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HomeMy WebLinkAbout#5016 - 06 - 2010 - FINALINSPECTION REPORT ROUTING SHEET To be attached to all inspection reports in-house only. Laboratory Cert. #: Laboratory Name: Inspection Type: Inspector Name 2 Inspection Date: Date Report Completed; Date Forwarded to Reviewer: Reviewed bv: Date Review Completed: Cover Letter to use: Unit Supervisor: Date Received: Date Forwarded to Alberta: Date Mailed: 5016 Lowes Company Iredell Distribution Field Maintenance Chet Whiting June 25, 2010 July 8 2010 July 8 2010 Todd Crawford Julv 9 2010 Insp. Initial X Insp. Reg. _ Insp. No Finding Insp. CP Gary Francies 8/20/2010 9/3/2010 ',tJF A&INtA. NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleen H. Sullins Governor Director September 7, 2010 5016 Mr. Rocky Everidge Lowes Company Iredell Distribution 711 Tomlin Mill Road Statesville, NC 28625 SUBJECT: North Carolina Wastewater/Groundwater Laboratory Certification (NC WW/GW LC) Maintenance Inspection Dear Mr. Everidge: Dee Freeman Secretary Enclosed is a report for the inspection performed on June 25, 2010 by Mr. Chet Whiting. I apologize for the delay in getting this report to you. Where finding(s) are cited in this report, a response is required. Within 30 days of receipt, please supply this office with a written item for item description of how these finding(s) were corrected. For certification maintenance, your laboratory must continue to carry out the requirements set forth in 15A NCAC 2H .0800. Copies of the checklists completed during the inspection may be requested from this office. Thank you for your cooperation during the inspection. If you wish to obtain an electronic copy of this report by email or if you have questions or need additional information please contact me at 828-296-4677. Sincerely, Cta,, Gary Francies Unit Supervisor Laboratory Section CC: Chet Whiting Master files CENR oWQ Laboratory Section NC Wastewater/Groundwater Laboratory Certification Branch One - 1623 Mail Service Center, Raleigh, North Carolina 27699-1623 N6fffiCarofina Location: 4405 Reedy Creek Road. Raleigh, North Carolina 27607-6445 Phone, 919-733-3908 t PAX: 919-733-6241 6l��c `ltr'Ralll, r Internet www.dwglab.org An EquaiOpportunity I Affinnn6ve Action Employer Customer Service: 1-877-623-6748 wvrw.ncwaterquality.org AUDITOR(S): Lowes Company Iredell Distribution NCO085120 Lowes Companies, Inc. 711 Tomlin Mill Road Statesville, NC 28625 5016 June 25, 2010 Field Maintenance Chet Whiting Rocky L. Everidge This laboratory was inspected to verify its compliance with the requirements of 15A NCAC 2H .0800 for the analysis of environmental samples. GENERAL COMMENTS: The laboratory was clean, well maintained and well organized. Benchsheets and documents were well designed and were easily retrievable for review. Findings A and B are new policies that have been implemented by our program since the last inspection A. Finding: The laboratory needs to increase the documentation of materials and reagents used. Requirement: All chemicals, reagents, standards and consumables used by the laboratory must have the following information documented: Date Received, Date Opened (in use), Vendor, Lot Number, and Expiration Date. A system (e.g., traceable identifiers) must be in place that links standard/reagent preparation information to analytical batches in which the solutions are used. Documentation of solution preparation must include the analyst's initials, date of preparation, the volume or weight of standard(s) used, the solvent and final volume of the solution. This information as well as the vendor, manufacturer, lot number, and expiration date must be retained' for chemicals, reagents, standards and consurabies used for a period of five years. Consumable materials such as pH buffers and lots of pre -made standards are included in this requirement. Ref: Quality Assurance Policies for Field Laboratories. Page 2 #5016 Lowes Company Iredeli Distribution pH -- Standard Methods, 18t" Edition, 4500 H+ S Comment: The temperature correction was not posted on the instrument. Technical Assistance for Field Analysis of pH states: All thermometers and temperature measuring devices must be checked every 12 months against a MIST certified or NIST traceable thermometer and the process documented even if the instrument is not used for reporting temperature results. To check a thermometer or the temperature sensor of a meter, read the temperature of the thermometer/meter against a NIST certified or NIST traceable thermometer and record the two temperatures. The thermometer/meter readings must be less than or equal to 1°C from the NIST certified or NIST traceable thermometer reading. The documentation must include the serial number of the NIST certified thermometer or NEST traceable thermometer that was used in the comparison. Also document any correction that applies on both the thermometer/meter and on a separate sheet to be filed. (NOTE: Other certified laboratories may provide assistance in meeting this requirement.) The correction was posted on the instrument during the inspection which adequately addresses this finding. No further response is necessary for this finding. B. Finding: Values are reported that exceed the method specified accuracy (0.1 S.U) for this analysis. Requirement: A variance of ± 0.1 pH unit represents the limit of accuracy under normal conditions, especially for measurement of water and poorly buffered solutions. For this reason, report pH values to the nearest 0.1 pH unit. Ref: Standard Methods, 181h Edition, 4500 H+ B. (6). C. Finding: The collection and analysis times are not clearly documented. Requirement: Data pertinent to each analysis must be maintained for five years. Certified Data must consist of date collected, time collected, samples site, sample collector, and sample analysis time. The field bench sheets must provide a space for the signature of the analyst, and proper units of measure for all analyses. Ref: 15A NCAC 2H .0805 (g) (1). Comment: Since pH is analyzed in situ, a statement indicating that collection and analysis times are the same may be added to the benchsheet, or the column header may be changed to "Time Col lected/Analyzed." IV. PAPER TRAIL INVESTIGATION: The paper trail consisted of comparing field testing records and contract lab reports to Discharge Monitoring Reports (DMRs) submitted to the North Carolina Division of Water Quality. Data were reviewed for Lowes Company Iredell Distribution (NPDES permit # NC0085120) for May, 2010. No transcription errors were detected. The facility appears to be doing a good job of accurately transcribing data. r •, Correcting the above -cited findings will help this lab to produce quality data and meet certification requirements. The inspector would like to thank the staff for its assistance during the inspection and data review process. Please respond to all findings. Report prepared by: Chet Whiting Date: July 8, 2010 Report reviewed by: Todd Crawford Date: July 9, 2010