WQ0039053_2022 Residual Annual Report_20230118 (2)

2022 ANNUAL REPORT
LAND APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
Prepared For:
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231B Suirunerfield Road
Summerfield, North Carolina 27358
January 2023

willcox&mabe
SOIL SOLUTIONS
January 17, 2023
NCDEQ-DWR Non -Discharge Branch
512 North Salisbury Street
9th Floor, Office #942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: 2022 LAND APPLICATION ANNUAL REPORT
Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as
specified in the above referenced permit on behalf of Bio-Nomic Services, Inc. (Bio-Nomics) for the above
referenced permit. WMSS compiled this report using data gathered during the compliance year by Bio-
Nomics. This data includes: 1) Class A Annual Distribution and Marketing / Surface Disposal Certification
and Summary Form (DMSDF), 2) Annual Residual Sampling Summary Form(s) (RSSF), 3) AnnuaI Pathogen
and Vector Attraction Reduction Form. (2T) if required, and 4) Analytical Data.
Bio-Nomics distributed a total of 556.24 Dry Tons of residual solids during the calendar year of 2022.
If there is any further information required or questions regarding this annual report please do not hesitate to
contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
SharedlWMSS Projects12015115-18 Bio-Nomics\Phase 09 - ENS Class A Permit12022 Annual Report12022 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions. PLLC / 7231 B Summerfield Road 1 Summerfield, NC 27358 / Rob 336.339.9128 or
Martin 336.312.13961www.willcoxmabesoil.com

Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
NC PERMIT # WQ0039053
Vaughn "Buck" Stevenson, Executive Vice President
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
2022 Greenville Utilities WTP (NC0082139) Dry Tons 556.24
2022 Total Dry Tons 556.24
2022 Total Dry Metric Tons 504.10

TABLE OF CONTENTS
SECTION NO. TITLE
I DMSDF
II RSSF
III PVRF (2T)
IV Analytical Data

DMSDF

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: BIO-NOMIC SERVICES, INC.
PHONE: [phone] COUNTY: GASTON OPERATOR: Vaughn "Buck" Stevenson - Vice President
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
p Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes Ci No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry, tons
_
Recipient Information
Amendment!
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
Greenville Utilities WTP NC0082139
177.5
177.5
City of Greenville
177.5
August
Greenville Utilities WTP NC0082139
378.74
378.74
City of Greenville
378.74
September
October
November
December
Total from FORM DMSDF (sup)
_
Totals: Annual (dry tons):
0
556.24
556.24....... ......... ........
556.24
Amendment(s) used:
Bulking Agent(s) used:
more space is required, attach a
Mona
information sheets (FORM DMSDF (supp)):
Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p yes*
0 No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(including but not limited to items 1-3 below) issued by the Division of Water Resources:
Signature of Permittee
Date
Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
*NO LAND APPLICATION OCCURRED DURING THE 2021 CALENDAR YEAR
DENR FORM DMSDF (12/2006)

RSSF

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or NPDES
#:
WWTP Name:
Residual Analysis Data
WQ0039053
Bio-Nomic Services, Inc.
NC0082139
Greenville Utilities WTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Ceiling
Conc. Limit
(mg g)a
Sample or Composite Date
4/4/22
8/24/22
8/24/22
8/24/22
8/24122
8/24I22
Percent Solids (%)
12.9
12.5
12.3
12.9
13
10.9
Arsenic
8.53
15.1
15.4
12.2
15.2
12.4
Cadmium
0.775
0.8
0.813
0.775
0.775
0.917
Copper
122
122
140
111
157
112
Lead
13.6
33.5
35
27.9
30.1
30.7
Mercury
0.109
1.22
1.28
1.23
1.12
1.4
Molybdenum
2.08
2.1
2.26
_1.94
2.19
2.29
Nickel
12.4
18.6
18.9
16.5
15.8
16.2
Selenium
3.88
4
4.07
3.88
3.88
4.59
Zinc
54.8
80
86.2
73.8
69.8
66.6
TKN
12500
21400
16500
12600
13500
14500
Ammonia- Nitrogen
860
800
813
775
775
917
Nitrate and Nitrite
48
38.5
39.8
38.5
35.7
67.9
Total Phosphorus
1890
3790
3390
2730
3530
3990
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T _1102 (26)
1-J7-013
Date
DENR FORM RSSF (12/2006)

PVRF (2T)

Greenville Utilities WTP is not required by permit to perform Pathogen Reduction or Vector
Attraction Reduction Monitoring, therefore no PVRF 2T Form has been included in this report.

ANALYTICAL DATA

Greenville Utilities WTP is an ongoing annual dredge and dewatering project at the alum lagoon at the
respective plant. Initial calculations for the alum lagoon cleanout at Greenville Utilities WTP indicated
that a bi-monthly (or 6 times per year) sampling frequency should be considered based upon an
anticipated 2,000 dry tons. This project was performed in accordance with a partial lagoon cleanout at
the facility. The residual solids were mechanically removed from the lagoons and stockpiled on site
prior to land application activities beginning. The project only lasted for approximately three months.
Five of the six composite nutrient and metal analyses were collected from the stockpile on the same day.
However, due to the amount of residuals that were land applied (556.24 DT's), only four analyses are
required by permit. WMSS, PLLC and Bio-Nomic Services, Inc. elected to use all six nutrient and
metal analyses that were collected during the two month window of actual land application activities
from the stockpiles to best represent the actual material being land applied. One TCLP analysis has also
been included. The project actually began in June of 2022 and finished in August 2022.

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 4, 2022
Greenville Utility Commision i#I
12.90 % Solids
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.250
12,500.000
25.000
Phosphorus
0.189
1,890.000
3.780
Potassium
0.044
442.000
0.884
PAN (injected)*
0.324
3,236.000
6.472
PAN (surface)*
0.281
2,806.000
5.612
Ammonia Nitrogen
0.086
860.000
1.720
Calcium
0.109
1,090.000
2.180
Calcium Carbonate Eq.
14.900
149,000.000
298.000
Magnesium
0.053
526.000
1.052
Sodium
0.019
194.000
0.388
Sulfur
---
6,020.000
12.040
Nitrate N / Nitrite N
---
48.000
0.096
Barium
-._
---
---Chloride
SAR
__
--'
---
0.43
Iron
---
25500.000
51.000
Ceiling Concen.
(Mg/Kg)
Aluminum
---
96,900.00
193.800
Arsenic
---
_ 8.53
0.017
75
Cadmium
---
0.775
0.002
85
Chromium
---
29.400
0.059_
-
Copper
---
122.00
0.244
4,300
Lead
---
13.60
0.027
840
Mercury
---
0.1090
_
0.000_
_
57
Molybdenum
---
2.08
0.004
_
75
Nickel
---
12.40
_
0.025_
_
420
Selenium
---
3.88
0.008
100
Zinc
---
54.80-
0.110
7,500
Waypoint Analytical 22-097-0001
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
•,I,
willcox&mabe
Prepared By: SOIL SOLUTIONS

Waypoi nt
ANALYTICAL
4/18/2022
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 22-097-0001
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/7/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
To_w e tic 6.loarr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypoint,.
ANALYTICAL
Report Number: 22-097-0001
Client Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID
Matrix
Date Collected
Date Received Method Lab ID
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
57416 GUC-1
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09:00
04/04/2022 09.00
04/07/2022
04/07/2022
04/07/2022
04/07/2022
04/07/2022
04/07/2022
04/07/2022
04/07/2022
04/07/2022
SM-2540G
SW-7471B
SM-4500-NH3C-TKN
4500NO3F-2011
6010D
SM-4500-NH3C
9045D
AOAC 955.01
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 9

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number :22-097-0001 REPORT OF ANALYSIS
Lab No : 57416
Sample ID : GUC-1
Report Date : 04/18/2022
Received : 04/07/2022
Tctwfc (I1r Grown/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 4/4/2022 9:00
Test Results Units MQL DE Date / Time By Analytical
Analyzed Method
Total Kjeldahl Nitrogen 12500 mg/Kg - dry 1940 1 04/14/22 09:30 JPJ iM-4500-NH3C-TKP
Calcium 1090 mg/Kg - dry 388 1 04/13/22 21:22 EAL 6010D
Magnesium 526 mg/Kg - dry 38.8 1 04/13/22 21:22 EAL 6010D
Sodium <194 mg/Kg - dry 194 1 04/13/22 21:22 EAL 6010D
Iron 25500 mg/Kg - dry 77.5 1 04/13/22 21:22 EAL 6010D
Aluminum 96900 mg/Kg - dry 194 5 04/14/22 10:38 EAL 6010D
Nitrate+Nitrite-N 48.0 mg/Kg - dry 36.9 1 04/12/22 15:25 ZBD 4500ND3F-2011
Chromium 29.4 mg/Kg - dry 1.94 1 04/13/22 21:22 EAL 6010D
Arsenic 8.53 mg/Kg - dry 3.88 1 04/13/22 21:22 EAL 6010D
Mercury <0.109 mg/Kg - dry 0.109 1 04/14/22 14:57 ZMT SW-7471B
pH 6.3 s.u. 1 04/14/22 16:03 DRS 9045D
Calcium Carbonate Equivalent 14.9 % 0.1 1 04/16/22 14:10 DXT AOAC 955.01
Total Volatile Solids 32.5 % 0.010 1 04/08/22 16:21 FMM SM-2540G
Molybdenum 2.08 mg/Kg - dry 1.94 1 04/13/22 21:22 EAL 6010D
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Lead 13.6 mg/Kg - dry 2.33 1 04/13/22 21:22 EAL 6010D
Manganese 476 mg/Kg - dry 3.88 1 04/13/22 21:22 EAL 6010D
Nickel 12.4 mg/Kg - dry 1.94 1 04/13/22 21:22 EAL 6010D
Potassium 442 mg/Kg - dry 77.5 1 04/13/22 21:22 EAL 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 9

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanafytical.com
Report Number : 22-097-0001 REPORT OF ANALYSIS
Lab No : 57416
Sample ID : GUC-1
Report Date : 04/18/2022
Received : 04/07/2022
1 z.w c pt GiPar
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 4/4/2022 9:00
Test
Results Units MQL DF Date / Time By Analytical
Analyzed Method
Selenium <3.88 mg/Kg - dry 3.88 1 04/13/22 21:22 EAL 6010D
Sulfur 6020 mg/Kg - dry 77.5 1 04/13/22 21:22 EAL 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture
87.1 % 0.010 1 04/08/22 16:21 FMM L609815
Total Solids 12.9 % 0.010 1 04/08/22 16:21 FMM SM-2540G
Phosphorus 1890 mg/Kg - dry 38.8 1 04/13/22 21:22 EAL 6010D
Copper 122 mg/Kg - dry 3.88 1 04/13/22 21:22 EAL 6010D
Zinc S4,8 mg/Kg - dry 9.69 1 04/13/22 21:22 EAL 6010D
Ammonia Nitrogen 860 mg/Kg - dry 775 1 04/14/22 14:30 ]PJ SM-4500-NH3C
Organic N 11620 mg/Kg - dry 1938 1 04/14/22 09:30 CALCULATION
Cadmium <0.775 mg/Kg - dry 0.775 1 04/13/22 21:22 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 4 of 9

Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticaLcom
Client: Bio-Nomic Servics Inc
Project: GUC
Lab Report Number: 22-097-0001
Date: 4/18/2022
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99678 (RB251)
Analyte: Aluminum
QC Batch No: L610755/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Arsenic
QC Batch No: L610755/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Calcium
QC Batch No: L610878/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Cadmium
QC Batch No: L610755/L609993
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Copper
QC Batch No: L610878/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Iron
QC Batch No: L6108781L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Potassium
QC Batch No: L610755/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Magnesium
Page 5 of 9

Waypoi nt..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: L610755/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Manganese
QC Batch No: L610878/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Sodium
QC Batch No: L610878/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Nickel
QC Batch No: L610755/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Lead
QC Batch No: L6107551L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Sulfur
QC Batch No: L6107551L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99678 (RB251)
Analyte: Selenium
QC Batch No: L6108781L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99678 (RB251)
Analyte: Zinc
QC Batch No: L610878/L609993
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 91031 (NE Cake)
Analyte: Mercury
QC Batch No: L611054/L610645
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 6 of 9

Waypol nt.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanaiyticai.com
Page 7 of 9

Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 22-097-0001
Shipping Method
Q Fed Ex 0 US Postal 0 Lab 0 Other
© UPS 0 Client Q Courier Thermometer ID: I
Shipping container/cooler uncompromised? © Yes
Q No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of Custody (COC) present?
COC agrees with sample label(s)?
O Yes
0 Yes
( Yes
( Yes
Q No
Q No
Q No
Q No
( Not Present
( Not Present
COC properly completed
(Yes QNo
Samples in proper containers?
Sample containers intact?
( Yes QNo
( Yes QNo
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time?
( Yes QNo
Cooler temperature in compliance?
(Yes QNo
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes 0 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Q Yes
Q Yes
Q No
Q No
( N/A
0 N/A
Trip Blanks received with VOAs
0 Yes
Q No (N/A
Low concentration EnCore samplers (48 hr)
T High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Soil VOA method 5035 — compliance criteria met 0 Yes Q No ( N/A
r High concentration container (48 hr)
Signature:
,Brandi Watson
Date & Time:
Page 8 of 9
04/07/2022 06:54:09

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Bio Nomic Srrvict Inc 06:53:05
7621 Whilcpinc Road GUC
`RAIN OF CUSTODY
[e-mail]
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Submitted By
Charge To
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Phone: 7 D J_, 6 9_ Hoop
Fax:
E-mail: V
Sample Information
Sample ID
Lab Number
(Lab Use
Only)
Collection Information
Container Information
Please Write In Desired Tests
Type
Dale
Time
Number
of Bottles
Type
Volume..
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Relinquished -By; (Signature)
Date
Time
Received By: (Signature)
Date
Time
Test Available
Special instructions or Remarks
Nitrogen Series: Total Kjetdahl, Ammonium. Nitrate & Organic Nitrogen.
Phosphorus(Iotal, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium. Sodium, Iron, Aluminum,
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Manganese, Copper. Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium. Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavetent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
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BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 24, 2022
Greenville Utility Commision #2
12.50 % Solids
5.9 nH
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Tort
(Mg/Kg x 0.002)
Nitrogen (TKN)
2.140
21,400.000
42.800
Phosphorus
0.379
3,790.000
7.580
Potassium
0.064
639.000
1.278
PAN (injected)*
0.496
4,958.500
9.9I7
PAN (surface)*
0.456
4,558.500
9.117
Ammonia Nitrogen
0.080
800.000
1.600
Calcium
0.128
1,280.000
2.560
Calcium Carbonate Eq.
10.200
102,000.000
204.000
Magnesium
_ 0.073
_
726.000
1.452
Sodium
_ 0.020
200.000
0.400
Sulfur
---
6,310.000
12.620
Nitrate N / Nitrite N
---
38.500
0.077
Barium
---
---
---
SAR
0.39
Chloride
---
---
---
Iron
---
28600.000
57.200
Ceiling Concen.
(MgIKg)
Aluminum
---
126,000.00
252.000
Arsenic
---
15.10
0.030
75
Cadmium
---
0.800
0.002
85
Chromium
_ ---
84.800
0.170
--
Copper
---
122.00
0.244
4,300
Lead
---
33.50
0.067
840
Mercury
_ ---
1.2200
0.002
57
Molybdenum
_ ---
2.10
0.004
75
Nickel
_ ---
18.60
0.037
420
Selenium
---
4.00
0.008
100
Zinc
---
80.00
0.160
7,500
Waypoint Analytical 22-237-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or<detection limits arc listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By:
SOIL SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 24, 2022
Greenville Utility Commision #3
12.30 % Solids
5.7 off
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0,002)
Nitrogen (TKN)
1.650
16,500.000
33.000
Phosphorus
0.339
3,390.000
6.780
Potassium
0.089
886.000
1.772
_
PAN (injected)*
0.399
_
3,990.200
7.980
PAN (surface)*
0.358
3,583.700
7.167
Ammonia Nitrogen
0.081
813.000
1.626
Calcium
0.I37
1,370.000
2.740
Calcium Carbonate Eq.
3.400
34,000.000
68.000
Magnesium
_ 0.098
984.000
1.968
Sodium
_ 0.020
203.000
0.406
Sulfur
---
6,200.000
_
12.400
Nitrate N / Nitrite N
---
39.800
0.080
Barium
---
---
---
SAR
0.36
Chloride
---
---
---
Iron
---
34700.000
69.400
Ceiling Concen.
(Mg/Kg)
Aluminum
---
129,000.00
258.000
Arsenic
---
15.40
0.031
r 75
Cadmium
---
0.813
_
0.002
85
Chromium
---
93.500
0.187
-
Copper
---
140.00
0.280
4,300
Lead
---
35.00
0.070
840
Mercury
---
1.2800
0.003
57
Molybdenum
---
2.26
0.005
75
Nickel
_ ---
18.90
0.038
420
Selenium
---
4.07
0.008
100
Zinc
---
86.20
0.172
7,500
Waypaint Analytical 22-237-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits arc listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By:SOIL SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 24, 2022
Greenville Utility Commision #4
12.90 % Solids
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.260
12,600.000
25.200
Phosphorus
0.273
2,730.000
5.460
Potassium
0.071
709.000
1.418
PAN (injected)*
0.318_
3,I78.500
6.357
PAN (surface)*
0.279
2,791.000
5.582
Ammonia Nitrogen
0.078
775.000
r
1.550
Calcium
0.112
_
1,120.000
2.240
Calcium Carbonate Eq.
_ 3.800
38,000.000
76.000
Magnesium
0.078
775.000
1.550
Sodium
0.019
I94.000
0.388
Sulfur
---
5,580.000
11.160
Nitrate N / Nitrite N
---
38.500
0.077
Barium
___
__
_
r
Chloride
--
_
--- L
Iron
---
28,700.00
57.400
Aluminum
---
122,000.00
244.000
Arsenic
_.-
12.20
0.024
Cadmium
---
0.775
_
0.002
Chromium
---
81.400
0.163
Copper
---
111.00
0.222
Lead
---
27.90
0.056
Mercury
---
1.2300
0.002
Molybdenum
---
1.94
0.004
Nickel
---
16.50
0.033
Selenium
---
3.88
0.008
Zinc
---
73.80
0.148
Waypoint Analytical 22-237-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
0.39
Ceiling Concen.
(M/K)
75
85
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
4
willcox&mabe
4,300
840
57
75
420
100
7,500
Prepared By; SOIL SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 24, 2022
Greenville Utility Commision #5
12.90 % Solids
5.8 pH
Parameter
Nitrogen (TKN)
1.350
Permit No. WQ0039053
Mg/Kg Dry Weight
(% x 10,000)
13,500.000
Pounds/Dry Ton
(Mg/Kg x 0.002)
27.000
Phosphorus
Potassium
0.353
0.076
3,530.000
762.000
7.060
PAN (injected)*
PAN (surface)*
Ammonia Nitrogen
Calcium
0.336
0.297
0.078
0.130
3,355.700
2,968.200
775.000
I,300.000
1.524
6.711
5.936
1.550
2.600
Calcium Carbonate Eq.
Magnesium
Sodium
3.700
0.085
0.019
37,000.000
853.000
194.000
74.000
Sulfur
Nitrate N / Nitrite N
4,600.000
35.700
1.706
0.388
9.200
0.071
Barium
Chloride
Iron
Aluminum
29,700.00
119,000.00
59.400
238.000
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
15.20
0.775
81.400
157.00
30.10
1.1200
2.19
15.80
3.88
69.80
0.030
0.002
0.163
0.314
0.060
0.002
0.004
0.032
0.008
0.140
SAR
0.37
Ceiling Concen.
(Mg/Kg)
Waypoint Analytical 22-237-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
..t.1
willcox&mabe
75
85
4,300
840
57
75
420
100
7,500
Prepared By: SOIL SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 24, 2022
Greenville Utility Commision #6
10.90 % Solids
5.8 pI-I
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.450
14,500.000
29.000
Phosphorus
0.399
3,990.000
_
7.980
Potassium
0.059
594.000
1.188
PAN (injected)*
0.370
3,701.500
7.403
PAN (surface)*
0.324
3,243.000
6.486
Ammonia Nitrogen
0.092
917.000
1.834
Calcium
0.135
1,350.000
2.700
Calcium Carbonate Eq.
_ 6.800
68,000.000
136.000
Magnesium
_ 0.071
_
706.000
1.412
Sodium
0.023
229.000
0.458
Sulfur
---
5,830.000
I1.660
Nitrate N / Nitrite N
---
67.900
0.136
Barium
---
--
---
SAR
0.41
Chloride
---
---
---
Iron
---
28,300.00
56.600
Ceiling Concen.
(Mg/Kg)
Aluminum
---
125,000.00
250.000
Arsenic
---
12.40
0.025
75
Cadmium
---
0.917
0.002
85
Chromium
---
89.200
0.178
-_
Copper
---
112.00
0.224
4,300
Lead
---
30.70
0.061
840
Mercury
---
I.4000
0.003
57
Molybdenum
---
2.29
0.005
75
Nickel
---
16.20
0.032
420
Selenium
---
4.59
0.009
100
Zinc
---
66.60
0.133
7,500
Waypoint Analytical 22-237-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
•.E.R
willcox&mabe
Prepared By: SOIL SOLUTIONS

Waypoint...
ANALYTICAL
9/8/2022
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 22-237-0006
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/25/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
1clati r 610 air
Pauric McGroary
Agronomist
Laboratorys Liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 20

Waypoint.
ANALYTICAL
Report Number: 22-237-0006
Client Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 SM-2540G WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 AOAC 955.01 WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 4500NO3F-2011 WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C-TKN WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 6010D WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 SW-7471B WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 SM-4500-N1-13C WP MTN
59046 GUC-2 Solids 08/24/2022 02:00 08/25/2022 9045D WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C-TKN WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 SM-2540G WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 4500NO3F-2011 WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 AOAC 955.01 WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 9045D WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 SW-7471B WP MTN
59047 GUC-3 Solids 08/24/2022 02:00 08/25/2022 6010D WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 SW-7471B WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 6010D WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 4500NO3F-2011 WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C TKN WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 SM-2540G WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 9045D WP MTN
59048 GUC-4 Solids 08/24/2022 02:00 08/25/2022 AOAC 955.01 WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 20

Waypoint,
ANALYTICAL
Report Number: 22-237-0006
Client Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NI3C WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 SM-2540G WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 AOAC 955.01 WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 9045D WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 SW-747113 WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 6010D WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 4500NO3F-2011 WP MTN
59049 GUC-5 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NI3C-TKN WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 9045D WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 SW-74718 WP MTN
59053 GUC-6 solids 08/24/2022 02:00 08/25/2022 6010D WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 4500NO3F-2011 WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C-TKN WP MTN
59053 GUC-6 solids 08/24/2022 02:00 08/25/2022 SM-4500-NH3C WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 SM-2540G WP MTN
59053 GUC-6 Solids 08/24/2022 02:00 08/25/2022 AOAC 955.01 WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 20

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number : 22-237-0006 REPORTOFANALYSIS
Lab No : 59046
Sample ID : GUC-2
Report Date : 09/08/2022
r/
Received : 08/25/2022
; f�WI•t p1 L IT/Owbj%
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test
Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 12.5 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Calcium 1280 mg/Kg - dry 400 1 08/30/22 19:26 EAL 6010D
Iron 28600 mg/Kg - dry 80.0 1 08/30/22 19:26 EAL 6010D
Aluminum 126000 mg/Kg - dry 200 5 09/01/22 12:00 EAL 6010D
Zinc 80.0 mg/Kg - dry 10.0 1 08/30/22 19:26 EAL 6010D
Chromium 84.8 mg/Kg - dry 2.00 1 08/30/22 19:26 EAL 6010D
Arsenic 15.1 mg/Kg - dry 4.00 1 08/30/22 19:26 EAL 6010D
Mercury <1.22 mg/Kg - dry 1.22 1 08/30/22 11:51 TJS SW-7471B
Test
Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen <800 mg/Kg - dry 800 1 09/01/22 12:30 JP] SM-4500-NH3C
Organic N 21440 mg/Kg - dry 2000 1 09/01/22 06:30 CALCULATION
Phosphorus 3790 mg/Kg - dry 40.0 1 08/30/22 19:26 EAL 6010D
Cadmium <0.800 mg/Kg - dry 0.800 1 08/30/22 19:26 EAL 6010D
Copper 122 mg/Kg - dry 4.00 1 08/30/22 19:26 EAL 6010D
Lead 33.5 mg/Kg - dry 2.40 1 08/30/22 19:26 EAL 6010D
Manganese 353 mg/Kg - dry 4.00 1 08/30/22 19:26 EAL 6010D
Nickel 18.6 mg/Kg - dry 2.00 1 08/30/22 19:26 EAL 6010D
Selenium <4.00 mg/Kg - dry 4.00 1 08/30/22 19:26 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 4 of 20

Waypoint,
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodfawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytjcai.com
Report Number :22-237-0006 REPORT OF ANALYSIS
Lab No : 59046
Sample ID : GUC-2
Report Date : 09/08/2022
Received : 08/25/2022
4
l aµrrc irl; 6-oar
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test
Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Sulfur
Analytical Method: SM-2540G
Test
6310 mg/Kg - dry 80.0 1 08/30/22 19:26 EAL 6010D
Results
Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture
87.5 % 0.010 1 08/29/22 17:09 FMM L634745
Total Kjeldahl Nitrogen 21400 mg/Kg - dry 2000 1 09/01/22 06:30 JPJ ;M-4500-NH3C-TKP
Potassium 639 mg/Kg - dry 80.0 1 08/30/22 19:26 EAL 6010D
Magnesium 726 mg/Kg - dry 40.0 1 08/30/22 19:26 EAL 6010D
Sodium <200 mg/Kg - dry 200 1 08/30/22 19:26 EAL 6010D
Nitrate+Nitrite-N <38.5 mg/Kg - dry 38.5 1 08/31/22 15:44 ZBD 4500NO3F-2011
pH 5.9 s.u. 1 09/01/22 15:00 ADM 9045D
Calcium Carbonate Equivalent 10.2 % 0.1 1 09/06/22 14:58 DM' AOAC 955.01
Total Volatile Solids 42.6 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Molybdenum 2.10 mg/Kg - dry 2.00 1 08/30/22 19:26 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 5 of 20

Waypoint
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Report Number : 22-237-0006
Lab No : 59047
Sample ID : GUC-3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa n aIytical. com
Project GUC
Information :
REPORT OFANALYSIS
Report Date : 09/08/2022
Received : 08/25/2022
.aur,•c fit Groom/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test
Results
Units
MQL
DF Date / Time
Analyzed
By Analytical
Method
Total Kjeldahl Nitrogen
Aluminum
Manganese
Copper
Cadmium
Lead
Calcium Carbonate Equivalent
Total Volatile Solids
Test
16500 mg/Kg - dry 2030
129000 mg/Kg - dry 203
384 mg/Kg - dry 4.07
140 mg/Kg - dry 4.07
<0.813 mg/Kg - dry 0.813
35.0 mg/Kg - dry 2.44
3.4 % 0.1
39.4 % 0.010
Results Units MQL
1 09/01/22 06:30 JPJ ;M-4500-NH3C TKP
5 09/01/22 12:05 EAL 6010D
1 08/30/22 19:31 EAL 6010D
1 08/30/22 19:31 EAL 6010D
1 08/30/22 19:31 EAL 6010D
1 08/30/22 19:31 EAL 6010D
1 09/06/22 14:58 DXT AOAC 955.01
1 08/29/22 17:09 FMM S1-2540G
DF Date / Time By
Analyzed
Analytical
Method
Ammonia Nitrogen
Nitrate+Nitrite-N
pH
Molybdenum
Potassium
Sodium
<813 mg/Kg - dry
<39.8 mg/Kg - dry
5.7 s.u.
2.26 mg/Kg - dry
886 mg/Kg - dry
<203 mg/Kg - dry
813 1 09/01/22 12:30 Pi
39.8 1 08/31/22 15:45 ZBD
1 09/01/22 15:00 ADM
2.03 1 08/30/22 19:31 EAL
81.3 1 08/30/22 19:31 EAL
203 1 08/30/22 19:31 EAL
SM-4500-NH3C
4500NO3F-2011
9045D
6010D
6010D
6010D
Qualifiers/
Definitions
DF
Dilution Factor
MQL Method Quantitation Limit
Page 6 of 20

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.com
Report Number :22-237-0006 REPORT OF ANALYSIS
Lab No : 59047
Sample ID : GUC-3
Report Date : 09/08/2022
Received : 08/25/2022
,unT me (rra r
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Total Solids 12.3 % 0.010 108/29/22 17:09 FMM SM-2540G
Moisture 87.7 % 0.010 1 08/29/22 17:09 FMM 5M-2540G
Phosphorus 3390 mg/Kg - dry 40.7 1 08/30/22 19:31 EAL 6010D
Sulfur 6200 mg/Kg - dry 81.3 1 08/30/22 19:31 EAL 6010D
Calcium 1370 mg/Kg - dry 407 I 08/30/22 19:31 EAL 6010D
Magnesium 984 mg/Kg - dry 40.7 1 08/30/22 19:31 EAL 6010D
Iron 34700 mg/Kg - dry 81.3 1 08/30/22 19:31 EAL 6010D
Zinc 86.2 mg/Kg - dry 10.2 1 08/30/22 19:31 EAL 6010D
Organic N 16500 mg/Kg - dry 2033 1 09/01/22 06:30 CALCULATION
Chromium 93.5 mg/Kg - dry 2.03 1 08/30/22 19:31 EAL 6010D
Nickel 18.9 mg/Kg - dry 2.03 1 08/30/22 19:31 EAL 6010D
Arsenic 15.4 mg/Kg - dry 4.07 I 08/30/22 19:31 EAL 6010D
Mercury <1.28 mg/Kg - dry 1.28 1 08/30/22 11:52 TJS SW-7471B
Selenium <4.07 mg/Kg - dry 4.07 1 08/30/22 19:31 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 7 of 20

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number : 22-237-0006 REPORT OF ANALYSIS
Lab No : 59048
Sample ID : GUC-4
Report Date : 09/08/2022
Received : 08/25/2022
t &roar
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test
Results Units MQL DE Date / Time By Analytical
Analyzed Method
Total Solids 12.9 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Calcium 1120 mg/Kg - dry 388 1 08/30/22 19:46 EAL 6010D
Iron 28700 mg/Kg - dry 77.5 1 08/30/22 19:46 EAL 6010D
Zinc 73.8 mg/Kg - dry 9.69 1 08/30/22 19:46 EAL 6010D
Chromium 81.4 mg/Kg - dry 1.94 1 08/30/22 19:46 EAL 6010D
Arsenic 12.2 mg/Kg - dry 3.88 1 08/30/22 19:46 EAL 6010D
Mercury <1.23 mg/Kg - dry 1.23 1 08/30/22 11:54 TJS SW-7471B
Test Results Units MQL OF Date /Time By Analytical
Analyzed Method
Ammonia Nitrogen <775 mg/Kg - dry 775 1 09/01/22 12:30 JP] SM-4500-NH3C
Organic N 12560 mg/Kg - dry 1938 1 09/01/22 06:30 CALCULATION
Phosphorus 2730 mg/Kg - dry 38.8 1 08/30/22 19:46 EAL 6010D
Copper 111 mg/Kg - dry 3.88 1 08/30/22 19:46 EAL 6010D
Lead 27.9 mg/Kg - dry 2.33 1 08/30/22 19:46 EAL 6010D
Manganese 319 mg/Kg - dry 3.88 1 08/30/22 19:46 EAL 6010D
Nickel 16.5 mg/Kg - dry 1.94 1 08/30/22 19:46 EAL 6010D
Selenium <3.88 mg/Kg - dry 3.88 1 08/30/22 19:46 EAL 6010D
Sulfur 5580 mg/Kg - dry 77.5 1 08/30/22 19:46 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 8 of 20

Waypoint
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyfical.com
Report Number : 22-237-0006 REPORT OF ANALYSIS
Lab No : 59048
Sample ID : GUC-4
Report Date : 09/08/2022
Received : 08/25/2022
-owr; c
�t Geooer
Pa uric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Analytical Method: SM-2540G
Test Results Units MQL DF Date ! Time By Analytical
Analyzed Batch
Moisture
87.1 % 0.010 1 08/29/22 17:09 FMM L634745
Total Kjeldahl Nitrogen 12600 mg/Kg - dry 1940 1 09/01/22 06:30 JPJ iM-4500-NH3C TKP
Potassium 709 mg/Kg - dry 77.5 1 08/30/22 19:46 EAL 6010D
Magnesium 775 mg/Kg - dry 38.8 1 08/30/22 19:46 EAL 6010D
Sodium <194 mg/Kg - dry 194 1 08/30/22 19:46 EAL 6010D
Aluminum 122000 mg/Kg - dry 194 5 09/01/22 12:10 EAL 6010D
Nitrate+Nitrite-N 38.5 mg/Kg - dry 37.4 1 08/31/22 15:46 ZBD 4500NO3F-2011
Cadmium <0,775 mg/Kg - dry 0.775 1 08/30/22 19:46 EAL 6010D
pH 5.7 s.u.
1 09/01/22 15:00 ADM 9045D
Calcium Carbonate Equivalent 3.8 % 0.1 1 09/06/22 14:58 DXT AOAC 955.01
Total Volatile Solids 41.4 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Molybdenum <1.94 mg/Kg - dry 1.94 1 08/30/22 19:46 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 9 of 20

•
Waypoint
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytica l.com
Report Number :22-237-0006 REPORT OF ANALYSIS
Lab No : 59049
Sample ID ; GUC-5
Report Date : 09/08/2022
Received : 08/25/2022
iic mt (rfow�
Pauric McGroary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Total Kjeldahl Nitrogen 13500 mg/Kg - dry 1940 1 09/01/22 06:30 JPJ ;M-4500-N1-13C-TKP
Aluminum 119000 mg/Kg - dry 194 5 09/01/22 12:15 EAL 6010D
Manganese 361 mg/Kg - dry 3.88 1 08/30/22 19:51 EAL 6010D
Copper 157 mg/Kg - dry 3.88 1 08/30/22 19:51 EAL 6010D
Cadmium <0.775 mg/Kg - dry 0.775 1 08/30/22 19:51 EAL 6010D
Lead 30.1 mg/Kg - dry 2.33 1 08/30/22 19:51 EAL 6010D
Calcium Carbonate Equivalent 3.7 0h 0.1 1 09/06/22 14:58 DXT AOAC 955.01
Total Volatile Solids 42.3 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Test
Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Ammonia Nitrogen <775 mg/Kg - dry 775 1 09/01/22 12:30 JPJ SM-4500-NH3C
Nitrate+Nitrite-N <35.7 mg/Kg - dry 35.7 1 08/31/22 15:46 Z8D 4500NO3F-2011
pH 5.8 s.u.
1 09/01/22 15:00 ADM 9045D
Molybdenum 2.19 mg/Kg - dry 1.94 1 08/30/22 19:51 EAL 6010D
Potassium 762 mg/Kg - dry 77.5 1 08/30/22 19:51 EAL 6010D
Sodium <194 mg/Kg - dry 194 1 08/30/22 19:51 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 10 of 20

Waypoint.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Caert
530 Woodlawn St
Belmont , NC 28012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number : 22-237-0006 REPORT OF ANALYSIS
Lab No : 59049
Sample ID : GUC-5
Report Date : 09/08/2022
Received : 08/25/2022
ut/ic rit Gfowy/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Total Solids 12.9 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Moisture 87.1 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Phosphorus 3530 mg/Kg - dry 38.8 I 08/30/22 19:51 EAL 6010D
Sulfur 4600 mg/Kg - dry 77.5 1 08/30/22 19:51 EAL 6010D
Calcium 1300 mg/Kg - dry 388 1 08/30/22 19:51 EAL 6010D
Magnesium 853 mg/Kg - dry 38.8 1 08/30/22 19:51 EAL 6010D
Iron 29700 mg/Kg - dry 77.5 1 08/30/22 19:51 EAL 6010D
Zinc 69.8 mg/Kg - dry 9.69 1 08/30/22 19:51 EAL 6010D
Organic N 13490 mg/Kg - dry 1938 1 09/01/22 06:30 CALCULATION
Chromium 81.4 mg/Kg - dry 1.94 1 08/30/22 19:51 EAL 6010D
Nickel 15.8 mg/Kg - dry 1.94 1 08/30/22 19:51 EAL 6010D
Arsenic 15.2 mg/Kg - dry 3.88 1 08/30/22 19:51 EAL 6010D
Mercury <1.12 mg/Kg - dry 1.12 1 08/30/22 11:55 TJS SW-7471B
Selenium <3.88 mg/Kg - dry 3.88 1 08/30/22 19:51 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 11 of 20

Waypoint
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 26012
Project GUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number : 22-237-0006 REPORTOFANALVSIS
Lab No : 59053
Sample ID : GUC-6
Report Date : 09/08/2022
Received : 08/25/2022
Todult pit Glace yr
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Total Solids 10.9 % 0.010 1 08/29/22 17:09 FMM SM-2540G
Calcium 1350 mg/Kg - dry 459 1 08/30/22 19:56 EAL 6010D
Iron 28300 mg/Kg - dry 91.7 1 08/30/22 19:56 EAL 6010D
Zinc 66.6 mg/Kg - dry 11.5 1 08/30/22 19:56 EAL 6010D
Chromium 89.2 mg/Kg - dry 2.29 1 08/30/22 19:56 EAL 6010D
Arsenic 12.4 mg/Kg - dry 4.59 1 08/30/22 19:56 EAL 6010D
Mercury <1.40 mg/Kg - dry 1.40 1 08/30/22 11:57 TJS SW-7471B
Test
Results Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen <917 mg/Kg - dry 917 1 09/01/22 12:30 JPJ SM-4500-NH3C
Organic N 14500 mg/Kg - dry 2294 1 09/01/22 06:30 CALCULATION
Phosphorus 3990 mg/Kg - dry 45.9 1 08/30/22 19:56 EAL 6010D
Copper 112 mg/Kg - dry 4.59 1 08/30/22 19:56 EAL 6010D
Lead 30.7 mg/Kg - dry 2.75 1 0B/30/22 19:56 EAL 6010D
Manganese 387 mg/Kg - dry 4.59 1 08/30/22 19:56 EAL 6010D
Nickel 16.2 mg/Kg - dry 2.29 1 08/30/22 19:56 EAL 6010D
Selenium <4,59 mg/Kg - dry 4.59 1 08/30/22 19:56 EAL 6010D
Sulfur 5830 mg/Kg - dry 91.7 1 08/30/22 19:56 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 12 of 20

Waypoint..
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Report Number : 22-237-0006
Lab No : 59053
Sample ID : GUC-6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project GUC
Information :
REPORT OPANALYSIS
Report Date : 09/08/2022
Received : 08/25/2022
laWit
Grow/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/24/2022 2:00
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Batch
Moisture
Total Kjeldahl Nitrogen
Potassium
Magnesium
Sodium
Aluminum
Nitrate+Nitrite-N
Cadmium
pH
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
89.1
0.010 1 08/29/22 17:09 FMM L634745
14500 mg/Kg - dry 2290
594 mg/Kg - dry 91.7
706 mg/Kg - dry 45.9
<229 mg/Kg - dry 229
125000 mg/Kg - dry 229
67.9 mg/Kg - dry 41.9
<0.917 mg/Kg - dry 0.917
5.8 s.u.
6.8 % 0.1
41.5 % 0.010
<2.29 mg/Kg - dry 2.29
1 09/01/22 06:30 JPJ iM-4500-NH3C TKP
1 08/30/22 19:56 EAL 6010D
1 08/30/22 19:56 EAL 6010D
I 08/30/22 19:56 EAL 6010D
5 09/01/22 12:20 EAL 6010D
1 08/31/22 15:48 ZBD 4500NO3F-2011
1 08/30/22 19:56 EAL 6010D
1 09/01/22 15:00 ADM 9045D
1 09/06/22 14:58 DXT ADAC 955.01
1 08/29/22 17:09 FMM SM-2540G
1 08/30/22 19:56 EAL 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
Page 13 of 20

Waypoint.
ANALYTICAL
Client: Bio-Nomic Servics Inc
Project: GUC
Lab Report Number: 22-237-0006
Date: 9/7/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 81430
QC Batch No: L635068/L634597
One or more internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 81430
Analyte: Aluminum
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Aluminum
QC Batch No: L635125/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Aluminum
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Arsenic
QC Batch No: L6350681L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Calcium
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Calcium
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Cadmium
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Cadmium
Page 14 of 20

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81430
Analyte: Chromium
QC Batch No: L6350681L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Chromium
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Copper
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Copper
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Iron
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Iron
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Potassium
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Potassium
QC Batch No: L6355151L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81430
Analyte: Magnesium
QC Batch No: L635068/L634597
Page 15 of 20

Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Magnesium
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Manganese
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Manganese
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Molybdenum
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Sodium
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Nickel
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to 1EC interference/matrix interference.
Sample 81430
Analyte: Nickel
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Phosphorus
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Lead
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Lead
QC Batch No: L635515/L634597
Page 16 of 20

Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81430
Analyte: Sulfur
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Selenium
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Selenium
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81430
Analyte: Zinc
QC Batch No: L635068/L634597
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81430
Analyte: Zinc
QC Batch No: L635515/L634597
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97816 (SIH01-4-6)
Analyte: Mercury
QC Batch No: L634956/L634624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 17 of 20

Waypoint.,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical,com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 22-237-0006
Shipping Method
* Fed Ex 0 US Postal Q Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised?
O Yes 0No
Number of coolers/boxes received T i
Custody seals intact on shipping container/cooler? Q Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? * Yes 0 No
COC properly completed
0 Yes 0 No
Samples in proper containers?
Sample containers intact?
*Yes QNo
QQ Yes 0No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time?
* Yes 0No
Cooler temperature in compliance?
Yes QNo
Cooler/Samples arrived at the laboratory on ice. * Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Water - VOA vials free of headspace
0 Yes
Q Yes
Trip Blanks received with VOAs
0 Yes
Q No * N/A
Q No * N/A
QNo *N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
r Low concentration EnCore samplers (48 hr)
r High concentration pre -weighed (methanol -14 d) r Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
r High concentration container (48 hr)
0 Yes
0 No
Signature:
David Lennon
Date & Time:
Page 18 of 20
08/25/2022 10:50:45

OZ to 6t acted
Project
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WASTEWATER SAMPLE TRAM
Waypoinl
7621 Whitepine Road Richmond VA 23237 Tel: [phone](
Submitted By
Phone:7D'-I_ -cocci
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GUC
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Sample Information
Y
Account #
LICa`4-i
Copy To
Jer' e_.
E-mail:
Lab Number
Sample ID (Lab Use
Only)
GUt-3
L714.G-1
Collection Information
Container Information
Please Write in Desired Tests
Type
x Grab
Composite
Grab
_ Composite
3r Grab
_Composite
'C Grab
Composite
Dale
Z`l-it
Time
Z:00 in
2:►6/�ar
2z2p,t
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Number
or Botiles
Type Volume
Glass
Plastic
Glass
K Plastic
Glass
Plastic
Glass
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SU 9-2 i _46.1� FFl rGE
oz
pint
qt
oz
Dint
qt
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x
x
x
x
x
Relinquished By: (Signature)
Test Availabte
Date
Zz
Time
3= 3arim_
Received By: (Signature)
Date
Time
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iran, Aluminum,
Manganese, Copper. Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride. Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
Special Instructions or Remarks

Dz ;o oz abed
Project
Sample ID
et-6
Lab Number
(Lab Use
Only)
5'\05.3
WASTEWATER SAMPLE TRANSl uII i 11111111111111111111111111111111111111111111111111111111111111
22-237-0006
45571
08-25-2022
Waypoint Anal, Bio-N6rnicSelvic.Inc 10:44•15
7621 Whitepine Road Richmond VA 23237 Tel: [phone] Fax: 81 GUC
Customer lnformatic
Submitted By
Charge To
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3o L.r Oo0e�—
c�>r.��� nL g'fo )Z
Phone:7QLl— 6- afl00
Collection information
Type
Grab
Composite
Grab
Composite
Grab
Composite
Grab
Composite
Date
Time
7corn
Fax:
Sample Information
Container Information
Number
of Bottles
Type
Glass
X. Plastic
Glass
Plastic
Glass
Plastic
Glass
Plastic
Volume
oz
pint
K q!
oz
_pint
qt
oz
pint
ql
oz
pint
at
Account #
Copy To
JD('J . e�
E-mall: ms-ai Ijil1•1arnie-,ec:n
x
Please Write in Desired Tests
$a3
x
x
Relinquished By: (Signature)
Test Available
Date
Time
3: 30r'/‘
Received By: (Signature)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days). Boron,
Chemical Oxygen Demand. Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved. Suspended, Total, Volatile)
t\f„ ofik:\
Date
Time
x
Special Instructions or Remarks
!`� C_ CJetz.A4

LINKS
Review your project
results
Visit us at:
www.eurofinsus.com/Env
4:% eu raft ns
Environment Testing
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-213280-1
Client Project/Site: Greenville Utilities
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Mr. Joel Coert
Si,101/LA
Authorized for release by:
4/11/2022 4:05:51 PM
David Fuller, Project Manager
[phone]
[e-mail]
The test results in this report meet all2003 NELAC, 2009 TNI, and 2016 TM requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the a -mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory,

Definitions/Glossary
Client: Bio-Namics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1..,
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
F2 MSIMSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report
n Listed under the "D" column to designate that the result is reported an a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoDIDOE)
MCL EPA recommended 'Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 27 4/11/2022

Sample Summary
Client: Bio-Nomics Services., Inc. Job ID: 680-213260-1
Project/Site: Greenville Utilities
Lab Sample ID Client Sample ID Matrix Collected Received
680-213280-1 Greenville WTP Sludge 03/29/22 10:00 03/30/22 11:00
9Eurofin 4/11/2022
Page 3of27

Case Narrative
Client: Bio-Nomics Services., Inc. Job ID: 680-21328D-1
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Laboratory: Eurofins Savannah
Narrative
Receipt
The sample was received on 3/30/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 3.5° C.
GC/MS VOA
Method 8260D: The leachate blank for preparation batch 680-713646 contained Chloroform above the reporting limit (RL). None of the
samples associated with this method blank contained the target compound; therefore, re -extraction and/or re -analysis of samples were
not performed.
No additional analytical or quality issues were noted, other than those
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described
GC Semi VOA
No analytical or quality issues were noted, other than those described
Metals
No analytical or quality issues were noted, other than those described
described above or in the Definitions/Glossary page.
in the Definitions/Glossary page.
in the Definitions/Glossary page.
in the Definitions/Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
9 Eurofins 4/11/2022
Page

Client Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Client Sample ID: Greenville WTP
Date Collected: 03/29/22 10:00
Date Received: 03/30/22 11:00
Lab Sample ID: 680-213280-1
Matrix: Sludge
Method: 8260D - Volatile Organic Compounds by GC/MS - TCLP
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1-Dichloroethene ND 0.0200 mg/L 04/04/22 17:48 20
1,2-Dichloroethane ND 0.0200 mg/L 04104/2217:48 20
1,4-Dichlorobenzene ND 0.0200 mg/L 04/04/22 17:48 20
2-Butanone (MEK) ND 0.200 mg/L 04/04/22 17:48 20
Benzene ND 0.0200 mg/L 04/04/22 17:48 20
Carbon tetrachloride ND 0.0200 mgfL 04/04122 17:48 20
Chlorobenzene ND 0.0200 mgfL 04/04/22 17:48 20
Chloroform ND 0.0200 mg/L 04/04/22 17:48 20
Tetrachloroethene ND 0.0200 mg/L 04/04122 17:48 20
Trichloroethene ND 0.0200 mg/L 0410412217:48 20
Vinyl chloride ND 0.0200 mg/L 04104/22 17:48 20
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 107 60- 124 04/04/22 17.48 20
4.Bremoluorobenzene (Surr) 99 70- 130 04/04/22 17:48 20
LDibromofuoramethane (Surr) 108 70- 130 04/04/22 17:48 20
Toluene-d8 (Surr) 111 70 _130 04/04/22 17:48 20
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
2,4,5-Trichlorophenol ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
2,4,6-Trichlorophenol ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
2,4-Dinilrotoluene ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
2-Methylphenol ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
3 & 4 Methylphenol ND 0.0500 mg/L 04/03/22 02:46 04/04/22 23:06 1
Hexachlorobenzene ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
Hexachlorobutadiene ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
Hexachroroethane ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
Nitrobenzene ND 0.0500 mg/L 04/03/22 02:48 04/04/22 23:06 1
Penlachlorophenol ND 0.250 mg/L 04/03/22 02:48 09/04/22 23:06 1
Pyridine ND 0.250 mg/L 04/03/22 02:48 04/04/22 23:06 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed 011 Fac
2, 4, 6-Trfbromophenol (Surr) 71 30.. 130 04/03/22 02:48 04/04/22 23:06 1
2-Fluorobiphenyl (Surr) 55 25- 130 04/03/22 02:48 04/04/22 23:06 1
2-Fluorophenol (Surr) 35 10. 130 04/03/22 02:48 04/04/22 23:06 1
Nitrobenzene-d5 (Surr) 51 30- 130 04/03/22 02:48 04/04/22 23:06 1
Phenol-d5 (Surr) 21 10.130 04/031'22 02:48 04/04/22 23:06 1
Terphenyl-d14 (Surr) 65 35- 131 04/03/22 02:48 04/0422 23:06 1
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Chlordane (technical) ND 0.0250 mg/L 04/05/22 14:42 09/06/22 16:46 1
Endrin ND 0.00250 mg/L 04/05/2214:42 04/06122 16:46 1
gamma-BHC (Lindane) ND 0.00250 mg/L 04/05/22 14:42 04/06/22 16:46 1
Heptachlor ND 0,00250 mgfL 04/052214:42 04/06/22 16:46 1
Heptachlor epoxide ND 0.00250 mg/L 04/05/22 14:42 04/06/22 16:46 1
Methoxychlor ND 0.00250 mgfL 04/05/22 19:42 04/06122 16:46 1
Toxaphene NO 0.250 mg/L 04/05/22 14:42 04/06122 16:46 1
Eurofins Savannah
Page 5 of 27 4/11/2022

Client Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Client Sample ID: Greenville WTP
Date Collected: 03/29/22 10:00
Date Received: 03/30/22 11:00
Lab Sample ID: 680-213280-1
Matrix: Sludge
Surrogate %Recovery Qualifier Limits Prepared Analyzed D11 Fac
DCB Decachlorobiphenyl 76 30- 130 04/05/22 14:42 04/0622 16:46 1
I Tetrachloro-m-xylene 66 30 - 130
04/05/22 14:42 04/0627 16:46 1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
PCB-1016 ND F2 0.0192 mg/Kg 03/31/22 17:21 04/01/2221:51 1
PCB-1221 ND 0.0163 mg/Kg 03/31/22 17:21 04/01/22 21:51 1
PCB-1232 ND 0.0163 mg/Kg 03/31/22 17:21 04101/22 21:51 1
PCB-1242 ND 0.0163 mg/Kg 03/31/22 17:21 04/01122 21:51 1
PCB-1248 ND 0.0163 mg/Kg 03/31/22 17:21 04/01/2221:51 1
PCB-1254 ND 0.0163 mg/Kg 03/31/22 17:21 04/01/22 21:51 1
PCB-1260 ND F2 0.0163 mg/Kg 03/31/22 17:21 04/01/22 21:51 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
Tetrachloro-m-xylene 79 22 - 130 03/31/22 17:21 04/01/22 21.51 1
LDC8 Decachlorobipherry! 67 25 - 138 03/31/22 17:21 04/0122 21:51 1
Method: 8151A - Herbicides (GC) - TCLP
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
2.4-0 ND 0.0122 mg/L 04/04/22 14:05 04/08/2220:10 1
Silvex (2,4,5-TP) ND 0.00957 mg/L 04/04/22 14:05 04/08/2220:10 1
Surrogate
DCAA
%Recovery Qualifier Limits Prepared Analyzed Di! Fac
48 26-137 04/04/22 14:05 04/08/22 20:10 1
Method: 6010D - Metals (ICP) - TCLP
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Arsenic ND 0.200 mg/L 04/04/22 09:36 04/05/22 12:39 1
Barium ND 1.00 mg/L 04/04/22 09:36 09/05122 12:39 1
Cadmium ND 0.100 mg/L 04/04/22 09:36 04/05/22 12:39 1
Chromium ND 0.200 mg/L 04/04/22 09:36 04/05/22 12:39 1
Lead ND 0.200 mg/L 04/04/22 09:36 04/05/22 12:39 1
Selenium ND 0.500 mgiL 09/04/22 09:36 04/05/22 12:39 1
Silver NO 0.100 mg/L 04/04/22 09:36 04/05/22 12:39 1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
`Mercury ND 0,0200 mg/L 04/04/22 09:57 04/04/22 14:57 1
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total ND 0.486 mg/Kg 04/05/22 09:50 04/05122 13:19 1
Sulfide ND 56.6 mg/Kg 03/31/22 09:41 03/31/22 12:33 1
Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Flashpoint >200 60.0 Degrees F 04/04/22 11:36 1
Temperature 19.7 HF 0.1 Celsius 04/04/22 13:43 1
Soil pH in Water 6.2 HF 0.1 PH Units 04/04/22 13:43 1
Eurofins Savannah
Page 6 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Method: 8260D - VoTatile Organic Compounds by GC/MS
Lab Sample 1D: MB 680-713938/9
Matrix: Solid
Analysis Batch: 713938
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1-Dichloroethene ND 0.00100 mg/L 04/04/2213:07 1
1,2-Dichloroelhane ND 0.00100 mg/L 04/04/22 13:07 1
1,4-Dichlorobenzene NO 0.00100 mglL 04/04/22 13:07 1
2-Bulanone (MEK) ND 0.0100 mg/L 04/04/22 13:07 1
Benzene ND 0.00100 mg/L 04104/22 13:07 1
Carbon tetrachloride ND 0.00100 mg/L 04/04/22 13:07 1
Chlorobenzene ND 0.00100 mg/L 04/04/2213:07 1
Chloroform ND 0.00100 mglL 04/04/22 13:07 1
Tetrachloroethene ND 0.00100 mg/L 04104/2213:07 1
Trichroroelhene ND 0.00100 mglL 04/04/22 13:07 1
Vinyl chloride NO 0.00100 mg/L 04/04122 13:07 1
Surrogate
MB MB
%Recovery Qualifier Limits
1,2-Dichioroethane-d4 (Surr) 107 60,124
4-Bromofluorobenzene (Surr) 101 70 - 130
Dibmmofluoromethane (Surr) 112 70 - 130
Toluene -dB (Surr) 117 70- 130
Lab Sample ID: LCS 68D-713938/4
Matrix: Solid
Analysis Batch: 713938
Prepared
Analyzed Dil Fac
04/0412213:07 1
04/04/2213:07 1
04/04/22 13:07 1
04/04/22 13:07 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
1,1-Dichloroethene 0.0500 0.05515 mg/L 110 70-130
1,2-Dichloroelhane 0.0500 0.04730 mg/L 95 70 _ 130
1,4-Dichlorobenzene 0.0500 0.04680 mg/L 94 70 -130
2-Bulanone (MEK) 0.250 0.2186 mg/L 87 69 -114
Benzene 0.0500 0.04710 mg/L 94 70.130
Carbon tetrachloride 0.0500 0.04562 mg/L 91 70.130
Chlorobenzene 0,0500 0.04878 mg/L 98 70.130
Chloroform 0.0500 0.05221 mg/L 104 70 - 130
Tetrachloroethene 0.0500 0.04586 mg/L 92 70 _ 130
Trichloroethene 0.0500 0.04667 mglL 93 70.130
Vinyl chloride 0.0500 0.05262 mg/L 105 66 - 129
LCS LCS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 97 60. 124
4-Bmmafluorobenzene (Surr) 100 70_ 130
Dibromofuoromethane (Surr) 112 70- 130
LToluene-d8 (Surr) 111 70. 130
Lab Sample ID: LCSD 680-713938/5
Matrix: Solid
Analysis Batch: 713938
Anatyte
1,1-Dichloroethene
1,2-Dichloroethane
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.0500 0.05798 mg/L 116 70. 130 5 20
0.0500 0.04935 mg/L 99 70.130 4 50
Eurofns Savannah
Page 7 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCSD 680-713938(5
Matrix: Solid
Analysis Batch: 713938
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Roe RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
1,4-Dichlorobenzene 0.0500 0.04711 mg/L 94 70.130 1 30
2-Butanone (MEK) 0.250 0.2202 mg/L 88 69.114 1 30
Benzene 0.0500 0.04819 mglL 96 70.130 2 30
Carbon tetrachloride 0.0500 0.04534 mglL 91 70 _ 130 1 30
Chlorobenzene 0.0500 0.04837 mg/L 97 70.130 1 30
Chloroform 0.0500 0.05140 mg/L 103 70 _ 130 2 30
Tetrachloroethene 0.0500 0.04570 mg/L 91 70 -130 0 30
Trichloroelhene 0.0500 0.04889 mglL 98 70 -130 5 30
Vinyl chloride 0.0500 0.05914 mg/L 118 66.129 12 30
LCSD LCSD
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Burr) 95 60 -124
4-Bromofluorobenzene (Burr) 107 70- 130
Dibromofluoromethane (Sun-) 110 70 - 130
Toluene-d8 (Surr) 109 70. 130
Lab Sample ID: LB 680-71364611-A
Matrix: Solid
Analysis Batch: 713938
Client Sample ID: Method Blank
Prep Type: TCLP
LB LB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Pao
1,1-Dichloroethene ND 0.0200 mg/L 04104122 15:04 20
1,2-Dichloroethane ND 0.0200 mglL 04/04122 15:04 20
1,4-Dichlorobenzene ND 0.0200 mg/L 04104122 15:04 20
2-Butanone (MEK) ND 0.200 mg/L 04104122 15:04 20
Benzene ND 0.0200 mglL 04104/22 15:04 20
Carbon tetrachloride ND 0.0200 mg/L 04/04/22 15:04 20
Chlorobenzene ND 0.0200 mg/L 04/04/22 15:04 20
Chloroform 0.02274 0.0200 mglL 04/04/22 15:04 20
Tetrachloroethene ND 0.0200 mg/L 04/04/22 15:04 20
Trichloroethene ND 0.0200 mglL 04/04/22 15:04 20
Vinyl chloride ND 0.0200 mg/L 04/04/22 15:04 20
LB LB
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI! Fac
1,2-Dichloroethene-d4 (Sun-) 107 60- 124 04/04/22 15:04 20
4-Bromofluorobenzene (Surr) 99 70. 130 04/04/22 15:04 20
Dibromofuoromethane (Burr) 109 70 -130 04/04/22 15:04 20
Toluene -dB (Surr) 116 70 _130 04/04/22 15:04 20
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-71387511-A
Matrix: Solid
Analysis Batch: 714065
Analyte
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713875
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
2, 4, 5-Tric h l prop h e n o I
2, 4, 6-Tric h l orop h e n o I
ND 0.0100 mg/L 04/03/22 02:48 04/04/22 14:51 1
ND 0.0100 mg/L 04/03/22 02:48 04104/22 14:51 1
Eurofins Savannah
Page 8 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-713875/1-A
Matrix: Solid
Analysis Batch: 714065
Analyte
2,4-Dinilrotoluene
2-Methylphenol
3 & 4 Melhylphenol
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Penlachlorophenal
Pyridine
Surrogate
MB MB
Result Qualifier
ND
ND
ND
ND
ND
ND
ND
ND
ND
MB MB
%Recovery Qualifier
RL
0.0100
0.0100
0.0100
0.0100
0.0100
0.0100
0.0100
0.0500
0.0500
Limits
2,4,6-Tribromophenol (Surr)
2-Fluorobiphenyl (Surr)
2-Fluorophenol (Sun)
Nitrobenzene-d5 (Surr)
Phenol-d5 (Surr)
Terphenyl-d14 (Surr)
PLab Sample ID: LCS 680-713875/3-A
Matrix: Solid
Analysis Batch: 714065
Analyte
2, 4, 5 -Tric h l o rop h e n of
2, 4, 6 -T r i c h l o rap h e n of
2,4-Dinitrotobuene
2-Methylphenol
3 & 4 Methylphenor
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachforophenol
Pyridine
Surrogate
2,4,6-Tribromophenal (Sun)
2-Fluorobiphenyl (Sun)
2-Ruorophenal (Surr)
Nitrobenzene-d5 (Surr)
Pheno!-d5 (Surr)
L Terphenyl-d14 (Surr)
70
57
30
50
20
64
30 -130
25.130
10 -130
30 _ 130
10-130
35- 131
Spike
Added
LCS LCS
%Recovery Qualifier
73
59
32
56
22
78
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.200
0.400
0.400
Limits
30 -130
25_ 130
10_ 130
30 -130
10. 130
35-131
MDL Unit
mg/L
mg/L
mg/L
mg/L
mg/L
rng1L
mg/L
mg/L
mg/L
LCS LCS
Result Qualifier Unit
0.1353
0.1301
0.1378
0.1058
0.09852
0.1382
0.1025
0.1044
0.1084
0.3062
0.1298
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713875
D Prepared
04/03/22 02:48
04/03/22 02:48
04/03/22 02:48
04/03/22 02:48
04/03/22 02:48
04/03/22 02:4B
04/03/22 02:48
04/03/22 02:48
04/03/22 02:48
Prepared
04/03/22 02:46
04/03/22 02:48
04/0322 02:48
04/03/22 02:48
04/03/22 02:48
04/0322 02.48
Client Sample
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg1L
mg/L
mg/L
mg/L
mg/L
D %Rec
Analyzed Dil Fac
04/04/22 14:51 1
04/04/22 14:51 1
04104/22 14:51 1
04104/22 14:51 1
04/04/22 14:51 1
04/04/22 14:51 1
04/04/22 14:51 1
04/04/22 14:51 1
04/04/22 14:51 1
Analyzed Dil Fac
04/04/22 14:51 1
04/0422 14:51 1
04/0422 14:51 1
04/0422 14:51 1
04/0422 14:51 1
04/0422 14:51 1
ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713875
%Rec
Limits
68 26.130
65 28.130
69 37 -130
53 21_130
49 19.130
69 30 -130
51 12- 130
52 12 _ 130
54 32 -130
77 24 _130
32 10_130
Eurofins Savannah
Page 9 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LB 680-713640/1-B
Matrix: Solid
Analysis Batch: 714065
Analyte
LB LB
Result Qualifier
2,4, 5-Trichlorop hens I
2, 4, 6-Tri c h i orop h e n o l
2,4-Dinitrololuene
2-Methylphenol
3 & 4 Methytphenol
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surrogate
2,4, 5-Tribromophenol (Surr)
2-Fluorobiphenyl (Surr)
2-Fluorophenol (Surr)
Nitrobenzene-o'5 (Surr)
Phenol-d5 (Surr)
Terphenyl-d14 (Surr)
ND
NO
ND
NO
ND
ND
ND
ND
ND
ND
ND
LB LB
%Recovery Qualifier
RL
0.0500
0.0500
0.0500
0.0500
0.0500
0.0500
0.0500
0.0500
0.0500
0.250
0.250
Limits
72
61
29
56
20
65
30-130
25 -130
10 -130
30-130
10 -130
35 - 131
MDL Unit
mglL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
mglL
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 713875
D Prepared Analyzed Oil Fac
04/03/22 02:48 04/04/22 15:16 1
04/03/22 02:48 04104122 15:16 1
04/03/22 02:48 04/04/22 15:16 1
04/03/22 02:48 04/04122 15:16 1
04/03/22 02:48 04/04/22 15:16 1
04/03/22 02:48 04/04/22 15:16 1
04/03/22 02:48 04/04/22 15:16 1
04/03/22 02:48 04104/22 15:16 1
04/03/22 02:48 04/04/22 15:16 1
04/03122 02:48 04/04/22 15:16 1
04/03/22 02:48 04/04/22 15:16 1
Prepared Analyzed Di! Fac
04103/22 02:48 04/04/22 15:16
04/03/22 02:48 04/04/22 15:16
04/03/22 02.48 04/04/22 15:16
04/03/22 02:48 04/04/22 15:16
04/03/22 02:48 04/0422 15:16
04/03/22 02:48 04/04/22 15:16
Method: 8081E - Organochlorine Pesticides (GC)
Lab Sample ID: MB 680-714282/1-A
Matrix: Solid
Analysis Batch: 714484
Analyte
Chlordane (technical)
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogate
MB MB
Result Qualifier
ND
ND
NO
ND
ND
ND
ND
MB MB
%Recovery Qualifier
DCB Decachlorobiphenyi
Tetrach/oro-m-xylene
Lab Sample ID: LCS 680-714282/3-A
Matrix: Solid
Analysis Batch: 714484
Analyte
82
57
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
RL
0.000500
0.0000500
0.0000500
0.0000500
0.0000500
0.0000500
0.00500
Limits
30- 130
30 - 130
MDL Unit
mg/L
mg/L
mg/L
mglL
mg/L
mg/L
mg/L
Spike LCS LCS
Added Result Qualifier Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 714282
D Prepared
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
Analyzed Dil Fac
04/06/22 15:06 1
04/06/22 15:06 1
04/06/22 15:06 1
04/06122 15:06 1
04/06/22 15:06 1
04/06/22 15:06 1
04/06/22 15:06 1
Prepared Analyzed Dil Fac
04/05/22 14:42 04/06/22 15:06 1
04/05/22 14:42 04/06/22 15:06 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 714282
%Rec
D %Rec Limits
0.0000400 0.00003840 J mg/L
0.0000400 0.00003977 J mglL
0.0000400 0.00003833 J mg/L
0.0000400 0.00003591 J mg/L
96
99
96
90
30 - 130
30 _ 130
30 _ 130
30-130
Eurofins Savannah
Page 10 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 680-71428213-A
Matrix: Solid
Analysis Batch: 714484
Analyte
Methoxychlor
Surrogate
LCS LCS
%Recovery Qualifier
DCB Decachlorablphenyl
`Tetrachloro-m-xylene
Lab Sample ID: LB 680-71364011-G
Matrix: Solid
Analysis Batch: 714484
Analyte
87
65
Spike
Added
LCS LCS
Result Qualifier Unit
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 714282
%Rec
D %Rec Limits
0.0000400 0.00004769 J
Limits
LB LB
Result Qualifier
30- 130
30- 130
Chlordane (technical)
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogate
DCB Decachlorobipheny!
Tetrachloro-m-xylene
ND
ND
ND
ND
ND
ND
ND
LB LB
%Recovery Qualifier
70
56
RL
MDL Unit
0.0250
0.00250
0.00250
0.00250
0.00250
0.00250
0.250
Limits
30-130
30-130
mgiL
mg1L
mg/L
mg/L
mglL
mg/L
mg/L
mglL
119 30-130
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 714282
D Prepared
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
04/05/22 14:42
Analyzed Dil Fac
04/06122 14:52 1
04/06/22 14:52 1
04/06/22 14:52 1
04/06/2214:52 1
04/06/22 14:52 1
04106/22 14:52 1
04/06/22 14:52 1
Prepared Analyzed Dil Fac
04/05/22 14:42 04106/22 14:52
04/05/22 14:42 04/06;22 14:52
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 680-713610/4-A
Matrix: Solid
Analysis Batch: 713767
Analyte
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Surrogate
Tetrachloro-m-xylene
DCB Decachloroblphenyl
MB MB
Result Qualifier
ND
ND
ND
ND
NO
ND
ND
MB MB
%Recovery Qualifier
Lab Sample ID: LCS 680-713610/8-A
Matrix: Solid
Analysis Batch: 713767
Anatyte
PCB-1016
82
70
RL
0.0192
0.0163
0.0163
0.0163
0.0163
0.0163
0.0163
Limits
22.130
25-138
Spike
Added
0.191
MDL Unit
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
LCS LCS
Result Qualifier Unit
0.1808
Page 11 of 27
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713610
D Prepared
03/31/22 17:21
03/31/22 17:21
03/31/22 17:21
03/31/22 17:21
03/31/22 17:21
03/31/22 17:21
03/31/22 17:21
Prepared
03/3122 17:21
03/31/22 17:21
Client Sample
mg/Kg
D %Rec
Analyzed Dil Fac
04/01/2219:42 1
04/01/22 19:42 1
04/01122 19:42 1
04/01/22 19:42 1
04/01/22 19:42 1
04/01/22 19:42 1
04/01/22 19:42 1
Analyzed D11 Fac
04/01/22 19.42 1
04/01/22 19:42 1
ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713610
%Rec
Limits
95 22 -130
Eurofins Savannah
4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: LCS 680-713610/8-A
Matrix: Solid
Analysis Batch: 713767
Analyte
PCB-1260
Surrogate
LCS LCS
%Recovery Qualifier
Totrachlona-m-xylene 89
LDCB Decachlorobipheny!
Lab Sample ID: 680-213260-1 MS
Matrix: Sludge
Analysis Batch: 713767
Analyte
PCB-1016
PCB-1260
Surrogate
Tetrachloro-m-xylene
DCB Decachlorobiphenyl
80
Spike
Added
0.191
Limits
22 -130
25 -138
Sample Sample Spike
Result Qualifier Added
ND F2 0,189
ND F2 0.189
MS MS
%Recovery Qualifier Limits
Lab Sample ID: 680-213280-1 MSD
Matrix: Sludge
Analysis Batch: 713767
Analyte
39 22-130
36 25 _ 138
Sample Sample
Result Qualifier
PCB-1016
PCB-1260
Surrogate
Tetrachloro-m-xylene
DCB Decachlorobipheny!
ND F2
ND F2
MSD MSD
%Recovery Qualifier
44
40
Spike
Added
0.189
0.189
Limits
22-130
25_ 138
LCS LCS
Result Qualifier Unit
0.1803
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713610
%Rec
D %Rec Limits
mg/Kg
MS MS
Result Qualifier Unit
0.09254
0.09314
mg/Kg
mg/Kg
MSD MSD
Result Qualifier Unit
0.1916 F2
0.2154 F2
mg/Kg
mg/Kg
94 24-151
Client Sample ID: Greenville WTP
Prep Type: Total/NA
Prep Batch: 713610
%Rec
D %Rec Limits
49 22.130
49 24 -151
Client Sample ID: Greenville WTP
Prep Type: Total/NA
Prep Batch: 713610
%Rec RPD
D %Rec Limits RAD Limit
102 22-130 70 50
114 24 - 151 79 50
Method: 8151A - Herbicides (GC)
Lab Sample ID: MB 680-714070/1-A
Matrix: Solid
Analysis Batch: 714925
Analyte
2,4-D
Silvex (2,4,5-TP)
Surrogate
DCAA
MB MB
Result Qualifier
NO
ND
MB MB
%Recovery Qualifier
56
RL
MDL Unit
0.00112
0.000880
mgiL
mg/
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 714070
D Prepared Analyzed Dil Fac
04104/22 14:05 04/05/22 18:24 1
04/04/22 14:05 04/08/22 18:24 1
Limits Prepared Analyzed Di! Fac
26 _ 137 04/04/22 14.05 04/0822 16.24 1
Eurofins Savannah
Page 12 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utilities
Job ID: 680-213280-1
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 680-714070/2-A
Matrix: Solid
Analysis Batch: 714925
Analyte
2,4-D
Silvex (2,4,5-TP)
Surrogate
Spike
Added
LCS LCS
Result Qualifier Unit
0.0128 0.007151
0.00320 0.001993
LCS LCS
%Recovery Qualifier Limits
DCAA
Lab Sample ID: LB 680-713640/1-F
Matrix: Solid
Analysis Batch: 714925
Analyte
2,4-D
Silvex (2,4,5-TP)
84
LB LB
Result Qualifier
ND
ND
26 - 137
LB LB
Surrogate %Recovery Qualifier
DCAA
Lab Sample ID: 680-213280-1 MS
Matrix: Sludge
Analysis Batch: 714925
Analyte
2,4-D
Silvex (2,4,5-TP)
54
Sample Sample
Result Qualifier
ND
ND
MS MS
Surrogate %Recovery Qualifier
RL
0.0125
0.00982
Limits
26-137
Spike
Added
0.140
0.0351
Limits
DCAA
Lab Sample ID: 680-213280-1 MSD
Matrix: Sludge
Analysis Batch: 714925
Anatyte
2,4-D
Silvex (2,4,5-TP)
86
Sample Sample
Result Qualifier
ND
ND
MSD MSD
Surrogate %Recovery Qualifier
26-137
Spike
Added
0.140
0.0351
Limits
DCAA 97
26 - 137
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 714070
%Rec
D %Rec Limits
MDL Unit
mg/L
mg/L
mg/L
mg/L
MS MS
Result Qualifier Unit
0.08031
0,02208
56 21.130
62 31 _144
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 714070
D Prepared Analyzed Dil Fac
04/04/22 14:05 04/08/22 18:02 1
04/04/22 14:05 04/08122 18:02 1
mg/L
mglL
MSD MSD
Result Qualifier Unit
0.08394
0.02341
mg/L
mg/L
Prepared Analyzed Dil Fac
04/04122 14:05 04/0822 18:02 1
Client Sample ID: Greenville WTP
Prep Type: TCLP
Prep Batch: 714070
%Rec
D %Rec Limits
57 21 _ 147
63 31-144
Client Sample ID: Greenville WTP
Prep Type: TCLP
Prep Batch: 714070
%Rec RPD
D %Rec Limits RPD Limit
60 21 -147 4 50
67 31 _ 144 6 50
Method: 6010D - Metals (ICP)
Lab Sample ID: LB 680-713979!3-A
Matrix: Solid
Analysis Batch: 714262
Analyte
LB LB
Result Qualifier
Arsenic
Barium
ND
ND
RL
0.200
1.00
MDL Unit
mg/L
mglL
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713979
D Prepared Analyzed Dil Pao
04/04/22 09:37 04/05/22 12:19 1
04/04/22 09:37 04/05/22 12:19 1
Eurofins Savannah
Page 13 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: LB 680-713979/3-A
Matrix: Solid
Analysis Batch: 714262
LB LB
Analyte Result Qualifier RL MDL Unit ID Prepared Analyzed Dil Fac
Cadmium ND 0.100 mg/L 04/04/22 09:37 04105/22 12:19 1
Chromium ND 0.200 mg/L 04/04/22 09:37 04/05/22 12:19 1
Lead ND 0.200 mg/L 04/04/22 09:37 04/05122 12:19 1
Selenium ND 0.500 mg/L 04/04/22 09:37 04105122 12:19 1
Silver ND 0.100 mg/L 04/04/22 09:37 04/05/22 12:19 1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713979
Lab Sample ID: MB 680-713979/1-A
Matrix: Solid
Analysis Batch: 714262
Analyte
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Lab Sample ID: LCS 680-713979/2-A
Matrix: Solid
Analysis Batch: 714262
Analyte
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713979
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
ND 0.0200 mg/L 04/04/22 09:36 04/05/22 12:13 1
ND 0.100 mg/L 04/04/22 09:36 04/05122 12:13 1
ND 0.0100 mg/L 04/04/22 09:36 04/05/22 12:13 1
ND 0.0200 mg/L 04/04/22 09:36 04/05122 12:13 1
ND 0.0200 mg/L 04/04/22 09:36 04/05/22 12:13 1
ND 0.0500 mg/L 04/04/22 09:36 04/05/22 12:13 1
ND 0.0100 mg/L 04/04/22 09:36 04/05/22 12:13 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713979
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
Arsenic 2.00 2.167 mg/L 108 80.120
Barium 2.00 2.156 mg/L 108 80 _120
Cadmium 1.00 1.115 mg/L 112 80 -120
Chromium 2.00 2.240 mg/L 112 80. 120
Lead 10.1 10.97 mg/L 109 80. 120
Selenium 2.00 2.158 mg/L 108 80-120
Silver 1.00 1.041 mg/L 104 80 _120
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 680-71398611-A
Matrix: Solid
Analysis Batch: 714090
Analyte
Mercury
Lab Sample ID: LCS 680-71398612-A
Matrix: Solid
Analysis Batch: 714090
Analyte
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713986
MB MB
Result Qualifier RL MDL Unit 0 Prepared Analyzed Dil Fac
ND 0.000200 mg/L 04/04/22 09:57 04/04/22 14:39 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713986
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
Mercury 0.250 0.2497 mg/L 100 60 -120
Eurofins Savannah
Page 14 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID; 680-213280-1
Project/Site: Greenville Utilities
Method: 7470A - Mercury (CVAA) (Continued)
Lab Sample ID: LB 680-71364011-E
Matrix: Solid
Analysis Batch: 714090
Analyte
Mercury
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 713986
LB LB
Result Qualifier RL MDL Unit D Prepared Analyzed DU Fac
ND 0.0200 mg/L 04/04/22 09:57 04/04/22 14:44 1
Method: 1010B - Ignitability, Pensky-Martens Closed -Cup Method
Lab Sample ID: MB 400-57251513
Matrix: Solid
Analysis Batch: 572515
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Flashpoint >200.0 60.0 Degrees F 09/04/22 11:36 1
Lab Sample ID: LCS 400-572515/1
Matrix: Solid
Analysis Batch: 572515
Analyte
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
Flashpoint 149 149.0 Degrees F 100 90 -110
Lab Sample ID: LCSD 400-57251512
Matrix: Solid
Analysis Batch: 572515
Analyte
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
Flashpoint
149 147.0 Degrees F 99 90 - 110 1 4
Method: 9012B - Cyanide, Total andor Amenable
r
Lab Sample ID: MB 680-71400911-B
Matrix: Solid
Analysis Batch: 714257
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 714202
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total ND 0.500 mg/Kg 04/05/22 09:50 04/05/22 13:19 1
Lab Sample ID: LCS 680-714009/2-B
Matrix: Solid
Analysis Batch: 714257
Analyte
LCyanide, Total
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 714202
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
1.00 0.9761 mg/Kg 98 85.115
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 680-71352711-A
Matrix: Solid
Analysis Batch: 713567
Analyte
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 713527
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
`Sulfide ND 60.0 mg/Kg 03/31/22 09:41 03/31/22 12:33 1
Eurofns Savannah
Page 15 of 27 4/11/2022

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: LCS 680-713527/2-A
Matrix: Solid
Analysis Batch: 713567
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 713527
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide 1250 1117 mg/Kg 89 50. 150
Lab Sample ID: LCSD 680-713527/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 713567 Prep Batch: 713527
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Sulfide 1250 1074 mg/Kg 86 50 -150 4 50
Eurofins Savannah
Page 16 of 27 4/11/2022

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 680-213260-1
Project/Site: Greenville Utilities
GC/MS VOA
Leach Batch: 713646
Lab Sample ID
680-213280-1
LB 680-713646/1-A
Analysis Batch: 713938
Lab Sample ID
680-213280-1
LB 680-71364611-A
MB 680-71393819
LCS 680-713936/4
LLCSD 680-713938/5
Client Sample ID
Greenville WTP
Method Blank
Client Sample ID
Greenville VVTP
Method Blank
Method Blank
Lab Control Samplo
Lab Control Sample Dup
Prep Type
TCLP
TCLP
Prep Type
Matrix
Sludge
Solid
Matrix
Method
1311
1311
Method
TCLP
TCLP
Total/NA
Total/NA
Total/NA
Sludge
Solid
Solid
Solid
Solid
8260D
8260D
8260D
8260D
6260D
Prep Batch
Prep Batch
713646 1.+1
713646
GC/MS Semi VOA
Leach Batch: 713640
Lab Sample ID
680-213280-1
LB 680-71364011-B
Prep Batch: 713875
Lab Sample ID
680-213280-1
LB 680-713640/1-B
MB 680-71387511-A
L LCS 680-713875/3-A
Analysis Batch: 714065
Ir Lab Sample ID
680-213280-1
LB 680-713640/1-B
{ MB 680-713875/1-A
LCS 680-713875/3-A
Client Sample ID
Greenville WTP
Method Blank
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Prep Type
TCLP
TCLP
Prep Type
TCLP
TCLP
Total/NA
Total/NA
Prep Type
TCLP
TCLP
Total/NA
Total/NA
Matrix
Sludge
Solid
Matrix
Sludge
Solid
Solid
Solid
Matrix
Sludge
Solid
Solid
Solid
Method
1311
1311
Method
Prep Batch
Prep Batch
3510C
3510C
3510C
3510C
Method
713640
713640
Prep Balch
8270E
8270E
8270E
8270E
713875
713875
713875
713675
GC Semi VOA
Prep Batch: 713610
Lab Sample ID
680-213280-1
I MB 680.71361014-A
LCS 680-713610/8-A
1680-213280-1 MS
680-213280-1 MSD
Leach Batch: 713640
Lab Sample ID
680-213280-1
LB 680-71364011-F
LB 680.713640/1-G
660-213280-1 MS
680-213280-1 MSD
Client Sample ID
Greenville WTP
Method Blank
Lab Control Sample
Greenville WTP
Greenville WTP
Client Sample ID
Prep Type
Total/NA
Total/NA
Total/NA
TotallNA
Total/NA
Matrix
Sludge
Solid
Solid
Sludge
Sludge
Prep Type Matrix
Greenville WTP
Method Blank
Method Blank
Greenville WTP
Greenville WTP
TCLP
TCLP
TCLP
TCLP
TCLP
Sludge
Solid
Solid
Sludge
Sludge
Method
3546
3546
3546
3546
3546
Prep Batch
Method Prep Batch
1311
1311
1311
1311
1311
Eurofins Savannah
Page 17 of 27 4/11/2022

Client: Bio-Nomics Services., Inc. Job ID: 680-213281) 1
Project/Site: Greenville Utilities
QC Association Summary
GC Semi VOA
Analysis Batch: 713767
Lab Sample ID
Client Sample ID
680-213280-1
MB 680-71361014-A
LCS 680-71361018-A
680-213280-1 MS
680.213280-1 MSD
Prep Batch: 714070
r680-213280-1
LB 680-71364011-F
MB 680-714070/1-A
LCS 680-714070/2-A
680-213280-1 MS
680-213280-1 MSD
Prep Batch: 714282
Lab Sample ID
Lab Sample ID
680-213280-1
LB 680-713640/1-G
MB 680.714282/1-A
LCS 680-714282/3-A
Analysis Batch: 714484
Lab Sample ID
680-213280-1
LB 680-713640/1-G
MB 680-714282/1-A
LCS 680-71428213-A
Analysis Batch: 714925
Lab Sample ID
680-213280-1
LB 680-71364011-F
MB 680-71407011-A
LCS 680-714070/2-A
680-213280-1 MS
680-213280-1 MSD
Greenville WTP
Method Blank
Lab Control Sample
Greenville WTP
Greenville WTP
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Greenville WTP
Greenville WTP
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Greenville WTP
Greenville WTP
Prep Type Matrix
Method
Total/NA Sludge 8082A
Total/NA Solid 8082A
Total/NA Solid 8082A
Total/NA Sludge 8082A
Total/NA Sludge 8082A
Prep Type Matrix
Method
TCLP Sludge 8151A
TCLP Solid 8151A
Total/NA Solid 8151A
Total/NA Solid 8151A
TCLP Sludge 8151A
TCLP Sludge 8151A
Prep Type Matrix Method
TCLP Sludge 3510C
TCLP Solid 3510C
Total/NA Solid 3510C
Total/NA Solid 3510C
Prep Type Matrix Method
TCLP Sludge 8081B
TCLP Solid 8081E
Total/NA Solid 8081E
TotaVNA Solid 8081B
Prep Type
TCLP
TCLP
Total/NA
Total/NA
TCLP
TCLP
Matrix Method
Sludge 8151A
Solid 8151A
Solid 8151A
Solid 8151A
Sludge 8151A
Sludge 8151A
Prep Batch
713610
713610
713610
713610
713610
Prep Batch
713640
713640
713640
713640
Prep Batch
713640
713640
Prep Batch
714282
714282
714282
714282
Prep Batch
714070
714070
714070
714070
714070
714070
Metals
Leach Batch: 713640
Lab Sample ID
680-213280-1
LLB 680-71364011-E
Prep Batch: 713979
rLab Sample ID
680-213280-1
LB 680-71397913-A
i MB 680-71397911-A
LCS 680-71397912-A
Client Sample ID
Greenville WTP
Method Blank
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Prep Type
TCLP
TCLP
Prep Type
TCLP
Total/NA
Total/NA
Total/NA
Matrix
Sludge
Solid
Matrix
Sludge
Solid
Solid
Solid
Method
1311
1311
Prep Batch
Method Prep Batch
3010A
3010A
3010A
3010A
713640
Eurofins Savannah
Page 18 of 27 4/11/2022

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 680-213260-1
Project/Site: Greenville Utilities
Metals
Prep Batch: 713966
fJ
Lab Sample ID
680-213280-1
LB 680-713640/1-E
MB 680-713986/1-A
LLCS 680-713986/2-A
Analysis Batch: 714090
Lab Sample ID
680-213280-1
LB 680-71364011-E
MB 680-71398611-A
LCS 680-71398612-A
Analysis Batch: 714262
r
Lab Sample ID
680-213280-1
LB 680-713979/3-A
MB 680-713979/1-A
LCS 680-71397912-A
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Client Sample ID
Prep Type
Matrix
Method
TCLP
TCLP
Total/NA
Tolal/NA
Prep Type
Sludge
Solid
Solid
Solid
Matrix
7470A
7470A
7470A
7470A
Method
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Method Blank
Lab Control Sample
TCLP
TCLP
Total/NA
Total/NA
Prep Type
TCLP
Total/NA
Total/NA
Total/NA
Sludge
Solid
Solid
Solid
Matrix
Sludge
Solid
Solid
Solid
7470A
7470A
7470A
7470A
Method
6010D
6010D
6010D
6010D
Prep Batch
713640
713640
Prep Batch
713986
713986
713986
713986
Prep Batch
713979
713979
713979
713979
General Chemistry
Analysis Batch: 572515
Lab Sample ID
680-213280-1
MB 400-572515/3
LCS 400-572515/1
LCSD 400-572515/2
(Prep Batch: 713527
I Lab Sample ID
680-213280-1
MB 680-713527/1-A
LCS 680-713527/2-A
LCSD 680-713527/3-A
Analysis Batch: 713567
Lab Sample ID
Client Sample ID
Greenville WTP
Method Blank
Lab Control Sample
Lab Control Sample Dup
Client Sample ID
Prep Type Matrix
Total/NA Sludge
Total/NA Solid
Total/NA Solid
Total/NA Solid
Prep Type Matrix
Greenville WTP
Method Blank
Lab Control Sample
Lab Control Sample Dup
Client Sample ID
680-213280-1
MB 680-713527/1-A
LCS 680-713527/2-A
LLCSD 680-713527/3-A
Leach Batch: 714009
r—
Lab Sample ID
680-213280-1
MB 680-714009/1-B
LCS 680-714009/2-B
Analysis Batch: 714011
Lab Sample ID
680-213280-1
Greenville WTP
Method Blank
Lab Control Sample
Lab Control Sample Dup
Client Sample ID
Greenville WTP
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Total/NA Sludge
Total/NA Solid
Total1NA Solid
Total/NA Solid
Prep Type Matrix
Total/NA Sludge
Total/NA Solid
Total/NA Solid
Total/NA Solid
Prep Type Matrix
Total/NA Sludge
Total/NA Solid
Total/NA Solid
Prep Type Matrix
Total/NA Sludge
Page 19 of 27
Method
1010E
10106
1010E
10108
Method
9030E
9030E
9030E
9030B
Method
9034
9034
9034
9034
Method
9013
9013
9013
Method
Prep Batch
Prep Batch
Prep Batch
713527
713527
713527
713527
Prep Batch
Prep Batch
Moisture - 2540
Eurofins Savannah
4/11/2022

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
General Chemistry (Continued)
Analysis Batch: 714011 (Continued)
Lab Sample ID
I MB 680-714011/1
680-213280-1 DU
Analysis Batch: 714063
Lab Sample ID
L680-213280-1
LCS 680-71406314
Prep Batch: 714202
Lab Sample ID
680-213280-1
I MB 680-714009/1-B
LLCS 680-714009/2-B
Analysis Batch: 714257
Lab Sample ID
680-213280-1
MB 680-714009/1-B
LCS 680-714009/2-B
Client Sample ID
Method Blank
Greenville WTP
Client Sample ID
Greenville WTP
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Lab Control Sample
Client Sample ID
Greenville WTP
Method Blank
Lab Control Sample
Prep Type Matrix
Total/NA Solid
Total/NA Sludge
Prep Type Matrix
Method
Moisture - 2540
Moisture - 2540
Method
Total/NA Sludge
Total/NA Solid
Prep Type Matrix
9045D
9045D
Method
Total/NA Sludge
Total/NA Solid
Total/NA Solid
Prep Type Matrix
Total/NA Sludge
Total/NA Solid
Tolal/NA Solid
90128
9012B
90128
Method
9012B
90128
9012E
Prep Batch
Prep Batch
Prep Batch
714009
714009
714009
Prep Batch
714202
714202
714202
Eurofins Savannah
Page 20 of 27 4/11/2022

Lab Chronicle
Client: Bio-Nomics Services., Inc. Job ID: 680-213260-1
Project/Site: Greenville Utilities
Client Sample ID: Greenville WTP
Date Collected: 03/29/22 10:00
Date Received: 03/30/22 11:00
r
Prep Type
Lab Sample ID: 680-213280-1
Matrix: Sludge
Batch Batch DU Initial Final Batch Prepared
Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
TCLP Leach 1311 25.00 g 500 mL 713646 03/31/22 19:20 J8 TAL SAV
TCLP Analysis 8260D 20 5 mL 5 mL 713938 04/04/22 17:48 P1C TAL SAV
Instrument ID: CMSAB
TCLP Leach 1311 100.00 g 2000 mL 713640 03/31/22 18:30 JB TAL SAV
TCLP Prep 3510C 100 mL 1 mL 713875 04/03/22 02:48 MR TAL SAV
TCLP Analysis 8270E 1 714065 04/04/22 23:06 TIC TAL SAV
Instrument ID: CMSE
TCLP Leach 1311 100.00 g 2000 mL 713640 03/31/22 18:30 JB TAL SAV
TCLP Prep 3510C 5 mL 1 mL 714282 04/05/22 14:42 LA TAL SAV
TCLP Analysis 8081B 1 714484 04/06/22 16:46 JCK TALSAV
instrument ID: CSGAA
Total/NA Prep 3546 15.62 g 5 mL 713610 03/31/22 17:21 PB TAL SAV
TotaL/NA Analysis 8082A 1 713767 04/01/22 21:51 JCK TAL SAV
Instrument ID: CSGJ
TCLP Leach 1311 100.00 g 2000 mL 713640 03/31/22 18:30 JB TAL SAV
TCLP Prep 8151A 11.5 mL 5 mL 714070 04/04/22 14:05 EC TAL SAV
TCLP Analysis 8151A 1 714925 04/08/22 20:10 JCK TAL SAV
Instrument ID: CSGS
TCLP Leach 1311 100.00 g 2000 mL 713640 03/31/22 18:30 JB TAL SAV
TCLP Prep 3010A 5 mL 50 mL 713979 04/04/22 09:36 JE TAL SAV
TCLP Analysis 6010D 1 714262 04/05/22 12:39 BCB TAL SAV
Instrument ID: ICPH
TCLP Leach 1311 100.00 g 2000 mL 713640 03/31/22 18:30 JB TAL SAV
TCLP Prep 7470A 0.50 mL 50 mL 713986 04/04/22 09:57 JKL TALSAV
TCLP Analysis 7470A 1 714090 04/04/22 14:57 JKL TAL SAV
Instrument ID: QuickTrace2
Tota11NA Analysis 1010B 1 1 g 1 g 572515 04/04/22 11:36 ANE TAL PEN
Instrument ID: Pyro
Total/NA Leach 9013 10.28 g 200 mL 714009 04/04/22 10:24 NVF TAL SAV
Total/NA Prep 9012B 6 mL 6 mL 714202 04/05/22 09:50 NVF TAL SAV
Total/NA Analysis 9012B 1 714257 04/05/22 13:19 NVF TAL SAV
Instrument ID: KONELAB4
Total/NA Prep 9030B 1.06 g 6 mL 713527 03/31/22 09:41 NVF TAL SAV
Total/NA Analysis 9034 1 6 mL 6 mL 713567 03/31/22 12:33 NVF TAL SAV
Instrument ID: NOEQU1P
Total/NA Analysis 9045D 1 20.47 g 20 mL 714063 04/04/22 13:43 SM TAL SAV
Instrument ID: GEpHMS
Total/NA Analysis Moisture - 2540 1 714011 04/04/22 10:28 ALG TAL SAV
Instrument ID: NOEQUIP
Laboratory References:
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 21 of 27 4/11/2022

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Laboratory: Eurofins Savannah
The accreditationslcertifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22
_South Carolina State 98001 06-30-22
Laboratory: Eurofins Pensacola
All accreditationslcertifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Alabama State 40150 06-30-22
ANAB ISO/IEC 17025 L2471 02-23-23
Arkansas DEO State 88-0689 09-01-22
California State 2510 06-30-22
Florida NELAP E81010 06-30-22
Georgia Stale E81010(FL) 06-30-22
Illinois NELAP 200041 10-09-22
Kansas NELAP E-10253 10-31-22
Kentucky (UST) State 53 06-30-22
Kentucky (WW) State KY98030 12-31-22
Louisiana NELAP 30976 06-30-22
Louisiana (OW) State LA017 12-31-22
Maryland State 233 09-30-22
Massachusetts State M-FL094 06-30-22
Michigan State 9912 06-30-22
North Carolina (WWISW) State 314 12-31-22
Oklahoma NELAP 9810 08.31-22
Pennsylvania NELAP 68-00467 01-31-23
South Carolina Stale 96026 06-30-22
Tennessee State TN02907 06-30-22
Texas NELAP T104704286 09-30-22
US Fish & Wildlife US Federal Programs 058448 07-31-22
USDA US Federal Programs P330-21-00056 05-17-24
Virginia NELAP 460166 06-14-22
West Virginia DEP State 136 05-31-22
Eurofins Savannah
Page 22 of 27 4/11/2022

Method Summary
Glient: Bio-Nomics Services„ Inc. Job ID: 680-213280-1
Project/Site: Greenville Utilities
Method Method Description Protocol Laboratory
8260D Volatile Organic Compounds by GC/MS SW846 TALSAV
8270E Semivolatile Organic Compounds (GC/MS) SW846 TALSAV
8081E Organochlorine Pesticides (GC) SW896 TAL SAV
8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL SAV
8151A Herbicides (GC) SW846 TAL SAV
6010D Metals (ICP) SW846 TALSAV
7470A Mercury (CVAA) SW846 TAL SAV
1010B lgnitability, Pensky-Martens Closed -Cup Method SW846 TAL PEN
9012B Cyanide, Total andor Amenable SW846 TAL SAV
9034 Sulfide, Acid Soluble and Insoluble (Titrimetrlc) SW846 TAL SAV
9045D pH SW846 TALSAV
Moisture - 2540 Percent Moisture SM TAL SAV
1311 TCLP Extraction SW846 TAL SAV
3010A Preparation, Total Metals SW846 TAL SAV
3510C Liquid -Liquid Extraction (Separatory Funnel) SW846 TAL SAV
3546 Microwave Extraction SW846 TAL SAV
5030E Purge and Trap SW846 TAL SAV
7470A Preparation, Mercury SW896 TAL SAV
8151A Extraction (Herbicides) SW846 TAL SAV
9012B Cyanide, TotalandlorAmenabie, Distillation SW846 TALSAV
9013 Cyanide Extraction (Solids and Oils) SW846 TAL SAV
9030E Sulfide, Distillation (Acid Soluble and Insoluble) SW846 TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of WaterAnd Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 23 of 27 4/11/2022

LestAmeca
5102 LaRoche Avenue
THE LEADER IN ENVIRONMENTAL TESTING
Chain of Custody Record
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Site Contact:
Lab:Contact< David Fuller
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Sample Identification
Page 24 of 27
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Relinquished by
L/11 /2022

LZ do ya abed
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Phone: [phone] Fax: [phone]
Client Information (Sub Contract Lab)
Client Contact:
Shipping/Receiving
Company:
Eurofins Environment Testing Southeast,
Address:
3355 McLemore Drive,
Cisy.
Pensacola
State. 2ip:
FL, 32514
Phone:
Sampler:
Phone:
Chain of Custody Record
11
II
I'III
Il'IIII
III
11111
tiff eurofins
Environment Testing
America
Due Date Requested:
4/5/2022
TAT Requested (days):
Lab PM:
Fuller, David
E-Mail:
[e-mail]
850-474.1001(Tel) 850-478-2671(Fax)
Email
Project Name.
Greenville Utilities
Site:
POo
WON:
P*CI 4
68025256
SSOwa:
Sam le Identification - Client ID (Lab ID)
Greenville WTP (680-213280.1)
Simple Date
3/29/22
Sample
Time
10:00
Eastem
Sample
Type
(C-comp,
Matrtx
a -..la.
o-wa,ueq
G-grab) ar.TI..,,.,,,.m,)
Preservation Code:
Solid
Accreditalions Required (See note{:
State - North Carolina (W W/S W ); State - South Carolina
Canter Tracking Nola).
Stale of Origin:
South Carolina
COC No
680-688461.1
0
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0
10tOlEd Ipnilabillly, PsnskyMarIons Closed -Cup
X
Analysis Requested
Page:
Page 1 of 1
Job At:
680-213280-1
Preservation Codes:
A -HCL
B- NaOH
C - Tr. Acetate
D - Nitric Add
E NaHSo4
F - McOH
G - Amchlor
H - Ascorbic Acid
I - Ice
.1 - DI Wale,
o K-EDTA
L•EDA
c
u Other:
0
0
x
St
S_p e c i a l Instructions/Note:
M - Hexane
N - None
O-ASNeO2
P - Na204S
0 - Na2S03
R - Na2S203
S - H2SO4
T - TSP Dodecahydrate
U - Acetone
V -MCAA
W - pH 4-5
2 - other (specify)
Note: Since Laboratory accrednedons are subject to change, Eurofins Environment Testing Southeast. LLC places the ownership of method, aoalyle & a credi{ation compliance upon out subcontract aboratories TM sample shi
does not currentty maintain accreditation In the State of Origin listed above for anelysisneate rlratrie being analyzed. the samples must be shipped back o the Eurofins Environment Testing SautheaoL LLC laboratory or other instructions col I be
P viron e t Testing
Southeaser t, LLC.
If the laboratory
status should be brought fa Eurofins Environment Testing Southeast, LLC attention immediately. If all requested atxretlilarieng are current to dare, return the signed Chain of Custody attesting to sold complicance to Eurdfms Environment Testing Southeast, LLC.
provided. Any changes to accreditation
Possible Hazard Identification
Unconfirmed
Deliverable Requested: I, II, III, IV, Other (specify)
Empty Kit Relinquished by:
Relinquished by:
Relinquished by.
Relinquished by:
Custody Seals Intact: 'Custody Seal No.:
a Yes A No
Pnmary Deliverable Rank: 2
Date:
Datef[imy_;
3--1
Daterrime:
Dalerrime:
/Lrac)
Company
r
Company
Company
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Cl Return To Client I= Disposal By Lab I= Archive Far Months
Special Instructions/QC Requirements:
Time:
`Melhod of Shipment
Received by:
Received by:
Received by:
CoolaVemperature(s) °C and Other Rerdarks:
Dale/rime:
eaten -me.
Company
Company
Da1eFTTii le: �,Fom an
Ver: 06/08/2021

Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc. Job Number: 680-213280-1
Login Number: 213280
List Number: 1
Creator: Sims, Robert D
Question
Answer Comment
List Source: Eurofins Savannah
Radioactivity wasn't checked or is </= background as measured by a survey NIA
meter,
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with ail pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time (excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely tilled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins Savannah
Page 26 of 27 4/11/2022

Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc. Job Number: 680-213280-1
Login Number: 213280
List Number: 2
Creator: Whitley, Adrian
Question
Answer Comment
List Source: Eurofins Pensacola
List Creation: 03131/22 01:29 PM
Radioactivity wasn't checked or is </= background as measured by a survey NIA
meter.
The coolers custody seal, if present, is intact. N/A
Sample custody seals, if present, are intact. N/A
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable, True
Cooler Temperature is recorded. True
COC is present. True
COC Is filled out in ink and legible. True
COC is filled out with all pertinent information. True
is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time (excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is N/A
<6mm (1/4" ).
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
4.8°C IRB
Eurofins Savannah
Page 27 of 27 4/11/2022