Loading...
HomeMy WebLinkAboutWQ0005603_Regional Office Physical File Scan Up To 12/7/2022ounty% MCDOWELL River.Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Location ID: 1P059WQ0005603MWll .i 4� Office VISitID Loc. Descr.: COATS AMERICAN MW-11 Sample ID: AB34864 PO Number# 8G1208 Date Received: 08/28/2008 Time Received: 07:45 Labworks LoginlD HPARKER Date Re o 'rted: I i epb Generated: 9/17/08 09/17/2008 Gib �lga� Collect Date: 01812612008 I Collect Time:: 10:12 I Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL 132-Counts from all filters were zero. NE -No established PQL 133- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. 65-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No CDC Yes/No Location ID: 1P059WQ0005603MWll o� Wkrg�, 0� C_ � y C 'C SE ® 9 2600 Asheville Regional Office g Rquifer PrQtecticn Visitil Loc. Descr.: COATS AMERICAN MW-11 Collect Date: 08/26/2008 1 Collect Time:: 10:12 Sample Qualifiers and Comments Sample ID: AB34809 PO Number# ARO Date Received: 08/26/2008 Time Received: 14:15 Labworks LoginlD KJIMISON Date Reported: 9/4/08 Report Generated: 09/04/2008 Sample Depth Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two, or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated NE -No established PQL B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. B5-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound NI -The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 Sample ID 1 P059W00005603 MW11 rtl COATSAMERICAN MW-11 .VC DWQ La6oratory Section Results Collect Date: Collect Time:: 08/26/2008 10:12 M1141yLe rrvdme ruL Result Qualifier Units Analyst/Date Approved By /Date Method Reference 8/28/08 8/28/08 MIC TOC in liquid 1 2.0 4.4 mg/L BSWANSON MOVERMAN Method Reference APHA531013-20th 8/28/08 9/8/08 rr� i Ion Chromatography TITLE_ mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/17/08 . Chloride 1.0 5.4 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9117108 Fluoride 0.4 0.4 U mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/17/08 Sulfate 2.0 33 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/17/08 NUT Phosphorus total as P in liquid Method Reference LaC10-115-01-lEF 0.02 0.20 mg/L as P MAJAYI CGREEN 8/29/08 913/08 MET 7429-90-5 AI by ICP 50 460 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9111/08 7440-38-2 As by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-38-3 BabyICP 10 100 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-70-2 Ca by ICP 0.10 18 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-47-3 Cr by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-50-8 Cu by ICPMS 2.0 11 ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7439-95-4 Mg by ICP 0.10 5.2 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11108 7439-96-5 Mn by ICP 10 890 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9111/08 7440-23-4 Na by ICP 0.10 84 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 3 1 P059 W 00005603MWl l Oescr.: COATS AMERICAN MW-11 Visit ID NC DWQ Laboratory Section Results Sample ID Collect Date: Collect Time:: AB34864 08/26/2008 10:12 "• ""' -.'YLC 1\4111C rug Result Qualifier Units Analyst/Date Approved By /Date 7440-02-0 Ni by ICPMS 10 10 U uglL DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7439-92-1 Pb by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3108 9/11/08 7782-49-2 Se by ICPMS - 5.0 5.0 U uglL DSTANLEY ESTAFFORD ' Method Reference EPA200.8 9/3/08 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 3 jVC (DWQQ Laboratory Section Results Sample ID AB34809 1P059Wd0005603MW11 Collect Date: 08/26/2008 Descr.: COATS AMERICAN MW-11 Collect Time:: 10:12 Visit ID I..AJ rf Analyze name FUL Kesun 4ualitier Units Analyst/Date Approved By /Date Sample temperature at receipt by lab 2.1 °C KJIMISON MMATHIS Method Reference 8/26/08 8/28/08 Total Dissolved Solids In liquid 12 280 mg/L KJIMISON CGREEN Method Reference APHA2540C-18TH 8/28/08 9/4/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM -ocation code_ I VQII71T WO 400,5"1 3 `%Yj W- 11 SAMPLE TYPE SAMPLE PRIORITY Counater Routine Quad No Serial No. ❑ Soil ❑ Emergency Lat. 3S 4-7 t Z, q Long. 9 ;? ' 01 / %; ` ❑ Other ❑ Chain of Custody Report To: ARO FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shou ipped by: Bus, rier Hand Del , Other: Purpose: Collector(s): jt&Ileytnn Date G d Time 10 : (Z Bas tin , Complair FIELD ANALYSES Owner pH 40o Spec. Cond.94 at 25°C Location or Site i7 t Temp.lo eC Odor Description of sampling point_ Appearance Sampling Method Field Analysis By: Remarks_ S�It>L Soma LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom] Coliform: MF Total 31604 /100m] OC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 cU Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non -cart) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 pMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NOZ + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write °DIS" in North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Lab Number V v ld 0s A04 N Date Received - —0 Tim Rec'd By: From:Bu , CoHand Del., Other: Data Entry By: Ck: Date Reported: Com fiance LUST, -Pesticide Study, Federal Trust, Other: (circle one) Sample Interval (Pumping time, air temp., etc.) Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolable Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Ran e TPH-BTEX Gasoline Range LAB USE ONLY .Temperature on arrival (IC): GROUNDWATER FIELD/LAB FORM Location code k PQ qVJ(300 — 1 SAMPLE TYPE SAMPLE PRIORITY County MC' ), o"Wel� [Z;— ter Routine Quad No Serial No. ❑ Soil El Emergency din. T Long. 92 c' Of ' ❑Other ❑ Chain of Custody Report To: ARO � RO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourier Hand Del / Other: Purpose: Collector(s): -.Ju.1IG' n' nn Date {AX, JOR Time jQ t i�2, Baseline, Complair FIELD ANALYSES Owner ( pn-� wria pH 4w Spec. Cond.94 at 250C Location'or Site Temp.lo eC Odor Description of sampling point_ Appearance Sampling Method 2un.t' Field Analysis By: Remarks Splt 52m 11 LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml OC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab iss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900' mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/1 Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS" in block. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Lab Number _ ems'-(wel Date Received_ 9- 20.0S% Time: Rec'd By: AI-N � From: Bus, Courier, Hand Del., Other: Data Entry By:_ Date Reported: Ck: Com fiance LUST, -Pesticide Study, Federal Trust, Other: (circle one) Sample Interval (Pumping time, air temp., etc.) Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Or anochlorine Pesticides Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY .Temperature on arrival (°C): % County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No COC Yes/No CMV E® Asheville Regional Office Ann Ofelr PrOtection Loc. Descr.: COATS AMERICAN MW-12 Sample ID: AB34815 PO Number# ARO Date Received: 08/26/2008 Time Received: 14:15 Labworks LoginlD KJIMISON Date Reported: 9/4/08 n -- .` 'C��/ / ((:�\'UA u�,J( Report Generated: 09/04/2008 d Location ID: 1P059W00005603MW12 I Collect Date: 08/26/2008 I Collect Time:: 10:25 I Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations 61-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL B2- Counts from all filters were zero. NE -No established PQL 63- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an un reserved or improperlychemical) X1- Sample not analyzed for this compound y p y preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 . County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Location ID: 1P059W00005603MW12 WA i fn L �Q I, L L� DO � � r 6-P 2 2 26-08 y -� Asheville Regicnad office Aguiky a lti WlsitlD Loc. Descr.: COATS AMERICA MW-12 Collect Date: 08/26/2008 Collect Time:: 10:25 Sample Qualifiers and Comments Sample ID: PO Number* Date Received: Time Received: Labworks LoginlD Date Reported: Report Generated: Sample Depth AB34865 8G1209 08/28/2008 07:45 HPARKER 9/17/08 09/17/2008 9 1 Lg D(� Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwq'iab.org under Staff Access A -Value reported is the average of two or more determinations 61-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL 62- Counts from all filters were zero. NE -No established PQL B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 no in ID: 1P059WQ0005603MW12 _,)c. Desc,.: COATS AMERICA MW-12 ✓isit ID NC DWQ Laboratory Section Results Collect Date: Collect Time:: 08/26/2008 10:25 ^ ay•� •�� r�tt Result Qualifier Units AnalystlDate Approved By /Date Method Reference 8/28108 8/28/08 MIC TOC In liquid 2.0 2.4 mg/L BSWANSON MOVERMAN Method Reference APHA5310B-20th 8/29108 9/8108 WET Ion Chromatography _TITLE_ mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/15/08 Chloride 1.0 33 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/15/08 Fluoride 0.4 2.0 U,P mg/L MIBRAHIMI MOVERMAN Method Reference EPA300.0 9/4/08 9/15/08 Sulfate 2.0 3.9 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4108 9/15/08 NUT Phosphorus total as P in liquid 0.02 0.11 mg/L as P MAJAYI CGREEN Method Reference LaC10-115-01-tEF 8129108 9/3108 MET 7429-90-5 Al by ICP 50 86 u91L PGAUTHIER ESTAFFORD Method Reference EPA 200.7 9/3/08 9111108 7440-38-2 As by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/3/08 9/11108 7440-38-3 Ba by ICP 10 53 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9/11/08 7440-70-2 Ca by ICP 0.10 . 35 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-43-9 Cd by ICPMS '1.0 1.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/3/08 9/11108 7440-47-3 Cr by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-50-8 CubyICPMS 2.0 4.7 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/3/08 9/11/08 7439-95-4 Mg by ICP 0.10 7.7 mg/L PGAUTHIER ESTAFFORD . Method Reference EPA200.7 9/3/08 9/11/08 7439-96-5 Mn by ICP 10 1100 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9/11/08 7440-23-4 Na by ICP 0.10 60 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9/11/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919)`733-3908 Page 2 of 3 NC (DWQ Laboratory Section Results Sample ID AB34865 on ID: 1PO59WQ0005603MW12 Collect Date: 08/26/2008 oc. Desc .: COATS AMERICA MW-12 Collect Time:: 10:25 ,.it ID CAS # Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date 7440 02 0 NI by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7439-92-1 Pb by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7782-49-2 Se by ICPMS - 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913108 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 3 XC DWQQ Laboratory Section Resufts Sample ID AB34815 rDeS 1P059WQ0005603MW12 Collect Date: 0812612008 COATS AMERICAN MW-12 Collect Time:: 10:25 UAs ax Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date Sample temperature at receipt by lab 2.1 °C KJIMISON MMATHIS Method Reference 8126/08 8/28/08 Total Dissolved Solids in liquid 12 268 mg[L KJIMISON CGREEN Method Reference APHA2540C-18TH 8/28/08 9/4/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 . Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code % V0.17 "I''W U OQO,S(-J j W t VV> 1 '4 SAMPLE TYPE County MC -DO ie� Ik Vater Quad No Serial No. ❑ Soil Lat. � (ir1 3�, Long. 2 f— L�1 ❑Other ❑ Chain of Custody Report To: ARO AFRO, MRO, RRO, WaRO, ,WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourier Hanid Del ,Other: Collector(s): Lille ' inr� ate Time 10% 1 Baseline, Complaint, Com liance LUST, -Pesticide Study, Federal Trust, Other: FIELD ANALYSES ' Owner LC � 2 (circle one) ' c__� PH 400 Spec. Cond.94 at 25eC Location or Site— 1jr Temp.lo eC Odor Description of sampling Appearance Sampling Method Field Analysis By: Remarks�,�f LABORATORY ANALYSES II North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION BOD 310 mg/L COD'High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L 03 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L - 0 mg/L Chromium: Hex 1032 ug/L Color, True 80 CU Cyanide 720 mg/L Lab Comments D' . Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900* mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2+ NO3 as N 6W mg/L mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS' in block. SAMPLE PRIORITY Routine Lab Number ❑ Emergency �� Date Received Time: 04 t 5 �,ne.�ita v7-1� Rec'd By: From:Bus, Courier, n De Other: Data Entry By:_ Date Reported: Sample Interval (Pumping time, air temp., etc.) Ag-Silver 4656 u /L Aluminum 6557 u /L tJ As- seni 46551 u /L s/ Ba-Ba 46558 u /L Ca-C ci 46552 mg/L C admiu 46559 u /L r-Chromium 559 u /L Cu-Copper 46562 u IL Fe -Iron 46563 u /L Hg-Mercury71900 u /L -Potassium 6555 mg/L M agnes m 46554 mg/L Mn-M nese 46565 u /L Na-Sod' 46556 mg/L Ni-Nic el u /L Pb- ad 46564 u /L S Selenium u /L Zinc 46567 u /L Ck: Or anochlorine Pesticides Or ano hos horns Pesticides Nitro en Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY .Temperature on arrival (eC): 'ray North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code Pti. �� 000 SAMPLE TYPE SAMPLE PRIORITY -�q %'� u County C !10vt3C'�� [ZVVater Routine Lab Number 9 - V Quad No Serial No. El Soil ❑ Emergency Date Received Time, Lat. 5 147 i 33•S-" Long. k;a Of 1�, ' El Other my�,IC� Rec'd By: From:Bu ourier Hand Del., El Chain of Custody Other: Report To: ARO FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ouner Hand Del , Other: Purpose: Collector(s): il; lletnn Date I Time Ba elinLe, Complaint, Com liance LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner <ti� (circle one) PH 400 Spec. Cond.94 at 251C Location or Site ay i CNn Temp.lo DC Odor Description of sampling point rvl 00 1,6r Appearance Sampling Method i?_M12 Sample Interval Field Analysis By: Remarks_ Sole- M�IQ I, (HumD. baiier.ec. LABORATORY ANALYSES I (Pumping time, air temp.. etc.) BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 u /L COD'High 340 mg/L Fluoride 951 mg/L AI -Aluminum 46557 u /L COD Low 335 mg/L Hardness: Total 900' mg/L As -Arsenic 46551 u /L Coliform: MF Fecal 31616 /loom1 Hardness (non-carb) 902 mg/L Ba-Barium 46558 u /L Coliform: MF Total 31504 /100ml Phenols 32730 ug/I Ca -Calcium 46552 m 2 TOC 680 mg/L Specific Cond. 95 pMhos/cm Cd-Cadmium 46559 u /L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 u /L Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Oil and Grease mg/L Hg-Mercury 71900 u /L pH 403 units K-Potassium 46555 m /L Alkalinity to pH 4.5 410 mg/L Mg -Magnesium 46554 m /L Alkalinity to pH 8.3 415 mg/L Mn-Manganese 46565 u /L Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 m /L Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel u /L Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 u /L Chloride 940 mg/L P: Total as P 665 mg/L Se -Selenium u /L Chromium: Hex 1032 ug/L Nitrate (NO3as N) 620 mg/L n-Zinc 46567 u /L Color: True 80 Cu Nitrite (NO2 as N) 615 mg/L Cyanide 720 mg/L Lab GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write °DIS" in block. Or anochlorine Pesticides Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY .Temperature on arrival (°C): County: MCDOWELL River Basin Report To AROAP I Collector: J VANN Sample ID; PO Number# Date Received: Time Received: Region: ARO �r-P 2o® rrr���,,,[� Labworks LoginlD Sample Matrix: GROUNDWATER J� f3 t� ! Ifs) 7y Date Reported: Loc. Type: MONITORING WELL t�1 �--•1` Report Generated: Emergency Yes/No S�iQ��il� Ke,,O f�c @ �ffiC� COC Yes/No I i }Q t. l VisitlD "IfOr rOtOCLIO Location ID: 1sCt� Loc. Descr,: COATS AMERICA MW-13 1P059WQ0005603MW73 Collect Date: 08/26/2008 Collect Time:: 10:35 Sample Depth Sample Qualifiers and Comments AB34866 8G1210 08/28/2008 07:45 HPARKER 9/12/08 09/12/2008 9 1.5)0 Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL 62- Counts from all filters were zero. NE -No established PQL 63- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed. to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No COC Yes/No RECEWEDD SEP ® 9 2000 ,Asheville Regional Office d�+ t�ifer Protection VisitlD Loc. Descr.: COATS AMERICAN MW-13 Sample ID: AB34816 PO Number# ARO Date Received: 08/26/2008 Time Received: 14:15 Labworks LoginlD KJIMISON Date Reported: 9/4/08 Report Generated: 09/04/2008 C)aq 5 019 I Location ID: 1P059WQ0005603MW73 I Collect Date: 08/26/2008 I Collect Time:: 10:35 I Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated B2-Counts from all filters were zero. NE -No established PQL B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. B5-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Pagel of 2 XC DWQ Laboratory Section Results Sample ID AB3486E VDr.: 1P059WO0006603MW13Collect Date: 08/26I2008 COATS AMERICA MW-13 Collect Time:: 10:35 Visit ID ..no m r�naryce FUL Result Qualifier Units Approved By /Date Method Reference 8/28/08 8/28/08 MET 7429-90-5 AI by ICP 50 84 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3108 9/11/08 7440-38-2 As by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7440-38-3 Be by ICP 10 130 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-70-2 Ca by ICP 0.10 33 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7440-47-3 Cr by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/2/08 9/11108 7440-50-8 Cu by ICPMS 2.0 390 ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7439-95-4 Mg by ICP 0.10 22 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9111/08 7439-96-5 Mn by ICP 10 1000 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-23-4 NabyICP 0.10 170 M91L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9111/08 7440-02-0 NI by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9111/08 7439-92-1 Pb by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623. (919) 733-3908 Page 2 of 2 IDNC D`l�1%QQ Laboratory Section 12esufts Sample ID AB34816 n : 1P059WQ0005603MW13 Collect Date: 08/26/2008 c. Descr.: COATS AMERICAN MW-13 Collect Time:: 10:35 Visit ID .,ham w rnnaryce name rc,tL Result Qualifier Units Analyst/Date Approved By /Date Sample temperature at receipt by lab 2.1 °C KJIMISON MMATHIS Method Reference 8/26/08 . 8128/08 Total Dissolved Solids In liquid 12 767 mg/L KJIMISON CGREEN Method Reference APHA2540C-18TH 8/28/08 9/4/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 t� North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code � PO 000 - 13 SAMPLE TYPE SAMPLE PRIORITY Q. County McDdWe k /ater Routine Lab Number ❑ Soil ❑ Emergency oa Quad No Serial No. Date Received - Time" Arne•✓/ca Lat. � u� / 10 $" Long. a I ' 17 " Other W -t3 Redd By: From:Bus, ourier, and Del., ❑ Chain of Custody Other: Report To: ARO FRO, MRO, RRO, WaRO, WiRO, Data Entry y: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ourier Hand Del Other: Purpose: Collector(s): JLJje nn Date Bas ine Co plaint, Com liance LIST, -Pesticide Study, Federal Trust, Other: FIE_ LD ANALYSES Owner (circle one) pH 400 Spec. Cond.94 at 25°C Location or Site tAs2XI T1 - Temp.10 eC Odor Description of sampling point GyLk,7jjAr7 (At Appearance Sampling Method ')-*'u-m t" Sample Interval Field Analysis By: Remarks Snl mpj-e sumo. a ec ea LABORATORY ANALYSES (Pumping time, air temp„ etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml C liform: MF Total 31504 /100ml mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 416 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab Comments For Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900' mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm tMQAP mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 _ mg/L NO2+ NO3 as N 630 mglL Wwamisutlatll mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L Analysis -submit filtered Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 a /L Cr-Chromium 46559 u /L Cu-Copper,46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel - u /L Pb-Lead 46564 u" /L Se -Selenium u /L Zn-Zinc 46567 u /L rnf,lal� M Or anochlorine Pesticides Or ano hos horus Pestici Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bo TPH-Gasoline Range TPH-BTEX Gasoline Ranc LAB USE ONLY .Temperature on arrival (°C): GROUNDWATER FIELD/LAB FORM Location code YU.1i"IWIN UgQ54D-5VIVV-I_9 County M C-7c e•11i Quad No Serial No. Lat. S `t7 i W, 3 Long. r 1 SAMPLE TYPE SAMPLE PRIORITY Ml<ater Routine ❑ Soil ❑ Emergency ❑ Other JI ❑ Chain of Custody Report To: RO RO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourie1,Hand Del Other: Purpose: Collector(s): ..Jt&ile Zo n Date 24 Time it3:�> Bas line, FIELD ANALYSES Owner pH 4w Spec. Cond.94 at 25°C Location or Site Temp.lo °C Odor Description of sampling Appearance Sampling Method Field Analysis By: Remarks LABORATORY_ ANALYSES �'L I BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 1100ml mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L H 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L 0 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Comments iss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900' mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/1 Spec Cond. 95 uMhos/cm mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + N% as N 630 mg/L P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write °DIS° in block. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Lab Number Q6�/Ca Date Received • Time: Rec'd By: j&ik' From:Bus, Courier, Hand Del., 'Other: Data Entry By: Ck: Date Reported: laint,cCom fiance LUST, -Pesticide Study, Federal Trust, Other: (circle one) Sample Interval (Pumping time, air temp., etc.) Ag-Silver46566. u /L + Ai -Aluminum 0557 u /L -Arsenic 6551 u /L t Ba- du 46558 u /L Ca-C ' m 46552 mg/L Cd admiu 46559 u /L r-Chromium 4r6559 u !L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m [L Magn sium 46554 m fL MnManjanese 46565 u /L Na-Sokm46556 mg/L Ni-N' kel u /L Pb ead 46564 u /L Selenium u /L Zn-Zinc 46567 u /L Or anochlorine Pesticides Oroano hos horns Pesticides Nitrogen Pesticides Acid' Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY .Temperature on arrival (IC): 1 County: MCDOWELL River Basin Report To AROAP CO.V rE 0i ii u l� Collector: J VANN Region: ARO VEP 2 2 2008 Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No 'I ,iiG�pfl��a V vagi heal Office COC Yes/No a S'ey6�1.tir '-n �jr)�--,11-- Location ID: 1P059WQ0005603MW14 i VisitlD COATS AMERICA MW-14 Collect Date: 08/26/2008 1 Collect Time:: 10:45 Sample Qualifiers and Comments Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Date Reported: Report Generated: Sample Depth AB34867 8131211 08/28/2008 07:45 HPARKER 9/17/08 09/17/2008 -�� CI � (s I C)<� Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations 61-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL 62-Counts from all filters were zero. NE -No established PQL B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound W-The component has been tentatively identified based on mass spectral library search and has an estimated value MUM Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No COC Yes/No Location ID: 1P059WQ0005603MW14 6L5CF�VE0 0P 0 9 2G08 Asheville Regional Office Aoulfer Protection l Loc. Descr.: COATS AMERICAN MW-14 Collect Date: 08/26/2008 Collect Time:: 10:45 Sample Qualifiers and Comments Sample ID: AB34817 PO Number # ARO Date Received: 08/26/2008 Time Received: 14:15 Labworks LoginlD KJIMISON Date Reported: 9/4108 Report Generated: 09/04/2008- Sample Depth Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated 62-Counts from all filters were zero. NE -No established PQL 63-Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of F, ID: 1 P059W00005603 MW14 Desor.: COATS AMERICA MW-14 ID NC DWQ Laboratory Section Results Collect Date: Collect Time:: 08/26/2008 10:45 ranaiyce name PQL Result Qualifier Units AnalysUDate Approved By /Date Method Reference 8/28/08 8/28/08 MIC TOC In liquid 2.0 5.6 mg/L' BSWANSON MOVERMAN Method Reference APHA5310B-20th 8/28108 9/8/08 WET NUT MET Ion Chromatography TITLE_ mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4108 9/15/08 Chloride 1.0 30 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9/15/08 Fluoride 0.4 2.0 U,P mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 9/4/08 9115/08 Sulfate 2.0 2.0 mg/L MIBRAHIMI MOVERMAN Method Reference EPA 300.0 Phosphorus total as P in liquid Method Reference Lac10-115-01-1EF 7429-90-5 AI by ICP 9/4/08 9/15/08 0.02 0.26 mg/L as P MAJAYI CGREEN 8/29/08 9/3108 50 1600 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-38-2 As by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-38-3 BabyICP 10 140 ug/L PGAUTHIER- ESTAFFORD Method Reference EPA200.7 913/08 9/11/08, 7440-70-2 Ca by ICP 0.10 60 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913/08 9/11108 7440-47-3 Cr by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-50-8 CubyICPMS 2.0 210 ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913/08 9/11/08 7439-954 Mg by ICP 0.10 38 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9/11/08 7439-96-5 Mn by ICP 10 530 ug/L PGAUTHIER ESTAFFORD • Method Reference EPA 200.7 9/3/08 9/11/08 7440-23-4 Na by ICP 0.10 64 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 3 NC DWQ Laboratory Section Results ,,6: 1 P059WQ0005603MW14 Descr.: COATS AMERICA MW-14 Vsit ID Sample ID AB348M Collect Date: 08/2612008 Collect Time:: 10:45 ur» 9F Anaiyte Name PQL Result Qualifier Units AnalystlDate Approved By /Date 7440 02 0 NI by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913/08 9/11/08 7439-92-1 Pb by ICPMS 10 22 ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3108 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 3 .NC DWQ Laboratory Section Resufts Sample ID VD 1 P059W00005603MW74 Collect Date: COATS AMERICAN MW-14 Collect Time:: Visit ID 08/26/2008 16:45 Anaiyie Name PQL Result Qualifier Units Analyst/Date Approved By (Date Sample temperature at recelpt by lab 2.1 °C KJIMISON MMATHIS Method Reference 8/26/08 8/28/08 Total Dissolved Solids In liquid 12 446 mg/L KJIMISON CGREEN Method Reference APHA254OC-18TH 8/28/08 9/4/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code YC�� `1 vJLy oC0,5(rfJ S »11— i `f County MG�©in3e�� Quad No Serial No. Lat. 35- Lf 1 ai, �, r Long. ka ` Ui ' (q, % u SAMPLE TYPE M1 ater ❑ Soil ❑ Other ❑ Chain of Custody SAMPLE PRIORITY Routine ❑ Emergency Report To: ARO FRO, MRO, RRO, WaRO, WiRO, III WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourier Hand Del , Other: Pur ose: Collector(s): Jtk l l,e Date ,�6 Time E FIELD ANALYSES Owner pH 400 Spec. Cond.94 at 25°C Location or Site f Temp.lo °C Odor Description of sampling Appearance Sampling Method Field Analysis By: Remarks So14- 1 ARf1RATf1RY ANAI YSFS �II BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml liform: MF Total 31504 • /100ml T C 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L arbon dioxide 405 mg/L 0 `I mg/L Chromium: Hex 1032 ug/L Color: True 80 cU Cyanide 720 mg/L Lab Comments Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L i Phenols 32730 ug/I S ecific Cond. 95 NMhos/cm mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + N% as N 630 mg/L _ I 5 mg/L Nitrate (NO3as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L For Dissolved Analysis -submit filtered sample and write 'DIS" in block. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION rr Lab NumberSVp+- t �M2 f/Ca Date Received 0 ��" �� nCoune I Rec'd By: From: Hand Del., Other: Data Entry y: Ck: Date Reported: plaint, Com fiance LUST, Pesticide Study, Federal Trust, Other: (circle one) (Pumping time, air temp., etc.) 66 u /L AI- uminum 46557 u /L As -A enic 46551 u /L Ba-13rium 46558 u /L Ca- Icium 46552 mg/L Cd- admium 46559 u /L Chromium 46559 u '/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 mg/L iN-Magnesiurn 46554 mg/L Mn- anganese 46565 u /L Na-S dium 46556 mg/L Ni-Ni kel u /L b-L ad 46564 u /L Se- elenium u /L Zinc 46567 u /L Pesticides rus Pesticides PCBs TPH-Diesel TPH-Gasoline Rangf TPH-BTEX Gasoline VIVLT .Tee mperaera ture on arrival (°C)� vy f . A �< 11 f txd OUNDWATER FIELD/LAB FORM Location code I V0.1i'1yJU (3CQ5_&.,0'-5 W I \N— I't SAMPLE TYPE County RC Q i elk ®�Vvater Quad No Serial No. ❑ Soil Lat. S �i / Q, ('a ` Long. . Dl 19r 7 ``_ El Other ❑ Chain of Custody Report To: ARO)FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY Routine Lab Number ❑ Emergency �� Date Received '9•?-(­4:9 Time: i .ft�'_ ltrnerfca Vj _ I Rec'd By: 4j4� From:Bus, Courier, Hand Del., `Other: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ourier Hand D'elr, Other: Purpose: Collector(s): JLJle U;()n Date Time_j0. IJ5— Baseline, Complaint, Com Hance LUST, -Pesticide Study, Federal Trust, Other: FIELD ANALYSES f Owner (circle one) pH 400 Spec. Cond.94 at 250C Location'or Site Temp.lo °C. Odor Description of sampling point Appearance Sampling Method _ Sample Interval Field Analysis, By: LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 - /100ml mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L i/ H 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L mg/L Chromium: Hex 1032 ug/L Color. True 80 Cu Cyanide 720 mg/L Lab Comments ss. Solids 70300 mg/L Fluoride 951 mg%L Hardness: Total 900' mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/l Specific Cond. 95 NMhos/cm 5 mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as-N 630 mg/L mg/L Nitrate (N%as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS" in block. (pumping time, air temp., etc.) 66 'u /L I -Aluminum 4 57 u /L AS rsenic 6551 u /L Ba-Ba • 46558 u /L Ca-C Ici 46552 mg/L C-Cadmiu 6559 u /L Cr-Chromium 4 59u /L Cu-Copper 46552 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46 54 m [L M Manganes 46565 u /L Na-S iu 655E mg/L Ni-Nick u /L b-L ad 4656 u /L S,p1selenium u /L Za Zinc 46567 u L Nitrogen Pesticides Acid Herbicides Semivolatile Volatile Organ TPH-Gasoline LAB USE ONLY .Temperature on arrival (°C): �. MCDOWELL Basin t To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No "SE-P 16 2GQO Asheville Regional Office Sample ID: PO Number# Date Received: Time Received: Labworks LoginlD Date Reported: Report Generated: COC Yes/No Aquifer Protection I =n �j Loc. Descr.: '�O�CJ�� Location ID: 1P059W00005603MW15 Collect Date: 08/26/2008 Collect Time:: 10:55 Sample Depth Sample Qualifiers and Comments Routine Qualifiers �� fit 1�.� �• For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated 62- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and < 20; Estimated B5-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB AB34868 8G1212 08/28/2008 07:45 HPARKER 9/11 /08 09/11/2008 q�la /'q g N3-Estimated concentration is < PQL and >MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution Q1-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected X1- Sample not analyzed for this compound Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Page 1 of 2 XC WQQ La6oratory Section Results Sample ID AB3486f 1P059WQ0005603MW15 Collect Date: 08/26/2008 Collect Time:: 10:66 �rQ w Anatyie name PQL Result Qualifier Units Analyst/Date Approved By /Date temperature Method Reference 8/28/08 8/28/08 MIC TOC In liquid 2.0 4.4 mg/L BSWANSON MOVERMAN Method Reference APHA5310B-20th 8/28/08 9/8108 MET 7429-90-5 AI by ICP 50 50 U ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.7 913/08 9/11108 7440-38-2 As by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 9/11/08 7440-38-3 Ba by ICP 10 140 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9111108 7440-70-2 Ca by ICP 0.10 67 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913108 9/11/08 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7440-47-3 Cr by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9111/08 .7439-95-4 Mg by ICP 0.10 30 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7439-96-5 MnbyICP 10 2000 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-23-4 NabyICP 0.10 52 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-02-0 NI by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9/11/08 7439-92-1 Pb by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2/08 9111/08 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3/08 s/»ma Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 North Carolina UNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION cation code pl3 (Q00 S��AMP��LE TYPE SAMPLE PRIORITY r / j P ounty MG�©iA1��1 ®N1later Routine Lab Numb �i I �l1 7V� ❑ Soil ❑ Emergency (i) � Quad No Serial No. Date Received —99 Qg TimeLat. 3r y7'�G, Long. Ff O! �(�. ( ❑Other Rec'd By: From: Bus, ourier, and Del., IElChain of Custody ' Other: Report To: ARO FRO, MRO, RRO, WaRO, WiRO, I Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ourier Hand Del Other: Purpose. Collector(s): -301e ZAn Date Time )U:SS- Baseline, Complaint, Com liance LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner (circle one) pH 40o Spec. Cond.94 at 250C Location'or Site Temp.lo °C Odor Description of sampling point Appearance Sampling Method Sample Interval Field Analysis By: Remarks SA4 m Pie umo, ai er. etc.) ARORATORY ANALYSES (Pumping time, air temp., etc.) C BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /10oml oliform: MF Total 31504 /100ml OC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab Comments Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900* mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/l Specific Cond. 95 uMhos/cm mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L mg/L Nitrate (NO3as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L g-Silver 46566 u /L ,,,"ANAiuminul 46557 u /L s rsenic 46551 u /L Ba- arium 46558 u /L Ca alcium 46552 m /L C Cadmium 46559 u /L Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Magnesium 46554 m /L Mn Manganese 46565 u /L• Na- odium 46556 m /L Ni- ickel u /L P Lead 46564 u /L e-Selenium u /L Zn-Zinc 46567 u /L Nitrogen Pesticides Acid Herbicides Semivolatile I I TPH-BTEX Gasoline Rance I LAB USE ONLY .Temperature on arrival (eC): n q GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. ( / Cfc. re'05 Cn I County: MCDOWELL Sample ID: AB34862 River Basin W A RQ PO Number # 8G1206 Report To �qF G AROAP �C? =� r Date Received: Time Received: 08/28/2008 07:45 Collector: J VANN © C Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-2 Location ID: 1P059WQ0005603MW2 Collect Date: 08/26/2008 Collect Time: 09:25 Sample Depth Result/ Method Anal sis CAS # Analyte Name PQL. Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/08 MMATHIS MIC TOC in liquid 2.0 2 U mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE_ mg/L EPA300.0 9/4/08 MOVERMAN Chloride 1.0 5.8 mg/L EPA300.0 9/4/08 MOVERMAN Fluoride 0.4 0.4 U mg/L EPA300.0 9/4/08 MOVERMAN Sulfate 2.0 5.3 mg/L EPA300.0 9/4/08 MOVERMAN NUT Phosphorus total as P in liquid 0.02 0.04 mg/Las P LaC10-115-01-1EF 8/29/08 CGREEN MET 7429-90-5 AI by ICP 50 50 U ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 47 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 19 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.6 ug/L EPA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 10 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 68 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 9.9 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description ofthe qualifier codes referto htp.;/[.. o.faLLn..,d�.��.:o��,i�.-�e[wq(ian[�.c�ry.�fi.�/..te<ha._ ouai„e..p..o„rt„a„ll.jwden„ro..pjy'e,L/glcl„lap/p2.�.[i, oftechassisb Page 1 of 1 %ounty: MCDOWELL Sample ID: AB34807 River Basin ��} WATERQ PO Number# ARO Report To AROAP O G Date Received: 08/26/2008 Time Received: 14:15 Collector. J VANN p -�C Labworks LoginlD KJIMISON Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AMERICAN MW-2 Location ID: 1P069WQ0005603MW2 Collect Date: 08/26/2008 Collect Time: 09:26 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °C 8/26/08 SMATHIS Total Dissolved Solids in liquid 12 110 mg/L APHA2540C-18TH 8/28108 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hte'// norcal.ncdenr.orpvebi�aayipn�_;pgnflppteq h—!ztaoaw ouarner codes « twd. cro tal,"c�,jpiwgLagiznfi°5o/tecnass zn Page 1 of 1 County: MCDOWELL tjq ASample ID: AB34863 sin PO Number # SG1207 /28/2008 J VANN ARO � r Time Received: 07:45 � Y Labworks LoginlD HPARKER CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/08 MMATHIS MIC TOC in liquid 2.0 2 U mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE_ mg/L EPA300.0 9/4/08 CGREEN Chloride 1.0 10 mg/L EPA300.0 9/4/08 CGREEN Fluoride 0.4 2.0 U,P mg/L EPA300.0 9/4108 CGREEN Sulfate 2.0 150 mg/L EPA300.0 9/4108 CGREEN NUT Phosphorus -total as P in liquid 0.02 0.02 U mg/Las P Lac10-115-01-1EF 8/29/08 CGREEN MET 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 16 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 1.1 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.6 ug/L EPA200.8 913/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 0.43 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 10 U ug/L EPA200.7 9/3108 ESTAFFORD 7440-23-5 Na by ICP 0.10 110 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to :�is.,o,,,rcel node_.:x(weciyy._ll�n[ ca..ry..nryp� zcnasrztgo.._.� cuauxer cede; <rcoal ucrcal: rcd_n...o.R[.;.-�p[.w....a.[ins!zc.�.rt.� .�/..fe.<n„_s�sn Page 1 of 1 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to :�is.,o,,,rcel node_.:x(weciyy._ll�n[ ca..ry..nryp� zcnasrztgo.._.� cuauxer cede; <rcoal ucrcal: rcd_n...o.R[.;.-�p[.w....a.[ins!zc.�.rt.� .�/..fe.<n„_s�sn Page 1 of 1 County: MCDOWELL Sample ID: AB34808 River Basin OF WAT �9 PO Number# ARO Report To AROAP O� QG Date Received: 08/26/2008 C. r Collector: J VANN � Time Received: 14:16 � Labworks LoginlD KJIMISON Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-10 Location ID: 1P059WQ0005603MW10 Collect Date: 08/26/2008 Collect Time: 09:60 Sample Depth CAS # Analyte Name Others Sample temperature at receipt by lab Total Dissolved Solids in liquid PQL Result/ Units Qualifier 2.1 °C 12 316 mg/L Method Analysis Validated by Reference Date 8/26/08 MMATHIS APHA254OC-18TH 8/28/08 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp;[(_Portof.n�d �co:ylwsbLyea[lal,!,iannr,oLmcha-stIf ayarn:Lcapes <htp:fi uortal_ncdun_r /webiwa/iai�!aar-.floltechass�sn Page 1 of 1 County: MCDOWELL Sample ID: AB34864 River Basin(} Report To W ATFi�yQ G PO Number # 8G1208 Collector: AROAP J VANN �O ^! Date Received: Time Received: 08/28/2008 07:46 Region: ARO Labworks LoginlD HPARKER Sample Matrix: GROUNDWATER Report Generated: 5/19/09 Loc. Type: MONITORING WELL D ate Reported: 12/20/2011 Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-11 Location ID: 1P059=000560311OW11 Collect Date: 08/26/2008 Collect Time: 10:12 Sample Depth CAS # AnalVte Name PQL Result/ Units Method Anal sis Validated by - Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/08 MMATHIS MIC TOC in liquid 2.0 4.4 mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography TITLE mg/L EPA300.0 9/4/08 MOVERMAN Chloride 1.0 5.4 mg/L EPA 300.0 9/4/08 MOVERMAN Fluoride 0.4 0.4 U mg/L EPA300.0 9/4/08 MOVERMAN Sulfate 2.0 33 mg/L EPA300.0 9/4/08 MOVERMAN NUT Phosphorus total as P in liquid 0.02 0.20 mg/Las P LaC10-115-01-1EF 8/29/08 CGREEN MET 7429-90-5 AI by ICP 50 460 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 100 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 18 mg/L EPA200.7 9/3108 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/3108 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 9/3/08 - ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 11 ug/L EPA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 6.2 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 890 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 84 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htpl(.pcn_Lncd=..: r ory�web�wa/Iab;naNnfieieechass�zeaozna 0u,HHer Codes cntp;// nona1.ncdenr,ore wen�w9 lagr_tefinng/teehessisb Page 1 of 1 County: MCDOWELL Sample ID: AB34809 VApl� River Basin To (7k O� pGp PO Number # ARO Report AROAP co r Date Received: Time Received: 08/26/2008 14:15 Collector: J VANN a Labworks LoginlD KJIMISON Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-11 Location ID: 1P059WQ0005603MWll Collect Date: 08/26/2008 Collect Time: 10:12 Sample Depth CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °C 8126/08 MMATHIS Total Dissolved Solids in liquid 12 280 mg/L APHA2540C-18TH 8/28/08 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp;[( nemi.pcd._ncorafvebi ap(aannro/eechasz!stttData Qualifier coxes rntp;f onalscd .nr,o ,.�prNia!I�i,,i:ca nflo Eha.nse> Page 1 of 1 Gounty: MCDOWELL Sample ID: AB34865 aiFR River Basin Q� PO Number # Date 8G1209 Report To AROAP ,O r Received: Time Received: 08/28/2008 07:45 Collector: J VANN Y Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICA MW-12 Location ID: 1P059WQ0005603MW12 Collect Date: 08/26/2008 Collect Time: 10:25 Sample Depth CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 0.9 Units °C Method Reference Analysis Date 8/28/08 Validated by MMATHIS MIC TOC in liquid 2.0 2.4 mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE_ mg/L EPA300.0 9/4108 MOVERMAN Chloride 1.0 33 mg/L EPA300.0 9/4/08 MOVERMAN Fluoride 0.4 2.0 U,P mg/L EPA 300.0 9/4/08 MOVERMAN Sulfate 2.0 3.9 mg/L EPA300.0 9/4/08 MOVERMAN NUT Phosphorus -total as P in liquid 0.02 0.11 mg/Las P LaclO-115-01-lEF 8129/08 CGREEN MET 7429-90-5 AI by ICP 50 86 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 53 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 35 mg/L EPA200.7 913/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.7 ug/L EPA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 7.7 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 1100 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 60 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/3108 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/3108 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp.j. j p Lecdenr.orgL epLa/Iab� cafinflo[LechassiztnDua Oualifler C°tic ortaLncd�nr a Leb Iab!aafinfio/[echasisb Page 1 of 1 County: MCDOWELL Sample ID: AB34815 River Basin VUATE�r'p PO Number # ARO To �pF G Report AROAP �4 Date Received: Time Received: 08/26/2008 14:15 Collector: J VANN t Labworks LoginlD KJIMISON Region: ARID Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-12 Location ID: 1PO59WQ0005603MW12 Collect Date: 08/26/2008 Collect Time: 10:25 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °C 8/26/08 MMATHIS Total Dissolved Solids in liquid 12 268 mg/L APHA2540C-18TH 8/28/08 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htd// n°rtal.ncdenrare/web/vac/iab/stafinflo/techa ssi,taoata o-rfier Codes <ntDJ/ oarY Lncd=_nr or8lweb/wagabk:afinfi°/[echaszizb Page 1 of 1 County: MCDOWELL Sample ID: AB34866 WAT�g River Basin 0� QGy PO Number# 8G1210 Report To AROAP Date Received: 08/28/2008 �O� >_ Time Received: 07:45 Collector: J VANN < Labworks LoginlD HPARKER Region: ARID Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICA MW-13 Location ID: 1P059WQ0005603MW13 Collect Date: 08/26/2008 Collect Time: 10:35 Sample Depth CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 0.9 Units °C Method Reference Analysis Date 8/28/08 Validated by MMATHIS MET 7429-90-5 Al by ICP 50 84 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/2/08 ESTAFFORD 7440-38-3 Ba by ICP 10 130 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 33 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/2/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 912/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 390 ug/L EPA200.8 9/2/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 22 mg/L EPA200.7 913/08 ESTAFFORD 7439-96-5 Mn by ICP 10 1000 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 170 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/2/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/2/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/2/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ntp',[! portal;P�denr.or¢/weL•/wo/I b tp„a„NnfipLteahaszlztkData Dual(flnr cone: <ntp:Il Ccrtas5denr.oralweb/wa/I,_b nnfinno te<haw'-Vt Page 1 of 1 County: MCDOWELL Sample ID: AB34816 River Basin 4VATF PO Number # ARO Report To AROAP �O "3G Date Received: 08/26/2008 co Time Received: 14:15 Collector: J VANN a Labworks LoginlD KJIMISON Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12l20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-13 Location ID: 1PO59WQ0005603MW13 Collect Date: 08/26/2008 Collect Time: 10:35 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °C 8/26/08 MMATHIS Total Dissolved Solids in liquid 12 767 mg/L APHA254OC-18TH 8/28/08 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fare detailed description of the qualifier codes refer to n2t,.;/j,�ortal,acd_ �r�,!weh(yL Llai,(_cuN.�.ftn/pechsslstkDat_�_alifler Codes rn.-1 portalncdnn—ryfwetvja�lag�_;��finri�gechassise? Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: AB34867 8G1211 08/28/2008 07:46 HPARKER 5/19/09 12/2012011 Loc. Descr.: COATS AMERICA MW-14 Location ID: 1P059WQ0005603MW14 Collect Date: 08/26/2008 Collect Time: 10:45 Sample Depth CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 0.9 Units °C Method Reference Analysis Date 8/28/08 Validated by MMATHIS MIC TOC in liquid 2.0 5.6 mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE_ mg/L EPA 300.0 9/4/08 MOVERMAN Chloride 1.0 30 mg/L EPA 300.0 9/4/08 MOVERMAN Fluoride 0.4 2.0 U,P mg/L EPA 300.0 9/4/08 MOVERMAN Sulfate 2.0 2.0 mg/L EPA 300.0 9/4/08 MOVERMAN NUT Phosphorus total as P in liquid 0.02 0.26 mg/Las P Lac10-115-01-1EF 8/29/08 CGREEN MET 7429-90-5 Al by ICP 50 1600 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 140 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 60 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 210 ug/L EPA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 38 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 530 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 64 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/3/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 22 ug/L EPA200.8 9/3/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp:/Lportai.ncdenr.oralweh/wcuahistafineo/techassisttDa;a ouaiieer codes.htn:/i ncrtai..ncdenroreL h/wcnab�s:afirnoj;,..�na�s_sn Page 1 of 1 County: MCDOWELL Sample ID: AB34817 River Basin Report To 04 `t'tArFq QG PO Number# ARO AROAPO� Date Received: 08/26/2008 Time Received: 14:15 Collector. J VANN Y Labworks LoginlD KJIMISON Region: ARO Report Generated: 5/19l09 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No Visit]D COC Yes/No Loc. Descr.: COATS AMERICAN MW-14 Location ID: 1PO69WQ0005603MW14 Collect Date: 08/26/2008 Collect Time: 10:45 Sample Depth Result/ Method Anal sis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °C 8/26/08 MMATHIS Total Dissolved Solids in liquid 12 446 mg/L APHA2540C-1BTH 8/28108 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nca:/� norcal.ncdanr.orx/wee�wa/lae�scaenflohecnas�scuc_:a_ oniieer rode: <nro:!! aortal.ncdenr.orelweeiwv/wn/nannflohechassec> Page 1 of 1 County: MCDOWELL Sample ID: AB34868 River Basin OF WATER PO Number # 8G1212 Report To AROAP Q� p Date Received: 08/28/2008 Time Received: 07:45 Collector: J VANN Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 t Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: Location ID: 1P059WQ0005603MW15 Collect Date: 08/26/2008 Collect Time: 10:55 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/08 MMATHIS MIC TOC in liquid 2.0 4.4 mg/L APHA5310B-20th 8/28/08 MOVERMAN MET 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 6.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Ba by ICP 10 140 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 67 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/2/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA200.8 9/2/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 9/2/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 30 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-96-5 Mn by ICP 10 2000 ug/L EPA200.7 9/3108 ESTAFFORD 7440-23-5 Na by ICP 0.10 52 mg/L EPA200.7 913/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 10 U ug/L EPA200.8 9/2/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 10 U ug/L EPA200.8 9/2/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to h wrtal.ncd=nr or�j. et�yiy[tabisca..e�fiojred aj., teo-:a opar er CodT,_o-// xrtal_ncdencora/web/wa/lab/»afinno/techassist> Page 1 of 1 ANr WO Laboratory,Section 12..suds County: MCDOWELL Sample ID: AB56685 River Basin �0F WATFgQ Gy PO Number # 10G0162 Report To AROAP �O t_ Date Received: 04/08/2010 Collector: B LAVERTY Y Time Received: 08:25 P LoginlD SMATHIS Region: ARID Report Report Generated: 4/23110 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW2COATS Collect Date: 04/06/2010 Collect Time: 10:00 Sample Depth CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 1.7 Units °C Method Reference Analysis Date 4/8/10 Validated by SMATHIS MET 7429-90-5 AI by ICP 50 640 ug/L EPA200.7 4/14110 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-38-3 Ba by ICP 10 66 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 19 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 5800 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 9.9 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 380 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 9,2 mg/L EPA200.7 4/14110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 13 ug/L EPA 200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ht // rc i m / b/ wn bl tae fi rt ch s•r tao t n rfi< C a htp:/( o°rtai.ncdenr.ore/web/we/lab/snff,So/techasslst> Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No VisitlD Loc. Descr.: COATS AMERICAN Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: AB56686 10GO163 04/08/2010 08:25 SMATHIS 4/23/10 12/20/2011 Location ID: 1P59MW2COATS Collect Date: 04/0612010 Collect Time: 10:00 Sample Depth CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 °C 4/8/10 SMATHIS MET 7429-90-5 Al by ICP 50 120 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-38-3 Ba by ICP 10 34 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 18 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 170 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 8.8 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 10 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.1.0 9.3 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ht : /8artai ncoenr ore/web/w°nabhtafinao/tcogs jLt#oaptIn_er codes �ht2, Lj o me nor.q vebLw,ab.JgW..Hena[,Egcn�.:ytz1> Page 1 of 1 County: MCDOWELL Sample ID: AB56687 River Basin OF WA7Ei9 PO Number# 10GO164 Q� Report To AROAP r�0� r Date Received: 04/08/2010 Collector: B LAVERTY j Y Time Received: 08:25 p Labworks LoginlD SMATHIS Region: ARO Report Generated: 4/23/10 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW10C0ATS Collect Date: 04/0612010 Collect Time: 10:16 Sample Depth CAS # LAB Analyte Name Sample temperature at receipt by lab PQL. Result/ Qualifier 1.7 Units °C Method Reference Analysis- Date 4/8/10 Validated by SMATHIS MET 7429-90-5 Al by ICP 50 50 U uglL EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by furnace 2.0 2.0 U ug/L EPA200.9 4/13/10 ESTAFFORD 7440-38-3 Ba by ICP 10 19 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 0.95 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 56 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 0.46 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 IOU ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 96 mg/L EPA200.7 4/14110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ht°•// mft i m o q/ b/ n b/st s fi /ern t no t o° r+re Codes OW-11 rt t m /w b/ a/i b/ nfl n /tech i t> Page 1 of 1 County: MCDOWELL Sample ID: AB56688 River Basin �0F `NAr�gp PO Number # 10G0165 Report To AROAP �O Date Received: 04/0812010 Collector: B LAVERTY Time Received: 08:25 p Y Labworks LoginlD SMATHIS Region: ARID Report Generated: 4/23/10 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL ' Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW11COATS Collect Date: 04/06/2010 Collect Time: 10:27 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 °C 4/8/10 SMATHIS MET 7429-90-5 Al by ICP 50 500 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by furnace 2.0 2.0 U ug/L EPA200.9 4/13/10 ESTAFFORD 7440-38-3 Ba by ICP 10 70 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 12 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICP 10 IOU ug/L EPA200.7 4/14/10 ESTAFFORD 7439-89-6 Fe by ICP 50 550 ug/L EPA 200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 3.6 mg/L EPA200.7 4114/10 ESTAFFORD 7439-96-5 Mn by ICP 10 59 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 15 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICP 10 IOU ug/L EPA200.7 4/14/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a data !led description of the qualifier codes refer to hja.Lfto;�a..,.�w..e..pr.,sr8NAMya lalLstafinfio%tagM5tstkDatyckmAlt_r Code, «tP.1LP ftj ncdenr orb/}v„e§bmg&YstgnN;J[eckgs,st> Page 1 of 1 County: MCDOWELL Sample ID: AB56689 River Basin �OF W14%9O Gy PO Number# 10GO166 Report To AROAP �O �— Date Received: 04/08/2010 Collector: LAVERTY Time Received: 08:25 p Labworks LoginlD SMATHIS Region: A RO Report Generated: 4/23/10 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW72COATS Collect Date: 04/06/2010 Collect Time: 10.41 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab PQL — Result/ Qualifier 1.7 Units °C Method Reference Analysis Date 4/8/10 Validated by SMATHIS NUT NO2+NO3 as N in liquid 0.02 0.02 U mg/L as N LaC10-107-04-1-c 4/12/10 CGREEN Nitrate as N in liquid 0.02 0.02 U mg/L as N Lachat107-04-1-c 4/13/10 CGREEN Nitrite as N in liquid 0.01 0.01 U mg/L as N Lachat107-04-1-c 4/8/10 CGREEN MET 7429-90-5 Al by ICP 50 52 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-38-3 Ba by ICP 10 97 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 48 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 11000 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 10 mg/L EPA 200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 2100 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 130 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA 200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nrp.1/�orta,aw�,r.ore/web,L iab swL;n/�_qSay.�scaoara ouaiinur co?.P.sshSnlLe rcai.ncdenr ace/wcy�ub/sfa..fi..n,.no/t�<na;z�� Page 1 of 1 County: River Basin Report To MCDOWELL AROAP �pF WArFR p �O Gy Sample ID: PO Number # Date Received: AB56690 10GO167 04/08/2010 Collector: Region: B LAVERTY ARO P Y Time Received: Labworks LoginlD 08:26 SMATHIS Report Generated: 4/23/10 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW13COATS Collect Date: 04/06/2010 Collect Time: 10:51 Sample Depth —A CAS # LAB Analyte Name Sample temperature at receipt by lab PQL — Result/ Qualifier 1.7 Units °c Method Reference Analysis Date 4/8/10 Validated by SMATHIS NUT NO2+NO3 as N in liquid 0.02 0.02 U mg/L as N LaclO-107-04-1-c 4112/10 CGREEN Nitrate as N in liquid 1 0.02 0.02 U mg/L as N Lachat107-04-1-c 4113/10 CGREEN Nitrite as N in liquid 0.01 0.01 U mg/L as N Lachat107-04-1-c 4/8/10 CGREEN MET 7429-90-5 Al by ICP 50 110 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by furnace 2.0 2.0 U ug/L EPA200.9 4/13/10 ESTAFFORD 7440-38-3 Ba by ICP 10 34 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 13 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4112/10 ESTAFFORD 7439-89-6 Fe by ICP 50 470 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 8.7 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 200 ug/L EPA200.7 4/14110 ESTAFFORD 7440-23-5 Na by ICP 0.10 74 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ht°-// 0-0g, C°des <ht°'// mn,l.,cdenr.org/web/wa/lab/swffne°/techassist> Page 1 of 1 County: MCDOWELL Sample ID: AB56691 WATFq River Basin pF p PO Number# 10GO168 Report To AROAP �C3a r Date Received: 04/08/2010 Time Received: 08:25 Collector: B LAVERTY 0 Labworks LoginlD SMATHIS Region: ARID Report Generated: 4/23/10 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59MW13COATS Collect Data: 04/0612010 Collect Time: 1117 Sample Depth CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 °0 4/8/10 SMATHIS MET 7429-90-5 AI by ICP 50 1700 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-38-3 Baby ICP 10 140 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-70-2 Ca by ICP 0.10 74 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 9900 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 47 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 470 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 51 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 21 ug/L EPA200.8 4/12/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 4/12/10 ESTAFFORD SEM 7439-96-5 Semivolatile Organics (BNAs) in liquid _TITLE_ ug/L EPA625/8270/3510 4/12/10 NGOOD 62-53-3 Aniline 12 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 108-95-2 Phenol 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 111-44-4 Bis(2-chloroethyl)ether 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 95-57-8 Chlorophenol, 2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 541-73-1 Dichlorobe nzene, 1,3 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 106-46-7 Dichlorobenzene, 1,4- 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 100-51-6 Benzyl alcohol 20 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 95-50-1 Dichlorobe nzene, 1,2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 95-48-7 Methylphenol, 2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 39638-32-9 Bis(2-chloroisopropyl)ether 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 106-44-5 Methylphenol, 4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 621-64-7 N-nitrosodi-n-propy lam ine 12 Not detected ug/L EPA62518270/3510 4/12/10 NGOOD 67-72-1 Hexachloroethane 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 98-95-3 Nitrobenzene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 78-59-1 Isophorone 12 Not detected ug/L EPA625/8270/3510 4112110 NGOOD Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer tohto:Hwnal.ncd/web/"Aab/staflnft/tea,aisi#Dato n ra r Codes ht •// rtai me / b/ Q/1 b/ mfl h /t chassi t> Page 1 of 3 ', " e. NC(DWQ La6oratorySection Wssults Location ID: 1 P59MW1 3COATS Sample ID: AB56691 Collect Date: 04/06/2010 Collect Time:: 11:17 SEM CAS # 88-75-5 Analvte Name Nitrophenol, 2- PQL 10 , Result/ Qualifier Not detected Units ug/L Method Reference EPA625/8270/3510 Analysis Date 4/12/10 Validated by NGOOD 105-67-9 Dimethylphenol, 2,4- 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 65-85-0 Benzoic acid 50 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 111-91-1 Bis(2-chloroethoxy)methane 12 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD " 120-83-2 Dichlorophenol, 2,4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 120-82-1 Trichlorobenzene, 1,2,4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 91-20-3 Naphthalene(SV) 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 106-47-8 Chloroaniline, 4- 20 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 87-68-3 Hexachlorobutadiene(SV) 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 59-50-7 Chloro-3-methyl phenol, 4- 20 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 91-57-6 Methyl naphthalene, 2- 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 77-47-4 Hexachlorocyclopentadiene 10 Not detected ug/L EPA626/8270/3510 4/12/10 NGOOD 88-06-2 Trichlorophenol, 2,4,6- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 95-95-4 Trichlorophenol, 2,4,5- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 91-58-7 Chloronaphthalene, 2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 88-74-4 Nitroaniline, 2- 50 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 131-11-3 Dimethyl phthalate 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 208-96-8 Acenaphthylene 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 606-20-2 Dinitrotoluene, 2,6- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 99-09-2 Nitroaniline, 3- 50 Not detected ug/L EPA625/8270/3510 4112110 NGOOD 83-32-9 Acenaphthene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 51-28-5 Dinitrophenol, 2,4- 50 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 100-02-7 Nitrophenol, 4- 50 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 132-64-9 Dibenzofuran 10 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 121-14-2 Dinitrotoluene, 2,4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 84-66-2 Diethyl phthalate 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 86-73-7 Fluorene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 100-01-6 Nitroaniline, 4- 50 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 534-52-1 Dinitro-2-methyl phenol, 4,6- 50 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 86-30-6 N-nitrosodiphenylamine 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 101-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 118-74-1 Hexachlorobenzene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 87-86-5 Pentachlorophenol 50 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 85-01-8 Phenanthrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 120-12-7 Anthracene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 84-74-2 Di-n-butyl phthalate 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 20644-0 Fluoranthene 10 Not detected ug/L EPA625/B270/3510 4/12/10 NGOOD 129-00-0 Pyrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 85-68-7 Butylbenzyl phthalate 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 91-94-1 Dichlorobe nzid1ne, 3,3'- 20 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 56-55-3 Benzo(a)anthracene 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 For 8 detailed description of the qualifier codes refer to Mp:JLe.:Lta enr.ora/web!"mAab/staNnB terna�sjnEQSd_RualiBcr [odes <hto:// oartal_nalpnr.ornhveb/wopab/staflnNo/techass Page 2 of 3 )�o NC WQ Laboratory Section [suf Location ID: 1P59MW13COATS Sample ID: AB56691 Collect Date: 04/06/2010 Collect Time:: 11:17 SEM CAS # 218-01-9 Analyte Name Chrysene PQL. — 10 Result/ Qualifier Not detected Units ug/L Method Reference EPA625/8270/3510 An— alygLis Date 4112/10 Validated by NGOOD 117-81-7 Bis(2-ethylhexyl)phthalate 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 117-84-0 Di-n-octyl phthalate 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 205-99-2 Benzo(b)fluoranthene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 207-08-9 Benzo(k)fluoranthene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 50-32-8 Benzo(a)pyrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 193-39-5 Indeno(1,2,3-cd)pyrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 53-70-3 Dibenzo(a,h)anthracene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 191-24-2 Benzo(g,h,i)perylene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD sv1- Hexamethyl cyclotrisiloxane 7 N1 ug/L EPA625/8270/3510 4/12/10 NGOOD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nio•// oartai �caati,Qr�w_�b� , b1st�ry_�;q/tecnass sl iaoa�a_oyAltner Lo�es�t p j-nqRain_sdenr.ora/wep[wyn,,.b/seaeneohechassltL Page 3 of 3 County: MCDOWELL Sample ID: AB56692 River Basin OF WATFq S0� PO Number # 10G0169 Report To AROAP r Date Received: 04/08/2010 Collector: B LAVERTY Y Time Received: 08:25 p Labworks LoginlD SMATHIS Region: ARO Report Generated: 5/6/10 Sample Matrix: GROUNDWATER D ate Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P69MW14COATS Collect Date: 04/06/2010 Collect Time: 11:17 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab PQL — Result/ Qualifier 1.7 Units °C Method Reference Analysis Date 418/10 Validated by SMATHIS MET 7429-90-5 Al by ICP 50 64 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by furnace 2.0 2.2 ug/L EPA200.9 4/13/10 ESTAFFORD 7440-38-3 Ba by ICP 10 130 ug/L EPA200.7 4/14110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 72 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 7200 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 46 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 450 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 50 mg/L EPA 200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4112/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12110 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp•// p n i w /w b/wpA b/ t e fi /t a, •I uo t Qualifier c d he ;// pgftal.,cdenr.org/web/wq/lab/`saFnflo/­techassist> Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARID Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Sample ID: AB74917 OpWA�Fi9 PO Number# ARO jr—I Date Received: 08/09/2011 Time Received: 08:25 0 Y Labworks LoginlD KJIMISON Report Generated: 8/23/11 Date Reported: 11/14/2011 Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW2 Collect Date: 08/08/2011 Collect Time: 09:08 Sample Depth CAS # Analyte Name PQL. Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 6.0 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 6.2 U mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a data [led description of the qualifier codes refer to http•/lportal ncdenr omANebtw(iMab/,Staltnfo/techassist#Deta aualifler codes http'//pOhal ncdenf om/web/we/lab/StaPonfoRPLhaSSI5b Page 1 of 1 County: MCDOWELL Sample ID: AB74918 River Basin �0F w'4rEi9Q PO Number # ARO Report To AROAP �O Date Received: Time Received: 08/09/2011 08:25 Collector: B LAVERTY Y ¢ LoginlD KJIMISON Region: ARIDLabworks Report Generated: 8/23/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Lac. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW2 Collect Date: 0810812011 Collect Time: 09:11 Sample Depth CAS # Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date Validated by Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 1000 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 41100 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detafled description of the qualifier codes refer to httn•l/oorlel nodenr.oratwebfwn4ab/staRnfoAechassist#Data Qualirter Codes <hllp*.//portal.nodenr.omfwebly slab/staflinfoRechassisU Page 1 of 1 County: MCDOWELL Sample ID: AB74928 River Basin �QF WATg19 G7 PO Number# ARO Report To AROAP O r Date Received: 08/09/2011 Collector: B LAVERTY P Y Time Received: 15:55 Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW2 Collect Date: 08/09/2011 Collect Time: 09:05 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 8/9/11 DLEAVITT Turbidity 1 150 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 154 U mg/L APHA25400-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hdp�dportal nrdenr ornAvebfwnNab/staffinfollechassist#Data Qualifier Codes chlto•//nodal nodenrorg/web/wollab/staffnfoltechassist> Page 1 of 1 County: MCDOWELL Sample ID: AB75029 River Basin �QFWA7,F9Q PO Number# 11G0688 Report To AROAP f�0 Y r' Date Received: 08111/2011 Collector: B LAVERTY j �C Time Received: 08:00 p Labworks LoginlD HMORGAN Region: ARO Report Generated: 9/12/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID`. 1P59COATSMW2 Collect Date: 08/09/2011 Collect Time: 09:05 Sample Depth CAS # Analvte Name LAB PQL. Result/ Units Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.9 °C 8/11/11 DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7429-90-5 AI by ICP 50 1300 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-38-3 Ba by ICP 10 89 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-70-2 Ca by ICP 0.1 23 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 12 ug/L EPA 200.8 8/15/11 ESTAFFORD1 7439-89-6 Fe by ICP 50 9100 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1/11 ESTAFFORDI 7440-09-7 K by ICP 0.1 1.1 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 12 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-96-5 Mn by ICP 10 686 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-23-5 Na by ICP 0.1 11 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-02-0 Ni by ICPMS 2 5.7 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-92-1 Pb by ICPMS 2 19 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 33 ug/L EPA 200.8 8/15/11 ESTAFFORDI Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to http•Uportal nodenr omMeb/wa/fab/staffinfoftechassist#Data Qualifier Codes <http•//nonal ncdenr oroAveb/wo/lab/staffinfo/techassist> Page 1 of 1 County: MCDOWELL Sample ID: AB74919 River Basin F WA PO Number # ARO Report To AROAP �11 G Date Received: 08/09/2011 r Collector: B LAVERTY j — Y Time Received: 08:25 Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW10 Collect Date: 08/08/2011 Collect Time: 09:26 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 1.9 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended In liquid 6.2 6.2 U mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to httrr//Portal ncdenr om/webhvn/lab/staRinfo/terhassist#Dato Quallfier Codes <h0a'/Poonal ncdenr oro/webiwa/lab/staflinfo/teehassist> Page 1 of 1 County: MCDOWELL Sample ID: AB74929 River Basin �OF NlATF9Q PO Number # ARID Report To AROAP .O Date Received: 08/09/2011 Collector: LAVERTY Time Received: 15:55 p Labworks LoginlD KJIMISON ARID RO Report Generated: 8/23/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Lac. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW10 Collect Date: 08/09/2011 Collect Time: 09:15 Sample Depth Result/ Method Analysis CAS # Analvte Name PQL Units Validated by — Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 8/9/11 DLEAVITT Turbidity 1 7.0 NTU APHA2130B-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 15 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description oflhe qualifier codes referlo http�l/oortalnrAenrornhvebhveAab/statriinfottoaassist#gala Qualifier Codeschttp7/podalnWenrorelweblwollab/staffnfo/techasslst> Page 1 of 1 County: MCDOWELL Sample ID: AB75030 River Basin WAiQ QG� PO Number# 11G0689 Report To AROAP �O� r Date Received: Time Received: 08/11/2011 08:00 Collector: B LAVERTY P Y Labworks LoginlD HMORGAN Region: ARID Report Generated: 1 Sample Matrix: GROUNDWATER Date Reported: 1/14/2011 1 1/14 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: IP59COATSMW10 Collect Date: 08/09/2011 Collect Time: 09:16 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by - Qualifier Reference Date LAB Sample temperature at receipt by lab 1.9 °C 8/11/11 DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7429-90-5 Al by ICP 50 180 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/18/11 ESTAFFORDI 7440-38-3 Ba by ICP 10 31 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 0.20 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-47-3 CrbylCPMS 10 11 ug/L EPA260.8 8/15/11 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 4.3 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-89-6 Fe by ICP 50 350 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1/11 ESTAFFORDI 7440-09-7 K by ICP 0.1 0.46 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-95-4 Mg by ICP 0.1 0.10 U mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-96-5 Mn by ICP 10 10 U ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-23-5 Na by ICP 0.1 45 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 10 U ug/L EPA 200.8 8/15/11 ESTAFFORDI Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to http'llnortal ncdenr orotweb'wn/lab/staRnfottechassist#Data Qualifier Codes <htloWportal node nr orrilwebWgilablstaff nfoltechassist> Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Sample ID: AB74920 OFVlA1Ff9 PO Number# ARO Date Received: 08109/2011 Time Received: 08:25 p Y Labworks LoginlD KJIMISON Report Generated: 8/23/11 Date Reported: 11/14/2011 Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P69COATSMW11 Collect Date: 08/08/2011 Collect Time: 09:39 Sample Depth CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 4.5 NTU APHA213013-20th 8/10111 CGREEN Residue —Suspended in liquid 6.2 6.2 U mg/L APHA2640D-20th 8/9/11 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 For a detailed description of the qualifier codes refer to htla'f/portal ncdenr omAvebhvo/lab/stafflnfo/techassist#Data Qualifier Codes <http://Portal.nodenr.org/weblwq/lablstaffinfo/techa5sist> Page 1 of 1 County: MCDOWELL Sample ID: AB74930 River Basin �oF wAT �Y PO Number# ARO Report To AROAP �O Date Received: 08/09/2011 j Time Received: 15:55p Collector: B LAVERTY I Labworks LoginlD KJIMISON Region: ARO Report Generated: 8123/11 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59C0ATSMW11 Collect Date: 08/0912011 Collect Time: 09:31 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 8/9/11 DLEAVITT Turbidity 1 1.9 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 6.5 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a detailed description ofthe qualifier codes refer to htto'lfportal ncdenr ornMeb/wgAab/staffinfottechassist#Data Qualifier Codes <htlp•Hporlal ncAenr ora/web/wgilab/staf8nfo/techasslst> Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARID Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No `O�CF�W ATF,9QG > a -c VisitlD Loc. Descr.: COATS AMERICAN Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: AB75031 11G0690 08/1112011 08:00 HMORGAN 9/12/11 11/14/2011 Location ID: IP59COATSMWII Collect Date: 08/09/2011 Collect Time: 09:31 Sample Depth CAS # Analyte Name LAB PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.9 °C 8/11/11 DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-38-3 Ba by ICP 10 100 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-70-2 Ca by ICP 0.1 26 mg/L EPA 200.7 8115/11 ESTAFFORDI 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8/16/11 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 7.9 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-89-6 Fe by ICP 50 2000 ug/L EPA 200.7 8115/11 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1/11 ESTAFFORDI 7440-09-7 K by ICP 0.1 6.3 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 9.1 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-96-5 Mn by ICP 10 590 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-23-5 Na by ICP 0.1 77 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-02-0 Ni by ICPMS 2 2.0 U ug/L EPA 200.8 8/15111 ESTAFFORDI 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 8/15111 ESTAFFORDI Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description of the qualifier codes referto hdnYlcortal ncdenr.oroAveblwn4ab/stafFnfoflechassist#Data Qualifier Codes<http://Po.lai.nodenr,ofglwebAwm;iab/staffinfoltechassiL> Page 1 of 1 County: MCDOWELL Sample ID: AB74921 River Basin pF WATF� QGy PO Number # ARO Report To AROAP �O� r Date Received: 08/09/2011 Collector: B LAVERTY P Time Received: 08:25 Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23/11 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1 P59COATSMWI 2 Collect Date: 0810812011 Collect Time: 09:48 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units Validated by — Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/22/11 CGREEN Turbidity 1 120 NTU APHA213OB-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 26 mg/L APHA2540D-20th 819/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htt 'ttoortal nrdenr oM Meb/wg4ab/stafrinfotterhassist#Data Qualifier Codes 011o7/oonal ncdenr oralweblwgilabfstaffnfo/lechassist> Page 1 of 1 County: MCDOWELL Sample ID: AB74931 River Basin Report =ppWATFgp Gy PO Number# ARO To AROAP �O r Date Received: 08/09/2011 Collector: B LAVERTY Time Received: 16:55 p Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Lotion I caD: 1P59COATSMWI2 Collect Date: 08/09/2011 Collect Time: 09:42 Sample Depth CAS # Analyte Name PQL Result/ Units Method Analysis Validated by — Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 8/22111 CGREEN Turbidity 1 120 NTU APHA2130B-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 17 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htin•llportal ncdenrorntwebfwn/lab/stamnfo/techassist#Data Qualifier Codes <httoWportaI.node nr.oralwebnvallab/staffinfoltechasslst> Page 1 of 1 County: MCDOWELL Sample ID: AB75032 River Basin pF 1NATF9 QGy PO Number # 11G0691 Report To AROAP �O� Date Received: 08111/2011 Collector: B LAVERTY j Time Received: 08:00 p -'Ic Labworks LoginlD HMORGAN Region: ARID Report Generated: 9/12/11 Sample Matrix: GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: IP59COATSMW12 Collect Date: 08/09/2011 Collect Time: 09:42 Sample Depth CAS # Anal rite Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.9 'C 8/11/11 DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7429-90-5 Al by ICP 50 90 ug/L EPA 200.7 8115/11 ESTAFFORDI 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-38-3 Ba by ICP 10 110 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 47 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 6.5 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-89-6 Fe by ICP 50 7900 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 9/1/11 ESTAFFORDI 7440-09-7 ` K by ICP 0.1 4.4 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 9.8 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-96-5 Mn by ICP 10 1900 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-23-5 Na by ICP 0.1 190 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7440-02-0 Ni by ICPMS 2 7,7 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7782-49-2 Se by ICPMS 5 6.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 8/15/11 ESTAFFORDI Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 For a detailed description of the qualifier codes refer to httniuoortel ncdenr omlweb/wnllab/stafflnfo/terhassist#Data Qualifier Codes <htta:Uaortal ncdenr om/web/wo/lab/stafBnfoltechassisi> Page 1 of 1 County: MCDOWELL Sample ID: AB74922 River Basin �0F WAT�Ap PO Number # ARO Report To AROAP �O G Date Received: 08/09/2011 r Collector: B LAVERTY j Y Time Received: 08:25 Region: ARO p Labworks LoginlD KJIMISON Sample Matrix: GROUNDWATER Report Generated: 8/23/11 L oc. Type: MONITORING WELL Date Reported: 11/14/2011 Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID. 1P59COATSMW13 Collect Date: 08/0812011 Collect Time: 09:54 Sample Depth CAS # Analyte Name Others PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 25 NTU APHA213013-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 34 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hdD:uoortal nedenr.ore/webfwo/lab/staHinfo/techassist#Data Qualifier Codes<htto://Dortal.nodenr.oro/webbvanab/staffinfottechassisb Page 1 of 1 County: MCDOWELL Sample ID: AB74923 River Basin Report To �OF WATFgQ G PO Number# ARID AROAP �O Date Received: 08/09/2011 C Collector: B LAVERTY > Y Time Received: 08:25 Region: ARID 0 Labworks LoginlD KJIMISON Sample Matrix: GROUNDWATER Report Generated: 8/23/11 Loc. Type: MONITORING WELL Date Reported: 11/14/2011 Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW14 Collect Date: 08/08/2011 Collect Time: 10:00 Sample Depth CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 80 NTU APHA2130B-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 47 mg/L APHA2540D-20th 8/9111 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description ofthe qualifier codes refer to hftn7loortal.nedenr.om/web/wa/lab/staffinfo/techossist#Data Qualifier Codes<http://portal.nodenr.org/webAvq/lab/stafrmfoltechasstst> Page 1 of 1 County: MCDOWELL Sample ID: AB74932 River Basin A—ZlyPO OG9 Number# ARO Report To AROAP r- Date Received: Time Received: 08/0912011 15:55 Collector: 8 LAVERTY 40F;-W 0 0 Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23111 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW14 Collect Date: 08/09/2011 Collect Time: 10:12 Sample Depth Result/ Method Analysis CAS # Analvte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 8/9/11 DLEAVITT Turbidity 1 40 NTU APHA21308-20th 8/10/11 CGREEN Residue —Suspended In liquid 6.2 16 mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description of the qualifier codes refer to hffp�liportal nedenr omMeblwgnablstaffinfoAechassist#Data Qualifier Codes <http://Portal-nodenr.org/weblwq/lab/staffinfoltechasslst> Page 1 of 1 County: MCDOWELL Sample ID: AB75033 River Basin wArF9 QG� PO Number # 11G0692 Report To AROAP `OCR l Date Received: 08/1112011 Time Received: 08:00 Collector: B LAVERTY < Labworks LoginlD HMORGAN Region: ARO Report Generated: 9/12/11 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Dew.: COATS AMERICAN Location ID: 1P59COATSMWI4 Collect Date: 08/09/2011 Collect Time: 10:12 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab PQL - Result/ Qualifier 1.9 Units °C Method Reference Analysis Date 8/11111 Validated by DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7429-90-5 Al by ICP 50 62 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-38-3 Ba by ICP 10 110 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-70-2 Ca by ICP 0.1 69 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-50-8 Cu by ICPMS 2 18 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-89-6 Fe by ICP 50 5800 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 911/11 ESTAFFORDI 7440-09-7 K by ICP 0.1 1.2 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-95-4 Mg by ICP 0.1 44 mg/L EPA 200.7 8/15/11 ESTAFFORDI 7439-96-5 Mn by ICP 10 990 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-23-5 Na by ICP 0.1 50 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 2.5 ug/L EPA 200.8 8115/11 ESTAFFORD1 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 101.1 ug/L EPA 200.8 8/15/11 ESTAFFORD1 Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a detailed description of the qualifier codes refer to he.rrraottal ncdenr orn/web/wq/IablstatBnfoitechassist#Deta Qualifier Codes <htto•//Portal ncdenr orgt ebiwa/lab/staffinfo/techassist> Page 1 of 1 County: MCDOWELL Sample ID: AB74924 River Basin Report To AROAP �Q�C WAr iQQ PO Number# ARID O Date Received: 08/09/2011 r Collector: B LAVERTY } Y Time Received: 08:25 Region: ARO Labworks LoginlD KJIMISON Sample Matrix: GROUNDWATER Report Generated: 8/23/11 .Loc. Type: MONITORING WELL D ate Reported: 11/14/2011 Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW15 Collect Date: 08/0812011 Collect Time: 10:09 Sample Depth CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1'.1 °C 8/9/11 DLEAVITT Turbidity 1 15 NTIJ APHA2130B-20th 8/10/11 CGREEN Residue —Suspended In liquid 6.2 6.2 U mg/L APHA2540D-20th 8/9/11 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a detailed description of the qualifier codes refer to http:llportal.nedenr.ornAveb/WaAab/staff ilfollechassfsl#Data Qualifier Codes <htto://portal.nedencomfwebnvollab/staffnfo/techassist> Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Ok Wq�$ Sample ID: AB94211 PO Number# 13GO266 Date Received: 04111/2013 > Time Received: 08:00 Labworks LoginlD HMORGAN Final Report Date: 4/22/13 Final Report Report Print Date: 05/16/2013 VisitlD Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC F E C E I"I.4U Location ID: 1P59COATSMW2 I Collect Date: 04/09/2013 1 Collect Time: 09:22 ; 1 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory puri CAS # Analyte Name PQL Result/ Units Method Qualifier Reference LAB Sample temperature at receipt by lab VOL 2.0 'C Office uifer Protection --- " Validated by Date 4/11/13 HMORGAN Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 1.6 ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-55-6 1, 1, 1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/62416260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8250 4/11/13 ACHANDLER 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 10061-02-6 trans- 1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to bsp,/[ ttxrca!,ns�gn.;plp,(w«_ynii�y�(.slaPn...�l;sh?:a=!&t.R1:133=..q;,x;!,ggr coee: <n�P;((pgrEai nc Gnr;crp,[; wq(ian(�caFlgfip(recnas,,,isr;, Page 1 of 2 XC cDWQ Laboratory Section Wsufts Location ID: 1P59C0ATSMW2 Sample ID: AB94211 Collect Date: 04/0912013 Collect Time:: 09:22 VOL Result/ Method AnatV CAS # Analyte Name PQL Units Validated by - Qualifier Reference Date 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-4174k,' , Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropyl benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-67-8 1,3,5-Trimethyl benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to n:,: ;r q.3rpai.ncge2r,q�g(�q«L/�cq!'z!�/s!afinR,c/techxss,L_tpDeta ggmq codgs <ntE[J gr:.a�.ncde,r.crpdye_n.,/vrq n(, ;flr5o�tgchppsist> Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code: 1 P59CoatsMW2 County: McDowell Quad Serial No. Lonq. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) X Routine ❑ Soil ❑ Emergency 1 ❑ Other ❑ Chain of Custody Lab Number Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:22 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American (circle one) pH 40o Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Temp.lo °C Odor Description of sampling point: Monitoring Well MW2 Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO,asN) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 ug/L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc46567 u /L 4Silica Organ chlorine Pesticides Organo hos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAs Boron Semivolatile Organics TPH-Diesel Ran e x Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): County: MCDOWELL V4ArZ� Sample ID: AB94212 River Basin U� %- PO Number # 13GO266 Report To AROAP �O� Date Received: 04/11/2013 Time Received: 08:00 Collector: B LAVERTY Labworks LoginlD HMORGAN Region: ARO - Final Report Date: 5/9/13 Sample Matrix: GROUNDWATER WELL Final Report Report Print D Lac. Type: MONITORING � � _ 4liyCl^ Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION N JUL e 2013 Location ID: 1P59COATSMW70 Collect Date: 04/09/2013 Collect Time; 09:3 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purpA Lslifer Protection Result/ Method Analysis CAS # Analyte Name PQL Qualifier Units Reference Validated by Date LAB Sample temperature at receipt by lab 2.0 °C 4/11/13 HMORGAN MET 7440-47-3 Cr- Dissolved. Chromium by ICPMS 10 IOU ug/L EPA 200.8 4/18/13 ESTAFFORD1 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 4/16/13 ESTAFFORD1 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORD1 7429-90-5 B by ICP 50 84 ug/L EPA200.7 4/18/13 ESTAFFORD1 7440-38-3 Ba by ICP 10 IOU ug/L EPA200.7 4/15/13 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 0.45 mg/L EPA200.7 4/15/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 4118/13 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.6 ug/L EPA200.8 4/18/13 ESTAFFORD1 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 4116/13 ESTAFFOKU1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 4/17/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 0.36 mg/L EPA200.7 4/15/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 0.20 mg/L EPA200.7 4/15/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 IOU ug/L EPA200.7 4/16/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 58 mg/L EPA200.7 4/15/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORD1 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 4118/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U J2 ug/L EPA200.8 4/18/13 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 4/18/13 ESTAFFORDI VOL 7429-90-5 Volatile Organics in liquid _TITLE_ ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-01-4 Vinyl Chloride 0:50 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nm:((.nor,_ai:�caenr crP,(xan/y;�iiat(spar.�fio/tr�nass,tg.[.�a;3 c ua�tne. Cp�ps<htp;/(,parq;�l,;nNenr.o;,gJw.eh(wq(?ah[stafirSolLeShasssi � Page 1 of 3 NC (DWQ Laboratory Section �Rfsufts Location ID: 1P59COATSMW10 Sample ID: AS94212 Collect Date: 04/09/2013 Collect Time:: 09:33 VOL CAS # Analyte Name PQL Result/ Units Method Ana[sis Validated by Qualifier Reference Date 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 1634-04-4 "Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-97-5 B'omoehlordm`ethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichlorop'ropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 107-06-2 _ _1;2-Dichloroethane' 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-55-6 1, 1, 1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER' 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-38-3 map-Xylene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed deSCAplIOo or the qualifier codes refer to heP, qor;A! _..... ;crq,(.nebL �,fla�jspannP.o/hchassstttt?aca Cjuxlifier Cnd«z <htF4! y�rtz!„nrd=pr,ory!giebjwg(:ab�a5_r.5o(te hays yT Page 2 of 3 NC 0WWQ Laboratory Section qi�fsufts Location ID: IP69COATSMWIO Sample ID: AB94212 Collect Date: 04/09/2013 Collect Time:: 09:33 VOL Result/ Method Anal sis CAS # Analyte Name PQL Units Validated by — Qualifier Reference Date 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Sample Comments MET:Thallium-J2-estimated-QC failure due to CI inter. from 3030C digestion. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hSe.; Lp.3.?1:^..sdftin�.R!rla•^-.P1.5• allablf.5?.fl^_AJ[esh�tt!39�`33a_.Slui!1.9er cog;: py,�porca., ,pesr,o_rp� n[yvq[i,?n[s_a=rno/f�sna:s m_ Page 3 of 3 County: MCDOWELL VqA Sample ID: AB94247 River Basin QF �?� PO Number # ARO Report To AROAP �'r+ vy Date Received: 04/1012013 Collector: B LAVERTY "I Time Received: 08:30 Labworks LoginlD KJIMISON Region: ARO Final Report Date: 4/22/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 05116/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: Location ID: 1P69COATSMW10 Collect Date: 04/0912013 Collect Time: 09:33 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.6 °C 4/10/13 RBYRD Turbidity 1 1 U NTU APHA21308-20th 4110/13 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description of the qualifier codes refer to hcg/j.e_�rtal;a�ge�r.r,�jweGhvq_ jslafin/1;Lchays!s{aba:z Qu�1 1 Cod: to:J: o°rtai.ncd=rtccrzlwah?wNlabl;tafin5�=:nasssr> Page 1 of 1 North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: 1 P59CoatsMW10 SAMPLE TYPE SAMPLE PRIORITY County: McDowell Water (Ground Water) X Routine Lab Number El soil El Emergency Quad No Serial No. Date Received Time: Lat. Long. ❑ Other Rec'd By: From:Bus, Courier, Hand Del., ❑ Chain of Custody Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:33 AM Baseline, Complaint, Com liance LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES �(circleone) PH 400 Spec. Cond.94 at 250C Temp.lo °C Odor Appearance DO, mg/L ORP, mV Field Analysis By: LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal31616 /loom[ Coliform: MF Total 31504 /10oml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 cu Cyanide 720 mg/L Lab Comments Owner: Coats American Location or Site: 630 American Thread Road Marion, NC Description of sampling point: Monitoring Well MW10 Sampling Method: External Well Pump Remarks Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Sample Interval (Pumping time, air temp., etc.) Ag-Silver 46566 ug/L AI -Aluminum 46557 ug/L X As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 u /L X Cr-Chromium 46559 u /L X Cu-Copper 46562 u /L X Fe -Iron 46563 u /L X Hg-Mercury 71900 u /L X K-Potassium 46555 m /L X Mg -Magnesium 46554 m /L X Mn-Manganese 46565 u /L X Na-Sodium 46556 m /L Ni-Nickel u /L X Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Please add thallium Silica Organochlorine Pesticides Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAs X Boron Semivolatile Organics TPH-Diesel Range X Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (IC): North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: 1 P59CoatsMW10 County: McDowell Quad No Serial No SAMPLE TYPE SAMPLE PRIORITY DC Water (Ground Water) DC Routine ❑ Soil ❑ Emergency 2 ❑ Other El Chain of Custody Lab Number Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, I'' �I Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:33 AM Baseline, Complaint, Com liance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American (circleone) pH 400 Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Temp.10 eC Odor Description of sampling point: Monitoring Well MW10 Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom[ Coliform: MF Total 31504 /100ml 'TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 cu Cyanide 720 mg/L Lab Com Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 ug/L AI -Aluminum 46557 ug/L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Silica Organochlorine Pesticides Organo hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAs Boron Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): County: MCDOWELL WAT� Sample ID: AB94213 River Basin O 1,7G PO Number # 13GO267 �� Report To AROAP r. Date Received: 04/11/2013 a Time Received: 08:00 Collector: B LAVERTY Labworks LoginlD HMORGAN Region: ARO Final Report Dat 5/9/13 Sample Matrix: Loc. Type: GROUNDWATER MONITORING WELL Final Report Report Print Dat : 51 6/201 f �, Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, N i JUL I j 20i� Location ID: lP59COATSMWIIR Collect Date: 04/09/2013 Collect Time: 09:46 SAFS@rh0A D_gP3t,; _ __, If this report is labeled preliminary report, the results have not been validated. Do not use for fifer CAS # LAB Analvte Name Sample temperature at receipt by lab PQL Result/ Qualifier 2.0 Units °C Method Reference Analysis Date 4/11/13 Validated by HMORGAN MET 7440-47-3 Cr- Dissolved Chromium by ICPMS 10 IOU ug/L EPA 200.8 4/18/13 ESTAFFORDI 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 4/16/13 ESTAFFORD1 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7429-90-5 B by ICP 50 50 U ug/L EPA200.7 4/18/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 53 ug/L EPA200.7 4/15/13 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 47 mg/L EPA200.7 4/15113 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 4/18/13 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.0 ug/L EPA200.8 4/18/13 ESTAFFORD1 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 4/16/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 4/17113 ESTAFFORDI 7440-09-7 K by ICP 0.10 2.7 mg/L EPA 200.7 4/15/13 ESTAFFORD1 7439-95-4 Mg by ICP 0.10 19 mg/L EPA200.7 4/15/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 IOU ug/L EPA200.7 4/16/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 17 mg/L EPA200.7 4/15/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/18/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U J2 ug/L EPA200.8 4/18/13 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 14 ug/L EPA200.8 4/18/13 ESTAFFORD1 VOL 7429-90-5 Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to riplL.e9ra!;nc,ggq.�,c�(weg/w3!!ash;,.ry.,n@sJ«sh�ts!nSH4ASaS1:.:1�fi.:r Ss�.^.-.t!hse:/La:!Sal.:nn?egr;o,{p,(�yeb[wq(,i_ah[}jafinfic[techassish Page 1 of 3 .NC OWQ La6oratory Section 1&sufts , Location ID: 1P59COATSMW11R Sample ID: AB94213 Collect Date: 04/09/2013 Collect Time:: 09:46 ► OH Result/ Method Analysis CAS # Analyte Name P L. Units Validated by Qualifier Reference Date 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-59-2 CIS-1,27Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-97-5 Bromochlo�omethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER' 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 95-63-6 1,2,4-Trimethyl benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp11-ppr!al,nc.�1,end,FG;L•nab(�;,�/lap(s;aryPFpJtephzsLtaDa:a dps!it@.e_,_con«$,�htp;/[,ynrca),ncnenr,crR/,p�.en!wg[(�h[scar,,,nt,,,o[eecna,;s�,xer Page 2 of 3 NC (DWWQ Laboratory Section 9?psufts Location ID: 1P69COATSMW11R Sample ID: AB94213 Collect Date: 04/09/2013 Collect Time:: 09:46 VOL CAS# 135-98-8 Analvte Name sec-Butylbenzene PQL 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 4/11/13 Validated by ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-46-7 p-Dichlorobenzene(1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-61-6 1,2,3-Trichlorobe nzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Sample Comments MET:Thallium-J2-estimated-QC failure due to Cl inter. from 3030C digestion. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a detailed description of the qualifier codes refer to net;[(,ngrpgf,ncdxnr;grpfuephyglla!��s;afinfic/tg hssi;tnt)ata gp�!ifi;r C;n�es,<hpppJ�portai,,pcAenr;org/�yeg[w�(la¢(ztaSnF.o[tgchags!st_ Page 3 of 3 County: MCDOWELL `NArg9 Sample ID: AB94248 River Basin 0� QG PO Number # ARID Report To AROAP '�� 43' Date Received: 04/10/2013 Time Received: 08:30 Collector: B LAVERTY LoginlD KJIMISON Region: ARIDLabworks Final Report Date: 4/22/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 05/16/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P59C0ATSMW11R Collect Date: 04/09/2013 Collect Time: 09:46 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.6 °C 4110/13 RBYRD Turbidity 1 1.1 NTU APHA2130B-20th 4110/13 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer tou�Jljt_ re.:[:,�urtai;ntden_,tg/woL/y,,g;'la,�(},!aHrl=o(tech.,is !_(uData _C}r Cpd?e <htpJ;,portal,;nr�lgnr;orp,(e�eh(wg[(y,n[ztd finit ^o[tPchaay_ Page 1 of 1 North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and- Natural Resources - DIVISION OF WATER QUALITY -GROUNDWATER SECTION 4 Location code: 1 P59CoatsMW11 R SAMPLE TYPE SAMPLE PRIORITY County: McDowell X Water (Ground Water) DC Routine Lab Number El soil El Emergency Quad No Serial No. El Other Date Received Time: Lat. Long. Rec'd By: From:Bus, Courier, Hand Del., ❑ Chain of Custody Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:46 AM Baseline, Complaint, Compliance) LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American `circle one) pH 400 Spec. Cond.94 at 25°C Location or Site: 630 American Thread Road Marion, NC Temp.lo °C Odor Description of sampling point: Monitoring Well MW11R Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.6 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 pMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 u /L X As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L X Cr-Chromium 46559 u /L X Cu-Copper 46562 u /L X Fe -Iron 46563 u /L X Hg-Mercury 71900 u /L X K-Potassium 46555 m /L X Mg -Magnesium 46554 m /L X Mn-Manganese 46565 u /L X Na-Sodium 46556 m /L Ni-Nickel u /L X Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Please add thallium Silica Organochlorine Pesticides Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAS X Boron Semivolatile Organics TPH-Diesel Range X Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: 1 P59CoatsMW11 R County: McDowell Quad No Serial No SAMPLE TYPE SAMPLE PRIORITY X Water (Ground Water) X Routine ❑ Soil ❑ Emergency 3 ❑ Other ❑ Chain of Custody Lab Number Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, I'' 'I Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:46 AM Baseline, Complaint, Compliance) LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American `circle one) pH 40o Spec. Cond.94at 250C Location or Site: 630 American Thread Road Marion, NC lo Temp.°C Odor Description of sampling point: Monitoring Well MW11 R Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom[ Coliform: MF Total 31504 /loom[ TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 ug/L As -Arsenic 46551 ug/L Ba-Barium 46558 ug/L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc46567 u /L Silica Organochlorine Pesticides Organophos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAs Boron Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): County: MCDOWELL WATF� Sample ID: AB94214 River Basin O& C1� PO Number # 13GO268 Report To AROAP Date Received: 04/11/2013 Time Received: 08:00 Collector: B LAVERTY `r Labworks LoginlD HMORGAN Region: ARO Final Report Date: 4/22/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 07/18/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P69COATSMWI2 I Collect Date: 04/09/2013 Collect Time: 10:00 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # AnalYte Name PQL Result/ Units Method Analysis sis Validated by Qualifier. Reference Date LAB Sample temperature at receipt by lab 2.0 °C 4/11/13 HMORGAN VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA6030/624/8260 4/11113 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected u9/L EPA5030/624/8260 4/11/13 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 156-60-5 trans- 1,2-Dich loroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ALHANULtK Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore detailed description of the qualifier codes rater to r,�p,:/,!.FGnei,:genr,,4tp��_ylaPl_al?fle�Le=.�t��FBaata_q; x;�r.,.er coaep <n�pl1syr;n)„�n(e.�r;9ffL1LqPL_�tl�n[;Sargfi;1ecnxzi:o Page 1 of 2 NC (DWQ La6oratory Section W§sults Location ID: 1P69COATSMWI2 Sample ID: AB94214 Collect Date: 04/09/2013 Collect Time:: 10:00 VOL CAS # 142-28-9 Analyte Name 1,3-Dichloropropane PQL - 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 4/11113 Validated by ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-90-7 Chlorobenzene 0.25 0.59 ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 0.42 ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 9549-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 135-98-8 sec -Butyl benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-61-6 1,2,3-Trichlorobe nzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to h;q/[,portatncgear„or,(wep(�yqrtan,/s;,aRnn.�y;e'r,assiegnpga„gurlr:r_tg<s,<n;p;/(,;,r..;a).:.te..epr,,os/;xen;.u�;lzni.,;aq;�soL•Ps^assist; Page 2 of 2 North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: 1 P59CoatsMW12 SAMPLE TYPE SAMPLE PRIORITY County: McDowell X Water (Ground Water) DU Routine Quad No Serial No. ❑ Soil ❑ Emergency Lat. Long. ❑ Other El Chain of Custody Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: 0 Lab Number Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Data Entry By: Ck: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 10:00 AM Baseline, Complaint, Compliance LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American (circle one) PH 40o Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Temp.to IC Odor Description of sampling point: Monitoring Well MW12 Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 pMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. (Pumping time, air temp., etc.) Ag-Silver 46566 ug/L AI -Aluminum 46557 ug/L As -Arsenic 46551 ug/L Ba-Barium 46558 ug/L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Silica JUL 1 % 2013 Organochlorine Pesticides Organo hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAs Boron Semivolatile Organics TPH-Diesel Range X Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): Asheville Regional Office — Aquifer ftlftfion_ _ County: River Basin Report To AROAP Collector: B LAVERTY Region: ARID Sample Matrix: BLANKWATER Loc. Type: TRIP BLANK Emergency Yes/No COC Yes/No A 0� '9�v y C3 � Final Report VisitlD Loc. Descr.: VOA TRIP BLANK Sample ID: AB94210 PO Number# 13GO264 Date Received: 04/11/2013 Time Received: 08:00 Labworks LoginlD HMORGAN Final Report Date: 4/22/13 Report Print Date: 07118/2013 � V E IV Location ID: VOATRIPBLANK I Collect Date: 04/09/2013 I Collect Time: 07:61 I Sample Depth +i If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory! a pose quit ilie Regional Protl Office Aquifer Pratecti®I ) Result/ Method Analysis Validated by CAS # Analvte Name PQL Qualifier Units Reference Date LAB Sample temperature at receipt by lab 2.0 °C 4/11/13 HMORGAN VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-60-5 trans- 1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 10061-02-6 trans- 1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to n; ;ll.2?rtai ;nc[1,enr;gryfweG/��_ ;yf;ta(jn�,p/techx _s!stNltatd C;ga!Ifier C� ez, tpp// po„r[ai_ncCem.pp(g,e6L;_g(xh[stafiaJ.tS cnasssr_ Page 1 of 2 NC DWQ Gafioratory Section �sufts Location ID: VOATRIPBLANK Sample ID: AB94210 Collect Date: 04/09/2013 Collect Time:: 07:61 VOL CAS # 142-28-9 Analyte Name 1,3-Dichloropropane PQL - 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 4/11/13 Validated by ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-93-4 .. .(EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8280 4/11/13 ACHANDLER 100-41-4 i r:l, fthylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/824/8280 4/11/13 ACHANDLER 108-38-3 m,p-Xylene . ... 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-06-6 tert-B utyl benzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 120-82-1 1,,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description oft he qualifier codes refer to htoll_norca(:ncdenrprs(N:«e/,..�pae(�pq.ryppo/eesnassl�tn�a;a_nuaurie. Cqd?s <htp(/J,portal_rig.t �.;o, ;4�gA 7Ltafin- gtte ha;sst. Page 2 of 2 1 North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: VOA Trip Blank SAMPLE TYPE SAMPLE PRIORITY County: Water Ground Water X Routine Ixl ( ) Lab Number Quad No Serial No. ❑ Soil ❑ Emergency TB Date Received Time: Lat. Long. ❑ Other Rec'd By: From:Bus, Courier, Hand Del., ❑ Chain of Custody Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 7:51 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: VOA Trip Blank �(circleone) pH 40o Spec. Cond.94 at 250C Location or Site: Temp.lo °C Odor Description of sampling point: Appearance DO, mg/L ORP, mV Sampling Method: Sample Interval Field Analysis By: Remarks I ARCIRATC)RYANAI YRFS (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom[ Coliform: MFTotal 31504 /loom[ TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Com Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 uMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L PO4 as P NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L NH4 - ammonium GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 ug/L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Silica Or ano hos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs MBAS Boron Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (IC): County; ,MCDOWELL O�.\NA Sample ID: AC00648 River Basin PO Number # 13GO783 Report To AROAP �y r Date Received: 09/25/2013 Collector: B LAVERTY "I Time Received: 08:15 Labworks LoginlD MSWIFT Region: ARO Final Report Date: 10/16/13 Sample Matrix: GROUNDWATER 'Final Report Report Print Date: 11/15/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION, NC Location ID: I P59COATSMWI 0 Collect Date: 09/23/2013 Collect Time: 11:11 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # LAB Analyte Name Sample temperature at receipt by lab P L Result/ Qualifier 1.6 Units °C Method Reference Analysis Date 9/25/13 Validated by HMORGAN MIC Turbidity 1.0 1 U NTU APHA2130B-20th 9/25/13 ESTAFFORD1 WET Residue -Suspended in liquid 6.2 12 U,P mg/L APHA2540D-20th 9/26/13 CGREEN MET 7440-22-4 Ag by ICPMS 1.0 14 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7429-90-5 AI by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORD1 7429-90-5 B by ICP 50 150 ug/L EPA200.1 1018/13 ESTAFFORD1 7440-38,3 Ba by ICP 10 11 ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 0.20 mg/L EPA200.7 10/3/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 1011/13 ESTAFFORD1 744047-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 1011/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 1013/13 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/10/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 0.36 mg/L EPA 200.7 10/3/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 0.10 U mg/L EPA200.7 10/3113 ESTAFFORD1 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA200.8 10/3/13 ESTAFFORDI 7440-23-5 Na by ICP 0A0 40 mg/L EPA200.7 10/3/13 ESTAFFORDI 7440-02-0 Ni.by ICPMS 2.0 2.0 U ug/L EPA200,8 10/1/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7782-49-2 Se by ICPMS,, 5.0 6.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 10/1/13 ESTAFFORDI VOL 7440-50-8 Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the quallFler codes refer toonaLnmenr.ors,+wet/y,.�nas,•;ptaflnflq[5rcnxsslsta12ata.. q,;.aiiner odes<ntF;Lf..ya[Sai.nccien..:o:,;/wen(wupan(statnto({echas.Fisc Page 1 of 3 NC (D WQ Laboratory Section Wssufts Location ID: 1P59COATSMW10 Sample ID: AC00648 Collect Date: 09/23/2013 Collect Time:: 11:11 VOL Result/ Method Analysis Validated by CAS # Analvte Name PQL Qualifier Units Reference Date 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected J2 ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 156-60-5 trans- 1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-38-3 m,p_Xylene 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp.!! ear?..I:ncdEnr: ? ,(y,•PcJsYgna�,,/ <.an.�flo(tecn.�s�?�taua[a_ uMill co�,Pz <h?E.(�pareai.nn�en:..,sL�eb/w at,�s[annflc [echass!s[> Page 2 of 3 NC OWWQ Ga6oratory Section g?,psufts Location ID: 1P69COATSMWIO Sample ID: AC00648 Collect Date: 09/23/2013 Collect Time:: 11:11 V>3L Result/ Method Analysis CAS # Analyte Name PQL Units' Validated by Qualifier Reference Date 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 120-82-1 1,2,4=Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Sample Comments :VOA-J2-estimated-2 analyte(s) failed < LCL in the CV. -:TSS-U,P-Sample was duplicated. PQL elevated for volume. Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hto://--i.ncgenr.orp,(y,b aq/��Utzoaeneo/tedL;st;Saeaga guxllfier Codes<h,(p;/!,po{{;J,pS,�ienr,org/w¢b/,yy(lah(3tafin�[,chasc_;b Page 3 of 3 County: • MCDOWELL F WA TF Sample ID: AC01053 River Basin 9pG PO Number # 13GO816 Report To AROAP _O'CQ Date Received: 10/1012013 Time Received: 08:11 Collector: B LAVERTY p, Labworks LoginlD MSWIFT Region: ARO Final Report Date: 10/30/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 11/2112013 Loc. Type: MONITORING WELL Emergency Yes/No VisitiD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: IP69COATSMW16 Collect Date: 10/08/2013 Collect Time: 14:14 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 °C 10/10/13 HMORGAN MET 7440-22A 'Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 130 ug/L EPA200.7 10/21/13 ESTAFFORD1 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7429-90-5 B by ICP 50 56 ug/L EPA200.7 10/24/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 150 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 80 mg/L EPA200.7 10/21/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.60 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7439-89-6 Fe by ICP 50 6600 ug/L EPA200.7 10/21/13 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/18/13 ESTAFFORD1 7440-09-7 K by ICP 0.10 1.9 mg/L EPA 200.7 10/21/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 28 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 1700 ug/L EPA200.7 10/21/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 39 mg/L EPA200.7 10/21/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 6.8 ug/L EPA200.8 10/22/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 10/16/13 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7440-66-6 Zn by ICP 10 IOU ug/L EPA200.7 10/21/13 ESTAFFORDI VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L 'EPA5030/624/8260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For edetailed description or the qualifier codes refer to ht9lLeortaL.c Am-r orr "fW=6/w4��d lstaRpflpJ(Yhaz_[aDat_(�ygiifigyCodeLshwJJ tal-je^.,; ,g¢(W..9Cab,[siaflnfioitttfiassirti Page 1 of 3 NC (DWQ Laboratory Section Wssufts Location ID: 1P69COATSMW16 Sample ID: AC01053 Collect Date: 10/08/2013 Collect Time:: 14:14 f VOL CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 156-60-5 trans- 1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA6030/624/8260 10/10/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 7143-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 10061-02-6 trans- 1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 127-18 4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 630-20-6• 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-184 1,2,3-Trcchloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 1OB-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trim ethyl benzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp-.11 P_4rtw,.nul a,.o eL=JwgJtab(gt.@nnfi.QLechasslnM t.q gLaLlfi r coges rnieJ!_pgrcarn�aenrsry,�,_en/wgf�annnfip�%ch.LLnt Page 2 of 3 NC DWQQ La6oratory Section (Wssufts Location ID:' ' 1P59COATSMWI5 Sample ID: AC01063 Collect Date: 10/08/2013 Collect Time:: 14:14 VVL CAS # Analyte Name PQL Result/ Units Method Anal sis Validated by Qualifier Reference Date 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Trichlorobe nzene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Sample Comments VOL:VOA-J2-estimated-1 analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes rater to htp:11 p_orcai.ncaen..on,L:ni, as�stag�eo�e ;nays �nuat_ — :L.ixer c.a:f< , :ii ,�at.ncaenr.c.atwenlw gab scaflnec?re:hasvzo Page 3 of 3 County: µ MCDOWELL \NAr Sample ID: AC01107 River Basin �? P PO Number # ARO 7 Report To AROAP Date Received: 10/09/2013 -1 Time Received: 10:00 Collector: B LAVERTY Labworks LoginlD KJIMISON2 Region: ARO Final Report Date: 10/29/13 Sample Matrix: GROUNDWATER Final R6001 t Report Print Date: 11/21/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: Location ID: 1P59COATSMWI6 Collect Date: 10/08/2013 Collect Time: 14:14 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name P Units �_ Result/ Metnoa Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.7 °C 10/9/13 RBYRD Turbidity 1 33 NTU APHA2130B-20th 10/10/13 CGREEN Residue —Suspended In liquid 6.2 12 mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hfedL.n..�d.�l,ns�?ncory,(yan(A;1nap(sp.3ryt,N.o/l��nxsssmuata_c.,qx;tberSRO =.�,<ntF;/j.ponat,�<�ie�r,crp,(wrn!w��.an[scartcno,:t�na:,z:n Page 1 of 1 County: y McDOWELL4 \Ng19 Sample ID: AC00650 River Basin �� QG' PO Number # 13GO786 Report To AROAP Date Received: 09/26/2013 > Time Received: 08:15 Collector: B LAVERTY a. Labworks LoginlD MSWIFT Region: ARO Final Report Date: 10/16/13 Sample Matrix: GROUNDWATER Final Repolrt Report Print Date: 11/15/2013 Loc. Type: WATERSUPPLY Emergency Yes/No Visit]D CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: IP69COATSSUMP Collect Date: 09/23/2013 Collect Time: 13:64 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # LAB Analvte Name Sample temperature at receipt by lab PQL Result/ Qualifier. 1.6 Units °C Method Reference Analysis Date 9/25/13 Validated by HMORGAN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORD1 7429-90-5 B by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 44 ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 39 mg/L EPA200.7 1013/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/1/13 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/10/13 ESTAFFORD1 7440-09-7 K by ICP 0.10 1.9 mg/L EPA 200.7 1.0/3/13 ESTAFFORD1 7439-95-4 Mg by ICP 0.10 19 mg/L EPA200.7 10/3/13 ESTAFFORDI 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA200.8 10/3/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 31 mg/L EPA200.7 1.0/3/13 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORD1 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/1/13 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 10/1113 ESTAFFORDI VOL 7440-50-8 Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 9/25113 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected J2 ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to has/i-eaGaLy�enco�°/w>nLq�iab ftfl. . hass_staua:a rt;I,rySN- ML,-,.b/gg(I;,Fj({tafinfig,/txhassrt> Page 1 of 3 NC (D WQ Laboratory Section (Rpsufts Location ID: 1P59COATSSUMP Sample ID: AC00650 Collect Date: 09/23/2013 Collect Time:: 13:54 VOL CAS # 75-09-2 Analvte Name Methylene Chloride PQL - 10 Result/ ualifier Not detected Units ug/L Method Reference EPA5030/62418260 Analysis Date 9/25/13 Validated by VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-34-3 M-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 7143-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 9547-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 9549-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to rt .n cl nr.-I-b , 4abtannno/trchassisrnea:a Q-45er cog; hcp;/�poGaln,�,d=,,r.a ��ery(�q[(rp[s;a9�r fio/le_chasF!m Page 2 of 3 NC D WQ Laboratory Section Wsufts Looation ID: . 1P69COATSSUMP Sample ID: AC00660 Collect Date: 09/23/2013 Collect Time:: 13:54 VOL CAS # 135-98-8 Analvte Name sec-Butylbenzene PQL — 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 9125/13 Validated by VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Sample Comments VOL:VOA-J2-estimated-2 analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description oft he qualifier codes refer to.htnl/.eoq,Lnc9e_;w=gy�gila�.(�,pary,�nQ/�r�Ca istaiia;a_cy�ltry�r c�da,=,<ofp�ri�ra),,ncden�,;c;R/w,rn[wan[sczr.�5c(�Pcnafsim Page 3 of 3 acoloso NC 1D` RLaboratory Section Qi�fsufts County: MCDOWELL Sample ID: AC01050 River Basin PO Number # 13GO812 Report To AROAP Date Received: 10110/2013 %- - Time Received: 08:11 Collector: B LAVERTY rr `>"" 's Labworks LoginlD MSWIFT Region: Ago Division of Water Resources Final Report Date: 10/30/13 Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Final Report Report Print Date: 10/30/2013 Emergency Yes/No VisiUD COC Yes/No Loc. Descr.: COATS AMERICAN 630.AMERICAN THREAD ROADD MARION NC Location ID: IP69COATSMW12 Collect Date: 10108/2013 Collect Time: 10:32 Sample Depth if this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 °C 10/10/13 HMORGAN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 77 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7429-90-5 B by ICP 50 220 ug/L EPA200.7 10/24/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 190 ug/L EPA200.7 10/21/13 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 93 mg/L EPA200.7 10/21/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 12000 ug/L EPA200.7 10/21/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/18/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 5.3 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 17 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 4400 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 160 mg/L EPA200.7 10/21/13 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 11 ug/L EPA200.8 10/22/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-28-0 Thallium (Tl) ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-66-6 Zn by ICP 10 13 ug/L EPA200.7 10/21/13 ESTAFFORD1 VOL Volatile Organics in liquid TITLE_ ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer toheu://oorear.ncdnnron,neorcon°:<h-Ho ear.nc&nr.or°/w°b/w/labhe,Bnfio/e°°h,,sin, Page 1 of 3 WC (DWR Laboratory Section fgsufts Location ID: 1P59COATSMW12 Sample ID: AC01050 Collect Date: 10/08/2013 Collect Time:: 10:32 VOL CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-95-3 ' Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 127-18-4 Tetra chloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 1.6 ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-38-3 rn,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 0.30 ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 Fora detaDed description of the qualifer codes referto h-// oorral.nM-r.-/web/wnnab/ssaPnflortecha::inpnara ooanner (odes<h[o:// oor[al.ncdenr.orc/web/wo/lab/snHnflo/rechas ls[ Page 2 of 3 NC q) WR Laboratory Section 1*sufts Location ID: 1P69COATSMWI2 Sample ID: AC01060 Collect Date: 10/0812013 Collect Time:: 10:32 VOL CAS # Analyte Name PQL Result/ Units Method Analysis Validated by — Qualifier Reference Date 135-98-8 sec -Butyl benzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 0.51 ug/L EPA50301624/8260 10/10/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 0.71 ug/L EPA50301624/8260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Trichlorobe nzene 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-61-6 1,2,3-Trichlorobe nzene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Sample Comments :VOA-J2-estimated-I analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a defalled description of the Qualifier codes refer to btn// portal ncdenr ora/web/wa/lab/stallnHo/rechassistMData QuallHer Codes <htn:// oaral.nalenr.or¢/web/wn/lab/staFnNo/eechassisn Page 3 of 3 AC01104 9VC 1DWW Laboratory Section 12esults County: MCDOWELL Sample ID: AC01104 River Basin PO Number # ARO Report To AROAP Date Received: 10109/2013 Time Received: 10:00 Collector: B LAVERTY Labworks LoginlD KJIMIKJIMI SON2 Region: tO Division Of Water Resources Final Report Date: 13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 10/29/2013 Loc. Type: MONITORING WELL Emergency Yes/No Visit!D COC Yes/No Loc. Descr.: Location ID: 1P59COATSMW12 Collect Date: 10108/2013 Collect Time: 10:32 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # AnalVte Name Others PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.7 °C 10/9/13 RBYRD Turbidity 1 150 NTU APHA2130B-20th 10/10/13 CGREEN Residue —Suspended in liquid 6.2 18 mg11- APHA2540D-20th 10/10/13 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a detailed description of the qualifier codes refer to // [ai c i r bf n b/ [ n n / n sinao [ n na c i h r/ [ i Page 1 of 1 n { County: McDOWELL WA�� Sample ID: AC00649 River Basin O� OC`+ 43G PO Number # 13GO784 Report To AROAP Date Received: 09/26/2013 Collector: B LAVERTY > `I d Time Received: 08:15 Labworks LoginlD MSWIFT Region: ARO - Final Report Date: 10/16/13 Sample Matrix: GROUNDWATER Final Repo it Report Print Date: 11/15/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P59COATSMWIIR Collect Date: 09/23/2013 Collect Time: 12:30 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis CAS # Analyte Name P QLL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.6 °C 9125/13 HMORGAN MIC Turbidity 1.0 1 U NTU APHA2130B-20th 9/25/13 ESTAFFORDI WET Residue -Suspended In liquid 6.2 6.2 U mg/L APHA2540D-20th 9/26/13 CGREEN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7429-90-5 B by ICP 50 50 U ug/L EPA200.7 1013/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 39 ug/L EPA200.7 10/3/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 38 mg/L EPA200.7 10/3/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.60 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 10/1/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1/13 ESTAFFORD1 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/10/13 ESTAFFORD1 7440-09-7 K by ICP 0.10 2.2 mg/L EPA200.7 10/3/13 ESTAFFORD1 7439-95-4 Mg by ICP 0.10 17 mg/L EPA200.7 10/3/13 ESTAFFORD1 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA200.8 1013/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 17 mg/L EPA200.7 10/3/13 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/1/13 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/1/13 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 10/1/13 ESTAFFORDI VOL 7440-50-8 Volatile Organics in liquid _TITLE ug/L EPA50301624/8260 9/25/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to het:&e9.rnoAoedr,,o pyPtpyc>La�CaEae„floCiE haasf :eS?=c3, �yx�inc� CWg} <hcp;/lpmsal.�r�enr;c. i@b�wg(igb(sjafifio[{gtha;Fi,}is Page 1 of 3 NC (DWQ Ga6oratory Section 1&sufts � " . ra Location ID: 1P69COATSMWIIR Sample ID: AC00649 Collect Date: 09/23/2013 Collect Time:: 12:30 VOL CAS # 74-83-9 Analyte Name Bromomethane PQL 1.0 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 9/25/13 Validated by VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/6260 9125/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected J2 ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 156-60-5 trans- 1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-274 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-934 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-38-3 rn,p-Xylene 1.0 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/26113 VANDREWS 9547-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-184 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-82-8 Isopropyl benzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ntpr,Grp(y an/;,qpp��(slaryaP,q(lEsh�sytrFxnp;n_�u�iiner coags„<hlp;/�;pprtayaca�r;ors/�ygi,,LgLn[ptafi�5p,(tecnas:im Page 2 of 3 . WC OWQ Ga6oratory Section �R§sufts Location ID: 1P59COATSMW11R Sample ID: AC00649 Collect Date: 09/23/2013 Collect Time:: 12:30 VUL CAS # 106-43-4 Analvte Name 4-Chlorotoluene PQL — 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 AnabLs Date 9125/13 Validated by VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 104-51-5 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS Sample Comments VOL:VOA-J2-estimated-2 analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to hto-// aorzai.ncden..orz/vrenp_b/seaenaohecba�fis;aoa_a _5;ua?leer coees<hto;usoMaIII .2ad�nrcx;ven/wal�ab/sannfio/tx.Cn Page 3 of 3 y County: MCDOWELL OF VIA Sample ID: AC01051 River Basin O QG PO Number # 13GO813 Report To AROAP �� Date Received: 10/1012013 Time Received: 08:11 C Collector: B LAVERTY a Labworks LoginlD MSWIFT Region: ARO Final Report Date: 10/30/13 Sample Matrix: GROUNDWATER Final Repo) Report Print Date: 11/21/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: 1P59COATSMWI3 Collect Date: 10/08/2013 Collect Time: 12:12 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 1.7 Units °C Method Reference Analysis Date 10/10/13 Validated by HMORGAN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 B by ICP 50 180 ug/L EPA200.7 10/24/13 ESTAFFORD1 7440-38-3 Ba by ICP 10 79 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 27 mg/L EPA200.7 10/21/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.60 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 3.4 ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 3600 ug/L EPA200.7 10/21/13 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/18/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 0.71 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 19 mg/L EPA 200.7 10/21/13 ESTAFFORD1 7439-96-5 Mn by ICP 10 670 ug/L EPA200.7 10/21/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 89 mg/L EPA200.7 10/21/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.8 ug/L EPA 200.8 10/22/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-66-6 Zn by ICP 10 13 ug/L EPA200.7 10/21/13 ESTAFFORDI ► 61-1 Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane-I 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nt:((L,grzai.ncpgnr.ory,�oi,n/w.yna_y[;,tary�ny/�ccnx rsegUa_a._5),ga!1.9e! �s.�as_<.hsat/.t=r4.at,os�e�� :. lstsn�yr.�(..an(yt�nnS l Ilass�m Page 1 of 3 NC 0WQ Laboratory Section &sufts « } Location ID: 1P59COATSMWI3 Sample ID: AC01051 Collect Date: 10/08/2013 Collect Time:: 12:12 VOL CAS # 75-09-2 - Analyte Name Methylene Chloride PQL 10 Result/ ualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 10/10/13 Validated by VANDREWS 156-60-5 trans- 1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS. 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichl6roethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer t0 ry ?/jPaL�l,n4ggnr crp,(wpn/µglta .•. nn Lchasrlrjaua;a,_r,;uAl�@4r cna«: <ncpJ,(_pa,�jn�,2cdenr,,or��; pb[wp[�ahj ast flnlaLta asslm Page 2 of 3 NC OWQQ La6oratory Section W §sufts Location ID: 1P69COATSMW13 Sample ID: AC01061 Collect Date: 10/08/2013 Collect Time:: 12:12 VUL CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS. 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS Sample Comments VOL:VOA-J2-estimated-1 analyte(s) failed < LCL in the CV. Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ntp;/L�,g4sai�n�q�„r�ry/w,n�wanacl:iafl�e Li�SCg��staeaca cungr CQggs <hie:Lla_ortal�cd4nr; L cnas if rt> Page 3 of 3 a t County: MCDOWELL WNArF19 Sample ID: AC01105 River Basin OF O� pG PO Number # ARO Report To AROAP r Date Received: 10/09/2013 Time Received: 10:00 Collector: B LAVERTY Labworks LoginlD KJIMISON2 Region: ARO Final Report Date: 10/29/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 11/21/2013 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: Location ID: 1P59COATSMW13 Collect Date: 10/08/2013 Collect Time: 12:12 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.7 °C 10/9/13 RBYRD Turbidity 1 4.3 NTU APHA2130B-20th 10/10/13 CGREEN Residue —Suspended in liquid 6.2 6.2 U mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to nm� o aai.�cden�.er •nob s, lab/s[afi.�fi Lgcha}Si_[R l�at; Quajlfixr CS+,do,�tpJ/portal n[ie; r.cr➢,(L¢Lwg(lyi7j{'a, flnfiojtechass.�st. q _._�� Page 1 of 1 County: MCDOWELL � q Sample ID: AC01062 River Basin PO Number # 13GO814 Report To AROAP t Date Received: 1011012013 Collector: B LAVERTY _ i Time Received: 08:11 Labworks LoginlD MSWIFT Region: ARO Final Report Date: 10/30/13 Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Final Report Report Print Date: 11/21/2013 Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: IP69COATSMW14 Collect Date: 10/08/2013 Collect Time: 13:46 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # LAB Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier 1.7 Units °C Method Reference Analysis Date 10/10/13 Validated by HMORGAN MET 7440-224 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 320 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 B by ICP 50 180 ug/L EPA200.7 10/24/13 ESTAFFORD1 7440-38-3 Ba by ICP 10 170 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 52 mg/L EPA200.7 10/21/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 36 ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 4700 ug/L EPA200.7 10/21/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/18/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 3.2 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 34 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 530 ug/L EPA200.7 10/21/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 100 mg/L EPA200.7 10/21/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.8 ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 12 ug/L EPA200.8 10/16/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 6.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-66-6 Zn by ICP 10 19 ug/L EPA200.7 10/21/13 ESTAFFORDI VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-67-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-63-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to,h3alL.rr.Qc�l:n<.e.Qe�srel.°b/w.n/_�akl:?.a9nfleL3xshasa'a?a4?aSa._S1:.aiI�IBL..CR+�FE..'.1!?s;/./.F.2rta).A!S.�4Ar.:4LRGW.n:lY.9(4�R>rF$aAP.`!9/.?^cha,F.s's„b Page 1 of 3 .NC (DWQ Laboratory Section W§sufts Location ID: 1P59C0ATSMW14 Sample ID: AC01062 Collect Date: 10/08/2013 Collect Time:: 13:46 VOL Result/ Method Analysis CAS # Analvte Name PQL Qualifier Units Reference Date Validated by 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-18-4 1,2,3-TrichIoropropane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-67-8 1, 3,5-Trimethyl benzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to ry;//_�,griai;nc�nr;cry,(web��.��jia�,r(p.�„gnNo(techa_s!_tatiataxt�cr codes.h[e:LLYortal; ncdenr.orp,/viea�t3�n5o/tgchasstsD Page 2 of 3 NC DWQ Ga6oratory Section �R§sufts Location ID: 1P59C0ATSMWI4 Sample ID: AC01052 Collect Date: 10/08/2013 Collect Time:: 13:46 VOL CAS # 135-98-8 Analyte Name sec-Butylbenzene PQL — 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Anajysi Date 10/10/13 Validated by VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Sample Comments :VOA-J2-estimated-I analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore detailed description of the qualifier codes refer to l,cel/..a;?.!�? �n5den,;,�;R(a:ag�w.n(racist,?rynfl.¢l1sshs;lr;ai�aca._quallrter„ce+gef,<.n..tF;I/..F.?[i�)..OSS�Snr;crp�(v(,Eh[wg(I,�h/stafinfio�pechptyiyts Page 3 of 3 ' 9V(' (DCVO Laboratory, S'ection T esult. County: MCDOWELL \NA7E Sample ID: AC01106 River Basin of O� QG PO Number # ARO Report To AROAP 9r Date Received: 10/09/2013 Collector: B LAVERTY "I Time Received: 10:00 Labworks LoginlD KJIMISON2 Region: ARO Final Report Date: 10/29/13 Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Final Report Report Print Date: 11/21/2013 Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: Location ID: 11359COATSMW14 Collect Date: 10108/2013 Collect Time: 13:46 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL. Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.7 'C 10/9/13 RBYRD Turbidity 1 20 NTU APHA213013-20th 10/10/13 CGREEN Residue —Suspended In liquid 6.2 40 . mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htn:!/ :_or�zr;pfiaenr, ;p,(y�an,L ;t1:3.?9n_gL _ ss!c�agzSa., guagg:Lco�Pf <ht¢IJ P.. tAl n dmt:s:.RLmbIPq&k-Vit0Ps 9Be�na:s scs Page 1 of 1