witli 1}ubhies>4 rxiiri in diE[taaetcr,
�' d]11p�2S S 7Si� welt~ LCiCivw Wlttl "'KC > 0.5'T*r[., (it # 19 1s tilt) anq Weft
djrssted acoordirMglyirx sMLUpie recej�iug Will) sodit) r]_
riosnlfatc L2�;,03) wide Uai ID; �!"L
Ovmi#lax lt#: 563fia Pace- Oana ytical5erjires, LLB
Page
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (6700 x 1.5400) = 100 = 103.18
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (12000 x 1.5400) = 100 = 184.8
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3600 x 1.5400) = 100 = 55.44
Na meq = Na mg/I = Molec.Wgt.Na = 103.18 = 23 = 4.48609
Ca meq = Ca mg/I = Molec.Wgt.Ca = 184.8 = 20 = 9.24
Mg meq = Mg mg/I = Molec.Wgt.Mg = 55.44 = 12 = 4.62
Sample Date Report Range Ratio
10/4/2022 10/1 /2022 - 1.7041
12/31 /2022
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.48609 = SgrRoot[0.5(9.24+4.62)] = 1.70412

SECTION 3

N
CL
2
v
o
CL
2
0)
CL
q.
a)
>
Ev)
m
a
a)
z
x
4)
<
Z
<rn
0
z
c
E
N
0
0
Q
m
M
-
0
E
2
-db
6
0
t-
E
!
clCl)
z
0
Zx
m
CD.
0
--ab
CD
E
c�V)
LO
12
(D
N
----------
-------- ------
-
0
2
1
1')
Lq
ca
m
0
.N
fL
.2
7U
o
ir
cc
ill
F-
2
.
w
0❑
<
0
❑
fl
CS
o
6
U)
0
D
CD
0
CD
0
0
0
0
E
O
C
0
r
I
ci
0
kn
0
N
9
0
.0
(D
2 rr
a) 0)
I -E
c c
< :a 8
z M (D
0
C) -J
too cm:
ca.
E
o o
PIT
CL
<
0)
E
w
c E
.0
CL
Id
_j
n
c
0
.2
o
0
e-
0
0
C)
Of
z
CL
IL
<
0
o &
0
z
13 0
c
U-
0
.2
w
z
"E
z
CD_
aci
a)
(1) o bi
't 4:-
0 (D
CL
O
N
z
-6

LL
rn
c
0
CL
0
0
0
f
0
E
Z�
C13
IDO
I
z
0
U)
U)
CL
CL
U)
0
w
Of
(D
�t�����nn0o
IIIIIIIIIII
En
cli
cn
'o
0
0
C�
I,,:
A
C�
C�
.
C',
F-
0
0
0
0
0
0
0
a
0
0
0
0
o
0
o
o
o
C3
o
a
a
0
CD
0
a
0
0
0
0
0
a
0
0
0
a
CD
0
C)
0
0
o
0
d
0
0
0
O
a
0
C)
0
0
0
0
0
0
0
0
C)
C>
C>
qOqq00oqqqq
0
0
0
0
CD
0
a
0
0
C)
0
0
0
0
0
0
0
0
CD
0
0
O
0
0
0
0
0
0
0
0
0
0
CD
C>C>CDCDOOOOCDOC)
0
0
0
0
o
O
d
a
q
0
0
0
0
0
0
CD
0
C,
rn
0
0
0
a
0
a
0
0
0
0
0
co
0
oc)oOOOOOCD
0
0
0
0
0
0
0
0
0
08
CD
O
q
O
a
d
O
q
a
q
q
0
C>
C)
0
0
0
a
0
0
0
0
r-
0
0
0
0
0
0
0
a
0
0
0
0
qqqqqOOOq
0
0
0
0
0
0
0
0
0
08
0
0
a
0
0
0
0
0
0
0
ci
O
0
CD
0
0
0
0
0
a
a
0
CD
0
CD
CD
0
0
0
CD
0
CD
o
a
O
a
q
0
q
a
o
0
q
0
0
0
0
0
0
0
0
0
0C)0C>oOoa
oo,:,
0
O
0
O
0
0
OO
O
O
O
O
0
0
C)
o
0
o
o
0
0
o
0
0
o
0
0
0
0
0
0
0
0
0
0
0
0
0
C)
0
a
a
0
0
O
0
cL
CL
0
LH
(D
E
CL
0
CL
E2
'a
0
2
m
F4
so_-
(n
mi
CL
C/)
-a
L
O.
O
O
0
� IV -.'

CL
t� a.
E
0
N
2
2
'b
E
LL
LL
LL
co
z
f2
cli
o
CL
2
CL
b
Z
M
00
<
0
r
IR
0
Cl)
C)
C)
Z
E
co
0
0
a
6
ci
0
E
c
o
E
c!
0
0
c
z
1)
0
0 .
C�
o
C�
0
E
':�
0
C
Cl
:�
Lo
m)
c
0,
0
0
Ci
C3
Ci
0
1�
a
0
0
m
o
-r-
X
D
M
D
CL
U)
U)
vi
rL
N
U)
in
0
0
C)
0
<
<
<
q
Cq
o
2
-d
v)
C?
cn
0?
Ir
M
n
Cj
N
'
C5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
CD
(C�
C�
R
0
0)
Lo
tn
m
us
C11
N
N
c
0
0
R
C-4
o
i2l
(0
U-
0
LL
x
z
LU
0
Al

�tnn��n��n
IIIIIIIIIII
N
W
try
0
co
P-
w
N
0
(a
0
OWD
CNN
LVOO)
CD
to
r-
0
C�
C�
0
C5
0
N
0
O
0
0
0
0
0
0
C)
0
0
0
0
0
0
0
0
0
0
0
0
a
a
0
0
0
0
a
O
O
4
O
O
q
q
q
q
O
q
0
C)
C)
0
0
0
0
0
0
a
0
O
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a
0
0
0
0
0
O
0
0
0
0
0
0
0
0
0
0
0
C�
C)
qqq
C)
0
0
c�C�
CD
0
O
0
O
0
O
0
CD
0
O
o
m
CD
o
o
o
o
o
O
CDO0000C)OCCO
C)
O
CD
O
CD
q
0
q
0
q
C)
q
0
O
0
q
CD
C�
0
q
0
q
0
CD
CD
a
0
0
0
0
a
0
0
rn
0
0
o
0
0
0
0
0
o
0
0
0
0
0
0
0
0
0
<D
a
0
0
q
q
q
q
q
q
q
q
C)
0
0
O
0
0
CD
a
0
0
0
0
0
0
0
O
O
O
d
q
q
O
O
q
O
q
0
0
0
0
0
0
0
0
0
CD
0
a
0044C!q4000q
0
0
0
CD
CD
0
0
0
CD
0
0
0
0
CD
a
0
0
0
0
0
0
0
0
CD
0
0
0
0
0
0
0
0
CD
(D
a
CD
0
0
0
0
0
0
0
q
q
O
q
O
q
q
q
q
p
q
0
0
0
0
0
0
0
p
O
0
C,
to
I
I
I
I
0
O
C,
0
0
C)
0
0
0
0
0
q
0
q
0
O
0
q
0
q
10
q
CD
C,
0
q
0
a
0
0
0
0
0
0
a
O
0
L
0
0
0
0
0
0
O
O
0
0
O
0
O
0
q
0
O
a
CR
0
q
0
O
0
q
0
q
0
q
0
O
0
0
0
0
0
0
a
a
0
0
0
0
LO
m
0
m
N
0
0
m
LU
-'d-
o
a
C)
N
0
-4:
CD
q
N
q
-g-
q
N
0
10
cn
�o
N
m
0
m
"t
m
10
4
q
0
q
Z
q
m
C,�
CD
q
N
C�
N
0
N
q
't
47
10
0
.
0
0
L3
E
2
0
<
—
E
E
E
2
cL
0
-a
2
-0
2c
<U
U
0
ch

(D
N
0
2
CL
<
o
2
Z
E
u
o
LL
tL
0
w
Z
a)
w
z
w
N
2CL
P
w
<
co
N
Z
N
C4
0
w
U)
w
w
a.
<
o
M
r-:
0)
N0
x
<
= L)
C)
x
w
z
0
E
a)
2
Y
O
ocn
0
0
E
:t--
c!
Cli
<
Z
m
0)
4
O
9
0
0
0
0
0
0
0E8
FY
C�
Ci
0
m
0
O
<
CD
LLJ
2
LO
I,-
Z()
<
z z
, 2N
m
CO
W
0
0 .
0 .
w
t:
U)
L4
0
Z)
D
CL
O
cn
U)
C'I
U
w
0
N
0
co
w
w
to
X
LU
NIL
o
a-
<o
W
0
O
Z
0 2
❑
0
U) <
C,
Z
wO
0
-2
0
W
<
w
CL
:)
Q
0
a)
cn
m
Z
z
w
x 0-1
<
a.
0
r-
(0
C�
0
❑
C
0
o
o
m
U�
U)
N
E
z
>:
U)
LIL
i
(D
—
=
-
7-J
0
z
EE
(n >-
(D <
0)
0
y
r-
0
0
0 0
0 0
CD
0
0
Z f
(0
0
=
—
I .
0 0
.
0
.
a
Z
w
m Z)
m
a)
3:
0
0 10
0
C�
0
C�
D
0
0
w
U) 0
(D U)
W
o
E
<
cn co
—
c,)
-
m
r>
E
w I
L)
. I
W
CD
W I
of
, .
of
. ,
(D W
Z)
0
LLI
i� :2
(n
q
N
Z
z
<
0 Z
,
<
N NN0
0 N
N
-
N
D
7�6
0
z
ui 0
w
-141
M X
wx
o L)
0
CL

N
0
M
0
0
E
m
Z.
LU
0
O
ti
-7-
1111111111111
11111111111111
1111111111111
111111111111
1111111111111
111111111111
1111111111111
1111111111111
111111111111
1111111111111
11111111111111
111111110101
IIIIIIIIIII
G
,
C)
" N
N
C)
�;
m
N
�D
0)
C�
C�
C>
C�
0
0
0
0
O
C>
C!
0
OO
0
0
OO
0
0
O
0
0
0
0
0
0
C)
0
0
0
0
a
0
0
C,
00000000000
q
q
q
q
q
C�
C�
q
q
q
q
O
0
0
0
0
a
0
0
0
0
0
C)C:�Oc)oc�00000
0
0
0
0
0
0
0
0
0
0
0
C>
O
q
q
O
o
O
0
0
0
CD
0
0
0
0
0
o
o
O
0
Cl
0
CD
0
0
0
a
0
a
0
o
0
O
C,
R
o0
q
0
CR
0
q
0
O
0
O
0
O
0
o
0
O
0
0
C)
C>
0
C>
C>
CD
C)
CD
C)
O
C)
0
0
0
0
CD
0
0
0
0
0
C,C,
0
C,
.
00
q
q
a
0
ooc>O(Do
CR
C�
q
C�
q
C�
O
0
o
C)
.
0
0
0
o
a
o
0
0
C)
0
0
0
0
0
a
0
0
0
0
q
0
o
0
R
0
q
0
q
a
O
0
R
0
q
0
R
0
q
0
R
0
a
a
0
a
0
0
(D
0
0
0
0
0
0
0
0
0
0
0
a
0
a
0
OqORqqORORq
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a
a
10 1
1
1
0
0
0
CD
0
0
0
0
a
0
0
0
0
00
0
0
0CR
0
CD
CR
a
q
0
0
a
q
0
q
0
q
O
0
O
O
0
0
OCDOOOC)OCDOOO
oc�0000000
C�
C�
CR
q
0.
CD,
0
R
0
00
0
0
0
0
0
0
a
0
0
C)
oc)Ooco0O000
0
R
0
0
0
0
0
CR
CD
q
0
q
0
q
0
0
0
q
0
0
0
q
Cl
C>
0
0
a
0
0
0
0
0
0
cn
-i
0
'tO
2
00
LO
LO
m
w
N
�
0
C)
0
co
0
0
6
C)
ci
N
C5
7
o
q
o
CD
q
o
CS
q
0
O
V�
rl-
LO
w
m
LO
w
<
07
^
O
o
q
r-
q
Ln
c�
q
N
q
N
q
N
q
t--
to
q
o
o
c3
o
I
o
o
o
o
lo
I
Lj
o
E
E
i>,
--
E
>
c
=
,
o
aso
Z
z,
U4
E
m
-a
o
cL
E2
--
0
-
4)
CD
-a
-6
=
cn
�L
.
2�
CL
<
F-
o
2Fo-
V)

CL
CL
0
2
2
Im a
CL
C.
<
m
u
>
0
'o
.z
Z
Eao)
b
u-LLU-
'o
0
cc
z
a)
w
F-
z
CL
W2
w
<
u
D
w
CL
U)
w",
Z
<
Lu
w
(D CL
Z 0
o
rn
< X
3
NN
<
<
S L)
WC)
o
C)
Z
O
Z
cm
O O
N cj
O
C'I
a
L)
ca
E
0)
m
CD 0
0
0
E
0)
2
y6
m
ci
5n 6n
6
c
E
E
n
<
O
O
o
0
C)
Cc,
E
c c�
m
c�
m
9
w
LO Lm o
LO
Z Z
CN
0 0
0
WW
0
c
0
0 O
0
F-
cr
I—
U3
U
18
6 6
6
.0
16
'0
fr x
w
,2
CL
w
N
ID
0
CD
U
CL
06
w
O
Ww
rr
W
CD
<
0
0
o o
o
O
Z
0
o
<
F--
IL
Z
w
<
0y
0
< <
Z
a.
W 0
cr
z
x
<
0
❑
C)
C?
M
'6
E
.2
0
z
>:
U)
0
Z
cn
Z
(D
U)0
h
0 0
o
0
0
n
w
Z w
U
6 6
0 CD
C� Iq
CD
0
0z
0
C�
OzU)
0
E
V�
0
w
w
o
m w
oo
Z LL
0 ..
2
W
0
<
W
5
U)
C14 CN
N
Z
z
<
0 Z
8
04 N
N
N
o
Z
w U
0
U)❑
:E
� CD
2z
<
m
co
W_3
0
fil

0
a2
LU
0
77
O
(D
(n
is O
r
E
0
rx
12
C
0 U,
LU
LO z
c 0
0
z
0
Z
m
rl
x
ui
r
2
O
co
0
0
0
17
11
iI
0
OR
-r-
IIIIIIIIIII
o
0cq
Ci
q
q
CO
0
0
ci
m
0
000qqq000oq
C)
0
0
0
0
C)
0
0
0
0
0
0
0
0
0
(D
0
0
0
0
0
a
0
C)
0
0
0
a
C)
C)
0
0
0
0
0CDCD
OOOO
C�
0
CD
0
0
0
a
CD
C)
0
0
0
CD
CD
0
0
O
CD
0
0
a
C)
O
0
R
CD
q
CD
R
0
q
0
q
CD
q
0
q
0
O
CD
q
0
O
C)
q
0
0
0
0
0
0
CD
C)
0
0
0
O
0000<Dc>ooc:)OCD
q
R
0
q
0
0
0
0
0
R
q
0
0
0
0
0
0
0
0
0
0
CD
rn
O
0
CD
0
0
0
0
0
0
0
0
C)
0
0
0
0
C>
0
0
0
0
0
co
O
0
C)
0
0
0
0
0
0
0
0
q
0
q
0
C�
0
q
0
q
C)
C�
0
C�
a
C�
C,
q
co�
cq:>
00000C)OCCDOCD
C:>Oc)c>0000000
0
O
0
q
0
0
0
0
0
CD
0
0
0
S
co
0
C)
0
0
q
q
0
0
0
0 0
0
0
0
qqOOOqOqq
00
0
o
0
CD
o
0
0
0
0
C)
0
0
0
0
C�
q
q
0
q
0
q
0
q
0
q
0
C�
0
C)
0
0
a
0
0
0
0
0
co
01
-
-
q
q
q
q
q
C�
CR
q
q
q
0
0
0
0
0
0
0
I
I
-
c-
m
m
w
w
N
N
q
O
(I
O
O
q
R
O
cl
co
2
o
E
E
E
.2
E,
L)
Ow
_ia
-a
<
ca
o
W
Fp-
r
w
r

11
CL
2
0
V;
2CL
JLI
w
U)
U)
E
(D
0
2
U-
U-
U-
m
T
z
Q�
(D
z
cn
m
2
m
cm?
'0
cq
cn
CQ
Im
0
0
C)
0
0
z
E
C\!
q
C'�
ro
c
CD
o
0
c
0
(D
"1
m
O
O
O
E
2
CD
E
c!
c!
<
Z
0)
0)
0)
0
0
0
m
Z
c�
o0
E
0
0
o
=
o
C�
0
c!
c!
caO
0
0
co
.0
'a)
m
m
>
=N
a
'0
Z)
D
.2-
0
v
a-
U)
Cl)
in
c
a
0
0
0
J
_j
_j
0
<
<
F
❑
O
-6
0
Lq
C)
Lq
0
U �
c
72
0
0
c
0
0
a
0
cc
6
00
C)
CM,
C;
0
-
'-,t)
T
LCOI
0
E
Lo
4
N
Cq
(N
cc
-'a
5,3
ca
❑
2�1
NZ4
N
C" i
0
1411.5
ce)

tli
A
E
tA
CD
C�
Ln
�g
�an���nn�
IIIIIIIIIII
16
O
o
O
o
O
o
1
0
o
Ci
rn
1
O
0
0
0
0
0
0
CD
0
0
LO
O
O
O
d
O
d
O
a
C)
0
0
0
C)
0
C)
0
0
a
0
0
0
0
0
a
0
a
0
a
CD
0
C)
0
0
O
0
d
0
q
0
q
C)
q
0
q
0
q
0
O
0
C)
0
0
C)
0
0
0
oc)CDOOCDOOOcc)
q
O
O
O
O
O
O
q
O
O
q
C)O000OClm
occ,
oc,
C>CDOOC>CDOO
qc�qq0C)0000=
C�
C�
q
o
o
0
o
O
O
O
O
C)
0
0
rn
0
C)
0
0
a
0
0
0
0
0
CD
0
q
CD
0
0
0
0
0
q
0
q
0
q
0
q
0
a
CD
o
co
0
C>
0
0
0
0
0
0
0
0
0
0
O
CD
0
O
a
q
0
d
0
q
0
q
0
O
0
q
0
q
0
q
0
0
0
0
0
a
0
a
o
0
q
0
0
o
q
0
o
to
o
q
q
o
O
q
0
0
0
0
0
0
a
0
0
0
0
Lo
c)
o
o
o
cD
o
o
o
o
o
qq00qqqqoq0
o
o
o
o
o
o
o
o
o
o
o
cD
o
o
o
c)
o
o
a
o
0
tt
o
o
c)
o
o
o
o
a
o
c
a
o
o
o
o
o
o
o
o
o
q
o
q
o
o
o
q
q
o
o
c
o
o
o
O
cD
o
a
o
o
o
o
o
o
o
o
o
o
O
o
o
o
q
o
o
O
o
q
o
q
O
q
n
q
o
q
o
0
o
q
o
q
o
O
o
o
o
o
o
o
_j
0
co
Lo
m
to
co
ul
0
cr)
co
o
o
o
o
<
0
q
E
2
E
cL
U4
ID
E
c-,
E
ro
8'
o
cL
E2
V
o
2
u)
cL
<
m
L)
Q)
a.
F
o
cl)
40.
co
9 r-- .2 re - �, F

w
CL
N
2CL
F-
a
(ID
2
w
a
CL
3:
M
M
P
LL
U-
LL
co
(D
Z
_a
a)
2
a
CL
2
c,�,
0.�
c.'
cli
N
"i
`2
N
N
E
0
0
0
U
m
0
C>
0
Ecm
2
oc>
o
E
�L'
E
c!
n
Z
a
0
17!
0
0
0
E
c�
Cl)
'��!
m
R
m
LO
LO
LO
o
C,?
0
c!
0
c!
0
CD
6
75
o
o
o
>
U
co
c>
0
F-
❑
CD
c)
0
m
0
m
C?
C?
'n
N
N
N
(D
(D
0
CD
0
0
0
cc
m
cq
cli
0
LO
R
N
R
CN
a)
C',
CD
0
0
C',
o
!
ME

II
U
z
>;
i
0
z
Z)
0
Lu
co Z
o 0
0 z
0
O
-
i�
pk
O
LL
CO
.....
-
Cl)
CD
C)
Lo
M
N
N
tn
CO
C�
cl�
C�
q
I-
C�
0
0
0
C)
0
0
d.
C)
0
0
0
0
0
0
C)
0
0
0
0
q
0
q
0
q
0
0
0
q
0
O
0
q
0
q
0
q
0
q
0
0
0
0
0
0
0
0
0
0
C>
a
0
CD
0
0
0
0
0
0
0
0
0
0
0
0
0
C>
0
0
0
0
0
0
0
0
0
0
0
0
0
q
O
0
0
O
O
O
a
0
C>
0
0
0
0
0
0
0
C)
00
0
00
CD
0
CD
CD
0
o
0
C>
0
0
00
0
C,
O
0
qqqc�c�qc>000qq
0
0
0
0
0
0
0
0
Cc)
o
o
o
C)
o
o
6
C5
6
C.
CD
O
0
0
0
0
0
0
0
0
0
0
a
0
0
0
C>
0
0
0
0
0
0
0
a
0
00
0
0
0
0
0
0
0
0
0
0
0
0
0
0
CD
0
0
0
0
0
0
0
00
0
0
0
r-
O
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a
0
o
0
0
0
0
0
0
q
CR
q
co
00000000
0
OCD
OCDOOCOCDC)
q
q
q
CR
q
q
o
C�
C,
q
oq
00
00
0
0
0
CD
0
0
0
0
U�
I I
I
0
0
0
0
0
0
0
0
a
0
0
0
o
0
0
0
0
0
0
a
0
0
CD
0
a
q
0
q
0
0
0
0
0
0
a
0
C>
0
0
0
0
0
0
0
0
0
a
0
0
0
0
co
0
C.
0
0
0
0
0
a
0
0
0
0
0
0
0
0
CR
0
(�
q 0
0 q
q 0
0
0
a
0
6
0
LLI
0
CD
0
0
0
V5
'r
E
2
E
:1
0
CL
a
0
m
CL
'a
L)
-2j)
2,
<
0
(n
O

0
E
0 9
N
a)
Q
OO
2
. o
CL
Fn
,
m
2
a)
a)
u)
(n
0
LL
LL
LL
ELL
z
x
A)
<
Z<
CL
o
I,,:
m
m
Coo
—1'-
(6
t6
C6
(D
a)
a
0
E
N
N
N
E
2
m
o
o
o
o
=
E
n
n
n
Cli
Z
m
m
m
of
z
o
o
o
E
':7�
Oh
c::!
o
o
o
c
a
co
o
0
0
0
0
w
w
W
W
o
<
<
<
<
Lo
lo
LO
O
Lq
Lq
Lq
o
o
cc
L'?
c
'o
ll�
om
ol
N
oF
co
o
Lcol
l
;o:
N
N
N
N
O
oo
O
o
m
4)
O
ci
7i 0
I
L
L
5
0
o
C7
a)
z
U)
tf
0
cl
(D
of o o
z co
II U
CL o
z < >

67
U)
O
-5.
S
E
0
CL
CL
< iL
U,
c
0
0
m cn
CD UJ
Ln z
a 0
0
c
z
0
m
O.
m
x
LU
c L:
4)
2 a
0
O
O
to
0
AF
tnn��auo0
11111911111
-
C�
-
r�
C-
i
-
C
-
CD
Lo
o
C5
0
0
o
o
0
6
6
6
0
CD
0
0
0
0
0
0
0
0
0
0
qqqqOOqOqOq
0
0
0
0
0
0
a
oa
C>
0
0
0
a
0
0
C>
0
a
0
0
N
C>
a
0
0
0
0
0
0
0
0
0
0
R
0
q
0
q
0
q
0
q
0
q
C)
q
0
q
0
q
0
q
O
q
0
0
0
0
0
0
C)
0
a
0
0
0
0
0
0
a
0
0
0
0
0
0
000000C)OOOC>
Oqqo0odq000
o
0
C)
o
O
0
R
C)
R
0
q
CD
O
0
q
0
q
0
O
0
q
0
R
0
R
C)
q
0
0
0
0
0
0
0
0
0
0
0
rn
0
0
0
a
0
0
0
0
0
0
0
0
0
0
CD
0
O
0
0
0
0
0
C)
0
00
0
0
0
0
0
0
0
0
0
0
0
0
R
0
R
0
R
0
q
0
q
0
R
C)
d
0
C�
0
q
0
R
C)
q
0
0
0
0
0
a
a0
0
0
CD
0
0
0
0
0
0
C)
a
0
0
0
0
0
C�
0
C>
C)
C3
.
0
Ci
0
q
1
0
0
C;
C
0
a
0
0
O
0
0
a
0
0
0
0
0
0
0
00000000qqq
0
0
0
0
0
0
0
0
0
C>
0
0
0
0
0
0
0
0
0
0
C)
o
o
o
o
o
o
o
o
o
o
o
o
O
o
q
o
O
o
O
o
O
o
O
o
q
c
O
a
O
o
O
o
R
o
o
o
o
a
o
a
a
o
o
o
o
o
o
o
o
o
o
o
o
o
o
o
0oaqqO00000
o
o
c
o
o
o
o
o
c
a
o
o
o
a
o
o
O
o
o
o
o
a
o
o
o
o
o
o
o
o
o
o
a
o
't
g
-t
m
I
N
r--
o
m
m
LU
'r
O
<
O
o
o
a
2
,3
o
4)
O
V
E
GAE
2
O
. 2
77D
Lq
ID
ca
E
M
o
2
-0
cL
<
U
<
C)
U
o
to
7o
L
o
CD
O CD
C11
LL
V LL
7;
0
ctl LL
GJ z
ar
0
Q cd

N
CL
c
o
cl
CL o.
c
L9
0)
o
U)
U)
to
z
E
LL
LL
(6
O
0
m
z
�o ,
N
0-
ui z
N
0)
2
b
N
U) (n ui N
Z
Lu w
CD a<
Z 0
a.
o0
cr
(D
wN
o
o
z
0
z
O
E
E
0
E
E
<
a
o
0
ZY
o
o
C',
E
4c
0 �L
F-
<
z z
z
C?
W
ui !z
FL U)
'a
...............
.0
W
.N
*0
i4
6
6
c
0
o
W
U)
(D
.2-
C-4
—C4
Lo
ui
m
m w
�o Q.-j
a.
C]f
W
0
Q)
o <
om
oz)
o
<
a.
Z
C)
<
75
1
2
cr -j
w <
cG
0
N
0=,
W
<
X
W
<
X
CL Z)
z
0 (L
ui 0
W
C, z
of X
<
0-
�2
0
00
6
m
C5
O
0
725
0
co
0?
0
c)
Cl
C,4
O
z
(D
(D
0
0 Lu
Z
<
Q)
U)
0
0
0
CD
0 CD
0
0
U) m
W0
m
CD
0
Z
Z UJ
0
0
0 �
oc
0
C�
0
0 z
U)
W
o
< E
LO
m
N
cs o
>- w
Z
o
F-
LL
�
2
Llj
0
. ..................
< W
CO
Z z
0 Z
<
a
0
0
0
z
w 0
n
cn
2
0
cq
Q
00
<
CL X
w
LL
0 0
cr
Im
LO
= 0
U) (D
0
Z
4) 0 0)
CU
0
CL
C
bA
2
1:2
0
0
EL -6
z < >
LL
U)
LL
:E
Of
0
cr
z

w
m
C
E
0
0
0
W
Ln z
c 0
0
z
0
CL
am
Of
c
x
w
.2
LL
O
Ll
MA
0
IR
co
IIIIIIIIIII
C�
0
C�
-It
li
0
C�
N
q
N
q
N
C�
N
U�
o
o
o
o
c)
o
o
o
Lo
c1l
o
000c:,oc)cD0000
R
oc)c>cDooc>acoo
o
q
o
q
o
q
o
q
o
q
o
q
o
O
o
O
o
q
o
q
o
q
o
o
R
o
o
R
o
o
q
a
R
o
R
a
q
o
O
a
o
o
o
C)
oc>oc>ocD0000cD
q
occc:>666666cs
c
q
o
q
o
q
o
q
cD
q
o
q
o
o
o
0
o
0
o
0
000cDOC>O0000
q
o
q
o
O
o
O
o
o
o
O
0
q
o
O
o
q
o
-
o
-
o
co
o
o
R
o
o
o
q
o
o
o
q
o
o
o
o
o
a
Cl
q
o
o
o
q
o
a
o
q
a
cD
a
o
c
a
a
q
o
cl
o
o
6
o
o
o
6
ti
o
0
o
o
q
o
o
IR
cD
cD
o
o
o
q
o
o
q
o
o
o
q
o
o
o
q
o
o
a
0
o
o
o
R
o
o
a
0
o
to
o
OocDcDooc000cD
o
0
0
o
cD
0
o
0
cD
o
o
c)
o
000000cDoa
qq0qq00qq
o
o
o
o
o
o
o
o
o
o
o
o
o
o
o
o
o
o
So
ES
6
o
6
o
o
O
o
c
0
o
o
0
c
o
o
q
c)
o
c
o.
o
o
S
o.
o
o0
0
q
o
o
0
o
c
o
00
a
o
o
o
0
o
0o
o
co
o
o
o
o
o
c
o
o
o
o
o
o
c
o
o
o
o
o
c
o
cD
o
o
o
o
o
0
o
0
o
0
0
o
cD
0
0
o
0
o
o
c)
0
0
-
o
0
0
-
o
0
o
-
o
cl
o
o
LUCS
m
<t
m
et
t-
B
N
r-
c\l
co
N
cc
N
cn
o
o
o
o
a
o
Lo
ID
E
E
E
E
>
Lq
E
c L
o
coL
o
a
cn
Cc a
cL
o
2
o
co
r4
2

SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
January 19, 2022
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Mt Holly - REVISED
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22010180
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/5/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 36

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„NQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010180
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/19/2022
CLIENT: Synagro
Project: Mt Holly - REVISED
WorkOrder Narrative:
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
22010180-OOIA MTL-TCLP-7(6010D): LCS-54221 exhibits high recovery for Silver. Sample is ND
for this analyte.
22010180-OOIA TCLP-SVOC_8270E: CCV exhibits high recovery for Hexachlorobutadiene. Sample
is ND for this analyte. Possible low bias for Pyridine due to low recovery in CCV. Compound
demonstrated adequate instrument sensitivity in RLC.
REVISED REPORT 1/19/22: Revised report includes revised report format to include MDL.
REVISED REPORT (II) 1/19/22: Revised report includes revised report format and lower
Revision Q
Page 2 of 36

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� Wo#: 22010180
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 1/19/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision v2
Page 3 of 36

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO WULES, JNGG Cuyahoga Falls, Ohio 44223
Analytical Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Mt Holly - REVISED
Lab SampleID Client Sample ID
22010180-001 Mt Holly
Tag No Date Collected
1/4/2022 12:00:00 PM
Workorder
Sample Summary
WO#: 22010180
l9 Jan-22
Date Received Matrix
1/5/2022 12:50:00 PM Sludge
Page 4 of 36

N
A
Or
a
z
OW
E*
co
0
m
m
ca
a_

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 22010180
Date Reported: 1/19/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2022 12:00:00 PM
Lab ID: 22010180-OOIA
Project: Mt Holly - REVISED
Client Sample ID Mt Holly
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
88.5
Surr: Phenol-d6
90.4
Surr: Nitrobenzene-d5
68.7
Surr: 2,4,6-Tribromophenol
107
Surr: 2-Fluorobiphenyl
71.1
Surr: p-Terphenyl-d14
109
SW7470A SW7470A Analyst: KLC
0.00200 mg/L 1 1/7/2022 5:13:00 PM
SW6010 SW301OA Analyst: MSK
0.500
mg/L
1
1/10/2022 11:39:00
AM
5.00
mg/L
1
1/10/2022 11:39:00
AM
0.100
mg/L
1
1/10/2022 11:39:00
AM
0.200
mg/L
1
1/10/2022 11:39:00
AM
0.500
mg/L
1
1/10/2022 11:39:00
AM
0.0500
mg/L
1
1/10/2022 11:39:00
AM
0.500
QL+ mg/L
1
1/10/2022 11:39:00
AM
SW8270 SW351OC Analyst: SFG
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.250
mg/L
5
1/13/2022 4:59:00 PM
0.125
QC+ mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
mg/L
5
1/13/2022 4:59:00 PM
0.125
QC- mg/L
5
1/13/2022 4:59:00 PM
10 - 157
%Rec
5
1/13/2022 4:59:00 PM
10 - 169
%Rec
5
1/13/2022 4:59:00 PM
32.1 - 130
%Rec
5
1/13/2022 4:59:00 PM
45.4 - 166
%Rec
5
1/13/2022 4:59:00 PM
35.7 - 130
%Rec
5
1/13/2022 4:59:00 PM
70 - 145
%Rec
5
1/13/2022 4:59:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG I
PL Permit Limit Revision v2
RL Reporting Detection Limit
Page 6 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 22010180
Date Reported: 1/19/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2022 12:00:00 PM
Lab ID: 22010180-OOIA
Project: Mt Holly - REVISED
Client Sample ID Mt Holly
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
78.0
Surr: DCB
83.3
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 97.5
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
96.7
Surr: Di brom ofl uorom ethane
101
Surr: Toluene-d8
101
SW8081 SW351OC Analyst: CSS
0.0250
mg/L
10
1/14/2022 12:17:00 AM
0.0500
mg/L
10
1/14/2022 12:17:00 AM
0.00500
mg/L
10
1/14/2022 12:17:00 AM
0.00500
mg/L
10
1/14/2022 12:17:00 AM
0.00500
mg/L
10
1/14/2022 12:17:00 AM
0.00500
mg/L
10
1/14/2022 12:17:00 AM
0.00500
mg/L
10
1/14/2022 12:17:00 AM
10 - 119
%Rec
10
1/14/2022 12:17:00 AM
10 - 119
%Rec
10
1/14/2022 12:17:00 AM
S W 8321
Analyst: RIS
0.500
mg/L
50
1/12/2022 1:12:00 AM
0.500
mg/L
50
1/12/2022 1:12:00 AM
70 - 130
%Rec
50
1/12/2022 1:12:00 AM
SW8260
SW1311M Analyst: NAW
0.250
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
5.00
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
2.50
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
0.250
mg/L
50
1/7/2022 3:55:00 PM
0.100
mg/L
50
1/7/2022 3:55:00 PM
70 - 130
%Rec
50
1/7/2022 3:55:00 PM
70 - 130
%Rec
50
1/7/2022 3:55:00 PM
70 - 130
%Rec
50
1/7/2022 3:55:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG I
PL Permit Limit Revision v2
RL Reporting Detection Limit
Page 7 of 36

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralorfas TEL: [phone] FAX.- [phone] WO#: 22010180
Website: http://www.settek.com Date Reported: 1/19/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2022 12:00:00 PM
Lab ID: 22010180-OOIA
Project: Mt Holly - REVISED
Client Sample ID Mt Holly
Analyses Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.481 mg/Kg
1
1/10/2022 11:41:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: ALT
Ignitability nonflammable
mm/sec
1
1/7/2022 2:56:08 PM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH 6.9
s.u.@19.9C
1
1/7/20224:13:17 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1
1/10/2022 11:41:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG I
PL Permit Limit Revision v2
RL Reporting Detection Limit
Page 8 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010180
Wehsite: http://www.settek.com
19 Tan-22
Client: Synagro
State: NW
Project: Mt Holly - REVISED
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010180-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Version #5
Page 9 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010180
Wehsite: http://www.settek.com
19 Tan-22
Client: Synagro
State: NW
Project: Mt Holly - REVISED
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010180-OOIA Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Version #5
Page 10 of 36

0
0
N
Fi
c�
0
E
J
O d
M LOT ry
f� CDao to
to r)
M d
rK
z z
0-
of �
0
d
N N
00
N N
J
� � L
N N
C6 ) _
Q fn E
Q) 'N J
d T
� J
Q
U
W
0
J
E m
r >
M w
O � �
� Y
IL
U)
O
a co
co >
Y
H CO IL
0
U wIL
J
Ci
O O O
O O O
r- r- r-
LO N
C6 O O
rn
U') U') U')
0 0 6 o 0 0 0 0 0 0
U') U') —O l0 l0 L6 U0 U0 U0 N
0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 o 0 0
Z Z Z Z Z Z Z Z Z Z m `) `)
N L
00
N O p
00
00
o o 0
N N U O O N 22N
O O N OPQ O
0 0 a)m o O O o o v
U U N 00 O O U O U i i i
Q Q Y N Q O O U U) (n (n
N W a) (O L :EO
2 m 0 0 0 H H
N
F."
O
CO
M
O
r
a)
CD

m
CJ
E
J
N
Im a
LO 0�
M � a
Z Z o
c �
in
75
N
N _
O
N E
n J
� L
_D
O N =
cl cl
Q N
E .N 3
a '•
c J
Q
LU
U
J
E N
Uj M
� N Y
a
Cn
U
O O o
a co
� m
U ? Y
H N a-
o
70 Z
0
U (D J
U H a
(D a
N U
L
N
a
a .U.
E m
m Co
U
CO
Q
O
0
0
O o
o =_
N
Q O
fl >,
E o m
in U Q
CO�� � CO CO O O
� �
CO I- M N I- I- U) N V M I- U')
cli Uf Uf 6 O C(7 N 6 Or-� Ln, V
U') CO -,I-N M -,I-M N I- CY)
N CO N CO O CO V V O V N � O
O O O
O O O O O O O O O O
0 0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 0 0 0
�f7 N N N
0 0 0 0 0 0 0 0 0 0
N N Ln N N N N N N
O O O O O O O O
N CO0 co Z M NN Z � I- N I- U) ON O
�� CR� CR CR r— N N N
00 00 O O O O
Nco
L
C �
0 0
N O p O
��00
c c :
o m O c o 0
c
E E
N N N N O O N
O O C E O m
O O N O O N O V cl H
U U_ O O U O U
cl c Y N� O Oco
L T
U Cn Cn Cn
coo U U U P
m
c�
E
J
Cl) 0
Im a
LO 0�
M � a
Z Z o
c �
[if in
a
N
N _
O
N E
� J
� L
_D
N O =
c6 C6 _
cl cl
Q N E
.N 3a '•
c J
Q
LU
U
J
E N
y M
N Y
a
Cn
U
O O o
a co
� m
Y
H N q-
-0 Z
0
U (D J
al
H Cl
N N
L
N
a
a .U.
E m
m Co
U
0
CO
Q
O
0
0
O o
o =_
N
� � O
E o coin U Q
c�
0
a
N N N N
N N C�
O
c2 co O rn
rn rn o
6 0 0
O m �2
CO
CO I- m N
0 0 0 0
N N Ln N
O O O
CR CC) CR
O O O
M
4-
0
N
ca
0-

0
0
N
A
U
:C
a
N
N _
O
N
n J
� L
_D
O (U =
cl cl
Q U)E
E .N 3
a '•
c J
Q
U
W
J
E C6
y M
� N Y
a
CO
U
O O
a co
� m
Y
H N q-
Z
O
U J
H CJ
� a
N N Q)
L
(U
a
a .V.
E m
m Co
U
0
CO
Q
O
0
0
O o
o =_
N
4) N
E Q) m
Co n a
N N N N N N N N N
O O � O i�:� 0 0 0
Co N N C� C''J
O
O o Cj r- Oro r-
rn o) Cp Cp �
0 0 0 0 0
I- r- U) N V m I- U)
N CJ V 6 C6 N CA U� zi
N O m Cf) N I- N n O
m m �mmmr
0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0
N N N
0 0 0 0 0 0
N � N N N O
N
O O O O O
M Z M U') C V O C%J O
CR Z CR CR m r v U)
O O O O O N N N
Nco
L
C N
0 0
N O O Cp
o c o 0
) c E E
N N O O N
m c E o C m-o
Z2 Q) O 00 O V H
O
O O U O U
o
(6 L L U (n (n (n
U U U H H
N
0
a
M
4-
0
cr)
m
ca
0-

N
N
A
U
:C
75
CJ
E
J
L
a
Cl) to 0�
to Im
M � a
zo zo
c �
in
75
n
N N
N N
O E
n � J
� � L
_D
U N =
cl cl
a U E
E .N 3
a '•
c J
Q
LU
U
J
C1
E O_
M
N Y
a
CO
n
d
J O �
H cO >
Y
co a-
70 Z
0
U (D J
H CJ
N
v
00 Cl)
� a
0
o o
0- T
E o Flo
U Q
0 0 0 0 0 0 0
0 0 0 0 0 0 0
�t
O O O O O O
0 0 0 0 0 0 0
z z z z z z z
75
c�
E
J
O
a
to to 0�
to Im
M t a
zo zo
c 0-
� (n
75
n
N N
N N
O E
n J
� � L
_D
U N =
cl cl
a U) E
a` > 3
co J
Q
U
LU
O �
M
� � Y
a
n
d
J O Q)
cO >
Y
co
Z
0
U J
Q CJ
U v o
J L
U
a
a .U.
E m
m Co
U
N
N
J J
0
o o
0- C T
E o m
i/ U Q
O O O O O O O
O O O O O O O
O O O O O O O
O O O O O O O
O O O O O O O
O O O O O O O
N N N N N N N
0 0 0 0 0 0 0
0 0 0 0 0 0 0
O O O O O O
o z 7 7 7 7�
N z N N N N N
N
0
a
M
4-
0
m
co
0-

75
N N
N N
O E
n J
D
ib
0 0
a
E .N 3
a '•
c J
Q
U
u1
J
E O_
Ui O i
Cl)
� N Y
a
CO
n
d
J O �
H >
Y
m co a-
Z
0
U U J
H CJ
� a
coN Q)
L
N
a
a .U.
E m
m Co
U
CO
Q
O
0
Q1 U
n U,
o �
R
N m
47 N
E o m
i/ U Q
O O O O O O O
�2 �2 �2 �2 10 10 10
o N v m m v
rn rn� rn rn rn
O O O O O O O
N
O O
O
O O O O O O O
O O O O O O O
O O O O O O O
N N N N N N N
0 0 0 0 0 0 0
0 0 0 0 0 0 0
O O O O O O
N z� N N C) V
� U o
U U
Q m E = E
U 2 a 7 Q
E O O N
i N (6 L co N
Q co U U J cn c/)
a a a a a a a
J J J J J J J
U U U U U U U
75
E
J
a-
M t a
zo zo
c 0-
� CO
N N
N N
O E
D
0 0
a U E
` .55
>
a , 3
co J
Q
U
u1
J
O �
U O i
M
Cl) Y
a
n
d
J O Q)
H >
Y
m co a-
Z
0
U Q J
Q CJ
� a
�
N Q)
L
U
a
a .0
E m
m Co
U
0
CO
Q
O
0
Q1 U
n U,
o �
R
N m
6
47 N
Cl >,
E o m
i/5 E)Q
J
O
O
O
O
O
O O
N
N
N
N
N
N N
m o � m � v) 00
0
N O m N (Dr-
N I� O O O) V
O O O O O O O
�2 �2 �2 �2 �2 �2 �2
o- v v I- o co
6 N m uf7 V �
O m O O O m
O O O O O O O
CY) O
N
O O
O
O O O O O O O
O O O O O O O
O O O O O O O
N N N N N N N
0 0 0 0 0 0 0
0 0 0 0 0 0 0
O O O O O O
z m � coo, rn m
� U o
U U
Q m E = E
U 2 a 7 Q
E O -O N N
i N (6 L N N
Q co U U J Cl) c/)
a a a a a a a
J J J J J J J
U U U U U U U
N
0
M
4-
0
m
cu
0-

75
CJ
E
J
O a-
a
LO N
to Im
M CO d
zo zo
c zT
in
n
75
N N _
N N E
n n
D
ib
0 0
a
E .N 3
a '•
c J
Q
U
u1
a a
a O 5
_ v >
� N Y
a
a
J O (D
H� n co
2 CO a-
Z
0
U (D J
U H a
(D a
m N N
L
N
a
a .U.
E m
m Co
U
N
N
v
LO
00 Cl)
� a
U U
fl >,
E o m
i/ U Q
O
O
N
O
O
1.
ii
U
U
2
a
75
c�
E
J
a-
a
LO N
to Im
M CO d
zo zo
c zT
[If in
n
75
N N _
N N E
n n
D
ib
0 0
a
.N 3a '•
c J
Q
U
u1
a a
a O 5
_ v >
Cl) Y
a
a
J O �
H� n m
2 CO a-
-0 Z
0
U (D J
H CJ
� a
U v (D
Of
J to
U
a
a .U.
E m
m Co
CO
N
N
N
cb co
J J
47 N
0- >,
E o m
i/) U Q
O
O
0
co
O
O
co
CJ
E
J
a 0
LO N
to Im
M CO d
zo zo
c 0-
� CO
n
a
N N _
N N E
D
0 0
a
2 .N 3
a
c J
Q
U
u1
a a
a O 5
_ v >
n
� � Y
a
a
J O Q)
2 CO a-
Z
0
U Q) J
Q CJ
� a
y v Q)
to
U
a
a .0
E m
m Co
U
CO
Q
O
0
O1 U
n u,
o �
R
N m
L
47 N
E o m
i/) U Q
C1
CO
0
N
O
i1
co
CJ
E
J
Cn
LO N
to Im
M CO d
zo zo
c zT
in
n
Flo
N N _
N N E
D
co co
0 0
a U E
E .N 3
a '•
c J
Q
U
u1
a a
a O m
v >
y_ n
� N Y
a
a
J O (D
H� n co
(� Y
2 m �
Z
0
U � J
H CJ
� a
N N Q)
L
N
a
a .0
E m
m Co
U
0
CO
Q
O
0
O1 U
n u,
o �
R
N m
b
U U
Cl >,
E o m
i/ U Q
O
N
O
O
26
U
U
2
a
J
U
P
M
0
�
m
o
�
cu
�
O
U U
� �
0
•�
R.
o
0
�
3 �
�
C1
on
O
0
a
O
bO�A
>
O
+�.
O
O
�
U
N
o
�
�
O
�
q6�

�
kr,
§
\
_
u a
a)
= 5
cu
\ CO
�
«
k
q
o �
§ CO
( §
/ 7 ƒ
3 O k
§
f
%
\
�\
�

0
N
M
Fi
U
F�
U a
0
E
T r)
a_O LO ry
LO
coo to
to
r)
M d
rK
z z
0-
of �
0
N N
CD
N N
M M E
0 0
Q N
Q) 'N J
d T
� J
Q
U
W
J_
E m
LO
LO>
_ M
O � �
� Y
QI M
cm -Fo
m n �
O co >
Y
CO CO IL
aio Z
0
U J
m IL
Ci
N M �
N
a
iZ U
E cu
co CO
U)
N
LO
0
LO U
N 16
N CO
E N N
con C) a
U
0
O I- M Mzl- O M O O O LO O O M M
M L0 L0 L0 t M M M M M M CO l0 � M M
M M LO —— O N— V V 0 0 0 M U) V M
M M I-� N Ln — Cfl E O M ——— CO N M O
M V M LO N co M co N CO co
co M CO LO N M O M 0 M M CO V V N N co r-
0 CO CO O Cfl M O I- Lo I- M M O
r— CA N M O') CO co
O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O (D O O O O O O O O O O O O
O O O Cl Cl Cl Cl Cl Cl Cl Cl
0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 0 0
N l0 LO LO V N N l0 l0
6 6 o C; o o CD C) C) C) C)
O V N N M Z� N N O M Q N N M C)
N M CA O
Cfl r Z n CO (fl � CO Z w M Cfl — Cfl
O O O O O O CD O O CD O O O O
O
C
CV
A 0
00. �
m m a�i c O
c t N
N O_ O_ O N (6 N Oi r O
0 0 O (6 O Z N O_ 0 C~ O_
O O Cfl
2 L L 0 O O O Oi LL � ..-. " 4 H
c c O O O N O N d Z N N 0-
-C
_H H O tOA O 0 U U Q C i i i i i i
6 CO 0 1 Q M 'C7 O O O O O O
V , V V U N N N N g N >. M M M M M M
r cNi cNi cNi 6 6 2 2 2 Z a a
N
F."
O
R-,
co
O
00
Q)
(B

O
N
M
A
�I
i"
�V+
CC
M
U a
m
O
E
J
O d
O LO
LO
coo to
to
M M
Z Z o
C ZT
C� Cn
0
IL
N N of
N N
M M E
� � J
� � L
_O
N N =
C6 C6 _
Q N E
C) 'N J
LL T 0
� J
Q
U
W
0
J_
E m
LO >
.O� LO w
_ M
O � �
� Y
QI U)
04 co
m n �
O co >
Y
CO CO IL
aio Z
0
UIL
J
Ci
N M �
0)
a
Q U
E cu
co CO
U)
0
N
Q
0
toLO
U
N
N m
E m m
co n C) a
U U
O O O O O O O O O O O O
M M M M M M M M M M M M
M O M lO M O Cfl O O M M 0 0 0 0 0 0
M M M N N M O M O
O M r— LQ V lf) N 00 N
O O
V N V M (D O O O (fl zT N N
(O � 0') 0)N � M (O CN lr- M
O O O O O O O O O O O
O I- O Mzl- O O O O O LO O M M M
M Ln Ln Ln t M M M M M M CO lO � M M
M O LO —— O N— V V 0 0 0 M L() V M
M M I-� N Ln — Cfl E O M ——— CO N M O
M V M LO N co M co N CO cc
V 0 0 0 M r— O M r— N M M O O CM �
M��� O O N O w 0 0� 0 0 V
M M r— CO r—
O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O (fl O O O O O O O O O O O O
00 00 00 00 00 — 00 CO CO CO CO CO
O O O Cl Cl Cl Cl Cl Cl Cl Cl
O O O O O O O O O O O O
Nl� l� —O l� V — CD O N N l� l
O O O o O o CD O O O O
_M N Q (D M O V 0M M O M
(q � � 00 Z � 00 (D CO CO LO r—
O O O O O O O O C7 C7 O O O
O
C
) 00�
C��6 O N C O
c t m
N O_ O_ O N CO N Oi '0 C' O
0 0 0 O CO c O 2 N O_ 0 C 0 H 0 O_
O O CQ
a,2 L L 0 O O O Oi LL .J LL H
c 0 O O O N O N 5-2 N N O_
oUUU��C������
6 co � � O a � � � � � co
r cNi cNi cNi 6 U 2 2 2 Z a a
N
F."
O
co
O
rn
Q)

0
N
M
Fi
U
F�
0
E
N r)
CD a_O LO ry
LO
coo to
to
r)
M d
rK
z z
0-
of �
m M N
N
a
Q U
E ca
co CO
U)
O
N
m m
� a
_N c N
E m m
co n C) a
M CO M M M M
0 0 00 Lo'T 00
M M C)
CO V r- 0 O M
m ai co � or- m
O O O Cl Cl Cl
Cl Cl Cl Cl Cl Cl
Cl Cl Cl O O O
O O O O O O O O O O O O
N N LO N O CD CD U') O O N LO
N
0 0 0 CD 0 0 CD 0 0 0 0
O o O
p p p p p p p p p p p p cfl O M
Z Z Z Z Z Z Z Z Z Z Z Z� ^ C) r-
O O O O O
O
C
A 0 0�
6 O N c O
O L N
C O_ O_ O N (0 N 2� C O
O (6 O N O_ 7 C amo~ 7 O_
L L 0 0 O O O N O EE =-. ..,i4H
U U O O O N N d Z N N O_
L L C.)i i i i i i
l0 CO i5 N O (0 (6 co Q (0 .o O O O O O O
V , V V U N N N N .O N >. U) U) U) U) U) U)
r N N N 6 6 2 2 2 2 a a
N
0
co
O
0
N
Q)
m
m
d

0
N
M
Fi
U
F�
U a
0
E
J
M d
O LO ry
LO
coo to
to
M LL
rK
z z
0-
of �
J_
E m
LO
LO>
_ M
O � �
� Y
QI (f)
04 co
m n �
O co >
Y
CO CO a.
ai Z_
0
Uco
IL
Ci
N M
J � �
N
a
Q U
E cu
co CO
U)
N
M
N
U U
J J
Q
_N c N
E m m
co n C) a
U U
0 �
C) c; M M M ;: M M M M M M M Cfl M M cMM CMO
m O m CD N 0 N N_ CD M O CD m 0 M O f— M
ON 0 0 O O N O O 4!�! M O
O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O O O O O O O O O O O O O O
O O O O O (D O O O O O O O O O O O O
O O O Cl Cl Cl Cl Cl Cl Cl Cl
O O O O O O O O O O O O
o 0 0 0 0 O O O O O LO LO
N N LO N L6 N l0 N N
C) O O o CD o o C) C) 0 0
ap Z 000. 000. � ONO. . 0 O O � � � O
O O C7 O O O O O O O O
O
C
A 0 O N O
Co O N C O
C L N
C O_ O_ O N CO N 2C= O
2 2O (6 OO N O_ 7 C~ 7 O_
O Cfl
2 L L 0 O O O LL .J LL H
c c O O O N O N (IZ N N O_
_U H H O tOA O U U U Q C i i i i i i
6
Q o Q y m m m a
V , V C)N V N N N g N >. U) U) U) U) U) co
r cNi cNi cNi 6 6 2 2 2 Z a a
CW
G
a
N
O
co
0
N
Q)
U)

75
N N
a a
N N
M M E
� � J
� � L
O N =
cl cl
a U E
E .N 3
a '•
c J
Q
U
w
J
C1
O �
N L >
M
� N Y
a
U U
N00
a a co
m
U ? Y
H N a-
Z
0
U � J
U H a
� a
O
M N
N Cl) N
L
N
a
a .V.
E m
m Co
U
W
E
R
O
0
00 >�
O o
o =_
N
o o
fl >,
E o m
Con a
a
Om N � O O �f7 L�2 �2
N N N
O O O O O O O O
v m r- co r- v Un Un
I-� Cfl N m m O O
O O O O O O O O
O o 0 0 0 0 g 0
0 0 0 0 0 0 0 0
0 0 0 0 0 0
0 0 0 0 0 0
N �f7 �f7 �f7 �f7 �f7
O O O O O O
0 O O O O O
O O O O O
ZCO N m m
m m m m rn
O O O O O
O O O O O
O O O O O
LD
X
U N O m
m
o c m m o L
O
L C E N N 47
U u1 01 = =
C1
O �
N L >
M
Cl) Y
a
U U
C9 co �
a Fu
co m
Y
H N a-
-0 Z
0
U Q) J
Q al
H CJ
O
M Q)
O
a
a .V.
E m
m Co
U
W
E
R
O
0
00 >�
O o
o =_
N
o � o
E o m
Co n a
a
0 0 0 0 0 0
m m m m m m
o m co vn r-m o o
N CO Ll7 m m
o m � m
m N m m
m m m m rn
0 0 0 0 0
O O O O O
0 0 0 0 0
Om N � O m0 �f7
N N N
O O O O O O O O
m r- r- v Un O m 0
m N 6 Cfl O m 0 m
m m r-m m m co r-
0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0
0 0 0 0 0 0
0 0 0 0 0 0
0 0 0 0 0 0
N �f7 �f7 �f7 �f7 �f7
O O O O O O
0 O O O O O
O O O O O
Q I- r- V U-) O O m
Z N rn O O mLx�
m m m m
O 0 O O O
O O O O O
O O O O O
LD
X
U o o m
= U U
co M L. ..
o c m m o
O
L C E Q) � N
U Lu 0) = =
c�
0

m
E
J
Cl)
a
rn to
00 to
M CO
CM a
zo zo
c �
in
75
n
N N
N N
CM CM E
� � J
� � L
_2)
O N =
cl cl
a U E
E .N 3
a '•
c J
Q
U
u1
J
C1
O �
N L >
M
N Y
a
U U
N 0
a a co
m
U ? Y
H N a-
Z
0
U � J
U H a
� a
O
Uc o
J M
N
a
a .V.
E m
co Co
U
LO
Cl)
Cl) CO
J J
o o
fl- � T
E o m
Co n a
a
O O O O O m O O
�2 �2 �2 �2 �2 �: �2 �2
O O O O O O O O
Un O v m N N I- m
m m I- m m�
O O O O O O O O
0 0 0 0 0 0 0
00 0 0 0 0 0 0 0
0 0 0 0 0 0
0
0 0
0
0
0
N
�f7 �f7
�f7
�f7
�f7
O
O O
O
O
O
O
O O
O
O
O
O
O O
O
O
O
O O
O
O
O
m
m
m
O
O 0
O
O
O �
0
O O
O
O
0
O O
O
O
N
X
U o o m
m
-o c m m o
O n
L C E N N 47
U W o1 2 2
m
E
J
rn t
M 00 to
CO
cn a
zo zo
c
[if in
C1
O �
N L >
M
Cl) Y
a
U U
C9 co �
a co m
Y
H N a-
-0 Z
0
U Q) J
Q al
H CJ
Y L
J M N
m �
LO
O
a
a .V.
E m
m Co
CO
LO
Cl)
M
LO
m m
a
o o
fl- � T
E o m
Co n a
m
m Un
m �
0 0 0 0 0 0 0
N �f7 �f7 �f7 �f7 �f7 �f7
O O O O O O O
O O O O O O O
O O O O O O O
O O O O O
z z z z z z zC,� 6
N
X
U o o m
Qco m U H
co
E m m 0
L Xo C N o o o Cl) Cl)
U H W 0) 2 2 2
N
0
M
4-
0
cr)
N
c6

\
�
§
\
_
u a
§
§ )
( §
E 7 ƒ
3 O k
§
f
%
\
�\
�
Q
q
0
#
q
_
�
_
�

m
CJ
E
J
Cl)
Im a
N CO 0L
co LO
M CO
� M CZ
o o z z
C ZT
75
N
N _
O
N
M J
� L
N =
cl cl
Q to
E .N 3
a '•
c J
Q
U
u1
a
e N
N >
C D
� Y
a
�I Cl)
H
fA O co �
U 00 co
O y a
U
Z
0
U � J
U H a
� a
CM
N
co
in Cl) N
J �
N
a
a .V.
E m
m Co
U
r- O
o � o
rn
Uf7 N O
6 C6 O
Nco
L
C (D
00
o p 00
0 0 0
E E
0 0
O
C/) C/) C/)
m
CJ
E
J
l
N CO 0L
M CO
f") CZ
zo zo
C ZT
[If C/)
75
N
N _
O
N E
M J
� L
_D
co C6 _
0 cl
a U) E
2 .N 3
a '•
c J
Q
U
u1
a
e co
N >
C
� Y
a
�I Cl)
H
fA O Q)
U 00 >
O> y a
U
Z
0
U � J
H CJ
m
N
J M N
Q
a
a .V.
E m
m Co
CO
O co rn
r-� 6 6
rn rn rn
U') o rn
Nco
L
C (D
0 o
0 0
00
0 0 0
E E
0 0
m
V i5 H
7 7 7
C/) C/) C/)
M
0
LO
N
o
�
0-
�
O N
O
� �
0
�
3 �
�
C1
on
0
a
O
ti
y
0
O
�
U
N
G
O
o
�
�
O

V a
0
E
J
d
N LO ry
'o 00
co LO
to r)
M d
Z
rK
z
ry
ry
0
d
ry
N _
O
N E
� J
L
N N
C6 ) _
Q fn E
Q) 'N J
d T 3
� J
Q
U
LU
v
a
CV!
E
E
C
Y
IL
U)
O �
w r >
� 3 Y
y a
� Z
0
U J
IL
N
to
co
M
N
U U
J J
E m Flo(6 — C
cn U Q
O
co
O
r-
r-
0
O
O
V
N
T
21
CW
G
7
a
N
0
co
O
N
Q)
(B
d

m
CJ
E
J
Im
to a
to 00
n
M � a
o zo z
C �
75
N
N _
O
N
n J
ai ib =
m m _
cl cl
a U
E .N 3
a '•
c J
Q
U
w
U
L
CW
V
7
N 75
N >
C D
� Y
a
LO
O(DQj � 7
N > Im
I Y
C N a-
� z
0
U (D J
H CJ
� a
O
O �
in 00 Cl)N
J �
N
a
a .V.
E m
co Co
U
to
Cl)
O
00
Cl)
13; N
Cl) CO
J J
47 N
0- >,
E o m
i/) U Q
O
O
rn
O
O
O
O
O
r-
m
c�
E
J
a-
co 00
i
M � a
zo z75
C �
a
N
N _
O
N E
_D
ai ai =
m m _
cl cl
a U
.N 3a '•
c J
Q
U
w
U �
v
Q1
V
7
y N
N >
C D
� Y
a
LO
(Da-e 7
I Y
C a-
� z
0
U (D J
H CJ
� a
00
O
d Cl) N
0 � �
a
a .V.
E m
m 00
a
D
Q
O
O
CO U
0
O U
C.jR
N CO
L
47 N
0- C T
E o m
i� U Q
rn
r-
O
O
O
m
CJ
E
J
Cl) 0
a
ali n 0�
co 00
M c a
zo zo
C 0-
0� CO
75
N
N _
O
N E
n
_D
ai ai =
m m _
cl cl
a U
2 .N 3
a
c J
Q
U
w
U
M
Q1
V
7
y N
N >
C )
� Y
a
0 CO
LO
a0 7
I Y
C N a-
� z
0
U Q) J
Q CJ
� a
O
Cl) —
O
00
d f) Q)
0
a
a .V.
E m
co Co
U
a
D
Q
O
O
U
O m C.jR
N CO
6
Q Q)
0- >,
E o co
i/) U Q
v
O
O
lf7

0
E
J
d
M f— ry
'o 00
co LO
to
r)
M IL
Z
Ir
z
C �
C� Cn
V a
m
IN
m
O
O
O
2
a
CW
G
a
N
0
co
0
00
N
Q)
(B
d

m
CJ
E
J
Im
n 00
to Im
M � a
o zo z
c �
in
75
O _
N
O E
� J
� L
_D
N =
cl cl
a U E
E .N 3
a >
c J
Q
U
w
Y
C1
E 75
N >
C D
� Y
a
t5 Cl)
N
7
a O (6
w 01 >
y y a
U
Z
0
U (D J
U H a
(D a
n
J M N
N
a
a .V.
E m
co Co
U
00
00
Cl)
w
m Cl)
� a
Q Q)
fl- � T
E o m
Con a
O
Ut
N
cl
z
m
c�
E
J
O a-
i 0000
co Im
M LO
to d
zo zo
c �
[If in
75
O _
N
O E
� J
� L
_D
N N =
cl cl
a U E
E .N 3
a >•
c J
Q
U
w
Y
tm
E 75
N >
C (D
� Y
a
R Cl)
� � N
7
a O (6
w 01 >
y y a
U
70 Z
0
U (D J
H CJ
n ..
c
Cl)co
Cl) N
J �
a
a .V.
E m
m Co
CO
00
M_
U co
J J
47 N
E o m
i/) U Q
00
0
O
Ut
rn
O
O
O
N
N
O
Ut
N
O
O
O
N
m
CJ
E
J
a-
n 00
to Im
M t a
zo zo
C 0-
� (n
75
O _
N
O E
J
� L
_D
N N =
(6 ( _
cl cl
a U E
2 .N 3
a >
c J
Q
U
w
Y
C1
E 75
N >
C )
� Y
a
t5 Cl)
Q)
7
a O (6
w G1 >
y y a
U
Z
0
U Q) J
Q CJ
n ..
0
W N
M_ Q)
of
a
a .V.
E m
m Co
U
CO
Q
O
O
O1 U
01 0
O V
R
N CO
L
E o m
i/) U Q
O
N
O
0
O
O
N
N
O
Ut
N
O
N
O
N
m
c�
E
J
N 0
n 00
to Im
M � a
zo zo
c �
in
75
O _
N
O E
� J
� L
_D
N � _
(6 (6 _
cl cl
a U) E
E .N 3
a >•
c J
Q
U
w
Y
C1
E 75
N >
C D
� Y
a
R
N
7
a O (6
w 01 >
y y a
U
70 Z
0
U (D J
H CJ
n ..
0 Cl)_ N
N
a
a .V.
E m
m Co
U
0
CO
Q
O
O
O1 U
m 0
O V
R
N CO
b
E o co
i/) U Q
O
cam
cam
CR
O
O
N
N
O
Ut
N
0
N_
N
0
U
co
CO
M
0
rn
>cu
N
o
�
�
o
U U
� �
0
Cl-
El
a
3 �
y
�
C1
bA
�
Ci
0
a
O
ti
y
o
O
O
�
U
N
G
O
o
�
�
O
�
q
W
UO
c4

M
.-I
u
Fi
U
F�
(6
0
E
N r)
co ry
co d
t0 m
co to
to
r)
M d
Z
rK
z
ry
ry
0
N
O _
N
O E
J
� L
2)
N N =
C6 ) _
Q N E
Q) 'N J
d T
� J
Q
U
LU
0
r
co
� M �
N
a
Q U
E ca
(6 CO
U)
0
N
Q
0
� U
Ci
N R
N CO
Q �
E _o m
cn U Q
N
F."
O

75
CJ
E
J
Im
a
n Cl)�
M � a
o zo z
c �
in
75
O _
N
O E
� J
� L
_D
N =
cl cl
a U E
E .N 3
a
c J
Q
U
u1
Y
C1
E 75
N >
C D
� Y
a
N Cl)
�a co
� 7
cU CO a-
zo
0
U (D J
U H a
(D a
01
n
J M N
N
a
a .V.
E m
m m
U
0
V
0
cl
z
0
a
m
(D
�+
Q)
N
L" Qj
C
C
co
U a
Co
C/)
C
Q
U
75
c�
E
J
L
n rn a
0�
to Im
M LO
to d
zo zo
c �
[If in
75
O _
N
O E
� J
� L
_D
N N =
cl cl
a U E
E .N 3
a '•
c J
Q
U
u1
Y
C1
E 75
N >
C D
� Y
a
N Cl)
�Q co
� 7
cU CO a-
-0 zo
0
U (D J
H CJ
01
n ..
00 U)
M_ N
a
a .V.
E m
m m
U
CO
Q
O
0
Q1 U
am U,
o �
R
N m
4) c N
E o co
i/ U Q
m
00
0
O
O
O
O
rn
V
0
co
U')
O
75
CJ
E
J
to 0
n rn a-
M t a
zo zo
c 0-
� (n
N
O _
N
O E
J
� L
_D
N N 2
cl cl
a U E
2 .N 3
a
c J
Q
U
u1
Y
C1
E 75
N >
C )
� Y
a
N Cl)
a) >
cU cA a-
zo
0
U Q) J
Q CJ
am
n
00
Cl)
0 M_ Q)
a
a .V.
E m
co Co
U
0
CO
Q
O
0
O1 U
rn d
o �
R
N m
E o m
i/) U Q
0
co
O
O
O
00
V
0
co
O
O
75
CJ
E
J
O �
n rn
to Im
M � a
zo zo
c �
in
N
O _
N
O E
� J
� L
_D
N � _
(6 (6 _
cl cl
a U) E
E .N 3
a '•
c J
Q
U
u1
Y
C1
E 75
N >
C D
� Y
a
N C/)
a co
� � 7
U N Y
a
70 zo
0
U � J
H CJ
00
01
n ..
0
Cl) Cl) N
J �
N
a
a .V.
E m
m m
U
00
O
00
0
O
CO
Cl)
CO
co
J
J
co
0�
of
Q)
Q
Q
m
E
Q)
c
co
>,
Co
Q)
co
co
>1
U
cn
U
Q
U
M
0
Tl-
�
m
o
�
cu
�
O
U U
� �
0
El
�
3 �
�
C1
on
0
a
O
y
0
O
�
U
N
G
O
o
�
�
O
�
q

m
c�
E
J
O �
LO a
n rn 0�
to Im
M � a
o o z z
c �
in
n
75
O _
N
O E
� J
� L
_D
N =
cl cl
a U E
E .N 3
a
c J
Q
U
w
Y
C1
E 75
N >
C D
� Y
a
N Cl)
�a co
� 7
cU CO a-
Z
0
U (D J
U H a
(D a
CO
CO CO
J J
Q Q)
0- >,
E o m
it U Q
m
c�
E
J
Cl)
LO a
n rn 0�
to Im
M � a
o o z z
c �
in
n
75
O _
N
O E
� J
� L
_D
N � _
cl cl
a U E
E .N 3
a
c J
Q
U
w
Y
C1
E 75
N >
C D
� Y
a
N Cl)
�Q co
� 7
cU CO a-
-0 Z
0
U (D J
H CJ
Q1
n ..
W N
Q)
N
a
a .V.
E m
m Co
U
x U
t �
J 10
� m
Q Q)
E o m
i/) U Q
O
6
rn
O
O
M
0
N
o
�
cu
�
O
U U
� �
0
�
3 �
�
C1
on
0
a
O
ti
O
�
U
N
G
O
IJ
�
�
O
�
q6�

kr,
N
00
00
M
A
U
:C
75
CJ
E
J
M a
N
M CO
� SO to
M a
o o z z
c zT
in
n
75
a
� J
� L
U ib _
cl cl
a U
E .N 3
a >
c J
Q
U
w
J
a)
E 75
N >
C D
� Y
a
U U
N N
d C) 03
00 >
U �: Y
H N a-
Z
0
U � J
H CJ
Cn
N
00
J M N
a
a .U.
E m
m Co
U
m Cl)
� a
U U
E o m
Co n a
O
C6
rn
O
O
O
s
cl cl O
Z z rn
O
V
a `"
�- i
0 6
V cl)V
N N
75
CJ
E
J
N r-)
LO a
N M
M 00 m
00 to
CO
f") a
zo zo
c �
in
n
75
a
� J
� L
_2)
co (6 _
0 cl
a U) E
2 .N 3
a >•
c J
Q
U
w
J
a)
E 75
N >
C
� Y
a
U U
Ct? N =5
d M 03
00 >
U �: Y
H N a-
Z
0
U � J
U H a
� a
Cn
N
00
00
M U)
J �
U
a
a .U.
E m
m Co
CO
U
U co
CO CO
J J
0) cl U
0- >,
E o —co
i/ U Q
m
rn 00 00
M
4-
0
cr)
cr)
�
m
o
�
cu
�
O N
O
� �
0
�
3 �
�
C1
on
0
a
O
ti
y
0
O
�
U
N
G
O
o
�
q

?iruai
a '6
arip°u 10 wuandm°no jlnaad$ :+CIoD AS([ aO�
a ti
m
B y
O
p�
O
xKr y
a
ti
a
r x
d
W 4 p
� q�aypsad �•
dijo-1 oa6euA!S
PIJ wx$ ,pd sa�u�eyo°� jo +a9�ON
7.
(Hwmww� Rnad) angw (s : ° SY42I is -k[ LLS
O e-mpeAbAtd (3
2 iaeae448uP141+� c ,ri9 'J+4eM 11gwM-"Q4 - MdN
.C7 �
� aldcswg 4ujo
v, u
a�
n
� 4
$ x Sao is g
l � L
td
v
p N
w
■ ti a
�ji
P�
ry
4
u
Page 34 of 36

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 22010180 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
1/5/2022 12:50:00 PM
1/6/2022 12:53:43 PM
1/6/2022 1:50:00 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition?
Yes
d❑
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present V
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
NC per email
1/4/22 per email
Rec'd by Tegan Richards
sample date 1/4/21 on coc
Page 35 of 36

summly Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHHQL4Ga1�23.INC Cuyahoga Falls, Ohio44223
�trrafyt�caf iaboralorJas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028
Cooler Information
Work Order Number: 22010180
Sample Log -In Check List
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
14.0
Goodl
Not Present
RcptNo: 1
Page 36 of 36

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number:
WWTP Name: Mt Holly WWTP NPDES Number:
Monitoring Period; From 01/01/2022 To 03131/2022
W00001863
NCO021156
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A;
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/1) (No Prior Test) All. 5/Procoss to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilie
Seta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlipahla fn alfnrnat:vn n fur ] !! Ta A nr f'la a Rl ..3nHo Mho 4 I7 ,:F . S , A-*-.
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6°'
MPN
Coliform
power per gram
MPN/g
of total solids
CFU
277,778
379,410
516,954
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
Collai
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt, 3 Option/Alt. 4
(V5 reduction)
(40-day bench)
(30-day berich) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt, 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying ---Unstable)
Option/Alt. 9
Option/Alt. 10
(injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503,33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that die pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T•1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made tinder my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater _
Prcpa -Al me au Title (type or print)
S ature reparor* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Alp
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 1/18/2022
Project: Mt. Holly
Date Sample Rcvd: 1/6/2022
Meritech Work Order # 01062273 Sample: Mt. Holly 1 Grab 1/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.81 % 1/7/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 486,188 cal/g dry wt 1/6/22 130 col/g dry wt SM 9222D
Meritech Work Order #
01062274 Sample: Mt Holly 2 Grab
1/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.78 % 1/7/22
0-100 %
SM 2540B
Fecal Coliform (SIudge)
516,854 col/g dry wt 1/6/22
130 col/g dry wt
SM 9222D
Meritech Work Order #
01062275 Sample: Mt. Holly 3 Grab
1/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.76 % 1/7/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
369,318 col/g dry wt 1/6/22
130 col/g drywt
SM 9222D
Meritech Work Order # 01062276 Sample: Mt. Holly 4 Grab 1/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.74 % 1/7/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 344,828 col/g dry wt 1/6/22 130 col/g dry wt SM 9222D
Meritech Work Order # 01062277 Sample: Mt. Holly 5 Grab 1/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.79 % 1/7/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 418,994 col/g dry wt 1/6/22 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Alex Fox Report Date: 1/18/2022
Client: Synagro
284 Boger Road Project: Mt. Holly
Mocksville, NC 27028 Date Sample Rcvd: 1/6/2022
Meritech Work Order # 01062278 Sample: Mt. Holly 6 Grab 1/6/22
Parameters
% Total Solids
Fecal Coliform (Sludge)
Results Analysis Date Reporting Limit Method
1.81 % 1/7/22 0-100 % SM 2540B
303,867 col/g dry wt 1/6/22 130 col/g dry wt SM 9222D
Meritech Work Order # 01062279 Sample: Mt. Holly 7 Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 1.80 % 1/7/22 0-100 %
Fecal Coliform (Sludge) 277,778 col/g dry wt 1/6/22 130 col/g dry wt
1/6/22
Method
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

m
ro
CD
1
a
o
C9-3
f
N
to
m
Q
a Q
3
�
Gr]
a
-3
N
r
�
r
❑a
ro
°ma
(5
C _.
j
3
emsCP
❑
CI�s
y
0
CD
v
r�
g v
�a
�p
�1
�
ro
mrr
w
cc
co
D
Ta
SCL
rJ
mG
xxVD
!`
N
N 1
(mp
m
O
Cti
m x
g ro
m
D
1
r
S
ro m
N Al M IDO
w o Z
O
¢
m
m
c
A5n G
m
CD
N
Cj
G
❑ m
G=Grab
a
m
m
} ro
I ro
m y
C=Composite
cn
..
m
c m
ID n z
m3
i
❑
Collection Sampo
Temp °C
� r O
LO
o
n 6
R�
m
O
m
v
x
Analysis
cr
c
1
cr
1e�41
w
N
W
m
10
p
n
�
n
M
n
n
m
m
1
1
N
a
a
ro
C
<
G
C
C
m
O m
Q
a
CD
CL
'Tl
21
m Z
nj
[
J
y
a
m
W
n
f
t
a�
3
a
❑
<
n
_
o
❑
❑
a m
Q
O
�
N
ro O
x
a�r2
aw
a
ro
El
'a
=
a
m
3
m
m
wo
m
a
<C
n
�r
N
C�7
Fjo
v
v
v
o
o
co
m
p
m
z
V
m
m
m
z
p
/�
�
❑
m
�
m
m
a
3
m
v
N
{Il
`
ElQ
7
m
El
L1`�Vf
x
z
W,
7J
W N tD
At
� (D
N 2 O �.
�
N O
°°fin
O

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 01/04/2022
Reported: 02/11 /2022
For: MT HOLLY
Comments:
4 1TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
220104-50-01 30 Day Benchscale MT HOLLY
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
4.3
EPA625-R-92/0 01/04/2022 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 220104-50-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

p 1C N m N
3 H
0
m m 3 m m 7
m 33+
j
a
m
CD I� COD
I0 C C
n. co d UD d vi a
i1D
N `cr e (D .6 m
co a a
�.
O
0
3 3 3 3
Q
3 3 3
IN
m w d w
m CD m m
Ow
•
K
mm
V
C
m
S
O
•+
c
O
C
ur
0
7
m
f
.C�
S'
7
CD
a-4
Q
o
.�
(A
-
y
Q
3 3 3 3
D
x
Fm
3 3 3 3
xN�
CD m m (o
a
r
Cn
9
N �
R
N
-. z _ w
�
0 w
o a d
N 7 3 a 3
c
o
3 a
0 'an (D Q
_
m m m a
0 o
:E is m
o�
n � � Z D
g<'A�
rJ.iZ3 '<<
o, t r- m
x
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 5

STATESVILLE
ANALYTICAL
Analytical Results
Synagro For: Mt Holly
284 Boger Rd
Mocksville, NC 27028
Entered: 1/04/22
Reported: 2/11/22
Sample ID: 220104-50-01
PARAMETER: Vector Attraction Reduction/Aerobically Divested Sludee 130da
Total Solids
Volatile Solids
% Volatile Solids
Week
1
0.62
0.47
0.7581
Week
2
0.59
0.44
0.7458
Week
3
0.59
0.44
0.7458
Week
4
0.55
0.41
0.7455
Week
5
0.54
0.40
0.7407
Week
6
0.52
0.39
0.7500
Volatile Solids Reduction: 0.7581 - 0.7500 X 100 = 4.3 %
0.7581- (0.7581 X 0.7500)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID 4 220104-50-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.62
0.48
0.7742
2
0.62
0.47
0.7581
3
0.62
0.45
0.7258
Average:
0.62
0.47
0.7581
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.59
0.44
0.7458
2
0.59
0.45
0.7627
3
0.59
0.43
0.7288
Average-,
0.59
0.44
0.7458
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.61
0.46
0.7541
2
0.58
0.44
0.7586
3
0.57
0.43
0.7544
Average:
0.59
0.44
0.7458
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.55
0.40
0.7273
2
0.55
0.41
0.7455
3
0.55
0.41
0.7455
Average:
0.55
0.41
0.7455
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.54
0.40
0.7407
2
0.54
0.40
0.7407
3
0.54
0.39
0.7222
Average:
0.54
0.40
0.7407
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.39
0.7500
2
0.52
0.38
0.7308
3
0.53
0.39
0.7358
Average:
0.52
0.39
0.7500
Van Kleeek Reduction: 0.7581 - 0.7500 X 100 = 4.3%
0,7581 - ( 0.7581 X 0.7500)
Final Result: 4.3%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: W 0001863
WWTP Name: Mt Holly WWTP - NPDES Number-. NCO021156
Monitoring Period: From 04/01/2022 To 06/30/2022
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I /A (time/temp) All. 2/13 (Alk Treatment) Ali. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B;
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
_ A D\ ----I t al.n F..lfn ii'nYii1(i A. f.-
AA A ll{:A Rllti
Parameter
LV n�IGA ..u.i1.. �.a iva
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excec-
of
Type
Technique
Minimum Geo. Mean Maximum units
dences
Analysis
Fecal
2x10to the 61'
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
604,027
805,320
965,517
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503,33/15A NCAC 02T.1107) - Please indicate option/alternative performed;
Option/Alt. 1
(VS reduction)
option/Alt. 2
(40-day bench)
Option/Alt. 3 Option/Alt. 4
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
tl"J'ection)
Option/Alt,10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503,32/15A NCAC 02T,1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen re uirements in 40 CFR 503,32/15A NCAC 02T,1106 and the. vector attraction
reduction requirement m 40 CFR 503.33/15A 1�ICAC 02T,1107 have not been met." (Please note if you cheek this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the ppathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclhiding fine and imprisonment."
Doug Shoudt Division Manager Wastewater
4epatuNam anti Title pe or print) ��772r -V of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 4/14/2022
Date Sample Rcvd: 4/6/2022
Meritech Work Order # 04062284 Sample: MH 1 Grab 4/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.47 % 4/7/22 0-100 % SM 2540E
Fecal Coliform (Sludge) 748,299 col/g dry wt 4/6/22 224 col/g dry wt SM 9222D
Meritech Work Order # 04062285 Sample: MH 2 Grab 4/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.49 % 4/7/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 604,027 col/g dry wt 4/6/22 130 col/g dry wt SM 9222D
Meritech Work Order #
04062286 Sample: MH 3 Grab
4/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.47 % 4/7/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
870,748 col/g dry wt 4/6/22
130 col/g dry wt
SM 9222D
Meritech Work Order #
04062287 Sample: MH 4 Grab
4/6/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.47 % 4/7/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
884,354 col/g dry wt 4/6/22
130 col/g dry wt
SM 9222D
Meritech Work Order # 04062288 Sample: MH 5 Grab 4/6/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.52 % 4/7/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 717,105 col/g dry wt 4/6/22 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel. [phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 04062289 Sample: MH 6 Grab
Parameters Results Analysis Date
% Total Solids 1.47 % 4/7/22
Fecal Coliform (Sludge) 911,565 col/g dry wt 4/6/22
Page 2
Report Date: 4/14/2022
Date Sample Rcvd: 4/6/2022
4/6/22
Reporting Limit Method
0-100 % SM 2540E
130 col/g dry wt SM 9222D
Meritech Work Order # 04062290 Sample: MH 7 Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 1.45 % 4/7/22 0-100
Fecal Coliform (Sludge) 965,S17 col/g dry wt 4/6/22 130 col/g dry wt
4/6/22
Method
SM 2540B
SM 9222D
I hereby certify that1 have reviewed and approve these data.cap
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

m
N
I
3
��
o
p
rL
ID
C
C
[MD
C
C
CL
{y
IN
ED
3
W
3s�
m
❑ m
`
C.L
m
W m
{
O w [L
m
p
m
133
`
m
mo
a
�1
W
c
_
cCD
..
a
IM
a
J
N7
C
N 1D
p w
d
fl1
m
V
CDR
!t
a7�-al
� =
ro
� �
✓�
o
x
o
70
CD
x
NZ
-0
co
m
CL
A
f
E
t�
M
o m
t
N m M m
CD O v �
m °�
o
m
o
o
x
b
❑ ,,
G = Grab
>
m
3
CD
CD
.,�
(�W
M.
C= Composite
5D 2
m
Ta
O��
a p
CAllectbn Sample
p
D
� o
—m
T'emp'C
Z-
C
z
o
�19
m
3
m
3
C
E
m
x
x
a
Vw
O
�
Analysis
mr
-
ff
�
N
m yr
C
(
A
b
T
m
m
m
m
°m_
W
]]
t
N
c
a(p
m
<
m
c.
a
m
c
2
c
0
n
M m
0
CL
c
SSS a
cr
a
�
m
N
Ci Z
c� {
'�
.�
<
.
In
C-
w
t
m
x
co
W
m
m
v
El
Z
o
❑Q
m
❑
Z w
Q
LL
m
im
m 0
d
n
n. m
ai
R
CT
j
CO
n
s
m
m
w
m
a
m 3
3
C7
C
❑
m
n
CO
Q
ET
p
m
O
O
rJl]
v
p
W
a
CD
;�
m
Wha
N
Z
=
µ
fl
❑
w
N
6
p
7
m
_
n
O
p
o
W
e
p
o
1
m
m
m
<
W
O
O
N
El
p
W

%VS R
(older, more conservative method)
%VS in 1 0.7818 - Enter in
%VS out 1 0.72501 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 26.42
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 7.27
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 04/06/2022
Reported: 05/10/2022
For: Mt Holly
Comments:
4 STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
220406-25-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
26.4
EPA625-R-92/0 04/06/2022 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

/ / 2 / / o ƒ ƒ
2
"
-
/
E
?
a
m m ■ m , /
k i `
f2
[
§
k k k�
- F 0 C
§
%
ar
3 ) j ) 3
] ] ] 3 '
E E E E
c
\ / /
w
_
2a
�
3
C_
k�
kI
CD
CL
93
cr
) 2 2 2 2
j ) § j
k
\ \ ] ]
\ E a E
& ID
° �%
I
# D
!
�.
0 7 ? o / ƒ
e R � ]
§13
0 k
} ƒ m m K 07
( " 5
CD ,
z\>�
•
' � \��J ]
PO Bo 2289 Statesville, NC 28687.704 872 4 97
A234

STATESVILLE
ANALYTICAL
t
Analytical Results
Synagro For: Mt Holly
284 Boger Rd
Mocksville, NC 27028
Entered: 4/6/22
Reported: 5/10/22
Sample ID: 220406-25-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
k 1 0.55 0.43 0.7818
Week 2 0.52 0.40 0.7692
Week
3
0.51
0.39
0.7647
Week
4
0.44
0.33
0.7500
Week
5
0.42
0.30
0.7143
Week
6
0.40
0.29
0.7250
Volatile Solids Reduction: 0.7818 - 0.7250 X 100 = 26.4 %
0.7818 - (0.7818 X 0.7250)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

30 Day Bench Worksheet
Sample ID # 220406-25-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.55
0.43
2
0.55
0.43
3
0.54
0.43
Average:
0.55
0.43
0.7818 1
WF.F,K 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.40
2
0.52
0.41
3
0.51
0.40
Average:
0.52
0.40
0.7692
WF,F.K 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.49
0.37
2
0.49
0.37
3
0.54
0.42
Average:
0.51
0.39
0.7647
1`N 01 o1:4t1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.44
0.35
2
0.43
0.32
3
0.44
0.32
Average:
0.44
0.33
0.7500
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.42
0.29
2
0.42
0.30
3
0.42
0.31
Average:
0.42
0.30
0.7143
1iil 01 b1 C('.
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.39
0.28
2
0.40
0.29
3
0.42
0.30
Average:
0.40
0.29
0.7250
Van Kleeck Reduction: 0.7818 - 0.7250 X 100 = 26.4 %
0.7818 - ( 0.7818 X 0.7250)
Final Result: 26.4%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number
WWTP Name: _ Mt Holly WWTP NPDES Number:
Monitoring Period: From 07/01/2022 To 09/30/2022 —
WQ0001863
NCO021156
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I /A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annllcahle to alternative narfnrmprl ([Trace A ne Place 1M. on -I.do +r.0 fnll..r.,:n...., .,;F... a..+...
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
dences
of
Analysis
Type
Technique
Fecal
2x10to the 6'b
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
1398
2726
3655
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gran of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifoirn)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt, 3 Option/Alt. 4
(VS redaction)
(40-day bench)
(30-daybench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt, 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt, 9
Option/Alt. 10
(injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"i certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This deternnination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
orsonnel properly gather and evaluate the information used to determine that the �pathogen and vector attraction reduction requirements have een met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Pre er Name and Title (type or print)
lgnature ofPreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applicr (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.16S
Contact: Alex Fox
Client: Synagro
284 B
Page 1
Report Date: 7/14/2022
oger Road Project: Mt. Holly
MocksviIle, NC 27028 Date Sample Rcvd: 7/7/2022
Meritech Work Order # 0707221-07 Sample: Mt 1 Grab
Parameters
Results Analysis Date
7/7/22
Reporting Limit Method
% Total Solids 1.94 % 7/8/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,812 CFU/gdry wt 7/7/22 130 CFU/gdry wt SM 9222D
Meritech Work Order # 070722108 Sample: Mt 2 Grab 7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.93 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,826 CFU/g dry wt
7/7/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 070722109 Sample: Mt 3 Grab 7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.92 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
3,315 CFU/g dry wt
7/7/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 070722110 Sample: Mt 4 Grab 7/7/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.94 % 7/8/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 3,515 CFU/g dry wt 7/7/22 130 CFU/g dry wt SM 9222D
Meritech Work Order # 070722111 Sample: Mt 5 Grab 7/7/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.95 % 7/8/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,398 CFU/g dry wt 7/7/22 130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
s
Contact: Alex Fox
Report Date:
Page 2
7/14/2022
Client: Synagro
284 Boger Road
Project:
Mt. Holly
MocksvilIe, NC 27028
Date Sample Rcvd:
7/7/2022
Meritech Work Order #
070722112 Sample:
Mt 6 Grab
7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.92 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,367 CFU/gdry wt
7/7/22
130 CFU/gdry wt
SM 9222D
Meritech Work Order #
070722113 Sample: Mt 7 Grab
7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.99 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
3,655 CFU/g dry wt
7/7/22
130 CFU/g dry wt
SM 9222D
I hereby certify that have reviewed and approve these data, (oc,
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

❑ ❑ ❑
U
u,
LA
z
v
CL (DCD C
S
6
,r m
x
fD Q
r-
i
m
r�r -
O
°Y
M.
-
m rn
D
O
:3
s
3
Q
ZY
a y
a
�.
Ca
-�
N it
�//�{ �/
9
l
rD
D
n0
n
Z
-�
Lu
n
Q OrD
O
m
�
o
N
ai
3
M
0
w
W o
c
rt
rn
m
(D
9
A
Ln
n
rD
Q
•
N
L
Vl
3
3 ❑
T
m o
t— ro
:3
z
Z o
-
n
z
y ti
3
CL
V
3
Mt
w
K
rD
Ln
I
'a
LA
ajaq
('�
�,
M
ran m
$ rD
rG
^
w
a_
m
'_
m
Q
R <
a
v
c
O
v
Ko-
c
C
Q
o
r
.Z7
3
r
c1
C
Pp
ro
rD
rrt
3
�
r
— C
0
d
N
W.
rD
Ve
O
CL 70
a
-
C
x r
rD
ry
tr`a
m
�'
-n
O
-p m T -0
a• x a
z
�
,
o.
•
�
o
C C (�
'� rn
7t
o �
❑
0
c`
n rD m
O p
r.fb
�
D
ro o0
,
ID
L,-, �'
a�,
vrD
N
ma
O
C
'o
2
❑
o m'
o
O
n =
p
A a
O
�c

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 07/06/2022
Reported: 08/09/2022
For: Mt Holly
Comments:
4 1TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
220706-33-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
24.2
EPA625-R-92/0 07/06/2022 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

0 7 17 I
��
:
k
C
CD CD CD CD C / e �
$°
U
}
} ( S k (a S k � \ �
�£
%
® ® � \ § k
)
2
§ �
E
j ) J J
3 3 .. 3
$
E E E
RI
K
}}
!
.0
§
eE
/
0
rL
}
/ /
CD CD
CD
. ,
�
o
.
) ) ) )
k
3 3 3
2
\■
f
E 2 2 9
E « « «
if
}
/
{
pi3
( cn
k�
®
7 ƒ / / 3
2 / \ }
) w § CD /
-
CD
CD
0
az>
kgkk@»®
.
� E 7; r
�7 \z'=3
7z>r
a =ƒram
PO Bo 2289 Statesville, NC 28687.704 872 4 97
A234

%VS R
(older, more conservative method)
%VS in 1 0.7903 - Enter in
%VS out 1 0.74071 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 24.20
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 6.28
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

STATESVILLE
ANALYTICAL
Synagro
284 Boger Rd
Mocksville, NC 27028
Entered: 7/6/22
Reported: 8/09/22
Sample ID: 220706-33-01
Analytical Results
For: Mt Holly
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids
Volatile Solids
% Volatile Solids
Week
1
0.62
0.49
0.7903
Week
2
0.64
0.49
0.7656
Week
3
0.54
0.41
0.7593
Week
4
0.56
0.43
0.7679
Week
5
0.51
0.37
0.7255
Week
6
0.54
0.40
0.7407
Volatile Solids Reduction
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
.7903 - 0.7407 X 100 = 24.2
0.7903 - (0.7903 X 0,7407)
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

30 Day Bench Worksheet
Sample ID # 220706-33-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.62
0.49
2
0.62
0.49
3
0.62
0.48
Average:
0.62
0.49
0.7903
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.66
0.51
2
0.64
0.49
3
0.62
0.48
Average:
0.64
0.49
0.7656
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.40
2
0.56
0.43
3
0.53
0.40
Average:
0.54
0.41
0.7593
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.58
0.45
_
2
0.55
0.42
3
0.56
0.43
Average:
0.56
0.43
0.7679
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.54
0.34
2
0.50
0.37
3
0.50
0.40
Average:
0.51
0.37
0.7255'
kIk"i DI DIN1511
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.56
0.41
2
0.54
0.40
3
0.51
0.38
Average:
0.54
0.40
0.7407
Van Kleeck Reduction: 0.7903 - 0.7407 X 100 - 24.2 %
0.7903 - ( 0.7903 X 0.7407)
Final Result: 24.2%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly
WWTP Name: Mt Holly WWTP
Monitoring Period: From 10/01/2022
WQ Permit Number: WQ9001863
NPDES Number: NCO021156
To 12/31/2022
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt, 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If anplicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo, Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6"
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
CFU
273,292
397,201
685,185
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
1
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt, 3 X
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt, 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
No vector attraction reduction alternatives were performed
(Inj ection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
X "I certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503,33/15A NCAC 02T.1107 have been met '
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to detennine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Dom Shoudt Division Manager Wastewater
Preparer Name and Title (type or print)
4 Z,*� 7—
Alex Fox TSS Synagro ^`
Land Applier Name and Title (if applicable) (type or print)

Zx�-z3
gnatur of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T,1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: A. Fax Page 1Report Date: 10/13/2022
Client: Synagro
284 Boger Road Project: Mount Holly
Mocksville, NC 27028 Date Sample Rcvd: 10/4/2022
Meritech Work Order # 100422235 Sample: MH 1 Grab 10/4/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
1.61 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
397,516 CFU/g drywt
10/4/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 100422236 Sample: MH 2 Grab 10/4/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.61 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
273,292 CFU/gdry wt
10/4/22
130 CFU/gdry wt
SM 9222D
Meritech Work Order #
100422237 Sample: MH 3 Grab
10/4/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% TotaI Solids
1.60 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
518,750 CFU/g dry wt
10/4/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
100422238 Sample: MH 4 Grab
10/4/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.59 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
389,937 CFU/g dry wt
10/4/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
100422239 Sample: MH 5 Grab
10/4/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.60 %
10/6/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
325,000 CFU/g dry wt
10/4/22
130 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 10/13/2022
Project: Mount Holly
Date Sample Rcvd: 10/4/2022
Meritech Work Order # 100422240 Sample: MH 6 Grab 10/4/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.62 % 10/6/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 685,185 CFU/g drywt 10/4/22 130 CFU/g dry wt SM 9222D
Meritech Work Order # 100422241 Sample: MH 7 Grab 10/4/22
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.60 % 10/6/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 318,750 CFU/g dry wt 10/4/22 130 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. �a - Z��z
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

C
❑
❑
❑
Ln
L,
�K
o
fD
4
�•
�
m
"
��
3 �
CD �
O
„
r
p
!�
-+
f
O
3
M
C
C
C
�
3
0.
\ rot
m
fD A
3
cr
c
CY
6
c
ra
*
`,/J
L J
0
fl
3 c 3 Z
m
a
3 0 F rn
n
Ln
_
CD
s
o
m n O
� V Z
O
CL
Ci I
a
�t
�-h
I'J
o^^ o z
n
o
�
LA
rt
G
v 3 .,� rn
O
oc
u,
rt
ro v
Q
o
c
�
as
o
n =
{'}
0
`c
�
o
Qj
D
O W W p
n
o
n
�
N
� w
n w
ti
v
d
fl
N
o
w
O N 0
3
�'iFR FRr)
00
N
a
3
s
G1
N
ro
` D
rD
Q
g
D
n
J
o
w
❑
0-(
-I
}jS
y
�
N
7
Q
r-
Z
o f
m
O
m
rD
p
oo
vi
n
rD 2
° :E
1
^
�c
ro
�
ro
fl
N
ro
c
[Ir
�
•*
v
v
m
0
(
�
1
n
m rD
ro
+
orD
�(
c
O
o
rt
to
x M
�ct
-0
m
-n
-0 Z
arc
T�•
n
m
o
m
2
VJoa
n,
v
:E �
c
1
^^nn
❑
as
y
'
cmi
_El
+
rD
J�
I
C) .1
0
#
a
N
A
Q
d
,
•V .�j
N

%VS R
(older, more conservative method)
%VS in 1 0.4700 - Enter in
%VS out 1 0.40001 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 24.82
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 14.89
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 10/04/2022
Reported: 11/14/2022
For: Mt Holly
Comments:
4 STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
221004-48-01 30 Day Benchscale MT Holly
Respectfully submitted,
X�- � � " �-' J, 1�1�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
21.0
EPA625-R-92/0 10/04/2022 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 221004-48-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

w
�
N
a
tk
v
ti
v
�ro
d
v
T
X
fi
5�
U
3
�
a
v
g
� .Dr
N
OC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 5

30 Day Bench Worksheet
Sample ID # 221004-48-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.60
0.48
2
0.60
0.47
3
0.60
0.47
Average:
0.60
0.47
0.7833
WF.F.K 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.61
0.48
2
0.60
0.48
3
0.61
0.47
Average:
0.61
0.48
1 0.7869
WVVIC 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.62
0.48
2
0.62
0.42
3
0.62
0.47
Average:
0.62
0.46
0.7419
WF.FK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.59
0.45
2
0.59
0.44
3
0.59
0.45
Average:
0.59
0.45
0.7627
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.57
0.44
2
0.58
0.43
3
0.57
0.43
Average:
0.57
0.43
0.7544
WFFK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.54
0.41
2
0.53
0.40
3
0.54
0.40
Average:
0.54
0.40
0.7407
Van Kleeck Reduction: 0.7833 - 0.7407 X 100 = 21.0 %
0.7833 - ( 0.7833 X 0.7407)
Final Result: 21.0%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

STATESVILLE
ANALYTICAL
Analytical Results
Synagro For: Mt Holly
284 Boger Rd
Mocksville, NC 27028
Entered: 10/4/22
Reported: 11/14/22
Sample ID: 221004-48-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids
Volatile Solids
% Volatile Solids
Week
1
0.60
0.47
0.7833
Week
2
0.61
0.48
0.7869
Week
3
0.62
0.46
0.7419
Week
4
0.59
0.45
0.7627
Week
5
0.57
0.43
0.7544
Week
6
0.54
0.40
0.7407
Volatile Solids Reduction: 0.7833 - 0.7407 X 100 = 21.0%
0.7833 - (0.7833 X 0.7407)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.4 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

SECTION 6

Agricultural Lime Application Log
Year: 2022
Project: MT Holly
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
CAA-41-1
(i.2
U.0 I /AU
LT-46-1
5.8
O.OT/AC
1 T/AC
08/01 /22
LT-46-2
6.2
O.OT/AC
LT-46-3
5.5
O.OT/AC
1 T/AC
08/01 /22
LT-46-4
5.9
O.OT/AC
LT-46-8
6.6
O.OT/AC
MG-37-1
6.5
O.OT/AC
GA-41-6
6.3
O.OT/Ac
GA-41-14
6.0
O.OT/AC
* Lime is ordered and will be spread soon

SECTION 7

\
c
\
\
K
z
\
a
=G w
± z #
¥ /
§ g 2 .� \
CO
C
2 =
2 E\
o5
2z
z
z
cn
m
c
w
C
2 =
2 E\
oe
2z
z
z
cn
m
c
w
z
x
co CD
co CD
0
\ U \ \ §
z \
zCL \
k B
Mn
uo
Qo
> >
J «
- CO-
k \
n
k 2
� o
a =_
��
/
_ NLO_
N ®
2
2
2 0
\ N/
2 0
N/
\
\ \ =
®7
F
%
§
F
%
§
0
k/
m e
) 04
±
m C)//
m o
/
® z =
�
k
3
-
'
/\ƒ \ \
k
U)\\ k\
tm o
}\
o
} 7
§
}=G E
&
e \ > m
§
co
\
g 2
0=
/
oo
u u
/
cn %
cn (0
t0o
0o
/
a
@ r
) /
a
a
cu
\
\
2
x E
z/
tm
E$
z/
E$$
2 )
2
u g
u
m
z
z
/ /
2
d_ 2
2
d_ m
�
Q 9
.uoo
§ 2 6 6
.moo
§ 2 6 6
a
§
CD
0
§ -
0
C _
2 E
/
E
/
E
) 6
§ )
= 9
®
= e
§
C
)
o
z _
% )
z _
§
/
m
/
\
)^
§ \
E
u u R
«
§ \
u u R
w «
ƒ /
¥
q
/
f
>
S E /
.,
E
§ 0
%
§
m .
'
. ,
u a
t% 2
,
J u a
'a 0) 3
�
Q k
F =
E _
2 Cl)
¥
¥
*
/
0)o
/
{
w
u Q
w
u
0
^k
k
C
2
{
k /
{
n k \
ca
w a a
w a=
_
.
« n
.
k=
m
o
.
k=
Cl)u*
o
z
_y 2
m
w
m
w
k 'j
E
= E
{ /
} 3
Co
� \
\k
/ \
} \
E /
/ y
\ \
�E
« e
/ �
E k
§ /
E a
/
f

M
C)O
O
c�
N
}
LL
c)
N
m
d
C
O
i = N
O M
E N
4-O
C Z
Z
M
Z
(n
cn
a
cn
w
0
Z
m O
O
a
R
Z
o
N
U CD
7
N
I-_
U
LO
CO
N
Q
m
C
co
r-_
N
m
N
O
c
—
C
co
N
r--
N
U
N
N
R
N
U
Q
cn O
—
C
c
0
2
Ncn
�
Q
rn
O
Z CDM
C
O
O)
�
�
O
>O
O O
N
�
Y
tm
m
—
cn
CD
O
C
O
3
a
o
ME
tM
Cl)
N
O
O
a
j
N
Z O
tm
E
e
>
R
U
(co
O
Z
N
`
M
0
Z
—
Y
N
i°
m CD CD
ENoo
N
J C
0
r
G
co
~
�
a
rn
�
E
c
C
Cp coZ
O
co
�n
O
+r
a
O
R
Na)
U
U
(o
E z3
w
Q
E CLO)
U
v C a)
O LL
M ^
p
O
U N
C
Mna
m
cc)C
0
U
m
LU
0
r
U
O
�
c
tm
U
)
N
N
O
Q
U
O
E m
E
_
o
Z
cn J
H

M
CD
O
O
Cn
N
LL
p
0
C
N
c)
co
a)
m
y
C
r
fC
N
i
QN
i
O
N
w
(Q
O _ E _
co Q Q
U E O a) O O
co U U co
U m E E O O 0 X
>, >, O- M >, X X — a)
U U N y : N N co N a)
m a� a� a, (onE N m m X )
m cUi cUi O m C) O O O — y X
O O O X O E O w N m m N 0 = O N- O .— O)
C 0 0 N � C �y L 0 m m>> m m a) E� .0 � L L .c r a j
m o (LU (LU o a M U CO CO m m ( LU m 0) m m 0 m o �_ m m a a m X
U `..' `..' Q U `..' C C 'O O O w .� C 'O
X o 0 0 m o x a� O O O m c c m o- 2)� zi o
a) o o U U a) Q Q Q o E E E E C y C O U a s (n (n N—
U
C
N Z
o e \ Q Q
m W 7 fA — tm — C C C C Di M C9 0 — Q—
U fA CC
Q m m U U U W 2 Y `1 Z Z Z O C. d d 0) 0) N N
C
O m
U) m
U)
m N
m
a) Q
O O Q
N o
L C
C
�_
N C y
a) .0 C
m
O O
0
O UL
OL i
a) n3 a-
Q U) :5
y o o U)
7 "O Lo Lo a)
U
i
U
E
y C_
p a) p=
C a) n p
4 C
C
p
CD
maU) p p 7
-O L a) �. i
�j
0+
C
U Zi OY
m r)CY
� a) y
a) C N �
O m U)
N
= E
O y
C i
O �\
O
C Lo O
m a) O
a+
_
.y
Z>
O
a) --I:- CY
E
y
y
R
> O a)
E U 'N
0 C a)
O C
m U)
a) O
O
O
E
a) (n m
O U
N m
-p m C Q
vi
. C a)
O
ch O
) a
O
C L
a) 0 0
a) O U)
y E U
CD
Q
O W
tm
C
N Lo a)
U) E .Z'
a) L
N
O
-Q
C
m m
m
7
rz —
O 0�
L U
rz—
E
— Z
O
O O
a E
U y U)
N m >,
N a)
E
O
U) i
3
c
rz
m
.N
Lo Lo o a) M
o c E
cn
U)
E 73
> U)=
a—
�_
m
cA U)
y
U)o
N
d
V CO E
"O
.O "O
N
m
U C
a O p y—
Q E N M
C m m
m
z N
a)
m
O CO C .E
N N a)
o O
fq
C
Q Q N
r
o Q N
N a)
n3
rz
a
is
N N
C
[� O L O
N m N N
,B z
a
E
m
T a)
a) 0_
a)
_
N Z> y
_ _
i O
M
p
U C E
Q N
Mv�i
U) Q
co U) n3 U)
w o 0
3
'� a)
—
d
E E Q m
; Q
U
> NM
O
ry�� C
U)—c
O L
YC O
C)
Q
O
O
N>E
CD p
m
OL
LL
LUU>U OLLo
X O
zwO
Q
}cM)
n)
aw�
U)
�
>
o
a
a)
o a-0
O U D
ow
i C
O L
>
C
a
C
Q
L L O—
O
y.E
U U)O m
N
a) a) .O
( L
V
y
_-
O a)
O C C
x
N
2� N 2� U)m
C:
O a) Q O
"O L
y
M
a)
_
a)
N
O
N
N
lN
CD
p�
Q O
m
m
n
CDC m
CQ
O
O
O U
m a)_
My
Mn
Q
L
Q a) E
o
N C N C
E U) t
(1) m
C
y
D
a)
p m y
w U a)
cn
o�� o
o
o -0-0�o
m a)
- aa))
>
C
+
CDa) U`
O .0 - C
-C m U O
o
N
d U
U
r
O
a) O O a)
U) >
a)U
Q
y
U)
cla
0)N
L
E
O O
O
L C
m C:
N
N
a
OU �' C a) >
N
X L
a) >
y
m
L)
m
L
E C O E a)
m
a) L °� C C
m O a) U
a)
a) n3
y
a) m
E>
Z
J LL — .N LL
m m O
LL C C C
+� E
H
m

o
C)
N
CD CD
co
>-
L
00
N
_0 U �
Z
ai o
x 0 a,= o
0 0 > LO
CO
o
L— r r
O kC
O O O
E Z Z
z
O
z
—
cn
a
cn
w
o
= r CN
O M
D O O
E Z Z
z
O
z
cn
a
cn
w
Z
x N m V
m 0 0
m 0 0
O
C 00
00 0
Q (n p
M
M
C.
—
Z O
Z O
N
i
0
O O
Mn >
V C) C)
C) CD—
Q0
— (0V
LO
0 LO
Q
U 00
U (0
N o o
Q
N C) CD
m
N M
N N
m
m
N
N
o o
c —
c �
o O
c
c coo
N CO
N N
0
U
(0
N
N
(0J
o
R N
U Q
N
U Q
V
00
cn
V) O O
co
__ N
0)(A CDO
CD
_ C N
N
O
c
0 2
cncn
c
0 2
0 0 U
Z
C
'
N -0 M
D-0 a) Cl)
CDZ a) CDC
Q O
Cl)
Z a) CD CDC
Q O
CD
C
Q c E
a)
H Z (n (n
R
0
C C
D O O
O
co
O
N
co
tm
d d
Y 00 00
CD O
Y
t
U U
m—
v
cn
—
cn 't
L
D o o
, o 0
3
a
-Io
a
o
5i
O
!-% tm 00
E
O
M^ a) N
E
�=
to
U J
(B
C) C)a
C) C)
CD CDa
CD O
=
j
i
x
N N
Z CD
01 a
N N
Z O O
tm e
E
>
W a
C)E
�
c U
�
U
M
z
z
L NCD
M
M
O —
z Y N
O
z Y
N
m BLOC)
y�oo
ke
ccN
E_ Noo
ENoo
co
G a0
J C
()
J C
()
O
a0+
p —
0 �
a0+
p
0 kn
M
o O
a (D
t
t
g E
E E
E
E E
E
U
to
C = 00
to
C = N
E
O O
CC
O N m
z Q
O N m
z C. c0
(D (D
a
CD0
0
m
0 0
'6
mW
AQ.
w
�
ma) a�
U 0 o
Q c�i
m
U 0 co
Q
00
U
vi vi
U
> 0 O
0 0 L`, L`,
%
0 0 L`,`, �
%
O
N
V ■ c_ w
"
U Ntm
S
U N
O) 0)00
� O J w
C m
C m
'
0
L Cl)
()
d
U
U M
N
W O
U
LV O
U
O
CO
N
,$tiuk'x 4,yki ON
r
r
fr
C
C
tm
a �
s;
_
'"' > Lo
N
'"' > (D
OR
C:)N
C)N
C)
U
I-
to
N
ca
Q
'F.''ar .�
Q
o
Q
\ (O
0
U
Y p r
1HVA4,i '� R
N
E E
+'
= O
N
E E
+'
= o
z
+n N
cn J
N
H
cn J
m
H
N0
� .o
.L
w E
E
O
� U
co -0
a) Z3
LL
2
V)
Q H
O
O U
Q U
N �
CO 0
m
Y O
m �
� U
m
`o
E Z
a) 0
0 E
O
a) w
E c
a) m
N O
c �
E -co-)E
c M
O o
M
O
c

O
C)
C)
C)O
�
co
}
LL
w
O
N
cu
C
O O
i= N N
M—
2 E N N
O p p
- Z Z
Z
M
O
Z
_
cnE
cn
a
fA
W
C
y 0
i= N N
O M—
N N
O p p
Z Z
Z
M
O
Z
_
cnE
cn
a
I fA
W
C
y 0
i= N N
O M
N j
O p p
Z Z
Z
M
O
Z
cn
cn
a
I fA N
W
O
Z
co C) C)
co 0 0
co 0 0
i
O
a
R
Z O
R N
Z O
fC N
Z O
0
VCD CD
CD CDV
CD CD
N
7 N
LO
7 LO
O
7
U c')
U c')
U (O
No CDQ
o
No CDQ
No o
Q m
N N
N N
N N
m
M
M
N
N
N
CO C)c
c _
o
CO CDc
c _
T
�o C)
c
c m
N N
N N
N N
N
N
N
U
N
R N
U
N
R N
U
N
R N
V Q oo
V Q Oo
U Q
cn C) C)
—
cn O C)—
r co
v) o o
— M
a)
_
a)
0
15cn
O
�
Z CD CDO
Q rn
Z tm CD CD
Q co
co
O
Z CD CD
Q
C
O
O)
D CD CDD
CO
C
O O
C CO
0 O O
C MO
N
O
Y 00 0°
Y
Y o rn
tm
VLO
fA Ln
N
fA (O
co
0)
C
O o o
O o
O 0
3
N (V N
a
o
N o
a
o
N o
a
o
-EE CC
o
C N
ME C
G
r
N
=
CD CDG
O O
O)
CD CDG
O O
O)
CDC)
O O
j
N N
Z O O
o
E
N N
Z O O
o
E
N N
Z O O
O) o
E
>
M (0
r U
M L
U
M �
c U
m
M
0 — c
m
M
0 —CC)
m
M
0 — co
L
N O O
E
y 0 0
E
N O O
E
co
J C
C)
J C
U
J C
U
r
Cl)O
0
00
0
O N
a LO
a (o
a
E
E
E
v
N in in
c
=
N in in
C
=
N in in
c
=
C
O
f° a LO
Z
C
O
M a LO
Z
C
O
M a co
Z
t
R U' U'
R U U
R U U
a
C O O
R
r O O
R
r O O
R
0 a) a)
() U LO
0 a) a)
() U LO
N a) a)
() U Ln
E ��
U U
W Q
E ��
U U
W Q
E L L
U U
W Q
E � �
c)
E � �
c)
E � �
c)
O a 0 N
O
ME
O a 0 N
O �` �`
ME
O a 0 N
O �` �`
"
ME
CO
y i
C) N
o
V e O
y i
U N
o
V e Ln
y i
U N
o
V 00
N
O) m I�
O) m a0
O) m a0
C
C
C
0
O
U O
?� U
?r U LO
0
W
r U
W o
r U
W
r U
C
O
C
C
C
Q
cotm
N
CO
> M
N
'"' > C:)
N a0
(0
> (O
N 00
C)
O
O
QQ
=
o (O
Q =
\
Q. _
\ N
o
°'
E �'
E �'
E
t}/! O
x
E
x O
E
x CD
Z
fA J
H
cn J
H
cn J
H

rn
o
N
O
co
>-Z
LL
w
O
co
c
O O
i= N N
O M
E N N
O p p
Z
Z
O
Z
—
fA
cn
a
fA
W
C
y 0
i= N N
O M
E N N
O p p
Z Z
Z
O
Z
Cn
cn
a
fA N
W
O
Z
m o O
m o O
i
O
C.
R
Z O
R N
Z O
N
V CD CD_
V CD CD
N
7 N
_
O
7 00
U m
U o
N CD CDQ
C CD CD
Q co
N co
N
m
m
N
N
Co o
c —
c-
�O CDc
c
(0
N co
N
N
N
U
N
R N
U
N
R N
U Q
U Q lid
N
fA C) C)—
C N
fA O O
— C
N
—
cn
N
—
c
OZ
7
tm 0 0
Q r-_
N
7
Z 0 0
Q co
N
C
O
O1
CD
O
Y CD CDCDNCD
Ot
v
— Ln
c
— Ln
cn 't
O o o
O o 0
a
3
a
o
o
ci
ai co
ME C
L
tm N
ME C
G
a.+
to
CD CDa
C) CDO
CD O
O
a
0)
j
N N
Z O O
01 e
E
N N
Z CD C)E
e
>
c
c U
�
U
Z
Z
m
m LO CD
M
O —
Y N
m
m co C)Z
M
O — co
Y N
Ln
N O O
E
N O O
E
N
J C
C)
J C
U
M
a Ln
a co
a,
E
E
v
to in in
c
= ao
to in in
c
2 rn
N
C
C O O
O �p �p
M C. Ln
Z
C cn cn
O �p �p
M C. Ln
Z
R (D (D
R U'(
a
O O
R
c O O
R
N N N
E ��
U U 00
W Q
N N N
E L L
U U O
w Q
E co co
U
E co co
U
O C. O O
O LL �
ME
O C. O O
O �` �`
"
ME
CO
U N
V N
a
U N
V e Lo
Mn
m cc)
m cc)
C
0
2
2r U co
?r U co
E
W O
U
LV N
U
O
r
r
C
O
C
C
a1
O
(
> (0
> Lo
00
O
C)C)
c.)
ca
Q
ty/!
rn
N
o
N
o N
o
O
C
N
E
=
C
N
E
=
m E
rn 6
d
R E
rn
CDU
d
Z
fA J
H
fA J
H

rn
CD
CD
Cn
N
LL
p
0
C
N
w
m
y
C
r
fC
N
i
QN
i
O
N
w
(Q
O _ E _
a a
U E O a) O O
co U U co
U m E E O O X
>, >, CL >, X X — a)
U U N y : N N co N a)
m a� a� a, (onE N m m X )
m cUi cUi O m C) O O O — y X
O O O X O E O w N m m N 0 = O N- O .— O)
C 0 0 N � C �y L 0 m m>> m m a) E� .0 � L L .c r a j
m o (LU (LU o a M U CO CO m m ( LU m 0) m m 0 m o �_ m m a a m X
U `..' `..' Q U `..' c c 'O O O w .� C 'O
X o 0 0 m o x a� O O O m c c m o- 2)� zi o
a) o o U U a) Q Q Q o E E E E C y C O U a s (n (n N—
U
C
N Z
o e \ Q Q
m W 7 fA — tm — C C C C Di M C9 0 — Q—
U fA CC
Q m m U U U W 2 Y `1 Z Z Z O C. d d 0) 0) N N
C
O
y � U) m
m N
a) Q
N o
C
C
a) 7 y
m
O O
0
O UL
OL i
a) n3 a-
U) :5
y o o U)
7 "O Lo Lo a)i
U
U
y C_
Q
p a) p=
C a) n p
C
7
CD
U) O �
'U a) �/
4
0
O
�
U Q
m
� a) y
a) C N �
O m U)
N
=
O y
r)CY
O �\
m
a+
_
C i
Z>
O
O
C Lo O
E
a) O
.y
a) --I:- CY
t
> O a)
U 'N
0 C y a)
O C
m U)
a) O
y
CD
O
a) (n m
O U
N m
-Q m C Q
y
. C a)
O
ch O
) a
O
C L
a) 0 0
N O O
y E U
Q
O W
tm
C
N Lo a)
E .Z'
a)CD L
N
-Q
C
m m
m
7
rz — ay+
O 0O
L U
rz —
O
— Z
O O
U y U)
N m
O
U) i
O
a
.N >,
Lo
cn
3
c
rz U) m
Lo o a) M
E 73
o c E
E
m
—
y
.E
> U)=
�_ U)o
cA U)
m
a�i
v CO E
o
o o
a)
m
U
a O p y—
Q E N M
C m m
m
z N
a)
O CO C .�
N N a)
415 O
fq
C
N
Q Qrz
r
O Q N E
N a)
n3
a
.�
N w
C
[� O L O
N m N N
,B z
a
E
m
T a)
LO
a) 0_
a)
_
N Z> y
_ _
i O
M
Q
U C E
Q N
M
U) Q
co
m U) n3 U)
w o o
3
'� a)
—
Q
m
E Q m
m
a Q
> N"
O
, . • a)
co C
E
O L
C O E
Q
a)
O E
U L
[�
Q c c)
Y> N
O ro .o
C
L
a) O
LU
O
O N C C
a C CD p
C O m
,�
LL
U Q O
O
L X O
n} `)
a) E
E w a)
o z
w� w
a)
�
L
> o
o
a)
L E
w E .o a) �
O U D
o
L C
'�
O L
>
j
a
C
Q
ay+ a)
L L O—
O E
yt. U y m
O N
L
a) a) .O
� L
V
y
�
_- C
O a)
O C 'L
x
N
N U) m
:
O 0
Q-0N
73 L
C
M
a)
N
y
N
lN
CD
Q�
Q O
m
m
n
o m
CQ
C
O
O
O U y
m a)_
M
73
Q
Q E
N
E U)
DM
p m
o
N C C
a) m
w U
ay)�
o
o ��
o
a)o
aa))o�
C,
Cl a) U`
O .0 C `�
m U O
o
N U
> d U_
y
C
U) a)
0 U)_
m U) >j U) i
O Q O O
m—
C
a) u "O
a
C
�
o
U Q O Q
U
O
r
> C
U
r
L
O- N
O 0 0 a) a)
m U) >
a)
U
y
y
°iS
L
N O N a)
E a) p U C
a) 0 0
E
_Q
m a)
L '�
c
O
U Q N
a)
OI
p
L O
C N>
N
X i
a) >
U
m
N L m
E C o E a)
m
a) L °� C C
n3 o a) U
a)
a) n3
y
y
a) m
E>
Z
J LL — .N LL
�o m m O
LL C C c
+� E
H
m

�
\
»
/
y
z
2 0 /
o a
a
05
7z
\
z
kCl)
w
z
=o
k
z
J
§
0
CD
L)
\
k
S
«
u
NC
%
_
N
2
2 61)
L
§
=
N
_
§
CD\
/
m
u
-
.5
/
CD
`
7 z
\
0
2
\
E
§
e 0\
2 7
/� CD
g
2
\
/ �
a�
2
#
\
E
\
U) \
U)
7
'
g
2
0 0
©
%
CO
u
u
/
�
\
t
R o
§
7
E
\
§
f-
s
/
2
E
2
%
/
.
u
2
n
z
/CD
0
CC)
.qoo
§
k
CD
\
2
k
§
-
_
>
t
/
0
6
r
)
6
§ \
\
_
@
§
0
)
2 )
2
_
2
G
\ 0
C
CD
k
L
W
\
u
«
R
)
/
E ¥
q
$
o0\
E
.2
%
f
J u \
m
2%
f
3
6
2
a. Cl)¥
u
f
u
=
L
` �`
/
°
^\
«
2
_
�
o
k
w
a
a
_
.
2
©
k E
7
=
m
z
m
w
k 'j
�E
= E
{ /
.! :
§ 2
(onE\&
t o
\k
/ %
\ /
E\
m y
\ \
�E
« e
/ �
E k
/
E§ a
/
f

M
m
O
(n
co
N
LL
pm
0
C
N
N
0
N
a)
y
C
y
fC
N
i
QN
i
o
N
y
C E
O _ _
Q Q
U E O a) O O
y U U U co
N co
O O
U N E U X
>, >, CL >, X X — a)
a) a)
N N 0) y N a) N U O O
N cUi cUi N C) a) a) O — y X
O O O X O O w N N O = O N- O .— O)
C 0 U N � C �y L 0 (6 N>> N" a) E N .0 � L L .c O Q- j
m W W CO Q M U (6 (6 (LU O 0) (6 (6 0 O Z_ a) O Q Q �p X
U `..' `..' Q U `..' c c 'O O O w .— C 'O
X O O o N O X a) 0 0 O N C C N ++ O- 2)� L L zi O
a) o o U U a) Q Q Q o C y C O U Q Q y y N—
U
C
N Z
o e \ Q Q
m W 7 fA 1 al Z C C C C Q M O — Q
U fA CC
Q M M U U U W M `1 `1 2 2 2 2 2 2 Z Z Z O C. d d 0) 0) �i N N
C
O
y >,.— U) (B
(B N
a) Q
Q
N 0
�_
m
O O
0
O UL
OL i
a) n3 a-
U) :5
y o o w
7 "O Lo Lo a)
U
i
U
y C_
Q
p O p=
4E�
C a) n p
4�
p
CD
may) p p 7
-O L a) �. i
�j
�,
C
U Zi OY
(B MCY
a) y
�
a) C)-0 N U
O (B U)
N
=
O y
O ff\
I
a+
_
C i
t5
a)Z>
o
C Lo O
E
a) a) O
.y
a) --I:-o
CY
> O a)
U 'N
0 C U)a)
`� M U)
U)O
O
a) (n m
N m
O
-p M C Q
y a) O
C N
C:,ch
O
O U
U) a
o
L
a) 0 0
a) N U)
y E U
w C
O W
O)
C
a)
-0 U) E Z
L
yr N
-0Q
Q
C
m mO
fC
7
N
i— ay+
O 0Lo
L U
i —
— Z
O O
U y U)
N m
O
U) i
(�
O
a
.N >,
Lo
i
cn
3
c
rz U) m
Lo o a) M
E 73
o c E
a—
y
> U)=
0_ U)o
cA U)
N
CO
VaO
(
U
Ca)
p
m
m
N
zO
CO
� a)
N 0
N
oCc
Om
�
r
o Q N
N a)
15
rz
a
is
N N
C
N L
N (B a) N
(B z
a
(B
a) 0_
+� a) -0
_
a) Z> U) t
i O
p
U C
Q N
M
N Q
m U) U)
w 0 0
3
'� a)
—
�
d
C Q
; C: mO
Q
>, N U
O
ry
ry�C a)
co
—c
L
0-
OE
LLC
,-
M
YN
OLL
LUU>>U
O
O
CD p
O mLL
Q Oo
XO
)
U) aw�
zwO
-
>
o
a
o a-0
O U D
ow
L C
=
O
a)
O
O U) m
a)
�
�
O_'N
LQ
N
N U) m
C:
O 0
Q
73
-0 L
M
N
O N
lN
CD
p�
Q O
m
m
CCxa)
n �
C
O
O
O U
m a)
MN fl-
Mn
Q Q a) E
N
E U) t
C
L D
p M y
o
N C C
a) m
y
a)
w U a)
o�� o
o
o ��
�o
m a)
- aa))
Eo a)(�
0 0.—-
� m Uo
o
N U
>a U_
C
U) a)
0 U)_
(B U) O U) i
O Q O O
M—
C
a) u "O
L
O Q p p
O Q U
O
O
r
> i
fn
U
O
L.L
C
a)
.� O C
O C O O a) a)
7 U L
(B (� a) N
>O
O«
>,
U Q
7
fn
C a)
oiS
x
L
N > a)
C L O O— a)
E a) U C
i
N 0 0
(B a)
d
i C
O
U Q N
OI N M a)
L O O O
OU C N>
N
x
a) >
y
(B
U
C
()
L
E_ O E a)
a) m L E C C
m O a) U
a)
a) M
y
a) (B
E>
Z
0 LL — .N LL
Q' �o (B (B O
LL c
Q'
E E
H
H M