WQ0024508_Monitoring - 11-2022_20221207

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
Type *
GW-59
WQ0024508
Carolina Research Center
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2022
Upload Document*
Carolina Research Center.pdf 2.72MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Arnie Ferguson
lhzC�-' ve�w[f
Reviewer: Gerald, Wanda
12/7/2022
This will be filled in automatically

Is the project number correct?* WQ0024508
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 12/8/2022

SUBMIT FORM ON YELLOW PAPER ONLY
FACILITY INFORMATION Please Pont Clewly ar Type
Facility Name: Carolina Research Center
Permit Name (if different): Sntithers Viscient LLC
Facility Address: 21AM Quakcnhush koad
Snow Crimp N(-' 27349 County AI:itTance _
Contact Person Cfns Zreske
Well Location7Site Name:
Telephone#: a t,-- tt -HI4I
No, of wells to be sampled
DEPARTMENT OF E14VIRONMENTAL QUALITY - DIV. OF WATER: RESOURCES
INFORMATION PROCESSING UNIT
617 MAIL SERVICE CENTER, RALEiGH, NC t7699-1617
:RMIT Number: !'tC?l)02450E Expiration Gate: ,April ?id- 0-2 t
rn-Discharge; UIC
'CUES Other
'PE OF PERMITTED [OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Rernediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Purnp ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): IN -3 Date sample collected: 1 l l6110 1
Well Depth: I I.No ft. Well Diameter: In.
Depth to Water Level t'25 : 739 ff. below measuring point screened Interval: ft, to ft,.
-
Measuring Point is ft. above land surface Relative M.P. Elevation: ft,
Volume of water pumped/bailed before sampling- 2,25 galloons
Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: FM YEs ❑ NO
FIELD ANALYSES;
pH u0ac0® Units Terrap, oo ,t o: 1,.� r
Spec. Cord. 00094_ trlvlhos
Odor uou55:
Appearance
If WELL
WAS
DRY at
time of
sampling,
check
Caere:
LABORATORY INFORMATION
Coate sample analyzed: i IIf] I I i30/203'
Laboratory Name: Pace Analytical
Services
Certification No. & 63. I_, 1
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COCA n0335
mg'L
Nitrite (NO) as N 00635
I-ng.!
Ph - Lead c;trcvi ugiL
Coliform: MF Fecal ;'s13t6 61.0
i1 OOmL
Nitrate (NO) as N C�uu(i <0.0 0
mgiL
%n - ?inc 01092 mar'L
Coliforrn: NIF Total :3I504
1100mll
Phosphorus: Total as P oo665 0.14
nig!L
_c: Uso h1PN r _ffiod fcr ,, uhl, ry t.d -Lrnijiuslr
OrthophcSp}gate 70507
mgtL
Other (Specify Compounds and Concentration Units).
)issofvee Solids:Total 70300 710
mg/L
Al - Aluminum 0i a05
mg1L
pt-1 (Lab) 00403
units
Ba - Barium 010- r
ugiL
TOC rincim 1.0
rtag,'L
Ca= Caiciuni 00 lu
mgiL
Chloride 00940 3.6
mglL
Cd - Cadmium 010
ugiL
Arsenic woro,
ugiL
Chromium Total mm",
ugiL
Crease and Oils o05R2
mglL
Cu - Copper 01041-
rngiL
ORGANICS: (by GC. GC/MS, HPLC)
Phenol a2 _?,
ugiL
Fe - Iron W0a5
ugiL
(Specify test and method . ATTACH LAB REPORT.)
Sulfate: rat a-,
rrigiL
Hg - Mercury 71 90u
ugiL
Lab Report Attached? ® Yes (1) ❑ No (0)
;peclfic Conductance 40025
[[Mhos
k- - Potassium 0ta':)ar
r oil-
VOC 7873 method # 9260
Total Ammonia ro6iri 0.'y
rnglL
Mg - MagreSiUnn 0092
rngiL
method #
iAmnx-ca Nrrrcgen HH,r _ Ammonia rimer,. intai
Mn - ftianganese 01055
ugiL
,method #
TKN as N 0032
mgfL
Ni - Nickel ro 0
ugiL
method #
For Remedlation Systems Only (Attach Lab Reports): influent Total VOCs: Ima/L Effluent Total VOCs: mg1L VOC Removal%
Perr,ir ee (or Authnr >a. -I Acent) Name ani Title - Please print or ripe

SUBMIT FORM ON YELLQ',%, PAPER ONLY
_! DEPARTMENT OF ENVIRONMENTAL QUALlr IV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM e � 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION pteese P nt Clearly Or Type PERMIT Number: ttt))-11;tIS Expiration date �li;t-12
Facility Name: Cjrolina Research i Cntcr Non -Discharge UIC
Pe mit Nance (iI clifferent) 4nttthers iscient LI- NPDES Other
Facility Address. =clhlf Quakerib sh Road TYPE OF PERMITTED OPERATION BEING MONITORED
Si1c„ j O'amp NC 2 7 9 Count} y Alrtmancc
❑Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remedialiom
Contact Person: Gus Licskc Telephone#; ;;,1 -,}7fg tt l II ❑ Potary Distributor ❑ Land Application of Sludge
Well Location`Site- Name: iJo, of cells to be sarrtplect;— El Source I-leat Purnp El Other:
SAMPLING INFORMATION
WELL ICI NUMBER (from Permit): NIL ` Gate sample col ected: 111161202e FIELD ANALYSES:
t-,ltell Depth: flft. Well Diameter: in. pH c10400: _ ??) units
Depth to Water Level 825€ . l �.<l I ft. below measuring point Scrucned Interval: ft, to fL Spec. fond, oo0g,:
Measuring Point is ft. abovo lanai surface Relative f,1.P. Elevation: ft. Odor =_raoB5:
Volume of water punped/hailed before sampling: I s gallons appearance
Temp. 0001, I 1.T 'C DRY at
Mhos time of
Samples for metals were collected unfiltered:
A YES
❑ NO and field acidified
❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 1 l l 1"-1 1 / 0 n'f3" 2
Laboratory Name:
Pace Anolvtis :al Services
Certification No, 1 `1, 40 633
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations,
COD 10335
trig/L
Nitrite (NO__) as N O'on01.5
mg/L.
Pb - Lead a 1o5l ugfL
Coliform: MF Fecal 31r16 n i1,0
it 00ml-
Nitrate (NO3) as N C-OC,20
1-0.20 mg/L
?n - Zinc 01092 mgtL
Coliform: MF Total 31504
!10flmL
Phosphorus: Total as P eocac
0.7`6 mg7L
�Noic: - nr eInva fhlghly1
Orthophosphate 7 4«7
Ing1L
Other (Specify Compounds and Concentration Units):
]1ssolved Solicls:Total 70 ,0 68.3
mgfL
AI - Aluminum DI1c5
mg]L
art (Lab) t?C;,r13
units
Ba - Barium 01007
ugfL
TOC ombo <?5.0
mg'L
Ca - Calcium 0r,916
mg/L
Chlclride 00940 r.I
mcd!L
Cd - Cadmium 101027
ug/L
Arsenic 01C-C2
ug/L
Chromium Total 0103A
ug/L
Grease and Oils 00552
mg:rL
Cu - Copper e,1042
mg1L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 327,3o
ug!L
Fe - Iron pl(C45
.. ug/L
(Specify test and method #. ATTACH LAD REPORT.)
Sulfate 009:45
rng=L
Had- Mercury 71900
uglL
Report Attached? ® (1) ❑ No (01
a
pe Iftc Conductance i_I I,Yi
111 Y1i1d5
K - Potassium 009
mgeL
�L/ab
3yYes.
V OC 787-3 method # 8260
Total Ammonia 00610 <0.10
mg/L
Mg - Magnesium r?mr
mg/L
method #
t. r n, wa Milrigan: fVH as (`1. tiny. c�ry 1':r�<Pn T�3eIi
kin - I'viancarr€ sc Ilio55
_ _ ug/L
method
TKN as N u0}?v
mg?L
Ni - Nickel 0ioG—,
ugfL
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VCCs: mg,tL Effluent Total VOCs: mg/L VOC Removal%
PernwfeF t:;r r uftr i e d +c7Pnl) Narr,� and Title - Tease print or type
G!N-50 Rev.06-C7-2018
here: 11

SUBL11T FORM 0111 YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV, OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM E � 1617 MAIL SERVICE CENTER. BALE GH, NC 27699.1617
FACILITY INFORMATION Please PontClea,fvorType PERMIT Number: W)[I{l I"()S Expiration U21e 'i) 30,2024
Fas illty Name: Carolina Reserlrch Center Non -Discharge UIC
Permit Name (if different): SioilheFS Viscmy LLC NPDES Other
Facility Address: '-')00 QLWIllenbUsh Road TYPE OF PERMITTED OPERATION' BEING MONITORED
I NC 27349 Colrnty Alaniance El Lagoon Ffemediation: lnfi!tration Gallery
I ❑ Spray Field Ej Remediation:
!Contact Person: Gue Zieskc Telephone#: 36_176-01-11
s El Rotary Distributer Land Application of Sludge
[Well Location/Site Name: No. of wells to be sampled: , El Water Source Heat Pump ® Othei:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): N1XV-1 mate sample collected; 1 if
Well Depth: ft. Well Diameter'
P
Depth to Water Level ,32 1r: ft. below maasuring point Screened Interval:
Measuring Paint is ft. above land surface Relative M.P. Elevation:
Volume ref water pumped1bailed before .sampling: gallons
)Samples for metals were collectod unfiltered: tA YES LJ NO and field acidified YES
] 6/'_t}e_v
in.
fit, to ft.
ft.
[ NO
FIELD ANALYSES:
pH ouaac: units Temp. 00oI6 `C
Spec. Cond. crowfaMhos
Odor 000s5
Appearance
If WELL
WAS
DRY at
time of
sampling,
check
here
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name:
Certification No.
PARAMETERS MOTE: Values should reflect
dissolved and colloidal concentration's.
COD oo335
mg/L
Nitrite (NO,) as N oo615
rng/L
Pb - Lead o1oFl ug/L
Coliform: MF Fecal 51616
11 COmL
Nitrate (NO.) as N nm2o
mg1L
2n - Zinc 010P2 mg1L
I Coliform: MF Total 15rr-1
11170mL
Phosphorus: Total as P oor 65
mg/L
iNotc
Orthophosphate 70507
mg/L
Other (Speci;v Compounds and Concentration Molts!:
issolved Solids:Tctal 70300
mg1L
Al - Aluminum al lo5
mg/L
pL4 (Lab) 100403
units
Ha - Barium 01007
ug/L
TOC 0ro5so
mg1L
Ca - Calcium oorID
mg1L
Chloride ocs:;a
mg/L
Cd - Cadmium e1o27
ug1L
Arsenic 01002
ug/L
Chromium: Total C1t134
ug/L
Grease and Oils ac552
mg/L
Cu - Copper 0104^
mg/L
ORGANICS: (by GC, GC17VIS, HPLC)
Phenol 32730
ug/L
Fe - Iron 0:+345
ugiL
(Specify test and method . ATTACH LAB REPORT.)
Sulfate oog-s
mg1L
Fig - Mercury 71900
ug/L
Lab Report Attached" [I Yes (1 ) ® No (0)
Specific Conductance 000P5
llmhos
h - Potassium oog37
mg/L
VOC 76'3 method
Total Ammonia Innf. Li
ang/L
tag - Magnesiltm 00927
mgfL
method #
Mn - [Manganese 01055
ugfL
method #
TkNE as N oo62
mg/1
Ni - Nickel ri1r57
ugfL
method
For Reme€ lation Systems Only (Attach Lab Reports);
Influent Total VOCs:
mg/L Effluent Total VOCs: mg/L VOC Removal%
a
Permitree (or Authorized Aienn Name and Title - Plcase Lir€nt er
Gvl-59 Rev, 06-07-21018
of Pe,m[ttee ',or Authorized Agent
— " —
tp
(Date)

A�acle Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kircey Ave. Suite 100
Huntersvifle, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research
Pace Project No.: 92637057
Sample: MW-2 Laldll): 92637057001 Collected: 11/16/22 12:40 Received; 11/16/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method.- SM 2540C-2015
Pace Analytical Services - Eden
Total Dissolved Solids
68,3 m g/L
30.5
1
11/22122 11:10
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L
0.20
5
11/18122 10:51
14797-55-8
MB* 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation
Method:
SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
30.0 CFU/100 mL
1.0
1
11/16/22 19:09 11/17/22 17:17
82600 MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
11/19/22 11:01
67-64-1
Benzene
ND ug/L
1.0
1
11/19/22 11:01
71-43-2
Bromobenzene
ND ug/L
1.0
1
11/19/22 11:01
108-86-1
Bromochloromethane
ND ug/L
1.0
1
11/19/22 11:01
74-97-5
Bromodichioromethane
ND ug/L
1.0
1
11/19/22 11:01
75-27-4
Brornoform
ND ug/L
1.0
1
11/19/22 11:01
75-25-2
Bromometh2ne
ND ug/L
2.0
1
11/19/22 11:01
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
11J19Z22 11:01
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
11/19/22 11:01
56-23-5
Chlorobenzene
ND ug/L
1.0
1
11/19/22 11:01
108-90-7
Chloroethane
ND ug/L
1.0
1
11/19/22 11:01
75-00-3
Chloroform
ND ug/L
1.0
1
11/19/22 11:01
67-66-3
Chloromethane
ND ug/L
1.0
1
11/19/22 11:01
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
11/19/22 11:01
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
11/19/22 11:01
106-43-4
1,2-Dibromo-3-chloroprop2ne
ND uig/L
2.0
1
11/19/22 11:01
96-12-8
Dibromochlorometh@ne
ND ug/L
1.0
1
11/19122 11:01
124-48-1
1,2-Diibromoethane (EDB)
ND ug/L
1'0
1
11/19122 11:01
106-93-4
Dibromomethane
ND ug/L
1.0
1
11/19/22 11:01
74-95-3
1 2-Dichlorobenzene
ND ug/L
1'0
1
11/19/22 11:01
95-50-1
1,3-Dilchlorobenzene
ND ug/L
1'0
1
11/1'9122 11:01
541-73-1
1,4-Dichloro benzene
ND ug/L
1,0
1
11/19/22 11:01
106-46-7
Dichloro,difluoromethane
ND ug/L
1.0
1
11/19/22 11:01
75-71-8
1, 1 -Dichloroethane
ND ug/L
1.0
1
11119/22 11:01
75-34-3
1,2-Dichloro,ethane
ND ug/L
1.0
1
11/19/22 11:01
107-06-2
1, 1 -Dichloroethene
ND ug/L
1.0
1
11/19/22 11,01
75-35-4
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
11119122 11V
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
11/19/22 11:01
156-60-5
1,2-Dichloroprop@ne
ND ug/L
1.0
1
11/19/22 11V
7,8,-87-5
1,3-Dichloropropane
ND ug/L
1'0
1
11/19/22 11:01
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
11/19/22 11:01
594.20-7
1,1-Dichloropropene
NE) ug/L
1.0
1
11/19/22 11:01
563-58-6
cis- 1, 3- Dichloropropene
ND ug/L
1.0
1
11/19122 11;01
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1210212022 10:53 AM without the written consent of Pace Analyticai Services, LLC.
Page 4 of 27

Pace Analytical Services, LLC
,a c�A niticl 9800 Kinzey Ave. Suite 100eaya
Huntersvitle, NC 28078
wwxpacelabstam [phone]
ANALYTICAL RESULTS
Project: Carolina Research
Pace Project No.: 92637057
Sample: MW-2
LablD: 92637057001 Collected:
11/16/22 12:40
Received: 11/16/22 14:35 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
trans-1,3-Dichloroprapene
ND ug/L
1.0
1
11119/22 11:01
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
11/19/22 11:01
108-20-3
Ethylbenzene
ND ug/L
1.0
1
11/19/22 11:01
100-41-4
Hexachloro-1,3-butadjene
ND ug/L
2,0
1
11/19/22 11:01
87-68-3
2-Hexanone
ND ug/L
5,0
1
11/19/22 11:01
591-78-6
p-lsopropyltotuene
ND ug/L
1.0
1
11/19/22 11:01
99-87-6
Methylene Chloride
ND ug/L
5.0
1
11/19/22 11:01
75-09-2
4- Methyl-2-penta none (MlBK)
ND ug/L
5.0
1
11/19/22 11:01
108.10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
11/19/22 11:01
1634-04-4
Naphthalene
ND ug/L
1.0
1
11/19/22 11:01
91-20-3
Styrene
ND ug/L
1.0
1
11/19/22 11:01
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1'0
1
11/19/22 11:01
630-20-6
1, 1 2,2-Tetractiloroethane
ND ug1L
1.0
1
11/19/22 11:01
79-34-5
Tetrachlaroethene
ND ugJL
1.0
1
11/19/22 11:01
127-18-4
Toluene
ND ugIL
1.0
1
11/19/22 11:01
108-88-3
1,2,3-Trichloroberizene
ND ug/L
1.0
1
11/19/22 11:01
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
11/19/22 11:01
120-82-1
1, 1,1 -Trichloroethane
ND ug/L
1.0
1
11/19/22 11:01
71-55-6
1, 1,2-Trictiloroethane
ND ug/L
1.0
1
11119/22 11:01
79-00-5
Trichloroethene
ND ug/L
1.0
1
11/19/22 11:01
79-01-6
Triclilorofluoromethane
ND ug/L
1.0
1
11/19/22 11:01
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
11/19/22 11:01
96-18-4
Vinyl acetate
ND ug/L
2.0
1
11/19/22 11:01
108-05-4
Vinyl chloride
ND ug/L
1.0
1
11/19/22 11:01
75-01-4
Xylene (Total)
ND ug/L
1.0
1
11/19/22 11:01
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
11/19/22 11:01
179601-23-1
o-Xylene
ND ug/L
1.0
1
11/19/22 11:01
95-47-6
Surrogates
4-Bromofluora benzene (S)
96 %
70-130
1
11/19/22 11:01
460-00-4
1,2-Dichloroethane-d4 (S)
113 %
70-130
1
11119/22 11:01
17060-07-0
Toluene-d8 (S)
101 %
70130
1
11/19/22 11:01
2037-26-5
300X IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Chloride
3.1 mg/L
1.0
1
11/18/22 19:15
16887-00-6
3501 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L
0.10
1
11129/22 14:12
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0
1993 Preparation
Method: EPA 365A Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.7'6 mg/L
0,050
1
11/29/22 18:22 11/30122 16:56
7723-14-0
Date: 12/0212022 10:53 AM
REPORT OF LABORATORY ANALYSIS
This report shai not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 27

Pace Analytical Services, LLC
KinceyAve. Suite 100
,980O
any
ace AnalHuntersville, NC 28078
www,p,acdabs.com [phone]
ANALYTICAL RESULTS
Project: Carolina Research
Pace Project No.: 92637057
Sample: MW-2 Labll): 92637057001 Collected: 11116/22 12A0 Received-, 11/16122 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310 B TOC Analyticai Method: SM 531OB-2014
Pace Analyticat Services - Asheville
Total Organic Carbon IND mg/L 25.0 25 11121/22 21:57 7440-44-0 D3
REPORT OF LABORATORY ANALYSIS
This report shaH not be reproduced, except in full,
Date: 12/02/2022 10:53 AM mthout the written consent of Pace Analytical Services, LLC. Page 6 of 27

�aceAnalytical
www,pacwabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Carolina Research
Pace Project No.: 92637057
Sample:: MW-3
Parameters
ANALYTICAL RESULTS
Lab ID: 92637057002 Collected: 11/16122 1215 Received: 11/16/22 14:35 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540E Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
72.0 mg/L
25,0
1
11/22122 11:10
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L
0.040
1
11118/22 10:07
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation
Method:
SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
67.0 CFU/100 mL
1,0
1
11/16/22 19:09 11/17/22 17:17
D6
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25,0
1
11/19122 11:20
67-64-1
Benzene
ND ug/L
1,0
1
11/19122 1120
71-43-2
Bromobenzene
ND ug/L
1'0
1
11/19122 11:20
108-86-1
Bromochloromethane
ND ug/L
1.0
1
11 /1 9t22 11:20
74-97-5
Bromodichlorom ethane
ND ug/L
1.0
1
11/19/22 11:20
75-27-4
Bromoform
ND ug/L
1.0
1
11/19/22 11:20
75-25-2
Bromomethane
ND ug/L
2.0
1
11/19122 11:20
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
11119122 11:20
78-93-3
Carbon tetrachloride
ND ugJL
1.0
1
11/19122 11:20
56-23-5
Chlorobenzene
ND ug/L
1.0
1
11/19122 11:20
108-90-7
Chloroetharre
ND ug/L
1.0
1
11/19/22 11:20
75-00-3
Chloroform
ND ug/L
1.0
1
11/19/22 11;20
67-66-3
Chloromethane
ND ug/L
1.0
1
11/19/22 11;20
74-87-3
2-Chlorctoluene
ND ug/L
1.0
1
11/19/22 11:20
95-49-8
4-Chlorotaluene
ND ug/L
1.0
1
11/19/22 11:20
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
11/19/22 11:20
96-12-8
Dibromochtorom ethane
ND ug/L
1.0
1
11/19/22 11:20
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
11/19/22 11:20
106-93-4
Dibromomethane
ND ug/L
1.0
1
11119122 11:20
74-95-3
1,2-Dichloroberizene
ND ug/L
1.0
1
11/19/22 11;20
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
11/19/22 11:20
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
11/19/22 11:20
106-46-7
DicNorod ifl uorom ethane
ND ug/L
1.0
1
11119/22 11:20
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
11/19122 11Q0
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
11/19/22 11:20
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
11 /19/22 11 Q0
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
11/19/22 11:20
156-59-2
trans-1 2-Dichloroethene
ND ug/L
1.0
1
11/19/22 11:20
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
11119/22 11:20
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
11/19/22 11:20
142-28-9
2,,2-Dichloropropane
ND ug/L
1.0
1
11119/22 11:20
594-20-7
1,1-Dichloropropene
ND ugIL
1.0
1
11/19/22 11:20
663-58-6
cis-1,3-Dir-hioropropene
ND ug/L
1.0
1
11/19/22 11:20
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shaV not be reproduced, except in full,
Date: 12/02/2022 10:53 AM without the w✓ritten consent of Pace Analytical Services, LLC. Page 7 of 27

�aceAnalyticalo
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research
Pace Pro] ect No.: 92637057
Sample: MW-3
Parameters
Lab ID: 92637057002 Collected: I1116/22 12:15
Results Units Report Limit DF
Received: 11/16/22 14:35 Matrix: Water
Prepared Analyzed CAS No, Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
trans-1,3-Dichloropropene
ND
ug/L
1.0
1
11119/22 11:20
10061-02-6
Diisopropyl ether
ND
ug1L
1.0
1
11119/22 11:20
108-20-3
Ethylbenzene
ND
ugIL
1.0
1
11119/22 11:20
100-41-4
Hexachloro-1,3-butadiene
ND
ug1L
2.0
1
11/19/22 11:20
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11119/22 11:20
591-78-6
p-1 sopropyl toluene
ND
ug/L
1A
1
11119/22 11:20
99-87-6
Methylene Chloride
ND
ug/L
5.0
1
11119/22 11:20
75-09-2
4- Methyl-2-penta none (M1BK)
ND
ug/L
5.0
1
11119/22 11:20
108-10-1
Methyl -tent -butyl ether
ND
ug/L
1.0
1
11/19/22 11:20
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/19122 11:20
91-20-3
Styrene
ND
ug/L
1'0
1
11/19/22 11:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
11/19/22 11:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
11/19122 11:20
79-34-5
Tetra chloroethen e
ND
ug/L
1.0
1
11/19122 11 �:20
127-18-4
Toluene
ND
ug/L
1.0
1
11119/22 11 :20
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/19/2211:20
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/19122 11:20
120-82-1
1, 1, 1 -Trichloroethane
ND
ugIL
1'0
1
11/19122 1 1:20
71-55-6
I , 1,2-Trichloroethane
ND
ug/L
1.0
1
11/19/22 11:20
79-00-5
Trichloroethene
ND
ug/L
1'0
1
11119/22 11:20
79-01-6
Tri ch lorofluorom ethane
ND
ug/L
1.0
1
11119122 11:20
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/19122 11:20
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/19/22 11:20
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/19/22 11:20
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
11/19/22 11:20
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/19/22 11:20
179601-23-1
o-Xylene
ND
ug/L
1.0
1
11/19/22 11:20
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
11/19/22 11:20
460-00-4
1,2-Dichloroethane-d4 (S)
114
%
70-130
1
11/19/22 11:20
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
11119/22 11:20
2037-26-5
300.0 IC Anions 28 Days
Analytical Method:
EPA 300.0 Rev 2.1
1993
Pace Analytical
Services - Asheville
Chloride 3.6 mg/L 1.0 1 11/18/22 19:31 16887-00-6
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia 0.22 mg/L 0.10 1 11129/22 14:14 7664-41-7
365.1 Phosphorus, Total Analytical Method: EPA 365A Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus 0,14 mg/L 0.050 1 11/29/22 18:22 11/30/22 16:57 7723-14-0
Date: 12/02/2022 10:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 27

aceAnalytical"'
www,pacelabs.carn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research
Pace Project No.: 92637057
Sample: MW-3 LablD: 92637057002 Collected. 11116122 12:15 Received: 11116/22 14:35 Matrix: Water
Parameters Results Units Report Lrrrht DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1'0 1 11/21/22 22:14 7440-44-0
Date- 12M2/2022 10:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fufl,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 27