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WQ0001077_Monitoring - 11-2022_20221214
Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * November Report Information Type * GW-59 WQ0001077 Innospec Active Chemicals Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* WQ0001077 2022-11 GWMW 3.25MB report.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). allen.robey@innospecinc.com Allen Robey Reviewer: Gerald, Wanda 12/14/2022 This will be filled in automatically Is the project number correct?* WQ0001077 Is the monitoring report accepted?* Yes No Regional Office* Mooresville Reviewer: _anonymous Review Date: 1/5/2023 GW-59A COMPLUNCE REPORT FORM Permft #Lq-4M-0j-7 (Submit one each monitoringperiod with GIV-59forms.) —f-- r .............. Enter date monitoring results were due. ( I —monitoring report (GIN-59 and GIN-59A) . . . ............ — YES be submitted after the established due date? . . . . . ............ . ..... ......... . . ....... . .... . ..... . ..... Was any required information missing on the GW-59 report forms? YE11 S . . . . .................... -- — ----- . .............. . ---- IF the answer to question I or 2 is 'YFS", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. V ..... . .................. .... .. .. .. .. .. .. ...... . .................. .. .. .. .. ....... .. ... . 1 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES �Q identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance. 4 Are any monitored constituents equal to or above the established standards? YES ISO .......................... . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. . . .......... ......... . ........... .. .. .. .. .. .. .. .. ............... .. .. ........................ --------- I If the answer to question 4 is to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: . . . . ................. ... . .. .. . . . . . ............. .. .. .. .. .. . ------ For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If —the answer to question 5' is —WO, ,slop to o section ",," 8 ................ -------- If the answer to question 5 is "YES". list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). ..................... . . ............ . ................ 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO . ......... ...... . ... .... .... ..... ....... . . ....... ................................................. . If the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office, 7 1 s the �-eirri fit—te il m`pi e' me n -"— "" . ........ . . . . . . . . . . . . .................................................................. ting previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO". contact the Regional Of within 90 ftfsZ an evaluation max b rectuired to determine the impact the waste disgosal system is having at the review and co1pplian boundaries surroundinq this facill!y. Failure to do so may subject the permittee to a Notice of Violationt fines, and/or penalties. 7 -iiii ----- - fh�"peii co rn p`ie" t I n g iWis", ii� monitoring report should sign below and submit - -------- form with OW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge,that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the, best of my knowledge. G�iz�-- 6dAgent)Date ge i'naturoemi&ermm .............................. - — ----- ...... . . . .. .. .. .. .. .. .. .......... . ......................... . GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY NDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM ITY INFORMATION Pieese-rani uieanyor Type Name: Innospec Performance Chemicals Name (ifdifferent): Address: 500 Hinkle Lane iry, NC 28144 County Rowan act Person. Clay White Telephone#: (704) 639-7920 Location/Site Name: Long Ferry Road No. of wells to be sampled. 3 °RMIT Number: Expiration Date: 6/30/2027 m-Discharge WQ0001077 UIC 'DES Other (PE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation- ED Rotary Distributor ❑ Land Application of Sludge ❑i Water Source Heat Pump❑ Other: SAMNLINU INFUKMA I IUN. =if WELL WELL ID NUMBER (from Permit). V'= Date sample collected: 11/8/2022 RELDANALYS€S: 1WAS Well Depth: 30 ft. Well Diameter: 2 in pH 00400: 5.77 S units Temp. 00010: 17.3 1C IDRY at Depth to Water Level 8254e: 20 ft. below measuring point Screened Interval: 30 ft, to 15 fl, Spec. Cond. 00094 µMhos €time of Measuring Point is 2 ft. above land surface relative M.P. E€evation: Odor 00085: NIL samplin< check Volume of water pumped/bailed before samplings 5 gallons Appearance Clear ihere;� Date sample analyzed: 11/10-18/2022 Laboratory Name: Statesville Analytical; Meritech PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 /L Pb - Lead 01051 Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 rng/L Zn - Zinc 01092 Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 _ mg/L No teU MPN method for hhl t bitl I Certification No. 440; 165 ug/L mgJL { . Use i g y ur same es> Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): liissolved Solids:Total 70300 143 mg/L Al - Aluminum o1105 mg/L MBAS = <0.1 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC oo680 <1.0 mg/L Ca - Calcium 00916 mg/L Chloride oos4o mg/L Cd - Cadmium 01027 ug/L Arsenic o1002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) r-]No (0) 1pecific Conductance 00095 184 µMhos K - Potassium o0937 mg/L VOC 7873 method # EPA 8260 Total Ammonia 00610 mg/L twig - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 1 mg/L Ni - Nickel olo67 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: _ mg/L VOC Removal% Allen Robey, SHE Director, NA _ A Permittee (or Authorized Anent) Name and Title - Please print or type Signature of Permtittee for AutWzed Anent) {Date GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print clearly or Type Facility Name: Innospec Performance Chemicals Permit Name (if different): Facility Address: 500 Hinkle Lane Salsbury, NC 28144 County Rowan act Person: Clay White Telephone#: (704) 639-7920 Location/Site Name: Long Ferry Road No. of wells to be sampled: 3 (from Permit) Non -Discharge WQ0001077 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon F] Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MV Date sample collected: 11/8/2022 FIELD ANALYSES: WAS Well Depth: 38 ft Well Diameter. 2 in pH 00400 5.24 units Temp. 00010; 16.4 �c DRY at Depth to Water Level 82546: 33 ft. below measuring point Screened Interval: 38 ft. to 18 ft Spec. Cond. 00094; µMhos time of Measuring Point is 2 ft. above band surface Relative M.P. Elevation: i4 Odor 000m: NIL sampling, Volume of water pumped/bailed before sampling: 3" gallons Appearance Turbid orange &- Samples for metals were collected unfiltered: F 1 YES ❑ NO and field acidified-. f-1 YES 1-1 NO hero Date sample analyzed: 11/10-18/2022 Laboratory Name: Statesville Analytical; Meritech Certification No. 440; 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead oimii ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 m9 /L C-diform: MF Total 31504 J100mL Phosphorus: Total as P 00665 mg/L {Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units).: Dissolved Solids:Total 70300 _ 52 mg/L Al - Aluminum 01105 mg/L MBAS = <0.1 m /L PH (Lab) 00403 units Ba - Barium 01007 ug/L TOC omm <5.0 mg/L Ca - Calcium oog16 mg/L Chloride oog4o mg/L Cd - Cadmium 01027 _ ug/L Arsenic oloo2 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? F xl Yes (1) 0 No Specific Conductance 00095 1 8 wlhir5 K - Potassium 00937 mg/L VOC 7873 method # EPA 8260 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Totao Mn - Manganese 01055 ug/L , method # TKN as N 00625 gnu Ni - Nickel oiw ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Allen Robey, SHE Director, NA Permtttee dor Authorized Agent) Nance and Title - Please print or type GW-59 Rev. 06-07-2018 Agent) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM JFACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 0/30/2027 Facility Name: Innospec Performance Chemicals Non -Discharge WQ0001077 UIC Permit Name (if different): NPDES Other Facility Address: 500 Hinkle Lame TYPE OF PITTE -OPERATION NG ITfREO Salsibury, NC 28144 County_ Rowan ❑ Lagoon p Remediation: Infiltration Gallery (ciy> star®)(zip) X Spray Field 0 Remediation: Contact Person: Clay White Telephone#. (704) 639-7920 F-1 Rotary Distributor F-1 Land Applicabon of Sludge Well Location/Site Name: Long Ferry Road No. of wells to be sampled: 3 © Water Source Heat Pump 0 Other. (from Permit) - -- WELL ID NUMBER (from Permit): NARN -8, Date sample collected: 11/8/2022 FIELD ANALYSES: WAS VVr_LL Well Depth: 40 ft. Well Diameter: 2 in. pH 00400: 5.42 units Temp. 15.5 on DRY at Depth to Water Level 82546: 22 ft. below measuring point Screened Interval: 40 ft. to _20 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 1 3 ft. above land surface Relative M.P. Elevation: ft,i Odor 00065: NIL sampling, Volume of water pumped/bailed before sampling: 9 gallons Appearance Yellow tint check Samples for metals were collected unfiltered: © YES © NO and field acidified: ❑ YES ❑ NO here r LABORATORY INFORMATION Date sample analyzed-- 11/10-1812022 Laboratory Name: Statesville Analytical; Meritech Certification No. 440; 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc olow mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 m /L 9 Other (Specify Compounds (p fy pounds and Concentration Units): issolved SolidsiTotal 70300 59 mg/L Al -Aluminum 01105 mg/L MBAS = <0.1 mg/L pH (Lab) 00403 units Ba - Barium 011007 ug/L TOC ooseo 1.06 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium; Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (1) ❑ No (0) pecific Conductance 00095 49 µMhos K - Potassium 00937 mg/L VOC 787a , method # EPA 8260 Total Ammonia ooseo mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nltrogen; NH3as R Ammonia Nitrogen, Total Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L ,method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Allen Robey, SHE Director, NA Permittee (or Authorized Agent) dame and Tale - Please print or type GW-59 Rev. 06-07-2018 Analytical Results Innospec Performance Chemicals US Company 500 Hinkle Lane Salisbury, NC 28144 "AT T P! , S V III IL �; , E INf Receive Date: Reported: For: Comments: Sample Number 11/09/2022 11 /29/2022 Monitoring Wells Parameter Sample ID Result Unit Method Analyzed Analyst 221109-13-01 Conductivity MW #6 184 umhos/cm SM2510B-2011 11/11/2022 MD 221109-13-01 MBAS MW #6 <0.1 mg/L SM5540C-2011 11/10/2022 MD 221109-13-01 TOC MW #6 <1.0 mg/L SM5310B 11/18/2022 MT 221109-13-01 Total Dissolved MW #6 143 mg/L SM 2540 C 18th Edition 11/10/2022 MD Solids 221109-13-01 VOC MW #6 See Attached SM6230D 11/16/2022 MT 221109-13-02 Conductivity MW #7 168 umhos/cm SM2510B-2011 11/11/2022 MD 221109-13-02 MBAS MW #7 <0.1 mg/L SM5540C-2011 11/10/2022 MD 221109-13-02 TOC MW #7 <5.0 mg/L SM5310B 11/18/2022 MT 221109-13-02 Total Dissolved MW #7 52 mg/L SM 2540 C 18th Edition 11/10/2022 MD Solids 221109-13-02 VOC MW #7 See Attached SM6230D 11/16/2022 MT 221109-13-03 Conductivity MW #8 49 umhos/cm SM2510B-2011 11/11/2022 MD 221109-13-03 MBAS MW #8 <0.1 mg/L SM5540C-2011 11/10/2022 MD 221109-13-03 TOC MW #8 1.06 mg/L SM5310B 11/18/2022 MT 221109-13-03 Total Dissolved MW #8 59 mg/L SM 2540 C 18th Edition 11/10/2022 MD Solids 221109-13-03 VOC MW #8 See Attached SM6230D 11/16/2022 MT Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 9 Condition of Receipt Sample Number 221109-13-01 Temp on Arrival: 1.0 pH on Arrival: <2 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Conductivity Received on Ice Parameter Schedule: MBAS Received on Ice Parameter Schedule: VOC Ascorbic Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Phosphoric Acid Received on Ice Chemicals in containers, lab Sample Number 221109-13-02 Temp on Arrival: 1.0 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Conductivity Received on Ice Parameter Schedule: MBAS Received on Ice Parameter Schedule: VOC Ascorbic Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Phosphoric Acid Received on Ice Chemicals in containers, lab Sample Number 221109-13-03 Temp on Arrival: 1.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 9 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Conductivity Received on Ice Parameter Schedule: MBAS Received on Ice Parameter Schedule: VOC Ascorbic Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Phosphoric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 9 O 110 x N N W N N (D G (D z n N W ol W • J O CD � CD � A J O N 1 41 10 J — - F XK o R_ , - - - C shy ec" t _ _d 1045 � i t s 3 S ' -ram,. P er %,� f .. _ , - ; . D. _ r a.- #.,_€�.,. S p _ by } byRA nqwwd by�z d Mown hy,�{ Ime end am pm Done Y OWN- COG g� _ end m Contact: C. Little Report Date: 11/28/2022 Client: Statesville Analytical 122 Court St Project: Innospec Statesville, NC 28677 Date Sample Rcvd: 11/11/2022 Meritech Work Order# 11112220 Sample: 221109-13-01 Grab 11/8/2022 Parameter TOC EPA 8260 Results <1.0 mg/L Attached Analysis Date 11/18/2022 11/16/2022 Reporting Limit 1.0 mg/L Metbod SM 5310C EPA 8260 Meritech Work Order# 11112221 Sample: 221109-1.3-02 Grab 11/8/2022 Parameter Results Analysis Date Reporting Limit Method TOC <5.00 mg/L 11/18/2022 5.00 mg/L SM 5310C EPA 8260 Attached 11/16/2022 EPA 8260 Meritech Work Order 4 11112222 Sample: 221109-13-03 Grab 11/8/2022 Parameter Results Analysis Date Reporting Limit Method TOC 1,06 mg/L 11/18/2022 1.0 mg/L SM 5310C EPA 8260 Attached 11/16/2022 EPA 8260 I hereby certify that I have reviewed and approve these data. �z Laboratory Represedraftive tel.(336)342-4748 fax.(336)342-1522 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 9 MERITECH, INC. Environmental Laboratories Laboratory Certification #165 f Client- Statesville Analytical Meritech 1D4: 11112220 Project: Innospec Analysis- 11/16/22 Client Sample ID: 221109-13-01 Analyst: VWV Sample Collection: 11/08/22 Dilution Factor: I Report Date: 11/22/22 SW-846-8260 VOLATILE ORGANICS -Water Acetone < 5.00 ug/L cis- 1,3-Dichloropropene < 0.500 ug/L Benzene < 0,500 ug/L trans- 1,3-Dichloropropene < 0.500 ug/L Broniobenzene < 0.500 ug/L Ethanol < 50.0 ug/L Brornodichloromethane < 0.500 ug/l, Ethyl benzene < 0.500 ug/L Brornochlorornethane < 0.500 u,-/L Hexachlorobutadiene < 0.500 Ug/L Brornoform < 0.500 ug/1. 2-Hexanone < 1.00 ug/L Brornornethane < 0.500 ug/L Isopropyl benzene < MOO ug/L 2-Butanone (MEK) < 5.00 ug/L p-Isopropyltoluene < MOO ug/L n-BL)tylberizene < 0.500 ug/L Methylene chloride < 0,500 ug/L sec-BUtylbenzene < 0,500 ug[L Methly Isobutyl Ketone (MIBK) < 0.500 ug/L tert-B utyl benzene < 0,500 ug/L Naphthalene < 0,500 ug/L Carbon Tetrachloride < MOO ug/L n-Propylbenzene < 0,500 ug/L Ch'orobenzene < 0.500 ugiL Styrene < MOO ug/L Chloroethane < 0.500 ug/L 1, 1, 1,2-Tetrachloroethane < 0.500 ug/L Chlorofon-n < 0,500 ug/L 1, 1,2,2-'retrachloroethane < 0.500 ug/L Chlorornethane < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/L 2-Clilorotoluene < 0.500 ug/L, Toluene - < 0.500 ug/L 4-ClilorotolueTIC < MOO ug/L III .. I -Trichloroethane < 0.500 ug/L Dibrorno ch lororn ethane < 0.500 ug/L 1, 1,2-Tiichloroethane < 0.500 ug/l, 1,2-Dibronio-3-chloropropane < 0.500 ug/L 'rrichloroethene (TCE) < 0.500 ug/L 1,2-Dibronioethane (FDB) < 0.500 ug/L, 1,2,3-Trichlorobenzene < 0.500 ug/L Dibrornornethane < MOO ugiL 1,2,4-71'richlorobenzene < 0,500 ug/L DichlorodiflUorornethane <, 0.500 ug/L 1,2,3-Trichloropropane < 0.500 Ug/L 1, 1 -Dichloroethane < 0.500 ug/L Trichlorofluoromethane < 0.500 tag/L. 12-Dichloroethane < 0.500 ug/L 1,2,4-Triniethylbenzene < 0,500 ug/L 1,4-Dichlorobenzene < 0.500 ug/L 1,3,5-Trirnethylbenzene < MOO ug/L 1,2-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 Lig/L 1,3-Dichloroberizene < 0.500 ug/L Vinyl chloride < MOO ug/L 1, 1 -Dichloroethene < 0.500 ug/L m/p-Xylenes < 1,00 ug/L cis- 1,2-Dichloroethene < MOO ug/L o-Xylene < MOO Lig/L trans- 1,2-Dichloroethene < MOO ug/L 1,2-Dichloropropane < 0,500 ug/L Additional Compounds 1,3-Dichloropropane < 0,500 Ug/1' Methyl-tert-butyl ether (NITBE) < 0.500 ug4, 2,2-Dieliloropropane < MOO ug/L Isopropyl ether (IPE) < MOO ug/L 1, 1 -Dichloropropene < 0.500 ug/L 1,2-Dicliloropropene < MOO Ug/L I hereby certify that I have reviewed and approve these data. Laboratory -Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1622 Fax PO Box 228 9 Statesville, NC 28687 9 704/872/4697 Page 6 of 9 MERITECH, INC. I't Environmental Laboratories v l Laboratory Certification ##165 Y 9f�1 Client: Statesville Analytical Meritech ID4.- 11112221 Project: Innospec Analysis: 11/16/22 Client Sample ID: 2211.09-13-02 Analyst: VWV Sample Collection: 11/08/22 Dilution Factor. I Report Date: 1 1/22/22 S'W-846-8260 VOLATILE ORGANICS -Water Acetone 5.58 ug/L cis-1,3-Dichloropropene <0.500 ug/L Benzene < 0.500 ug/L. trans-1,3-Dichloropropene < 0.500 ug/L Bromobenzene < 0.500 ug/L Ethanol < 50.0 ug/L, Bromodichloromethane < MOO ug/L Ethyl benzene < MOO ug/L Bromochloromethane < 0.500 ug/l. flexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < 5.00 ug/L p-Isopropyltoluene < 0.500 ug/L n-Butylbenzene < 0.500 ug/L ]Methylene chloride < 0.500 ug/L sec -Butyl benzene < 0.500 ug/l.. Methly Isobutyl Ketone (MIRK) < 0.500 ug/L tert-Butylbenzene < 0.500 ug/L Naphthalene < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L rr-Propylbenzene < 0.500 ug/L Chlorobenzene < 0.500 ug/L Styrene < 0.500 ug/L Chloroethane < 0.500 ug/L 1,1,1,2-Tetrachloroethane < 0.500 ug/'I, Chloroform < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L Chloromethane < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/1. 2-Chlorotoluene <0.500 ug/L Toluene <0,500 ug/L 4-Chlorotoluene <MOO ug/L 1, 1, 1 -Trichloroethane <0.500 ug/L Dibromochloromethane < 0.500 ug/L 1,1,2-Trichl,oroethane < 0.500 ug/L 1,2-Dibromo-3-chloropropane < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L 1,2-Dibrornoethane (EDB) < 0.500 ug/L 1,2,3-Trichlorobenzene < 0.500 ug/L Dibromomethane < 0.500 ug/L. 1„2,4-Trichlorobenzene < MOO ug/L Dichlorodifluoromethane <0.500 ug/L 1,2,3-Trichloropropane <0.500 ug/L 1,1-Dich.loroetltane <MOO ug/L Trichlorofluorometliane <0.500 ug/L 1,2-Dichloroethane <0.500 ug/L 1,2,4-Trimethylbenzene <0.500 ug/L 1,4-Dichlorobenzene <0.500 ug/L 1,3,5-Trim ethyl benzene <0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1,3-Dichlorobenzene < MOO ug/L Vinyl chloride < 0.500 ug/L 1,I-Dichloroethene <0.500 UeL rn/p-Xylenes < 1.00 ug/L cis-1,2-Dichloroethene <0.500 trgCL a-:X.ylene <0.500 ug/L trans-1,2-Dichloroethene <0.500 ug/l., 1,2-Dichloropropane < 0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ugiL 2,2-Dichloropropane < MOO ug/L Isopropyl ether ('IPE) < 0.500 ug/L. I,1-Dichloropropene <0..500 ug/L 1,2-Dichloropropene <MOO ug/l, i hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 9 MERITECH, INC. P, Environmental Laboratories Laboratory Certification #165 Client: Statesville Analytical Meritech ID#: 11112222 Project: Innospec Analysis: 11/16/22 Client Sample ID: 221109-13-03 Analyst: VWV Sample Collection: 11/08/22 Dilution Factor: I Report Date: 11/22/22 SW-846-8260 VOLATILE ORGANICS - Water Acetone 7.39 ug/L cis- 1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L, trans- 1,3-Dichloropropene < 0.500 ug/L Bromobenzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichlorornethane < 0.500 Ug(L Ethyl benzene < 0,500 ug/L Bronioebloromethane < 0.500 Ug/l, Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromornethane < 0.500 ug1l, lsopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < MO ug/L p4sopropyltoluene < 0.500 ug/t, n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 Lig/L see -Butyl benzene < 0.500 ug/L Methly lsobutyl Ketone (MIBK) < 0.500 ug/L tert-Butylbenzene < 0.500 ug/L Naphthalene < 0.500 ug/L Carbon Tetrachloride < MOO ug/L n-Propyl benzene < M00 ug/L Chlorobenzene < 0.500 ug/L Styrene we 0.500 ug/L Chloroethane < 0.500 ug/L 1, 1, 1,2-Tetrachloroethane < 0.500 ug/L Chlorofonn < 0.500 ug/L 1, 1,2,2-Tetrachloroethane < M00 ug/L Chloromethane < MOO ug/L Tetrachloroethene (PCE) < 0.500 ug/L 2-Chlorotoluene < 0.500 ug/L. Toluene < 0,500 ug/l, 4-Chlorotoluene < 0.500 ug/L 1, 1, 1 -Trichloroethane < M00 ug/L Dibrornochloroniethane < 0.500 ug/L 1, 1,2-Trichloroethane < M00 ug/L 1,2-Dibrorno-3 -chi oropropane < 0,500 ugCL Trichloroethene (TCE) < 0.500 ug/L 1,2-Dibrornoethane (EDB) < 0.500 Ug/l, 1,2,3-Trichlorobenzene < 0.500 ug/L Dibrornornethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L Dichlarodifluoromethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 uWL.. ],I-Dichloroethane < 0.500 ug/L Trichlorofluorometfiane < 0.500 ug/L I 2-Dichloroethane < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 qo.' 1,4-Dichlorobenzene < 0.500 ug/L 1,3,5-Trimethylbenzene < 0,500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1,3-Dichlorobenzene < 0,500 ug/L Vinyl chloride < 0.500 ug/L 1, 1 -Dichloroethene < 0.500 ug/L rn/p-Xylenes < 1,00 ug/L cis- 1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,2-Dichloroethene < 0.500 ug/L 1,2-Dichloropi-opane < 0.500 ug/L Additional Compounds 1,3-Dieliloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 2,2-Dichloropropane < MOO ug/l, Isopropyl ether (lPE) < 0.500 ugil. 1, 1 -Dichloropropene < 0.500 ug/L 1,2-Dichloropropene < 0.500 ug/L I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco, Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax PO Box 228 9 Statesville, NC 28687 9 704/872/4697 Page 8 of 9 �t8 Chain of Custody Record (COC) NPDES#: MERITECH, INC. Statesville Analytical "hone: PO Box 228 -ax: -> ENVIRONMENTAL LABORATORIES 122 Court S email: 642 Tamca Rd, Phone: 336-342-4748 Statesville r N7 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@ meritechlabs,com Attention: urn Around Time* 1 ¢ Ii It 1 � S. i 1 *RUSH work needs prior approval, How would you Ilk e report sent? ar A I circle all that a ly: Email (preferr I, Fax, Mail Std 10 s) 3 - 5 Da s 24 48 Hr-s Sampling Dates & Times Person Taking Sample (Sign/Print): Lab Use Only Sample Location and/or 10 # Start End comp? # of On ice? pH OK? Date Time Date Time Grab? Cont.Test(s)Requiredyes 1 No Cl OK? iJG 10 CA-1 ► } "0 E i Zoe K 4- �` 1 60 Temperature Upon Receipt: Method f *** Decfilorinatian €0.5 ppm} of AmmoniaCyanide, Phenol and TKN samples must be lane in thefield prior to preservation. Shipment: Comments: � ��� 0. �L Compositor # UPS ` Jug # Fed Ex Are terse re ult fu regal purposes? Yeses No Report results in mgji mg/kg ugjt Hand Delivery Relinquished t : Time: f /r)A Received b : /2ki y 11 t o j , 1 Time: � . l t Other Relinquished by: I a Time: rl Received by Date: Time: Relinquished by: Date: Time: Re_ ,ved by' D -_ rn �t M N p 00 N o a r- r- 00 00 N U Z ai N V) 00 N N X 0 m O n