WQ0035049_Monitoring - 11-2022_20221221 (2)

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
WQ0035049
Maple Hill WWTF
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
G W-59
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2022
Upload Document*
November2022_NDMR_ND... 4.81 MB
PDF Only
November2022_Grou ndwat... 3.12MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-7, NDAR-2, NDMLR, GW-59).
[e-mail]
Kenny Keel
12/21 /2022
This will be filled in automatically

Reviewer: Gerald, Wanda
Is the project number correct?* WQ0035049
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 1/11/2023

SUBMIT FORM ON YELLOW PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
rgA"Li I T I NI-UKIVIA I IUN crease Print clearly or Type
Facility Name: Maple Hill WWTF - Wastewater Irrigation System
Permit Name (if different):
Facility Address: 306 Maple Hill School Rd
'HE
NC 28454-7612 County Pander
Contact Person- Christopher Pickett Telephone#: [phone]
Well Location/Site Name: MW-1 No. of wells to be sampled: 4
SAMPLING INFORMATION (from Permit)
WELL ID NUMBER (from Permit): MW-1 Date sample collected: 11/7/2022
Well Depth: 20 ft, Well Diameter: 2 in.
Depth to Water Level 82546: 12.5 ft. below measuring point Screened Interval: 3 ft, to 20
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 33
Volume of water pumped/bailed before sampling: 10 gallons
for metals were
and field acidified: El YES F-1 NO
IENT OF ENVIRONMENT & NATURAL RESOURCES
OF WATER QUALITY4NFORMATION PROCESSING UNIT
NC276994617 Phone: [phone]
or WQ0035049 Expiration Date: March 31
WQ0035049 UIC
lutb Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon 0 Remediation: Infiltration Gallery
Spray Field El Remediation:
ED Rotary Distributor El Land Application of Sludge
F-1 Water Source Heat Pump El Other:
FIELD ANALYSES:
WAS
PH 00400: 4.3 units Temp. 0001o: 20.0 oc
DRY at
Spec. Cond. 00094; gMhos
time of
Odor 000w: None
samplir
check
Appearance Tan
herer
ate sample analyzed: November 7--November 2512022 Laboratory Name: Environmental Chemists, Inc, Certification No. 94
%RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations,
COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1 /100mi- Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 --mg/L
Coliform: MF Total 315o4 /100ml- Phosphorus: Total as Poo665 mg/L
(Note: use MPN method for highly turbid samples)
Orthophosphate 70507 ma/L
solved Solids:Total 70300 73
mg/L
PH (Lab) 00403 4.3
units
TOC oowo 4.6
mg/L
Chloride 00940 18
mg/L
Arsenic 01002
ug/L
Grease and Oils oo552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
fie Conductance =95
gMhos
Total Ammonia omio <0.2
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
TKIN as N 00625 mg/L
Other (Specify Compounds and Concentration Units):
At - Aluminum ol im mg/L
Be - Barium o=7 Ug/L
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
Fe - Iron 01045
ug/L
Hg - Mercury 71900
Ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese 01055
uall-
Ni - Nickel 01067 ug/L
For Remediation Systems Only (Attach Lab Reports): - Influent Total VOCs:
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? El Yes (1) M No (0)
VOC 78732: method #
mg/L Effluent Total VOCs:
method #
method #
method #
mg/L VOC Rernoval%
Christopher Pickett /Superintendent
Permittee (or Authorized Agent) Name and Title - Please print or type 1216/2022
GW-59 Rev. 2/2010 Signature of Pe ittee (or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: E=1617
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Maple Hill WWTF - Wastewater Irrigation System
DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: W00035049 Expiration Date: March 31, 2026
Non -Discharge W00035049 UIC
Permit Name (if different):
NPDES Other
Facility Address: 306 Maple Hill School Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
Maple Hill NC 28454-7612 County Pander
❑ Lagoon g ❑ Remediatlon: Infiltration Gallery
® Spray Field ❑ Remediatlon:
Contact Person: Christopher Pickett
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: MW-2
No. of wells to be sampled: 4
from Permit)If
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 11/7/2022
WELL
FIELD ANALYSES: WAS
Well Depth: 12 ft,
Well Diameter: 2 in,
pH oo400: 5.9 units Temp. 000lo: 20.5 eC DRY at
Depth to Water Level 82546: 9.2 ft. below measuring point Screened Interval: 3 ft. to
12
ft, Spec. Cond. 00094: µMhos time of
Measuring Point is 3 ft, above land surface
Relative M.P. Elevation: 31.5 ft•
sampling,
odor 00065; Slight Sulfur
Volume of water pumped/bailed before sampling: 10
gallons
check
Appearance White/Tan here:®
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: November-7 November 125 /2022 Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 K0.04
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use M PN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Tota17o3o0 368 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.9 units
Ba - Barium 01007
ug/L
TOC oomo 10.3 mg/L
Ca - Calcium oo916
mg1L
Chloride 0094o 32 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and 011s 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
Specific Conductance 00095
µMhos
Total Ammonia oo6lo 0.3
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
TKN as N 00625
mg/L
For Remediation Systems Only (Attach Lab Reports):
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
K - Potassium 00937
mg/L
VOC 78732; method #
Mg - Magnesium 00927
mg/L
method #
Mn - Manganese oio55
ug/L
method #
Ni - Nickel 01067
ug/L
method #
cent Total VOCs:
mg/L Effluent Total VOCs: mg/L VOC Removal1%
Ghrtstopher Pickett (superintendent vtr9 ,i ,y 'rz� 12 /6 /2022
Permittee (or Authorized Agent) Name and Title - Piease print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Facility Name: Maple Hill WWTF - Wastewater Irrigation System
Permit Name (if different):
Facility Address: 306 Maple Hill School Rd
ME
NC
County Pander
OF WATER QUALITY -INFORMATION PROCESSING UNIT
CENTER, RALEIGH, NO 27699-1617 Phone:
PERMIT Number: W00035049 Expiration Date:
Non -Discharge W00035049 UlC
NPDES
Contact Person: Christopher Pickett Telephone#: [phone]
Well Location/Site Name: MW-3 No. of wells to be sampled: 4
from- Permit)
SAMPLING INFORMATION I
WELL ID NUMBER (from Permit): MW-3 Date sample collected: 11 /712022
Well Depth: 20 ft, Well Diameter: 2 in.
Depth to Water Level 82546: 6.2 ft. below measuring point Screened Interval: 3 ft, to 20 ft.
Measuring Point is 3 ft, above land surface Relative M.P. Elevation: 34.5
Volume of water pumped/bailed before sampling: 10 gallons
were
I and field acidified: El YES El NO
733-3221
31
'PE OF PERMITTED OPERATION BEING MONITORED
171 Lagoon ❑ Remediation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
F❑1 Water Source Heat Pump E71 Other:
FIELD ANALYSES:
WAS
pH 00400: 6.1 units Temp. 000lo: 19.7 oc
DRY at
Spec. Cond. 00094: IaMhos
time of
Odor 00085: None
sampling,
check
Appearance Tan
here: El
ate sample analyzed: Novenber/ 7 - November 125 /2022 Laboratory Name: Environmental Chemists, Inc. Certification No. 94
%RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD o0335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /10OmL Nitrate (NO3) as IN 00620 <0,02 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100ml- Phosphorus: Total as Poo665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units
solved Solids:Total 70300 253
mg/L
pH (Lab) 00403 6.1
units
TOC oo68o 6.4
mg/L
Chloride 0094070—
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
fic Conductance 00095
AMhos
Total Ammonia oosio <0.2
mg/L
(Ammonia Nitrogen; NH3aS N; Ammonia Nitrogen, Total)
TKN as N oo625 mg/L
Al - Aluminum oil o5 mg/L
Be - Barium 01007 ug/L
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
Fe - Iron 01045
ug/L
Hg - Mercury 71900
ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese olo55
ug/L
. Ni - Nickel 01067
ug/L
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? M Yes (1) D No (0)
VOC 78732: method #
method #
method #
method #
mg/L Effluent Total VOCs:
mg/L VOC Removal%
Christopher Pickett / Superintendent
Permittee (or Authorized Agent) Name and Title - Please print or type 12/6/2022
GW-59 Rev. 2/2010 Signature of PerAittee {or Agent) (Date)

SUBMIT FORM ON YEL40W PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Maple Hill WWTF - Wastewater
Permit Name (if different):
Facility Address: 306 Maple Hill School Rd
Maple Hill NC
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
or Type 1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: [phone]
IPERMIT Number: WQ0035049 Expiration Date: March 31, 2026
Non -Discharge WQ0035049 UIC
NPDES i Other
County Pender
Contact Person: Christopher Pickett Telephone#: [phone]
Well Location/Site Name: MW-4 No. of wells to be sampled: 4
SAMPLING INFORMATION ttom
Parma) t
WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11 / 7 / 2022
Well Depth: 20 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 9.5 ft. below measuring point Screened Interval: 3 ft. to 20 ft.
Measuring Point is 3 —ft. above land surface Relative M.P. Elevation: 35.5
Volume of water pumped/bailed before sampling: 10 gallons
Samples for metals were collected unfiltered: El YES El NO
0 and field acidified: FIYES n NO
'PE OF PERMITTED OPERATION BEING MONITORED —
El Lagoon rl Remediation: Infiltration Gallery
M Spray Field 17 Remediation:
1771 Rotary Distributor El Land Application of Sludge
El Water Source Heat Pump E3 Other:
FIELD ANALYSES:
WAS
pH 0040o: 6.3 units Temp. oom: 19.3 oc
DRY at
Spec. Cond. 00094: gMhos
time of
Odor 000m None
samplir
check
Appearance Tan
here: F
ate sample analyzed: November - 7 - November 25 /2022
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
%RAMETERS NOTE: Values should reflect dissolved and Colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 <0,02 mg/L Pb - Lead oimi ug/L
Coliform: MF Fecal 31616 <1 /100mL N I itrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
solved Solids:Total 7030o 330 mg/L A[ - Aluminum at lo5 mg/L
pH (Lab) o0403 6.3 units Be - Barium 01007 ug/L
TOC omo 5.9
mg/L
Chloride 00940 17
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
Specific Conductance 00095
AMhos
Total Ammonia 00610 <0.02
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
TKN as N 00625
mg/L
For Remediation Systems Only (Attach Lab Reports):
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
ug/L
Cu - Copper 01G42
mg/L
Fe - Iron 01045
ug/L
Hg - Mercury 71900
ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese o1o55
ug/L
Ni - Nickel 01067
ug/L
Total VOCs:
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? El Yes (1) El No (0)
VOC 78732: method #
method #
mg/L Effluent Total VOCs:
method #
method #
mg/L VOC Rernoval%_
Christopher Pickett ]Superintendent zaw
Perm ittee (or Authorized Agent) Name and Title -Please print or type 1 Z 6 /2022
Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev. 2/2010

M'Mnk" 3
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Ine,
6602 Windyi-111 Wa3r Wjhrxlington, NC 28405 ' 910.3910223 [Ab * S1!0392A424F,1'X
710 Bowsertown Road, Manteo, NC 27954 ' 252,473,57021 Lab Fax
25`-A Wfli-ningtiln Hi?
0 ',hway, Jac.k-sonville, NC 2854f) ' 910-UT5843 Lab/Fa).,
infro ; environmentalcliemisui,com
Pander County Utility Operations Date of Report: Nov 25, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2022-2-2146
Project ID: Maple Hill WWTF (Monitoring Wells)
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-54316 Site: MW-1 1117/2022 12:10 PM Water JCB/Envirochem
Test
Method
Results Date Ana lv7ed
Color
Color
Tan
11107/2=
Depth to water, ft.
Depth to Water, Ft,
12.5 feet
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev. ZO, 1993
< 0.2 mg/l.
11/14/2022
Gallons bailed before sampling
Gallons Bailed before sampling
10gallons
11/07/2022
Odor
Qualitative
None
11/0712022
Total Dissolved Solids (TDS)
SM 2540 C-2015
73 mg/L
11/08/2022
Temperature
SM 2550 B-2010
20.0C
11/07/2022
pH
SM 4500 H 8-2011
4.3 units
11/07/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
4.6 mg/L
11108/2022
Fecal Coliform
SM 9222 D-201 5 MF
<1 Colonies/100ml-
11107t2022
Chloride
SM4500 Cl E-2a11
18 mg/L
11/08/2022
Nitrate Nitrogen (Call:)
Nitrite Nitrogen
EPA 353.2, Rev 1 20, 1 1993
< 0.02 mg/L
11/08/2022
Nitrate+Nftrite-Nitrogen
EPA 353 2, Rev, 20. 1993
0.14mglL
11108/2022
Nitrate Nitrogen
Subtraction Method
0,14 mg/L
11/23/2022
Report # M 2022-22146
Page I of 5

mental Chem, "osts, ine"
Qu Environ
' A 4
'4
too, C 28405 91 ,ab
6602 Wirtdiyffll Way, Wilrning I
9103924424,1ax
C',,�.......... 710'wr, Ba6ertowRoad, Ma-nteq, NC 279,54 252,473.570-2 Lab/Fax
' R'R
2 -A Wi Vflle, N
,55 flniingtoil lihghway, ;ackson C'28540 ffi 910,3473F43 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
Ponder County Utility Operations Date of Report: Nov 25, 2022
Post Office Box 995 Customer PO #-
Burgaw NC 28425 Customer 10: 08100095
Attention- Report #: 2022-22146
Project ID: Maple Hill WWTF (Monitoring Wells)
Lab ID Sample ID: Collect Datefrfme Matrix Sampled by
22-54317 Site: MW-2 1117/2022 12:30 PM Water JCB/Envirochem
Test
N=.
Results Date AnalvzAd
Color
color
White/Tan
11/07/2022
Depth to water, ft
Depth to Water, Ft
9.2 feet
1110712022
Ammonia Nitrogen
EPA 350A, Rev. 2 0,1993
0.3mg/L
11/14/2022
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
11/07/2022
Odor
Qualitative
Slight Sulfur
1110712022
Total Dissolved Solids (TDS)
SM 2540 C-2015
368 mg/L
11/08/2022
Temperature
SM 2550 B-201 0
20.5 C
11/07/2022
pH
SM 4500 H B-2.011
5.9units
11107/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
10.3mg/L
11/08/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/07/2022
Chloride
SM4500CIE-2CII
32 mg/L
1110812022
Nitrate Nitrogen (Catc)
Nitrite Nitrogen
EPA i532, Rev, 2.0, 1993
< 0.02 mg/L
11/08/2022
Nitrate+Nftrite-Nitrogen
EPA 353.2, Rev, 2.0. 1993
0-04 mg/L
11/08/2022
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
11/23/2022
RIVOrf fk. '2022-22146
Page 2 of 5

En-Vironmental Chemlists, Irm,
66-92 Windmill Way, W2l9'3Ei.1gton, NC 28405 9U-1392-0223 Lah 910 392.4424 Fax
R
710Bowsertr,)mi Road, Mai -ik '54 1 252,47337M2 Lab/F-ax
�c,NC279
25•-9-A WiljnLngton Highway, facLsonville, NC 28540 ' 910,347-9843 Lab/Pax
ANALYTICAL & CONSULTING CHEMISTS
info
Pender County Utility Operations Date of Report: Nov 25, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28426 Customer ID. 08100095
Attention: Report #: 2022-22146
Project ID: Maple Hill WWTF (Monitoring Wells)
Lab ID Sample ID: Collect Datefrime Matrix Sampled by
22-54318 Site: MW-3 1117/2022 12,50 PM Water JCB/Envirochem
Test Method Results Date Analyzed
Color
Color
Depth to water, ft.
Depth to Water, Ft
Ammonia Nitrogen
EPA 3501, Rev, 2 0,1993
Gallons bailed before sampling
Gallons Bailed Wore sampling
Odor
Qualitative
Total Dissolved Solids (TDS)
SM 2540 G-2015
Temperature
SM255OB-2010
pH
SM 4500 H B-2011
Total Organic Carbon (TOC)
SM 5310 B-2014
Fecal Coliform
SM 9222 0-2015 MF
Chloride
SM4500 Cl E-2011
Nitrate Nitrogen {Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.6,1993
Nitrate+Nitrite-Nitrogen
EPA 353.Z Rev, ZO, 1993
Nitrate Nitrogen
subtraction Method
Tan
1110712022
7.5 feet
11/07/2022
< 0.2 mg/L
11/14/2022
10gallons
11/07/2022
None
11/0712022
253 mg/L
11/0812022
19.7 C
11/0712022
6.1 units
11/07/2022
6.4 mg/L
11/08/2022
<1 Colonies/100ml-
11/07/2022
30 mg/L
11/08/2022
* 0.02 mg/L
11/08/2022
* 0.02 mgtL
11/08/2022
<0.02 mg/L
11/23=22
RePor! # 2022-22146 Page 3 of 5

ANALYrICAL & CONSUONG CHEMIM
En-virommental Chem ]"Ists, Inpe.
66,02 Wliiidmilf Way, Wflnii-igtin, NC 28405 , 930,392,0723 J-ab , 910392,4424'Bix
V
710 Bowsertwvn- Road, NIanteo, NC 27954 - 252.473,55702 Lab/Fax
255-A 'Alth-uiigtoi-t Highivay, Jacksonville, NC -23540 - 910347,5843 Lab/Fa-x
into 1:4-"Cnv i to n rn cm t a Ich em is ts. C Ofil
Pender County Utility Operations Date of Report: Nov 25, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention. Report M 2022-22146
Project ID: Maple Hill WWTF (Monitoring Wells)
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-54319 Site: MW-4 11/7/20" 1:10PM Water JCB/Envirochem
IM
Results Date Analyzed
Color
Color
Tan
11/07/2022
Depth to water, ft.
Depth to Water. Ft,
9,5 feet
11107/2022
Ammonia Nitrogen
EPA 350, 1, Rev. ZO, 1993
< 0.2 mg1L
11/14/2022
Gallons bailed before sampling
Gallons Sailed Wore sampling
10gallons
11/07/2022
Odor
Qualitative
None
11/07/2022
Total Dissolved Solids (TDS)
SM 2540 C-201 5
330 mg/L
11/0812022
Temperature
SM 2550 B-201 0
19.3 C
11/07/2022
pH
SM 4500 H B-2011
6.3 units
11/0712022
Total Organic Carbon (TOC)
SM 5310 E3,2014
5.9 mg/L
11/08/2022
Fecal Coliform
SIM 9222 D-2015 MF
<1 Colonies/100ml-
11/07t2022
Chloride
SM4500 CI E-2011
17 mg/L
11/0812022
Nitrate Nitrogen (Cale)
Nitrite kitrogen
EPA 3532, Rev 2 0 1993
< 0.02 mg/L
11/08/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1093
< 0.02 mg/L
11/08/2022
Nitrate Nitrogen
Subtraction Method
<0.02 mgIL
11/23/2022
R Mitt # 2072-22146 Page 4 of 5

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rt771-7-7

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
P-ni I r-('Tlnkl AKIn (%UAIKI f%C
6602 Windmill Way Wilmington, NC 28406
OFFICE- 910-392-0223 FAX [phone]
[e-mail]
CLIENT: Pender County Utilities
PROJECT NAME: Maple Hill WWTP Monitoring Wells
REPORT NO: 2—Lf
ADDRESS:
CONTACT NAME:
PO NO.,
REPORT TO: Chris Pickett, ORC
PHONE/FAX:
COPY TO:
email::
-QAUDI 1z'rV0=- I - 1-91--* = - Atli - 1., .1
Sample Identification
Collection
E
e
E
Ir
W
PRESERVATION
ANALYSIS REQUESTED
Qate
Time
Temp
8
-
0
0
tu
a0
Well:
irk C—
C
P
1 61/31 ko
x
TDS, 0, NO2
G
G
Depth to water: 0
x
NO3, NH3
G
G
gallons bailed: 14
x
Fecal Coliform
G
G
pH (flield).
fq. 1A
C
P
x
Total Organic Carbon
G
G
odor (field):
C
P
G
G
C
P
G
G
C
P
Total of 4 wells: due In March, July, November.
Transfer
Relinquished By:
Daterrime
By:
DatefTime
9.
-Received
2.
Delivered By: Rei
Comments:
13
e Rpcipested:

ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
Analytical & Consulting Chemists
6602 Windmill Way Wilmington, NC 28406
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: Pender County Utilities
PROJECT NAME: Maple Hill WWTP Monitoring- Wells
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO., Chris Pickett, ORC
PHONEIFAX:
COPY TO:
lemail::
QAMDI 9= Tvo=. I - I f! - ­1
Sample Identification
Collection
1
E
W
.3
ri
0
0
0
q "0
0 P�
0
Is -j
86
:E E
W
to
z
PRESERVATION
U1, -31- —ZIUC190, vEner.
ANALYSIS REQUESTED
Date
Time
Temp
W
z
j
�
I "
;c
0
9
Well:
4-14 �;Z`
1,21-11
C ---
P
x
TDS, Cl, NO2
G
G
Depth to water: t a
G
P—
x
NO3, NH3
G
G
gallons bailed:
C
P
i
I x
Fecal Coliform
G
G
pH (field :
C
P
x
Total Organic Carbon
G
G
odor(field):
C
P
G
G
9
C
P
G
G
C
P
'Total of 4 wells: due In March, July, November.
Transfer
Relinquished By:
Daterrime
Received By:
Daterrinne
2.
M 9ample
Delivered By:_ Received By.-_ f 49 Date:
Comments: rj
Time-0 rt- -Z
ROUND:
"N.2d,

6602 Windmill Way Wilmington, NC 28406
ENVIRONMENTAL CHEMISTS, INC OFFICE, 910-392-0223 FAX [phone]
Analytical i 6ns Iting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS.* DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Pender County Utilities PROJECT NAME: Maple Hill WWTP Monitoring Wells REPORT NO. Q I -A ""If "D"
ADDRESS: CONTACT NAME: PO NO:
REPORT TO: Chris Pickett, ORC PHONE/FAX:
COPY TO:
Sam -pled By: IZARADI = TVMC. I
Sample Identification
Collection
E
E 0
0
oil
E
¢
—
PRESERVATION
I — ­911, %a I — tZLI UU111,
Q%J = C1011, bL = ZALICIge, Uhler:
Dote,
Time
Temp
ANALYSIS REQUESTED
2!
o
0
o
o
w
Well:
C
P
Z,
x
TDS, CI, NO2
G
-----
Depth to water:
F- [1 j
gallons bailed,
--
C
P
--J
x
x
NO3, NH3
Fecal Coliform
G
_C
G%
_P
-
G
Gl--.
pH (field):
odor (field):
C
P
x
Total Organic Carbon
G
G
G
'41 f
C
_G
P
G
G
C
P
G
G_T
Total of 4 wells; due In March July, November,
Transfer
Relinquished By: _T_
DatelTime
Received BY
Dateffirne
12
TarnnPraftirp vuhan
--mesampie Kgqupsteel:
Delivered By:
—Received By: . .. ..... . .... Date:-
Comments: ........ —

6602 Windmill Way Wilmington, MC 28406
ENVIRONMENTAL CHEMISTS, INC OFFICE. 910-392-0223 FAX 910-392
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION 4 94 NCDHHS: DLS CERTIFICATION # 37729 -4424
[e-mail]
CLIENT: Pender cou
ADDRESS:
Sample Identification
Well:
Ji
Depth to water: pq
gallons bailed: f a
pH (field}:
odor (field)- >A?—
Utilities COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME. Maple Hill WVVTP Monitoring
Wells REPORT NO: 1'1�"
CONTACT NAME: PO NO:
REPORT TO: Chris Pickett, ORC PHONE/FAX:
COPY TO: email:: --------------
Collection SAMPLE TYPE: I = Influent, E Effluent, W = Well, ST = Stream, SO » Soil, SL = Sludge, Other.,
4D PRESERVATION
C, Lu
E EL
of 4 WOUS: due In March, July, November.
03 � Temp 0 0 e:, 2 E 0 z 0 ANALYSIS REQUESTED
X = z F-
0
C
G G SY311
C P TDS, C
G 2
C P x NO3,
x Fecal C(
C P
G G
C P Total OLgan
G G
C P
G G
C P
G G
Received By. •
2.
Temperature When Recelyed:cceptc!111:111: ­— —Rejecte ........ .... ... ...
Delivered By: -----.Resampl R q e sted
7 ),1 Time:
Comments: Received By-_._._...____ ----.-,-.__Date
4N—ROUN`DT U R
NH3
iform
Carbon

Analytical & Consulting Chemists
CLIENT: Pender County Utilities
ADDRESS,
Sample Identification
Z-11Z '
4 wells: due in March, July, November.
kill
6602 Windmill Way Wilmington, NC 28405
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-0223 FAX [phone]
NCDENR: DWQ CERTIFICATION # 94 NCOut- ,,, t C
MK I IrK.A I ION # 37729 [e-mail]
OLLECTION AND CHAIN OF CUSTODY
:'ROJECT NAME: Maple Hill WWTp Monitoring Wells REPORT NO-
"ONTACT NAME: PO NO:
1EP0 ; RT TO: Chris Pickett, ORC PHONE/FAX:
I
,OPY, TO: email::
Alection
r=
IF
E 0
0
C
mttuent,
I=
U1
M
z
= Effluent,
PRESERVATION
W
= Well,
ST =
Stream,
SO = Soil, SL = Sludge, Other:
ANALYSIS REQUESTED
Time
Temp
0
=
0
W
0
z
0
g
P
x
TDS, Cl, NO2
G
G
C
P
G
G
x
NO3, NI-13
C
G
P
G
x
Fecal Coliform
C
P
G
G
x
T
Total Organic Carbon
C
P
G
G
C
P
G
G
C
—G
P
G
e I Received By:
Temperature when Received, Accepted:Rejected;'
, '' ' I --j— --
Delivered By: -�Resample =eted:
_Received By:
Comments: Time:. e �--aLSL-
TURNAROUND:

Q . fni F-ef,-"m q-0
JE.nw. Iroanamernal h4ail-wTtA
66Q V'Vi�,,dnwfl, I;VayVIV, III, L,-jA, NC 26405 91,0392,4424 klN
710 Bowsermwr, Road, Alvlanteo, NC,27954 252,473,1,5702
25;-,A Wllrnftvon 1-fighwav, T- IN
9110,347,5843L,1,17w
ANALYTICAL & CONSULTING CHEMISTS inh)(dycnviroynnental�h - L ernis(S.Coin,
,
Pender County Utility Operations
Date of Report: Nov 16, 2022
most Office Box 995
Customer Po #:
Burgaw NC 28425
Customer ID: 08100095
Attention-.
Report #.- 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-52108 Site: Zone 1
10/24/2022
11:45 AM Solid/Sludge Chris Pickett
Test
Method -
Results Date Analyzed
of Fertility
Calcium
EPA 200.7
392 mg/kg
11104/2022
Copper
EPA 2003
1.57mgJkg
11/04/2022
Magnesium
EPA 2001
102 mg/kg
11/04/2022
Manganese
EPA 200,7
3.58 mg/kg
11/04/2022
Potassium
EPA 200,7
54.6 mg/kg
11/04/2022
Sodium
EPA 20D,7
<51.1 mg/kg
11/04/2022
Zinc
EPA 2001
9.91 mg/kg
11/04/2022
Acidity (Sol[ Fertility)
NCDA-Agronomic Division
5 meq/1 OOg
11101/2022
Base Saturation
NCDA-Agronomic Division
37.9%
11/16/2022
Cation Exchange Capacity
NCDA-Agmnomic Division
7.70 meq/1 OOg
11/1612022
Exchangeable Sodium Percentage
NCOA-Agronomic Division
2,90 %
11/16/2022
Humic Matter
NCOA-Agronomic Division
19A %
11/10/2022
Total Solids (%)
SM 2540 EI
76.0%
10/26/2022
Total Phosphorus
SM 4500 P F
81.2 mg/kg
11/02/2022
PH SW 846 Method 9045D
Result estimated Analyzed out of 15 minutes hold time.
4,36units
11/01/2022
Reporl� 20,72,21243
Page *, or 1"

-0
nvirarimem
U, C28 1) 910223 Lab 9101,39-2,4424 Fax
660' W'Ind!vkill !A�ay, Wihanin�, ri� N - W 5 9`10,3 . .... 7/Fax '71564 2-51473,5702 LAO , NC 10 Bowsertoivn Road, Nlaiitvcn
7 —0,347,5843 Lab'Fax
-owvi le, NC 28-540 V fighway, Jacks -A' ni, I2-5 5
ANALYTICAL & CONSULTING CHEMISTS iv "o ct4er vi ro I I M C ra a I c h C I r 131 S,CoIn
Pender County Utility Operations Date of Report: Nov 16, 2022
Post Office Box 995 Customer PO #.
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
22-52112 Site: Zone 2 10124/2022 11:49 AM Solid/Sludge Chris Pickett
Test Method
Soil Fertility
Results Date Analyzed
Calcium
EPA 200 7
399 mglkg
11/04/2022
Copper
EPA 200 7
<0.967mgikg
11/04/2022
Magnesium
EPA 200 7
139 mg/kg
11/04/2022
Manganese
EPA 200 7
1.65 mg/kg
11/04/2022
Potassium
EPA2007
120 mg/kg
11/04/2022
Sodium
EPA 200 7
206 mg/kg
11/04/2022
Zinc
EPA 200 7
13.3 mg/kg
11/04/2022
Aridity (Soil Fertility)
NCOA-Agronomic Division
7 meq11 OOg
11101/2022
Base Saturation
NGDA-Agronomic Division
33J %
11116/2022
Cation Exchange Capacity
NCDA-Agronomic Division
10.2meq/100g
11116/2022
Exchangeable Sodium Percentage
NCDA-Agronomic Division
8.80%
11/1612022
Humic Matter
NCDA-Agronomic Division
21A %
11110/2022
Total Solids M
SM 2540 B
82,5%
10/26/2022
Total Phosphorus
SM 4500 P F
108 mg/kg
1110212022
pH
SW 846 Method 9045D
4.90 units
1110112022
Result estimated Analyzed out of 15
minutes hold time.
Peport A 2022-21246 Page 2 of I 9

Ekxia✓dxY+ %vazu UAn.emlC.uw#
x.w°,Xu,.i`%d�l...
x j(`411,y Y11;r1d,'rM 1,Alay brt g'a'168r; tzi NC 2821.,,f 910,39 0223 Lai �`�3„0...}9
42 i.
i
,¥ r
xzO ..
fi Bow,,erfown Road 10wita {7 NC 277954 `` 2 )Af3. Y 02
E 1%
i
ANALYTICAL & CONSULTING CHEMISTS
Pender County utility Operations Date of Report: Nov 16, 2022
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention:
Report M 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID:
Collect Date/Time Matrix Samples! by
22-52113 Site: Zone 3
10/24/2022 11:56 AM SolidlSludge Chris Pickett
Test
Method Results Date Analyzed
Soil Fertility
Calcium
EPA 200 7 357 mglkg
11/04/2022
Copper
EPA 200 7 <0, 886 mg/kg
11/04/2022
Magnesium
EPA2007 153 mg/kg
11104/2022
Manganese
EPA 2a0 7 <0.886 mg/kg
11/04/2022
Potassium
EPA 200 7 51.8 mglkg
1110412022
Sodium
EPA 2003 209 mg/kg
11/04/2022
Zinc
FPA200.7 1,85mg/kg
11104/2022
Acidity (Soil Fertility)
NCDA-Agronomic Division 5 meq/100g
11/01/2022
Base Saturation
KDA-Agronomic Division 36.8 %
11/16/2022
Cation Exchange Capacity
NCDA-Agronomic Division 8,60 meq/100g
11/16/2022
Exchangeable Sodium Percentage
NCDA-Agronomic Division 10.6 %
11/16/2022
Humic Matter
NCDA-Agronomic Division - 15-3%
11/10/2022
Total Solids (%)
SM 2540 6 82.8 %
10/2612022
Total Phosphorus
sM 4500 P F 64,9 mg/kg
11102/2022
pH
SW 846 Method 9045D 4.74 units
11 /0112022
Result estimated Analyzed out of 15 minutes
hold time.
Report #.�2Q22-2ti46 page 3ot91,:�.,�,,.�,.

E rev i r o -n. B. a
ir Jr "I Wn 0 12,0223 1 vb 9103 2,442,1 FaMM
(i66�2 V;' d ni, y; Wilmington, NC 28405 9 j.29
5 252 4' 1,57702 L It. Fax
71() Bow�wrtovvn ant Road, jVeo, NC 27 9 4
Y55-A Wi lynington f 1 gh1vay, jar ksonvi fle, NC 28540 910347,58431,ab/Fax
ANALYTICAL & CONSULTING CHEMISTS ink)
Pender County Utility Operations Date of Report: Nov 16, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2022-21248
Project 10: Maple Hill Sprayfield
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-52114 site: Zone 4 10/24/2022 12:01 PM Solid/Sludge Chris Pickett
Test Method
Soil Fertility
Calcium
EPA 200 7
Copper
EPA 200 7
Magnesium
EPA 200 7
Manganese
EPA 200 7
Potassium
EPA 200 7
Sodium
EPA 200 7
Zinc
EPA 200 7
Acidity (Soil Fertility)
NCDA-AgronoMir- DwiSion
Base Saturation
NCDA-Aflronoffuc DMS-Wn
Cation Exchange Capacity
NCDA-Agronomic DiVISIon
Exchangeable Sodium Percentage
NCDA-Agronomic Division
H I umi I c - Matte ' r
NC DA- I A9660011C Division
Total Solids M
SM 2540 8
Total Phosphorus
SM 4500 P F
pH
SW 846 Method 9045D
Result estimated Analyzed out of 15
Minutes hold time,
Results Date Analyzed
2050 mg/kg
1110412022
1.21 mg/kg
11104/2022
352 mg/kg
11/04/2022
1.34 mg/kg
11/0412022
52.7 mg/kg
1110412022
206 mgikg
11/04/2022
5.99 mg1kg
11/04/2022
2 meq/1 OOg
11/01/2022
88.0%
11116/2022
15.1 meq/100g
11/16/2022
5.90%
11/16/2022
9.04%
11/1012022
74.8 %
10/26/2022
57.7 mg/kg
11/02/2022
6.33 units
11/01/2022
Repwt # 2022-21248 Page 4 of 71

wa ZL�!."Ivlvon' riaqeirdtal chie ista-" Liaac.
6602 Windn'dIll WayIt' i1mingt of i, NC 28401-5 , 910.392-101223 Lalri ' 910,392.44-2,4' fA'X
o B1 4 ,tArFertcwni�c,,ad,Ncli�itec,,NC27954 , 252,Vi,570.21-ab/Fax
Pender County Utility Operations
Date of Report Nov 16, 2022
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID- 08100095
Attention:
Report #: 2022-21248
Project ID. Maple Hill Sprayfield
Lab ID Sample ID.-
Collect Date/Time Matrix Sampled by
22-52115 Site: Zone 5
10124/2022
12:07 PM Solid/Sludge Chris Pickett
Test
Method
Results Date Analyzed
Soil Fertility
Calcium
EPA2007
572 mg/kg
11/04/2029
Copper
EPA2007
<0.955 mg/kg
11/04/2022
Magnesium
EPA2007
164 mg/kg
11/04/2022
Manganese
EPA2007
1 .05 mgIkg
11/04/2022
Potassium
EPA2007
54.5 mg/kg
11/0412022
Sodium
EPA2007
151 mg/kg
11/04/2022
Zinc
EPA 200 7
2700 mg/kg
11/04/2022
Acidity (Soil Fertility)
NCOA-Agronomic Division
2 meq/1 OOg
11/01/2022
Base Saturation
NCDA-Agronomic Division
78.1 %
11/16/2022
Cation Exchange Capacity
INICDA-Agronomic Division
5,90meq/100g
11/16/2022
Exchangeable Sodium Percentage
NCOA-Agranornic Division
11.0%
11/1612022
Flu M-ic Matter
NCDA-Agronornfic Division
8.24%
1111012022
Total Solids (%)
SM 2540 B
85.8%
10126/2022
Total Phosphorus
SM 4500 P F
80A mg/kg
11102/2022
pH
Sw 646 Method 9045D
5.60 units
11/0112022
Result estmated Analyzed out of 15 minutes hold time,
Report# 2022-21248 Page5afll

11 iR ern, t
zt
'60Q Wh nw�fl ), 14A I r,ingt-iW 28405 n 910,391021,lb 9103912,,'M2-JF,-14
710 Bov,scrtown Road, Manteo, NC27954 252,473,5702 Lat,/F-wx
25 '5 ,1 5--A Wflmii-,gton Highway, lacksonville, NC 2854f) 1 911 ,347, 84,1 f ,+,'Fax
ANALYTICAL & CONSULTING CHEMISTS
Pender County Utility Operations Date of Report: Nov 16, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-52116 site: Zone 6 1012412022 12.23 PM Solid/Sludge Chris Pickett
Test Method Results Date Analyzed
Soil Fertility
Calcium
EPA 200.7
Copper
EPA 200 7
Magnesium
EPA 200 7
Manganese
EPA 200 7
Potassium
EPA 200 7
Sodium
EPA 200 7
Zinc
EPA 200 7
Acidity (Soil Fertility)
NCDA-Agronomic Division
Base Saturation
NCDA-Agronomic Division
Cation Exchange Capacity
NCDA-Agronomic Division
Exchangeable Sodium Percentage
NGDA-Agiranornic Division
Hurnic Matter
NCDK-Agronbrnid Division
Total Solids M
SM 2540 B
Total Phosphorus
SM 4500 P F
SW 846 Method 9045D
pH 6 )A
;
l
Result estimated Analyzed cut 01 urninuies. a E
me.
901 mg1kq
11/04/2022
1 .27 mg1kg
11/04/2022
268 mg/kg
11/04/2022
1,22 mg/kg
11/04/2022
82.0 mg/kg
11/0412022
277 mglkg
11104/2022
7.76 mg/kg
11104/2022
4 meq11 OOg
11/01/2022
65,0%
11/16/2022
10.6 meq/1 OOg
11/16/2022
11.3%
11/16/2022
17.6%
11/1012022
77.6%
10/26/2022
86.2 mg/kg
11102/2022
5.50 units
11101/2022
Report # 2022-21248 Page 5 of I I

28405
W2 1AV3indmill Way!N-Jhnington� W- 5 91-031,92,0223 Lab %0,92 -)1 Fax
' 710 Bowsertown Road, Manteo, NCZ795,4 1-5-.473,1',7021,ablf-ax
25l
14103475 inin I � 5- A WH �gtonfi lgl way , NC28540 843 Lab Fi
ANALYTICAL & CONSULTING CHEMISTS in"'o
Pender County Utility Operations
Date of Report: Nov 16, 2022
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention:
Report #: 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-52117 Site: Zone 7
10/24/2022
12:29 PM Solid/Sludge Chris Pickett
Test
Method
Results Date Analyzed
Soil Fertility
Calcium
EPA 2M7
565 mg/kg
11104/2022
Copper
EPA2007
1,06 mgikg
11104/2022
Magnesium
EPA 200 7
218 mgikg
11104/2022
Manganese
EPA2007
1.22 mg/kg
11/04/2022
Potassium
EPA 200 7
84.2 mg/kg
11104/2022
Sodium
EPA 200,7
291 mg/kg
11/04/2022
Zinc
EPA 2001
5.00 mg/kg
11104/2022
Acidity (Soil Fertility)
NCDA-Agronomic Division
5 meq/1 OOg
11/01/2022
Base Saturation
NCDA-Agronomic Division
49,5%
11/16/2022
Cation Exchange Capacity
NCDA-Agronarnic Division
9.70 meq/1 OOg
11/16/2022
Exchangeable Sodium Percentage
NCDA-Agronomic Division
13.0%
11/16/2022
Hum,lc Matter
-NCoA-A4ronbrnic Division
23.2%
11/10/2022
Total Solids M
SM 2540 B
75,6%
10/26/2022
Total Phosphorus
SM 4500 P F
181 mg/kg
11/0212022
pH
SW 846 Method 9045D
5.41 units
1110112022
ResUltestmated Analyzed out of 15 minutes
hold time.
Report # 2022-21248 Page 7 of 11

T-
4
P't
WITOW 103110IM-11 UJXAeMMPNwa,�� 1111 Ell
Wa 'Allidmifl y, WiltnUil-ti)n, NC 28405 910-3 392,02233 L91 ab 0.392,4424 Fax
710 Bowsertown RoadWnteu,.N'. 27954 , 252,473-57e,)2 Lab/Fiax-
259- A Wi 111,minglon I fighway, jacksofivi'lle, NC 285-10 1 9101,347,58843 Li-ibf Fax
ANALYTICAL & CONSULTING CHEMISTS sl r eavironmeran'K
Pender County Utility Operations Date of Report: Nov 16, 2022
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #-. 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID- Collect Date/Time Matrix Sampled by
22-52118 Site, ZGne 8 10/24/2022 12:35 PM Solid/Sludge Chris Pickett
Test
Method
Soil Fertility
Calcium
EPA 200 7
Copper
EPA 200 7
Magnesium
EPA 200 7
Manganese
EPA 2007
Potassium
EPA 2007
Sodium
EPA 200 7
Zinc
EPA 200 7
Acidity (Soil Fertility)
NCDA-Agronomic Division
Base Saturation
NCDA-Agronomic Division
Cation Exchange Capacity
NCDA-Agronomic Division
Exchangeable Sodium Percentage
NCDA-Agronomic Division
Humic Matter
NCDAAgronomit Division
Total Solids M
SM 2540 6
Total Phosphorus
Sin 4500 P F
pH
SW 846 Method 9MD
Resu It estimated Analyzed out of 15
minutes hold time.
Results Date Analyzed
477 mg/kg
11/04/2022
1.24 mglkg
11/04/2022
205 mg/kg
11/04/2022
< 1. 13 mg/kg
11104/2022
67.3 mg/kg
11104/2022
197 mg/kg
11104/2022
5.85 mg/kg
11104/2022
5 meqf1 OOg
11/01/2022
46.5%
1111612022
9.10meq/10og
11/16/2022
9A0 %
11116/2022
17.3%
11/10/2022
72,7%
10126/2022
65.9 mg/kg
11/0212022
5.19 units
11 /0 1 Q022
Repo # 2022-21248 Page 8 of 11

H V Ehlsl 91 MEC. e
_L Y%71ror rn�l 46'sl U V
I �,Vay
66o2 WmdynM ; Wil-aungton, NC 2,q615 9 10,392 011,23 Lab, 910392,1424 Fit, 71�)Bow,,;ert,)),NrR,,,-,d,Manleo,,NC27954
2,55,A Wilmington Highwa,v. Jacksonvifle, NC ?,8540 - 911(1,34TM43 1,1bl/rax
ANALYTICAL & CONSULTING CHEWSTS ic"fo
Pender County Utility Operations Date of Report: Nov 16, 2022
Post Office Box 995 Customer PO #:
Burgaw NC, 28425 Customer ID: 08100095
Attention: Report #: 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-52119 Site: Zone 9 10/24/2022 1242 PM SolidlSludge Chris Pickett
Test Method Results Date Analyzed
Soil Fertility
Calcium
1:r^/VwJ
Copper
EPA 200.7
Magnesium
EPA 20012
Manganese
EPA 200.7
Potassium
EPA 200.7
Sodium
EPA 007
Zinc
EPA 200.7
Acidity (Soil Fertility)
NCDXAgmnoffk Division
Base Saturation
NCOA-Agronomic Division
Cation Exchange Capacity
NCDA-Agronomic Division
Exchangeable Sodium Percentage
NCDA-Agranomic Division
H I urnic I Matter 11 - -
NC 11 DA Ag ronomic Division
Total Solids (%)
SM 2540 B
Total Phosphorus
SM 4500 P F
pH
SW M Method 9045D
Result est mated Analyzed out of 15
minutes hold time,
465 mglkg
1110412022
<0.730 mg/kg
1110412022
119 mg/kg
11/04/2022
0.918mg/kg
11104/2022
<36,6 mg/kg
11/0412022
<36,5 mg/kg
1110412022
3.42 mg/kg
1110412022
<0.01 meq/100g
11101/2022
99.7%
11/16/2022
3.40meq/100g
11/16/2022
4.70%
1111612022
2.47%
11 /1 W2022
89.8 %
10/26/2022
80.6 mg/kg
1110212022
6.62 units
11/0112022
Report2022-21248 Page 9 of 11

771
B'"11,777. MELT-el r"I -01 ad, Ulm, r
5�v
nchniflWay, K alaiwx n, Ni 28405 910,392,022,3Lab 9103914424 Fax
6602 Vh�
7- B('-)WSerk),,%rr 14md, Niaritem NC r7954 2-57,4"1'5702 i,ab/Fax
k - ingtor 255-A W) in flighway, Jac kson fllel, NC 28540 910,3 4 7-51 8 4 3 La b a X
ANALY-nCAL & CONSULI"ING CHEMISTS
Pender County Utility Operations
Date of Report: Nov 16, 2022
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention:
Report #. 2022-21248
Project ID: Maple Hill Sprayfield
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-52120 Site: Zone 10
10/2412022 12:48 PM Solid/Sludge Chris Pickett
Test Method
Soil Fertility
Calcium
Crki4uu;
Copper
EPA 200 7
Magnesium
EPA 2007
Manganese
EPA 2007
Potassium
EPA 200 7
Sodium
EPA 2007
Zinc
EPA 200 7
Acidity (Soil Fertility)
NCOA-Agronomic Dms on
Base Saturation
NCDA-Agronomic Division
Cation Exchange Capacity
NCDA-Agronomic Division
Exchangeable Sodium Percentage
NCDA-Agronomic Division
Hu m'ic- Matter
NCIDA-Agrononnic Division
Total Solids (11G)
SM 2540 8
Total Phosphorus
SM 4500 P F
pH
Sw 846 Method 9045D
Result estimated Analyzed out of 15
minutes hold time,
Results Date Analyzed
221 mg/kg
11/04/2022
<0.780mglkg
11/04/2022
66. 9 mg/kg
11/04/2022
<0.780 mg/kg
11104/2022
<39.0 mg/kg
11104/2022
<39.0 mg/kg
11/04/2022
2.06 mg/kg
11104/2022
3 meq/1 OOg
11/0112022
41,0%
11116/2022
4.30 meq/1 OOg
1111612022
4.00%
11/1612022
6.28%
11/10/2022
80.0%
10/26/2022
27.7 mg/kg
11102/2022
5.16units
11101/2022
Report# 2022-24248 Page lOofil

T� A ";R 0
Kit -, nea 1 1 i e r ra i t
A-L
I'D 6042 VVI �r, d j, I I 'K zy, VV; 1 J to 1 840-, 91-392,0223 Lab 91039144-24 Fa,,
'�-5702 La' ' F
710 bowsertnwr Road, i �P, NC 279 4 � Z147- 4X
7., , b
03 Jacksoinville, NNC 28540 9E 5842, Le...TeX
55-A VV gton Hjghwa 4 34
ANALYTICAL & CONSUMNG CHEMISTS
Pender County Utility Operations
Post Office Box 995
Burgaw NC 28425
Attention:
Lab ID Sample ID:
22-52121 Site: Zone I I
Date of Report: Nov 16, 2022
Customer PO #:
Customer ID: 08100095
Report #: 2022-21248
Project ID.- Maple Hit[ Sprayfield
Collect Date/Time Matrix Sampled by
10124/2022 12:53 PM Solid/Sludge Chris Pickett
Test Method Results Date Analyzed
Soil Fertility
Calcium
Copper
EPA 200 7
Magnesium
EPA 2007
Manganese
EPA 2007
Potassium
EPA 200 7
Sodium
EPA 200 7
Zinc
EPA 200 7
Acidity (Soil Fertility)
NCDA-Agronomic Division
Base Saturation
NCDA-Agmnoinic DMsion
Cation Exchange Capacity
NCDA-Agronomic Division
Exchangeable Sodium Percentage
NGDA-Agronomic Division
H 11 umic Matter
NWA-Agrandmid Division'
Total Solids M
SM 2540 B
Total Phosphorus
SM 4500 P F
PH
SW 846 Method 9045D
Result estimated. Analyzed out of 15
minutes hold time,
Comment: Results reported on a dry weight basis.
Reviewed by:
1390 mg/kg
11/04/2022
2,08 mg/kg
11/04/2022
400 mg/kg
11/04/2022
2.61 mg/kg
11/04/2022
<47.5mg/kg
11/04/2022
214 mg/kg
11104/2022
12,0 mg/kg
11/04/2022
5 meq/1 OOg
11/0112022
68.8%
11/1612022
15.0meq/100g
11116/2022
6,20%
11/16/2022
16.1010
11 /1012022
72.8%
10/26/2022
77.2 mg/kg
11102/2022
5.50units
11/01/2022
Report# 2022-2'1248 Page 11 alf 11

Environmental Chemist, Ills., Wilmington, NIC Lab #94
Sample Receipt Cheddist
Da t e Report Number-
6602 WindrrifflWay
VVilmington, NC 28405
910392.0223
P1kfciAPt of sampie: CC HEK4 Pickup m Client Delivery U 1UP S [,I Fedrx D
-7
0 1 i Werf' COSTOdy seals present on the cooler' YES 1_3 NO I I
00he" 1-3
K , \J� 'LI , f custody seals were present, were they intartfuribrokelo
ri-inal temperature upon receipt_!L -C Corrected temperature Lip
How temperature taken: 0 Temperature Biank Against Battles
IR Gun 10:PhaniasTraceabie S/N 1 9251 165. JR Gun Correction Factor 'C: 0,0
'0
Lq YES 0 IN 0 3, If temperaNure of cooler, exceeded VC, was ProjeCt V1gr,/QA notified?
YES 0 No
s (refinquished/received) follciwad?
NTE S� E N 0 Were sample Vs listed
'DES
0
LAI' ES 0 NO 6 Were samples Us listed on sample containers?
11 -0
YES 0 NO 7. VVere collection date and time listed on the COC?
v
YES 10 NO err, tests to be performed listed or., the COU ,
IN
a YES 10 NO 9, Did sa III pies arrive In proper Carl taine r5 for east; test?
YLS I ®r (40 11 Did saniples arrive in good con&ticm for each
_11 Was adequate sample volume available
OT YES 1[3 NO 12. "V%cre &,,,imp�esreceived Within proper holding time fharrequesi­e;­J test -
0 L-1 VVercacid Preserve(] samples received at YES
'd pl­!,�12?
ES e_ q/am e sarrtpies received a,
15 �,'trestill 3desjFiir)lest-eceivedatapH>9?
YES U N 0 16,�, Were iJH3!TKN/Pheno1 received at a chlorine residual of <5 oj/i
idual ctt "5
5, YES C1 NO 17. Were Stflfide/Cyanide rece'Wed at a chlori
NO 18, Were orthophosphate samples fiftered in the fil' WiNn 15 rnitiutf�,0
TOC/kVatWes are PH chrd<ed iat time 0 analysis and retarder an the benchsheel,
cterina sjrripies are Gin dKed V CU I uritic-, at Urne of analysis an recorded or, the berich, Sheet
;Sample Preservation,., (,NlUst be, completed for anq samples incorrectiy preserved or with headspace)
Sample's)
were received incorrectfy preserved and were adjusted accordingly
by adding (circle one): H2SD, HNO3 HC1 NaOH
,rne orpreservation, more than one preservative is needed, notare in corninents below
rout e: Notify customer s?? ,tce imir,_,diatcs�y fit inzorrectly QresErved sarnpips Obtain a new 5amola of
iotifk, the stae fib pf d;rar�_I_d to Fte;l'rzed b'ythn rust mer, who was
olatiles Sainplefs
were received with h
DOC. QA.002 Rev I
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OFFICE: 910-392-0223 IFAIX 910-392-44 4
Anatpul Consulbog C herrirsis DEMR: nwo cER-riFICAMN # 94 NCONHS: DLS CERWICATION ft 37? 3 irslrs ra is sisrr rri�l h irsa€p si
COLLECTION AND CHAJN OF CUSTODY
,t: Ponder County 1J 111 Sri lci OJ T l i14� . Mapl Hill �' l3nrari t td3 i� i°its:
REPORT O:
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HONEIF ; a
Ancg
TO:
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-
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PRESERVATION �{
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ANALYSIS REQUESTED ED "
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ENVIRONMENTAL CHEMISTS,
INC 6602 Windmill Way !!!ruin ton, NIC 28406
OFFICE., 10-392-0223 FAX [phone]
Annly#tcal & Consulting Chemists
NCDEN11- DWO CERWICATIO ~3 # 94 NCEPI-IRS; US CERWIC 110N 0 37720 lnf rrvlronmentatcliamists.carat
COLLECTION AND CHAIN OF CUSTODY
tans
Mierlt: PGndGr CtoUfn Will 0 orations PROJECT NAME: Maple Hill VWMWT P S rma 'aid, REPORT NO;
CONTACT NAME,
PO Nc): s
COPY TO,
emallt
«faa l
SAMPLE TYM I Influent, vontg Well, ST = Stream, SO Sall, SL Sludge, Other;
Collection
PRESERVATION
Sit 5f a IdentificationC
zANALYSIS
REQUESTED
Date
Time�� �$ �, � 0� � �
d 0
k
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{y}g
pp
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rsw
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+'y� �g g
i r&a[0.sfor p
�g�y q yy ryg� �} �q {�.gypgq� ppypq
C44YfIlip quishod £5 n 6dFNA'!Sg $ iS#FS8
�g �µgy� �( �p �gry gq, ¢ �yy _
r !"Local ed B Daitemme ^.
Temperature whA 3x
Accepted:
ccept& • _ ej t� .
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Delivered
lvDate.
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Comments:
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