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HomeMy WebLinkAboutWQ0005603_Historial GW Forms• GVV59A COMPLIANCE REPORT FORM Permit # WQOW5603 (Submit one each motiltoring period with GW-59 forms) I Enter date monitoring results were due. 1 N 31, E ) Will this monitoring report (GW-59 and GW-59A) YES be submitted after the established due date? NO Z x Was any required information missing on the CW-59 report forms? YES No IF the answer to question 1 or 2 is "YES", list in the space provided below the well is Mication numbers) and x explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional ofce for guidance. x 4 Are any monitored constituents equal to or above the established standards? If the answer to question 4 is "NO", skip to section B. YES x NO If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentrations) exceeding standards in the space provided below., MW #12 TDS 720 MGA MW M2 LEAD 0.033 MG/L MANGANESE S.I4 MG/L MANGANESE 0.744 MG/L 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same wells) in the last two years? x If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 Is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each the occurrence (for last two years). ti Are the monitoring well Listed in section S located at or beyond the review boundary? YES NO if the answer is "YES", a groundwater qualityx AL "Noe, Ama OFFICE 1MAMEDJATELY FOR GUIDANC. If thanswer is monitoringCONTACT b Improperly Y A p Y located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving:this YES NO groundwater quality problem? if the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 Is "NO". contact the Regional Office within 90 days• an evaluation may be re uired to determine the f act the waste dls asal s m Js havdn .at tits v'eecand com dance boundaries surroundin rrrrlttee to once of flotation fines.. and/or penal fes. Division of Water Resources MAY 21 2015 MAY 2 6 2015 ROC INF MATtORSECTION SS1NG UNr g The person compieting thr--t_hg /� onitgring re ort should sign beJaw and submit this form with GW-59 forms fo regiri $(. f ' d'> �t Yl sr J�a tled t the:top of the current GW--59 form. Asheville Regional Ofii�e �tiere�,yacknowl�edg�that�t�"s`�Ewve inforrrta`ti�nras eua r�"'�"`cI}�ie'r�f�"`" ot�" (�"`�� ±is report,(Comphanc i Report Signature of Permit .(or Authorized Agent) Date MV-59A 17J8/7-403 MW #2 MANGANESE 1.38 mg/I AUGUST 2013 MANGANESE 1.44 MG/L APRIL 2014 LEAD 0.59 MG/L APRIL 2104 LEAD 0.005 MG/L AUGUST 2014 MANGANESE 1.23 MG/L AUGUST 2014 LEAD 0.043 MG/L DECEMBER 2014 MANGANESE.1.20 MG/L DECEMBER 2014 MW #12 MANGANESE 2.85 MG/L APRIL 2013 TDS 654 MG/L APRIL 2013 MANGANESE 4.06 MG/L AUGUST 2013 TDS 590 MG/L AUGUST 2013 MANGANESE 4.19 MG/L APRIL 2014 TDS 587 MG/L APRIL 2014 TDS 680 MG/L AUGUST 2014 MANGANESE 4.56 MG/L AUGUST 2014 TDS 672 MG/L DECEMBER 2014 MANGANESE 2.39 MG/L DECEMBER 2014 MW #13 TDS 561 MG/L AUGUST 2014 'SUBMIT FORM ON YELLOW PAPER ONLY - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: COATS AMERICAN Permit Name (if different): WIII - - _ M 28752 County -. - MCQ� Coriteyt person: Qd11LIP PIiTMAN tee , Telephone C. Well Location/ Site Name: Mw lln/A h Pond- No. of Wells to be Well Identification Number (irons Permit): PAW #10 for GmundwaterTreatimi Systems Well Depth: 18 fl: Well Diameter, 2 in. Check One: ❑ Influent (98) Screened interval: N/ 1ft. to N A - It. Cj Effluent (99) Depth to Water Level: _2 ft. below measuring point. Measuring Point(M.P.) is:. 2-3.. It. above land surface. Relative M.P. Elevation in it.: Gallons of water pumped/balled before sampling: 3 Date sample collected; 1 15 Field -analysis: pM 7.80 , Specific Conductance " uMhoa 12 Temp. °C, Odor Appearance PARAMETERS (Samples for metals were colledted COD _ mg/l Conform: MF Fecal /100m1 Coliform: MF Total /100mi (Note: Use ?APR mstbad for highly turbid samples) Dissolved Solids: Total 4123125 139 mg/i pH (when analyzed) A121LI5 7.3 units TOC _M26 15 51.0 mgll Chloride _ 4LZ915 Is mg/I Arsenic 41 slis <0.005 m A 9 Grease and Oils mgn Phenol rng/f Sulfate 4127ZI5 27.8 mgA Specific Conductance uMhos Total Ammonia mg/l TKN as N mg/l OP ENVIRONMENT & NATURAL RteSOUMCES TY UIViSiON,'QROUNDWATER SECTION PERMIT M W0005603 E?(pIRATiON DATI=: Noil•biacharge UIC NPOE8 APE OR paRM1 OPERATION BEING MONITORED Re rrtedlatfan: infiltration t3a►lery Spray Field Rwadiatian: Rolaty Distributor Land Application of Sludge Other. Ham Values should reflect dissolved and colloidal concentrations. - Date sample analyzed: SEE BELOW Laboratory Name: H Certificatlori No, YES NO -and field acidified Nitrite (NO2) as N MI Nitrate (NO3) as N mI Phosphorus: Total as P9/27/15 ,� mg/I Orthophosphate m /l At - Aluminum 4/20/15 <0.050 mg/i Ba - Barium AIII <0.005 mg/I CS - Calcium 28 15 <0 50 U_ Cd - Cadmlum 4/28/15 mg/1 <_010iff Chromium: Total _a/28/15 <0.005 rmi-igg/ Cu - Copper mg/l. Fe - iron mg/I Hg - Mercury mg/l K - Potassium mg/I g Mg - Magnesium 9128/1s <o.,s� Mn - Manganese 4,13,8115' <o oo5 mg/I YES N(5j N1- Nickel IF <0.00s m�li Pb : Lea 5 5 rng/i Zn - Zinc mg/I Ammonia Nitrogen mgli Other (313ecily Compounds and Concentration Units) 5 <0.005 M SODlu...M 4/30 15 52.6 MG L ORGANICS: (GC,GC/MS,NPLC) (81pbelly test and method & Attach•lab report.) Report Attached? Yes (t) No (0) VOC : method 0 a method # _ - GROUiVDWATE 3 QUALITY MONiTORING: COMPLIANCE REPORT FORM 'SUBMIT FORM ON Y t t n + PAPER ONLY Print Clearly or Type Facility Name: -COATS AMERICAN Permit Name (it different):� Fanhily Addrman- 630 AMERICAN THREAD RD Well Location/ Site County n ICUONVELL Telephone l#: 828.-756-4111 No. of Wells to be Sampled: _,„ 7 Well Ideritilloation Number (from Permit): MW #11R Well Depth: 30 ft. Well Diameter: 2 in. For Oroundw4terTr"Imentsyll ms Screened interval: N/A It, to Check One: ❑ Influent (e8) 7.3 . 111i1Ar ._ tt. CI Effluent (99) Depth to Water Level ft. below measuring point Measuring Point (M.P.) is:_2_, R. above land surface. Relative M.P; Elevation in fL: . Gallons of water pumped/bailed before sampling: ,...33' Date sample collected: .421 1! Fieldsnalysis: pH 8•44 Specific Conductance uMhos Temp. 15 °C.Odor Appearance PARAMETERS (Samples for metals were coile6ted COD Coliform: MF Fecal /1 onm Coliform: Mf Total /100ml (Note: Use MPH method for highly turbid simples) Dissolved Solids: Total 123/15 229 mg/i pH (when analyzed) AJ21LIS 8.3 units TOC 9126/15 <1.0 mg/l Chloride 4127/15 Y2.3 mg/t Arsenic 4/2s/15 <0.005 mg/1 Grease and Oils milli milli Sulfate AWI't s -- _ 34 5 mg/I Specific Conductance uNlhos Total Ammonia milli TKN as 14 mg/1 WtVARTMENT OF ENVIRONMENT 3 NATURAL RE9.OURCES WATER QUALITY DIVISION, GROUNDWATER SECTION. r: i636 MAIL SERVICe ita N PERMIT tf; WQ000$603 Non -Discharge EXPi'RATION DATE: -NPD-ESU_eUIG QE l!W% 7T= OPERATION BEING MQNiTOR'ED .........._lagoon ROMediallon: Infiltration gallery $P ray Field � Remedlailm: Aolaryr Cfttdbutor Land Application of Sludge Other. lei - Yalues should reflect dlssoived and colloidal concentralloRe, Date sample analyzed! SEE BELOW Laboratory Name: Certification No. 50 unfiltered, _ XYES NO and field aeldff Nitrite (NO2) as N mg/i Nitrate (NO3) as N mg/f Phosphorus: Total as p 4lUjI5 0_22 m /1 Orthbohosphate mg I 9/ AI - Aluminum.4/ a ji5 0.144 mg/i Ba - Barium _a/2a/15 0 o3s Ca - Calcium 413!2SES 34 0g/� Cd - Cadmium 4 _-_ . m f Chromium: Total 4/28/15' <o.005 mg/1 Cu - Copper mg/I Fe - iron mg/l Fig - Meroury mg/1 K - Potassium -----------.- Mg -Magnesium a 28 15 - 16.1 mg/l Mn - Manganeseyalla5` <0•005mg/I led YES up) NI - Nickel 4 2s/is <0.005 � Pb?. Lead-4=15 < '" mg/� Zn - Zino mg/1 Ammonia Nitrogen_mgfl Other (Specify Compounds and Concentration Units). SF 4 28/15 . ' .Niltly mnngM SQDIUM IG/L 4/28/15 ORGANIC$; (Gc,i3C/Ms,Hnt.c) (Specify test and imifhgd 8. Attach lab report.) RePOrt Attached! Yes—(1) No -(p) VOC : method # - method 'SUBMIT FORM ON ]I,EUM PAPER ONLY GROUNDWATER QUALITY MONITORING: Please Print Cleariv or Facilily Name: COATS AMERCIAN- Permit Name (if dlfferent): •••{.Y� .• IY\. caioc � County MCDOWELL Contact Person: PHILLIP PiTTMAN Telephones- 82_._..8-7 1; Well Location/ Site Name: #12 No. of Wells to be Sampled: Well identification3 umber(fromPermit). MW#12_ ForGrountlwsterTreatment5ysterrte Weil Depth: N A ft. W ll Aiameter .2.. _ in- Check One: Ci Influent (98) Screened interval; ( ft. to / It. p Effluent (99) Depth to Water Level: 8.3 It. below measuring point. Measuring Point (M.P.) is 2.6 It. alcove land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/leaked before sampling: 2.5 Dais sample collected: 4.21 .15 Field-saalysis: pH 7.14 , Specific Conductance' ' Umhos Temp. -13 °C, Odor Appearance OF 1 RESOURCES SECTION PERMIT #: W40005603 EXIsIFaATIOiV HATE: - Non -Discharge Ulc NPD98 nQ��aJ Li:.I OPERATION BEING MONiTOREt l lagoon Rernedlallon: InfH►ratlon Gallery Spray Field .,._..�Romedl ke, Rotary Distributor �.-._- • Land Application of Sludge NOTE: Values ahouId reflect dissofved and colloidal concentrallons,, ' t)ate sample analyted: SEE BELOW Laboratory Name: Certilica#on No. 50 -- PARAMETERS (Samples for metals were ooiledted unfiltered X YES No and field acidified COD Caliform: MF Fecal mg/1-Nitrite /i OOml (NO2) as N Nitrate (NO,3) as N / mgI Coliform: MF Total /100ml m Phosphorus: Total as P 1s o.27 mg/l (Note: Use MPH method for highly turbid samples) Orthophosphate Mfl Dissolved Solids: Total 4/23/15 720 trig/I Al - AlUminum 4 28 15 0.077 mg/I PH (when analyzed) 4/ 6.9 units Ba - BariUm4/28/15 0.172 �i29 m� TOC.ALM115 Chloride27/15 2.15 mg/I 6.0 mg/i Ca - Calcium Cd . Cadinlurti-4/28/15 < , mg/t mg/I Arsenic 4/20115 Grease and Oils <0.005 mgil mg/1 Chromium-, Total _4/28/15L Cu - Copper.$ <0 005 m /I Phenol Sulfate 4/27/15 mgi! <10 mgli _ Fe -Iron Hg -Mercury m g/I mg/I Specific Conductance - uMhos K - Potassium m ___._ mg/i Total Ammonia TKN as N mg/f Mg - Magnesium 4/2s/15 1s.3 mg/I mg/ Mn -Manganese , mg/I G W-59 Rev. 0312000 YES NI - Nickel 4 2s/15.- 0.009 mgll Pb - Lead_4/2s/is <0 005 MO Zn - Zinc mg/t Ammonia Nitrogen mg/I Other 18pecify Compounds and Concentration Units) SODfUM G/L ar3f1/1� 134 MG L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report,) Report Attt;ched? Yes, , �() Na . (0) VOC : method # method # method # SUBMIT FORM ON YEjji = PAPER ONLY GROUNDWATER QUALITY MONITORING: ca-ma-1I 111`tf'UC1MA I Isaa Please Print Clearly or Type Facility Name: -OATS AM RI 4N Permit Name (if different): Facility Address:S30 AMERICAN THREAD RD `e�' 28752 County-MmWLLI Contact Person: PHILLI"ITTIVIAN Telephone #: 828-756-4111 Well Location/ Site Name: - MW13/EFFLUENT No. of Weiis to be Sampled. 7Well Identlitcation Number (from Permit): MW #13 ForGGs bimdweter Treetlnsnl.9 t iiii Well Depth: 15• ft. Well Diameter. _ in, y bi Screened Interval: N A _ it. to N A it. Check One: I3 Influent (90) Depth to Water Level: 8 ft. below measuring point. Effluent ($9 Measuring Point (M.P.) is: 2.6 It. above land surface. Relative M.P: Elevation In fit.: _ Gallons of water pumped/balled. before sampling: 3 ' Date sample collected: 15 Field•analysis: pH_ 6.68 Specific Conductance uMhos Temp. --34 . -0. Odor Appearance OF ENViRONMENT & NATURAL RESOURCES tY b "2-1. V, GROUNDWATER SECTION PERMIT #; W00005603 EXPIRATION DATE: Non-Dtscherge D{O NPDES X. TOP Lagoon . gOPERATION BEING MONITORED X. - Helnedlailon: Intlitration t3atiety _.. _ Spray Field _._ RliriitxNation R018ri D18111butor � Land Appliontion of Sludge NOTE: Values should refiect dissolved and • Colloidal coneentrailons. Data sample analyzed: SEE BELOW Laboratory Name: - Certification No. _50 PARAM YERa (Samples for metals were colledted unfiltered YES NO COD Xmg/l and.lield acidified Conform: MF Fecal /100ml Nitrite. (NO2) as N Nitrate (NO3) as N mg/I Coliiorm. MF.Total Use MPH /100mi Phosphorus: Totai as P4L2VZ o.24mg/l g (Note: tndthod for highly turbid samples) Dissolved Solids: Total 4/23/15 149 mg/I Orthdphosphat@ Al - Aluminum VMS 0.0 mg/1 pH (when analyzed) 4LZ1115 TOC 4/26/15 6.4 units <1.0 Ba - Barium 0.026 mg/1 mg/I CS Chloride 4J27/15 Arsenic mg/1 C mg/i - C81CiWtr14 28 15 Cd - Cadmlu - 4 28 15 1 , mg/I mg/i _4/28L15 Grease and Oils <0.005 mg/I mg/i Chromium: Total412s/15� Cu -Capper <0.005 mg/I Phenol Sulfate 4/22/1s mgli <10 mg/l Fe -iron Hg - Mercury mg/1 mg/l Specific Conductance - Total Ammonia uMhos K - Potasslu • mg/I mg/i TKN as N, mgll Mg - Magnesium 9/?a/15 to 8 mg/I Mn - Manganese�2s/1- `. o rng/1 YES - C) 'Ni-- Nickel 4 28/15 <0.005 moll Pb - Lea Zn • Zinc o.00s` AmmOhia Nitrogen mi mgA Othor (specify Compounds and Concentration units) LENIUM V28115 20 5 MG L ORGANIC$: (GC,G' C/MS,H0LC) (SO601fY test and mathod #. Attach lab report.) Report Attached? Yea tt) No (p) VOC method d a method # method # f 'SUBMIT FORM ON yIJ■(■Qtij( PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM rs s.aLl i 1 rNI:UHMw r 1UN PJease Print Clearly or Type Facility Name: COATS AMERICAN Permlt Name (it different);, ■�■/'■ ■ • -11V G0I ✓i County WOUWELL AN Contact Person:-PHILLIP P17TM" l 1 Telephone #: 828-756-4111 Well Location/ Site Name: MW #14/AERATION No. of Wells to be 8ampfad:. Well ldenttficaU15 Number (from Permit): MW #14 �rGrountlweter Trtelmeiif Sytiteinr Well Depth: ft. Wen Diameter 2 in. Cheek One: ❑ influent 98' Scr*eened Interval: N/A6 . ft. to N/A - IL, p Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) Is:_ 2.6 ft. above land surface. Relative M.P. Elevation In ft.: _- Gallons of water pumped/balled before sampling: 3 Date sample collected: 4 21 15 . Field,analysts: pH 6.9 , Specific Conductance - Umhos Temp. 13 °C, Odor Appearance OF ENVIRONHIENT A NATURAL RESOURCES TV.- DIVISION, GROUNDWATER SECTION PERMIT #; Ncn•Qtsoharge WQ0006503 EXPIAA710N• DATE: - U(C NPDES 'T-Q-- R— iMIx= OPERATION BEING I+AONITORED x - Lagoon �.._.._Remsdtatlon: Infiitration Gallery sPmy Field Helnedietlon: Rotary Distributor — Land Application of Sludge _:._.-. Other,' NAIL Values should refiect•dissolved and colloidal conrenttatlonst. • Data sample aneWed: sFF RFI pW Laboratory Name: C Ceftificatfori No: 50 AAAAME'TERS (Samples for metals; were collected unfiltered X YES —NO and "old acidified COD mg/l Nitrite (NO2) as N mg/I Coliform. MF Fecal /100MI Nitrate (NO3) as N Coliform: MF Total /100ml Phosphorus: Total SS P 4 27 15 <0.16m (Note: Use MPH msihod for highly turbid samples) QrthOphasph$te mg/l Dissolved Solids: Total4/2a/i s 321 mg/l Al - Aluminum 0.214 mg/I pH (when analyzed) 4aW/ 6.8 units Ba —Barium 412glis 0-090 mg/l TOC 26I15 179 M9/1 Ca - .Calciurft_-4/30/15 61. mg/I Chloride 4/27/15 5.0 cmg/i Cd - Cadmturri 4/2a/15 <0.00 '2 mg/l Arsenic 4/28/15 -and <0005 mg/I Chromium; Total 4/28/15' <0.005 mg/I Grease Oils m9/1 Cu - Copper ._ —. mg/l Phenol Sulfate 4/27/15 mg/1 <10 mg/I Fe - Iron Hg - Mercury mg/1 mg/€ Specific Conductance uMhos K - Potet;(;jum mg/I Total Ammonia mg/l Mg - Magne9lum 4/30/15 34.3 TKN as N mg/I Mn - Moganese�8/.15• 0.182 nig PNILLIP PITTMAN GW-59 R ev. D3/2000 YES NO) - Ni - Nickel4/28/15 <0.005 .mgA Pb?, Lead 4/2s/is <o 0�3 MO Zn - Zinc mg/t Ammonia Nitrogen mgti Other (Speci(y Compounds and Concentration Units) M 4 28 15 to nnq Mr /1 SnnllfM� q/2g 15 131 MG ORGANICS: (GC,Gc%MS,HPL0) .(Speclfy test and Method C Attach lab report.) Relwrt Attached? Yes (I) No (0) VOG : method # method # method # MAY 18, 2015 SUBMIT FORM ON YELLOW PAPER ONLY - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Facility Name: MATS _AMERICAN Permit Name (ii different): Facility Address: 630 AMERICAN THREAD RD MAt nti "� �t5 21MEW County MCDOWELL Contact Person: PHILLIP PITTMAN_ rw) — Telephone M 828-756-4111 Well Location/ Silo Name: MW ff15/ASH POND No. of Wells to be Sampled: 7 Well Identification Number (from Permii:) POIt?rOu-_.9yatem I ft Well Depth. 16 . Wndwffiar et1 Diameter; 2 in. ne: ❑ ite Treatment 98 Screened. Interval: - N/A _ ff. ro N/A it. Check L7 Effluent �) Depth to Water Level: ft. below measuring point. 99) Lftasuring Point (M.P.) Is: 2.6 It. above land surface. Relative M:P. Elevation In fl.: Gallons of water pumped/balled before sampling: _a Date sample collected: 4 21/15 Field -analysis: pH 6.89 - Specific Conductance ' Umhos Temp. 15 ' aC, Odor Appearance IMENT 8 NATURAL FIESOURCE3 t3R0uNDWATER SECTION, PERMIT #, Wg0005603 EXPIRATION iOtd DATE; Non -Discharge UIC- NPDES 12S OE P 1if4�17rr�r1 -�--_....e OPERATION BEiNG MONITORED Lagoon infiltration eallery SPIRY Field Remediatton Rotary D1stt1bu10r „___ .-.Land Applioatlon of sludge _..- .... 01her. NQM Values should re�fiect dissolved and colloidal concentratfotys.- Data sample analyzed: Laboratory Name: R TE Certification No, PApQM�ERS (Samples for metals were aofledted unfiltered. 9 rYES NO and field acidified COD - Coliform: MF Fecal mg/I /100ml Nitrite. (NO2) as N Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P Mg/I (!`Tote: Use MPH mdlhod for hIgW turbid samples) Orthophosphate mg/I � Dissolved Solids: Total M23/15 pH (when analyzed) 4/21/25 358 mg/i 6.8 units Al - Aluminum s/.211JIS _ Ba - Barium <0 05o mg/l TOC 4/26/15 2.08 mg/1 Ca - CalcIUtn_4130/15 0.090 80.2 mg/I mg/I Chloride 4/27/15 45.0 mg/t Cd - Cadmium 4/213/15 <6.-f F mg/I Arsenic 4/28/15 50.025 mg/I Chromium: Total J28/15 <0.005 mg/I Grease'and Oils mg/l CU = Copper ._ mg/I g/ Phenol Sulfate _412711E mg/I 20.7 mg/I Fe - Iron Hg - Mercury mg/1 S ecific Conductance p uMhds K - Patasstum "--M24/— mg/t mg/I Total Ammonia TKN >1s N mg/i Mg - Magne9lUlt'1 4 28 15 ,; 25.7 mg/1 - mg/t Mh - Manganese 4J28hss 0 03 _ mg/t - YES ND) 'Ni - Nicks 4 28 is <0005 mgA Pb - Lea<0 005 zn - zinc . mg/I Amrhonfa Nitrogen tfigl! Other (specify Compounds and Concentration Units) _.SELENIUM 4 28 15 en Da_ MG/L —sonrr t-- nn-� -._. 4/28J15 17 2 MG/L ORGANICS: (G.C;fJC/MS,HPLC) (Specify test and Method N. Attach lab report.) Report Attached? Yes 0) No (o) VOC method # = method # method # c W v ffjq6i';-Tav'wCH- . _ fit£'. P�)ST 4.%F KCEE BOX 0556 - #5 PINEWOOD PL.A.c A DP, GRANITE FALLS. PWORT11 CA OLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#02) COLLECTION DATE: 4/21/2015 PERMIT #: COLLECTION TIME: 07:34 ADDRESS' Coats America (Wells) RECEIVED DATE: 4/21/2015 P.O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED: 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 111 mg/L 4123115 lag Chloride 8.5 mg/L 4127/15 lag T. Phosphorus 0.27 mg/L 4/27/15 jdg TOC see attached Sulfate see attached metals see attached pH 7.8 su's 4/21115 lag 3 LOG ID: 1504-393 REPORTED BY: NC CERTIFIED LA.B # 50 Tony Gragg, Lab Supervisor I POST OFFICE BOX 1 Q55 . 45 PINE1,A/OOD PLAZA 08. GRANITE. FALLS, fi10RIt I CARO LINA 26630 (828) 39644444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 4/21/2015 PERMIT #: COLLECTION TIME. 07:39 j ADDRESS: Coats America (Wells) RECEIVED DATE: 4/21/2015 '! F.O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED: 5/1212015 ANAL YSI S ". ANALYSIS RESULTS UNITS DATE ANALYST TOS 139 mg/L 4/23/15 lag Chloride 5.8 mg/L 4127/16 lag T. Phosphorus <0.16 mg/L 4/27/15 jdg TOO see attached Sulfate see attached metals see attached pH 7.3 su's 4121115 lag LOG ID: 1504-394 REPORTED BY: NC CERTIFIED LAB # 50 j Tony Gragg, Lab Supervisor py POST 0FRCE BOX 1056 • 05 PINEWOOD PLAZA DR. GRAM TE FALLS, NORTH CA910UNA 28630 (828) 396-4444 SAMPLE: Coats America (MW#11) COLLECTION DATE. 4/21/2015 PERMIT#: COLLECTION TIME., 07:44 ADDRESS: Coats America (Wells) RECEIVED DATE: 4121/2015 P.O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED: 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 229 mg/L 4123115 lag Chloride 12.3 mg1L 4/27/15 lag T. Phosphorus 0.22 mg/L 4/27115 jdg TOC see attached Sulfate see attached metals see attached pH 8.3 su's 4/21115 lag LOG ID: 1504-395 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor wo raw6rcaq POST OF ICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE PALLS, NORTH GAROL&JA 28630 (828) 396-4444 SAMPLE: Coats Arberica (MW#12) COLLECTION DATE.- 4/21/2015 PERMIT COLLECTION TIME: 07:50 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/21/2015 P,O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED. 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 720 mg/L 4/23/15 lag Chloride 6.0 mg/L 4127/15 lag T. Phosphorus 0.27 mg/L 4127/15 jdg TOC see attached Sulfate see attached metals see attached pH 6.9 su's 4/21/15 lag LOG ID: 1504-396 REPORTED BY: NC CERTIFIED LAB # 50 fp, 6a" Tony Gragg.. Lab Supervisor TECH L00,51"i1c. NOTSH 1, POST OFF;CE BOX !056 • #E5 Plr4IEWO,00 Pi A7A DR GRANjTE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE.• Coats America (MW#13) COLLECTION DATE., 4/21/2016 PERMIT#., COLLECTION TIME: 07:55 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/21/2015 P.O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED: 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TOS 149 mg/L 4123/15 lag Chloride <5.0 mg/L 4/27/15 lag T. Phosphorus 0.24 mg/L 4127/15 jdg TOC see attached Sulfate see attached metals see attached pH 6.4 su's 4/21/15 lag LOG ID: 1504-397 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, 1,ab Supervisor IM Ts am TECH 1r;. POST OFFICE BOX 1056 , #5 PINEWOOD OOD PLAZA DP GRANITE FALLS, NORTH CAFxC14„EN'A 23630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 4/21/2015 PERMIT #. COLLECTION TIME: 08.00 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/21/2015 P.O. Box 368 RECEIVED TIME: 12:45 Marion, NC 28752 REPORTED: 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 321 mg/L 4/23115 lag Chloride <5.0 mg/L 4/27/15 lag T. Phosphorus <0.16 mg/L 4/27I15 jdg TOC see attached Sulfate see attached metals see attached pH 6.8 su's 4/21/15 lag LOG ID: 1504-398 REPORTED BY: NC CERTIFIED LAB II 50 fe� (" Tony Gragg, Lab Supervisor trig:. POST OFFICE SOX 1056 • 05 DINEW000 PLAZA CDR. i GRAIN11TE FALLS, MOFI```H Ari0€j'ANA 28630 E (828) 396-4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: t 4/21/2015 s PERMIT #: COLLECTION TIME. 08;05 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/21/2015 P.O. Box 368 RECEIVED TIME., 12:45 Marion, NC 28752 REPORTED: 5/12/2015 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TbS 358 mg/L 4/23/15 lag Chloride <5.0 mg/L 4/27115 lag T. Phosphorus 0.21 mg/L 4/27/15 jdg TOG see attached Sulfate see attached metals see attached pH 6.8 su's 4/21/15 lag LOG ID: 1504-399 REPORTED BY: NC CERTIFIED L11B # 50 fbi. y Tony Gragg, Lab Supervisor RESEARCh & ANAI,yTICAI, LA ORATORIES, INC. For: Water Tech Labs, Inc. P.O. Box 1056 Granite Falls, NC 28630 Attn: Joe Gragg Report of Analysis 5/1/2015 �y NC#34 Z:CA NC tt37701 ? Sri )kiD AN�';�+4ti Client Sample ID: Site: Coats MW2 Water Tech Labs Lab Sample ID: Collection Date: 3415-01 < 4/21/2015 7:34 Aluminum, Total EPA 200.7 2.74 mg/L 0.05 AA 4/28/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 200.7 0.100 mg/L 0.005 AA 4/28/2015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 4/28/2015 Calcium, Total EPA 200.7 18.9 mg/L 0.5 AA 4/28/2015 Chromium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Lead, Total EPA 200.7 0,033 mg/L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 9.96 mg/L 0.5 AA 4/28/2015 Manganese, Total EPA 200.7 0.744 mg/L 0.005 AA 4/28/2015 Nickel, Total EPA 200.7 0.008 mg/L 0.005 AA 4/28/2015 Selenium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 200.7 10.7 mg/L 0.5 AA 4/28/2015 Sulfate SM 4500 SO4 E-1997 <10 mg/L 10 KL 4/2712015 Total Organic Carbon SM 5310 B-2000 <1.0 mg/L 1 CC 4/26/2015 NA = not analyzed .._ ....................... .... ............ .___..._,._............_ .. - — -.-.................._....._ ...... _-. .. ............. P.O. Box 473 106 Short Street Kernerswile, North Carolina 27284 Tel; 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 ral coa basic v1d RESEARCH ANA[YTiCA1 Report of Analysis LA 4RATORIESF INC. 5I1/2015 For: Water Tech Labs, Inc. h��`1G: iA ctYrf'�•,.� P.O. Box 1056 �'�;•��,�., Granite Falls, NC 28630 tt NC #34Cn Attn: Joe Gragg w NC U770.1 .• +011 a A tl Client Sample ID: Coats MW10 Lab Sample ID: 3415-02 Site: Water Tech Labs Collection Date: 4/21/2015 7:39 yPar'a'trie#ew Ike i od ��pf��ie Limit Anal `st Anaysls DateiTlme K rya .�1" r-.—.- Aluminum, Total EPA 200.7 <0.050 mg/L 0.05 AA 4/28/2015 Arsenic, Total EPA 200,7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 412812015 Calcium, Total EPA 200.7 <0.500 mg/L 0.5 AA 4/28/2015 Chromium, Total EPA 200.7 <0.005 mg1L 0.005 AA 4/28/2015 Lead, Total EPA 2003 <0.005 mg/L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 <0.500 mg1L 0.5 AA 412812015 Manganese, Total EPA 2007 <0.005 mg/L 0.005 AA 4128/2015 Nickel, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Selenium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 2003 52.6 mg/L 0.5 AA 4/30/2015 Sulfate SM 4500 SO4 E-1997 27.8 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 <1.0 mg/L 1 CC 4/26/2015 NA = not analyzed __..__......_...__..... _.... _._..._.. _ __— __,....._._..,._.__.....__..,..........._......--........................................ _._..... __.... _._................................ ..__....._._.....-__... - _.... _--- .___....__..._...,_.__.._.. ... __.. P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 ral coa basic Od RESEARCIi & ANA1yTICA[ Report of Analysis L A oRATORIES, INC. 5/1/2015 �1{iUllll0t For: Water Tech Labs Inc. ••'••••••. •� ,�' • �•�• P.O. Box 1056 ``~ Granite Falls, NC 28630' c �• Z:Cn to NC#34 w NC #37701 Attn: Joe Gragg Client Sample ID: Coats MWi 1 R Lab Sample ID: 3415-03 Site: Water Tech Labs Collection Date: 4/21/2015 7:44 C r�its���.��e �Unni Anayst C�naivstaDateRimeu,_ , Aluminum, Total EPA 200.7 0.144 mg/L 0.05 AA 4128/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 200.7 0.035 mg/L 0.005 AA 4/28/2015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 4128/2015. Calcium, Total EPA 200.7 43.0 mg/L 0.5 AA 4/30/2015 Chromium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Lead, Total EPA 200.7 <0.005 mg1L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 16.1 mg/L 0.5 AA 4/28/2015 Manganese, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Nickel, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Selenium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 200.7 15.2 mg/L 0.5 AA 4/28/2015 Sulfate SM 4500 SO4 E-1997 34.5 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 <1 A6 mg/L 1 CC 4/26/2015 NA = not analyzed - .....-- ----- ................................................... ....... ............. ..... ......... ...... ...... . _.... --- ... _:. - - _ P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996.0326 www,randalabs.com Page 1 ral coa basic vld RESEARCh ANA1YTICA[ LA ORATORIfSr INC. Report of Analysis 5/1/2015 •' �►a err �•. For: Water Tech Labs Inc. O`G .•••••C•••.1,�'i P.O. Box 1056 �7 Granite Falls, NC 28630 4 I o ��NC#34 OZ*-Cp: Attn: Joe Gragg+ :• NC #37701 •� Client Sample ID: Coats MW12 Lab Sample ID: 3415.04 Site: Water Tech Labs Collection Bate: 4/21/2015 7:50 Aluminum, Total EPA 200.7 0.077 mg/L 0.05 AA 4/28/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0,005 AA 4/2812015 Barium, Total EPA 200.7 0.172 mg/L 0.005 AA 4/28/2015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 4/28/2015 Calcium, Total EPA 200.7 129 mg/L 0.5 AA 4/30/2015 Chromium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Lead, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 18.3 mg/L 0.5 AA 4/28/2015 Manganese, Total EPA 200.7 .5.14 mg/L 0.005 AA 4/30/2015 Nickel, Total EPA 200.7 0.009 mg/L 0.005 AA 4/28/2015 Selenium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 200.7 134 mg/L 0.5 AA 4/30/2015 Sulfate SM 4500 SO4 E-1997 <10 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 2.15 mg/L 1 CC 4/26/2015 NA = not analyzed _......... -.._..... :........._._....-_._................ ........ ._...__............ _..----------._:_ .._.__.--....... ... .._ ......... ..--._ --- ......... ..... P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 ral coa basic v1d RESEARCh & ANA[YTlCA1 Report of Analysis LA ORATORIES, INC. 5/1/2015 For: Water Tech Labs, Inc, ,w,+*.C,�s'+6 f.tri P.O. Box 1056 a2� Granite Falls, NC 28630 ;� .. . ca NC t#34 Attn: Joe Gragg _NCtt37701 ''�t1!ltits'" Client Sample ID: Coats MW13 Lab Sample ID: 3415-05 Site: Water Tech Labs Collection Date: 4/21/2015• 7:55 ;" . `' "..,�a l ry 1 1 nays Anajr� sDa#etTame Aluminum, Total EPA 200.7 0,051 mg/L 0.05 AA 4/28/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 200.7 0.026 mg/L 0.005 AA 4/28/2015 Cadmium, Total' EPA 200,7 <0,002 mg/L 0.002' AA 4128/2015 Calcium, Total, EPA 200.7 15.5 mg/L ,0.5 AA 4/28/2015 Chromium, Total. EPA 2001 <0.005 mg/L 0,005 AA 4/2812015 Lead, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 10.8 mg/L 0.5 AA 4/28/2015 Manganese, Total EPA 200.7 0,006 mg/L 0.005 AA 4/28/2015 Nickel, Total EPA 200.7 <0.005 mg/L 0.005. AA 4/28/2015 Selenium, Total EPA 200.7 <0:005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 200:7 20.5 . mg/L 0.5 AA 4/28/1015 Sulfate SM 4500 SO4 E-1997 <10 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 <1.0 mg/L 1 CC 4/26/2015 NA = not analyzed ... _... __...................... _..... _...... . _ — .. ...................... ..................... _...... ... P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel. 336-996-2841 Fax: 336 996-0326 www.randalabs.com Page 1 ral coo basic v1d RESEARCh ANA1yTlCAt LAORATORIESF INC. For: Water Tech Labs, Inc. P.O, Box 1056 Granite Falls, NC 28630 Attn: Joe Gragg Report of Analysis 5/1 /2015 pltu�uiiii 441 NC434 NC #37701 Client Sample ID: Coats MW14 Lab Sample ID: 3415-06 Site: Water Tech Labs Collection Date: 4/21/2015 8:00 Aluminum, Total EPA 200.7 0.214 mg/L 0.05 AA 4/28/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 200.7 0.090 mg/L 0.005 AA 4/2812015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 4/28/2015 Calcium, Total EPA 200.7 61.8 mg/L 0.5 AA 4/30/2015 Chromium, Total EPA 200.7 <0,005 mg/L 0.005 AA 4/28/2015 Lead, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Magnesium, Total EPA 200.7 34.3 mg/L 0.5 AA 4/30/2015 Manganese, Total EPA 200.7 0.182 mg/L 0.005 AA 4/28/2015 Nickel, Total EPA 200.7 <0.005 mg/L 0.006 AA 412812015 Selenium, Total EPA 200.7 <0.005 mg/L 0,005 AA 4/28/2015 Sodium, Total EPA 200.7 13.1 mg/L 0.5 AA 4/28/2015 Sulfate SM 4500 SO4 E-1997 <10 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 1.79 mg/L 1 CC 4/2612015 NA = not analyzed _ Pwo.-_-.— ..... ..... 2' '7"2 ...__........._...__..._ -- --- - ,Bax.—473 106—Short— Street----Kernersville..., North_ Caro{ina___8.4.. Tel: 336-996-2841 Fax: 336-996-0326 www.randalabs.com Page 1 ral coa basic v1d RESEARCii & ANALyT-ICA't LA ORATORIES? ITC. For: Water Tech Labs, Inc. P.O. Box 1056 Granite. Falls, NO 28680 Attn: Joe Gragg Report of Analysis 5/1 /2015 "00 Gib rJ :a M NC 434 ;~ NC #37701 Client Sample ID: Site: Coats MW15 Water Tech Labs Lab Sample ID: Collection Date: 3415-07 4/21/2015 8:05 a r,X etho ' "a.,� eK rtr Liriit s s ltatel7lme , - zAnai y=Anal Aluminum, Total EPA 200.7 <0.050 mg/L 0,05 AA 4/28/2015 Arsenic, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Barium, Total EPA 2007 0.090 mg/L 0.005 AA 4/28/2015 Cadmium, Total EPA 200.7 <0.002 mg/L 0.002 AA 4/28/2015 Calcium, Total EPA 200.7 80.2 mg/L 0.5 AA 4/30/2015 Chromium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Lead, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Magnesium, -Total EPA 200.7 25.7 mg/L 0.5 AA 4/28/2015 Manganese, Total EPA 200.7 0,603 mg/L 0.005 AA 4/28/2016 Nickel, Total EPA.200.7 <0.005 mg/L 0:005 AA 4/28/2015 Selenium, Total EPA 200.7 <0.005 mg/L 0.005 AA 4/28/2015 Sodium, Total EPA 200.7 17.2 mg/L 0.5 AA 4/28/2015 Sulfate SM 4500 SO4 E 1997 20.7 mg/L 10 KL 4/27/2015 Total Organic Carbon SM 5310 B-2000 2.08 mg/L 1 CC 4126/2015 NA =not analyzed ,_....... .......:.., --___- .. _...__ . _._....-- — -- — . _ _:.m _ ......._-._---- . — _........_.._ . ......—_.... ........ _...,....: P:O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel, 336=996-2841 Fax: 336-996-0326 www.rantlalabs.com Page 1 ral coa basic v1d CHAIN OF CUSTODY - Analytical Request Client Name:40--a.p�, Address: Report to: Phone: PO Number:.�� Preservatives y Sample Identification b v z z o° o x_ {C� � RS U S� M N U O .pry tl4 ~ Z-- W i U) L w �73 Ir C) Z K 0 7 r • �.ozzi -x (3 s k10 7Z7 ' K 14P491 t .- 111101111114 .wan e_- Temperature ("C) y Received on Ice: Y / N Seated Cooler. Y / N Samples Intact Y / N Additional Comments: WATER TECH LABS, INC PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: Requested Analyses / 7- < 0.2 Upon Field Temp. (C°) Comments [Inman MMEM 30000 3®E®N 13MOME OMMEE Sampler. Signature Tinted Name of Sampler ,ipnature of Sampler. Q_ CHAIN OF CUSTODY - Analytical Request Client Name: Address: :Report to: Phone: PO Nu rtber: 4 nci Sample Identification z U on A" EM Received on ice: Y 7 N Sealed Cooler: Y / N Samples Intact Y / N Preservatives U N 0 os U :: + U E0M 'c v N' c x WATER TECH LABS, INC. PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: pH Checked Upon C12 < 0.2 ma/1 Won Field Temp. (C°) I Comments Printed Name of Sampler: .SQ m , I ud4f I.S Signature of Sampler: 'i t It I q—" ) F' (GW-59A COMPLIANCE REPORT FORM Permit # WQ0005603 (Submit vote each nronitoring'period with GW-59 forms.) Enter date monitoring 'results were due, tl[ao� is �i Will this monitoring report (GW.59 and Gy�.gg,q� be submitted after the established due date? WWas any required information missing on the Cw•-59 report farms? !F the answer tob question 1 or 2 is "YES ;list in the space provided below the well identification numbers) and explain the problems encountered in obtaining the required information. 3 Arc any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing ldrntiflcation plate, area overgrown, etc.)? If the answer is `•}'es cotuact the Regional Office forbttidartce. 4 Are any monitored constituents equal to or above the established standards? !f the answer to question 4 is "NO" skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below, MW #12 TDS 672 MG/L MW #2 LEAD 0.043 MG/L MW #14 MANGANESE 1.25 MG/L MANGANESE 2.39 MG/L MANGANESE 1.20 MG/L CHLOROFORM 10.1 PPB x YES I,Nb x 18 S For the constituents identified In question 4 above, have standards been exceeded previously for the 1'ES NO same constituent(s) in the same well(s) In the last two years? x !f the answer to question 51s NO", skip to section 8. If the answer to question 5 Is "YES" list in the space provided below, each we# with constituent(s) exceeding standards, concentration(s) sported, and sample collection date for each occurrenee (for the last years), SEE ATTACHED PAPER b Are the monitoring wells listed in section 54ocated at Tor If the answerls "YES", a groundwater quality problem maybe oc OFFICEIMMEDIATELYFOR GUIDANCE. If the answer Is "NO'; m located, contact the Regional Office. 7 boun l..1/f Y ! H 1, ► r rtt-tt�GtONAL g wells may be Improperly Is the perrrittee implementing previously approved actions required by the Division involving this groundwater quality problem? If the answer to question 7 is 'YES-, describe those actions in the space orovidarl t„�1nU. Iftha ancu,nr #--..--A2__ ._ ...._.. The person completing this portion ((SW-59A) of the monitoring report should sign below and submit "this form with GW-59 forms for required wells to the address provided at the top of the current Giv :5o Fes,_ ua[e NO x NO GNV-59A 12/812OD3 MW #2 MANGANESE 1.38 MG/L AUGUST 2013 MANGANESE 1.44 MG/L APRIL 2014 LEAD 0.59 MG/L APRIL 2014 LEAD 0.005 MG/L AUGUST 2014 MANGANESE 1.23 MG/L AUGUST 2014 MW #12 MANGANESE 2.85 MG/L APRIL 2013 TDS 654 MG/L APRIL 2013 MANGANESE 4.06 MG/L AUGUST 2013 TDS 590 MG/L AUGUST 2013 MANGANESE 4.19 MG/L APRIL 2014 TDS 587MG/L APRIL 2014 TDS 680 MG/L AUGUST 2014 MANGANESE 4.56 MG/L AUGUST 2014 MW #13'TDS 561 MG/L AUGUST 2014 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Narne*, COATS AMER"N Permit Name (if different): Facility Address: 630 AMERICAN THREAD RD MARION 28752 , (Ca y(zip) Contact, Person:--- PHILLIP PITTMAN Well LoCdtion/,$1tp Name: Ww #10 --------------- SUBMIT FORM OMYELLOW PAPER ONLY, Please Print Clearly or County - - MCDOWELL Telephone #: 828-756-4111 No. of Wells to be Sampled: 7 .vveiiio.entiticatton-Number,(from Permit): Mw#10. For Groundviater Tn!itinent systems, I Well Depth: 18 fti Well DiaMeter,-,2. in. One: (rifluent (98) ,Screened Interval: NIA ft. toN/A Chec 'k Dq0th to W ' ateirlevel: j5_L-_ft. below measuring point171 Effluent (99) . MeaswifigPoirit (M.P..) is: — ft. above land surface. Relafive:M.P. Elevation in ft.: Gallons of water-pumped/balled before sampling. --!_ Date sample collected'i ,Field analysis. pH 6 5 Specific Conductance Umhos Temp. 8 q. Odor Appearance 11401VIintm. I)EVAnTmENT OF- ENVIRONMENT & NATURAL RESOURCES WATER GUALITY DIVISION,.GROUNDWATER SEC71ON 166 MAIL SERVICE CENTER -Phone: Q19) 733-3221 3 'PERMIT #: W00005603 EXPIRATION bATE:. 'Non-DischArge -NPDES JYPE OF PERMITTED OPERATION BEING MONITORED Lagoon -Remedialion: Infiltration Gallery Spray, Fieto Rotary Distributor Land Application of, Sludge, Other",, NOTE- 'Values should reflect dissolved and, colloidal. concentrations: Date,sample analyzed: — SEE BELOW Laboratory Name: = = WATER TECH Certification No. 50 (Sample's for metals were collected unfiltered X - YES NO and field acidified COD M911 1 1 00MI Nitrite (NO2) as U Nitrate (NO, '), as. N. 3 - — mg/1" . - mg/I Colitbrm:MF Fecal ..­. Cohf6rm:'MFT6taI /I 06MI Phosphp.rUs:,T0tal as PIZ/22/14" �0.16rn9/l (Note Use MPN method ' lor highly turbid samples) OrthophosphateDissolve,d SohdS:. Total 12/10/14 145, m 9/1 Al -Alurbintifty 12/11/14 '0.131 mg/1 pf+ (When, analyzed) 12/9/14 7.3 —units. Ba - Barium'-,'12/11114 <0.005 M 911TOC ," ,12/11/14 1M644 mg/I mg/l, Pa -CalckM 12/11/14� Cd - Cadmium 12L11114 ' <0.500 mg/OhIdide: . <0.002 n91I Ars'ej*12ji1/34 <D.005 tT ' Chromium:(�tal12/11/14 <0.065 Mg/l Grease and.011s, Mg/1 Cu - Copper nign Pbenol mg/1 Fe, -iron mg/l Sulfate 12l1Ua_ 30.9 fn -Hg - MercUry Mg/l Specific Ocinductance _uMhos K Potassium M911 ,,Total Ammonia, i*ng/1 Mg -MagnesJurn 12/11/14 <O.'500 M g/l TKN as N mg/i Bain -Manganesd 1241/14 40.005 mg/( YES NO) N! - Nickel12/11/14 Pb - Lead 12/11/14 <0,005 rng/I Zn - Zinc _MCl/l Ammonia Nitrogen, Mg/l Other (Specify Corripounds and Concentration units) SELENIUM .12/11114 <5.55s MG SODIUM 12/11/14 40.7 MG/L ORGANICS: (GC,GC /MS HPLQ .(Specify test:an4 method lf. Attach lab report) -RipportAttachdd? No_(0) VOC method it s26o B method-# SUBMIT FORM ON YEu_ow PAPER ONLY GROUNDWATER QUALITY MONITORING: Please Print Clearly or Type Facility Name: ATSAMERICAN Permit Name (if different); Facility Address: 630 AMERICAN 714RFAD RD ,MARION 011-3 NC 28752 fVICDOWELL t°gy) t oy tz �l County Contact Person: PHILLI PITTMAN Telephone #: a7aas6 4111 Well Location/ Site Name: �� 11R/ASH POND No. of Wells to be Sampled: 7 (from .Patmf[) Well tden#iffcaiion Number (from Per Mw ra111tFor Groundwater Treatmelit Systems Well Depth: so tt. Well Diameter. 2 in. Screened Interval: N/A ft. to NIA ft. ChecicOne: ❑ Influent (9$) ?epth to Water Level: 7.6 tt. below measuring point. 0 Effluent (99) Measuring Point (M.P.) is: it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: 12/9/14 Field analysis: pH, 8 8 , Specific Conductance UMhos Temp.. ,g °C, Odor Appearance DEPARTMENT OF- ENVIRONMENT & NATURAL RESOURCES 'WATER QUALITY DIVISION; GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT f#: W00005603 EXPIRATION DATE: Non -Discharge Vic NPDES TYPE OF PEfiM= OPERATION BEING MONITORED x Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations: Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. so PARR IE ERR (Samples for metals were collected unfiltered x YES NO and field acidified COD mg/t /1DOml Nitrite (NO2) as N Nitrate (NO3) as N mg/l mg/I Coliform: MF Fecal .Coliform: MF Total /1 OOmi Phosphorus: Total as P 12/22/14 0.18 rn (Mote: Use MPN'metttod for highly turbid samples) 'SOlidst OrihophOSplaate lilg DissolvedTotal 22/10114 226 rngll. At - Aluminum 12/11/14 0.202 rn pH" (when analyzed) 12/9/14 8.3 units Ba - Barium 12/11/14 0.033 mg/l TOC 12/11/14 <1.0 mg/1i 7.3 Ca - (" 61C1Um 12/11/14 23.6 --- Chloride 12116/i4 Arsenic _12/ii11a . m,g/t <0.005 mgil Cd.- -Cadmium 12 13f74 Chromium: Total 12/11/14 mgA � <0.005 mg/l Grease and Oilsmg/l Cu;- Copper mg/l Phenol Sulfate 12/11/14 26.2 mg//I Ng -foie Mercury mg/I Specific Conductance Total Ammonia utVlhos K -Potassium mg/l TKN as N mg/l Mg - Magnesium 12/11/14 17.1 mg/t mg/i Mn - Manganese _12a1/1a <0.005 mg/l -YES NO) Ni - Nickel-z/11/14 <0.005 mg/l Pb . L.eaci 12/11/14 <0.005 mtgA Zn Zinc Mgt[ Ammonia Nitrogen mg/l Other (Specify Compounds and Concentration Units) SELENIUM 12/12/14 <0.005 MG/1 SODIUM 12/11/14, 15.9 Wr ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes x (1) No _____ (0) VOC n : method # = 9260 B : method # SUBMIT -FORM ON YELL 0 'PER W_PA_ -ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM please Pant Clearly.0r, Facillty Name-1 COATSAMERICAN. Permit Narnei (if,0jffqfenQ:.., Facility Ad0res!.k_ 630 AMERI.CAN THREAD RD CoUnly— C. M MCDOWELL (Cgy) ntact Person: PHILUP PW4��,il_ (rip) Telephone If, 828-756-4111 W40-Lo(rAtion/ Site Name:- - mw12/—""N1 No. of Wells to be Sarn pl6d: 7 Well Ir P. mity mw4fii deritlfl:7 Zri un�ber(from-"P_er For, Groundwater Trptinant Systems Well Depth:, it. Well'Djarrieter. -z- in, Check.One- 0 Screened Interval: NIA ft. IO__2L/_A- fL- *th t 11 Effluent (99) o Water Level: fl. below measuriog.point, i 0 Mbasudn' P int;(M-P-) is: ft. above land surface. R61ative M.P. Efe'vation.in, . ft., , Gallons of watEir. Pumped/bailed before scampting: 4-5 bate sample collected: .. I21IL14 Field analysis., Specific'Cor;dUctance uMhos Temp. QC, Odor Appearance DEPARTMENT OF'90VIRONMENT & NATURAL RESOURCES WATER QUALITY DjvISION,, GROUNDWATER SECTION 1636 MAIL SERVtCE.CENTER wQ000s603 EXPIRATION DATE: P-0ischarne.. Ulc. TYPE -OF EERW= OPERATION BEING �MONITORED x Lagoon —Rernediation: Infiltration Gallery Spray Field Reffiediation. Rolaiy Distributof Land Application of. Sludge Other NOTE: Values should reflect dlssalved and cot loidat concentrations. Date sample analyzed: SEE BELOW 'Laboratory Name: WATER TECH Certification No. 50 E!ARAM,gjERaA$amples for Metals were collected unfiltered X YES NO and field acidified' —'YES NO) COP �Cbfiform: MF Fecal Mg/i m /IQQ 1, Nitrite (NO2.) as N ltrate (NO3) a, N s N mg/l mg/1 Ni � Nickel 12/ft/14 Pb Lead It/11/14 0.011 eo;005 Cldljfbim: M'FTotaI _/1,00IT11 PhbSphdrus:Totalas' '2/'/" 2-22, mg/I - Zn -Zinc M -co (Npt0:.Usa MPN:mathcd'far highly turbid samples) Dissolved, Solids: Total 1-2/10/14. 672, Oft6 hosphate- p mg/1 Ammonia Nitrogen,,,. m 1, pH (whbn analyzed) 12/9114 mg/I 7.2 units At - AlUmInUM 12/12114 Ba - Barium 0.083 1`119A 0.166 Other (specify Compounds and Concentration Units) 2.53 mg/j, i0.0 . .12/1112 Qa,- CajCibn`]� 12/11114 - Mg/l 68.2 M , 9/1 12L11114 <0.0 05 MG/L Arsenic- r4 I Cd,- CadMium,1VM/14' <0,002 M 9/1 12/11/24 1 L2.9 MG/L jzLimm . <0.00S Chroin, ium: TotaVIVII/14 <0.005 mgj1 Oroase'and 01 Is' mg/1 Cu - Copper mg/I Phenol Sulfate 1'2lL1a4_ mg/I <10 -mg/I F6 - fron Hg - Mercury mg/I ORGANICS: (Gc,' GCIMS,HPLC) Specific. Cond.uctance uMhos K - Potasslu mg1l I (Specify test and method #. Attach 'Report Attahed? Yes�1 lab report.) N0) Total A Orita TKN mg/ !Ag- agneslum12/11/14 mg/l VOC method# = 8260E �mg asN mg/11 Mn - Manganese. 12111/14 2.39 mg4 method It SUBMIT FORM ON YELLQW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility'Narkie: COATSAMERICAN Permit Name (it different): ------ Facility AddresS: 630AMERICAN THREAD RD MARION NC 28752 (Car) isuea> ice) County MCDOWELL Contact Person; PHILUP PITTMAN Telephone #:82s-756-4111 Well Location/ Site Name: MW 13JEFFLUENT No. of Wells to be Sampled: 7 Well Identification Number (from Permit): MW a13 Well Depth: is it. Well Diameter in. For Groundwater Treatment systems y Check,One:13 Influent (98) Screened Interval:—_WA_ft. to N A it. Q Depth to Water Level: 1o.z ft. below measuring point. Effluent: (99) Measuring Point (M.P.) is: It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2 Date sample collected: 1z/9/14 Field analysis: pH, 6-5 _ _ , Specific Conductance I ' umhos Temp. 14 °C, Odor Appearance MTMENT OF 'EHVIFIONMENT & NATURAL RESOURCES :R QUALITY DIVISION, GROUNDWATER SECTION MAIL SERVICE CENTER PERMIT #: WQ0005603 EXPIRATION DATE: NOn-Discharge UIC NPDES IYPP QFPRMITTED OPERATION BEING MONITORED x . Lagoon Remedialion: infiltration Gallery Spray Field Rernedlation: Rotary Distributor - —Land Application of Sludge Other. _ NOTF: Values should reflect dissolved and, colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Narna: - w4jER T Certification No. 50 PARAMETERS. (Samples for metals were collected unfiltered X YES NO and field acidified CO©. mg/1 /100ml Nitrite'(NO2) as N Nitrate (Nos) as N mg/l mg/l Goliform: MF Fecal Coliform: MF Total /100ml Phosphorus: Total as P 12/22/14 6.19 mg/I ;Mate: Use h1PN method for highly turbid samples) Orthophosphate m t Oissolved,Solids: Total 12/10/14 mg/l Al - Aluminum 12/11/14 0.056 mg/l pH (when analyzed) 12/9/14 6`9 units Ba - Barium 12/11/14 0.032 TOC i2e 1/14 yi6/ 4 ChlChloride1zJ 2.62 mg/l c mg/1 . Ca - Calcii Tj 12/11/14 Cd - .Cadmium-12111/14 11.3 mg/l m i 9/ <0.002 Arsenic 12/11/14. <0.005 mg/I Chromium: Total 12/11/14 <005 mg/l Grease and Oils mg!! Cu -Cro apper mg/l Phenol Sulfate 12/11/14 12.1 mg/I F(g _ lMercury m Specific Conductance uMhos K - Potassfurn mg/I Total Ammonia ITI Mg - Magnesium 12/11/14 7.60 mg/l TKN as N' mg/l Mn - Manganese 12/11/14 0.175 mg/I YES NO) Ni - Nickel 12111/14 0.007 mg/l Pb - Lead 12%11/14 <0.005 mqA Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration"Units) SELENIUM 12/11/14 0.005 MG/L SODIUM 12/11/14 57.9 MG/L ORGANICS: (GC.GC/MS,HPI_C) (Specify test and method #. Attach lab report.) Report Attached?. Yes x (1) No (0) VOC : method # = 8260 B method # SUBMIT FORM ON YE,LLQ V GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FOCI ITY INFQRP11ATFOPI Please Print Clearly or.7yps Facility Name: COATS AMERICAN Permit Name. (if different): Facility Address:. 630 AMERICAN THREAD RD tSuaat}, MARION NC 28752 County MCDOWELL (City) (swm) - txwt Contact- Person; PHILLIP PITI'MAN Welt Location/ Site Name: - MW 14/AfRAT10N Telephone #: 828-756 4111 No. of welts to be Sampled: 7 Well, Identihcatian Number (horn Fermft): MW #14 Tom sI Well Depth- 1s it. WeDiameter.2 ScEeened Interval . NIA in. F0C Groundwater Treatment Systems Check One: ❑. Influent 98 t ft. to /A N it Depth to Water Level: 7.5 ft. below measuring point. 0 .Effluent (99) Measuring Point (M.P.) is: • It. above land surface. Relative AtI P. Elevation in #t.: Gallons,of water pumped/bailed before sampling: 3 Date sample collected: 12/9/14 t=ieldanalysis: pN s.$ _, ., Specific.Conductarice ulv4hos Temp. 14 *C, Odor Appearance ONLY , QEPARTMENT OF 'ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WQ0005603 EXPIRATI DATE: Non-Dischargp UIC NPDES T-Y' E QF PE_ R ]±En OPERATION BEING MONITORED x Lagoon Rernediation: infiltration Gallory Spray Field Remediation Rotary Distributor land Application of Sludge Other MTE: Values should reflect dissolved and • colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. so pA�AI M (Samples for metals were collected unfittered X YES NO COD and field acidified Coliform: MF Fecal f>igil 1100Ml Nitrite (NO2) as N Nftra�te (NO3) as N m f mg Cotiform: MF Total t10Qml' Phosphorus: Total as ,P.12/22/14 <6.16 mg/1 (Note: Use MPN method for highly turbld samples} Dissolved Solids: Total rrtglf Ortl Iopho$phatra' mg/l 12,10/14 pt'f..(when. analyzed) 12/9/14 444 7.1- units AI - Aluminum 12/11/14 Ba - Barium _12/11/14 o.a76 tng4 TOC 12/11/14 Chloride 3.87 fllg/l Ca _ Calcitlrrt 12/11/14 . 0.129 mg/I 61,9 �visiz4 Ar$@rIIC 12 11 14 fng/t <0.005 i�ngtl Cd - Cadmiumiu��4 Cf rtitillttm: Total 12 11/14 <0 002 mj <0.005 m l Grease -and Oils mg/1 Cu. = C€ipper 9+� mg/I Phenol Sulfate 12 11/14 specific mg/I <10T mg/i. Fe - Iron.. H9 - Mercury mg/I mg/I Conductance uMhos. K - Potassium mgli Total Ammonia l`KN as N mg/I Mg h a r�esltim iz111n4 <o:aos mgli Mn - Manganese 12t11/14. 1.25 mg/I YES Np) Ni - Nickel_ 12/11/14 <0.005 mg/l Pb - Lead 12/11/14 0:011 11 mg/l Zn = Zinc mgA Ammonia Nitrogen mg/l Other (specify Compounds and Concentration Units) SELENIUM 12111114 <O.0o5 MG L SODIUM 12111/14 43.6 MG/L ORGANICS: (GC,GC/MS,HPLC) (Specify test 'and method #. Attach lab report.) Report Attached?. Yes x (1) No (0) VOC method' # = szso B method # SUBMIT FORM ON YELLOIAr PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Prinf Clearly or Type Facility Name: COATS AMERICAN Permit Name (if different): _ Facifity Address: 630 AME& N THREAD RD tSuset) ._... _ LLtViARION NC 28752 County MCDOWELL ~- ~ tc4r) ts+�u+) - [Zip) Contact Person: PHtLLIP PITFMAN Telephone 9: 828as6-4221 Well Location/ Site Name: _ _MMI ASH POND No. of Well to be Sampled 7 twain Pc t 'Well Identification Number (from ,Permit): MW ##15 1:or Groundwater TreatattQnt°Systems Well Deptlt. 16 it. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: N/A It. to N/A it. ❑Effluent (99) Depth to Water Level: 9.3 ft. below measuring point. Measuring Point (M.P.), is: It. above land surface. Relative M.P. Elevation in ft.: Gallons of water puri)ped/bailed before sampling: 1 Date sample collected: 1z/9/14 'seid analysis: pH 6.7 , Specific Conductance uMhos Temp. 19 °G, Odor Appearance DEPARTMENT OF 'ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL. SERVICE CENTER PERMIT. #: WCL0005603 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTi=n OPERATION BEING MONITORED x Lagoon Remediation: infiltration Gallery Spray Field Rotary Distributor Other: Refnediation: land Application ot'Sludge NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 50 _ PARAME,TERS'(Samples for metals were collected unfiltered x . YES NO and field acidified COD .m9/1 /100m! Nitrite (NO2) as N Nitrate (NO3) as N mg/l mg/i Coliform: MF Fecal Cofiform: MF Total /100ml Phosphorus: Total as P_jZj2V 4 0.21 mg/l (Note: Use IAPN method for highly turbid samples) Orthophosphate, mgl Dissolved -Solids: Total 12/10/14 366 mg/I Al - Aluminum 12/11/14 0.038 m I H when analyzed) 12/9/14' P ( Y ?---- 7.0 units Ba -Barium _12/11/14 Doss M 9/1 T0C _12/11/24 Chloride 12/16/14 2.07 mg/l Ca - Calcium mg/l _ Arsenic 12/ Off <5.0 mg/l <0.005 mg/l Cd . Cadmium__ 12/11/14 Chromium: Total 12/11/i4 <0;002 � 1 <o.005 mg I Grease and C3its mg/l Cu -Copper mg/I Phenol Sulfate 12/11/14 mg/I Fe -Iron mg/t Specific Conductance <10 mg/I umhos Hg - Mercury K - Potassium mg/1 mg/1 Total Ammonia mg/1 Mg -- Magnesium 12 11114 32.3 mg/l TKN as-'N mg/I Mn- Manganese 1211i/la a635 mg/1 YES NO) Ni - Nickel 12/11/14 <0.005 mg/l Pb - Learj_12/21/14 <6.005 mg/l Zn - Zinc mg/l Ammonia Nitrogen mg/l Other (Specify Compounds and Concentration Units) SELENIUM 12/11/14 <0.005 MG/L SODIUM 12/11/14 �- — 9.27 MG/L ORGANICS: (GC.GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes x (1) No (0) voc : method # c 8260 S method #1 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: COATS AMERICAN Permit Name;(ddifferprit): , MARION NC 28752 MCDOWELL 't Person:— ; - County-, on QPHILL11 PITTWW" C Telephone 828-756.4112 Well Location/ -Site Nama.- SEVIER BACK -GROUND No. Of Wells to be Sampled:. Well entiFUZ Number (from Permit), MW#2 Well Depth: __ 75 For Gmundwater Treatinent $Ystems en, -!—in. Seteened Interval. N/A Chec'k0ne:E] inf luent (98) ft. to WA_ It. Depth to Water Level:_-34-r. It. bel6w I 1 11 1 easuring point, 0 Effluent (99) Measuring Point (M.P.) is: 7_3it. above land surface. Relative M.P. Elevation In ft.: TGallons.of Water 06rhp6ftailed before sampling: _.e2_ Date sample dollected, Fiqldanalysis: pH 8:0 ,'Specific Conductance: ttfvihos "Temp. 7 . OC, Odor Appearance PEPARTMEiff OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #.,'W- Q0005603 EXPIRATION DATE: N6n-Oischarne_ UIC NPDF `TYPE _QE_P_E,R_M_J= OPERATION BEING MONITORED Lagoon -Remediation: Inliftration Gallery Spray Field Remedlation: HOIM Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sampleanafyzeq: SEE BELOW 'Laboratory-NaMe. WATER TECH Certification No,, 50. RARAM9tEAFtf($ampi.es for metals were collpcted unfilteredI a .COD -L—YES' , —NO and field acidified ,C0fff6TM-', MF'F06al rpgll /I OOMI Nitrite - -N (NO2) as Nitrate (NO ).as N: 3 mg/l mg4 �C011fo.rn,W. Total /100,ml Phosphorus: Totaictis P��� - mg (Note '! use hiph. method for highly turbid -samples) Dissolved Si Total 12/10114 !`4 IT1911 Orthloph osphate,_ . All - Aluminum 12i11/14 mgA i.06 (when anialyk6d). 12/9/14 18 units 'Barium 12/1 Ba IDA- M 9/1 '0.123 M 9/1 .,0 T _G - i2/11/24 " . . , - Chloride: <1.0 Ca ­Calcibm i2t1144 35.1. M 9A Ar,senj(.- 12/11/14,.. itt 1. 7 '005 ITI 911 Cd - Cadmium 121i1/14 I Chromi6rn: Total 1za1/141- <0.002:mgA, 0.6o7mg/1 .GreAso:�ind' .,its Phenolg/l mg/l Cu - C'Oppe m Sulfate -12 14 <10 m19/1 Fe - Iron -Hg - Mercury mg/l mg/1 Specific, Conductance uMh — 0$, K­ Potassfu mgA TotafAmmonia ; . mg/l Mg�,_ Magnesium. gtil/i 4 19.2 mg/1 TKN as N . . mg/l I 1 Mn. Manganese. U/Ii/14 1.2 1 0 mg/1 YES — NO) Ni- Nickel 1?111114_ 0.010 - mg/I Pb - Lea H12111/14 oO.04 Zn - Zinc mg/l Ammonia Nitrogen mWl Other (Specify Comp'ounds'.and Concentration Units) SELENIUM 12/11/14 MG/L SODIUM. 11/14 11.3 MG/L ORGANICS: (GC,GC/MS.HPLC) (Specify test and. method #. Attach' lab report.) Report Attached? Yes -A—(!) No (0) voc Method #f = 8260 B method-# ;tiq�illitgl RESEARCh & ANA1yTICAL�ur''�J• bORATWES, INC. ,,;� •• • � cr 1- z :' Analytical/Prooess Consultations B t • �f •......, Cj 4 Water Tech Labs, Inc. Date Sample Collected 12/09/14 P.O. Box 1056 Date Sample Received : 12/11/14 Granite Falls, NC 28630 Date Sample Analyzed 12/11/14 Attn: Joe Gragg Date of Report 01/02/15 Analyses Performed by : CC -KL -AA Lab Sample Number -------------------- 801287 Parameter Storet # Results TOC (00680) 2.07 mg/1 Sodium,Tot (00929) 9.27 mg/l Selenium,Tot (01147) <0.005 mg/1 Sulfate (00945) <10 mg/l Aluminum,Tot (01105) 0.038 mg/l Arsenic,Tot (01002) c0.005 mg/l Barium,Tot (01007) 0.088 mg/l Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/l Calcium,Tot (00916) 72.1 mg/l Lead,Tot (01051) <0.005 mg/l rHagnesium,Tot (00927) 32.3 mg/1 Manganese,Tot (01055) 0.635 mg/l Nickel,Tot (01067) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICA Number MW15 Time Collected (Hrs) 1000 P.O. Box 473. 106 Short Street - Kernersvilla, North Carolina 27284. 336-996-2841 , Fax 336-996-0326 www.rendelabs.com RESEARCh & ANA[YTiCAL F- -I- L:A ORATORVS, INC. Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected ; 22/09/14 P.O. Box 1056 Date Sample Received : 12/11/14 Granite Falls, RTC 28630 Date Sample Analyzed : 12/11/14 Attn: Joe Gragg Date of Report 01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801286 Parameter Storet # Results TOC (00680) 3.87 mg/l Sodium,Tot (00929) 43.6 mg/l Selenium,Tot (01147) <0.005 mg/l Sulfate (00945) <10 mg/l Aluminum, Tot (01105) 0.476 mg/l Arsenic,Tot • (01002) <0.005 mg/l Barium,Tot (01007) 0.129 mg/l Cadmium,Tot (01027) <0.062 mg/l Chromium,Tot (01034) <0.005 mg/l Calc um,Tot (00916) 61.9 mg/l Lead,Tot (01051) 0.011 mg/J. Magnesium,Tot (00927) 37.4 mg/1 Manganese;Tot (01055) 1.25 mg/l Nickel,Tot (01067) <0.005 mg/l Clients Sample Source COATS AMERICA Number MW14 Time Collected Mrs) - 1 0930 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 338-996-0328 www.randolobs.com - RESEARch & ANA1.'�T(CAL LAbORATORIES,, INC. NC41 Anelytical/Process Consultations M +t,NED AN�� �•}' Water Tech Labs, Inc. Date Sample Collected 12/09/14. P.O. Box 105.E Date Sample Received 12/11/14 Granite Palls, NC 28630 Date Sample Analyzed 12/11/14 Attn: Joe Gragg Date of Report 01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801285 a aC �.-.qC SSR L^�==��sC��aaa.-:c��Cvcca��-����c=��accaa�cc�-� ---•---��rc_�_�....--.-...-.-tee= Parameter Storet ## Results TOC (00680) 2.62 mg/l Sodium,Tot (00929) 57.9 mg/l Selenium,Tot (01147) <0.005 mg/l Sulfate (00945) 12,1 mg/1 Aluminum,Tot (01105) 0.056 mg/l Arsenic,Tot (01002) 40.005 mg/1 Barium,Tot (01007) 0.032 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Chromium,Tot (01034) <0.005 mg/1 Calcium,Tot (00916) 11.8 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 7.60 mg/l Manganese,Tot (01055) 0.175 mg/l Nickel,Tot (01067) 0.007 mg/1 -------------------- Clients Sample Source COATS XMERICA Number MW13 Time Collected (Hrs) 0923 P.O. Box 473 • 106 Short Street @ Kernersville, North Caroline 27264. 336-996.2841 • Fax 336-996.0326 www.randetabs.com tttuuurf� RESEAR�Ch & A,NA1.YTiCA +' LZORATORiES INC. >Nc134 _ Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected 12/09/14 P.O. Box 1056 Date Sample Received 12/12/14 Granite Falls, NC 28630 Date Sample Analyzed : 22/11/14 Attn:, Joe Gragg Date of Report : `01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801284 Parameter Storet # Results TOC (00690) 2.53 mg/l Sodium,Tot (00929) 72,.9 mg/l Selenium,Tot (911.47) 40.005 mg/l Sulfate (00945) <10 mg/l Aluminum,Tot (01105) 0.083 mg/l Arsenic.,Tot (01002) <0.005 mg/1 Barium,Tot> (01007) 0.16.6 mg/l Cadmium,Tot (01027) <0,002 mg/l Chromium,Tot (01034) <0,005 mg/l Calcium,Tot (0091(5) 68.2 mg/l Lead,Tot (01052) <0.005 mg/l Magnesium,Tot (00927) 18.6 mg/l Manganese',Tot '(01055) 2.39 mg/l Nickel,Tot (01067) 0.011 mg/l -------------------- Clients Sample Source COATS AMERICA Number MW12 Time Collected (Hrs) 0910 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284.336-996-2641 • Fax 335-996-0326 www.randelabo.com eir►►►►4r RESEARCh & ANAL}/TICAi UbORATOMES, INC. •`•r`r� ' '� �" �'�'� ''• +qM t Analytical/Process Consultations M NC #34 : a 3/ aCtd., Water Tech Labs. Inc. Date Sample Collected 12/09/14 P.D. Box ,1056 Date Sample Received 12/11/14 Granite Falls, NC 28630 Date Sample Analyzed 12/11/14 Attn.: Joe Gragg Date of Report 01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801283 a a�aa x as as tea= ac an a c^.^.c o n o== o�vo � c as a. a c a a a a C a a c c a c c c a c a G as a s aes c as a a a eases aaa as a Parameter Storet # Results TOC (00680) <1.0 mg/l Sodium,Tot (00929) 15.9 mg/1 Selenium,Tot (01147) <0.005 mg/1 Sulfate (00945) 26.2 mg/1 A.luminum,Tot (01105) 0.202 mg/1 Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.033 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Chromium,TOt (01034) <0.005 mg/1 Calcium,Tot (00916) 23.6 mg/1 Lead,Tot (01051) <0.005 mg/1 Magnesium,Tot (00927) 17.1 mg/1 Manganes'e,Tot (01055) <0.005 mg/1 Ni.ckel,Tot (01067) <0.005 mg/1 -------------------- Clients Sample Source COATS AMERICA Number MW11R Time Collected (Hrs) 0900 P.O. Box 473 • 1 OB Short Street • Kernarsvllle, North Carolina 272B4 , 336-996.2841 • Fax 338-996-0326 www.randelabs.aom RESEARCh & A►NALYACA1 LkORATORVS, INC. Analytical/Process Consultations z H0 #34 Water Tech Labs. Inc. Date Sample Collected 12/09/14 P.O. Box 1056 Date Sample Received 12/11/1.4 Granite Falls, NC 28630 Date Sample Analyzed 12/11,/14 Attn: Joe Gragg Date of Report 01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801282 Parameter Storet # Results TOC (00680) <1.O mg/1 Sodium,Tot (00929) 4.0.7 mg/1 Seleriium,Tot (011417) <0.005 mg/1 Sulfate (00945) 30.9 mg/1 Aluminum,Tot (011:05) 0,131 mg/1 Arsen c,Tot (01002) <0.005 mg/l Barium,Tot (01007) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Chromium,Tot (01034) <0.005 mg/l Calcium,Tot (00916) <0,500 mg/1 Lead,Tot (01051) <0,005 mg/1 Magnesium,Tot (00927) <0.500 mg/1 Manganese,Tot (01055) <0.005 mg/1 Nickel,Tot (01067) <0.,005 mg/1 -------------------- Clients Sample Source COATS AMERICA Number W410 Time Collected (Hrs) 090'0 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284. 338-99B-2841 • Fax 336-998-032B wwwirandalabs.com TICA� ♦ '�f{{{lttfl��� t I, LbCRATWES, INC. `•.e.Q....RESEARch&ANA1y�r,r � "1�%ZMO ��ft' NC 04 Analytical/Process Consultations Cw Water Tech Labs. Inc. Date Sample Collected : 12/09/14 P.O. Box 1056 Date Sample Received 12/11/14 Granite Falls, ITC 2863.0 Date Sample Analyzed 12/11/14 Attn: Joe Gragg Date of Report 01/02/15 Analyses Performed by CC -KL -AA Lab Sample Number -------------------- 801261 Parameter Storet # Results TOC (00680) <1.0 mg/l Sodium,Tot (00929) 11,3 mg/l Selenium,Tot (01147) <0,005 mg/1 Sulfate (00945) <10 mg/1 , Aluminum,Tot (01105) 2.06 mg/1 Arsenio,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.123 mg/l £admium,Tot. (0102.7) <0.002 mg/1 Chromium,Tot (01034) 0.007 mg/1 Calcium,Tot (00916) 35.1 mg/l Lead, Tot {01051} 0,043 mg/1 Magnesium,Tot- (00927) 19.2 mg/1 Manganese,Tot (01055) 1.20 mg/l Ni.ckel,Tot (01067) 0,010 mg/1 -------------------- Clients Sample Source COATS AMERICA Number MP72 Time Collected (Hrs) 0855 R 0, Box 473 a 106 Short Street • Kernersvilla, North Carolina 27284.336-.996-2841 " Fax 836-996-0326 www.randelabs.com i CHAIN OF CUSTODY = Analytical Request Client Name: 0 �S e Address: Report .to: Phone: PO Number: Preserval Sample IdentificationIt TV A a,• U cc �' � M P 1 11w Ts- 7 "� c -1 t0'. rJ V1 y { WATER TECH LABS', INC, PO8OX,1056 GRANITE PALLS, NC' 2863.0 PHONE: (828) 396=44444 Project Name: Project Number: Requested Analyses pH Checked Upon Receipt 0I2 < 0.2.mg/l, U on: Recei t !� 47 j I Field Temp. (C°) Comments zs tik✓ 1'- 4 y "L 7, y 5„f ®���—�®MMMM®O® M Sample Condition Upon Receipt Relinquished By Company Date - Time Accepted By Company Date Time r r � i'�'i1®-'�k✓'�"/'...�"i ' L. III VIF NNW® Sampler Name and Signature Date Printed Naffne of Sampler's ' M 1 ' � F i r CHAIN OF CUSTODY -Analytical Request Client Name:(] Address: i Report to:: Phone: PO Number: A°11 WATER TECH LABS, INC. PO BOX 1056, GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: pH Checked Upon :12.< 0.2 rnnll I Innn v 'n c ;1 Sample Identification ti `'� w 0' A + �5 U U ai. M Q Field Temp. (C') Comments m a f► i-q:t 1 X1k, k It 11 low M } 2- x F x 114 Temperature (°G)' /a 1 Received on Ice: Y / N - Sealed Cooler. Y / N Samples lotact Y / N AdditionalComments: • - r . r . _ Printed Name of Sampler..rQ` ! 1$ y1q. Signature of Sarnpler, qufMirgy� UboRxtoRi s, 1rqc. Analyttcd/Procm ccimc,tfsmorss rnsruafs°c Chemical Anatysisfor Seleded Parameters and Water Sample ldMtffl-ed as Coats American A Water Tech Labs Ine. Pro ect colledEd 09 December 2014 I. Volatile Organics Quantitation EPA Method 8260 B Limit MW2 MW10 MwllR MW12 MWi3 MW14 Arwi3 Parameter j lob 1pgn �b j�n Ipp Acitone 25 BQL BQL SQL BQL BQL SQL BQL Acrolein 100 BQL BQL BQL BQL BQL BQL BQL Actyotvuile 100 BQL BQL BQL BQL BQL BQL BQL Bemene 0,s BQL BQL BQL BQL BQL BQL BQL Sromoheav= 0:3 BQL BQL BQL BQL BQL BQL BQL Bromochhrroamthane 0,5 BQL SQL BQL BQL BQL BQL BQL Bra modirNarontetbane 0.5 BQL BQL BQL BQL BQL BQL BQL Bromafonn 1.0 BQL BQL BQL BQL BQL BQL BQL Bronwaidhsne 1.0 SQL BQL BQL BQL BQL BQL BQL 2-Butaalono 25 BQL BQL BQL BQL BQL BQL BQL Carbon Disulfide 5.0 BQL BQL BQL BQL BQL BQL BQL Carbon Tettachlcride 0.5 BQL BQL BQL BQL BQL BQL BQL Chlmobeame 0;51 BQL BQL RQI BQL BQL SQL BQL CMoroetbaae 110 BQL BQL BQL :BQL. BQL BQL BQL 2-Clrloroetbyl viayl ether 5.0 BQL BQL BQL SQL BQL BQL BQL ( tilotnform 05" r= l0 i ` 3 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 2-Chlomtn�tene 0,5 BQL BQL BQL BQL BQL BQL BQL 4-CHozatoluene, 0.5' BQL BQL BQL BQL BQL BQL BQL Cis-1,2-11ahtoroethene PA BQL BQL BQL BQL BQL BQL BQL Chi-1,3-Vchloropropens 0.5 BQL BQL BQL- BQL BQL SQL BQL la-Dibromo-3-CWoxopmpcne(DBCP) 5.0 BQL BQL BQL SQL BQL BQL BQL 1,2Dibromedume (BDB) 0.5 BQL BQL BQL BQL BQL BQL BQL Dibromocblommetbana 03 BQL BQL BQL BQL BQL BQL BQL Dlbmmomethsno 03 BQL SQL BQL BQL BQL BQL BQL 1,2-Mclil robcnzena a's BQL BQL BQL BQL BQL SQL BQL 1.3-Dichlatoliemene U BQL B.QL BQL- BQL BQL BQL BQL 1;4-Dichlorobemene a's BQL BQL BQL BQL BQL BQL BQL 1,17Dichlareethaae Q5 BQL BQL SQL BQL BQL BQL BQL 1,2-Dichletoetbape 0:5 BQL BQL BQL SQL BQL BQL BQL M-Dicwtoethetae 0,3 IBQL BQL BQL BQL BQL BQL B.QL D chlarofoutomethane 0:3 BQL BQL BQL BQL BQL BQL BQL 1,2-131chtnuipuipane 0.5` BQL BQL BQL - BQL BQL BQL BQL 1,3-Dicblpropropano 0.5 BQL BQL BQL BQL BQL BQL, BQL 2,2-Dichkrbpiopano 0.5 SQL SQL SQL BQL BQL BQL BQL M-➢ichloropmpene 0:3 BQL BQL BQL BQL BQL BQL BQL Ethyl 'Bea mo 0.5, BQL BQL BQL BQL BQL BQL BQL 2-11exana w 5:6 BQL BQL BQL BQL BQL BQL BQL B!B . 0.3- BQL BQL BQL BQL BQL BQL BQL I-Propylbenzene 0.5 SQL BQL BQL BQL BQL BQL BQL 4 Methyl-2-Pa>itanone 5.0 BQL BQL BQL BQL BQL BQL BQL Methylltaiide 1.0 BQL BQL BQL BQL BQL BQL BQL *efticw Chloddat 5,0• BQL BQL BQL BQL BQL ;BQL BQL MTBB a, BQL BQL SQL SQL BQL BQL BQL Naphthalene 0.5 BQL BQL BQL BQL BQL BQL BQL M-Butyl iwane 0:5BQL BQL BQL BQL BQL BQL BQi N-Prarpy 0's BQL BQL BQL SQL SQL BQL BQL p-150propyitolueno 0.5: BQL -BQL BQL BQL BQL BQL BQL 3eo-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL SQL Styrene Ms BQL BQL BQL BQL BQL BQL SQL 'Geri-Butyibenzwe 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,1,24euaehloroetl 0.5 BQL BQL BQL BQL BQL BQL- BQL 1,1;2,2.Teirarlt wathsne a's BQL BQL BQL SQL BQL BQL BQL Tct=M'crottlime 0,5 BQL BQL BQL BQL BQL BQL BQL Toluene , 0.3 BQL BQL BQL BQL BQL BQL BQL Trans 1,2-IilChtolnetl o5 BQL . BQL; BQL BQL BQL BQL BQL Trans-0-Alcbloropropene 0S BQL BQL BQL BQL BQL BQL BQL Trans-1,4-Dicbiuro-2-butene 5,0 BQL BQL HQL BQL BQL BQL BQL 1.2,3-Ttiohlowbetnena 0:5 'SQL BQL BQL BQL BQL BQL• SQL 1,2,4-TiUblorobemem M SQL SQL BQL BQL BQL BQL. BQL 1112-Trkhloroetbaae 05 SQL BQL BQL BQL BQL SQL BQL 1,1,2-Triohlo'moae etb0:5 BQL BQL BQL BQL BQL SQL BQL Ti cb1ometbeue 0.5 BQL BQL, BQL BQL BQL BQL BQL Tdchlowntioniounhano 0.5- SQL BQL, BQ4';14" BQL BQL BQL BQL 1,2,3-Triottipropanc 0.5 SQL SQL BQL " BQL BQL BQL BQL 1;24.Ttitnethylhenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,3,5-Trimeithylbenzene, 0,5 BQL BQL BQL BQL BQL BQL BQL Vinyl ACerate 1.0 SQL BQL BQL BQL BQL. BQL. BQL. Vbtyl Ckbrlde, 0.5 SQL BQL BQL SQL BQL BQL BQL TouJXytmsa 1.0 BQL BQL BQL BQL BQL BQL SQL DilutionFaacr i Sample Number 901281 801282 A01283 801284 841285 801286 901287 SwupleDatte 12/09114 17109114 12f09114 12109h,l 12/09/14 12/091114 12109114 Sample Tune (bra) 0855 0900 0910 0916 0923 0930 1000 Aria" NM' NM NM 1w NM 23m NM DateAnalyzed12/16/14 12/16/I4 12/161/4 12/17/144 12117A4 12/17/14/2117/14 Time Anab med 2233 2305 2337 0009 0041 0113 0146 SarrogateRecovery Rant is DBFM (70-130%) ' 108% 104% 1 t I% 114% 111°la 107°!o l I4%a Toluene-dil (70-130%) 104% 980/0 111% 100% 103% 97% 97% 4=BFB (70-1300K) 93% 93% 960/o 960/6 99% 101% 101% BQL a BCkw Q.Mf ewtiM Limits ppb Q pact perr hcltiott POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALL. NORTH IAROLINA 28630 (828) 396-4444 SAMPLE.- Coats America (MW#16) PERMIT ff., ADDRESS: Coats America (Wells) P.O. Box 368 Marion, NC 28752 COLLECTION DATE: 12/9/2014 COLLECTION TIME: 10:00 RECEIVED DATE: 1-2/9/2014 RECEIVED TIME• 11:50 REPORTED: 12131120,14 LOG- ID: 1412-172 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab, 8upervisor SAMPLt-* Coats Amedca.(MW#14) COLLECTIONDATE: 121912014 PERMIT A: COLLECTION TIME: 09:30 ADDRESS: Coats America (Wells) RECEIVED DATE.* 12/9/2014 P.O. Box 368 RECEIVED TIME: 11:50 Marion, NC 28752 REPORTED: 12131/2014 LOG -1D.*' 1412-171 REPORTED BY: NC CERTIFIED LAB # 50 Ton'y Gragg, Lab Su-p'qryjS0r POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA 08. GRANITE FALLS, NORTH CAROLINA 28WO (828) 396-4444 SAMPLE: Coats America (MW#1 3) COLLECTION DATE: 12/9/2014 PERMIT A. COLLECTION TIME. 09:23 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/9/2014 P.O. Box 368 RECEIVED TIME: 11:50 Marion, NC 28752 REPORTED: 12/31/2014 ANAL YSIS, ANALYSIS PESULTS� --'-UNIT ----- ----- TDS 282 mg[L 12/10/14 lag Chloride <5.0 mg/L 12/16/14 lag T. Phosphorus 0.19 mg/L 12/22/14 jdg TOC see attached Sulfate see attached metals see attached pH 6.9 su's 12/9/14 lag Vods see attached LOG ID: 1412-170 REPORTED BY: NC CERTIFIED LAB # SO- fb� * Tony Gragg, Lab Supervisor POST'OFFICE BOX, 1056 PINEW000 PLAZA DR. GRANITE MLS. NORTH CAROLINA 2W30 (k8) 3964444 SAMPLE., Coats America (MW#1 2) COLLECTION DATE: 12/9/2014 PEIRMITA. COLLECTION TIME., 09:16 ADDRESS: Coats America (Wells) RECEIVED DATE., 12/9/2014 P.O. Box 368 Ma . rion, NC 28752 RECEIVED TIME., 1150 1 REPORTED: 12/31/2014 LOG ID: 14,12-169 PEPORTED BY: NC CERT1FIED LA13 # 50 T60y Gragg, Jab,Superivlsor q PO aTO/tj+pF/��Fpp'IpC ' arz [[4 �y� !�§ ply j }yy�4t€�yi[pEj�i`� OtO#�,Dy PLAZA p, DR. (828) 30&4444 SAMPLE: Goats America (MW#1.1,) COLLECTION DATE. 12/9/2014 PERMIT #: COLLECTION TIME 09:10 ;ADDRESS: Coats America (Wells) RECEIVED DATE.` 12/9/2014, P.Q. Box 368 RECEIVED TIME., 11:50 Marion, NO. 28752 REPORTED. 12/31 /20:14 TDS 216 mg/L 12110/14 lag. chloride 7.3 mg/L 12/16/14 tag T. Phosphorus 0.18 mg/L 12122/14 jdg TOC see attached' Sulfate see attached metals see attached OH 8.3 sWs 1279/14 tag voc's see attached 4��#S'''� � r :.�� ��,. 1'- � t '�.. "� "x �"n''�., � b +t-'�` '� �•'^�" a ",, r«- r `�a 'T n } �a� ".x �s .-4- m�, 4 }` i -`�-?s`�r ;1'� .., 4�, zI i�ZN ..R 1 MISS--, sus z .� �a ss ^•- "``.#."tax s `�, m fir: ar , € � tP �'� ` � '� e §� { ^ � . �*€ � � r �� �� LOG -ID 1412-168 REPORCEIi.BY: NC CERTIFIED LAB I# 5i Tony Gragg, Lab Supervisor MOTE C 0 LORS.inc. POST OFFICE BOX 1056 - #5 PfNEWOOD PLAZA DR. GRANITE FALLS; NORTH ' CAROLINA. 9,8630 (828) 396-4444 SAMPLE, 'Coats Ah,iOka (MW#1 0) PERMIT ADDRESS., Cdaits America (Wells) P.Q. PDX 36p Marion;, NC 287512 -COLLEGTIDNDATE: 12/9/2014 C,Q4LEQT10,N-.T,1ME.-. 09:00 RECEIVEUDATE- 12/9/2014 RECEIVED 77ME,." 11 :50 REPORTED: 12/3112014 7A4, M. TOAY"Grag& La b, Slpoorvisor MCH LONSinc, yr POST OFFICE BOX 1056. - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (824) 3964444 ,.SAMPLE., Coats Amedca (MW#02) COLLECTION DATE: 12/9/2014 PERMITM COLLECTION TIME., 08:55 ADDRESS: Coats America (Wells' RECEIVED DATE., 12/9/2014 P.O. Box,368 RECEIVED TIME. 11:50 'Marion, NC 28752 TDS 108 mg/L 12110/14 lag Chloride 9.8 mgiL 12116/14 lag T. Phosphorus 0.41 mg/L 12122/14 -jd§ TOC see attached, Sulfate gee attached metals see attached PH su's 12/9/14 lag tee attached LOG Q 1412-166 REPORTED BY' NC CERTIFIED LAB .50 Uny GfuggjLab Supervisor GW;-59A COMPLIANCE REPORT FORM Permit # WQ0005603 (Submir one each monitoring perlod with 0b-59 forms.) i 1 Enter.dte monitoring resuits were due. { 9/30/14 1 Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? X 2 Was any•required information missing on the GW-59 report forms? YES NO IF the all to question 9 or 2 is YES ; list in the space provided below the wel; identification number(s) and explain the problems encountered in obtaining the required information. i ! ; 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, tmJDeked or missing cap, missing YES NO identifications plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO if the an wer to question 4 is NO°, skip to section 8. If the an, ever to question 4 is "YES" list the affected wells individually with consdtuent(s) and concentration(s) , exceedin'Rstandards in the space provided below. MW #121 TDS 680 mg/I MW #13 TDS 561 mg/I MW #2 Total Lead 0.050 mgJl Manganese 4.56 mg/I Manganese 1.23 mg/1 1 I 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same co�tstituent(s) in the same well(s) in the last two years? x If the answer to question 5 is 'NO", skip to section 8, If the answer to question 5 is "YES'; list in the space provided below, each well with constituent(s) exceeding standard$, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW #2 jLead 0.59 mg/1 April 2014 MW #12 TDS 587 mg/I April 2014 I:Manganese 1.44 mg/I April 2014 TD5 654 mg/ April 013 Manganese 4.19 April 2014 ;Manganese 1.38 mg/1 August 2013 TDS 590 mg/I August 2013 Manganese 85 m Jl Ap i Manganese 4.06 mg/I August 2013 2 6 Are the ronitoring wells listed in section 5 located at or beyond the review boundary? YES NO x If the an wer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE.IMMEDiATELY FOR GUIDANCE. If the answer is "NO". monitoring. wells maybe improperly located; ontact the Regional Office. i 7 Is the pernmittee implementing previously approved actions required by the Division• involving this YES NO groundwater quality problem? if the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7is "NO", contact the Regional Office within 90 days, • an evaluation maybe required %o determine the Impact the waste disposal.system is havin at the retj etG-andxofri' lFai%i boundaries surrounding this facility. Fallure to do so may subiect the permittb(iE&•a-Nbtill of io tion fines, and/or penalties. SEP 16'2014 ii �C�)!7%^.p`l 'l'.j p:% ji �: g The person completing this portion (GW-59A) of -the monitoring report should sign below and submit this form with; G W-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 1 hereby aicknowiedge that thewabove Info�matlon was eye uaf?dtand the lnformafTon sub tied w"th�is mow@ sieport,;(Cmp13e, Redport GW 59A) lsitrue a d complete to the best of my,krxowledge,,xrr _..' . .. ,.,...._, J 9/11/14 E;g fED Signature of Permitte ' orAuthorized Agent) Date RE Division cfWater lesout f :es SEP 2 2 2014 GW-$9A 12/8/2003 Water Quality Regional Operations Asheville Regional Office SUBMIT FORM ON YELLOW: PAPER. ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Facility Name: COATS AMERICAN Permit Name (if different): Facility Address' 630 AMERICAN THREAD RD MARION (SUceq NC 28752 McDOWELL COUr1t (sine) (�) Contact Person: PHILLIP PITTMAN Telephone 0: 828a56=4111 SEVIER BACKGROUND Well Location/ Site Name: No. of Wells to be Sampled: 7 . Well Identification Number (from Permit): MW #z Foi Groundwater Treatmeni Systems Well Depth: 75 ft. Well Diameter-.,6 in• Check One: ❑ In (98) Screened Interval: N/A ft. to N/A ft. 0 Depth to Water Level: 35.4 ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevation.in ft.: Gallons of water pumped/bailed before sampling: 67 Date sample collected: 8-14-14 Field analysis: pH _ 6 91 Specific Conductance uMhos Temp. 15.8 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION,. GROUNDWATER SECTION 163E MAIL.SERVICE CENTER F'tRtViIT #: w40005603 EXPIRATION DATE: Non=Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X . Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 50 PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P8/25 0.31 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate m/I g Dissolved Solids: Total 8/15 110 mg/I Al - Aluminum 8/22 3.54 TOCw 8/ 6 analyzed) $/14 7.9 units Ba - Barium 8/22 n 16a ml g/ <1.0 mg/I Ca - Calcium 8/22 �a' mg/I Chloride 8/22' 7.25 mg/I 8zz Cd - Cadmium / <o 002 Mg/I Arsenic _8/22 0.007 mg/l Chromium: Total 8/22 <0.005 Rj l Grease and Oils mg/I Cu - Copper mg/1 Phenol mg/I Fe - Iron mg/I Sulfate 8/22 12.0 mg/I Hg -Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 8/22 20.1 mg/I TKN as N mg/l Mn - Manganese 8/22 1.23 mg/1 YES NO) Ni - Nickel_8122 0.012 mg/I Pb - Lead. 8/22 0.050 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) _ SELENIUM 8/22 <0.005mg/I SODIUM 8/22 12.9 mg/I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes . (1) No . (0) VOC method # = method ii = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING - COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: COATSAMERICAN Permit Name (if different): Facility Address: 630 AMERICAN THREAD RD I5ueeq MARION NC 28752 County McDO WELL (Chy)• Iswb) (Twl PHI PITTMAN 828-156-4111 Contact Person; Telephone #: Well Location/MW 10/ASH POND 7 Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): Mwttlo `For Groundwater Treatment Systems Well Depth: 18 it. Well Diameter•. 2 in. Check One: ❑ Influent (98) Screened Interval: NIA ft. to N/A ft. 0 Effluent 99 Depth to Water Level: 15.3 ft. below measuring point. ) Measuring Point (M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: Date sample collected: 8-14-14 Field analysis: pH _ 6•44 , Specific Conductance uMhas . Temp. 16.0 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION. -GROUNDWATER SECTION .PERMIT #: WQ0005603 EXPIRATION DATE: Non -Discharge UIC NPDES .TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rofary Distributor Land Application of Sludge Other, NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATERTECH Certification No. 50 PARAMETERS (Samples for metals were collected unfiltered X YES NO 'and field acidified COD mg/I Nitrite (NO2) as N mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P B/2s <0.16 mg/I (Note; Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 8/11 179 mg/I Al -Aluminum 8/22 . 0.060 mg/I pH (when analyzed) 8/14 6i0 units Ba -Barium 8/zz o.00s mg/1 TOC mg/I Ca - Calcium 8/22 �s01i mg/I Chloride 8/22' <5.0 mg/I Cd - Cadmium 8/22 <0.o02 mg/I Arsenic 8/22 <0.005 mg/l Chromium: Total 8/22 <0.005 mg/l Grease and Oils mg/l Cu - Copper mg/I Phenol mg/l Fe - Iron mg/I Sulfate 8/22 49•1 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 8/22 <0.500 mg/l TKN as N trig/I Mn - Manganese 8/22 <0.005 mg/I GW-59 Rev. 0372000 YES NO) Ni - Nickel_ 8/22 <0.005 mg/I Pb - Lead 8/22 <0.00s mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SELENIUM 8122 <0.005mg/I SODIUM 8/22 71.0 mg/I ORGANICS: (GC,GCIMS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes . (1) No (0) VOC : method # = method # = - rilethod'# SUBMIT F6RM ON YELL W.PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: COATS AMERICAN Permit Name (if different): MARION "-" NC 28752 County McDOWELL is+rJ PHILLIP:PITTMAPI�awt lzw) 828-756-4111 Contact Person: Telephone #: Well Location/ Site Name: MW 11R/ASH POND No. of Wells to be Sampled: 7 Ilrom Permit Well Identiiication Number from Permit: MW #11R ( ) For Groundwater Treatment'SysCelms Well Depth: 30 it. Well Diameter 2 in. Check One: ❑ Influent (9$) Screened Interval: N/A it. to _N/A . it. 0 Effluent (99) Depth to Water Level: 7.7 it. below measuring point. Measuring Point (M.P.) is: 2 ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: 8/14/14 Field analysis: pH 7•88 , Specific Conductance Umhos . Temp. 17.5 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT A NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1536: MAIL SERVICE CENTER .PERMIT #: WQ0005603 EXPIRATION DATE: Nori-Discharge UIC NODES 'TYPE OF PERMITTED OPERATION BEING MONITORED _X _ Lagoon Remediation: infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 50 PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 8/25 0.17 .mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 8/15 224 mg/I Al - Aluminum 8/22 0.574 mg/l phi (when analyzed) 8/14 8.0 units Ba - Barium s/22 0.044 mg/I TOO 8 26 1.25 mg/I Ca - Calcium 8/22 _42.6 mg/I Chloride 8/22 <5.0 mg/I Cd - Cadmium 8/22 <0,002 mg/I Arsenic 8/22 a5 <0.0mg/I Chromium: Total 8/22 <0.005 mg/1 Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/l Sulfate 8/22 34.4 mg/l Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/l Total Ammonia mg/1 Mg - Magnesium 8/22 23.6 mg/l TKN as N Tng/1 Mn -Manganese 8/22 <0.005 mg/I YES NO) Ni - Nickel 8/22 <0.005 mg/I Pb - Lead 8/22 <0.005 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/i Other (Specify Compounds and Concentration Units) SELENIUM 8/22 <0.005 mg I SODIUM 8/22 16.7 mg/I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = :.-method-# _._.._.__..__..___...__....._... SUBMIT FORM ON QW PAPER ONLY I - DEPARTMENT OF ENVIRONMENT 6 NATURALRESOURCES GROUNDWATER QUALITY MONITORING: WATER QUALITY DIVISION, GROUNDWATER SECTION 1616 MAIL:SERVICE CENTER COMPLIANCE REPORT FORM Rol Kir;u .Mr 97AGG-19olp 1010%799_979, Facility Name: COATS AMERICAN Permit Name (if different): Facility Address: 630 AMERICAN THREAD RD 28752 tC°Yt PHILLIP PITTMAI�"�t (ZIP)Contact Person: Well Location/ Site Name: MW 12/EFFLUENT Print Clearly or'Type County McuuvvtLL Telephone #: 828-756-4111 No. of Wells to be Sampled: 7 07— moll Well Identification Number (from Permit): MW #12 For Groundwater Treat'menl Systems Well Depth: 13 ft. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: N/A ft. to N/A ft. Effluent (99) Depth to Water Level: 10.1 it. below measuring point. Measuring Point (M.P.) is: 2.6 ft. above land surface. Relative M.P. Elevation in ft.' Gallons of water pumped/bailed before sampling: 1 Date sample collected: 8/14/14 Field analysis: pH 6.67 , Specific Conductance Umhos Temp. 17.7 °C, Odor Appearance PERMIT #: WQ0005603 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon Remediation: Infiltration Gallery Spray Feld Remediation: Rotary Distributor —Land Application of Sludge - Other. NOTE: Values should reflect dissolved and. colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 5o PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal 1100ml Nitrate (NO3) as N mgll Coliform: MF Total /100ml Phosphorus: Total as P Ms 0.24 mg/I (Note:.Use MPN method for highly turbid samples) Orthophosphate mg/1 Dissolved Solids: Total 8/15 680 ntgA Al - Aluminum 8/22 0.135 mg/I pH (when analyzed) 8/14 6.8 units Ba - Barium 8/22 0.205 mg/1 TOC 8/26 1,94. mg/I Ca - Calcium 8/22 111 mg/I Chloride 8/22 ' <5.0 mg/I Cd - Cadmium 8/22 <0.002 mg/1 Afsenic 8/22 <n.n05 mg/I Chromium: Total. 8/22 <0.005 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 8/22 <10 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg%l Mg - Magnesium 8/22 18.8 mg/( TKN as N mg/I Mn - Manganese 8/22 4.56 mg/l GW-59 Rev, 03/2000 YES NO) Ni - Nickel 8/2a 0.010 mg/I Pb - Lead 9/22 <0.005 mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds.and Concentration Units) SELENIUM 8/22 <0.005 mg/1 SOnluM 8122 111 mg/I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC_ : method # = method # = 9/11/14 SUBMIT FORM ON YELLOW PAPER ONLY , GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print clearly or Type Facility. Name: COATS AMERICAN Permit Name (if different): s (ueeq ,MAR ON NC 28752 County. McDOWELL, (city)' PHILLIPRITTMAW''°) trro) 828-756-4111 Contact Person: Telephone.#: Well Location/ Site Name: MW 13/INFLUENT No. of Wells to be Sampled:. Well Identification Number (from Permit): rviw IT IS For Groundwater Treatment Systems Well Depth: 15 it. Well Diameter: 2 in.: Check One: ❑ lnfiuent (98) Screened Interval: N/A it. to N/A fL 0 Effluent (99) Depth to Water Level: 11.2 ft. below measuring point. Measuring Point (M.P.) is: 2.6 it. above land surface. Relative M.P. Elevation.in ft.: Gallons of water pumped/bailed before sampling: 1 Date sample collected: 8/14/14 Field analysis: pH 6.12 . , Specific Conductance uMhos Temp. 17.5 QC, Odor Appearance ENVIRONMENT & NATURAL RESOURCES DIVISION, GROUNDWATER SECTION :E CENTER PERNIIT #: WQ00056021 EXPIRATION DATE: Non -Discharge UIC NRDES TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon Remediation: Infiltration Gallery Spray Feld -Remediation: Rolary Distributor Land Application of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 50 PARAMETERS (Samples for metals were coilected unfiltered X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phosphorus: Total as P 8/25 0.67 mg/I (Note: Use MIPN method for highly turbid samples) Orthophosphate mg/1 Dissolved Solids: Total 8/15 561 mg/I Al - Aluminum 8/22 0.1.95 mg/l pH (when analyzed) 8114 6.3 units Ba - Barium 8122 0.112 mg/I TOC 8/26 2.58 mg/I Ca - Calcium 8/22 33.6 mg/I Chloride 8/22 ' . e.75 mg/I Cd - Cadmium 8122 <0.002 mg/l Arsenic 8122 <0.005 mg/I Chromium: Total 8/22 <0.005 mg/1 Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron. mg/l Sulfate J22 <.10 mg/I Hg -. Mercury mg/1 Specific Conductance uMhos K - Potassium mg/l Total Ammonia mg/1 Mg : Magnesium 8/22 . 22.2 mg/l TKN as N mg/I Mn - Manganese 8/22 0.753 mg/l YES NO) Ni - Nickel 8/22 <0.005 mg/I Pb - Lead 8/22 <0.005 mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SELENIUM 8122 <0.005 m01 SODIUM 8/22 144 mg/I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method C Attach lab report.) Report Attached? Yes -(I) No (0) VOC method #,= method # = ,rluv. ualeuuu SUBMIT FORM ON YELLOW PAPER.ONLY DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: WATER QUALITY DIVISION,. GROUNDWATER SECTION .1634 MAIL SERVICE CENTER COMPLIANCE REPORT FORM :'Rat F(r-i .Nf 97aao-Into oh. . 10,0%799_9991 Please Print Clearly or Type Facility dame: COATS AMERICAN Permit Name (if different): Facility Address: 630 AMERICAN THREAD RD (Sireaq MARION . NC _ 28752 County McDOWELL liar) PHILLIP PITTMANIs"10) lro) Contact Person: Telephone#: 828-756 4111 Well Location/ Site Name: MW 14/AERATION No. of Wells to be Sampled: 7 .. trom Permlq ; Well Identification Number (from Permit): MW #14 For Groundwater Treatment Systems Well Depth: 15 ft. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: NIA ft. to N/A ft. 1 ❑ Effluent (99) Depth to Water Level: 7.5 ft. below measuring point: Measuring Point (M.P.) is: 2.6 ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: 8/i4/14 Field analysis: pH 6.44 , Specific Conductance . ' -uMhos Temp. 16.8 aC, Odor Appearance PERMIT #: WCQ0005603 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED. OPERATION BEING MONITORED X Lagoon Remediation: Infiltration Gallery Spray Feld Remediation: Rotary Distributor _Land Application of Sludge Other. NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. so PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified COD ,mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 8/25 0.28 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 8/15 405. rng/l Al -Aluminum 8/22 0.464 mg/l pH (when analyzed) s/14 6.7 units Ba - Barium 8/22 0.132 mg/I TOC 8/26 2.93 mg/I Ca - Calcium 8/22 64.4 mg/I Chloride 8/22' . <s.0. mg/I Cd - Cadmium 8/22 <0.002 mg/I Arsenic s/z2 <0.005 mg/I Chromium: Total 8/22 <0.005 mg/I Grease and Oils mg/I. Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate. 8/22 <10 mg/l Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/1 Mg -Magnesium 8/22 38.4 mg/l TKN as N mg/I . Mn - Manganese 8/22 0.997 mg/l GW-59 Rev. 0312000 YES NO) Ni - Nickel 8/22 <0.005 mg/I Pb - Lead 8/22 <0.005 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SELENIUM 8/22 <0.005 mg/I _ SODIUM 8/22 35.7 me ORGANICS: (GC,GC/MS,HPLC) - (Specify test and method #. Attach lab report.) Report Attached? Yes —(I) No (0) VOC method # = method # = ___._.._.....�..._._...__.__-____..method..ly=-­_.....,..._..__ �....___,.._.... _. SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATE13 QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: COATS AMERICAN Permit Name (if different): Facility Address: 630 AMERICAN THREAD RD MARION tsuee�l NC 28752 County McDOWELL. Icily( PHILLIP PITTMAR"' (zip) Contact Person: Telephone #: 828-756-4111 Well Location/ Site Name: MW WASH POND No. of Wells to be Sampled: 7 from Pe Q Well Identification Number (from Permit): Mw#15 : For Groundwater Treatment'Systems Well Depth: 16 it. Well Diameter: 2 in. Check One: 0 Influent (98) Screened Interval: N/A ft. to N/A. fL 13 Effluent (99) Depth to Water Level: 9.2 ft below measuring point. Measuring Point (M.P.) iss_2.iz ft. above land surface. Relative M.P. Elevation.in ft.: Gallons of water pumped/bailed before sampling: 1 Date sample collected: 8/14/14 Field analysis: pH 6.37 Specific Conductance uMhos Temp. 18.1 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636.MAIL SERVICE CENTER #f: WQ0005603 EXPIRATION DATE: NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X. Lagoon Remediation: Infiltration Gallery Spray -Field Remediation: Rotary Distributor Land Application of Sludge Other.__ NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE BELOW Laboratory Name: WATER TECH Certification No. 50 PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified . YES NO) COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel 8/22 <0.005 mg/I Coliform: MF Fecal /1 OOml Nitrate (NO3) as N mg/I Pb - Lead 8/22 <0.005 mg/I Coliform: MF Total /100ml Phosphorus: Total as P 8/25 <0.16 mg/I Zn - Zinc . mg/1 (Note: Use MPN method for highly turbid samples) Orthophosphate mg/1 Ammonia Nitrogen mg/I Dissolved Solids: Total 8/15 364, Mg/I Al - Aluminum 8/22 0.056 mg/I Other (Specify Compounds and Concentration Units) pH (when analyzed)_ 8114 6.6 units Ba -Barium 8/22 0.126 mgA -J OC 8/26 1.82 mg/I Ca - Calcium 8/22 85.9 mg/I SELENIUM 8/22.' <0.005 mg/1 Chloride 8/22 <5.0 mg/I Cd - Cadmium 8/27 <0,002 mg/I SODIUM 8/22 10.9 mg/I Arsenic 8/22 <0.005 mg/I Chromium: Total 8/22 <0.005 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC) Sulfate 8/22 <10 mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report.) Specific. Conductance uMhos K - Potassium mg/I Report Attached? Yes (1) No (0) Total Ammonia mg/I Mg - Magnesium 8/22 36.6 mg/I VOC method # - TKN. as N rIg/I Mn - Manganese 8/22 0.781 mg/I method # = GW-59 Rev. 03/2000 ldfiTERiTECH iLRDS./tic., POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE. Coats America (MW#02) PERMIT A ADDRESS: Coats America (Wells) P.O. Box 368 Marion, NC 28752 ' ANA.YSJ i9NALY IS ., :.'I SULTS' ;UNITS:' TDS 110 mg/L Chloride 7.25 mg/L T. Phosphorus 0.31 mg1L TOO <1.0 mg/L Sulfate 12.0 mg/L metals see attached pH 7.9 su's COLLECTION DATE: 8/14/2014 COLLECTION TIME: 08:45 RECEIVED DATE: 8/14/2014 RECEIVED TIME., 15:00 REPORTED: 9/5/2014 8114/14 leg LOG 10: 1408-215 REPORTED BY: NC CERTIFIED LAB # 50 fv�- Tony Gragg, Lab Supervisor IdRrERe rjFCH L11e5.l c. POST OFFICE BOX 1056 a #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#10) COLLECTION DATE. 8/14/2014 PERMIT#. COLLECTION TIME. •08:55 ADDRESS: Coats America (Wells) RECEIVED DATE: 811412014 P.O. Box 368 RECEIVED TIME., 15:00 Marion, NC 28752 REPORTED. 9/5/2014 ANA :Y-8-1S .... l E5Ul:7S. ' : 1IV1 5:;:...:. oA-TE .. .. : A1VtliYS7 ,. TDS 179 mg/L 8/15/14 lag Chloride <5.0 mg/L 8/22/14 lag T. Phosphorus <0.16 mg/L 8/25/14 Jdg TOC <1.0 mg/L 8/26/14 Sulfate 49.1 mg/L 8/22114 metals see attached pH 6.9 su's 8/14/14 lag 7 LOG ID: 1408-216 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor URrEfF rECH LRDS.1nc. POST OFFICE BOX 1056 • I15 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (820) 396-4444 SAMPLE: Coats America (MW#11) COLLECTION DATE: 8/14/2014 PERMIT A COLLECTION TIME., 09:10 ADDRESS: Coats America (Wells) RECEIVED DATE., 8/14/2014 P.O. Box 368 RECEIVED TIME., 15:00 Marion, NC 28752 REPORTED: 9/5/2014 r '5.:. ANA �'StS .`. ;`. RESULTS ., IJIVI S . :..DATE Af�fA�.�'ST .: . TDS 224 mg/L 8/15114 lag Chloride <5.0 mg/L 6122/14 lag T. Phosphorus 0.17 mg/L 8125/14 1dg TOC 1.25 mg/L 8/26/14 Sulfate 34.4 mg/L 8122/14 metals see attached pH 8.0 su's 8/14/14 lag LOG ID: 1408-217 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor 1dRTKR rcCH LRDS.lnc. POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 8/14/2014 PERMITA' COLLECTION TIME: 09:25 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2014 P.O. Box 368 RECEIVED TIME., 15:00 Marion, NC 28752 REPORTED: 9/5/2014 ANA4Y-SIS RESULTS LINTS - AN, IYST TDS 680 mg/L 8/15/14 lag Chloride <5.0 mg/L 8/22114 lag T. Phosphorus 0.24 mg/L 8/25114 1d9 TOC 1.94 mg/L 8/26/14 Sulfate <10 mg/L 8/22114 metals see attached pH 6.8 su's 8/14114 lag LOG ID: 1408-218 REPORTED BY: NC CERTIFIED LAB # 50 f�600 Tony Gragg, Lab Supervisor 'KCH L.RDS-inc. POST OFFICE BOX i05B • ,#5 PINEWOOD PLAZA0H. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396.4444 SAMPLE: Coats America (MW#13) COLLECTION DATE: -8/14/2014 PERMIT A COLLECTION TIME: 09:35 ADDRESS: Coats America (Wells) RECEIVED DATE: 811412014 P.O. Box 368 RECEIVED TIME: 15:00 Marlon, NC 28752 REPORTED: 9/5/2014 iVAi- y ' RE%kTS UNITS l A?"1= ANALYST. . TDS 561 mg/L 8/15/14 lag Chloride 9.75 mg/L 8/22/14 lag T. Phosphorus 0.67 mg/L• 8/25/14 Idg TOC 2.58 mg/L. 8/20/14 Sulfate <10 mg/L 8/22/14 metals see attached pH 6.3 su's 8/14/14 lag LOG ID: 1408-219 REPORTED BY: NC CERTIFIED LAB # 50 f�* Tony Gmgg, Lab Supervisor ii j rff jq rvCH L1185.1nc- POST OFFICE BOX 1056 • 95 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (825) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE., 8/14/2014 PERMIT #: COLLECTION TIME: 09:45 ADDRESS: Coats America ,(Wells) RECEIVED DATE: 8/14/2014 P.O. Box 368 RECEIVED TIME. 15:00 Marion, NC 28752 _ REPORTED- 9/5/2014 :.AM ANAL YtIS RESULTS :. UNIT- DA7-,E� ... ANALYST TDS 405 mg/L 8115/14 lag Chloride <5.0 mg/L 6/22/14 lag T. Phosphorus 0.28 mg/L 8/25/14 Idg TOC 2.93 mg/L 8/26114 Sulfate 410 mg/L 8/22/14 metals see attached pH 6.7 su's 8/14114 lag LOG ID: 1408-220 REPORTED BY: NC CERTIFIED LAB # 5 Tony Gragg, Lab Supervisor 1dfirKjR4TffCH L1185-inc, POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH GAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 8/14/2014 PERMIT #: COLLECTION TIME: 09:55 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2014 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 9/5/2014 ,4N,4.LYSI ` ...1 Stl�TS.. UNIT-9 DAIrE <AIVALYSr TDS 364 mg1L 6/15114 lag Chloride <5.0 mg/L 8122/14 lag T. Phosphorus <0.16 mg1L 8t25/14 )dg TOC 1.82 mg/L 8/26/14 Sulfate <10 mg/L 8/22/14 metals see attached pH 6.6 su's 8/14114 lag LOG ID: 1408-221 REPORTED BY: NC CERTIFIED LAB # 50 fll� Tony Gragg, Lab Supervisor RESf:ARCh & ANALYTICAL' L boRAToRics' INC. AnalyHcal/Process Consultations August 27, 2014 Water Tech Labs P.O. Box 1056 Granite Falls, NC 28630 Attention: Joe Gragg Project Name: Coats American I: Miscellaneous MW2 MW10 MW11R MW12 MW13 MW14 MW15 Date Parameters unit Results Results Results Results Results Results Results Analyzed TOC mg/I. <1.0 <1.0 115 1.94 2.58 2.93 1.82 08/26/14 Sample Number 792536 792537 792538 792539 792540 792541 792542 Sample Date 08/14/14 08/14/14 08/14/14 08/14/14 08/14/14 08/14/14 08/14/14 Sample Time 0845 0855 0910 0925 0935 0945 0955 mgf L = milligrams per I iter =parts per million (ppm) < = Less than or below detection limit �'++�rrllrl/dt�t RESEARCh & ANALyTiCA1 LABORATORIES, INC. Analytical/Process Consultations » 's W.- ZED Water Tech Labs. Inc. Date Sample Collected 08/14/14 P.O. Box 1056 Date Sample Received 08/22/14 Granite Falls, NC 28630 Date Sample Analyzed 08/22/14 Attn: Joe Gragg Date of Report 09/02/14 Analyses Performed by AA -KL Lab Sample Number -------------------- 793163 Parameter ^�^^-Storet # Results Magnesium,Tot (00927) 20,1 mg/1 Lead,Tot (01051) 0.050 mg/1 Manganese,Tot (01055) 1.23 mg/1 Aluminum,Tot (01165) 3.54 mg/1 Calcium,Tot (00916) 34.7 mg/l Chromium,Tot. (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) 0.012 mg/l Sodium,Tot (00929) 12.9 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0,164 mg/l Arsenic,Tot (01002) 0.007 mg/l Sulfate (00945) 12.0 mg/1 Clients Sample Source Number Time Collected (Hrs) -------------------- MW2 COATS 0845 P.O, Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com ANAty RESEARCh & ANA[YTICA1 .•••"""'•••• '�. pry ` LAbORATORiES INC. owl4 N0#34 Z' Analytical/Process Consultations li Water Tech Labs. Inc. Date Sample Collected 08/14/14 P.O. Box 1056 bate Sample Received 08/22/14 Granite Falls, NC 28630 Date Sample Analyzed 08/22/14 Attn: Joe Gragg Date of Report 09/02/14. Analyses Performed by AA -KL Lab Sample Number -------------------- 793164 Parameter T Storet # Results Magnesium,Tot (00927) <0.500 mg/l Lead,Tot (01051) <0.005 mg/l Manganeae,Tot (01055) <0.005 mg/1 Aluminum,Tot (01105) 0.060 mg/1 Calcium,Tot (00916) <0.500 mg/l Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 71.0 mg/1 Selenium,Tot (01147) <0.005 mg/l Barium,Tot (02007) 0,005 mg/l Arsenic,Tot (01002) <0.005 mg/1 Sulfate (00945) 49.1 mg/l -------------------- Clients Sample Source MW10 Number COATS Time Collected (Hrs) 0855 I P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-986-0326 www,randslabs.com a�3 { RESEARCh & ANALyTICA[ f a LAbORATORIE5, INC.. Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected 08/14/14 P.O. Box 105.6 Date Sample Received 08/22/14 Granite Falls, NC 28630 Date Sample Analyzed ; 08/22/14 Attn: Joe Gragg Date of Report 09/02/14 Analyses Performed by AA -KL Lab Sample Number -------------------- 793165 Parameter^-^^ Storet # Results Magnesium,Tot (00927) 23.6 mg/1 Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) <0.005 mg/l A1uminum,Tot (01105) 0,574 mg/l Calcium,Tot (00916) 42.6 mg/l Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 16.7 mg/l Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.044 mg/l Arsenic,Tot (01002) <0.005 mg/l Sulfate (00945) 34.4 mg/1 Clients Sample Source Number Time Collected (Hrs) -------------------- 'MW11R COATS 0910 P 0, Box 473 • 106 Short Street - Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com +��4�«urrrr�ri RESEARCh & ANALyTICAB C r LAbORATORVS, INC. {MeOR � y� Analytical/Process Consultations �1'+ NED MARV -W, Water Tech Labs. Inc. Date Sample Collected OB/14/14 P.O. Box 1056 Date Sample Received 08/22/14 Granite Falls, NC 28630 Date Sample Analyzed 08/22/14 Attn: Joe Gragg Date of Report 09/02/14 Analyses Performed by AA -KL Lab Sample Number -------------------- 793166 Parameter Storet # Results Magnesium,Tot (00927) 18.8 mg/1 Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (`01055) 4,56 mg/1 Aluminum,Tot (01105) 0.135 mg/l Calcium,Tot (00916) ill mg/1 Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) 0,010 mg/1 Sodium,Tot (00929) 111 mg/1 Selenium,Tot (01147) c0.005 mg/1 Barium,Tot (0 10 07) 0.205 mg/1 Arsenic,Tot (01002) <0.005 mg/l. Sulfate (00945) <10 mg/1 'Clients Sample Source Number Time Collected (Hrs) --------------- MW12 COATS 0925 P.O. Box 473 • 106 Short Street - Kernersville, North Carolina 272a4 336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCh & ANA1yTICA1 ••', �'�&.......,,, � ''� - LAbORATORIES, INC. t. to NC Z. Analytical/Process Consultations + �,..0,� Water Tech Labs. Tnc. Date Sample Collected 08/14/14 08/22/14 P.O. Box 1056 Date Sample Received Date Sample Analyzed 08/22/14 Granite Falls, NC 28630 Date of Report 09/02/14 Attn: Joe Gragg Analyses Performed by AA -KL Lab Sample Number 793168 Parameter y r�Storet #^ `w Results Magnesium,Tot (00927) 38.4 mg/1 Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 0,997 mg/l Aluminum,Tot (01105) 0.464 mg/1 Calcium,TOt (00916) 64.4 mg/l Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) e0.002 mg/1 Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 35.7 mg/l Selenium,Tot (0`1147) <0.005 mg/l Barium,Tot (01007) 0,132 mg/l Arsenic,Tot (01002) <0.005 mg/1. Sulfate (00945) <10 mg/l Clients Sample Source Number Time Collected (Hrs) -------------------- MW14 COATS 0945 P. 0. Box 473 1 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-D326 www,rBndatabs.com �'���{{1111111II r RESEARch & ANAiyTICA1 i4 r0��.� ,......� ,,,!/., +o A ' LAbORATORIES, INC. o ; NCB �_ ., "- Analytical/Process Consultations +� G `d/R�ZO�; Water Tech. Labs. Inc. Date Sample Collected : 08/14/14 P.O. Box 1056 Date Sample Received : 08/22/14 Granite Falls, NC 28630 Date Sample Analyzed 08/22/14 At Joe Gragg Date of Report : 09/02/14 Analyses Performed by : AA -KL Lab sample Number -------------------- 793169 Parameter Storet # Results Magnesium,Tot (00927) 36.6 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (03.055) 0.781 mg/l Aluminum,Tot (01105) 0.056 mg/l Calcium,Tot (00916) 85.9 mg/1 Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 10.9 mg/l Selenium,Tot (01147) <0,005 mg/1 Barium,Tot (01007) 0.126 mg/l Arsenic,Tot (02002) <0.005 mg/1 Sulfate (00945) <10 mg/l Clients Sample Source Number Time Collected (Hrs) -------------------- MW15 COATS 0955 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27264 • 336-996-2841 • Fax 336-996-0326 www.randalabs,00m rcx O, kal, ; it tvko,4 ol mt14 1 z (8011l'v 1"lf!, �%.uj ftl, 1 o,and -l- aw'd rat-,,qvTtei t?-"qs,iq ,� i;2�i-I I Iqmov"a DC)iln�;Iy i� M rr!�%uti, I z! i tuj is-vlf I! 5e I I 'n a I awif I vvv=O7a L.11M LIA-INUE JKEPORT FORM Permit # L)g 0,6 (Submit one each monitoring period with GW=59 forms.) 1 Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) be. submitted after the established due date? YES NO 2 Was any required information missing on the GW-59 report forms? YES NO iF the answer to question 1 or 2 is 'YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Y'es ", contact the Regional Once for guidance. YES NO 4 Are any monitored constituents equal to or above the established standards? YE NO If the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO if the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Vioiation fines, and/or penalties. g The person completing this portion (GW--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 hereby acknowledge thafthe above Information was evaluated and the ]nfocirtiation submitted�n#hls ,tin report..(Complta Repgrf rGW9A) Is true and comple4e to it►e best ofkrnowledge �/_ - _. OPP Signat of Permitte rAuthorized Agent) Date j GW-59A 12/8/2003 GW 59-A COMPLIANCE REPORT FORM ANSWER TO QUESTION #4 MW #2 LEAD O.OS9 MG/L MANGANESE 1.44 MG/L NICKEL 0.016 MG/L MW #12 TDS S87 MG/L MANGANESE 4.19 MG/L ANSWER TO QUESTION #5 MW #2 MANGANESE 1.38 MG/L (AUGUST 2013) MW #12 TDS S90 MG/L- (AUGUST 2013) MANGANESE 4.06 MG/L (AUGUST 2013) TDS 6S4 MG/L (APRIL 2013) MANGANESE 2.85 MG/L (APRIL 3013) GROUNDWATER QUALITY MONIT COMPLIANCE REPORT FORM FACILITY INFORMATION Facility Name: `-Lt - . Permit Name (if different): - Facility Address: Contact Person: ' l It I t Well Location/ Site Name: SUBMIL �g ON YE 61s 6� F43`�t`u N Ga+`��Si°° " 201Q Please PrAVbleaay or Type Telephone #:5s-i7 Flo -Lj I I I No. of Wells to be, Sampled: _ Well Identification Number (from Permit): & - Well Depth: 9 For Groundwater Treatment Systems P ft. Well Diameter: in. Screened Interval: >UA it. to 11i ,j ft Check One: ❑ Influent (98 ) El Depth to Water Level'. - � ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 9, 3 ft. above land surface. Relative M.P. Elevation in fit.: Gallons of water pumped/bailed before sampling: (00 Date sample collected: Field analysis: pH (D: , Specific Conductance uMhos Temp. 1_�1_°C, Odor Appearance PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH NC 27699-1636 Phone: M 919) 733-3221 PERMIT #: I,t C OC (oU3 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE F PER OPERATION BEING MONITORED Lagoon Reinedialion: Infiltration Gallery Spray Field Remediation: Rotary oislributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: ;5Pe 3t'lr2 �4 Laboratory Name: 1 eP,h % Certification No. PARAMETERS (Samples for metals were collected unfiltered--l_YE5 NO COD mg/I. Nitrite (NO2) as N and field acidified m /1 Coliform: MF Fecal Coliform: MF Total /100ml Nitrate (NO3) as N mg/I g /100ml Phosphorus: Total as P P '� -� , �W— mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate m /l Dissolved Solids: Totals -I-) Q mg/1 AI - Aluminum y-Is s,Ib mg/I pH (when analyzed) y-10 TOC (Di? units � ( Ba - Barium LI-) S C3 � t-13 mg/I _ Chloridee -,�5 � mg/1 Ca - Calcium_y-15 '�'1 b mg/I _L] _U Arsenic -q-15 : S mg/I C01 mg/l Cd - Cadmium 4 -15 Chromium: Total, LI-IS mg/I m /I Grease and Oils mg/I Cu - Copper mg/1 g Phenol Sulfate mg/I Fe - Iron mJ/l Specific Conductance mg/I uMhos Hg -Mercury K - Potassium mg/I Total AmmoniaKN N mg/I Mg = Magnesium �-15 mg/I mg/I mg/I Mn -Manganese-�1- IS 1 mg/I YES NO) Ni - Nickel. I mg/1 Pb - Lead W -15 C�(Nscli mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab r_eport.) Report Attached? Yes (1) No (0) VOID method # = method #. _ :SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Ccial5 Arne l`('u n Permit Name (if different): Facility Address: 1p7n�ir�1P e '�� ,� T hd P<< �� �dt t11r ] 6 1,,� (5lreeq (c lY) n� C -7 a. County -- fl'Zc.,rnt� �e i 1 1'i,i \\ i � i it ca vt (zip) 0 Contact Person:_, 1 Telephone #:��5-i�1�-•+-} li 1 Well Location/ Site Name: w 1 U h i�i^ nr1 No: of Wells to be Sampled: (Irom Permll) Well Identification Number (from Permit): (Y) L,u i Ca For Groundwater Treatment Systems Well Depth: 1 2 it. � Well Diameter: _� in. Check One: ❑ Influent (98) Screened Interval: �jT_ It. to � j � tt. C7 .Effluent (99) Depth to Water Level: ) S� Z ft. below measuring point. Measuring Point (M.P.) is:Q � -3 ft. above land surface. Relative M.P. Elevation in fit.: Gallons of water pumped/bailed before sampling: Date sample collected: -/O -I q Field analysis: pH , Specific Conductance ' uMhos Temp. 1 1 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER. RALEIGH, NC 27699-1636 Phone: 19191731-1ss PERMIT #: L-� C1 CC(Z It G EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5ee 0r-, ,.) Laboratory Name: Us)a W i p CI h Certification No. 5 f� PARAMETERS (Samples for metals were collected unfiltered)� YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total. as P 41-:)y C,ge\ m if (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total q • 15 1 r S mg/I pH (when analyzed) 9 -1 c) -5,9 units TOC y-15 4� 1.0 m /I Chloride y- o�S 45: O mg/I Arsenic �4 -1 S c:Cs mg/I Grease and Oils mg/I Phenol g Sulfate _q- 15 mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N Orthophosphate 9 m /I g/I Al -Aluminum LH S Ba - Barium L4--.1 S d, �:�;;z 9/I Ca - Calcium L1-►5}.k.a , g/I Cd - Cadmium L4-IS' < "cs2 g/I Chromium: Total LI -IS {e .c5 pSmg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium Y-15 3• - g/I YES NO) Ni - Nickel q-i5 so oGSmg/I Pb - Lead L4-- l5 4n,005- mg/I Zn -Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ZpLq �• 4. �C\i iim Li — iS 'at�i Mtf i v� r� ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # _ method method#= eer[K that. to 1hR hpst of my knnwlorfno onri r,euor III— i..v.......r .., w..4 �!Y •L!- __ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION - Please Print Clearly or Type Facility Name:. CcCn,�s AY-nPft�Carn Permit Name (if different): Facility Address:jp_3D d Contact Person: I'Ditt it Well Location/ Site Name: County I r" IJQk Qe l 1 Telephone M IM -9510-L1 I I I No. of Wells to be Sampled:.,. 0 = Well Identification Number (from Permit): m 11 R For Groundwater Treatment Systems Well Depth: _ 3c) ft. Well Diameter.. 9 in. Check One: ❑ Influent (98) Screened Interval: AT ft. to � ft. ❑Effluent (99) Depth to Water Level: �_ft. below measuring point. Measuring Point (M.P.) is:�q_ It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: —_ Date sample collected: L4 - ir`;-• 1�1 Field analysis: pH D ,.l Specific Conductance uMhos . Temp. --E-L_°C, Odor Appearance ' DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WFIALEIGH—NC ATER QUALITY DIVISION, GROUNDWATER SECTION 36 MAIL SERVICE CENTER 27699-1636 Phone: 919 733-3221 PERMIT #: WO C(Y05t-,� EXPIRATION DATE: Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: ee 13o01.0 Laboratory Name: Gk-lk e 'Tech Certification No. — 5(" PARAMETERS (Samples for metals were collected unfiltered --YES NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg /1 Coliform: MF Fecal Coliform: MF Total /100ml m/I Phosphorus: Total as P y-ZL( ZD,*1 mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total -15 a� Orthophosphate mg/I mg/I pH (when analyzed) i) - I O 9 `7 units 41-IS Al - Aluminum y-)S Ba - Barium W-15 0 14(C'`) mg/I r) (DR mg/I TOG 1 o mg/I Ca - Calcium W-IS 3ru mg/I Chloride LI- S Arsenic 1. 9.0 mg/I 40 005 mg/I Cd - Cadmium ►,�; Chromium: Total L4-K S1),co� mg/I {o o5 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate mg/I mg/I Fe -Iron Hg - Mercury mg/I m /I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium �-1-I5 a313 mg/I TKN as N mg/I Mn - Manganese.9-5 <o •cos mg/I GW-59 Rev. 0312000 Signature of Perm' ee for Aulhori Ag YES No) Ni - Nickel "O'coS mg/I Pb - Lead id -IS 4('s'oa"; mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) JCJ�i �;r14 M � ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOID : method # = method # = method # = or type GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: — Permit Name (if Facility Address: Contact Person: i'Ili I I Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County l 1 111: Fix le I / Telephone #: _ 1h$ - 95(c -LI 1 l No. of Wells to be Sampled:.._ I Well Identification Number (from Permit): f ) \-) l For Groundwater Treatment Systems Well Depth: 13 it. Well Diameter: LS in. Check One: ❑ Influent (98) Screened Interval: :J A r� ft. to "0 f) it. ❑ Effluent (99) : Depth to Water Level ' ft. below measuring point. Measuring Point (M.P.) is: O • to ft. above land surface. Relative M.P. Elevation in fit.: Gallons of water pumped/bailed before sampling: -1 s -5 Date sample collected: i -1 Field analysis: pH Aa-(—, Specific Conductance uMhos . Temp. Q °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: L Qa OU" alp C` .3 EXPIRATION DATE: _ Non -Discharge UIC- NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: __ NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: See. , f)aLZ Laboratory Name: TP Ch Certification No. S� PARAMETERS (Samples for metals were collected unfilteredX_YE5 NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I mg/I Coliform: MF Fecal Coliform: MF Total /100ml Phosphorus: Total as P �I �Ll Q mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate m /1 Dissolved Solids: �-I-15 SS9 mg/I Al - Aluminum LHS 0'0q� mg/I pH (when analyzed) L.I•-IO b, to units Ba - Barium -15 C", W`-) mg/I TOC _LI -15 1 I <�q mg/I l7, 5 mg/I Ca - Calcium _14-IS 1 o. Cd - Cadmium. mg/I mg/I Chloride L4 -QS LI Arsenic -15 4 o• o(::S mg/I Chromium: Total 4 - I S cos- mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate LI-15 g z l �,o mg/I Iron Hg - Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - MagnesiumiInQ mg/I TKN as N mg/I Mn - Manganese. G q , lei mg/I YES NO) Ni - Nickel ' -1S 0100q mg/I Pb - Lead '-I - IS <r QQ5 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) r:rliDn-, 'Y -1 5 'Ct t �, C ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #.. Attach lab report.) ReportAttached? Yes (1) No (0) VOC method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: 1 ' DEPARTMENT OF ENVIRONMENT & 14ATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM 1636 MAIL SERVICE CENTER 4CILITY INFORMATION Please Print Clearly or Type RAL"L NC 27t399-1.636 Phone: 919 733-32, Facility Name:--L Permit Name (if di Fa,Qility Address:_ Contact Person: 9'1)011 Well Location/ Site Name: County. I L l C IA')( L)P t 1 Telephone M '' r No. of Wells to be Sampled: Well Identification Number (from Permit): M LO For Groundwater Treatment Systems Well Depth: �J ft. Well Diameter: _al in. Check One: ❑ lnflUent (98) Screened Interval: . N r it. to __�} A ft. Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is: 9--ko ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _"— Date sample collected: -10- 14 Field analysis: pH S_ , Specific Conductance uMhos Temp. __L9_1°C, Odor Appearance PERMIT #: W Q Ot ©5l 103 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _ ep Laboratory Name: QC•h Certification No. _ ��]c' PARAMETERS (Samples for metals were collected unfilteredX_YE5 NO and field acidified COD mg/I /100ml Nitrite (NO2) as N . Nitrate (NO3) as N mg /I Coliform: MF Fecal Coliform: MF Total /100ml m/I g Phosphorus: Total as P A -1 () , t m /I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total )I-isI (05mg/l Al-AlurninumI- O U ( mg/I�5 pH (when analyzed) L1 -Ire TOG i-1- S.1 units Ba - Barium >_ - 5 < I 1 t' mg/1 /1s > mg/I Ca - Calcium I_ - Cd - Cadmium IL - i 1 mg/I o to mg/I Chloride I 2)',5 Arsenic U-1 S <0(00S mg/I Chromium: Total LI -15' �IDC� mg/l Grease and Oils mg/I Cu _ Copper mg/I Phenol m /1 F I YES NO) Ni - Nickel_ 44-1.c� 41:3,CuS mg/I Pb - Lead y -1 S c7 `CAS mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 4,ty> Sulfate 4-1.5 m-4 He Mercury mg/I mg/I ORGANICS: (GC,GC/MS,HPLC) Specific Conductance Total Ammonia uMhgs Kg Potassium mg/I (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) TKN as N mg/I mg/I Mg - Magnesium'- -15' Mn - Manganese'A--15 ''1, mg/I D VOC :method # 1 VCX9 mg/I ; method # = method # = F;T=Tl If• 1 • llPA ai I111-f l 1 1 1 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: t-- l_(_ 1 D Permit Name (if different): Contact Person:1/411 111 p Well Location/ Site Name: — SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County. MC' CbLk.a(�) I Telephone #: 2N No. of Wells to be Sampled: Well Identification Number (from Permit): For Groundwater Treatment Systems Well Depth:. � 5 it. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval:.��_ it. to \� ft. El Effluent (99) Depth to Water Level: `�l=G ft. below measuring point. Measuring Point (M.P.) is: q— L- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: -5 Date sample collected: Field analysis: pH_L-- 1 Q , Specific Conductance uMhos Temp. ___i�__°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WQ DMS(063 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5eF Laboratory Name: I Qnee( -Te c-h Certification No. Sr) PARAMETERS (Samples for metals were collected unfilteredYES NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N m /I Coliform: MF Fecal Coliform: MF Total /100ml mg/I Phosphorus: Total as P�- o o aD mgg/I (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total -1S ?,SSA Orthophosphate m/I mg/I pH (when analyzed) tni. '-) units AlAI - Aluminum 14-H Ba - Barium U -19' C,bb mg/I LL)RS m /1 9 TOC 4-1- 15 `�.S 010R mg/I Ca - Calcium .-IS r• 5, mg/I Chloride � `i ' • Arsenic LI - 1 S LSj O mg/I �0,0mg/I Cd -Cadmium � 1-15 Chromium: Total L1-15 �. C� � ,n`� m /I npC Grease and Oils mg/I Cu -Copper - , mg/I g mg/I Phenol Sulfate �1-1,5 mg/I t� O mg/I Fe - Iron- Hg - Mercury m /I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium Li-15 mg/I. TKN as N mg/I Mn - Manganese_( -1 5 mg/I —YES NO) Ni - Nickel -1-15 40,00s mg/I Pb - Lead !A -)5 4 Q I E ,5 m9/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ltan; ttiU-1S 4 r-jt r 11 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes -(I) No (0) VOC : method # = : method # = method # -- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION ' Please Print Clearly or Type Facility Name: Ct'a n A me C I Cn(`� Permit Name (if different): Facility Address: 0-210 Ayy) Ci can ' tI 'c' d 2C mnc i h() Rofeeq iCay) �) C i .a e Q' 9 S `D County C Ch a \e, 11 Contact Person: A� . tl (Zip) .Telephone #: �S�� � `��5t� ..y I I 1 Well Location/ Site Name: PO wIld , No. of Wells to be Sampled: (Iro Permll) Well Identification Number (from Permit): py-)j.0 1. For Groundwater Treatment Systems Well Depth: Iln ft. Well ,ra Diameter: in. Check One: ❑ Influent (98) Screened Interval: t% O ft. to � ft. 0 Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:0 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 9,25 - 5 Date sample collected: A -ID --U Field analysis: pH Ce D , Specific Conductance ' uMhos Temp. f 2 °C, Odor Appearance PERMIT #: (A) Non -Discharge DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ✓ Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: 0. 000 5t0� NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 'bee. jam, r) U c,3 Laboratory Name: _ t L)Q— - P r Tl'C 11 Certification No. (1 PARAMETERS (Samples for metals were collected unfiltered ✓ YES NO and field acidified COD mg/I Nitrite (NO2) as'N mg/l Coliform: MF Fecal /10.Oml Nitrate (NO3) as N m /I Coliform: MF Total /100ml Phnsnhnrrlc• Total nc D zl _�i1 1 ri .11� .....gr, (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total u-) 5 -2) 1L mg/I pH (when analyzed) _I4-Ic7 ( units TOC 14 -15 i , 33 mg/I Chloride 47-a5 S, n mg/I Arsenic _y I S mg/I Grease and Oils mg/I Phenol /I Orthophosphate m /l Al - Aluminum u-15 t°>,�'�� mg/1 Ba - Barium L) - I S a .( i mg/I Ca - Calcium_L4 -15 'l 1 mg/I Cd - Cadmium. f-1-IS 4 o , ©(7yD mg/1 Chromium: Total 9-1 5 c)S mg/I Cu - Copper mg/I YES NO) Ni - Nickell--15 46, S m I Pb - Lead- 4-1- IS < D mil Zn - Zinc 9/ mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) . Sulfate I-1-1 Specific Conductance p Total Ammonia TKN as N �.I �� mg/l g uMhos mg/I mg/I He - iron g Mercury K - Potassium Mg - Magnesium Mn - Manganese y_ Is ' (i ,�ujp mg/l m9/I mg/I m /I g mg/} ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes VOC (1) No (0) method # = method # = method # 1 • .U91 KUMr . IRI�w rle ECH Lfifi i lnc. POST OFFICE BOX 1056 < #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#02) COLLECTION DATE: 4/10/2014 PERMIT #. COLLECTION TIME: 08:39 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/10/2014 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED: 5/6/2014 ANALYSIS RESULTS UNITS. DATE ANALYST TDS 98 mg/L 4115/14 lag Chloride 5.8 mg/L 4125/14 lag T. Phosphorus 0.56 mg/L 4/24/14 jdg TOC <1.0 mg/L 4/15/14 Sulfate 12.1 mg/L 4/15/14 metals. ' see attached pH 7.7 su's 4/10/14 lag ' OG ID: 1404-219 REPORTED BY: NC CERTIFIED LAB # Tony Gragg, Lab Supervisor fiffiTEROrcH myssinc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR, GRANITE FALLS, NORTH CAROLINA 26630 (828) 396-4444 SAMPLE: Coats America (MW#10) COLLECTIONDA.TE: 4/10/2014 PERMIT #: COLLECTION TIME: 08:46 ADDRESS: Coats America (Wells) RECEIVED DATE. 4/10/2014 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED: 5/612014. ANALYSIS UNITS DATE1 ANALYST TDS. 138 mg/L 4/15/14 lag Chloride <5.0 mg/L 4/25/14 lag T. Phosphorus 0.20 mg/L 4/24/14 Jdg TOC <1.0 mglL 4/16114 Sulfate 38.3 mg/L 4/15/14 metals see attached pH 7.1 su's 4/10114 lag LOG ID: 1404-220 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor HrER6rECH LJVHS i11C. POST OFFICE BOX 1056 • 95 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 'SAMPLE: Coats America (MW#11) COLLECTION DATE: 4/10/2014 PERMIT #: COLLECTION TIME: 08:55 ADDRESS: Coats America (Wells) RECEIVED DATE.' 4/10/2014 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED., 5/6/2014 AN.YSlS ANALYSIS RESULTS UNITS- DATE ANALYST TDS 209 mg/L 4/15114 lag Chloride 22.0 mg/L 4/25114 lag T. Phosphorus <0.16 mg/L 4/24/14 Jdg TOC <1.0 mg/L 4/15/14 Sulfate 33.4 mg/L 4/15/14 metals see attached pH 8.7 su's 4/10/14 lag LOG ID: 1404-221 REPORTED BY: NC%.CERTIFIED I.AB # 50 fok"'t Tony Gragg, Lab Supervisor 1dfiTE'R4rrCH ./RC. POST OFFICE BOX 1056 • 45 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#12) COLLECTION DATE. ' 4/10/2014 PERMIT #: COLLECTION TIME., 09:02 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/10/2014 P.Q. Box 368 RECEIVED TIME: 14;00 Marion, NC 28752 REPORTED: 5/6/2014 AALYSI` . ANALYSIS RESULTS UNITS DATE ANALYST TDS 587 mg/L 4/16/14 lag Chloride 17.5 mg/L 4/25/14 lag T. Phosphorus 0.20 mg/L 4/24114 Jdg TOC 1.84 mg/L 4115/14 Sulfate <10.0 mg/L 4/15/14 metals see attached pH 6.9 su's 4/10/14 lag LOG ID: 1404-222 REPORTED BY: NC CERTIFIED LAB N 50 Tony Gragg; Lab Supervisor wwrRincH POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA OR, GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#13) COLLECTION DATE: 4/10/2014 PERMIT #: COLLECTION TIME. 09:10 ADDRESS: Coats America (Wells) RECEIVED DATE.' 4/10/2014 P.O. Box 368 RECEIVED TIME: 14:00 Marion, NC 28752 REPORTED: 5/6/2014 AN LYSI ANALYSIS RESULTS VNITS DATE ANALYST TDS 165 mg/L 4115114 lag Chloride <5.0 mg/L 4/25/14 lag T. Phosphorus 0.19 mg/L 4/24/14 idg TOO <1.0 mg/L 4/15114 Sulfate 18.9 mg/L 4/15/14 metals see attached pH 6.6 su's 4110/14 lag LOG ID: 1404-223 REPORTED BY: NC CERTIFIED LAB # 50 f&l (" Tony Gragg, Lab Supervisor jqR4rr H Lfi85Jnc. • it i POST OFFICE BO7 1056 • 45 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#14) COLLECTION IDA TE: 4/10/2014 PERMIT #: COLLECTION TIME: 09:15 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/10/2014 RO. Box 368 RECEIVED TIME 14:00 Marion, NC 28752 REPORTED: 5/6/2014 N YSI ANALYSIS RESULTS UNITS' (DATE ANALYST'. TDS 329 mg/L 4/15/14 lag Chloride <5.0 mg/L 4/25/14 lag T. Phosphorus 0.22 mg/L 4/24114 Jdg TOG 2.08 mg/L 4/15/14 Sulfate <10.0 mg/L 4/15/14 metals see attached pH 6.9 su's 4/10114 lag LOG ID: 1404-224 REPORTED BY: NC CERTIFIED LAB # Tony Gragg, Lab Supervisor unnen4reCH LAMM.. POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396.4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 4/10/2014 PERMIT A- COLLECTION TIME: 09:20 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/10/2014 P.O. Box 368 RECEIVED TIME: 14:00 Marion, NC 28752 REPORTED. 5/6/2014 ;ANALYSIS ANALYSIS RESULTS UNITS . DATE ANALYST TDS 311 mg/L 4/15/14 lag Chloride <5.0 mg/L 4/25/14 lag T. Phosphorus <0.16 mg1L 4/24/14 jdg TOO 1.33 mg/L 4115/14 Sulfate <10.0 mg/L 4/15114 metals see attached pH 6.8 su's 4/10114 lag LOGID: .1404-225 REPORTED BY: NC CERTIFIED LAB # 50 fll�" Tony Gragg, Late Supervisor • ttt�llllllll _. RESEARCh & ANA1)/TICA1 ���`b` � acyr;�►.,,� ... £` Ub0RAT0RIES, INC. �`4` ''��t ►��ti,��. w•0 i t: Analytical/Process Consultations NC#34 z, �°o+� p��D1A��►+ �+o� Water Tech Labs. Inc. Date Sample Collected 04/10/14 P,O, Sox 1056 Date Sample Received 04/15/14 Granite Falls, NC 28630 Date Sample Analyzed 04/15/14 Attn: Joe Gragg Date of Report 04/25/14 Analyses Performed by CC -KL -JC Lab Sample Number -------------------- 783125 Parameter Storet # Results TOC <1-0 mg/l Sulfate (00945) 12.1 mg/l Aluminum,Tot (01105) 5.10 mg/l Arsenic,Tot (01002) 0.007 mg/l Harium,Tot (01007) 0,173 mg/l Cadmium,Tot (01027) <0,002 mg/l Chromium,Tot (01034) 0.008 mg/l Calcium,Tot (00916) 37.6 mg/l Lead,Tot (01051) 0.059 mg/1 Magnesium,Tot (00927) 20.0 mg/l Manganese,Tot (01055) 1.44 mg/l Nickel,Tot (01067) 0.016 mg/l Selenium,Tot (01147) <0.005 mg/l. Sodium,Tot (00929) 12.3 mg/l -------------------- Clients Sample Source MW2 Number COATS AMERICAN Time Collected (Hrs) 0839 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax 336-996-0326 www.randalabs,00m RESEARCH & ANA[.yTICAL 4�1�& ANSI Y�� LABORATORIES INC. Y _ _ NC #34 z: Analytical/Process Consultations ++ •• �R C'tp `�,,�, t101 .Water Tech Labs. Inc. Date Sample Collected ; 04/10/14 P.O. Box 1056 Date Sample Received 04/15/14 Granite Falls, NC 28630 Date Sample Analyzed 04/15/14 Attn: Joe Gragg Date of Report 04/25/14 Analyses Performed by CC -KI, -JC Lab Sample Number -------------------- 783126 Parameter Storet # Results TOC <1.0 mg/1 Sulfate (00945) 38.3 mg/1 Aluminum,Tot (01105) 0.134 mg/l Arsenic,Tot (01002) <0.005 mg/l Barium,Tot (01007) 0.009 mg/1 Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/1 Calcium,Tot (00916) <0.500 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) <0.500 mg/l Manganese,Tot (01055) <0.005 mg/l Nickel,Tot (01067) <0.005 mg/1 Selenium,Tot (01147) <0.005 mg/1 Sodium,Tot (00929) 59.3 mg/l r 4 t` ----------------- 7-- Clients Sample Source MW10 Number COATS AMERICAN Time Collected (Hrs) 0846 P.O. Box 473 - 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs,com RESEARCh & ANA1yTICA1 LAbORATWES, INC. NC MIX zc Analytical/Process Consultations a Water Tech Labs. Inc. Date Sample Collected 04/10/14 P.O. Box 1056 Date Sample Received 04/15/14 Granite F'alls., NC 28630 Date Sample Analyzed 0.4/15/14 Attn: Joe Gragg Date of Report 04/25/14 Analyses Performed by CC -KL -JC -AA Lab Sample Number -------------------- 783127 Parameter Storet # Results TOC <1.0 mg/l Sulfate (00945) 33.4 mg/1 Aluminum,Tot (01103) 0.462 mg/1 Arsenic,Tot (01002) <0,005 mg/1 Barium,Tot (01007) 0.038 mg/1 Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/l Calcium,Tot. (00916) 43.0 mg/l Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 23.0 mg/1 Manganese,Tot (01055) <0.005 mg/l Nicicel,Tot (01067) <0.005 mg/l Selenium,Tot (01147) <0.005 mg/l Sodium, Tot (00929) 16.2 mg/1 -------------------- Clients Sample Source Z MW11R Number COATS AMERICAN Time Collected (Hrs) OB55 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27264 • 336.996-2B41 • Fax 336-996-0326 www.randalabs.com . 4 RESEARCh & ANALyTICA1 c(l -- LAb®RATWES, INC. 3 Analytical/Process Consultations r � i •� ti ANA®A 10 Water Tech Labs. Inc. Date Sample Collected 04/10/14 P.O. Box 1056 Date Sample Received : 04/15/24 Granite Falls, NC 28630 Date Sample Analyzed 04/15/14 Attn: Joe Gragg Date of Report 04/25/14 .Analyses Performed by CC -KL -JC -AA Lab Sample Number -------------------- 783128 Parameter Storet # Results TOC 1.84 mg/1 Sulfate (00945) <10.0 mg/l Aluminum,Tot (01105) 0.028 mg/l Arsenic,Tot (01002) <0,005 mg/l Barium,Tot (01007) 0.147 mg/1 Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/l Calcium,Tot (00916) 102 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 16.2 mg/l Manganese,Tot (01055) 4.19 mg/l Nickel,Tot (01067) 0,009 mg/l Selenium,Tot (01147) <0.005 mg/l Sodium,Tot (00929) 89.1 mg/1 -------------------- Clients Sample Source MW12 Number COATS AMFRICAN Time Collected (Hrs) 0902 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com L r= RESEARCh & ANA[yTYCA1 LABORATORIES, INC. Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected : 04/10/14 P.O. Box 1056 Date Sample Received 04/15/14 Granite Falls, NC 28630 Date Sample Analyzed 04/15/14 Attn: Joe Bragg Date of Report 04/25/14 Analyses Performed by CC --KL -JC -AA Lab Sample Number -------------------- 783129 Parameter Storet # Results TUC <1.0 mg/l Sulfate (00945) 18.9 mg/1 Aluminum,Tot (01105) 0,101 mg/l Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.029 mg/l Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/l Calcium,Tot (00916) 11.8 mg/l Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 7,88 mg/l Manganese,Tot (01055) 0.022 mg/l Nickel,Tot (01067) <0.005 mg/l Selenium,Tot (01147) <0.005 mg/l Sodium,Tot (00929) 41.6 mg/1 -------------------- Clients Sample Source MW13 Number COATS AMERICAN Time Collected (Hrs) 0910 P.O. Box 473 • 106 Short Street • Kernersvi Ile, North Carolina 27284 • 336.996.2841 • Fax 336-996-0326 www.randalabs.00m RESEARCh & ANA1YTICAL LABORATORIES, INC. Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected 04/10/14 ,P.O. Box 1056 Date Sample Received 04/15/14 Granite Falls, NC 2BG30 Date Sample Analyzed 04/15/14 Attn: Joe Gragg Date of Report 04/25/14 Analyses Performed by CC -KL -JC -AA Lab Sample Number -------------------- 783130 Parameter Storet # Results TOC 2.08 mg/l Sulfate (00945) <10.0 mg/l Aluminum,Tot (01105) 0.260 mg/l Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.085 mg/l Cadmium,Tot (01027) <0.002 mg/l Chromium,Tot (01034) <0.005 mg/1 Calcium,Tot (00916) 65.0 mg/l Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 42.0 mg/l Manganese,Tot (01055) 0.521 mg/1 Nickel,Tot (01067) <0.005 mg/l Selenium,Tot (01147) <0.005 mg/1 Sodium,Tot (00929) 18.4 mg/l. Clients Sample Source Number Time Collected (Hrs) -------------------- MW14 COATS AMERICAN 0915 P.O. Box 473 • 106 Short Street • Kernersville, North Caroline 27284 • 336-996-2B41 • Pax 336-996-0328 www.randelabs.com RESEARCh St ANA1yTiCAI s,••`(:)�&ALdr;'' ...... LAbORATORIES, INC. Analytical/Process Consultations rt t a• 07 *er'�i�i�f�U ANP�� d•i� Water Tech Labs, Inc. Date Sample Collected: 04/10/14 P.O. Box 1056 Date Sample Received 04/15/14 Granite Falls, NC'28630 Date Sample Analyzed : 04/15/14 Attn: Joe Gragg Date of Report 04/25/14 Analyses Performed by CC -KL -JC -AA Lab Sample Number -------------------- 763131 Parameter Storet # Results TOC 1.33 mg/l Sulfate (00945) <10.0 mg/l Aluminum,Tot (01105) 0.032 mg/l Arsenic,Tot (01002) <0.005 mg/l Barium,Tot (01007) 0.090 mg/1 Cadmium,Tot (01027) <0,002 mg/1 Chromium,Tot (01034,) <0.005 mg/l Calcium, Tot (00916) 72.5 mg/1 Lead,Tot (01051) <0.005 mg/1 Magnesium,Tot (00927) 32.4 mg/1 Manganese,Tot (01055) 0.240 mg/1 Nickel,Tot (01067) <0.005 mg/l, v Selenium,Tot (01147) <0.005 mg/l Sodium,Tot (00929) 6.47 mg/l -------------------- Clients Sample Source MW15 Number COATS AMERICAN Time Collected (Hrs) 0920 P.O. Box 473 • 106. Short Street • Kernersville, North Carolina. 27284 • 336-996-2641 • Fax 336-996-0326 www.randelabs.wrn CHAIN OF CUSTODY - Analytical Request Client Name: Ufi -5 Address: Report to: Phone: PO Number: i� p(•+ rV3 we I is WATER TECH LABS, INC. PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: Requested Analyses pH Checked Upon Receipt Preservatives Cl2 < 0.2 mgA Upon Receipt Sample Identification tV p v b U U z-! U Q .� 0 + O Y 1 �cnC7 .2 N .- 0 aR , � 0 r L Cd x � y Feld Temp. (C') Comments iili f - . . Temperature (°C) _ d /S Received on Ice: Y/ N Zc J d f Sealed Cooler: Y / N rl Samples Intact Y / N Additional Comments: Printed Name of Sampler. d ,t ) !,, Signature of Sampler: CHAIN OF CUSTODY - Analytical Request Client Name: CM s Address: Report to: Phone: PO Number: 3Ylbnhci C4 � 5 WATER TECH LABS, INC. PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 39674444 Project Name: Project Number: Requested Analyses r VA 111163 to] Sample Identificaffou1 � � W Field Temp- Sampie`Condit on Upon Receipt Relinquished Sy Company' ^ i7 to ` Time ,-, Accepted By Company Date Time _ - � S I� WM IM Additional Sampler Name and Signature Date Printed Name of Samp]- Signature of Sampl a i ,r C/ruva rernut # U)(.�) JklJOUX) D (Submit one each monitoring period with GYV=59 forms.) 1 Enter date monitoring results were due. p` Will this monitoring report (GW-59 and GW-59A) YES NO be. submitted after the established due date? 2 1 ri n =sue- Was any required information missing on the GW-59 report forms? r ;p �i,;q 1 H V] L1 r) �,.. $ y 0 O a y _I _ . iF the answer to question 1 or 2 is 'YES", list in the space provided below the well'!ldelnti icafion number(s) and , explain the problems encountered in obtaining the required information.- . U? F E 6 10 2014 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked=or'missing cap; m►ssmg �- ES NO identification plate, area overgrown, etc.)? If the answer is "Y'es• ", contact the Regional Ojf1ce for guidance. 4 Are any monitored constituents equal to or above the established standards? YES O If the answer to question 4 is `NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s) exceeding standards in the space provided below. ,� dYl� rnU-) ly nrlLL) mw l J i D S (O' Q mb� Dim afvs e 0-341 L ci d v f0 3-L V`)onlcantls e- r11an(Cpnest 090 �, Q�1es� �� m9 `9I� t✓,c� s"1 �^���� O,g�s 3h� 0 5 5 For tH constituents identifi din question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is `NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reportedand sample collection date for each occyirrence (for the last two years). 71 705 5 q)m�yi,� prla�tc gnrs� I3` n��'�- % 1 0S N m�� ,o� m f- 6 Are Me monitoring wells listed in section 5 located at or beyond the review boun ry? YES ]NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES, descri a ose actREQ) provided elow. If the to 7 is "NO", answer question cont ct the NK 4 90 da s• an evaluation ma be required to determine the impact, the wa to disposal s stem is havin at the eview and compliance boundaries surroundin this facility. Failure to do so may sub"ect the ermi ee to a Notice of Violation fines, and/or penalties. FEB 1 4 4 FEB 0 4 2014 Water 6ualihl Regional Operations Asheville Re tonal Office i�`1A RQUALPSECT€ N NMRAhltTm«wmim Io g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. hereby ackno�rlec)ge thattheaEiove�info�mation Nas evaluathd"'�nd the`3nfo IR7a io�`s"'� "•� �'y' i' t n ubmltted n #hls i Come jiiotttae best " :re ort: Iiarice Re o 9A) istrue and complet of msknovvled eg. Signature of Perini to or Authorized e-nt) Date es GW-59A 12/8/2003 tr<. GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:- Permit Name (if,i Facility Address: Contact Person: Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I I Iv L)UI ) ('A I Telephone #: "' � No. of Wells to be Sampled: Well Identification Number (from Permit): it'd W 'IA-9— Well Depth: 30 ft. Well Diameter: Screened Interval: AM A ft. to ft. Depth to Water Level: "I 1 2ft. below measuring point. Measuring Point (M.P.) is:_5_ it. above land surface. Gallons of water pumped/bailed before sampling: �3 Field analysis: pH 9 > Specific Conductance . Temp. , °C, Odor A For Groundwater Treatment Systems in. Check One: ❑ Influent (98) El Effluent (99) Relative M.P. Elevation in #t.: Date sample collected: j ppearance PARAMETERS (Samples for metals were collected unfifte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPH method for highly turbid samples) ` , .R C�V Dissolved Solids: Total mg/I pH (when analyzed) i'�,1 IM CA, a units TOC l';4J 71 I ,' mg/I Chloride I i1 .I � 3 mg/I Arsenic _i :) o'dO`amg/I Grease and �ils Phenol mg/I mg/I Sulfate mg/I Specific Conductance Total Ammonia TKN as N uMhos mg/I mg/I Rev. 03/2000 Umhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phnnac 191 M 779-19, PERMIT #: LAJO 60'Sb EXEXPIRATION DATE - Non -Discharge UIC NPDES TYPE QE PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _ 5ee % Oow Laboratory Name: 2C -T61Qh Certification No. _ sc) red__,4i,_YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P �o�ng/l Orthophosphate mg/I Al - Aluminum _16t 9 i`-] ; 9�`'7 mg/I Ba -Barium I R 1 I `I �� mg/I Ca - Calcium P mg/I Cd - Cadmium i 1 /r��(3fi� mg/i Chromium: Total I'a ®^ W5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I � Mg - Magnesium �� mg/I Mn -Manganese lad i'! ' ' 0IQ mg/l YES NO) Ni- Nickel � `1 t SG 1�6 mg/I Pb - Lead i t'7 G1CaJ'a mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ; cd l taco' t ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. At ach lab report.) ReportAttached? Yes 1 } No (0) VOC method # = q%oo r method # = method # = GROUNDIWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: , t:.0� Permit Name (if;different): Facility Address: PC) Contact Person: Pt1l I1 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I f tL r LJl t' i I Telephone #: Z S11ri=d No. of Wells to be Sampled: Well Identification Number (from Permit): YYlta!•-] - For Groundwater Treatment Systems Well Depth: 13 ft. Well Diameter. Q in. Check One: ❑ Influent (98) Screened Interval; N)� A ft. to T ft. ❑ Effluent (99) Depth to Water Level: 10 ft. below measuring point. Measuring Point (M.P.) is: a L10 it.'above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: r� , S Date sample collected: ° Field analysis: 'pH (a, , Specific Conductance ' uMhos . -Temp. I °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: L'JQo L)()S(.e03 Non -Discharge NPDES EXPIRATION DATE: UIC TYPE OF PERMITTED OPERATION BEING MONITORED iz�l agoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: e 2 Be,low Laboratory Name: f. C Certification No. S(� PARAMETERS (Samples for metals were collected unfiltered_NL_YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MFFecal /100ml Nitrate (NO3) as N mg/I Coliform: MF'Total /100m1 Phosphorus: Total as P g/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 10'� mg/I Al- Aluminum 1Q) ij-i b- 0st1 mg/I pH (when analyzed) units Ba - Barium , r Q mg/I TOC IrAla"I 01, S mg/I Ca - Calcium -I mg/I Chloride _L�)1�' )'pie ` mgll Cd -Cadmium 1 `� C� �i��- mg/I Arsenic _ _)a V 1`1 <o,oas mg/I Chromium: Total '%J11.1 40'W5 mg/1 Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 1a I-ql 1 t a mg/1 Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 11) "� mg/I TKN as N mg/I Mn - Manganese i° !r 171, (r'! i mg/I YES NO) Ni - Nickel i,3--li I � 0,019 mg/I Pb - Lean ia I I `D 4.010mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5�'l er<� van IA1 tij:j I-?P f)-,c, G ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes i/(1) No (0) VOC : method # _ 9 auto B method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM NAGILI I Y iNl-UHMATIUN Please Print Clearly or Type Facility Name: Locks AyAp i(-Or) Permit Name (if different): Facility �/Address: ` o) C7X L/) Mu A\ t on y (Sireel) A (Cny)� I I }'(state) (tip) County Contact Person: ) c� `?1+11 vtc�rt Telephone #: 99's-'IS(0`Ll! i t Well Location/ Site Name:'. er TnT1QPrd No. of Wells to be Sampled: Well Identification Number (from Permit): '(Y1W 1:� For Groundwater Treatment Systems Well Depth: Is ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: ti'iA ft. to O A ft. El Effluent (99) Depth to Water Level: 9• 11 ft. below measuring point. Measuring Point (M.P.) is: '�•U ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: Field analysis: pH , Specific Conductance uMhos . Temp. t °C, Odor Appearance DEPARTMENT OF ENVIRONMENT I£ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: W(A, B00 (o03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application -of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: See e law Laboratory Name: _ r t a i in Certification No — PARAMETERS PARAMETERS (Samples for metals were collected unfiltered_4—YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF; Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phosnhorus- Tntnl as P I I ILI A.2 mn/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total )�)l 19,- QIQ mg/I pH (when analyzed) r: , units Chloride I a 11 I� a � mg/I Arsenic I �.) i `'I 4 0 Ot% mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1r0r) mg/I Specific Contluctance - uMhos Total Ammonia mg/I TKN as N mg/l Orthophosphate mg/I Al - Aluminum.) 9 l 19 0 ,1 ',)&- mg/I Ba - Barium IQ 10 b,©q mg/I Ca - Calcium 12 4 117 mg/I Cd - Cadmium b-ll 40-00E- mg/I Chromium: Total 40100S mg/I Cu - Copper mg/1 Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium )012) mg/I Mn - Manganese ). i"� " 0.66S-1 ma/I YES NO) Ni-Nickel ,. 0, 0,6. mg/I Pb - Leant !a , V:) mg/1 Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) �0-1-PA1yry� ja�� 4—om5 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ROC ReportAftached? Yes V (1) No (0) method # = Aj c�tGC� r method # = method # = GW-59 Rev. 0312000 ee Clk4-) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_, Permit Name (if' diff Facility Address: vn^ _ - . - I Contact Person: 'I'1 lit I Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County Iy V� IX)tjSP 1 Telephone #: 2skg _r7 c�(o ` No. of Wells to be Sampled: Well Identification Number (from Permit): rbt,_� )LI Well Depth: ) it. Well Diameter: Z in Screened Interval: ft. to ft. Depth to Water Level: D 13ft. below measuring point. Measuring Point (M.P.) is: gAo ft. above land surface. Re Gallons of water pumped/bailed before sampling: Field analysis: pH Lo-1 , Specific Conductance . Temp. q °C, Odor AP For Groundwater Treatment Systems Check One: ❑ Influent (98) ❑ Effluent (99) lative M.P. Elevation in ft.: Date sample collected: 13 pearance PARAMETERS' (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total ° { mg/I pH (when, analyzed) -1 units TOC 1q, i�l � , R S mg/I Chloride iR * i R 4 S,; f') mg/I Arsenic l �1 4otQ�� mg/I Grease and bils mg/I Phenol mg/I Sulfate 1@14D 410, 6 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT Non -Discharge NPDES EXPIRATION DATE: UIC TYPE OF PERMITTED OPERATION BEING MONITORED L Lagoon Remedialion: Infiltration Gallery Spray Field Remediafion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _ iwflow LaboratoryName: ? A la kj_A Certification No. b V'YES NO and field acidified to (NO2) as N mg/l ate (NO3) as N mg/I sphorus: Total as P 1'3 i I 1 0100 mg/I Orthophosphate �— mg/1 Al - Aluminum ISI P-1 3I ' mg/I Ba - Barium `� i 0 mg/I Ca - Calcium 13 mg/I m Cd - Cadmiu`, 1, 1. mg/I Chromium: Total t611D ° b rODI mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium 171 g mg/I Mn - Manganese I t -;S R3. mg/I YES NO) Ni - Nickel f !a-)1 0,( i 3 mg/I Pb- Lead Ia)'1 ` 0,mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,Gr-/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes V (1) No (0) VOC : method #.= method # = method # = Rev. 03/2000 GROUNDjWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: %- Permit Name (if� differe FMc litx Address: I Contact Person-, '{mil I I! Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I ►1 '�- �Jllt t i P. i Telephone #: -11 SLI-e No. of Wells to be Sampled: Well Identification Number (from Permit): 1 5 For Groundwater Treatment Systems Well Depth: I to it. Well Diameter-: � in. Check One: ❑ Influent (98) Screened Interval: l ft. to ft. El Effluent (99) Depth to Water Level: A. + 9 ft. below measuring point. Measuring Point (M.P.) is: `LU ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 1 TS Date sample collected: Field analysis: .pH ( Specific Conductance ' uMhos . Temp._°C, Odor Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: bi a (jW Non -Discharge NPDES b3EXPIRATION DATE: UIC TYPE PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Application of Sludge NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: See 1Pj LW Laboratory Name: Ocr_La .-(,p� Certification No. c�'�, PARAMETERS (Samples for metals were collected unfiltered 'VYES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total J100ml Phosphorus: Total as P-)PL d+g/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total ' 1 a mg/I Al - Aluminum ` mg/1 pH (when anal zed) , l �h units Ba - Barium t mg/I TOC ) `� i t `'1 mg/I Ca - Calcium I, mg/I Chloride 1 l s "o mg/I Cd - Cadmium i Ga. )Z mg Arsenic I !2 PID n•005 mg/I Chromium: Total 19 40,005 mg Grease and Oils mg/I Cu - Copper mg Phenol mg/I Fe - Iron mg/l Sulfate i T t: mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/1 Total Ammonia mg/I Mg - Magnesium -IrA t m /l g TKN as N mg/I Mn -Manganese � + �� � mg/1 YES NO) Ni-Nickel I off' !� < 0 f 0 S mg/I Pb - Leads f `'"r1 mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GClMS,HPLC) (Specify test and method #. At ach lab report.) ReportAttached? Yes1) No VOC : method # _ %Ia(pL method # = method # = tui r uuaunaeu Hgeny Name ano -tit e;.Allease print or type Rev, D3/2000 Signature of Permiltee (or Aulhonzea-,vgent) ,� (Dale) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facility_Address: ?t Contact Person: �_' 1)% 1 t `i Well Location/ Site Name'. SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I 1 + — 14 )I b} `- 1. Telephone M '� -r , . No. of Wells to be Sampled: Well Identification Number (from Permit): M1'3.i ;4 Well Depth: ft. Well D'ameter: � in Screened Interval: ;01 1$ ft. to /U A ft. Depth to Water,Level: `'� ft. below measuring point. Measuring Point (M.P.) is:a13 ft. above land surface. R Gallons of water pumped/bailed before sampling: IQ Field analysis: pH (Q qQ Specific Conductance . Temp. �°C, Odor Ap For Groundwater Treatment Systems Check one: ❑ Influent (98) El Effluent (99) elative M.P. Elevation in ft.: _ Date sample collected: I,9 - pearance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly to bid samples) Dissolved Solids: Total JQL4 mg/I pH (when alyzed) (a: units NY-) TOC ( o- ' mg/I Chloride i S �-S IC> mg/I Arsenic, `�i mg/I Grease and ils mg/I Phenol mg/I Sulfate R I I I 40d•© mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Rev. D312000 uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: i ` 0005 -31 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE PF PERMITTED OPERATION BEING MONITORED NZ Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: See 1' �, Lj Laboratory Name: WOk-1 F C 'P S2 0, 4 9014 Certification No. 'Sci red____�N YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P i 046 mg/I Orthophosphate mg/I Al - Aluminum '"1 ' mg/I Ba - Barium mg/I Ca -Calcium it `� mg Cd -Cadmium 1• I M 40• mg/I Chromium: Total 1� 0,a)S mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium j�� mg/I Mn - Manganese 1 0 N mg/I YES NO) "'�'ie"�'''��"`. 'A"') Ni - Nickel I� 1 t� COR mg/I Pb - Lear) !`� na,)i � mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ,- d '1 LO O� j�nel ksl t ORGANICS: (GC,GC/MS,HPLO) (Specify test and method #. Attach lab report.) Report Attached? Yes �1) No (0) VOC method # = ?Rub 6 method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: L -5 Permit Name (if diff,p�eynt): ri Well Identification Number (from Permit): For Groundwater Treatment Systems Well Depth: 11� it. Well Diameter.- _ in. Check One: ❑ Influent (98) Screened Interval: ft. to roN ^ ft. ElEffluent (99) Depth to WaterLevel:_ft. below measuring point. Measuring Point (M.P.) is: a a it. above land surface. Relative M.P. Elevation in #t.: Gallons of water pumped/bailed before sampling: Date sample collected: 19 P91 i Field analysis: pH t4: A ; Specific Conductance ' uMhos Temp. �t� °C, Odor Appearance PARAMETERS (Samples for metals were collected unfilteredYES COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total iWls� 1V mg/I pH (when analyzed) 1 ') lo;H units TO I M1;T1 �— 4,1 �G mg/I Chloride ! T" 45,6 mg/I Arsenic IQ l e r 00S mg/I Grease and b ils mg/I Phenol mg/l Sulfate ?sU=L- mg/I Specific Con uctance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: t9191 733-19: PERMIT #: U,) a0C, 0 S0 )_.3 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE O.F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Rotary Distributor Other: Remedialion: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: See Ze_�ticll Laboratory Name: I -Ire Certification No. sn NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P I 0 : L22mg/I Orthophosphate Al - Aluminum jq)F-1 0,9�� mg/I mg/I Ba - Barium i,,A I i ") mg/I Ca -Calcium t 1 t'l L/7"s�Ot mg/I Cd - Cadmium tr' 1 Q <o boo- mg/I Chromium: Total 41DUS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium mg/I Mg - Magnesium f i'— 40 ,5W mg/I Mn - Manganese_ IST) 19' 41)a OaS mg/I YES NO) Ni -Nickel t' - 1 f : b n mg/I Pb - Lean / f`-? L -I'O s mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 4 6ef��� P1^ 1 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes X (1) No (0) VOC : method # = � GkIAO R method # = method # = Rev, 03/2000 1dfiTffR6TJ9CH-117C. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS. NORTH CAROLINA 28630 (828) 396-4444 SAMPLE. Coats America (MW#02) COLLECTION DATE: 12/17/2013 PERMIT #: COLLECTION TIME: 08:56 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.O. Box 368 RECEIVED TIME. 14:00 Marion, NC 28752 REPORTED: 1 /16/2014 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 104 mg/L 12/18/13 lag Chloride <5.0 mg/L 12/18/13 lag T. Phosphorus 0.40 mg/L 1/3/14 jdg TOC 1.62 mg/L 12/27/13 Sulfate <10.0 mg/L 12/27/13 metals see attached pH 7.5 su's 12/17/13 lag P.ECEI ED/DENROAR JANI 0 0 20 14 Water Quality Regiond Operations Cecuion LOG ID: 1312-321 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor ,* E u s- .lrtc. POST OFFICE BOX 1056 , #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Co is America (MW#10) COLLECTION DATE: 12/17/2013 PERMIT #. COLLECTION TIME: 09:00 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.C. Box 368 RECEIVED TIME: 14:00 Mai ion, NC 28752 REPORTED: 1 /16/2014 - ANALYSIS£Y ANALYSIS RESULTS UNITS : DA-TE - :: ANALYST TDS 128 mg/L 12/18/132 lag Chloride <5.0 mg/L 12/18/13 lag T. Phosphorus 0.22 mg/L 1/3/14 jdg TOC <1.0 mg/L 12/27/13 Sulfate 30.4 mg/L 12/27/13 metals see attached pH 6.8 su's 12/17/13 lag LOG ID: 131 Division f Water EDrces F E S 1 4 2014 I Water Qualit Asheviy Regional Operations lle Regional Office REPORTED BY: NC CERTIFIED LAB # 50 S" k Tony Gragg, Lab Supervisor .Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE., Coats America (MW#11) COLLECTION DATE 12/17/2013 PERMIT #. COLLECTION TIME., 09:16 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED: 1 /16/2014 ANALYSIS: RESULTS ; ..UNITS � TDS 209 mg/L Chloride 22.3 mg/L T. Phosphorus 0.36 mg/L TOC 1.76 mg/L Sulfate 57.9 mg/L metals see attached pH 8.5 su's LOG ID: 1312-323 z• — DATE ANALYST 12/18/13 lag 12/18/13 lag 1/3/14 jdg 12/27/13 12/27/13 12/17/13 lag REPORTED BY: NCCERTIFIED LAB # 50 fo� Tony Gragg, Lab Supervisor TER6TECH. µ .Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 12/17/2013 PERMIT #: COLLECTION TIME: 09:26 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.O. Box 368 RECEIVED TIME: 14:00 Marion, NC 28752 REPORTED: 1 /16/2014 t TDS 672 mg/L 12/18/13 Chloride 13.3 mg/L 12/18/13 T. Phosphorus 0.25 mg/L 1/3/14 TOC 2.55 mg/L 12/27/13 Sulfate 11.2 ma/L 12/27/13 metals see attached pH 7.1 su's 12/17/13 , ANALY lag lag jdg lag LOG ID: 1312-324 REPORTED BY: NC CERTIFIED LAB # 50 7 Tony Gragg, Lab Supervisor URTER6TECH Lowfizinc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#13) COLLECTION DATE., 12/17/2013 PERMIT #: COLLECTION TIME: 09:31 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED: 1 /16/2014 _ -- ��A�Ysrs � , • V ANAL-;YSIS : ' "'RESULTS _ UNITS; -"DA- TE:r ANALYST TDS 219 mg/L 12/18/13 lag Chloride 6.3 mg/L 12/18/13 lag T. Phosphorus 0.38 mg/L 1/3/14 jdg TOC 1.23 mg/L 12/27/13 Sulfate 26.2 mg/L 12/27/13 metals see attached pH 6.6 su's 12/17/13 lag LOG ID: 1312-325 REPORTED BY: NC CERTIFIED LAB # 50 fft.-t' * - Tony Gragg, Lab Supervisor TKR679CH .III c. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 12/17/2013' PERMITA- COLLECTION TIME: 09:44 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/17/2013 P.O. Box 368 RECEIVED TIME: 14:00 Marion, NC 28752 REPORTED: 1 /16/2014 ANALYSIS AN;4LYSIS RESULTS . UNITS DATE ANALYST TDS 397 mg/L 12/18/13 lag Chloride <5.0 mg/L 12/18/13 lag T. Phosphorus 0.40 mg/L 1/3/14 jdg TOC 2.95 mg/L 12/27/13 Sulfate <10.0 mg/L 12/27/13 metals see attached pH 7.0 su's 12/17/13 lag LOG ID: 1312-326 REPORTED BY: NC CERTIFIED LAB # 50 1 Tony Gragg, Lab Supervisor MOTER6TECH LANS-117C. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 12/17/2013 PERMIT #.' COLLECTION TIME., 10:06 ADDRESS., Coats America (Wells) RECEIVED DATE., 12/17/2013 P.O. Box 368 RECEIVED TIME., 14:00 Marion, NC 28752 REPORTED: 1/16/2014 TDS 305 mg/L 12/18/13 lag Chloride <5.0 mg/L 12/18/13 lag T. Phosphorus 0.33 mg/L 1/3/14 jdg TOC 1.79 mg/L 12/27/13 Sulfate 17*0 m,/L 12/27/13 metals see attached pH 6.6 su's 12/17/13 lag j 2— LOG ID: 1312-327 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor RESEARCh & ANA1YTICAt Ubo AT®f ks, INC. Analytical/Process Consultations January 8, 2014 Water Tech Labs P.O. Box 1056 Granite Falls, NC 28630 Attention: Joe Gragg Project Name: Coats American J��, U A!VALYT� �rrr #34 Mi 11• Miscellaneous MW2 MW10 MW11R ' MW12 MW13 MW14 MW15 Date Parameters Unit Results Results Results Results Results Results Results Analyzed Aluminum, Total mg/L 1.11 0.232 0.187 0.221 0.138 3.31 0.135 12/31/13 Arsenic, Total mg/L 0.006 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 12/31/13 Barium, Total mg/L 0.060 0.008 0.068 0.174 0.039 0.151 0.109 12/31/13 Cadmium, Total mg/L <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 12/31/13 Chromium, Total mg/L <0.005 <0.005 0.005 <0.005 <0.005 0.005 <0.005 12/31/13 Calcium, Total mg/L 17.9 <0.500 116 107 15.7 78.3 70.5 12/31/13 Lead, Total mg/L 0.015 <0.005 0.032 <0,005 <0.005 0.014 0.007 12/31/13 Magnesium, Total mg/L 9.32 <0.500 36.5 17.2 10.3 49.8 24.9 12/31/13 Manganese, Total mg/L 0.341 <0.005 0.008 4.67 0.057 0.883 1.50 12/31/13 Nickel, Total mg/L 0.008 0.040 0.014 0.012 0.005 0.013 <0.005 12/31/13 Selenium, Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 12/31/13 Sodium, Total mg/L 8.79 55.1 21.1 139 69.7 34.7 12.9 01/03/14 Sulfate mg/L <10.0 30.4 57.9 11.2 26.2 <10.0 17.0 12/27/13 TOC mg/L 1.62 <1.0 1.76 2.55 1.23 2.95 1.79 12/27/13 Sample Number 775168 775169 775170 775171 775172 775173 775174 Sample Date 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 Sample Time ---- ---- ---- ---- ---- ---- ---- mg/L = milligrams per Liter = parts per million (ppm) < = Less than or below detection limit w= LAb®•g 6Cs INC. CCtt-W•r o °N H34 zi Analytical/Process Consultations ��!aECpA' •� r0 Chemical Analysis for Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs, Inc. Project, collected 17 December 2013) I. Volatile Organics Quantitation EPA Method 8260 B Limit MW2 MW10 MW11R MW12 MW13 MW14 MW15 Parameter (ppb) JRpb) (Anb) IPebl (aobl (nnbl lrebl (nnb) Acetone 25 BQL BQL BQL BQL BQL BQL BQL Acrolein 100 BQL BQL BQL BQL BQL BQL BQL Acrylonitrile 100 BQL BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL 0.23 J BQL BQL BQL Bromobenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Bromochloromethane 0.5 BQL BQL BQL BQL BQL BQL BQL ne Bromodichlorometha 0.5 BQL BQL BQL BQL BQL BQL BQL Bromoform 1.0 BQL BQL BQL BQL BQL BQL BQL Bromomethane I.0 BQL BQL BQL BQL BQL BQL BQL 2-Butanone 25 BQL BQL BQL BQL BQL BQL BQL Carbon Disulfide 5.0 BQL BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL BQL Chlorobenzene 0.5 BQL BQL BQL 0.46 J BQL BQL BQL Chloroethane 1.0 BQL BQL BQL BQL BQL SQL BQL 2-Chloroethyl vinyl ether 5.0 BQL BQL BQL BQL BQL BQL - - BQL Chloroform 0.5 BQL BQL BQL BQL BQL BQL BQL Chloromethane 1.0 BQL BQL BQL BQL BQL BQL BQL 2-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL BQL 4-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL BQL Cis-1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2-Dibromo 3-Chloropropane(DBCP) 5.0 BQL BQL BQL BQL BQL BQL BQL 1,2-Dibromoethane (EDB) 0.5 BQL BQL BQL BQL BQL BQL BQL Dibromochloromethme 0.5 BQL BQL BQL BQL BQL BQL BQL Dibromomethane 0.5 SQL BQL BQL BQL BQL BQL BQL 1,2-Dichlorobenzene 0.5 BQL BQL BQL 0.18 J BQL BQL BQL 1,3-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,4-Dichlorobemene - 0.5 BQL BQL BQL 0.14 J BQL BQL BQL 1,1-Dichloroethene 0.5 BQL BQL BQL 0.181 BQL BQL BQL 1,2-Dichloroethme 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1-Dichloroethene 0.5 BQL BQL BQL 0.13J BQL BQL BQL Dichloroflouromethane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2-Dichloropropane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,3-Dichloropropane 0.5 BQL BQL BQL _ BQL BQL BQL BQL 2,2-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL Ethyl Benzene 0.5 BQL BQL BQL BQL BQL BQL BQL 2-Hezanone 5.0 BQL BQL BQL BQL BQL BQL BQL RE 0.5 BQL SQL BQL BQL BQL BQL BQL 1-Propylbenzene 0.5 BQL BQL BQL 0.12 J BQL BQL BQL 4-Methyl-2-Pentanone 5.0 BQL BQL BQL BQL BQL BQL BQL Methyl Iodide 1.0 BQL BQL BQL BQL BQL BQL BQL Methylene Chloride 5.0 BQL BQL BQL BQL BQL BQL BQL MTBE 0.5 BQL BQL BQL BQL BQL BQL BQL Naphthalene 0.5 BQL BQL BQL BQL BQL BQL BQL N-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL N-Propylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL p-Isopropyltoluene 0.5 BQL BQL BQL BQL BQL BQL BQL Sec-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL BQL Tert-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,1,2-Tetrachloroethane 015 BQL BQL BQL BQL BQL BQL BQL 1, 1,2,2-Tetrachloroetbane 0.5 BQL BQL BQL BQL BQL BQL BQL Tetrachloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL BQL BQL BQL BQL BQL Trans-1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Trans-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL Trans-1,4-Dichloro-2-butene 5.0 BQL BQL BQL BQL BQL BQL BQL 1,2,3-Trichlorobenzene 0.5 - ' BQL BQL BQL BQL BQL BQL BQL 1,2,4-Trichlorobemene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,1-Trichloroethane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,2-Trichloroethane 0.5 BQL BQL BQL BQL BQL BQL BQL Tichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Trichloro➢uoromethahe 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2,3-Trichloropropane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2,4-Trimethylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,3,5-Trimethylbemene 0.5 BQL BQL BQL BQL ' BQL BQL BQL Vinyl Acetate 1.0 BQL BQL BQL BQL BQL BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL BQL Total Xylenes 1.0 BQL BQL BQL BQL BQL BQL BQL Dilution Factor I I I I I I I Sample Number 775168 775169 775170 775171 775172 775173 775174 Sample Date 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 12/17/13 Sample Time (hrs) ---- ---- ---- ---- ---- --- Analyst NM NM NM NM NM NM NM -Date Analyzed 12/28/13 -12/28/13 12/28/13 12/28/13 -12/31/13 12/31/13 12/31/13 Time Analyzed 0315 0346 0417 0449 1605 1637 1709 Surrogate Recovery Range DBFM (70-130%) 102% 103% 87% 104% 105% 105% 110% Toluene-d8 (70-130%) 98% 98% 96% 98% 93% 95% 89% 4-BFB (70-130%) 99% 95% 96% 96% 92% 98% 94% BQL - Below Quantitation Limits ppb = pwl per billion CHAIN OF CUSTODY - Analytical Request Client Narne: �'p C, co r, Address:. Report to: Phone: PONunber: B)Or) Jo(i'n LA vl u WATER TECH LABS, INC. . PO BOX 1056 GRANITE FALLS, NC 28630 PHONE. (828).396-4444 Project Name: Project Number: Requested Analyses :J pH Checked —Upon Receipt Preservatives C12 < 02 g/1 Upon Receipt Saiiiple Ideatification 0 z 0 12, 0 C/I 5 J N 7- U 0 V A tl 0 010 1-4 'r 5 0 M C/) Z z Field Temp. (C*) Comments ry-N LI-15 X, Temperature (*61 7 1;-130 Received on Ice: Y / N L 7 Ova ISealed Cooler: Y / N ISanples Intact: I Y / N Additional Comments: L- W-211plidir-Marfie and,Signature-.-. - Printed Name of Sampler: Sam bucl�t. Signature of Sampler: 13-1 -)3 A CHi IN OF CUSTODY - Analytical Request Client Name: 0.0ah Amp u(y r Address: Report) to: Phone P O Ntinzb er: WATER TECH ]CABS, INC. PO BOX 1056 GRANITE FALLS., NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: Requested Analyses .I / 7 / � pH Checked Upon Receip Preservatives Cl2 < 0.2 mg/I Upon Receip } 4,. ' Sample Identification N •9 d ! � O z o boo N U o� cd J1 DO � 1 F, `. � � Cd z Field Temp. (C°) Comments i is-1743 0:06 r X X x X i .f .. o 12-30 Temperature (, C) Received on Ice: Y / Nlad 77 12 j �CLS Sealed Cooler,: Y / N Samples Intact Y / N Additional Comments; • - - • • - - Printed Name of Sampler: uckginS Signature of Sampler.60L �A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if Facilitv Address: Contact Person: 'I'Q1111 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County t rI' UL)L>JC I I Telephone #:2A -`]S(o y 111 No. of Wells to be Sampled:.._ Well Identification Number (from Permit): M W d,@ For Groundwater Treatment Systems Well Depth: - is it. Well Diameter: (c in. Check One: ❑ Influent (98) Screened Interval: A)l A- ft. to �_ it. ❑ Effluent (99) Depth to Water Level:—Qft. below measuring point. Measuring Point (M.P.) is:-al-1-3 ft. above land surface. Relative M.P. Elevation In ft.: Gallons of water pumped/bailed before sampling: (00_ Date sample collected: Field analysis: pH-1 , Specific Conductance uMhos Temp. I'- °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: LtW 00005003 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE PF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: �® Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: DPP CAP �. Laboratory Name: Wa}pr=f-P^1� Certification No. Sn PARAMETERS (Samples for metals were collected unfilteredX_YE5 NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 9-Z-7 0.33 mg/I (Note: Use MPN method for highly turbid samples) " Orthophosphate mg/I .Dissolved Solids: Total S-Q Cho mg/I Al- Aluminum 'R-rl y, 19 mg/I pH (when analyzed) units Ba - Barium 9 -'] d .14% mg/I TOC 4'--1 < 1 O mg/I Ca - Calcilim �-'] 30-o mg/I Chloride 9 -26 -7. o mg/I Cd - Cadmium Q `7 4.O. 00z.- mg/I Arsenic 16 -r1 0. MCI mg/I Chromium: Total 2-1 o•ooto mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium IS-1 mg/I TKN as N mg/I Mn - Manganese $-7 1 "39 mg/I YES NO) Cn 9 r! Fu m co D M Uoi Ni- Nickel _%- `7 6 . r Iq rag I .. Pb - Lead '7 O ; 0�53 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Selenium 5 -_9 4D.OL:55 ,Q 5o,AiJrh a-:1 ORGANICS:. (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ROC Report Attached? Yes (1) No (0) method # = method # method # SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Coc345 AmerimtA Permit Name (if different): Facility Address: TO ,k as mcicioe\ Mreel) A)C 9-82509 C ICnY) Sal) (ZtD) County rn �yW e.1 1 Contact Person: 11 t Q Telephone #: _q88 -` S 6-411 1 Well Location/ Site Name: W t No. of Wells to be Sampled: _ prom em,Iq Well Identification Number (from Permit): M W IQ For Groundwater Treatment Systems Well Depth: 1$ ft. Well Diameter: 7-in- Check One: ❑ Influent (98) Screened Interval: 0 A it. to to Pl ft. ❑ Effluent (99) Depth to Water Level:_12. ft. below measuring point. Measuring Point (M.P.) is: 4 j 3 ft. above land surface. Relative M.P. Elevation In ft.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: �- Field analysis: pHto— S , Specific Conductance umhos . Temp. .Ito OC, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 733-3Z PERMIT #: W G? O00-5k0&3 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: _ - NOTE: Values should reflect dissolved and . colloidal concentrations. -/ Date sample analyzed: e �P1t)L-) Laboratory Name: L. er -3-er h Certification No. __ SO PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MFTotal /100ml Phosphorus: Total as P%•27 40.Ito mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate nag/I Dissolved Solids: Total 2-9 1 mg/l AI - Aluminum 9`) 0.1 9 mg/I pH (when analyzed) 5--h lc�'� units Ba -Barium • I 0 .0 3 mg/I TOC %- 71 � 1.o mg/I Ca - Calcium V -r1 4 co , 50() mg/I Chloride %- Zt e 5 . o Mg Cd -Cadmium 9- - 7 40 . 00 Z mg/I Arsenic 4s-'•1 40.005mg/I Chromium: Total %-7 �� 00S m /I 9 Grease and Oils mg/I Cu - Copper mg/I Phenol rl mg/1 Fe - Iron mg/I Sulfate %- mg/l Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 9 -7 1-0-Sop mg/I TKN as N mg/I Mn - Manganese_` `1 0. oo 5 mg/I YES NO) Ni - Nickel- S-r] 0 rOCxl mg/1 Pb - Lead - rJ Co,OoK mg/( Zn - Zinc mg/1 Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) SelPniurv� -'� 40 0 5 ma IQ ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method.# = method # method # _ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: COOL "s A1rerinctr\ Permit Name (if d[Werent - Facility Address: 01 3toT5 _ Contact Person: w13,11 Well Location/ Site Name: County m� L&we 11 Telephone #: g98 '15(c -y 11 l No. of Wells to be Sampled:_ Well Identification Number (from Permit): MW l I R For Groundwater Treatment Systems Well Depth: 30 ft. Well Diameter: Z in. Check One: ❑ influent (98) Screened Interval: �A ft. to pil A ft. Depth to Water Level: 5 El Effluent (99) p �_ft. below measuring point. Measuring Point (M.P.) is: d it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: 'r' -6 -13 Field analysis: pH '1 11 , Specific Conductance UMhos Temp. 19 °C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total g-G 210 mg/I pH (when analyzed) 'R-la -7 -7 units TOC -4 -r] ,1.0 mg/I Chloride 9.210 S .'O mg/I Arsenic _19-9 4t)•UoS mg/I Grease and Oils mg/I Phenol mg/I Sulfate �' •`1 S9 -lo mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-16ns phnnc- 1Q1 M 777_99' PERMIT #: t.O© 0003( Q3 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE 9F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5ee, f3Plo Laboratory Name: . LA�ker -feed Certification No. 56 feredy YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P9-2'i ZI mg/I Orthophosphate mg/I Al -Aluminum 4- -9 0 IZS mg/I Ba - Barium 9 -'1 0 , 0LI(0 mg/I Ca - Calcium V -9 02;-9 mg/I. Cd - Cadmium-Fs-'1 40• 002- mg/I Chromium: Total <0.005 mgll Cu - Copper mg/I Fe - Iron mg/l Hg - Mercury mg/I. K - Potassium mg/I Mg - Magnesium Ov-:j -41.9 mg/I Mn - Manganese-9-1 40-005mg/I YES NO) ' Ni - Nickel 0 Zy mg/1 Pb - Lead;s 4 0. Oo S mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) 1 T% . Z nno 1. 4 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: L—t7 Permit Name (if differen ContactPerson:'YUI III Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County f I lk- t—.Dwy( t Telephone #: _aw -115(1) -4. No. of Wells to be Sampled: Well Identification Number (from Permit): M W -12 For Groundwater Treatment Systems Well Depth: 13 ft. Well Diameter- a in. Check One: ❑ Influent (98) Screened Interval: .N A ft. to M A it. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is: a.(o ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 9- Date sample collected: Field analysis: pH 61 � , Specific Conductance ' uMhos Temp. 19 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W Q 0W S(003 Non -Discharge EXPIRATION DATE: UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Applicalion of sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: See Selo Laboratory Name: LCUi1eL Tcar) Certification No. SO PARAMETERS (Samples for metals were collected unfiltered_VYES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P_9-2-7 0• �5mg/I (Note: Use MPN method for high[ turbid samples) Orthophosphate mg/I Dissolved Solids: Total - mg/I Al - Aluminum �- `7 0.1 t y mg/I pH (when analyzed)'Ato (o,R units Ba - BariumC)ISd mg/I TOC'R - 9 2,2-2 mg/I Ca.- Calcium mg/I Chloride (k •26 5.0 mg/I Cd - Cadmium Arsenic 9.9 4-0•00S mg/I Chromium: Total -S-9 <0,U05 mg/I Grease and Oils mg/l Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate is - q •6 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/1 Total Ammonia mg/I Mg - Magnesium mg/I TKN as N mg/I Mn - Manganese W • 7 LA , O(o mg/I -322 YES NO) Ni - Nickel- S - "] 0, O%S mg/1 Pb - Lead YS '' 1 40, S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 1141 O, Cen ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # method # SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: 0—m-A5 Amerimtan Permit Name (if djif�rent)* Fa4ity_Address: ` d COX apgs Contact Person: VD1 1I1 Well Location/ Site Name: County 1 r lc k10t.R.)e U Telephone #: 2k— No. of Wells to be Sampled: Well Identification Number (from Permit): JM ( ) -13 For Groundwater Treatment Systems Well Depth: 15 ft. Well Dia eter•: Z in. Check One; ❑ Influent (98) Screened Interval: Ail A ft. to eJj A it. ❑ Effluent (99) Depth to Water Level:�_ft. below measuring point. Measuring Point (M.P.) is:Z-•V ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: Date sample collected: g _13 Field analysis: pH 6• X, Specific Conductance uMhos Temp. % % °C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for high) turbid samples) Dissolved Solids: Total 'i•Q( Zllo pH (wh n analyzed) Q - b W •rl mg/I • 1 units TOC 1.31 mg/I Chloride Sr • Zto <5.O mg/I Arsenic 4--') 40-05o5 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 4's •'� Ztp•O mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: LA )I60050o3 Non -Discharge NPDES e: EXPIRATION DATE: UIC TYPE aF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: SPe 13e1O1 ) Laboratory Name:. _ Wa-t er -I-eC h Certification No. 5o IeredI/YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as PS -V7 40.1 bmg/I Orthophosphate mg/I Al - Aluminum_ 1 O•L)24 mg/I Ba - Barium �— O •U 0 mg/1 Ca - Calcium III Mg Cd -Cadmium Zmg/I Chromium: Total • rl n Ioy5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium -9 mg/I Mn - Manganese O , Z. mg/I. YES NO) Ni - Nickel_ $t �,0 mg/I Pb - Lean_ g • 73 C • QCK5 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) r \'1 o n, • h 4 o a'S rY1�S o ORGANICS: (GC,GC/MS.HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = � RO►tifllfha4 In the hac► of .nu Ln nudn.l..........� t-..r...c a�._ :-�----"— __-'- _-... _ .. .. _ . method# GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: • L;UC11 Permit Name (if different): Facilitv Address:_ Contact Person: � 1�r1J 1111 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type „0- �$ County f11C G)W t?11 �l Telephone #: 5�2�-r7Jn-�111 406 ' on No. of Wells to be Sampled: Well Identification Number (from Permit): Mt,J - tij Well Depth: lS 'it. Well Diameter: Z Screened Interval: � A ft. to NIA ft. Depth to Water Level: to ft. below measuring point Measuring Point (M.P.) is: 2•• to ft. above land surface. Gallons of water pumped/bailed before sampling: 3 Field analysis: pH._12 , Specific Conductance 1 For Groundwater Treatment Systems in. Checkone: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation In ft.: Date sample collected: �- -(a - 13 uMhos Temp. $ °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH NC 27699-1636 Phone: 919 733-3221 PERMIT #:LA-)&0()UcS(D6,3 EXPIRATION -DATE: Non -Discharge UIC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infillrallon Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: _ 3pe )3e) LJ Laboratory Name: -_ waked 'Tee h Certification No.— e) PARAMETERS (Samples for metals were collected unfiltered__1%.ZYES NO and field acidified COD mg/l Nitrite (NO2) as N mg /I Coliform: MF Fecal /100ml Nitrate (NO3) as N m/I g Coliform: MF Total /100mI Phosphorus: Total as P �-2''] t:�Z1 mg/I (Note: Use MPN method for highl turbid samples) Orthophosphate mg/I Dissolved Solids: Total .Q �- (o a4p mg/I O l Al - AluminuW1, mg/I pH (when analyzed) g •rl (c�. R units Ba - BariumO- I t-1 mg/I TOC t-I,g(a mg/I Ca - CalciumS, mg/I Chloride • ac(e $ 5.0 mg/f Cd - Cadmiu02 mg/I Arsenic -�1 40.005 mg/I Chromium: T<O .OUS mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate �- r1 mg/I fo1. t` mg/I Fe - Iron Hg - Mercury m /I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia TKN as N mgll Mg - Magnesium -g - `7 3S mg/I mg/I Mn - Manganese_%-`l Q, S70 mg/I YES NO) Ni - Nickel �'� Pb - LeZ ' 9 b , c� 2�(1 mg/1 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mgll Other (Specify Compounds and Concentration Units) _6eNeniom TEI�.OfJ ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #.Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Names Permit Name (if Contact Person: 9i 1 1111 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I t 11-i LX�), 3t? t I Telephone M %'r7 No. of Wells to be Sampted: Well Identification Number (from Permit): DOLO -'1 Well Depth: 1-6 ft. Well Diameter: Z in Screened Interval:_ it. to ft. Depth to Water Level: to - q ft. below measuring point. Measuring Point (M.P.) is: 2• �o ft. above land surface. Re Gallons of water pumped/bailed before sampling: Field analysis: pH (0- L , Specific Conductance Temp. - —°C, Odor At) For Groundwater Treatment Systems Check One: ❑ Influent (98) ❑ Effluent (99) lative M.P. Elevation in #t.: Date sample collected:-13 uMhos )earance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total S-9 (oo m9 /l pH (when analyzed) lz�- (o (o• k-o units TOC c6 • I 3.30 mg/I Chloride _S' -2 Cc 46. mg/I Arsenic a • q 4o•oo-s mg/I Grease and Oils mg/I Phenol mg/I Sulfate • to mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT #: W Non -Discharge DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: UIC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remediallon: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Laboratory Name: (" Certification No. 0 red V YES NO and field acidified Nitrite (NO2) as N mg/I9 Nitrate'(NO3) as N m /I Phosphorus: Total as PS •21 404to mg/I Orthophosphate mg/I Al -Aluminum 0a -'"1 0 q y mg/I Ba - Barium 18 • 2 mg/I Ca - Calcium -Tl -7G . mg/I Cd - Cadmium S_ •' 1 4o • OOZmg/I Chromium: Total �•'-7 LO.oCS mg/I. Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury m /I K - Potassium mg/l Mg - Magnesium g • r1 26 • mg/I Mn - Manganese_g _� t "L mg/I 3-3 YES NO) Ni - Nickel_ �s • `� �, pJ S _ mg/I Pb - Leari'R • rj O •[�\� mg/I Zn - Zinc. mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ���� �•r] 2..2 mat 0 �e 1•e� iy cr 8• -`1 � � tx�2 n� �t ORGANICS: (GC;GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = method # = GW-59A COMPLIANCE REPORT FORM Permit # UJ® M05&o03 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( -12 --13) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 9 or 2 is "YES', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "k'es ", contact the Regional Ofce forguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s) exceeding standards in the space provided below. M W # ly W Z Mw12 7 D S 54b��.SL Lead C�.os3^►��.R DS 59orna',A, 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES". list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). M��- n^ W-t� m w 41 % +}-12-1.3 14-q-13 y-4-13 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO if the answer is "YES", a -groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation Fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby ackn.' e e thatAh6,f-above 1iiG nation wasy'Rfil' ated and the infocimatiQn submltied�n ibis wtitt� a ;report (Comp,ian Report GW 59A} !s true d complete to theLbest of my knowle(ge „wti',# Signa a of Permittee Authorize Agent) Date GIB'-59A 12/8/2003 , id Pr,rR6Tx.cn Ln POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#02) COLLECTION DATE. 8/6/2013 PERMIT #. -COLLECTION TIME. 07:45 ADDRESS., Coats America (Wells) RECEIVED DATE. 8/6/2013 P.O. Box 368 Marion, NC 28752 RECEIVED TIME: 14:30 REPORTED: 9/4/2013 . ANALYSIS;` ANALYSIS RESULTS UNITS : DATE . - -.'ANAL TDS 96 mg/L 8/9/13 lag Chloride 7.0 mg/L 8/26/13 lag T. Phosphorus 0.33 mg/L 8/27113 jdg TOC <1.0 mg/L 817/13 Sulfate 124 mg/L 817/13 metals see attached pH 7.4 su's 816/13 lag LOG ID: 1308-106 REPORTED BY: NC CERTIFIED LAB # 50 fl�. Tony Gragg, Lab Supervisor w#wrzwR6TvcHLR' S.Inc. POST OFFICE SOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 8/6/2013 PERMIT A COLLECTION TIME. 07:56 ADDRESS: Coats America (Wells) RECEIVED DATE., 8/6/2013 P.O. Box 368 RECEIVED TIME: 14:30 Marion, NC 28752 REPORTED., 9/4/2013 ANAL) ANALYSIS: RESULTS . UNITS- TDS 120 mg/L Chloride <5.0 mg/L T. Phosphorus <0.16 mg/L TOC • <1.0 mg/L Sulfate 26.4 mg/L metals see attached pH 6.7 su's IS, DATE ANALYST, 8/9/13 lag 8/26/13 lag 8/27113 jdg 817/13 817/13 8/6/13 lag LOG 1D. 1308-107 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)3964444 SAMPLE., Coats America (MW#1 1) COLLECTION DATE.- 8/6/2013 PERMIT COLLECTION TIME: 08:02 ADDRESS., Coats America (Wells) RECEIVED DATE: 8/612013 P.O. Box 368 RECEIVED TIME. 14:30 Marion, NC 28752 REPORTED., 9/4/2013 HA. LYSIS :,. --A ANALYSIS . &L-.-. IRES T 'S. UNITS %7� ANALYST TDS 210 mg/L 819/13 lag Chloride 5.0 mg/L 8/26/13 lag T. Phosphows 0.21 mg/L 8/27/13 idg TOC - <1.0 mg/L 8/7/13 Sulfate 38.6 mg/L 8/7/13 metals see attached pH 8.4 stfs 8/6113 lag LOG JD: 1308-108 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor wiwTvR6rr- cH 1 s./nc. POST OFFICE BOX 1056 • n5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 8/6/2013 PERMITA- COLLECTION TIME. 08:13 ADDRESS., Coats America (Wells) RECEIVED DATE: 8/6/2013 P.O. Box 368 RECEIVED TIME." 14:30 Marion, NC 28752 REPORTED. 9/4/2013 ANALYSIS: ANALYSIS: , . RESULTS UNITS :... DATE ANALYST TDS 590 mg/L 8/9/13 lag Chloride 5.0 mg/L 8/26113 lag T. Phosphorus 0.25 mg/L 8/27113 jdg TOG - 2.28 mg/L 8/7/13 Sulfate 58.0 mg/L 817/13 metals see attached pH 6.8 su's 8/6/13 lag LOG ID: 1308-109 REPORTED BY: NC CERTIFIED LAB # 50 f�(Aliff Tony Gragg, Lab Supervisor vrxR6rtrcHLan, POST OFFICE SOX 1056 - #5 PINEWOOD PLAZNDR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#13) COLLECTION PATE: 8/6/2013 PERMIT A COLLECTION TIME: 08:19 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/6/2013 P.O. Box 368 RECEIVED TIME: 14:30 Marion, NC 28752 REPORTED. 9/4/2013 ANALYSIS ; ANALYSIS RESCILFS UNITS DATE ANALYST .; TDS 216 mg/L 8/9/13 lag Chloride <5.0 mg/L 8126113 lag T. Phosphorus <0.16 ' mg/L 8/27/13 jdg TOC 1.31 mg/L 817/13 Sulfate 26.0 mg/L 8/7/13 metals see attached pH 6.2 su's 8/6/13 lag LOG ID: 1308-110 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor URrAwCH .r/nc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE., Coats America (MW#1 4) COLLECTION DATE: 8/6/2013 PERMIT#. COLLECTION TIME: 08:24 ADDRESS., Coats America (Wells) RECEIVED DATE., 8/6/2013 P.O. Sox 368 RECEIVED TIME., 14:30 Marion, NC 28752 REPORTED: 91412013 ANALYSIS; LTS RESU -UNITS. DATE ANALYST TDS 546 mg/L 8/9/13 lag Chloride <5.0 mg/L 8126113 lag .T. Phosphorus 0.21 mg/L 8/27113 jdg TOC 4.96 mg/L 8/7113 Sulfate 61.1 mg/L 8/7/13 metals see attached pH 6.8 su's 8/6/13 lag LOG ID: 1308-111 REPORTED BY: NC CERTIFIED LAB # 50 f�'. * Tony Gragg, Lab Supervisor r warm R rcH I a— s-c_ POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 8/6/2013 PERMIT A COLLECTION TIME: 08:33 ADDRESS., Coats America (Wells) RECEIVED DATE: 8/6/2013 P.O. Box 368 RECEIVED TIME.- 14:30 Marion, -NC 28752 REPORTED: 9/4/2013 AN�4LYSIS ANALYSIS RESULTS :. UNITS ' DATE ANALYST:. TDS 360 mg/L 8/9/13 lag Chloride <5.0 mg/L 8/26/13 lag T. Phosphorus <0.16 mg/L 8/27/13 jdg TOC 3.30 mg/L 817/13 Sulfate 65.6 mg/L 8/7/13 metals see attached pH 6.7 su's 816113 lag LOG ID: 1308-112 REPORTED BY: NC_ CERTEFIED LAB # 50 Tony Gragg, Lab Supervisor RESEARCh & ANA1yTiCA[ LABORATORIES, INC. 4 „ ¢ •+ o : cn NCf34 - Analytical/Process Consultations BRED Water Tech Labs. Inc. Date Sample Collected : 08/06/13 P.O. Box 1056 Date Sample Received : 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed : 08/'07/13 Attn: Joe Gragg Date of Report : 08/14/13 Analyses Performed by : AP -KL -JC Lab Sample Number 764566 Parameter Storet # Results TOC (00680) <1.0 mg/1 Sulfate (00945) 124 mg/l Magnesium,Tot (00927) 15:7 mg/1 Lead,Tot (01051) 0.053 mg/l Manganese,Tot (01055) 1.38 mg/1 Aluminum,Tot (01105) 4.19 mg/l Calcium,Tot (00916) 30.0 mg/l Chromium,Tot (01034) 0.006 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) 0.019 mg/l Sodium,Tot (00929) 9.70 mg/l Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.148 mg/l Arsenic,Tot (01002) 0.009 mg/l -------------------- Clients Sample Source COATS AMERICAN MW2 Number Time Collected (Hrs) 0745 P.O. Box 473. 106 Short Street - Kernersville, North Carolina 27284.336-996-2841 - Fax 336-996-0326 www.randalabs.com RESEARch & ANAIYTICAI. LAbORATORIES, INC. Analytical/Process Consultations Cs C *RED A% Water Tech Labs. Inc. Date Sample Collected : 08/06/13 P.O. Box 1056 Date Sample Received : 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed : 08/07/13. Attn: Joe Gragg Date of Report : 08/14/13 Analyses Performed by : AP -KL -JC Lab Sample Number -------------- 764567 Parameter Storet # Results TOC (00680) <1.0 mg/l Sulfate (00945) 26.4 mg/l Magnesium,Tot (00927) <0.500 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) <0.005 mg/l Aluminum,Tot (01105) 0.137 mg/l Calcium,Tot (00916) <0.500 mg/l Chromium,Tot (01034). <0.005 mg/1 .Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) 0.009 mg/1 Sodium,Tot (00929) 49.6 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.013 mg/l Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICAN MW10 Number Time Collected (Hrs) 0756 P.O. Box 473. 106 Short Street,• Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCh & ANALyTICA1 LZORATORIES, INC. Analytical/Process Consultations W. :- ac a cc NC r� ' ����f�Y''• 5 Water Tech Labs. Inc. Date Sample Collected : 08/06/13 P.O. Box 1056 Date Sample Received : 08/07/13 Granite_ Falls, NC 28630 Date Sample Analyzed : 08/07/13 Attn: Joe Gragg Date of Report : 08/14/13 Analyses Performed by : AP -KL -JC Lab Sample Number -------------------- 764568 Parameter Storet # Results TOC (00680) <1.0 mg/l Sulfate (00945) 38.6 mg/l Magnesium,Tot (00927) 21.9 mg/l Lead,Tot (01051) <0.005 mg/l Ma.nganese,Tot (01055) <0.005 mg/l Aluminum,Tot (01105) 0.125 mg/l Calcium,Tot (00916) 68.4 m4/1 Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027,) <0.002 mg/l Nickel,Tot (01067) 0.024 mg/l Sodium,Tot (00929) 17.2 mg/l Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0,046 mg/l Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample -Source COATS AMERICAN MW11R Number Time Collected (Hrs) 0802 P.O. Box 473. 106 Short Street - Kernersville, North Carolina 27284.336-996-2841 - Fax 336-996-0326 www.randalabs.com Aft RESEARch & ANA[yTICA1 ` LABORATORIES, INC. M �:y Zt PZ ,•. = NO �i34 _ -p, Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected : 08/06/13 P.O. Box 1056 Date Sample Received : 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed : 08/07/13 Attn: Joe Gragg. Date of Report : 08/14/13 Analyses Performed by : AP -KL -JC Lab Sample Number -------------------- 764569 x Parameter Storet # Results TOC 2.28 mg/l Sulfate (00945) 58.0 mg/l Magnesium,Tot (00927) 13.9 mg/l Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 4.06 mg/l Aluminum,Tot (01105) 0.114 mg/l Calcium,Tot (00916) 92.1 mg/l Chromium,Tot (01034) <0..005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) 0.048 mg/l Sodium,Tot (0'0929) 114 mg/l Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.150 mg/1 Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICAN MW12 Number Time Collected (Hrs) 0813 P.O. Box 473. 106 Short Street • Kernersville. North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCLI & ANALYTICAL �ION •••• r .•••4 C•••. ++ -_ LkO-RATORIES, INC. 0 a • NOWz• #34 _ Analytical/Process Consultations J- ��i � •'•• �REGKb4' �5 •�•� Water Tech Labs. Inc. Date Sample Collected 08/06/13 P.O. Box 1056 Date Sample Received 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed 08/07/13 Attn: Joe Gragg Date of Report 08/14/13 - Analyses Performed by AP -KL -JC Lab Sample Number -------------------- 764570 Parameter Storet # Results TOC (00680) 1.31 mg/1 Sulfate (00945) 26.0 mg/l Magnesium,Tot (00927) 7.20 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) 0.182 mg/l Aluminum,Tot (01105) 0.029 mg/l Calcium,Tot (00916) 11.4 mg/l Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) 0..012 mg/l Sodium,Tot (00929) 62.1 mg/l Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.030 mg/l Arsenic,Tot (01002) <0.005 mg/1 -------------------- Clients Sample Source COATS AMERICAN MW13 Number Time Collected (Hrs) 0819 P. 0. Box 473. 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARch & ANA[yTICA1 LAhORATORIES, INC. Analytical/Process Consultations v Water Tech Labs. Inc. Date Sample Collected 08/06/13 P.O. Box 1056 Date Sample Received 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed 08/07/13 Attn: Joe Gragg. Date of Report 08/14/13 Analyses Performed by AP -KL -JC Lab Sample Number . -------------------- 764571 Parameter Storet # Results TOC (00680) 4.96 mg/l Sulfate (00945) 61.1 mg/1 Magnesium,Tot (00927) 35.2 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) 0.570 mg/l Aluminum,Tot (01105) 0.196 mg/l Calcium,Tot (00916) 55.9 mg/1 Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) 0.030 mg/l Sodium,Tot (00929) 92.4 mg/1 Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.144 mg/1 Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICAN MW14 Number Time Collected (Hrs) 0824 P. 0. Box 473. 106 Short Street - Kernersville, North Carolina 27284.336-996-2841 - Fax 336-996-0326 uwwv.randalabs.com RESEARch & ANA[yTICA[ LAbORATORIE- , INC. Analytical/Process Consultations ,�1�iir r rU��i ¢ � NC Z! cn Z. #34 � b Water Tech Labs. Inc. Date Sample Collected : 08/06/13 P.O. Box 1056 Date Sample Received : 08/07/13 Granite Falls, NC 28630 Date Sample Analyzed : 08/07/13 Attn: Joe Gragg Date of Report : 08/14/13 Analyses Performed by : AP -KL -JC `Lab Sample Number ----------------- 764572 Parameter Storet # Results TOC 3.30 mg/1 Sulfate (00945) 65.6 mg/l Magnesium,Tot (00927) 26.1 mg/l Lead,Tot (01051) 0.013 mg/l Manganese,Tot (01055) 1.23 mg/l Aluminum,Tot (01105) 0.794 mg/l Calcium,Tot (00916) 79.4 mg/l Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) 0.045 mg/l Sodium,Tot (00929) 22.2 mg/l Selenium,Tot (01147) <0.002 mg/l Barium,Tot (01007) 0.132 mg/1 Arsenic,Tot (01002) <0.005 mg/1 -------------------- Clients Sample Source COATS AMERICAN MW15 Number Time Collected (Hrs) 0833 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:J. Permit Name (if Facilitv Address: Contact Person:- 3:311 11 1 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County 11'Lr1l(iW+t-1 t Telephone #: Rai -r 'f --' No. of Wells to be Sampled: Well Identification Number (from Permit): T11 W " cat Well Depth: it. Well Diameter: _ Screened Interval: ft. to } Pf ft. Depth to Water Level: Left. below measuring point. Measuring Point (M.P.) is: ft. above land surface. Gallons of water pumped/bailed before sampling: Field analysis: pH_ 1 , Specific Conductance Temp. °C, Odor A PARAMETERS (Samples for metals were collected i COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total 1100ml (Note: Use MPH method for high) turbid samples) Dissolved Solids: Total t4-12- 90 mg/I PH (when analyzed) `� -9 �+ 1 units TOC_ -1N Z'1 . r� mg/I Chloride LI-12 (n::3 mg/I Arsenic Ll -1 1 L 01 CQS mg/I Grease and Oils mg/I Phenol mg/I Sulfate y +11 �- I©_ mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I For Groundwater Treatment Systems in. Check One: ❑ Influent (98) ❑ Effluent (99) DEPARTMENT OF ENVIRONMENT & NATURAL RESC WATER QUALITY DIVISION, GROUNDWATER SECTIO 1636 MAIL SERVICE CENTER PERMIT #: W QW05(.00 EXPIRATION DATE: _ Non -Discharge UIC -,* O NPDES TYPE PERMITTED OPERATION BEING MONITORED 0 Q Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: (D Rotary Distributor Land Applic U I Sludge Other: NOTE: Values should reflect dissolved and MAY 2 12013 colloidal concentrations. Relative M.P. Elevation in ft: WATER QUALITY SECTION` _(� Date sample collected: Date sample analyzed: (it' &, rC) f'I�RMATION PROCESSING UNIT uMhos Laboratory Name: _ �APC 'TPQb ppearance Certification No. ered/NYES NO and field acidified Nitrite (NO2) as N mg/l Nitrate (NO3) as N mg/I Phosphorus: Total as P C/ fZyLIR mg/I Orthophosphate. mg/I Al - Aluminum H rl1 o, R 3 mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd -Cadmium '� -11 o. on a- mg/l Chromium: Total -i 1 6,WS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium -I Irk mg/I Mn - Manganese_C-I-11 6.316 mg/I /\ YES NO) Ni - Nickel y -11 <a �5 mg/1 Pb -Lead-0 I mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) M; M l ElIPOiJrn L)-11 LCi= OS f �tj sz Sr)cl i L) 14- l l ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No, (0) VOC method # = method # _ method # = Rev. 03/2000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: C-ap American Permit Name (if different : Facility Address: T O Contact Person: ram=( Well Location/ Site Name: County f 11' L)O let 1 Telephone #: 2as -15(o - Ll No. of Wells to be Sampled:. Well Identification Number (from Permit): ML-0- 16 For Groundwater Treatment Systems Well Depth: 1 %_ it. Well Qiameter.. a in. Check One: ❑ Influent (98) Scr11 eened lnlerval: n3 Pt ft. to iJ I A �ft. ElEffluent (99) Depth to Water Level: to .1 ft. below measuring point. Measuring Point (M.P.) is: a,3 it. above land surface. Relative M.P. Elevation in Gallons of water pumped/bailed before sampling: "— Date sample collected: Field analysis: pH tD , Specific Conductance uMhos Temp._°C, Odor Appearance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total LI - IZ 1N Lk mg/I pH (when analyzed)'-1 -R units TOC f-1- 2G 1.0 mg/I Chloride 41 1 to . 3 mg/I Arsenic y -11 4 a.0O5 mg/I Grease and Oils mg/I Phenol mg/I Sulfate !A -IN ZR.L1 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/l DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 733-32: PERMIT #: W O C' WS (o 03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. -9 -/ Date sample analyzed: OS& t? Ip t.') LaboratoryName: 16�cffi,1 -Tec-h Certification No. qn red_ /\ YES -NO and. field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 9-1Q Lo,18 mg/I Orthophosphate mg/I AI - Aluminum 14-11 40.C)RS mg/I Ba - Barium _N -11 O .00(0 mg/I Ca - Calcium LI-11 LD s5oo mg/I Cd - Cadmium 4-11 4 0 009 mg/I Chromium: Total W -11 4, 0 , 005 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium �1-11 Lo �oomg/I Mn - Manganese 4-11 40.005 mg/l —A YES NO) Ni - Nickel_ _`I-11 4.0. L05 mg/I Pb - Leader -11 O f 00's mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/l Other (SpecifyCompoundsand Concentration Units) 10.0 0 • f0 Ma I .Q Se.lPYli LJm y -11 0.66 5 MA a ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = 'SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: cpalb American Permit Name (if different Facilitv Address: FAD C)X `6te$ Contact Person: rf Well Location/ Site Name: County Telephone #: ' 11510 -L No. of Wells to be Sampled: Well Identification Number (from Permit): 1 I 1(; For Groundwater Treatment Systems Well Depth: '6� ft. Well Diameter- cZ in. Check0ne: ❑ Influent (98) Screened Interval: —N- ft. to 1 ft. ❑ Effluent (99) Depth to Water Level: ff. below measuring point. Measuring Point (M.P.) is: a it. above land surface. Relative M.P. Elevation in #t.: Gallons of water pumped/bailed before sampling: 9 Date sample collected: ^ Field analysis: pH S - O , Specific Conductance uMhos Temp. Z0 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: 19191733-325 PERMIT #: LA)& (M()S(D03 'EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5 P %ln c Laboratory Name: 1 Pr Teoun Certification No. 50 PARAMETERS (Samples for metals were -collected unfiltered A YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P y -29 LO•l to mg/I (Note: Use MPN method for highly turbid samples) Orthbphosphate mg/I Dissolved Solids: Total L>-12 ZZ2 mg/I Al - Aluminum LI-11 46. 025 mg/I pH (when analyzed) L1-051 units Ba - Barium Ll -1k 01038 mg/I TOC y-I1 mg/I Ca - Calcium Ll-I1 36. to mg/I Chloride tJ- -1'Z to 5 mg/I Cd -Cadmium U-11 10-00--L mg/I Arsenic LA-1) 40.005 mg/I Chromium: Total L4-I1 40IM5 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate AWA mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg -Magnesium 14-11 1'71-9 mg/I TKN as N mg/I Mn -Manganese LA -11 1,01005 mg/I _,EYES NO) Ni - Nickel y -11 4 0 -008 mg/1 Pb - Lean `^I-1 1_ 4o cm,5, mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:s Permit Name (if Facility Address: Contact Person:3:ff 1% "' Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County f f 'V tJUWC t 1 Telephone #: No. of Wells to be Sampled: Well Identification Number (from Permit): M W - I Z- For Groundwater Treatment Systems Well Depth: I r_� ft. Well Diameter. Q in. Check One: ❑ Influent (98) Screened Interval: ft. to it. ElEffluent (99) Depth to Water Level: 8 ft. below measuring point. Measuring Point (M.P.) is: ISO ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: I & 5 Date sample collected: LA -13 Field analysis: pH S Specific Conductance uMhos Temp. °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phnno- M M 777-17- PERMIT #: LO Q 0oa 5(c03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: S,ee 5fl e-m-z Laboratory Name: (A--) T-e to Certification No. O PARAMETERS (Samples for metals were collected unfiltered )k YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P L-1-29 �O.l b mg/I (Note: Use MPN method for highly turbid samples) LHZ tDSLI Orthophosphate mg/I Dissolved Solids: Total mg/I Al -Aluminum 4-11 4 b. oZS mg/I pH (when analyzed) CI units. Ba - Barium L1 -11 0, 101 mg/I TOC -11 mg/i Ca - Calcium 14 -11 r12. 3 a mg/I Chloride 4-12 (o.o mg/I Cd - Cadmium -11 L.p100Z mg/I Arsenic L1-11 40-U05 mg/I Chromium: Total LI-11 4.0�UUS mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate y-I 1 ti b• O mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 14-11 13.6 mg/I TKN as N mg/I Mn - Manganese L1 -11 21 $5 mg/I x YES NO) Ni - Nickel. L� 11 mg/1 Pb - Lead-9 -1 1 4 O• DOS mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) iL4 -I I R'g Mall 14 -1 t O Lc� 4I,9, ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # _ method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if FAddress: M ('I br., Contact P Well Location/ Site Name: n SUBMIT FORM ON YELLOW PAPER ONLY Please Pr/nt Clearly or Type County 9 f 11 ' kJU t Telephone #: No. of Wells to be Sampled: Well Identification Number (from Permit): VY)W -13 For Groundwater Treatment Systems Well Depth: 151 ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: �F ft. to &jI A ft. El Effluent (99) Depth to Water Level:__Q'!_g below measuring point. Measuring Point (M.P.) is: I -AD ft. above land surface. Relative M.P. Elevation In ft.: Gallons of water pumped/bailed before sampling: 1 5 Date sample collected: y.'4-1.3 Field analysis: pH 3 , Specific Conductance uMhos Temp. __U0_ °C, Odor Appearance PARAMETERS (Samples for metals were collected unfilte -COD mg/l Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total a-12 Zl0 mg/I pH (when analyzed) 4-01 65 units TOC 4-It 1 it-15 mg/I Chloride W-1Z 45to mg/I Arsenic y -1l /,0 -005 mgll Grease and Oils mg/I Phenol mg/I Sulfate -11 43 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 phnnP* 1a7 41 7'41-111, PERMIT#:t#-)c?Ocx36(o03 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: _ NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: LaboratoryName: -_ WQ} P r T Certification No. SO red_ A YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as PL4-Z9 40,16 mg/I Orthophosphate mg/I Al - Aluminum LI-11 D1024 mg/I Ba - Barium LA - I I �9.5 mg/I Ca - Calcium-11 0l (00 mg/I Cd -Cadmium �� -1 1 c� .002 mg/I Chromium: Total LI -11 t o.006 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium -y-11 (D.50 mg/I Mn - Manganese_U -11 b.Od2 mg/I YES NO) . Ni -Nickel. �I-11 4,6,t0S mg/1 Pb - Lead LA -1 1 0 005 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) t M —t Ven*Om 14- rn ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:S Permit Name (if i Facility Address: Contact Person:r' I 1!i" Well Location/ Site Name:. SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I I I' I Telephone #: 0%1 (o. No. of Wells to be Sampled: Well Identification Number (from Permit): - I For Groundwater Treatment Systems Well Depth: Is ft. Well Diameter- 2 in. Check One: ❑ Influent (98) Screened Interval: AAA ft. to J ft. ❑ Effluent (99) Depth to Water Level: lot I to ft. below measuring point. Measuring Point (M.P.) is: a 1 to ft. above land surface. Relative M.P. Elevation In ft.: Gallons of water pumped/bailed before sampling: 2.aS Date sample collected: y -4 Field analysis: pH0 , Specific Conductance _ uMhos Temp. 1 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:'lam Q00C) %(a03 EXPIRATION DATE: Non -Discharge NPDES UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _ Laboratory Name: W er T� h0�— Certification No. _ IC-10 PARAMETERS (Samples for metals were collected unfiltered)� YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total. /100ml Phosphorus: Total as P U-Zq L�,tlo mnLl (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total y -I 'Z 39 (o mg/I pH (when analyzed) 11-4 6-0 units TOC q-11 , 5$ mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate LA -►1 t-Ib I 55 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum 1�_ F. So,n25 mg/I Ba -Barium y -11 D, o$ 1 mg/I Ca - Calcium 14 -11 (PLA i to mg/I Cd - Cadmium 9 -11 4 o , oo—r- mg/I Chromium: Total A-lj 40-(�5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium Ll-11 140.9 mg/I Mn - Manganese y--11 h,?0'1 ma/I YES NO) Ni - Nickell I C b, c S mg/I Pb - Lead Ll -11 4.o . 005 mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) � i ot,r% Delfni om y -11 4.0,OOS nna ,Q ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes(1) No (0) VOC . : method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: L Permit Name (if Facility Address: Contact Person: V It I►I Well Location/ Site Name: Al 'SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I I ►- lu 3 ue 11 Telephone #: (D No. of Wells to be Sampled: Well Identification Number (from Permit): M LA) -15 Well Depth: 1 to it. Well DiameterZ Screened Interval: A -)I f ft. to X- ft. Depth to Water Level: 3 ft. below measuring point. Measuring Point (M.P.) is:_La It. above land surface. Gallons of water pumped/bailed before sampling: � Field analysis: pH (oI 4 _ , Specific Conductance . Temp. 1q QC, Odor A PARAMETERS (Samples for metals were collected un COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH method for high) turbid samples) Dissolved Solids: Total -12 0 m9 /I pH (when analyzed) L1-G (o%Ll units TOC L` -11 I , c50 mg/I Chloride 'A-12 45, O g m /I Arsenic W-11 mg/I Grease and Oils Phenol Sulfate -11 mg/1 mg/I 22, to mg/I Specific Conductance - uMhos Total Ammonia TKN as N mg/I mg/1 For Groundwater Treatment Systems in. Check one: ❑ Influent (98) El Effluent (99) Relative M.P. Elevation In ft.: Date sample collected: uMhos DDearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W Q 0WSkc03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5 FolA%_0 Laboratory Name: kPr Tech Certification No. 50 tared A YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as Py-29 1,0,I b mg/I Orthophosphate mg/I Al - Aluminum A-11 4.b.cx5 mg/1 Ba - Barium 4-11 6,pgI mg/I Ca - Calcium _ 4 -11 "7 2 1 mg/I Cd -Cadmium 14-1 I mg/I Chromium: Total 4-11 4.O,yo5 m9 /I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium A-1 I 2S,q mg/I Mn -Manganese -11 1,35 mg/I RYES NO) - Ni - Nickel L1-11 4,0,005 g/ m I Pb - Lead L1-11 0 1005 mg/I -Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) - 1 16A _Se 1-ent orv-N L1-11 �o.t�S m4 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # m 011-4 4 _ RTER4T CH L178-5.Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#02) COLLECTIONDATE: 4/9/2013 PERMITA- COLLECTION TIME: 09:13 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/9/2013 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST' . TDS 90 mg/L 4/12/13 lag Chloride 6.3 mg/L 4/12/13 lag T. Phosphorus 0.18 mg/L 4/29/13 )dg TOC <1,0 mg/L 4/11/13 Sulfate <10.0 mg/L 4/11/13 metals see attached pH 7.9 su's 4/9/13 lag LOG ID: 1304-199 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor I 1d r , 4mcm murs.Inc. 4 POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28530 (828) 396-4444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 4/9/2013 PERMIT #. COLLECTION TIME: 09:23. ADDRESS: Coats America (Wells) RECEIVED DATE., 4/9/2013 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS 'RESULTS UNITS DATE ANALYST TDS 144 mg/L 4112113 lag Chloride 6.3 mg/L 4112/13 lag T. Phosphorus <0.16 mg/L 4/29/13 ldg TOC <1.0 mg/L 4111/13 Sulfate 38.4 mg/L 4/11/13 metals see attached pH 6.6 su's 4/9/13 lag ' LOG ID: 1304-200 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor IdOrER ECH LITIPSInc. POST OFFICE BOX 1056 • 46 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#11 B) COLLECTION DATE: 4/9/2013 PERMIT #: COLLECTION TIME: 09:35 ADDRESS: RECEIVED DATE: 4/9/2013 RECEIVED TIME: 15:00 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 222 mg/L 4/12/13 lag Chloride 6.5 mg/L 4/12/13 lag T. Phosphorus <0.16 mg/L 4129/13 ldg TOC <1.0 mg/L 4/11/13 Sulfate 51.4 mg/L 4/11/13 metals see attached pH 8.5 su's 4/9113 lag ,a LOG ID: 1304-201 REPORTED BY: NC CERTIFIED LAB # 50 fl� Tony Gragg, Lab Supervisor M POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 4/9/2013 PERMITA- COLLECTION TIME: 09:48 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/9/2013 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS .654 mg/L 4/12/13 lag Chloride 6.0 mg/L 4/12113 lag T. Phosphorus <0.16 mg/L 4/29/13 Jdg TOC 1.96 mg/L 4/11/13 Sulfate <10.0 mg/L 4/11/13 metals see attached pH 6.8 su's 4/9/13 lag LOG ID: 1304-202 REPORTED BY: NC CERTIFIED LAB # 50 fo� * Tony Gragg, Lab Supervisor "RiTECH LRE•ICiC. f POST OFFICE BOX 1056 • 45 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#13) COLLECTION DATE: 4/9/2013 PERMIT #: COLLECTION TIME: 10:01 ADDRESS: Coats America (Wells) RECEIVED DATE. 4/9/2013 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 210 mg/L 4112/13 lag Chloride <5.0 mg/L 4/12/13 lag T. Phosphorus <0.16 mg/L 4/29113 jdg TOC 1.45 mg/L 4/11113 Sulfate 43.9 mg/L 4111/13 metals see attached pH 6.3 su's 4/9113 lag LOG ID: 1304-203 REPORTED BY: NBC, CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor miumirrCH LIT11.5-inc, i POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 4/9/2013 PERMIT #: COLLECTION TIME: 10:08 ADDRESS: Coats America (Wells) RECEIVED DATE 4/9/2013 P.O. Box 368 RECEIVED TIME: 15:00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 396 mg/L 4/12113 lag Chloride <5.0 mg/L 4/12/13 lag T. Phosphorus <0.16 mg/L 4/29/13 jdg TOC 2.38 mg/L 4/11/13 Sulfate 40.5 mg/L 4/11/13 metals see attached pH 6.7 su's 419113 lag LOG ID: 1304-204 REPORTED BY: NC CERTIFIED LAB # 50 ff� * Tony Gragg, Lab Supervisor ldfirEriv e POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS. NORTH CAROLINA 28630 (828) 39&4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 4/9/2013 PERMIT #: COLLECTION TIME: 10:18 ADDRESS: Coats America (Wells) RECEIVED DATE.- 4/9/2013 P.O. Box 368 RECEIVED TIME: 15.00 Marion, NC 28752 REPORTED: 5/10/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS 330 mg/L 4/12113 lag Chloride <5.0 mg/L 4/12/13 lag T. Phosphorus <0.16 mg/L 4/29/13 Jdg TOC 1.50 mg/L 4/11113 Sulfate 22.6 mg/L 4/11/13 metals see attached pH 6.6 su's - 419/13 lag LOG ID: 1304-205 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor RESEARCh & ANA1yTICA1 LAbORATWES, INC. Analytical/Process Consultations ♦iit��►I Iltfl�tl ly Z w . . V. 14; 416) ANw `ii` �40ti11'311106 Water Tech Labs. Inc. Date Sample Collected 04/09/13 P.O. Box 1056 Date Sample Received 04/11/13 Granite Falls, NC 28630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report 05/01/13 Analyses Performed by JC -SK Lab Sample Number ----------------- 755496 Parameter Storet # - Results Magnesium,Tot (00927) 7.32 mg/l Lead,Tot (01051) 0.012 mg/l Manganese,Tot (01055) 0.316 mg/1 Aluminum,Tot (01105) 0.823 mg/1 Calcium,Tot (00916) 13.7 mg/1 Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 9.30 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.055 mg/1 Arsenic,Tot (01002) <0.005 mg/1 TOC <1.0 mg/1 Sulfate (00945) <10.0 mg/1 -------------------- Clients Sample Source MW2 Number COATS AMERICAN. Time Collected Mrs) 0913 P.O, Box 473 • 108 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalabs.com onx ANAL yp to LAbORATORiES, INC. rc f flow Analytical/ rocess Consultations ` Water Tech Lab a. Inc.zoo. o��o Sample Collected ' o�/o�/�y P.O. Box 1056 Date Sample Received 04/11/13 Granite Falls, mc 28630 Date Sample Analyzed . 04/11/13 Attn: doe oragg ' Date of Report 05/01/13 Analyses Performed by ; JC -SK _ Lab Sample Number -----^---'---------- ' 7ss4y7 Parameter Storet # Results . Magneainm,rot (00927) ^o,sno mg/l Lead'Tot (01051) <o'oos mg/l Mazgna000c'rpt (01055) ^o'oos.mg/l Alomioum,zpt (01105) ^n'nas mg/l Calcium,Tot (VOyzs) *n.soo mg/l zhromium,Tot (01034) <o.00s mg/1 ' oadmiom,rot (010e7) ^u.ouz mg/l miokal,Tot <01067> <0.005 mg/1 Godium,Tot (00929) *6.8 mg/l Seleoiom,rot (01147) <n.00s mg/l aazinm'Tot (01007) 0.006 mg/l Aroenlo,Tot (0I002) <u'oos mg/l ' ToC <z.o mg/l Sulfate (00945) 38.4 mg/l ` ------------- Clienta.aamgIo Source Mw10 Number ' COATS JmxERICaN Time Collected (ors) oecs P,c\Box 473^106 Short Street ^Ko,nerovme,North Carolina a7o84^336-goo'e841-Fax o3G'9aa-0oeO ` ttti►�l Ir11UO,?,d RESEARCh & ANA[.YTICA[ ``'���+& +cry, Oi*`� LAbORATWES, INC. NC #34' c+q Analytical/Process Consultations t C► ' ��i�, it► , .......... A ...... Water Tech. Labs. Inc. Date Sample Collected 64/09/13 P.O- Box 1056 Date Sample Received 04/11/13 Granite Falls, NC 28630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report 05/01/13 Analyses Performed by JC -SK Lab Sample Number -------------------- 755498 Parameter Storet # Results Magnesium,Tot (00927) 17.9 mg/1 Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) <0.005 mg/1 Aluminum,Tot (01105) <0.025 mg/1 Calcium,Tot (00916) 36.6 mg/1 Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) <0.005 mg/1 Sodium,Tot (00929) 17.3 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.038 mg/1 Arsenic,Tot (01002) <0.005 mg/1 TOC <1.0 mg/l Sulfate (00945) 51.4 mg/l -------------------- Clients Sample Source MW11 Number COATS AMERICAN Time Collected (Hrs) 0935 P 0. Box 473 • 106 Short Street • Kernersville, North Carolina 272B4 • 336-996-2841 • Fax 336-996-0326 www,randelahs.com 1"r4F RESEARCh & A NALyTiCAL LAbORATWES, INC. .'1� _ # e Analytical/Process Consultations S J �lllrrayU,1�� Water Tech Labs. Inc. Date Sample Collected 04/09/13 P.O. Box 1056 Date Sample Received : 04/11/13 Granite Falls, NC 28630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report 05/01/13 Analyses Performed by : LTC -SK Lab Sample Number --------------------- 755499 Parameter Storet #k Results Magnesium,Tot (00927) 13.6 mg/1 Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 2.85 mg/l Aluminum,Tot (01105) <0.025 mg/1 Calcium,Tot (00916) 72.3 mg/l Chromium,Tot (010#34) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (0167) 0.007 mg/1 Sodium,Tot (00929) 128 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007). 0.101 mg/1 Arsenic,Tot (01002) <0.005 mg/1 TOC 1.96 mg/1 Sulfate (00945) <10.0 mg/l Clients Sample Source Number Time Collected (Hrs) -------------------- MW12 COATS AMERICAN 0948 P.O. Box 473 • 10B Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randelabs.com 14161111 % RESEARchANALyTicAL &.!rT/'rr�r - LABORATORIES, INC. wt1c;�- 0.Nw No #34 x, ' .. Analytical/Process Consultations { S +. 4b `r� f��13 AN',V0 �'►t� Water Tech Labs. Inc. Date Sample Collected 04/09/13 Q.O. Box 1056 Date Sample Received : 04/11/13 Granite Falls, NC 28630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report : 05/01/13 Analyses Performed by JC -SK Lab Sample Number -------------------- 755500 --------------- Parameter Storet # Results Magnesium,Tot (00927) 6.50 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) 0.042 mg/l Aluminum,Tot (01105) 0.032 mg/1 Calcium,Tot (00916) 9.60 mg/l Chromium,Tot (01034) <0.005'mg/1 Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 65.2 mg/l Selen.ium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.025 mg/l Arsenic,Tot (01002) <0.005 mg/1 TOC - 1.45 mg/1 } Sulfate (00945) 43.9 mg/l -------------------- Clients Sample Source MW13 Number COATS AMERICAN Time Collected (Hrs) 1001 P.O. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com �,,�j�111111►►tt RESEARCh & ANA[yTlCA[ �'o .`ZL AN +° �yr, Clio yi L.Ab®RAT®RlES, INC. i( V f� `;4'±4. D . va - to IVC #3� + Analytical/Process Consultations ta►aY��s Water Tech Labs, Inc. Date Sample Collected : 04/09/13 P.O. Sox 1056 Date Sample Received 04/11/13 Granite Falls, NC 28630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report : 05/01/13 Analyses Performed by ; J'C -SK Lab Sample Number -------------------- 755501 Parameter Storet # Results Magnesium,Tot (00927) 40.7 mg/l Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 0.307 mg/l Aluminum,Tot (01105) <0.025 mg/l Calcium,Tot (00916) 64,6 mg/l Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 20.2 mg/l Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0,081 mg/l Arsenic,Tot (01002) <0.005 mg/1 TOC 2.38 mg/l Sulfate (00945) 40.5 mg/l -------------------- Clients Sample Source MW14 Number COATS AMERICAN Time Collected (Hrs) 1008 P.O. Box 473 • 106 Short Street - Kernersville, North Carolina 27284 - 336-996-2e41 - Fax 336-996-0326 www,randalabs.com tttttlrlpb�! RESEARCH & ANALyTICAI LABORATORIES INC. -' 1q0,#34 Analytical/Process Consultations i Water Tech Labs. Inc. Date Sample Collected 04/09/13 P.O. Box 1056 Date Sample Received 04/11/13 Granite Falls, NC 26630 Date Sample Analyzed 04/11/13 Attn: Joe Gragg Date of Report 05/01/13 Analyses Performed by JC -SK Lab Sample Number ---------------- 755502 Parameter Storet # Results Magnesium,Tot (00927) 25.8 mg/1 Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) 1.35 mg/l Aluminum,Tot (01105) <0.025 mg/1 Calcium,Tot (00916) 72.1 mg/1 Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 10.9 mg/1 Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.097 mg/l Arsenic,Tot (01602) <0.005 mg/l TOC 1.50 mg/l Sulfate (00945) 22.6 mg/l -------------------- Clients Sample Source MW15 - Number COATS AMERICAN Time Collected (Hr5) 1018 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randelabs,aom G W-59A COMPLIANCE REPORT FORM Permit (Submit one each monitoring period with 0T 59 forms.) ] Enter date monitoring results were due: - - Will this monitoring report (GW-59 and GW-59A) DES NO be submitted after the established due date? ' I Was any required information missing on the GW-59 report forms? v YES NO IF the answer to question I or 2 is "YES', list in the space provided below the weli identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked oFconcentration(s) ing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office 4 Are any monitored constituents equal to or above the established standards? YES NO if the answer to question 4 is `NO ;skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with conslituent exceeding standards in the space provided below: rnw i� to LA3 2 DS �5�1 Iz mgn�a�iese►3 rn al, I mQr'l these . Z,g 5 rn�I1,l� 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answeL ion 5 is NO, skip to section 8. If the answstion 5 is "YES'; list in the space provided below, each wellwith constituents) exceedingstandards, cion(s) reported, and sample collection date for each occurrence (for the fast two years).iC� e , Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem maybe occurring. CONTACT THE REGIONAL Ale OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO" monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this, groundwater quality problem? YES NO If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surroundin this fac r1ity, Failure to do so maV sub ect the Permittee to a Notice of Violation fines, and/or penalties 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. GW-59A 12/8/2003 C l V oats North America Coats North America �uiie'r';urojuteflctiori To Whom It May Concern: Due to some structural damage to the casing around MW 11, we had to 630 American Thread Road Post OfFice Box 368 FEg12����Marion, North Carolina 28752 Telephone: 828/756-4111 FAX: 828/756-7108 eville l Office abandon this well. We have had a replacement well drilled to replace it. It has been pumped several times by Brett Laverty with the State Office in Swannanoa, but has not been fully developed. We are in hopes that we will have this well developed and ready to sample by our next sampling date which is in April. If you have any questions, feel free to call Sara Hudgins or Phillip Pittman at Coats North America. Our phone number is (828)756-4111 extensions 3291 or 3368. Thank You, Sara Hudgins SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: (' ( S A Cr e it CQr`. Permit Name (if diffe(ent): Facility Address: ©X- r _ Contact Person: ` INI ►lk. Well Location/ Site Name: County Mc f] t., ce I Telephone #: RN -1 No. of Wells to be Sampled: —j— Well Identification Number (from Permit): MW-Z For Groundwater Treatment Systems Well Depth: IS it. Well Diameter: 6 in. Check One: ❑ Influent (98) Screened Interval: ft. to ft. 11 Effluent (99) Depth to Water Level: � � k� ft. below measuring point. Measuring Point (M.P.) is: a 1 3 ft. above land surface. Relative M.P. Elevation in ft.:— Gallons of water pumped/bailed before sampling: inb— Date sample collected: IS-J Field analysis: pH ° , Specific Conductance ' uMhos Temp. QC, Odor Appearance PARAMETERS (Samples for metals were collected unft COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total IZ -Ii mg/I pH (when analyzed) Z- : '090 units TOC I Z--1'A 41 mg/I Chloride I Z-�Uo S.,(,) mg/I Arsenic t Z--Zko 40,005 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1 _I t� mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I FED 12 2013 -- I Z DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WCX Non -Discharge_ NPDES EXPIRATION DATE: S -2011 UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . — colloidal concentrations. HB 04 20;11 Date sample analyzed: 5e ( P jet 0 Laboratory Name: LU to l "iCU,, Certification No. :ered&_YE5 NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P./-243 L,o mg/I Orthophosphate mg/I Al - Aluminum/Z-7-b mg/I Ba - Barium 1Z-Z.i.o C). it 1 mg/I Ca - Calcium 12 & I'-i ; Z mg/I Cd - Cadmium IZ-16 40.00Z. mg/I Chromium: Total 12 -Z.Io L 0,5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/1 Mg - Magnesium It-Zlo c.CP1 mg/I Mn - Manganese_ )'Z--Z(,o ' o' 23 ' mg/I YES NO) Ni - Nickel iZ-ZL O-W l mg/I Pb - Learl 17--Z(o h (-3 3 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ((ll f)deQlt\1Cn 17- -3 1 :5dYl0x ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. ach lab report.) Report Attached? Yesi ) No (0) VOC method # _ .3 method # = method # = GW-59 Rev. 0312000 Asheville Regional Office GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:, Permit Name (it Facility Address Contact Person:r1J114 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I I" LA )L X 0, t t Telephone # 2S - -t No. of Wells to be Sampled: Well Identification Number (from Permit): MI __O-I For Groundwater Treatment Systems Well Depth: I 11R it. Well Diameter: �- in. Check One: ❑ Influent (98) Screened Interval: •�3 '"'J it. to ft. ❑ Effluent (99) Depth to Water Level:16, 9_ft. below measuring point. Measuring Point (M.P.) isZ, 2-1 it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b�iled'before sampling: 3 Date sample collected: Field analysis: pH '�-11 ` Specific Conductance ' uMhos Temp. lk °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:UL '310C Ck5 C'C73 EXPIRATION DATE: I i Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: _ , 5EN E;b" Laboratory Name: i- ('r T h Certification No. En PARAMETERS (Samples for metals were collected unfiltered1% YES NO • and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal 1100ml Nitrate (NO3) as N mg/I Coliform: MF Total. /100m1 Phosphorus: Total as P-] -Z-) b,'Z�k mg/I (Note: Use MPN method for highly turbid samples) 1 Zq Orthophosphate mg/1 Dissolved Solids: Total 1 Z-1 q mg/I Al - Aluminum IZ-Zb O; mg/I pH (when analyzed) )'Z-I'3 I � 1 units Ba - Barium I'Z-ZId b'(n mg/I TOC IZ- 41 mg/I Ca - Calcium - L . ` mg/I Chloride 12-L6 1 1 ' mg/I Cd - Cadmium 12-- Z mg/I Arsenic iZ-Z(o 40, 065 mg/l Chromium: Total 12 -DO' b, On mg/i Grease and Oils mg/I Cu - Copper mg/I Phenol mg/1 Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/l Specific Conductance uMhos K - Potassium mg/1 Total Ammonia mg/I Mg -Magnesium i2 -Z o 4 06* mg/I TKN as N mg/I Mn - Manganese [Z-Zk' 4b. < mg/I Rev. 0312000 YES NO) Ni - Nickel 2-Z , mg/I Pb - Lean )Z-ZL to1,toS mg/,I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ii -,r� ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes__\,/_(1) No (0) VOC : method # = rs2,(Dy A method # method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: i Permit Name (if Fac,`ility ,address: Contact Person:WD1111 Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County If►�411 t�f�It Telephone M No. of Wells to be Sampled: Well Identification NuLnber (from Permit): r0Q 1 L For Groundwater Treatment Systems Well Depth: 1 J It. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval: k: ft. to _ it. ❑ Effluent (99) Depth to Water Level: I + ft. below measuring point. Measuring Point (M.P.) is:? ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b filed before sampling: L_ Date sample collected: If:3 Field analysis: pH 1 Specific Conductance * Umhos Temp. ___L]—°C, Odor Appearance PARAMETERS (Samples for metals were collected un COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total IZ -1 4 (,oqZ mg/I pH (when analyzed) 12-I 3 units TOC 17--IL1 mg/I Chloride 1'Z-� In 4.c;; G mg/I Arsenic 1I2..-Z;to L, d r 00S mgll Grease and Oils mg/I Phenol. rng/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:Lk) QEXPIRATION DAT7`70Non-Discharge UIC NPDES TYPEDF PERMITTED OPERATION BEING MONITO Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: S50e Laboratory Name: _% ate iILP Certification No.i`� tered)S,_YE5 NO and field acidified Nitrite (NO2) as N mg/I Nitrate (Nog) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum M-Z+6 mg/I Ba - Barium mg/I Ca - Calcium V,-- to Ct mg/I Cd -( �Z_0 ,002 mg/I Chromium: Total M-_Z(a' L,0.00S mg/I Cu.- Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium _1' -t(o G mg/I ZiC�S'C Mn - Manganese IZ-be; mg/I YES NO) Ni - Nickel 7_ Z (Y'n -2(o mg/1 Pb - Lear9_ I' c�� (-�c�� rpg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) =1 LZ -,i.i Mo M-P, ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. A tach lab report.) ROC Rep6rt Attached? Yes(1)- No (0) method # _ LVr O ` method # _ method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: ( t l t I J Permit Name (if dif rent): Facility Address: Contact Person: Well Location/ Site Name: "SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I ► )L- X Telephone M No. of Wells to be Sampled: Well Identification Number (from Permit): M t_k. - 1 -S For Groundwater Treatment Systems Well Depth: I _'C" ft. Well Diameter..- in. Check One: ❑ Influent (98) Screened Interval:_ ft. to AA A ft. ❑ Effluent (99) Depth to Water Level: -L ft. below measuring point. Measuring Point (M.P.) fs:Z- tO ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pump'e_d/ba'led before sampling: �_ Date sample collected: Zi ) 2 Field analysis: pH� , Specific Conductance uMhos Temp. 1 QC, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coiiform: MF Total /100ml Pho (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total IZ-14 c;c,)9 mg/I pH (when analyzed) Z-1 o 13 units TOC 12_-1 _ y C> mg/I Chloride Z- 2Z o Z' O mg/I Arsenic 12-ZG� 46'C0- mg/I Grease and Oils mg/I Phenol mg/I . Sulfate mg/I Specific Conductance - uMhos Total Ammonia mg/I TKN as N mg/I Rev. 0312000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: ( ty� bb05(063 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Rerhedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: '�'yP 'Pce- Laboratory Name: _LQOO V of TOCt" Certification No. 8 D _;AYES NO and field acidified to (NO2) as N mg/I ate (NO3) as N mg/1 sphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum J7_-'' ► c1Ci( mg/I Ba - Barium - c) o b4 S mg/I Ca - Cal ciu' rn - I I I S. mg/I Cd - Cadmium I'Z-Zug Z'01OOC-mg/I Chromium: Total _GL?to LO.Cismg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium 'Z' (o mg/I Mn - Manganese � �?.(o n. 00mg/I /� YES NO) Ni - Nickel- (') � (~C`� mg/I Pb - Lead` . -? (P L r')(•_ C s mg/I Zn - Zinc mg/1 Ammonia Nitrogen mgll Other (Specify Compounds and Concentration Units) I 0 � ORGANICS: (GC,GC/MS,HPLG) (Specify -test and method #. Attach lab report.) Report Attached? Yes_�,_/_(1) NO—� ((000) VOC method # method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address Coritact Person: i'l It I t I Well Location/ Site Name: r\. SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I o P- L A r' I Telephone M z J No. of Wells to be Sampled: Well Identification Nu ber (from Permit): Pn W -1'1 For Groundwater Treatment Systems Well Depth. - ft. Well iameter•: z in. Check One: ❑ Influent (98) Screened Interval: A.) -p► ft. to _ ft. El Effluent (99) Depth -to Water Level. 9%", V ft. below measuring point. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: Z t -S Date sample collected: L-73 Field analysis: pH LO -` , Specific Conductance uMhos Temp. °C, Odor. Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: [,C.C�� �in(�j EXPIRATION DATE: Non -Discharge UIC NPDES TY E F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: ' e f OLD j Laboratory Name: P Certification No. _ 15 ) PARAMETERS (Samples for metals were collected unfiltered---'A-YES -NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N rng/I Coliform: MF Total /1 OOmI Phosphorus: Total as P�-2-/ E6,1(6mg/I (Note: Use MPN method for Dissolved '� �' OrthOphOSphate mg/l Solids: To�g,h�lyr,bldsamples) mgll Al - Aluminum 12-2i<� 0,`L" mg/I pH (when analyzed) TOC) C� units 2 Ba - BariumL- ZZI,5 �, I i '�' mg/I -1u1 Chloride 1 Z-Z(O ,"1'Z mg/I �S O mg/I Ca - Calcium )'Z- 2 a Cd - Cadmlum.!'L-Zip 21C_). t:Zmg/I mg/I Arsenic i 2.,-Z t., 4,U 0OS mg/l Chromium: Total j'Z-Z(o' 40, M'S mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate I` -I mg/1 f 6 O mg/I Fe - Iron Hg - Mercury mg/I mg/I. Specific Conductance uMhos K - Potassium g Total Ammonia TKN as N mg/I Mg - Magnesium i Li -2 '`"1� m /1 g mg/I Mn -Manganese (o � mg/I Permittee (or *uthartzed A am d Tit - Please GW-59 c Signature of Permilte (o Rev. 03/2000 r Authorized enl) _YES NO) Ni - Nickel- 0— 4D,C mg/I Pb - Lead_IZ?sI Q LD's mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes __,_( ­I) No (0) VOC method # 6 method #. = method # _ _N_ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Permit Name (if Facility Address: I t r r1 laueeq Jl,� C: t 2 Count ICnY) 5) le (rQ) y Contact Person: ' t i Telephone #:'I (n'q Well Location/ Site Name. t e r No. of Wells to be Sampled: __ (0 (IremPermit) Well Identification Number (from Permit): For Groundwater Treatment Systems Well Depth: ft. Well Di meter: in. Check One: ❑ Influent (98) Screened Interval: ft. to ft. p Effluent (99) Depth to Water Level: _'111i'3 ft. below measuring point. Measuring Point (M.P.) is: t la ft. above land surf) ce. Relative M.P. Elevation in ft.: Gallons of water pumped/bpiled before sampling: Date sample collected: Field analysis: pH_J.P_ -_ , Specific Conductance uMhos . Temp._°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: Lk)(a CYCO&O03 EXPIRATION DATE: Non -Discharge U IC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Laboratory Name: t a pc- Certification No. —Ell) PARAMETERS (Samples for metals were collected unfiltered--A—YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P_I -Z-I < -ft mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 12 L1 4lo-L mg/l Orthophosphate Al - Aluminum -Z(o mg/I mg/I pH (when analyzed) ' t units Ba - Barium K a mg/I TOC mg/I _0 mg%I Ca. - Calcium - Cd - Cadmium - iJ mg/I mg/I Chloride IZ Arsenic j2 - Z coIg/I Chromium: Total I2-2(o' 1).00S mg/I Grease and Oils mg/I Cu - Copper mg/l Phenol ` 1Z-1 mg/I Fe - Iron mg/I Sulfate mg/l Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium Z �r mg/I TKN as N mg/I Mn - Manganese 2- 2 Q ' mg/I Rev. D3/2000 A YES _ . NO) Ni - Nickel-Jz" ,('4S Mg/1 Pb - Lead— fZ-7C� 0 mg/1 Zn -Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. A)tach lab report.) Report Attached? Yes(1) No (0) VOC : method # = method it = method # = GW-59A COMPLIANCE REPORT FORM Permit # -wa"' (pL,�j (Submit one each monitoring period with Gil-59 forms.) 1 Enter date monitoring results were due. p - be submitted after the established due date? Will this monitoring report (GW-59 and GW-59A) YES NO 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 9 or 2'is 'YES", list in the space provided below the weh' identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or'missing cap, missing identification plate; area overgrown, etc.)? If the answer is ••Yes ", contact the Regional Officefor guidance. YES NO 4, Are any monitored constituents equal to or above the established standards? YES O If the answer to question 4 is `NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. mLQ 1Z T 05 (00'Z IM ),Z fy) w? L&- 1 c��3 mr I ivy w IZ MGoc n esC Z;U me m w i3 i fl5 50q me j,Q mt,�� rY1Gn anPsc o-fi33 s lx m 15 (Ylan%nn sz 1 �3 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO ' If the answer to question 5 is `NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). L`iZ, M(18 :nP, - Z�r-13 rr �.J Q �S-�l"l� T1�5 5C3 8M, jj �S Q-1 tti'1W 7 frac�gne ; lrI rn1.1 I2. 1 I DS 51 t) mC&I"o 12 -h -i 1 f�a�oni'sz 3 .i17E�m �,R y '3 - .Z TDS Sir o rn �,Q �1=1� - I I �� nes I . nes n -Ic,- 1 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring' report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. `.�, M w^_'Gi:'.T't...m: .w.'-i3' wM, .vr �Y;ST+.......r )rv.:Jx A+-r^aF.•.an i herefiyacknowle`dgeihat,�the,�bove`.;iriformatlon wasze�aluat�d andhthe In�oc�matiph submltiedTntiilsy'��' report (Complta eport'GW59A) is and complete to the ti®st of my kn wledge K: w ;t.',. -ZJS -)3 Signature of Permitte or Authorized Agent) Date r I1Q ,rjF% GW-59A 12/8/2003 A WRTEROTECH POST OFFICE BOX 1056 • n5 PINEWOOD PLAZA DR GRANITE FALLS. NORTH CAROL INA 28630 (828)396-4444 SAMPLE. Coats America (MW#02) COLLECTION DATE: 12/1.3/2012 PERMIT #. COLLECTION TIME: 07:30 ADDRESS: Coats America (Wells) RECEIVED DATE:. 12/13/2012 P.O. Box 368 RECEIVED TIME. 13:45 Marion, NC 28752 REPORTED: 1 /18/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST �-ZuIfate <10.0 mg/L 12/14/12 \,efiloride 5.0 mg/L 12/26/12 lag T. Phosphorus 0.38 mg/L 1/2/13 jdg toc <1 mg/L 12/14/12 \.XS 118 mg/L 12/14/12 metals see attached PH * >holding time 6.9 su's 12/13/12 lag voc see attached LOG ID: 1212-239 REPORTED BY: NC CERTIFIED LAB # 50 fee'. ( `' t Tony Gragg, Lab Supervisor a A wjqrER&.rEcm __ POST OFFICEE BOY: 1056 • #5 PINEI OOD PLAZZA D.R. GRANITE FALLS, NORTH CAROLINA 28633 (828)396-4444 SAMPLE: Coats America (MW#10) COLLECTION DATE 12/13/2012 PERMIT #: COLLECTION TIME., 07:45 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/13/2012 P.O. Box 368 RECEIVED TIME: 13:45 Marion, NC 28752 REPORTED: 1 /18/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST 'VSulfate 26.5 mg/L 12/14/12 hloride 7.8 mg/L 12/26/12 lag T. Phosphorus 0.24 mg/L 1/2/13 jdg toc <1 mg/L 12/14/12 S 124 mg/L 12/14/12 lag metals see attached pH * >holding time 7.1 su's 12/13/12 lag voc see attached f LOG ID: 1212-240 REPORTED BY: NC CERTIFIED LAB # 50 i .111C. POST OFFICE BOX 1056 • I'S PINEWOOD PLAZA DR GRANITE FALLS. NORTH CAROLINA. 28630 (828)396-4444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 12/13/2012 PERMIT #: COLLECTION TIME. 08:00 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/13/2012 P.O. Box 368 RECEIVED TIME: 13:45 Marion, NC 28752 REPORTED: 1 /18/2013 ANAL YSI S ANALYSIS RESULTS UNITS DATE ANALYST ,,/Sulfate 11.2 mg/L 12/14/12 ,,Chloride <5.0 mg/L 12/26/12 lag T. Phosphorus <0.16 mg/L 112/13 jdg toc 2.62 mg/L 12/14/12 TDS 642 mg/L 12/14/12 lag metals see attached pH ' >holding time 6.7 su's 12/13/12 lag voc see attached LOG 1D: 1212-241 REPORTED BY: NC CERTIFIED LAB # 50 Trmv OraacT T.ah Cnnervicnr i POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANIT; FALLS. NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#13) COLLECTION DATE: 12/13/2012 PERMIT #: COLLECTION TIME: 08:15 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/13/2012 P.O. Box 368 RECEIVED TIME.' 13:45 Marion, NC 28752 REPORTED: 1 /18/2013 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST �,,.,iSulfate 68.1 mg/L 12/14/12 ,,6hloride <5.0 mg/L 12/26/12 lag T. Phosphorus 0.20 mg/L 1/2/13 jdg toc 4.30 mg/L 12/14/12 TDS 509 mg/L 12/14/12 lag metals see attached PH ' >holding time 6.6 su's 12/13/12 lag voc see attached LOG ID: 1212-242 REPORTED BY: NC CERTIFIED LAB # 50 POS T OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS. NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 12/13/2012 PERMIT #: COLLECTION TIME: 08:30 ADDRESS: Coats America (Wells) RECEIVED DATE. 12/13/2012 P.O. Box 368 Marion, NC 28752 RECEIVED TIME: 13:45 REPORTED: 1 M R/1)ni q ANAL YSI S ANALYSIS RESULTS UNITS DATE ANALYST sulfate <10.0 mg/L 12/14/12 VC5hloride <5.0 mg/L 12/26/12 lag T. Phosphorus <0.16 mg/L 1/2/13 jdg toc 2.72 mg/L 12/14/12 J;p6S 497 mg/L 12/14/12 lag metals see attached PH ' >holding time 6.7 su's 12/13/12 lag voc see attached LOG ID: 1212-243 REPORTED BY: NC CERTIFIED LAB # 50 fkt A MR TER I _-cm ffss Inc. . ?OAT OFFICE BOX 1056 • n5 PINEWOOD PLAZA DR. GRANITE FALLS. NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Coats America (MW#15) COLLECTION DATE: 12/13/2012 PERMIT #: COLLECTION TIME: 08:45 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/13/2012 P.O. Box 368 Marion, NC 28752 RECEIVED TIME: 13:45 RFPnRTFn' -- -"'--• / Iv/GV IJ ANALYSIS NALYSIS EF,,Xulfate RESULTS UNITS DATE ANALYST 99.6 mg/L 12/14/12 \Aloride <5.0 mg/L 12/26/12 lag T. Phosphorus <0.16 mg/L 1/2/13 jdg tooc 2.79 mg/L 12/14/12 'V/,I DS 462 mg/L 12/14/12 lag metals see attached PH " >holding time 6.9 su's 12/13/12 lag voc see attached LOG ID: 1212-244 REPORTED BY: NC CERTIFIED LAB # 50 CHAIN OF CUSTODY - Analytical Request Client Name: Q �ML'f (C?�r1.. Address: Report to: Phone: PO Number: Preservatives o Sample Identification U b �' 7 O + x - UD � S q N _ U OCd Z "Q !243-1 L 9 3C) I � :oo 3 $ :30 emperature (°C) j eceived on Ice: Y / N waled Cooler: Y / N amples Intact Y / N Mitional Comments: WATER TECH LABS, INC. PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: Requested Analyses M MWENNNO ME owmamem 0NOM00N ffimOI►11IIDlm Printed Name of Sampler: sm-a Signature of Samplek pH Checked Upon Receipt C12 < 0.2 mg/1 Upon Receipt Field Temp. (C°) I Comments ins 1 Z-1,3-1 RESEARCh & ANAI}rrial LAb4RATORIES, INC. Analyflcd/Process ConsuftWons January 8, 2013 Water Tech Labs P.O. Box 1056 Granite falls, NC 28630 Attention: Joe Gragg . Project Name: Coats American H.Miscellaneous MW2 MW10 MW12 MW13 MW14 MW15 Date Parameters unit Results Resuftff Results Results watts Results Anal=d Aluminum, Total mg/L 3.11 0.044 0.080 0.399 0.267 0.034 12/26/12 Arsenic, Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 12/26/12 Barium, Total mg/L 0.111 0.009 0.112 0.045 0.113 0.133 I2/26/12 Cadmium, Total mg/L <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 12/26/12 Chromium, Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 12/26/12 Calcium, Total mg/L 17.2 <0.500 53.9 11.5 88.0 74.1 12/26/12 Lead, Total mg/L 0.030 <0.005 <0.005 <0.005 0.005 <0.005 12/26/12 Magnesium, Total mg/L 9.09 <0.500 9.44 8.68 56.4 24.6 12/26/12 Manganese, Total mg/L 0.835 <0.005 2.08 0.402 0.760 1.38 12/26/12 Nickel, Total mg/L 0.007 <0.005 0.009 0.008 <0.005 <0.005 12/26/12 Selenium, Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 12/31/12 Sodium, Total mg/L 12.1 39.2 186 207 44.1 563 12/31/12 Sulfate mg/L <10.0 26.5 11.2 68.1 <10.0 99.6 01/07/13 TOC mg/L <1 <l 2.62 4.30 2.72 2.79 12/27/12 Sample Number 747193 747194 747195 747196 747197 747198. Sample Date 12/13/12 12/13/12 12/13/12 12/13/12 12/13/12 12/13/12 Sample Time 0730 0745 0800 0815 0830 0845 ml L = milligrams per Liter = parts per million (ppm) < = Less than or below detection limit ,s RESEARck & ANA(yT16At Ub( mmitks, INC. Arelyticcl/Process C0r=MC dons Chemical Analyslsfor Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs, Inc Proiec4 collected 13 December 2012) I. Volatile Organics Quantitetlon EPA Method 8260 B Umlt Mw2 Mw10 Mw12 Mw13 Parameter fa ►-ba l>2Rhi lot imw LM Mw14 Mwls Aedone Loll 18>IX Aaakm 25 too BQL SOL BQl SOL BQL ROL BOL QL Aayloaflr0a Benzene 10o SOL QL BQL BQL BQL Bmmobernme D's SOLDs SQL BQL QL BQL SQL BQL BQL g4 Bmmacblaamdhatto BnomodkhI mmahme OS 0A SOL QL SOL L BQL SOL SOL Bromo(orm SOL SOL 13�QjL 13QL BQQL SOL BQL BQL eBroxw3dil to 25 BQL DQL BQL BQL SOL SOL SOL BQL BQL CarbonDkUW* 05 BQL BQL SOL SOL BQL BQL BQL BQL BQL BQL CaboaTdraebiwide as BQL BQL BQL SQL BQL SQL SQL l�mlee IA SOL SOL SOL SOL SOL BQL 2-Qkao 2 Cb{omtbyl ether ChIMIAM 5.0 BQL BQLSOL SOL Cblomnmhmm �A 78 BQL SOL SQL SQL BQL SQL BQL BQL 2 Chlorototadta 4•Cldorotalutue OS 05 Q L SQL SQL SQL BQL SQL SQL BQL tit-1,2-DiebloroMpc 0.5 SOL BQL BQL SQL BQL BRQL !Is i3•DieLlpraptppeoe l KD> ) OS 5.0 BQL QQLL BQL RO QL SQL SOL J-DhVMDdlCfa(EDB) 1,2.Dr�romodltaae(EDS) 05 SQL BQL SOL BOLL SOL D3mmoahb modhane D16mmomahrae p SO QL BQL SQL SQL BQL 1.2-DkUotobczeae as BQL SQL BQL SOL SQQL SOL SOL BQL 1.3•Dirblombmrme lA-Dkhlombemme OS BQL BQL SOL SOL ROLSOL SOL BQL t.l-Dichtoroahaaa OS OS SQL BQL SOL SQL BQSOL L QL BQL 12•Dkbloroahaao (Diehbro OS 0.5 SQL BQL BQL SOL SQL SQL SQL BQL SQL SOL omometbanaa I Z Dichlaropmpsne as OS SQL SOL SQL QL SO SQL BQL SQL SQL SQL 1.3•Dkhlaropmpaac W-Dichlompropmte 0.5BQQL OS SOL SOLL QL SOL BQL SQL SQL BQL SQL l.l-Dkhbmpmpme 05 BQL QL SOL BQL SOL SQL SQL SQL amwne S 0 BQL SOL SQL BQL SOL BQL BQL SQL BQL SQL IPE I-PromaccZew 0.5 BQL BQL QL BQ SOL SQL BQL SQL SQL SOL .4•Mahyl-2-Pemmoae 0.5 5.0 BQL BQL SOL QL SOL QL SOL Mettry4lodidt �� LlorRe 1.0 3.0 BQL SQL BQL BQL BQQL MTBE Neplalutlate as 0.5 06L VOL Z6 # Q a . •Suyfbm:me �P3 05 OS QL SOL BQL BQL SOL SQL SQL BQL BQL pyhducae SNYThename OS _SQL BQL SQL BQL SQL BQL BQL Q L SIYfdte as 05 SOL SOL SOL BQQL SOL QL Tat-Bulylhcradte QS BQL BQL BQL SQL SOL SOL 1.1.1.2 Tamehlorodhaoe 1.1.2I-Tdrachlomettme OS OS SOL BQL SQL SQL SQL BQL SQL am BQL Tetrurldorwhene OS BQL SQL SOL Q SQL SQL SQL SOL SQL Tofu= Trons•1.2-Dkldoroetlrae OS BQL BQQL SOL BQL SOL BQL SOL SOL QQL Tr®s-13-Meblampmpene 0,5 SOL BQL BQL BQL SQL Trans l 4 Dkhloro 2-bateae I.23•Trkh%Tobw= 3.0 0.5 BQL BQL SOL � BQL SOL BQL as RQL SOL SQL SOL12.4-TrWorobemeaa SOL BQL SOL SOL 1.1.1-Tridaomahane 1.1.2-Trialdomahaae 0.5 05 SOLgQL SQL SOL SOL SOL 13QL SOLL Tvkhbmahme TrkNomllamoatelhm Os SQL BQL Q SQL SQL BQL SQL SQL QL SQL o ,a-T6chl—Pmp-prop OS 0.5 BQL BQL BQL BQL BQL DQL BQL BQL t.2.4-Tmrtethyllsmme 1.35-Trimethyibmzam as 0.5 BQL SQL SQL gQQL BQL SQL BQL v'tt 1.0 SQL BQL QL QL. BQL BQL SQL BQL SQL SQL SQL chbfAcetae Vhryl Chloride ToW Xyk= 0.5 1.0 BQL SQL BQL BQL SQL SQL BQL BQL BQL BQL BQL - BQL MUM Factor r , I, Sample Number 747193 747194 747195 747196 747197 747198 Sample Date Samplemme(hra) 12/13/12 12/J13112 12J13/12 12113112 12/13/12 12/13/ 12 Analyst Ono, 0745 0800 0815 0930 0840 NM NM NM NM NM NM Date Analyzed 122V12 12/27/12 1227112 12/27/12 32/27/12 1227112 TimeAualynd 2051 2124 2157 241 2304 2334 Surrogate Recovery Rauge DBFM (70-1300/a) 102% 1050/0 104% 102% 103% 103% Toluent3•d8 (70-130%) 97% 990% 95% 99% 101% 119% 4-BFB (70-1309/6) 98% 1030% 99% 99% 102% 101% GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: 1, X[=� Permit Name (if different): EacilitV Address: 'Po Contact Person:111111119, Well Location/ Site Name: SUBMIT FORM -ON -YELLOW PAPER ONLY j Please Print Clearly or Type County - mu _I)C G'� l I Telephone #: 312 -Is6 -4I No. of Wells to be Sampled: Well Identification Number (from Permit): M W - Z. For Groundwater Treatment Systems Well Depth: is ft. Well lameter_10 in. Check One: ❑ Influent (98) Screened Interval: V A ft. to—m A ft_ ❑ Effluent (99) Depth to Water Level: -Sq-Ln ft. below measuring point. Measuring Point (M:P.) ts: Z.3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _(aa Date sample collected: Field analysis: pH '7. o , Specific Conductance ' uMhos . Temp. 1$' °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 ph—.. rot of -Yaa-no- PERMIT #:LJ&0M54003 EXPIRATION DATE: Non -Discharge UIC NPDES I TYPE QE PERMITTED OPERATION BEING MONITORED' Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: t\D ` Rotary Distributor Land Application of Sludge N Other: L NOTE, Values should reflect dissolved andRE IV . colloidal concentrations. �` °ED Date sample analyzed: 5 C- L C3 L=Lo 1 ® C �'J'� Laboratory Name: WNICIE T€ Certification No. So DWQ/BOG Unit PARAMETERS (Samples for metals were collected unfiltered_XYES NO and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I mg/I Coliform: MF Total /100ml .9hosphorus: Total as P.5-?9--1Z 0.14 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Dissolved Solids: Total 9' - \`� -m Ioz mg/l Al - Aluminum l -Zo -I2 H '1b mg/I pH (when analyzed) 9 - ly-1z ,�?&C 'I .cam units Ba - Barium 2 - Zo -1Z 0- 4-01 mg/I Q--L0-17- \•o mg/I (a S Ca - Calcium. 2-Zo -IZ 31• to mg/I *hloride a -U - m Arsenic �3 -to -m I mg/I <0.005 mg/I Cd - Cadmium k -20 - 12 Chromium: Total 9-2047- z o.00z- mg/I mg/I I o- 00-S Grease and Oils mg/I Cu - Copper mg/l.. Phenol �t�Ifate q-2U -12 mg/I 14y Fe - Iron m /I Specific Conductance mg/I uMhos Hg - Mercury K - Potassium mg/I mg /I Total Ammonia mg/I Mg - Magnesium-Zo-12 1'1. 1 me6/1 TKN as N MCA Mn - Manganese 9-20-1? I .'13 / /\ YES NO) Ni- Nickel__-Zo -IZ o.otto mg/I Pb - Lean k -20 - I Z o •0to'7 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/l Other (Specify Compounds and Concentration Units) �sl�nior►-. �-2o-IZ Co OOSrY+s(Q S�Ccl�unn Fs-Zo-l? 10 q r,+at •R ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report. Report Attached? Yes (1) No (0) VOID : method # = mg I method # = method # = - �_ .- a ..., ..- _... .- - •- -- - --- - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ' Facility Name: — Permit Name (if Facility Address: Contact Person:tJliiQJ Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County —III' It` 1�]ot )Q 1l Telephone #: 172 151, -L No. of Wells to be ,Sampled: Well Identification Number (from Permit): M. LO - 10 Screened For Groundwater Treatment Systems Well Depth:. i�_ii. Well Diameter•:�� in. Check One: ❑ Influent (98) Interval: �t' `-- ft. to —tiT_ it. ❑ Effluent (99) Depth to Water Level: ►Z ft. below measuring point. Measuring Point (M.P.) is:-Z-3 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3_ Date sample collected: Field analysis: pH (o • Specific Conductance umhos Temp. �� °C, Odor Appearance -1 2 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 733-37: PERMIT #: W Q d0C3� loth EXPIRATION DATE: 5 - Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED �— Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: S L'L Cut= n 1 RECEIVE) Laboratory Name: t 0 RI C F_ 1 f e t4 n�T it h Certification No. 5o PARAMETERS (Samples for metals were collected unfiltered A YES NO and field acidified COD Mg/jr /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg /I Coliform: MF Fecal Coliform: MF Total /100m1 Phosphorus: Total as P-2-2&-1z 40.1e m/I g mg /I (Note: Use MPN method for highly turbid samples) Orthophosphate m/I Dissolved Solids: Total-1'7-12 I M mg/I Al - Aluminum. -Zo-17- o.18�{ mg/I pH (when analyzed)9-14-tz TOC 5 -7®-12 -113 units �.1•o Ba - Barium T-Zo-12 o.of3 mg/I Chloride G-7-1'-t2- mg/1- < S.0 mg/I Ca - Calcium 8-2o-t2 Cd - Cadmium-i�-Zo -t2 <0.50o mg/I mg/I < o.00z. Arsenic _9 -2o - L2 40.005 mg/I Chromium: Total -26-li 4.o.00s mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate 8-2e-tz mg/I `� mg/I Fe -Iron Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I m /I g Total Ammonia mg/I o Mg - Magnesium Z-IZ <0050o TKN as N mg/I Mn - Manganese E-20-12 '4o•o0S mg/I X YES NO) DWQ/BOG Ni - Nickel _�-2o-1z Co oos mg/I Pb - Lead 4 -Zo -tmg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) e enion., -7a-12 <o.005m .SZ ^� ir�rtr. -20-1Z 446W mall ORGANICS: (GC,GC/MS,HPLC) (Specify -test and method #. Attach lab report ) Report Attached? Yes (1) No :�40) VOC : method # = : method # = : method # '00/ `SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: L�QM 17i11Ni I LUI I Permit Name (if different): Facility Address: tab Ribs. �IDR mar •.b (Street) Z8 C O •IZip County - lit gowe Icay) i � r f" Contact Person: Telephone M Well Location/ Site Name: C No. of Wells to be Sampled: Well Identification Number (from Permit): M, W - 10 For Groundwater Treatment Systems Well Depth: 19 ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: N_ ft. tom_ ft. ❑ Effluent (99) Depth to Water Level: . Z ft. below measuring point. Measuring Point (M.P.) is:'Z9 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _ 3 Date sample collected: ' Field analysis: pH (o • , Specific Conductance ' uMhos Temp. 23 °C, Odor Appearance -12 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W q 000E� 1c03 EXPIRATION DATE: 5' Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —A Lagoon Remedialion• Infiltration Galle Spray Field Rolary Distributor Other: ry Remedialion: _ Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: S L1_ (� =1 n _1 RECEIVE, Laboratory Name: f .J RT £ tZ 1 £C t4 nC T;I_ Certification No. 5o PARAMETERS (Samples for metals were collected unfiltered X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg /I Coliform: MF Fecal /100ml Nitrate (NO3) as N m/I Coliform: MF Total /i 00MI Phnsnhnri ic- Tntnl ne ID Q� -7-►� n .�.�. j* Ir- 9n (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total _9 -1'?-12 1 M mg/I pH (when analyzed)_2-IS-Iz 'I13 units TOC `a -20-12 /,1. 0 mg/1 Chloride S,-2C-t2. < So mg/I Arsenic -4 -zo - Grease and Oils Phenol mg/I mg/I mg/1 Sulfate g-Zo-IZ Zb.'l mg/I Specific Conductance Total Ammonia TKN as N uMhos mg/I mg/I Orthophosphate m /I Al - Aluminum 2-Zo-12- 0.1814 mg/I Ba - Barium B - Zo -12 0.013 mg/I Ca - Calcium.?�20-12 <o.5oO mg/I Cd - Cadmium--2o -t2 c o.00z_ mg/I Chromium: Total -20-12. 4 o ,005 mg/1 Cu - Copper mg/l Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium.? -70 J Z e- 11,500 mg/I �40.00S Mn - Manganese 8-20-12 mall X YES NO) DWQ/BOG Ni - Nickel_ -2o-1Z Ld dos mg/I _i� Pb - Lead-Zo -1 Z Go . oo S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) eflipM Ap.00srn 5b1ic�fY�-20-t-Z ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report ) Report Attached? Yes 0) No (0) VOC method # = method # = method # = A ,�e�Ae-& &)w - �<) 1 0ra—t�ugus�- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: kJ Well Identification Number (from Permit): Ali �1 I A For Groundwater Treatment Systems Well Depth: ) it. Well Diameter: 7- in. Check One: ❑ Influent (98) Screened Interval: it. to it. ❑ Effluent (99) Depth to Water Level: H,9 ft. below measuring point. Measuring Point (M.P.) is:ALI-_ it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ?% Date sample collected: Field analysis: pH (0. S , Specific Conductance Umhos Temp. 2-1 °C, Odor Appearance -12 DEPARTMENT OF ENVIRONMENT & NATURAL RESOU WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER I PERMIT #: W 0000d5w03 EXPIRATION DATE: - Non -Discharge U IC NPDES TYPE F PERMITTED OPERATION BEING MONITOR Lagoon Remedialion: Infiltration Gi Spray Field Rotary Distributor Other: Remedialion: Land Application of Sludge . NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 5de fSelatA) Laboratory Name: wer T _eln Certification No. So PARAMETERS (Samples for metals were collected unfiltered--2_YE5 NO and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N m /I Coliform: MF Total /100m1 mg/I g Phosphorus: Total as P ���'�-lZ �0l'7 m /I (Note: Use MPH method for highly turbid samples) , . Orthophosphate mg/I Dissolved Solids: Total 9-17 -) Z 190 mg/I Al - Aluminum J -ZoA 2 o.1 Og mg/I pH (when analyzed) 12-14m1Z (-.`? units Ba- Barium_ -Zo-IT oblo(c, mg/I TOC'9 -Zo -1 Z. f.95' mg/I 45eo Ca - Calcium _S-2®-1 Z 11.1 mg/I Chloride V-Z1*01& Arsenic _'P- Zo-- Z mg/I 40- 009 mg/I Cd - Cadmium_fi-Z®-I- Chromium: Total'i-Zo-Vt _ 0.007- mg/I <o, cog mg/I Grease and Oils mg/I, Cu - Copper mg/I Phenol Sulfate -2_0 --1Z mg/I, mg/I Fe - Iron Hg -Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 9 -10-I Z S Z3 mg/I TKN as N mg/I Mn - Manganese 9-ZoJV 6.149 mg/I __ -YES NO) Ni- Nickel_ 2-2o-1 z 40.005 mg/I Pb - Leads -Z®- IZ /_o .00S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) _ —ele tor, % -20 -rt 40.66S tM4).k S,drl . 0 rn '6 - Zo - t7_ 11-12.® , p ORGANICS: (GC,GC/Ms,HPLC). (Specify test and method #. Attach lab report.) Report Attached? Yes—(1). No Le"(0) VOC : method # = method # method 4 = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM 'FACILITY INFORMATION ' A Please Print Clearly or Type Facility Name: CDQkS� A V\ r j CaA Permit Name (if different): Facility Address:'20 501, BUS CQC3.t Inn Istreeq JU C_ 74krt SZ lCey) 1e lZZ County ths- pow e l t Contact Person: i li r Telephone #: ?Zd `?*t , Well Location/ Site Name: f C' No. of Wells to be Sampled: _ (Iron Permll) Well Identification Number (from•Permit): rALO- 11 Depth: t For Groundwater Treatment Systems Well De P 3 Jt. Well Diameter: Z in. Check0ne: ❑ Influent 98 Screened Interval: /V IT ft. to ft. P —1]� 11 ti. below measuring point. Effluent 99 Depth 10 Water-Leve{: � • ( ) Measuring Point (M.P.) is: .lo "iL:above land surface. Relative M.P. Elevation in ft:: Gallons of water pumped/bailed before sampling: 3W Date sample collected: 9 l 1-IZ Field analysis: pH Lo r , Specific Conductance ' uMhos Temp. 21 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WQpt :j 1p03 EXPIRATION DATE: 5 Non -Discharge UIC NPDES TYPE F P RMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Other: Land Application of Sludge NOTE: Values should reflect dissolved and . colloidal concentrations. (� Date sample analyzed: - - eww RECEIVED Laboratory Name:.LA-)A-TLle -rr-C (lf� ( 7n12 Certification No. So PARAMETERS (Samples for metals were collected unfiftered_:�__YES NO COD and field acidified mg/I /100ml _ Nitrite (NO2) as N Nitrate (NO3) as N mg/I Coliform: MF Fecal Coliform: MF Total /100ml m /I Phosphorus: Total as P -28-12 O.1'7 mgg/I (Note: Use MPH method for highly turbid Dissolved Solids: Total _$'-17-12 samples) t%b mg/I Orthophosphate AI - Aluminum 8 -Zo-12 mg/I pH (when analyzed) $-J%A 11L k..q units Ba - Barium V-2t]-1? mg/I mg/1 TOC -20-12 7-1 mg/I <S;o mg/I Ca - Calcium_ 2-?o-12 Cd -Cadmium S =20-17• <o.Sop mg/I Z-o -00z. Chloride . 4i •2:1- Iz Arsenic Ss •Zo-tz 40.005 mg/I Chromium: Total V-Zo-12 mg/I 4 o.coS mg/I Grease and Oils mg/I 'Cu - Copper m g /I Phenol Sulfate -20-1Z. mg/I mg/I Fe -Iron Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I g/I Total Ammonia TKN as N mg/I Mg - Magnesium 9-2o-1Z mg/I mg/I Mn - Manganese -20-12 999r�g/l X YES NO) D — Ni - Nickel 8 -•ZC) -12 G o Co mg/I Pb - Lean S -?o -12 <o. C�S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) U�i1it� �•�:� Sele.iliun'i 8-7A-1-4 Lb�OoSrr I,Q ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report ) Report Attached? Yes (1) No (0) VOC method # = method # = method # SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name S AlMeCiMft Permit Name (if different): Facility Address:eTd (Street) We Well ll ( �iY);vl . County.— Contact Person: ) t+nan Telephone #: $2� ''1S(o -q 1k X Well Location/ Site Name: SP ;e C U t1 No. of Wells to be Sampled: _ - (Irom ermll) Well Identification Number (from Permit):._ M U-) - 11, For Groundwater Treatment Systems Well Depth: 13 ­ft. Well Diameter �_ in. -Check One: ❑ Influent .(98) Screened Interval: �I— ft. to —_ it, Depth to Water Level: 10 It. below measuring point. ❑ Effluent (99) Measuring Point (M.P.) is: Z , 6 it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: —�— Date sample collected: - tA-1Z- Field analysis: pH rl, Z , Specific Conductance uMhos Temp. Z1 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:WG. MC%;o03 Non -Discharge EXPIRATION DATE: S -ZO 1l UIC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. RECEIVED Date sample analyzed: 5 Er Laboratory Name: _W BTC CZ T£ 4t ACT ),; o Certification No. _ 50 PARAMETERS (Samples for metals were collected unfiltered A YES NO and field acidified COD mg/I /100ml Nitrite (NO2) as N _ Nitrate (NO3) as N m /I Coliform: MF Fecal Coliform: MF Total /100m1 mg/I. g •Phosphorus: Total as P_�-Zq-1Z D•m9 /I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: ;T'otal!j l2 nFr) mg/I Al - Aluminum -20-12. 0. 10k mg/I pH (when analyzed) S_-1q-I2 1 - TOC %- Z O -17- '1,39 l units Ba - Barium 9-Zo - Iz 0.139 mg/I -- mg/I Chloride � �Z1 -1'L 5:d mg/I "w-Zo Ca : Calcium S- Zo -Iz Cd - Cadmium_ 'Ps -Zo-12 54 . I mg/I 4-a.007-mg/I Arsenic -1Z. 40,005 mg/I Chromium: Total �r -ZO=►2 40 •ooSmg/I Grease and Oils mg/I Cu - Copper. mg/I Phenol Sulfate—-Zo-IZ Z2r mg/I mg/I Fe - Iron Hg - Mercury /I mg/l Specific Conductance uMhos K - Potassium mg mg/I Total Ammonia mg/I Mg - Magnesium Q -Zo -12 11 S mg/I TKN as N mg/I %Mn - Manganese -ZO =tZ z, Scl mg/I .�uvn rr nit X YES NO) Ni - Nickel �-Za -12 L g/ Pb-Lead _ W-20-1 a tbmg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Pleniem '20-1 L.D.I�U�/� -o- D9ma 0 ORGANICS: (GC,GC/MS,HPLC) (Specify test arid method #. Attach lab report.) Report Attached? Yes (1) No � (0) VOC : method # - mall -my method#= Certify that, to the best of my knowledge and belief_ ihp infnrmafiAn i✓ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (it d Facility Address:_ Contact Person: Well Location/ Site Na e. SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I f t'�11— 7elephone #: LS -75fo No. of Wells to be Sampled: Well Identification Number (from Permit): (Y) U) -13 For Groundwater Treatment Systems Well Depth: 15 it. Well Diameter: 2 in. Check One: ❑ influent (98) Screened Interval: . ft_ to �_ ft. El Effluent (99) Depth to Water Level: 12•"l ft. below measuring point. Measuring Point (M.P.) is: Z- to ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3%y Date sample collected: 9 - W- jZ Field analysis: pH b "1 Specific Conductance uMhos Temp. Z-*Z °C, Odor Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: LA-_> QCKD0,S(o63 Non -Discharge NPDES EXPIRATION DATE: -2011 UIC TYPE OF PERMITTED OPERATION BEING MONITORED —�� Lagoon Aemedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and .RECEI'VED colloidal concentrations. Date sample analyzed: _ 5 C r- oW QC I (. o Z 0 ;Z Laboratory Name: w NT£ t2 Te, vM information Proce sins t fnit Certification No. Sb DWQ/BOG PARAMETERS (Samples for metals were collected unfiltered__,)(_�YES NO and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as .N Nitrate (NO3) as N m /I Coliform: MF Totaf /100m1 mgg/I g Phosphorus: Total as P �-ZFr-)Z <o.�tq-n /I (Note: Use MPN method for hlghl turbid Samples) P Dissolved Solids: '- Orthophosphate mg/I Total - Z 31 mg/I. pH (when analyzed)_�'r-14-12 7-0 units Al - Aluminum i-n-l? Ba - Barium 9-7O-IZ D. 1tcA mg/I TOC 19-20 -1`- 1 q "1 mg/I Ca - Calcibm_ h' -1Z. 0. u4y mg/I )to .6 mg/I Chloride _2 -Z1- IZ 4 S.O mg/I Cd - Cadmium 16 - 7 0 -IZ < b -OOZ mg/I Arsenic 2 -Zo -17- a.00s mg/I Chromium: Total l Z0-12 4.0,o05 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate Ss =Zo -12 2 mg/I g He - IMercu ron g �' mg/I Specific Conductance uMhos K - Potassium mg/I mg/I Total Ammonia mg/I Mg - Magnesium B-ZO-IZ- 10.71 mg/I TKN as N mg/I Mn - Manganese _'-Zo-17 U-415.E mg/I (or Author( Agent) Name and __X__YES NO) Ni - Nickel_F-Z0-1Z /10.00 mg/l Pb -LearL mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes (1) No �i (0) VOC method # = method # _ method # = print or type GW-59 Rev. 03/2000 lee EWAWo V GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: l�(X Permit Name (if di e Facility Address: Contact Person .A � Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County 1tt` L �11)J)� I 1 Telephone #: ��IQ -` No. of Wells to be Sampled: Well Identification Number (from Permit): _m t_AJ- 1Li For Groundwater Treatment Systems Well Depth: 5 it. Well lameter Z in. Check One: ❑ Influent (98) Screened Interval: ft. to it- El Effluent (99) Depth to Water Level: 1 it. below measuring point. Measuring Point (M.P.) is: Z• b ft. above land surface. Relative M.P. Elevation in ft.- Gallons of water pumped/bailed before sampling: .Z Date sample collected: Field analysis: pH__Us'3_ Specific Conductance uMhos . Temp. U °C, Odor Appearance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid sample``s� Dissolved Solids: Total 2-11-12 �1L12 mg/I pW(when analyzed) V-1a-VZ -q units TOC %-2o-1 3.Z5 mg/I Chloride 2-7-1-1'Z 4$. > mg/I Arsenic $ - Zo -1-1 oo S mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1i -Zo -12 11. mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I - - method # method # �= a .. , -..- _.. . .. . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WCCJOc5cQp3 EXPIRATION DATE: Zbl Non -Discharge U IC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. %CVJ Date sample analyzed: �[r �F_lft� Laboratory Name: �)C0 r 'T _ (` � ACT 1 6 2012. Certification No. _ 5c) Information Processing Unit red /� YES NO and field acidified Nitrite (NO2) as N m /I Nitrate (NO3) as N mg/I Phosphorus: Total as P� -2� - I Z e-o.)(,m9/I Orthophosphate mg/I 9 Al - Aluminum''-Zo-12 o.(.,sko mg/I Ba - Barium -20 - l2 0. 1 8 mg/I Ca - Calcium _ S 'Zo -1Z q1.2 g Cd - Cadmium -Zo -17 <a.00Z mg/I Chromium: Total 9 -Zo -l2 40, OoS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I k - Potassium mg/I Mg - Magnesium S-70-IZ S3.8 mg/I Mn - Manganese_V-20 Al o• 4o� mg/I _YES NO) Ni - Nickel 9 - ZD -M L O.00 S mg/I Pb - Lear: -Zo -1 O ppq mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SelQnion,-20-1'L Lo 005 I.SZ 4 i von - - IZ QtA Z �'+19t1 J- ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No _X (0) VOC : method # = i,�n.�co ��� t+uuiunze gents Name and. Title -Please print or type GW-59 -Z'-) - Rev. 03/2000 Stgnalure of Permillee or prized Agent) V GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:' k: ,1. Permit Name (if d jjere Facilitv Address O Contact Person:Yt1J11ll_ Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County t l Ke llrit g e l 1. Telephone #:.R?S- 790 -u No. of Wells to be Sampled: Well Identification Number (from Permit): M -1 For Groundwater Treatment Systems Well Depth: 10 it. Well D'ameter•: Z "1- Check One: ❑ Influent (98) 0 Screened Interval. _ ft. to A_ ft. Depth to Water Level-.. 12- 1 it. below measuring point' El Effluent (99) Measuring Point (M.P.) is: Z.le ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b iled before sampling: _,� Date sample collected: IR _)L4 -I IL Field analysis: pH�9 , Specific Conductance ' uMhos . Temp. Z0 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGHNC 27699-1636 Phone: (919) 733-32: PERMIT #: Flo Q 000 Non -Discharge NPDES EXPIRATION DATE: UIC TYPE PF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . ®� colloidal concentrations. Date sample analyzed: �j[L t�Dtti) OCT f � LaboratoryName: _W ft t Qe T£ to 'in Certification No. SO recessing Unit DWQ/BOG PARAMETERS (Samples for metals were collected unfiltered A YES NO and field acidified COD Coliform: MF Fecal mg/I /100m1 Nitrite (NO2) as N Nitrate (NO3) as N mg/I Coliform.: MF Total /100ml Phosphorus: Total as PI-ZSr-IZ 4-,W mg/I mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Totals-0-12 -,,A? mg/I Al -Aluminum. 2-ZO-12 0 OV9 mg/1 pH (when analyzed) 1,�-ltA -1Z Vs '°l Z units Ba - Barium -9 -20 - Z 0 . 11 R mg/I TOC -Z® 1-L 3 11 mg/I mg/1 Ca - Calcium -Za-1Z Cd-Cadmium S-Zo-1Z 126.0 mg/I mg/I Chloride 4o.007- Arsenic 9-Zo-ft 40.Op5 mg/I Chromium: Total S-2a-12 4o.c�b5 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate-io-1Z mg/l 113 mg/I Fe -Iron Hg - Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium ' zo-1Z. - Z.4i mg/I TKN as N m ga Uang., n. YES NO) Ni - Nickel '�-Zo-1Z 46.00S mg/I Pb - LeadB-Zo-tZ o,nos mg/I Zn -'Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Ix1iu� -20-12 Z0�T,Q. ORGANICS: (GC,GC/MS,HPLC). (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No X_ (0) VOC : method # = method 1 certify that, to the best of my knowledge nnri hatie f oin infnnimnfin.. tit, :_ .L GW-59 Rev. 0312000 re of Nerfnillee (or or type �• vv---)yFi UU10' PLIANCE REPORT FORM Permit (Suhmit one each monitoring period with GFV forms.) I 1 Enter date monitoring results were due. - Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? YES NO 2 Was any required information missing on the GW-59 report forms? ` IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the YES NO. required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "?es ", YES NO contact the Regional Office for giiidance. 4 Are any monitored constituents equal to or above the established standards? If the answer to question 4 is "NO", skip to section 8. - YES NO If the.answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MLC41 L.*ctd 0-0l99 �.Q rn w e-- Z. _ ► 05 150 nncalJL (AGAta4esc d . 93,�k AlargQne6,e z,sq nQj� 5 For the constituents identified in quescri same constituent(s) in the same well(s) in the last two years? tion 4 above, have standards been exceeded previouslJ�ng YES NO If the answer to question 5 is `NO'; skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(sstandards, concentration(s) reported, and sample collection date for each occurrence (for the last tw rY1 t•v Z' fYi4rnPs 1,1� �+�3L i2 -lam -11 -� 1'L (ylgc�gnes e Z,`;;3'&nP5 _ C Mein �'onese- 1- tot rA814 `i -3-17- 7DS ;5 56—�JQ. � -9 - �� - l iI t_raa 6.05G M2,IJL 4 -3> 1'� i PS Sao m�Z 3,�6 DS �� ®�, �t-tql Are the monitoring wells listed inlocated at or beyond the review boundary?YE 0if the answeris "YES', a groundwater quality problem maybe occurring. CONTACT THE REGOFFICE IMMEDIATELY FOR GUIDANCE. If the "NO', answer is monitoring wells maybe improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be re wired to determine the im act the was osal s stem ► s havtn co boundaries at the review and m liance surroundingthis facili Fai ma sub'ect the permittee to a Notice of Violation fines, and/or penalties It7fpr tloQ O1VQ/eOGsig9 Ij g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 here6yacknowledge that;thR, ove Information was eValuatc d and the Information submltted�nthis report (Compliance Report GW 59A} is true and complete to the best of my knowledgeA _..., �P,,-e ignature of (or Authorized Agent) Date GW-59A 12/8/2003 rm tl lire LITYS,Inc. POST OFFICE BOX 1056 4 #15 PINEWOOD PLAZA DR, GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#02) COLLECTION DATE: 8/14/2012 PERMIT #: COLLECTION TIME: 09:05 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NO 28752 REPORTED: 9/21 /2012 .ANALYST ANALYSIS RESULT'S UNITS dATE ANALYST Sulfate 144 mg/L 8/20/12 Chloride 6.5 mg/L 8/21/12 lag T. Phosphorus 0.46 mg1L 8/28/12 jdg too <1.0 mg/L 8/20/12 TDS 102 mg/1- 8/17/12 lag metals see attached pH ` >holding time 7.0 su's 8/14112 lag LOG ID: 1208-202 REPORTED BY: NC CERTIFIED LAB # 5 Tony Gragg, Lab Supervisor . rivi POST OFFICE BOX 1056 • #5 PINEWOOO PLAZA DR. GRANITE FALLS, NORTH CAROLlNA 28630 (828) 396-4444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 8/14/2012 PERMIT #: COLLECTION TIME. 09:15 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: 9/21 /2012 AN, ANALYSIS RESULTS {WITS DATE ANALYST Sulfate 26.7 mg/L 8/20/12 Chloride <5.0 mg/L 8121/12 lag T. Phosphorus <0.16 mg/L 8/28/12 Jdg toc <1.0 mg/L 8/20/12. TDS 108 mg/L 8/17/12 lag metals see attached PH ' >holding time 7.3 su's 8114/12 lag LOG ID: 1208-203, REPORTED BY: NC,CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor WrtivnrcH LRES,ll,.. A POST OFFICE 8OX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#11) COLLECTION DATE: 8/14/2012 PERMIT #: COLLECTION TIME: 09:20 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P,O. Box 368 RECEIVED TIME: 14:50 Marion, NC `28752 REPORTED: 9/2112012 ANALYSIS ,4NA ysi$ RESULTS L/NITS DAATE ANALYST Sulfate 40.2 mg/L 8/20/12 Chloride <5.0 mg/L 8/21/12 lag T. Phosphorus 0.17 mg/L 8/28/12 jdg toc 2.78 mg/L 8120112 TDS 180 mg/L 8/17/12 lag metals see attached pH ">holding time 6.7 su's 8114/12 lag i LOG ID:, 1208-204 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor idivrERiTECH ITIF.S.Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#12) COLLECTION DATE: 8/14/2012 PERMIT #: COLLECTION TIME., 09:25 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P.O, Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: 9/21 /2012 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Sulfate 22.8 mg/L 8/20/12 Chloride <5.0 mg/L 8/21/12 lag T. Phosphorus 0.24 mg/L 8/28112 jdg toc 3.39 mg/L 8/20112 TDS 750 mg/L 8/17/12 lag metals see attached pH ` >holding time 7.1 su's 8/14/12 lag LOG ID: 1208-205 REPORTED BY: NC CERTIFIED LAB #f 50 fl�6" Tony Gragg, Lab Supervisor pwrEnirEcH Livas,c. a POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28830 (828) 396-4444 SAMPLE., Coats America (MW#13) COLLECTION DATE: 8/1412012 PERMIT #: COLLECTION TIME: 09:30 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: 9/21 /2012 ANAL.YSI S ANALYSIS RESULTS UNITS DATE ANALYST Sulfate 24.4 mg/L 8/20/12 Chlorlde <5.0 mg/L 8/21112 lag T. Phosphorus <0.16 mg/L 8/28112 jdg toc 1.97 mg/L 8/20/12 TDS 331 mg/L 8/17112 lag metals see attached pH >holding time 7.0 su's 8/14/12 lag LOG ID: 1208-206 REPORTED BY: NBC` CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor rriv4 mcH LRES.Inc, POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE., 8/14l2012 PERMIT #: COLLECTION TIME: 09:35 ADDRESS: Coats America (Wells) RECEIVED DATE: 8/14/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: 9/21 /2012 ANAL YSIS ANALYSIS. RESULTS UNITS DATE ANALYST Sulfate 11.5 mg/L 8/20/12 Chloride <5.0 mg/L 8121112 lag T. Phosphorus <0.16 mg/L 8/28/12 Idg too 3.25 mg/L 8/20112 TDS 442 mg/L 8/17/12 lag metals see attached pH >holding time 6.9 su's 8/14/12 lag E LOG ID: 1208-207 REPORTED BY: N�Ce CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor idivrEpwirEcHLES. In c. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 26630 (828) 396-4444 SAMPLE: Coats America (MW#15) COLLECTION DATE: 8/14/2012 PERMIT #: COLLECTION TIME: 09:40 ADDRESS: Coats America (Wells) RECEIVED DATE, 8/14/2012 P.O. Box 368 RECEIVED TIME; 14:50 Marion, NC 28752 REPORTED. 9/21 /2012 ANALYSIS. . ANALYSIS RESULTS UNITS DATE ANALYST Sulfate 113 mg1L 8/20112 Chloride <5.0 mg/L 8121/12 lag T. Phosphorus 0.78 mg/L 8/28/12 jdg too 3.1.1 mg/L 8/20112 TDS 398 mg/L 8/17/12 metals see attached pH">holdingtime 7.2 su's 8/14112 lag LOG ID: 1208-208 REPORTED BY: NC, CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor Ys: �0` G��& Ah1ACYTj �P i� RESEARCh & ANAiyTICA1 ��. .... ,..• • LAbORATWES INC. NC #34 Analytical/Process Consultations Water Tech Labs, Inc. Date Sample Collected 08/14/12 P,O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 28630 Date Sample Analyzed 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by AD -JC -KL Lab Sample Number 738428 Parameter Storet ## Results TOC, (00680) <1.0 mg/l Magnesium,Tot (00927) 17.1 mg/l Lead,Tot (01051) 0.067 mg/l Manganese,Tot (01055) 1.73 mg/l Aluminum,Tot (01105) 4.76 mg/1 Calcium,Tot (00916) 32.6 mg/l Chromium,Tot (01034) 0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) 0.016 mg/l Sodi.um, Tot (00929) 1.0.9 mg/1. Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0,201 mg/1 Arsenic, Tot •(01002) <0.005 mg/l Sulfate (00945) 144 mg/l -------------------- Clients Sample Source COATS AMERICAN Number MONITORING WELLS MW2 Time Collected (Hrs) 0905 P.O. Box 473 • 106 Short Street - Karnersville, North Carolina 272B4 •336-996-2841 ^ Fax 336-996.0326 www,randalabs.com 4®,etvISRIIil1'r , RESEARCh & ANA1yTICAL LABORATORIES, INC No #34 Analytical/Process Consultations ; t +�ll�f7ff1�j1� Water Tech Labs. Inc. Date Sample Collected : 08/14/12 P.O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 28630 Date Sample Analyzed 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by JC -AP -KL .Lab Sample Number --------------------- 738429 Parameter Storet # Results TOC (00680) <1.0 mg/1 Magnesium,Tot (00927) <0.500 mg/1 Lead, Tot (01051) <0.005 mg/l Mariganese,Tot (01055) <0.005 mg/l Aluminum,Tot (01105) 0.184 mg/l Calcium,Tot (00916) <0.500 mg/1 Chromium,Tot (01034) <0,005 mg/l Cadmium,Tot (01027), <0.002 mg/1 Nickel,Tot (01067) <0.005 mg/1 Sodium,`Zot (00929) 44,8 mg/1 1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.013 mg/l Arsenic,Tot (01002) <0.005 mg/1 Sulfate (00945) 26.7 mg/l -------------------- Clients Sample Source COATS AMERICAN Number MONITORING WELLS MW1(Z' Time Collected (Hrs) 0915 P, 0, Box 473 ^ 106 Short Street • Kernersville, North Carolina 27284 ^ 336.996-2841 • Fax 336-996-0326 www.randalabs.com - RESEARCh & ANA1YT9CAL LAbOIRATWES, INC. Analytical/Process Consultations U) NC#34 Q 4v r,G � • rqEC'tdQ' �� �• 'PIED AN�'��� 14111Idf111o1�4 Water Tech Labs. Inc. Date Sample Collected 08/14/12 P.O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 28630 Date Sample Analyzed 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by AP -JC -KL Lab Sample Number ------------------- 738430 Parameter Storet # Results TOC (00680) 2.78 mg/l Magnesium,Tot (00927) 5.28 mg/1 Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 0.748 mg/l Aluminum,Tot (01105) 0.108 mg/l Calcium,Tot (00916) 17.7 mg/l Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 42.0 mg/1 Selenium,Tot (01147) <0.005 mg/1 Barium,Tot (01007) 0.106 mg/l Arsenic,Tot (01002) <0.005 mg/1 Sulfate (00945) 40.2 mg/1 -------------------- Clients Sample Source COATS AMERICAN Number MONITORING WELLS MW1k Time Collected (Hrs) 0920 _ P.O. Box 473 > 106 Short Straot • Kernersvilla, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www,randalabs.com RESEARCh ANA1yTICAi LAbORATORlES, INC. NC1f.T1' IjOyA � r Analytical/Process Consultations Od` Water Tech Labs, Inc. Date Sample Collected 08/14/12 P.O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 26630 Date Sample Analyzed 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by : AD -KL -JC, Lab Sample Number -------------------- 738431 Parameter Storet # Results TOC (00680) 3.39.mg/l 1 Sulfate (00945) 22.8 mg/l Magnesium,Tot (00927) 11.5 mg/l Lead,Tot (01051) <0.005 mg/l Manganese,Tot (01055) 2.59 mg/1 Aluminum,Tot (01105) 0.106 mg/l Calcium,Tot (00916) 59.1 mg/1 Chromium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) 0.010 mg/l Sodium,Tot (00929) 209 mg/1 Selenium,Tot (01147) <0.005 mg/l Barium, -Tot (01007) 0.139 mg/1 Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICAN Number MONITORING WELLS MW1',\ Time Collected (Hrs) 0925 P.O. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 •336-996-2841 - Fax 336-996-0326 www.randalebs.com 4 `,,1�`�Tlrirlpjttt • 11,E �``� r��,,jt� RESEARCh & ANALyTICA1 �,• • ,,. ;...H,.. ,,. LAb®RATWES INC. Analytical/Process Consultations 4 Water Tech Labs. Inc. Date Sample Collected 08/14/12 P.O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 28630 Date,Sample Analyzed : 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by AD -KL -JC Lab Sample Number ----------------- 738432 Parameter Storet # Results TOC (00680) Sulfate (00945) Magnesium,Tot' (00927) Lead,Tot (01051) Manganese,Tot (010.55) Aluminum,Tot (01105) Calcium,Tot (00916) Chromium,Tot (01034) Cadmium,Tot (0102.7) Nickel,Tot (01067) Sodium,Tot (00929) Selenium,Tot (01147) Barium,Tot (01007) Arsenic,Tot (01002) Clients Sample Source Number Time Collected (Hrs)' 1.97 mg/l i 24.4 mg/l 10.7 mg/1 <0.005 mg/l 0.403 mg/1 0,169 mg/l 16.0 mg/l <0.005 mg/1" <0.002 mg/1 <0.005 mg/l 108 mg/1 �0.005 mg/1 0.044 mg/1 <0.005 mg/l -------------------- COATS AMERICAN MONITORING WELLS MW13 0930 r P.O. Box 473 - 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996.0326 www.randalabs.com �'®�0147lii9,r'e RESEARCh&ANA��/T�CA� ........ LABORATORIES, INC. #34 - Analytical/Process Consultations Water Tech Labs, Inc. Date Sample Collected 08/14/12 P.O. Box 1056 Date Sample Received 06/20/12 Granite Falls, NC 28630 Date Sample Analyzed 08/20/12 Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by ; AD -KL -JC Lab Sample Number -------------------- 738433 - ----------------------------------------------------------------------------- Parameter Storet # Results TOC (00680) 3.25 mg/l Sulfate (00945) 11.5 mg/l Magnesium,Tot (00927) 53.8 mg/l Lead,Tot (01051) 0.009 mg/l Manganese,Tot (01055) 0.906 mg/l Aluminum,Tot (01105) 0:656 mg/1 Calcium,Tot (00916) 87.2 mg/l Chromium,Tot (01034) <0.005 mg/1 Cadmium,Tot (01027) <0.002 mg/l Nickel,Tot (01067) <0.005 mg/l Sodium,Tot (00929) 44.2 mg/l Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.120 mg/1 Arsenic,Tot (01002) <0.005 mg/l -------------------- Clients Sample Source COATS AMERICAN Number MONITORING WELLS MWly Time Collected (Hrs) 0935 P.O, Box 473 . 106 Short Street, Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-995-0326 www.randslabs,com RESEARCh & ANALyT9CAL LAbORATORiES,.INC. Analytical/Process Consultations ,,`���►►tll►d�trr, � ANAL p +r +Sr NC #34 x: N � g � v Water Tech Labs. Inc. Date Sample Collected : 08/14,/12 P.O. Box 1056 Date Sample Received 08/20/12 Granite Falls, NC 28630 Date Sample Analyzed ; 08/20/12. Attn: Joe Gragg Date of Report 08/30/12 Analyses Performed by : AD -KL -JC Lab Sample Number ----------------- 738434 Parameter Storet # Results TOC (00680) 3.11 mg/l Sulfate (00945) 113 mg/l Magnesium,Tot (00927.) 32.8 mg/l Lead,Tot (01051) <0.005 mg/1 Manganese,Tot (01055) 0.849 mg/l Aluminum,Tot (01105) 0.029 mg/1 Calcium,Tot (00916) 86.0 mg/1 Chrcmium,Tot (01034) <0.005 mg/l Cadmium,Tot (01027) <0.002 mg/1 Nickel,Tot (01067) <0.005 mg./l Sodium,Tot (00929) 37.9 mg/1 Selenium,Tot (01147) <0.005 mg/l Barium,Tot (01007) 0.118 mg/l Arsenic,Tot (01002) <0.005 mg/1 -------------------- Clients Sample Source COATS AMERICAN Number. MONITORING WELLS MW1 5- Time Collected (Hrs) 0940 P.O. Box 473 • 106 Short Street • Kernersville, North Caroline 27284. 336-996-2841 • Fax 336-996-0326 www.randelabs.com CHAIN OF CUSTODY - Analytical Request Client Name: %n �n J�%/!�✓ Address: C u Report to: Phone: PO Number: WATER TECH LABS, INC. PO BOX 1056 - GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number: Reauested Analvses pH Checked Upon Receipt Preservatives Cl2 < 0.2 mg/I Upon Receipt U Sample Identification Q N o O J Q' �' N U `� "` rn F x Field Temp. (C") Comments w t,. Ltd I Stan Temperature (`C) Received on lee: Y / N i (7 Sealed Cooler Y / N Samples Intact Y / N Additional Comments. Sampler _ and _ Date Printed of Samp1er. JtR b gnature WLJg,,CV d - .V M CHAIN OF CUSTODY - Analytical Request Client Name: Cffk (Yl f i(I yL Address: Report to: Phone: PO Number: Preservatives Sample Identification U OR 0 z z x �q + o ¢, , �., N � U m z cc5 z Mm 41 • • • • • • • • 'D • • )1� ' Temperature (°G) a� Received on Ice: y / Sealed Cooler. y / N Samples Intact Y / N Additional Comments: WATER TECH LABS, INC_ PO BOX 1056 GRANITE FALLS, NC 28630 PHONE: (828) 396-4444 Project Name: Project Number GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if d) Facility Address:_ Contact Person: V111 III Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type Z County —Mc 010LL)C--LL P'!57elephone #: _ _?U- 7% - 4 )1) No. of Wells to be Sampied: „__1_ Well Identification Number (from Permit): M le) - Z For Groundwater Treatment Systems Well Depth: �5 it. Well lameter:.�_ in. Check One: ❑ Influent (98) Screened Interval: /ifT it. to ft. El Effluent (99) Depth to Water Level: 7+ ft. below measuring point. Measuring Point (M.P.) is: a,3 ft. above land surface. Relative M.P. Elevation inft,: Gallons of water pumped/bailed before sampling: _Up Date sample collected: Field analysis: pH I , Specific Conductance uMhos . Temp. -AQ 'C, Odor Appearance Z DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WQWIJb(003 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ✓ Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of SI Other: dge _- ,a NOTE: Values should reflect dissolved and . D colloidal concentrations. C: CD _ Date sample analyzed: C- 13 G I-6 W M Laboratory Name: W AT 171- 1Z 7-C- Certification No. c� E2 PARAMETERS (Samples for metals were collected unfiltered,_ —YES NO and field acidified COD mg/1 Nitrite (NO2) as N mg /1 Coliform: MF Fecal /100ml Nitrate (NO3) as N m/I Coliform: MF Total /100ml Phnsnhnri ic• Tntal 9e 0 U-zfi_'1 A.L.+Q'.� �11 (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total + ?-/ Z 01 pH (when analyzed) _9-3-/Z TOC N-JO -Iz <I.o mg/l units mg/1 Chloride 41-10-12 -7%o mg/I Arsenic y-5-17- b•oog mg/I Grease and Oils Phenol mg/1 mg/I Sulfate 17 ,-7- mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I GW-59 Rev. 03/2000 Orthophosphate mg/I Al - Aluminum' -5-17- y,09 mg/I Ba -Barium H -5- t z a-1%,2 mg/I Ca - Calcium. 14-5-1z 3'7,o mg/I Cd - Cadmium 14-5-17- <o.goZ mg/I Chromium: Total y -5-1 i a ,0c>n mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I. Mg - Magnesium q-S-IZ )9,11 mg/I Mn - Manganesey-5-1i /- (-/ m❑/I YES NO) Ni - Nickel -s-1Z &Ptc. mg/I Pb - Lea y - - I?- a ,059 mg/I Zn - Zinc mg Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) �eleninm �1-5-12 <o,00s ,,,ilk SodiuM / -5-1Z /0•'7 malt ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes-I(l) No ✓(0) VOC ; method # = method # = method # = Name and Title - Please print or type .O MAY 212012 Agent) Information Processing Unit DWO/BOG 5 - )'7 V Z- V/ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: 1 I)(i"I Permit Name (if di ere Facility Address: Contact Person:='rullip Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY - Please Print Clearly or Type Countv. iTelephone #: �,n-%Sfo - U I I) No. of Wells to be Sampled:_ Well Identification Number (from Permit): _M W An Well Depth: For Groundwater Treatment Systems P it. Well iameter: Z in. Check One: ❑ Influent (98) Screened Interval: It. to ft. Depth to Water Level: ]lot 1 ft. below measuring point. 0 Effluent (99) Measuring Point (M.P.) is: ` a ft. above land surface. Relative M.P. Elevation in )ft.: Gallons of water pumped/bailed before sampling:.. 3— Date sample collected: Field analysis: pH 71,0 Specific Conductance uMhos Temp. —-°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:W&000 15W3 EXPIRATION DATE: S -Zoi 1 Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Z. E ZELDLAD Laboratory Name: Ik) I C rZ -T- _ 0 H Certification No. �5h PARAMETERS (Samples for metals were collected unfiltered-3—kYES NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I Coliform: MF Fecal Coliform: MF Total /100ml mg/I Phosphorus: Total as P 9-2to-)z <o.ttgng/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4-4-)Z 13-1 Orthophosphate mg/I mg/I pH (when analyzed) 4-3 -1 Z '7.0 units Al - Aluminum _y-S-lz Ba - Barium 9 - s - i 2 0.0c06 mg/I TOC_ x-J.0 mg/I 8,5 Ca - Calcium z1-5- I2. 0 . nz0 t-ng/I Lo,Soo mg/I Chloride'-/-ltc-)z Arsenic 14-5-1Z mg/I 40•oo5 mg/I Cd-Cadmium q-5-17- Chromium:Totaly-5-1z' L.0.007- mg/I co.00s mg /I Grease and Oils mg/I Cu - Copper m/i Phenoron Sulfa el q - 5 -) z 'Z � 7 mg/l mg/1 Hg - (Mercury m9/I Specific Conductance K - Potassium mg/1 mg/I otal Ammonia N TKN mg/I Mg - Magnesium y - 5 -1Z 4o.t500 mg/I mg/I Mn - Manganese N -5-1'7- 4.0.o05 mg/I YES NO) Ni -Nickel. y-S-Iz 40.005 mg/I Pb - Leant y -5 -12 4 o 00 S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5elenio—M 44-5-I z �o oos r►,,i,� O t m 7- Ai /. M ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No V` (0) VOC method # = method # = method #._ r.....+r .,u�J111-�n•l3�lll�)�► ��� 1l�uf �l�rr�i .�Ti .. .0/ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (it d Facilitv Address: - Contact Person:�VWllj1. Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type 2 S County rbO W O 1 3relephone'#:_r`�l�-7S(o -L/1) j 1.1 No. of Wells to be Sampled:..—� Well Identification Number (from Permit): POW--11 For Groundwater Treatment Systems Well Depth: 13,0 it. Well Diameter: z in. Check One: ❑ Influent (98) Screened Interval: n1IT_ ft. to. NII� f(. [] Effluent (99) Depth to Water Level: 103G ft, below measuring point. Measuring Point (M.P.) is:3. b ft. above land surface. Relative M.P. Elevation in ff.: Gallons of water pumped/bailed before sampling: J5 Date sample collected: Field analysis: pH Ln• y Specific Conductance ' uMhos . Temp. 12 QC, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION; GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 713_1r. PERMIT #: W 61,O005(oo,3 EXPIRATION DATE: S -Zo II Non -Discharge U IC NPDES_ TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon Remedtalion: Infiltration, Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. -1 Z Date sample analyzed: 5eI77: 13t-Lnt,,,) Laboratory Name: W B 7 r= 2 Certification No. - 5n PARAMETERS (Samples for metals were collected unfilteredYES NO and field acidified COD mg/1 Nitrite (NO2) as N mg /I Coliform: MF Fecal /100ml Nitrate (NO3) as N m/I Coliform: MF Total /100ml Phncnhnn ic• Tntal ne ID 4_7 r. _/� 9n (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total `i-Q-12 17(2 mg/I pH (when analyzed) 41-3-t 2 69 units TOC q-Ib-lz z .IZ mg/I Chloride y - I to-- 17- ter, mg/I Arsenic q-5-I-z '40.00$ mg/I Grease and Oils mg/I Phenol rng/I Sulfate y - 5 -1 2- 33. b mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum y-.5-it 6.377, mg/I ea : 13arium 14-5 -12. O. c744 mg/I Ca - Calcium 4 -5- ► z 18.7- mg/I Cd - Cadmium 4-5-IZ. 40.00z mg/I Chromium: Total q-5-1 i Lo, oos mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium y -5-12- 5.8tA mg/I Mn - Manganese ma/I A YES NO) Ni -Nickel y-5-17_ 40.Obs mg/I Pb - Lean'4 - 5 -1 2 Lo, 005 mg/I Zn - Zinc rng/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Selen;oa, y-t -17- . /,o .0 0S Bunn 4^5-t2 314.Z MAI 0 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No ✓ (0) VOC : method # = method # method # _ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: — Permit Name (if F-Wility Address: Contact Person'.�1111144 Well Location/ Site Nar e. SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I f IL: t X )L.c_ )'I ( _ Telephone #: `l8 ' - No. of Wells to be Sampled: dram rermnt Well Identification Number (from Permit): j 1,A1 `) Z Well Depth: it. Well Diameter: 7- in. For Groundwater Treatment Systems Screened Interval: ft. to _�_ ft. Check One: ❑ Influent (98) Depth to Water Level: 989 ft. below measuring point. ❑ Effluent (99) Measuring Point (M.P.) is: 2. io ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling:/ d5 Date sample collected: Field analysis: pH -7' 2 , Specific Conductance ' uMhos Temp. 89°C; Odor Appearance -)Z DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: W& OW5003 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: ',) E = Q) r 1 CW Laboratory Name: _mil) A'rF_i EC_" Certification No. 50 PARAMETERS (Samples for metals were collected unfiltered NO and field acidified COD OD mg/I /100m1 Nitrite (NO2) as N Nitrate (NO3) as N /I Coliform: MF Fecal Coliform: MF Total Use /100ml mg/I Phosphorus: Total as P N Zb-) z a.19 mg/I (Note: MPN method for highly turbid samples) Dissolved Solids: Total4-9-/Z (Pol OrthOphosphate mg/I mg/I pH (when analyzed) 4)-3-) Z. 7# Z. units Al - Aluminum q-5-12 Ba - Barium y-5 -I2 A. /og/ mg/1 D. /y/ TOC _H-/ 0 -1 Z z o mg/1 Ca - Calcium. Q -5 -12 mg/I mg/I Chloride y-1 fo'-12 I Z . Arsenic 41-5 -) Z mg/1 Cd - Cadmium_ y-5 -1 Z <0,007- mg/I Grease and Oils mg/1 Chromium: Total 14s-1 z' i <o,OOS mg/I Phenol mg/I Cu - Copper mg/I •Sulfate q-5-I Z A> mg/I '7 m /I Fe : Iron H Mercury g ry mg/1 Specific Conductance uMhos K -Potassium mg/1 mg/I Total Ammonia TKN as N mg/I Mg - Magnesium q-S-12 /y. 3 mg/I mg/I Mn - Manganese 1-5-It 3-IoSr mg/I (or GW-59 Rev. 03/2000 —A YES NO) Ni - Nickel y-s•-IZ 0,069 mg/I Pb - Lead -Al -5 -1 Z- o o Iq mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) vele(li onn -S - I z 40,OOS avil —�odiym `I-S-Iz _zoonzq..11 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes 0) No _ / (0) VOC method # = or type method # = method # = -1.7 -/ Z a GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_, Permit Name (if d Facility Address:_ Contact Person: UII111f) Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY. Please Print Clearly or Type County f I iL IXI!rl-2Y-/ f �elephone M - 80rps- 2iS( - No. of Wells to be Sampled: Well Identification Number (from Permit): MLA) -13 For Groundwater Treatment Systems Well Depth: . is it. Well Diameter. z- in. Check One: ❑ Influent (98) Screened Interval: JO ft. to - A ft. El Effluent (99) Depth to Water Level: �,'ft. below measuring point. Measuring Point (M.P.) is:_a-( ft. above land surface. Relative M.P. Elevation in ft.:. Gallons of water pumped/bailed before sampling: ? Date sample collected: 14-3-1Z. Field analysis: pH— to1 3 , Specific Conductance ' uMhos . Temp. _I LS °C, Odor Appearance DEPARTMENT OF ENVIRONMiENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:'IA}4 OW Non -Discharge EXPIRATION DATE: U NPDES. TYPE OF PERMITTED OPERATION BEING MONITORED —N Lagoon Reinedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of SIu d Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: EL .13t WLA3 Laboratory Name: 1A3 RT9_Q T r^ Certification No. 56 PARAMETERS (Samples for metals were collected unfiltered__ p_YES NO and field,acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg /I m/I Coliform: MF Fecal Coliform: MF Total /100m1 Phosphorus: Total as Py-2(--)Z 0,19 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total q-Q-)Z 'L76 m9/1 Al : Aluminum L/-5-fZ. 0.4.19 mg/I pH (when analyzed) L4 - 3-12 16,3 units Ba - Barium Lit- 5 -1 2 6.0316 mg/I TOC y -I b -12 Z's"I mg/I Ca - Calcium `i -5 - I z ll, z mg/I Chloride y -1 b -1 Z /4, S' mg/I Cd - Cadmium 14-5 -12 Lo-oo z- mg/I Arsenic All- 5 - I z ►moo . oos a mg/I Chromium: Total y- s -12 4a • ooS mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron m g /I Sulfate _q-S -I Z Specific Conductance y'�,$ mg/I uMhos Hg -Mercury K -Potassium mg/I mg/I Total Ammonia mg/I Mg - Magnesium y-5-IZ 7,72- mg/I TKN as N mg/I Mn -Manganese y-5 -t2 0.z)3 mg/I (or GW-59 -Rev. 0312000 ge —YES NO) Ni -Nickel y-s -12, O• DOR mg/I Pb - Lead T76 _ri 0,009mg/l Zn - Zinc , mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) fnionn ��s-►z <o,00s r►al,k ORGANICS: (GC-,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No ✓ (0) VOC : method # = method # = method # _ - mease print or type S 47-4- / Z -6/ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Contact Person: I�J Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Prinf Clearly or Type County I I IQ: VUtA-YiU_- Telephone #: S 20o - 750 - y I I I No: of Wells to be Sampled:.. r7 Well Identification Number (from Permit): mw- N For Groundwater Treatment Systems Well Depth: IS ft. Well Djameter: - Z. in. Check One: ❑ Influent (98) Screened Interval: ---NIA ft. to /V A it. El Effluent (99) Depth to Water Level: 9-3 ft. below measuring point. Measuring Point (M.P.) is: Z, io ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ZoS Date sample collected: 4-3-1'L Field analysis: pH 401E , Specific Conductance ' uMhos . Temp. /9 °C, Odor Appearance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved 'Solids: Total ?-I Z , B3 mg/I pH (when analyzed) 14-3-17- (o,grr units TOC (I-10 -17- 2, 51 mg/I Chloride 4- lip-: I z < s. o mg/I Arsenic _y- mg/I Grease and Oils mg/I Phenol mg/l Sulfate '1-5 -1 Z 1v. o mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITfl:WSLOooir(oo3 EXPIRATION DATE: 5 -Zoll Non -Discharge U1C NPDES TYPE QF PERMITTED OPERATION BEING MONITORED Lagoon - Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: - NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _5 C- L 5 E 1 OW Laboratory Name: W R !E0 TECH Certification No. 50 YYES NO) Ni - Nickel -4-5 -►z <0,00s mg/I Pb - Lead y-S -112- o -o(oS mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) - 5eleAium y-5 -1Z 40, M� f,k Soliur, q-5-12 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No ✓ (0) VOID method # = method # = method # . . . �w�wwee�se�.� red A YES NO_ and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 9-zb-iz to if Orthophosphate mg/I Al - Aluminum y=5-12 Z,Fry mg/I Ba -Barium LI-5 -12 0,1 Zq mg/I Ca - Calcium 4-5-t2 73.3 mg/I Cd - Cadmium 4-S -11- 4o.00z mg/I Chromium: Total y-5-12 40.005 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/[ Mg - Magnesium �1-s-Iz y9.7 mg/I Mn - Manganese Al-6 -1 z O, 135 mg/I 40/ SUBMIT FORM ON YELLOW PAPER ONLY - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Coa}S Anner t on Permit Name (if different): Faciliitty` Address: ``}}�' o io s' '3&i' pireeqA) Q $`%S 2 lChy) 1e) lZt t County MCivOWr1_L Contact Person: Ili Qi �n Telephone #:-249-2-%-'1/// Well Location/ Site Name: Jler' No. of Wells to be Sampled: Well Identification Number (from Permit): M W -15 For Groundwater Treatment Systems Well Depth: � to it, ! Well Diameter- Z in. Check One: ❑ Influent (98) Screened Interval: �IJ�A ft. to N A ft. El Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is: Z, to It. above land surface. Relative M.P. Elevation in fit.: Gallons of water pumped/bailed before sampling: _1 25 Date sample collected: Field analysis: pH t�� , Specific Conductance uMhos Temp. 19 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 733-32: PERMIT#: wd10005to03 Non -Discharge EXPIRATION DATE: S -2011 UIC NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 51_ C- 15ELDW Laboratory Name: Wo:.ker-rcClej Certification No. 5o PARAMETERS (Samples for metals were collected unfiltered___�_YE5 NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phnsnhnn ts- Tnfnl ne PLJ-21e -12 46.1(o. _n (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total q-9-12 353 mg/I pH (when analyzed) 14-3-12 Lo, k- units. TOC N-10 -1 Z 21 IS mg/I Chloride y-JL=1 Z LS:o mg/I Arsenic 4 -5 -12 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 4-5 -IZ y3.o mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum _y-s-i L 40.0- s rng/I Ba - Barium 4 -5 -1 z 0.1) 5 mg/I Ca - Calcium 14-5 -12 172, 3 mg/I Cd - Cadmium N-5 -1 z 4o ooz mg/I Chromium: Total4-5-Iz 4o. 0o5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium 1-4-5-17- 3 3.Io mg/I Mn - Manganese 'q-5 - I Z / • / 3 ma/I X YES NO) Ni - Nickel 9-5 -► z 40100 s mg/I Pb - Lead y-5-12 1-0,bo S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5elen►um 14-5 -) z o,ods Mal,lZ Soa i o rv, LI -S- 12. Z 1 14 M p ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report. Report Attached? Yes (1) No (0) VOC : method # = method#= nerl�t�� fhel In Otis hec• i .., L � .a � � � � GW-59A C0IVIPLIANCE REPORT FORM Permit (Submit one each monitoring period wish GiV-59 forms.) 1 Enter date monitoring results were due. -)7 - Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? v YES NO iF the answer to question 1 or 2 is 'YES , list in the space provided below the well identification numbers))and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "?'es", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? V YES NO if the answer to question 4 is 'NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. MW Z LiNd n-OSa Mil Q• mw Z -rps (pot rn91.z MW 1Ll nnQ5Qnes(: I•lo1 "'Q Maganese mead o. o�oS �-� 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in ,the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. v If the answer to question 5 is "YES" list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). rnW.Iz Mo. oW)Me 2.q3 nM,3l,• S q-II maaof) 0sa ow Z. I - Id M61a iz -to - II TOO 575r-aj.A 4-It mu�anesr mW iZ z•lomg�,,l? Iz-Io-II -r os S t 0 me l.k 'Tos Sworn y -14 - l l 6 Are the monitoring wells li ed in section 5 located at or beyond the review boundary? YE5 NO if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If.the answer is "NO") monitoring wells may be improperly located; contact the Regional Office. 7 is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to,question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days• an evaluation maybe required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this_ facility. Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for requiredwells to the address provided at the top of the current GW-59 form. 1 herebyacknowledge tfiat theabove Informatlon`was evaltiaEea and the information submitted In th s report (Compliance Report GW59A) fs true and complete o the best of my kn owiedgeAAA t - -12 Signature of Pe ittee (or Authorized Agent) Date rr VV en. ,1�O RECEWE® - T 17 TECH _..... .._.. _....Inc. POST OFFICE BOX 1056 • ##5 PINEWOOD PLAZA DR. P AY 2 g 2612 GRANITE FALLS, NORTH A CAAAAROLINA 28630(828)396 Asheville Regional office SAMPLE. Coats America (MW#02) COLLECTION DATE: 4/3/2x 12 Aq IfE?l hr otection ' PERMITA* COLLECTION TIME: 09:15 ADDRESS. Coats America (Wells) RECEIVED DATE: 4/3/2012 P.O. Box 368 RECEIVED TIME., 14:50 Marion, NC 28752 REPORTED: 5/11/2012 ANALYSIS � .. ANALYSIS'` : RESULTS (!NITS DATE _ :ANALYST Sulfate 12.2 mg/L 4/5/12 vi`hlodde 7.0 mg/L 4/16/12 lag T. Phosphorus 0.48 mg/L 4/26/12 jdg toc <1.0 mg/L 4/10/12 "^S 101 mg/L 4/9/12 lag metals see attached pH >holding time 7.1 su's 4/3/12 lag 9 LOG ID: 1204-040 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor w#wTER6rv-cHLjqv-s.1nc POST OFFICE BOX 1056 n5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 4/3/2012 PERMITA- COLLECTION TIME. 09:20 ADDRESS: Coats America (Wells) RECEIVED DATE., 4/3/2012 P.O. Box 368 RECEIVED TIME., 14:50 Marion, NC 28752 REPORTED: '5/11/2012 ANALYSIS =` ANALYSIS ; :RESULTS UN1TS DATE :ANALYST -> Sulfate 32.7 mg/L 4/5/12 Chloride 8.5 mg/L . 4/16/12 lag T. Phosphorus <0.16 mg/L 4/26112 jdg toc <1.0 mg/L 4/10/12 JfDS 127 mg/L 4/9/12 lag metals see attached pH ' >holding time 7.0 su's 4/3112 lag LOG ID., 1204-041 REPORTED BY: NC CERTIFIED LAB # 50 fp� Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTHCAAAAROLINA 28630 A (828) 396`f` 44 SAMPLE. , Coats America (MW#11) COLLECTION DATE: 4/3/2012 ' PERMIT* COLLECTION TIME: 09:40 ADDRESS., Coats America (Wells) RECEIVED DATE: 4/3/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28T52 REPORTED. 5/11/2012 ANALYSIS _ - ANALYSIS = RESULTS UN1TS ©ATE `ANALYST = Sulfate 33.6 mg/L 4/5/12 chloride 9.3 mg/L 4/16/12 lag T. Phosphorus <0.16 mg/L 4/26/12 jdg toc 2.12 mg/L 4/10/12 %,At$ 176 mg1L 4/911,2 Iag metals see attached pH ' >holding time 6.3 su's 413/12 lag LOG ID: 1204-042 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#12) PERMIT & ADDRESS: Coats America (Wells) P.O. Box 368 Marion, NC 28752 COLLECTION DATE: 4/3/2012 COLLECTION TIME.- 09:47 RECEIVED DATE: 4/3/2012 RECEIVED TIME: 14:50 REPORTED: 5/11/2012 10.7 mg/L 4/5/12 Sulfate %Aoride 12.3 mg/L 4116112 tag T. Phosphorus 0.19 mg/L 4/26112 jdg toc 2.30 mg/L 4110112 419/2... metals see attached pH ' >holding time 7.0 su's 4/3/12 lag LOG ID: 1204-043 REPORTED BY: NC CERTIFIED LAB # 50 fk�'. 60" Tony Gragg, Lab Supervisor R6 KCH LROSinc. POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#13) COLLECTION DATE: 4/3/2012 PERMIT A COLLECTION TIME. 09:57 ADDRESS: Coats America (Wells) RECEIVED DATE. 4/3/2012 P.O. Box 368 RECEIVED TIME., 14:50 Marion, NC 28752 REPORTED: '5/11/2012 ,�nrAc.Yses ANALYSIS :-RESULTS Ul1(tTS 'DATE � ANALYST Sulfate 47.8 mg/L 4/5/12 %iloride 19.8 mg/L 4116/12 lag T. Phosphorus 0.19 mg/L 4126112 jdg toc 2.57 mg/L 4/10/12 S 276 mg/L 419/12 lag metals see attached PH'>holdingtime 6.3 su's 4/3112 lag LOG ID: 1204-044 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab 3upervisor LBO .w F4i, rvCH I Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 4/3/2012 PERMIT A COLLECTION TIME: 10:04 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/3/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: -5/11/2012 ANALYSIS ANALYSIS.` RESULTS UNITS DAZE 'ANALYST Sulfate <10.0 mg/L 4/5112 %.Zhloride <5.0 mg/L 4/16/12 lag T. Phosphorus 0.22 mg/L 4/26112 jdg toc 2.51 mg/L 4/10/12 %,4'DS 383 mg/L 419/12 lag metals see attached pH ' >holding time 6.7 su's 413/12 lag LOG ID: 1204-045 REPORTED BY: -NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR - GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#15) COLLECTION DATE. 4/3/2012 PERMIT A COLLECTION TIME. 10:16 ADDRESS: Coats America (Wells) RECEIVED DATE: 4/3/2012 P.O. Box 368 RECEIVED TIME: 14:50 Marion, NC 28752 REPORTED: 5/1.1 /2012 ANALYSIS RESCLLTS UNITS ©ATE ANALYST Sulfate 43.0 mg/L 4/5112 -,_Aloride <5.0 mg/L 4/16/12 lag T. Phosphorus <0.16 mg/L 4/26/12 jdg toc 2.18 mg/L 4/10/12 ''Y S 353 mg/L 4/9/12 lag metals see attached pH ">holding time 7.0 su's 4/3/12 lag LOG ID: 1204-046 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor i'���ttlilll�lr' ��. RESEARCh St ANAL TICAI. C r NC. = o� LAboRATORIES , I� z;ca NC#34 Analytical/Process Consultations NecidirFj9-•.....••' �5 '0i ���ir�ED ANP �`~ Water Tech Labs. Inc. Date Sample Collected 04/03/12 P.O. Box 1056 Date Sample Received 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed 04/05/12 Attn: Joe Gragg Date of Report 04/13/12 Analyses Performed by JC -MS Lab Sample Number --------------------- 728516 --------------------- Parameter Storet # Results Magnesium,Tot (00927) 19.8 mg/l Calcium,Tot (00916) 37.0 mg/l Sodium,Tot (00929) 10.7 mg/l vLhromium,Tot (01034) 0.007 mg/l veadmium,Tot (01027) <0.002 mg/1 vilickel,Tot (01067) 0.016 mg/l %Zelenium,Tot (01147) <0.005 mg/l %Aarium,Tot (01007) 0.182 mg/1 %oKrsenic,Tot (01002) 0.008 mg/1 Manganes�,Tot (01455) 1;61..mg/l.; Aluminum,Tot (01105) 4.09 mg/1 vgulfate (00945) 12.2 mg/l -------------------- Clients Sample Source COATS AMERICAN MW 2 Number Time Collected (Hrs) 0915 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284 + 336-996-2841 • Fax 336-996-0326 www.randelabs.com 10 RESEARCIi & ANAI TICA1 ,•••,�=�..C.,rTi . - UbORATORIES, INC.ca NC #34 Z. Analytical/Process Consultations . 't�..O'� �. • ,,' Water Tech Labs. Inc. Date Sample Collected : 04/03/12 P.O. Box 1056 Date Sample Received : 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed : 04/05:/12 Attn: Joe Gragg Date of Report : 04/13/12 Analyses Performed by : JC -MS Lab Sample Number -------------------- 728517 Parameter Storet # Results Magnesium,Tot (00927) Calcium,Tot (00916) Sodium,Tot (00929) vehromium, Tot (01034) %,,dadmium,Tot (01027) �ickel,Tot (01067) %,delenium,Tot (01147) %Aarium,Tot (01007) �Xrsenic,Tot (01002) :. VZead,Tot (01051) VAanganese,Tot (01055) Aluminum,Tot (01105) sulfate (00945) Clients Sample Source Number Time Collected (Hrs) <0.500 mg/l <0:500 mg/l 47.3 mg/1 <0.005 mg/l <0.002 mg/l <0.005 mg/l <0.005 mg/l 0.020 mg/l <0.005 mg/1 <0.005 tng/l <0.005 mg/l 0.066 mg/l 32.7 mg/l -------------------- COATS AMERICAN MW 10 0920 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCh & ANAIyTICA1 LABORATORIES, INC. Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected : 04/03/12 P.O. Box 1056 Date Sample Received : 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed : 04/05/12 Attn: Joe Gragg Date of Report : 04/13/12 . Analyses Performed by : JC -MS Lab Sample Number -------------------- 728518 Parameter Storet # Results Magnesium,Tot (00927) 5.86 mg/1 Calcium,Tot (00916) 18.2 mg/l Sodium,Tot (00929) 34.2 mg/l t/hromium,Tot (01034) <0.005 mg/l X/admium,Tot (01027) <0.002 mg/l %4ickel,Tot (01067) <0.005 mg/l %4elenium,Tot (01147) c0.005 mg/l %Xarium,Tot (01007) 0.099 mg/l %,ersenic,Tot (01002) <0.005 mg/l %,eead,Tot (01051) <0.005 mg/1 Aluminum,Tot, (01105) 0.372 mg/l %ulfate (00945) 33.6 mg/l -------------------- Clients Sample Source COATS AMERICAN MW 11 Number Time Collected (Hrs) 0940 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax 336-996-0326 www.randalabs.com - RESEARch & ANA[yTICA1 LAboR* ATWE!�INC. Analytical/Process Consultations Water Tech Labs. Inc. P.O. Box 1056 Granite Falls, NC 28630 Attn: Joe Gragg ♦♦`��►Fi cly �YTj fti =�. O: N NC#34 z: RED Date Sample Collected 04/03/12 Date Sample Received 04/05/1.2 Date Sample Analyzed 04/05/12 Date of Report 04/13/12 Analyses Performed by JC -MS Lab Sample Number -------------------- 728519 --------------------------- Parameter Storet # Results Magnesium,Tot (00927) 14.3 mg/1 Calcium,Tot (00.916) 79.8 mg/l Sodium,Tot (00929) 201 mg/l �hromium,Tot (01034) <0.005 mg/i %Zadmium,Tot (01027) <0.002 mg/l dickel,Tot (01067) 0.008 mg/1 `4elenium,Tot (01147) <0.005 mg/l %Xarium,Tot (01007) 0.141 mg/1 Al.<rsenic,Tot (01002) <0.005 mg/1 Lead, Tot (0.1051} _ 0 _019 `mg/1- Manganes,Tot COlb55).68 mg/1 Aluminum,Tot (01105)- 0.104 mg/l Veulfate (00945) 10.7 mg/l -------------------- Clients Sample Source COATS AMERICAN MW 12 Number Time Collected (Hrs) 0947 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284 •336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCh & ANA[YTICA[ ` gjN A..... •��'• LAhORATORIES, INC. CO- ; M • ' Analytical/Process Consultations Zw Water Tech Labs. Inc. Date Sample Collected 04/03/12 P.O. Box 1056 Date Sample Received 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed 04/05/12 Attn: Joe Gragg Date of Report 04/13/12 Analyses Performed by JC -MS Lab Sample Number 728520 Parameter Storet # Results Magnesium,Tot (00927) 7.72 mg/l Calcium,Tot (00916) 11.2 mg/1 Sodium,Tot (00929) 79.0 mg/l t,,dhromium,Tot (01034) <0.005 mg/l %Xadmium,Tot (01027) <0.002 mg/l vNrickel,Tot (01067) 0.008 mg/l %Xelenium,Tot (01147) <0.005 mg/l 1/garium,Tot (01007) 0.036 mg/l VKXsenic,Tot (01002) <0.005 mg/l %,Zead,Tot, (01051) 0.009 mg/l vl�tariganee, Tot:; . (01055).. -= 0 213 'mg/1 Aluminum,Tot (01105) 0.619 mg/1 -vXulfate (00945) 47.8 mg/l -------------------- Clients Sample Source COATS AMERICAN MW 13 Number Time Collected (Hrs) 0957 P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27264.336-996-2841 • Fax 336-996-0326 www.randalabs.com VIS��,uui,���i RESEARCh & ANALyTICA1 '`�� cYr *�y UbORATOI&S INC. te v =¢cwo NC �:cn Analytical/Process Consultations qp ED AK Water Tech Labs. Inc. Date Sample Collected : 04/03/12 P.O. Box 1056 Date Sample Received : 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed : 04/05/12 Attn: Joe Gragg Date of Report : 04/13/12 Analyses Performed by : JC -MS Lab Sample Number -------------------- 728521 Parameter Storet # Results Magnesium,Tot (00927) 48.7 mg/l Calcium,Tot (00916) 73.3 mg/l Sodium,Tot (00929) 24.8 mg/1 .-Aromium,Tot (01034) <0.005 mg/1 %Xadmium,Tot (01027) <0.002 mg/l %,4ickel,Tot (01067) <0.005 mg/l %Zelenium,Tot (01147) <0.005 mg/l %,4arium,Tot (01007) 0.129 mg/1 v&rsenic,Tot (01002) <0.005 mg/l Lead,Tot� (O1d51) OV 065 mgJl �ian..ganese,Tot C01455) = r� 135 mg/�...' Aluminum,Tot (01105) 2.84 mg/l ,,,g'ulfate (00945) <10.0 mg/l -------------------- Clients Sample Source COATS AMERICAN MW 14 Number Time Collected (Hrs) 1004 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284.336-996-2841 • Fax 336-996-0326 www.randalebs.com 'twives I1100re. + rr Ij RESEARCh & ANA1yTICAL er`'Q v+�' •••n••••..'? '�.. UbORATWES, INC.A daI--. H A' ; c" NO �i34 z' cn Analytical/Process Consultations trllil/y� Water Tech Labs. Inc. Date Sample Collected : 04/03/12 P.O. Box 1056 Date Sample Received : 04/05/12 Granite Falls, NC 28630 Date Sample Analyzed 04/05/12 Attn: Joe Gragg Date of Report : 04/13/12 Analyses Performed by : JC -MS Lab Sample Number -------------------- 728522 Parameter Storet # Results Magnesium,Tot (00927) 33.6 mg/1 Calcium,Tot (00916) 72.3 mg/l Sodium,Tot (00929) 21.4.mg/1 vCeromium,Tot (01034) <0.005 mg/l �admium,Tot (01027) <0.002 mg/l %Xickel,Tot (01067) <0.005 mg/l V relenium,Tot (01147) <0.005 mg/1 %Afarium,Tot (01007) 0.115 mg/l %'4rXsenic,Tot (01002) <0.005 mg/l a/Lead,Tot (01051) <0.005 mg/1 Aluminum,Tot (01105) <0.025 mg/1 %-S'Oulfate (00945) 43.0 mg/1 -------------------- Clients Sample Source COATS AMERICAN MW 15 Number Time Collected (Hrs) 1016 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284.336-99&2841 • Fax 336-996-0326 www.randalabs.com Page 1 of 2 VROOTEST Laboratory Report Lab Location X' Lab Location 'C' NC/UVW Cent* 067 NC1DW Cert# 37731 NC/W W CerL* 103 NC/DW Cert#. 37733 6701 Conference Dr, Raleigh, NC 27607 6300 Ramada Dr, Suite C2, Clemmons,'NC 27012 Ph: (919) 834-4984 Fax (919) 834-6497 Ph: (336) 766-7846 Fax (336) 766-2514 Project No.: 01 Project ID: COATS AMERICA MW — Prepared for — Jon Gragg Water Tech Labs PO Box 1056 Granite Falls, NC 28630 Report -Date: 4111 /2012 Date Received: 4/4/2012 Work Order #: 1204-00325 Cust. Code: WATERT Cust. P.O.#: INCL TOC RESULTS No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 001 MONITORING WELL #2 4/3/2012 9:15 GW . Grab 4 +1- 2 deg C Test Performed Method Results Lab Loc DatYed Time Qualifier Total Organic Carbon 5310C <1.0 mglL R 4110112 14.58 No. Sample ID Date Sampled Time Sampled Matrix Sample Type. Condition 002 MONITORING WELL #10 413/2012 9:20 GW Grab 4 +1- 2 deg C Test Performed Method Results Lab Loc Daatyzed Time Qualifier Total Organic Carbon 6310C <1.0 mglL R 4110/12 14.58 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 003 MONITORING WELL #11 4/3/2012 9:40 GW Grab 4 +1- 2 deg C ' Test Performed Method Results Lab Loc DateyZed Time Qualifier Total Organic Carbon 5310C ' 2.12 mglL R 4110112 14.68 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 004 MONITORING WELL #12 4/312012 9:47 GW Grab 4 +1- 2 deg C Test Performed Method Results fib Loc Dated Time Qualifier Total Organic Carbon 5310C 2.30 mg/L R 4110112 14:68 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 006 MONITORING WELL #13 4/3/2012 9:57 GW Grab 4 +/- 2 deg C Test Performed Method Results lab-Loc Da W� Time Qualifier Total Organic Carbon 6310C 2.67 mg1L R 4110112 14:68 9 Telephone: (919) 834-4984 Fax: (919) 834-6497 1TRJTEST 6701 Conference Drive Raleigh, NC 27607 Telephone: (919) 834-4984 Fax. (919) 834-6497 Laboratory Report Work Order # 1204-00325 Page 2 of 2 NClWW Cart #: 067 NC/DW Cart #: 37731 No. Sample ID 006 MONITORING WELL #14 Date Sampled 413/2012 Time Sampled Matrix 10:04 GW Sample Type Condition Grab 4 +1- 2 deg C Test Performed Method Results Lab Loc Dared Time Qualifier Total Organic Carbon 5310C 2.61 mg1L R 4110112 14:58 No. Sample ID 007 MONITORING WELL #15 Date Sampled 413/2012 Time Sampled Matrix 10:16 GW Sample Type Condition Grab 4 +1- 2 deg C Test Performed Method Results l�nal zed Lab Loc at Time Qualifier Total Organic Carbon 5310C 2.18 mg1L R 4110112 14:58 Reviewed by: / E'tG�z�-L:c ter-...e�.��,,��►Lc1/ for Tritest, Inc. GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:— ( ILQ�t Permit Name (if different): Facility Address:C> Contact Person.'�WJlj) P Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I P► MY.t 1 a t �_ Telephone #:'633 - 9 b -L No. of Wells to be Sampled: Well Identification Number ber (from Permit): t} to -- Z For Groundwater Treatment Systems Well Depth: '7 � it. `Well Diameter: � in.. Check One: ❑ Influent (98) Screened Interval: ) it. to it. Depth to Water Level: r ft. below measuring point. ❑ Effluent (99) p J . Measuring Point (M.P.) is: 9: -3 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 352 Date sample collected: Field analysis: pH (0,G_17 ,Specific Conductance uMhos Temp. %a °C, Odor Appearance ' • _ DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES-- AR QUALITY DIVISION, GROUNDWATER SECTION NOW163T6',MAILS ERVICE CENTERALIGH NC 27699-1636 Phone: 919 I733-fi21 — PERMIT #: t t)CZCCbSkz,03 EXPIRATION DATE: t;} L Non -Discharge UIC 1" - ri NPDES O o 1 - e' TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery 2, CC r Spray Field Remediation: �0 r� Rotary Distributor Land Application of Sludge Other: I �? NOTE: Values should reflect dissolved and . �� colloidal concentrations. 'f "� Fs1V Date sample analyzed: a_e JAN 1 2 2012 Laboratory Name: Certification No, vrrnation i'rucggs►r�g nit PARAMETERS (Samples for metals were collected unfiltered X YES NO ' and field acidified COD mg/I Nitrite (NO2) as N mg /I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MFTotal /100ml Phosphorus: Total as P_Iz-la-il <c•Iton.t/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total Ia-)a-I1 � IC,� mg/1 Al -Aluminum ,-5,39 mg/I pH (when analyzed) la-h• 11 6 zs units Ba - Barium 12-Lo - 1 \ Ca. t 3ta m TOC _1,a -�? - \ Chloride la -1 rj 4 1, l mg/I mg/I Ca - Calcium l z--(o -I t Cd - Cadmium_. i z. -6.-� t z�, mg/I mg/I v . o© Arsenic i a (yi\ (I (D5 mg/l Chromium: Total /2 -�-it Go, 1 -S m lI g Grease and Oils mg/I Cu -Copper mg/1 Phenol Sulfate _ �a-1r,-1\ mg/I 1y. \ mg/I Fe - Iron Hg -Mercury m /I g mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium /Z-L-// ► �,o m /I g TKN as N m /I Mn - 1'z-� - l' _ YES NO) - -- Ni - Nickel )z -(, -I 1 0 of z mg/I Pb- Lean iZ -& -1/ o-O"fz- mg/1 Zn - Zinc mg/I 'Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓(1) No (0) VOC D -'I : method # = & 2i o 0 method#= ceft(fy that, to the best of tmtf knotrtltedne nnri hafiaf fho infmmofinn :-A I-:- ____ .._ .___ ame lie - Please print or r G W-59 Re; , 03/2000 of 0 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address: Corilact Person:.�1S Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County t 4`111ephone #: .X , V -1 No. of Wells to be Sampled: prom rermn) Well Identification Number (from Permit): MW --1 Well Depth: �g For Groundwater Treatment systems P t ft.- Well Diameter.: _ in. Check One: ❑ Influent 98 Screened Interval: :+J � ( ) �_ ft. to �,�1 f-- ft. Depth to Water Level: lh. e[p Effluent99ft. below measuring point. ( Measuring Point (M.P.) is: 2 ; ft. above land surface. Relative M.P. Elevation in #t.: 2 Gallons of water pumped/bailed before sampling: 3 Date sample collected: Field analysis: pH 1 •Q , Specific Conductance ' Temp. . 1`1 °C, Odor Appearance _ PARAMETERS (Samples for metals were collected unfit COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total 1100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total Iz-Iz-)t qln mg/I pH (when analyzed) Iz. o -t\ -7, o units TOC_1­7 -Ci -1\ 1-\,0 mg/I Chloride i\,D mg/I Arsenic IZ-t✓ t\ 4',c)•OoS mg/I Grease and Oils mg/I Phenol mg/I IZ Sulfate -k-t\ mg/I Specific Conductance uMhos Total. Ammonia mg/I TKN as N mg/I umhos ' • a -DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH NC 27fi99-1636 Phone: 919 733-3221 PERMIT #: UO C_:kW05 (063 EXPIRATION DATE: " ' 61 Non -Discharge UIC NPDES__ TYPE OF PERMITTED OPERATION BEING MONITORED �— Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: �F�t�t'Ic`st,y Laboratory Name:--1_�7rd+,er- Certification No. tered A YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg /I Phosphorus: Total as P IZ-1Z-1k 4o.iiamg/I Orthophosphate m9/I Al - Aluminum I Ao-I mg/I Ba - Barium I� -(>-1\ C,. ��� mg/I Ca - Calcium _12-(o- mg/I Cd- Cadmium 1Z-(,)-I1 CQ&OOz. mg/I Chromium: Total_iz-to-i1 4C.005 mg/I Cu - Copper mg/I Fe - Iron mg/I, Hg - Mercury _ mg/I K - Potassium mg/I Mg - Magnesium i z -6 - i 1 2, 0.5Cc) mg/I Mn - Manganese iZ-to-0 4p:ut5 mg/I X YES NO) Ni - Nickel i Z-L,-1 1 mg/I Pb - Lead I Z -b- t I G G t ; mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units), ORGANICS: ('GC,GC/MS,HPLC) (Specify test and method #. Atjach lab report.) Report Attached? Yes V (1) No (0) VOC method # = eZ 1 b p _ method # = method # r rmittee (or Aulharizert�4geO Name and Title - Please print or type `GW-59 ReV. 03/2000 Signature of Permaleei raurnnd7ad n­rn GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: 1 i A•1" Permit Name (if different): Facility Address: 7•C)• Contact Person. nk\t Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY - Please Print Clearly or Type County t I +,- `, AsC 1 \ Telephone No. of Wells to be Sampled:. Well Identification Number (from Permit): T�'ttij - } For Groundwater Treatment Systems Well Depth: %'2' Cam, it. Well Diameter: -Z- in. Check One: ❑ Influent (98) Screened Interval: u It. to A..' ft. Effluent (.99) Depth to Water Level: 1L�•C! ft. below measuring point. Measuring Point (M.P.) is: 3, Ic ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: Date sample collected: 21 b -1 ) Field analysis: pHSpecific Conductance uMhos . Temp. t `l °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) 733 32: PERMIT#:WC'�L_)00 063, EXPIRATION DATE: "201 1 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NQ—Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: _ Sep ph(Aiy,lk) Laboratory Name: 04 ko x 1 e n h Certification No. _ 56 PARAMETERS (Samples for metals were collected unfiltered x YES NO and field acidified COD Coliform: MF Fecal mg/I /100m1 Nitrite (NO2) as N Nitrate (NO3) as N mg/I Coliform: MFTotal /100ml Phosphorus: Total as P-12--1:3--11 mg/I 40•16mg /I (Note: Use MPN method for highly turbid samples) " Orthophosphate m/I Dissolved Solids: Total IZ-)2 -11 L < mg/I Al - Aluminum-) z -6-1A 0'9')D m9/I pH'(when analyzed)iz -(c -1 1 (o.0 ; units Ba - Barium � L -h - t 1 0, 0`1 b mg/I TOC _tz -r-r - j\ u. � mg/I Ca - Calcium 'z -�o '3 mg/I Chloride -1 S-� _I'� � Arsenic t mg/I mg/I Cd - Cadmium 17.4-1 - t Chromium: Total 1a-IV i.1 4 o. 00'a mg/I /'d.c'5 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate _i'Z -lo- mg/I mg/I Fe - Iron Hg - Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg /1 Total Ammonia � mg/I Mg - Magnesium a (�-1►3 m /I ' ` g TKN as N mg/I Mn - Manganese mg/I t cettity that to the best of my knnwianna nnri honof itio .s., ► ., X YES NO) Ni - Nickel IZ-G-t1 mg/I Pb - Lead LZ 40Dos mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) '15F'�en10nn ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓ (1) No (0) VOC method # _ (a y1O O method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: l (,t i"r') 1-tf Ytl'f itC4t� Permit Name (if different): Facility Address: 17 b pp '?') obi • ri (Sveeq tcays �C County ?�r (9:.� Contact Person: k• ` Isar to°I ` �., 2 i{ n Telephone #: - Well Location/ Site Name: .7t is i Ni i'��`IuL COP No. of Wells to be Sam Well Identification Number (from Permit): M W - 1y For Groundwater Well Depth: )"'7) it. Well Diameter 7� in. Check One: ElScreened Interval: %ice ) IA ft. to � ft. ❑ I Depth to Water Level: _eft, below measuring point. Measuring Point (M.P.) is:kc) ft. above land surface. Relative M.P. Elevati Gallons of water pumped/bailed before sampling: -�— Date sample collet Field analysis: pH k to Specific Conductance uMh Temp. 1 tO °C, Odor Appearance l\ — DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (919) PERMIT #: L,JU 00C%Sio Non -Discharge EXPIRATION DATE: S -'Z0 t M1 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED --—_.Lagoon Remedi o1 r V RaQn�J:L;� i rjuT�" n, n i tration Gallery Remediation: _ Land Application of Sludge should reflect dissolved and . I concentrations. lialyzed: Certification No. _ S0 PARAMETERS (Samples for metals were collected unfiltered A YES NO and field acidified COD mg/I Nitrite (NO2) as N m /I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phnsnhnnic• Tntal ac P 12-1*"� t Z6.ti.,Y, /I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total _I z°-I �-/ 1 Sib m9 /I pH (when analyzed) ZZ-G-1I f .to"3 units TOC _ f Z--Cl -11 "? 1v mg/I Chloride 1 G--1 S- I I m /l Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate _1z.-try - mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I ` GW-59 Rev. 03/2000 Orthophosphate mg/I Al - Aluminum J'Z-(, - t 1 0. o'73 mg/I Ba - Barium _1 z - to - � i 6. 017U mg/I Ca - Calcium /'z-1,-, - (1 y1?,3 mg/I Cd - Cadmium/Z -to - i► 4o-00 Z mg/I Chromium: Total 7"7-_1r•1; 4'0•e,c� mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium i'2 -4,-11 mg/I Mn - Manganese 7-1/ c me/I _YES NO) Ni -Nickel. 0, 007 mg/I Pb - Leads /�2 -U -/ / <o d7la S m9/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SeiPni U.,-� !:� '% ••1 I Ld UL� .�iti�C;�� Socki or-,, 12_-G - I 1 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓ (1) No (0) VOC( : method # L-) ID' method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: (__ lL-i Ary-P(►CCI►'" Permit Name (if different): Facility Address: __ Pb. 'N ay Contact Person:. Well Location/ Site Name: county me Qnwe t Telephone #: `'a' • 1 I 1 No. of Wells to be Sampled: Well Identification Number (from Permit):_ fnW -)* For Groundwater Treatment Systems Well Depth: LS ft. Well Diameter: 19 in. Check One: ❑ Influent (98) Screened Interval: "N ft. to �% it. El Effluent ('99) Depth to Water Level: _ft. below measuring point. Measuring Point (M.P_) is::a l ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling:_ Date sample collected: I:a -6 Field analysis: pH fo+ a 1e , Specific Conductance uMhos . Temp. I ka °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT N: IA3 0, t)oo "-1 O 3 EXPIRATION DATE: _ �" ZO I j Non -Discharge UIC_ NPDES TYPE 9F PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of.Sludge Other: NOTE; Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: See 6c`pu; Laboratory Name: o t Certification No. SiJ PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I mg/I Coliform: MF Total /100ml Phosphorus: Total as P1z-/3ii 1-0,)& mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total l � -1 � -/► 43 mg/I AlAI -Aluminum _%z-tom-rl � O•bds mg/I pH (when analyzed) 1Z-L �' - I \ (o- a -_ units Ba -Barium /Z-t- -) mg/I TOC I`�- I J Chloride _/Z-11-0 z. L! b '- mg/I mg/1 Ca - Calcium 12--c,� - i I Cd - Cadmium _%2-c,, •-I I 1 �{ c� tng/I c.e .00 �� mg/I g Arsenic _j z - e� �-/ ! z c7• ��c>s . mg/I Chromium: Total i���lo•-61 C ��,ar�� mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate r z- to -i f mg/I 4/0- c mg/I Fe - Iron Hg -Mercury m /I 9 mg/I Specific Conductance LlMhos K - Potassium mg/I Total Ammonia mg/I Mg- Magnesium _) Z!L-ll mg/I TKN as N mg/I Mn - Manganese_iz-(o-0 mg/I il ✓ YES NO) Ni - Nickel_ f a -f, --a n 00(o mg/I Pb - LeacL/z--10--/I L ary )J mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ('iP(1►t�f1.1 !. -fr -') D Z n c�t�x� �ti-•ca,` �. 5QL�io 12- (11 -1 1 L3 4 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. ttach lab report.) Report Attached? Yes (1) No (0) VOC 0 DL method # - _ (o; 11G p method # _ �i SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING - COMPLIANCE REPORT FORM FACILITY INFORMATION - Please Print Clearly or Type Facility Name: LCl-va Permit Name (if different): - Facility Address: Pvita Y,� r. , - - - - Contact Person: Well Location/ Site Name: County 1 ham V-b06 \ Telephone #: LA I \ No. of Wells to be Sampled: Well Identification Number (from Permit): DoU.a For Groundwater Treatment Systems Well Depth: 1 1,5 ft. Well Diameter: _ in. Check One: ❑ Influent (98) Screened Interval: ) _ Depth to Water Level: Gi . _ ft. below measuring point. 0 Effluent (99) Measuring Point.(M.P.) is: It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling:_ Date sample collected: Field analysis: pH [,2A 5 Specific Conductance ' uMhos Temp. ►b 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT-#: •WaCX-)C)SO0 j EXPIRATION DATE: Non -Discharge U IC NPDES TYPE OF'PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Laboratory Name: u--1cxke f t PC1^L Certification No. t PARAMETERS (Samples for metals were collected unfiltered _YES NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N m /I Coliform: MF Fecal Coliform: MF Total 1100m1 Phosphorus: Total as P lz %:III mg/I zp 9 +gym /I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Dissolved Solids: Total/ZIZ-I) Z14/ mg/1 Al -Aluminum &- -11 �?.qy mg/I pH (when analyzed) W-0- -Ca-11 Wq units Ba - Barium _j7�--(- -1) 0.•f mg/I TOC _j'z- ° , 22 ? - mg/I 4-?; 5 mg/I Ca - Calcium 1'z; &, -!/ Cd - Cadmium -7 L,3 mg/I Lo• W4- mg/I Chloride Jz_/ -l7 Arsenic /Z-&-/) 4c) -y2S mgll Chromium: Total l2-fv-0' 40•0o.5 mg/I Grease and Oils mg/I Cu - Copper mg/l Phenol Sulfate L2 -do -f f mg/I �I� mg/I Fe - Iron Hg - Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia TKN as N mg/I Mg -. Magnesium 12-t�-1) 55: g m /I mg/1 Mn - Manganese_ E -k' -I I f~ c t� 1 m9/I. e (or 73 x YES NO) Ni-Nickel mg/I Pb - Lead I' -6 i t -03LI_ mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5'yF>I/y}PcI�1�nJn-� Cc 05���. 1)'� ORGANICS: (GC,GCIMS,HPLC) (Specify test and method #. Altach lab report.) Report Attached? Yes V (1) No (0) VOC (? 1L : method # _ jig 10 0 method # = method # _ or type GW-59 Rev. 03/2000 Agent) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: (, '0A! A rVl Permit Name (if different): Facility Address: ` c-, Q} hl 0-1 —_ 01 ( tt 3 "�' tscat t �� o/ County fC Icnr) _ Contact Person^ t `i ' �� Q D4elephone #: Well Location/ Site Name: a�'u' e9 ShTJd No. of Wells to be Sampled: "_ Well Identification Number (from Permit): L') - Well Depth: �(p For Groundwater Treatment Systems P �� ft. Well Diameter-- in. Check One: ❑ Influent (98) Screened Interval: �_ ft. to Wit,} 1 � ft_ Depth to Water Level: it. below measuring point. ❑ Effluent (99) Measuring Point (M.P.) is: ft. above land surfa e. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ja Date sample collected: %-j Field analysis: pH Iv r 17 , Specific Conductance ' uMhos Temp. J_O°C, Odor Aonearanr.P DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER'OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: L J GLC-005 Ca6,3 EXPIRATION DATE: S �d Non -Discharge t Itf NPDES TYPE F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Laboratory Name: 1A IXIL 1Jl t ( Ln Certification No. 60 PARAMETERS (Samples for metals were collected unfilteredk_YE5 NO and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NOZ) as N Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P-1a 1;3•il Go./U mg/1 m /I (Note: Use MPH method for highly Dissolved Solids: Total l turbid samples) /��61 3kQ Orthophosphate mg/I g mg/I pH (w en analyzed) /'7 units Al - Aluminum./62-6-// Ba -Barium l-Lo-/I 400- �� mg/1 (7• `c�� TOC� Chloride t"- / L mg/I �� S mg/I Ca - Calcium )�_(„ /f Cd - Cadmium /-2 j/ '� mg/I m /I 4 Q.OGQ - Arsenic 1�-� -l% Grease and Oils �o ©c75 mg/I Chromium: Total fa -to-ft " cO..y(:-S mg/I mg/1 Phenol mg/I Cu - Copper mg/I Sulfate i-19-i/ Specific mg/I r`�i n mg/I Fe - Iron Hg - Mercury mg/I m /I Conductance Total Ammonia uMhos K - Potassium 9 mg/l TKN as N mg/I Mg - Magnesium mg/I mg/l Mn - Manganese L -(a-1 mg/I _( YES NO) Ni -Nickel /,'2--<9 // -0 «� mg/I Pb - Lead/-L-2 / .0 Cf')-mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify.test and method #. Attach lab report.) Report Attached? Yes t%(1) No (0) VOC AL method # = (ajD a method # method # = Ml • � aria Y�nl��� i�ycct Permittee (or Authonzeci iigenl) a —me and Title Please print or type r / G1N 59 t Ad g <✓�! Rev. 03/2000 Signature of Perm ittee (o Aulhorized Agent) ,�-, v �• -�yti %.v1v1r1,L'11N UE REPORT FORM Permit # (Submit one each monitoring period with GFV-59 forms.) 1 Enter date monitoring results were due. ( —(d -j �) Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? YES NO 2 Was any required information missing on the GW-59 report forms? IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. YES NO 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes ", conlact the Regional Office for guidance. YES NO 4 Are any monitored constituents equal to or above the established standards? Fthenswer to question 4is 'NO" skip to section 8. nswer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s) ing standards in the space provided below: c (VI wz [U.7� rnwtiZ �Z.lc� YES NO 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is 'NO'; skip to section 8. if the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence'(for the last two years). i D S. frn w I Z L S coo> L( -1 C( - 11 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem maybe occurring, CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO'; monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO if the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report shoulaf sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 herebyacknowlec)ge that thQ; Bove information was evaluat6d4,bnd the information subinitted-Tithis s", report_(Compliance ReportGW59A) Is true and complete to the`6 st of my knowi@a9e v �z �- ,; Signature of Perm' ee (or Authorized Agent) Date GNV-59A 12/8/2003 Lfiffi _ -ins.. P08T OFFICE EOX Iar55 EfNEir(I6615 ELAZA biq. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#02) PERMIT #: ADDRESS: Coats America (Wells) P.O. Box 368 Marion, NC 28752 COLLECTIONDATE. 12/6/2011 COLLECTION TIME. • 07:00 RECEIVED DATE: 12/6/2011 RECEIVED TIME.- 13:45 RFPOPTFn• LOG ID: 1112-176 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor 6T.V H Inc. . r POST OFFICE BOX 1056 -4 #5 PINEWOOD PLAZA DR., GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Coats America (MW#10) COLLECTION DATE: 12/6/2011 _ PERMIT A COLLECTION TIME 07:30 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/6/2011 P.O. Box 368 Marion, NC 28752 RECEIVED TIME., 13:45 REPORTED: 12/29/2011 :. ANALYSIS ANALYS/S RESULTS U/VITS DATE ANgLYST ✓Sulfate 14A mg/L 12/8/11 ✓Chloride 11.0 mg/L 12/15/11 lag T. Phosphorus <0.16 mg/L 12/13/11 jdg. toc <1.0 mg/L 12/9/11 `/FDS 96 mg/L 12/12111 lag metals see attached voc see attached LOG ID: 1112-177 REPORTED.BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor - MRTER'�- XCH .Inc. POST OFFICE BOX 1056 • n5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE., Coats America (MW#11) PERMIT #: ADDRESS: Coats America (Wells) P.O. Box 368 Marion, NC 28752 COLLECTION DATE., 12/6/2011 COLLECTION TIME: 08:00 RECEIVED DATE: 12/6/2011 RECEIVED TIME., 13:45 REPORTED: 12/29/2011 LOG ID: 1112-178 REPORTED BY: NC CERTIFIED LAB # 50 ff�* Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 • 95 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROL►NA 28630 (828) 39&4444 SAMPLE., Coats America (MW#12) COLLECTION DATE: 12/6/2011 PERMIT A COLLECTION TIME. • 08:30 ADDRESS: Coats America (Wells) RECEIVED DATE., 12/6/2011 P.O. Box 368 RECEIVED TIME., 13:45 Marion, NC 28752 REPORTED: 12/29/2011 �4NALYSIS ANALYSIS : RESULTS ......... ,DATE ANALYST ✓Sulfate <10.0 mg/L 12/8111 ✓Chloride 11.5 mg/L IW5/11 lag T. Phosphorus <0.16 mg/L 12/13/11 jdg toc 2.76 mg/L _ 12/9111 TDS .510 mg/L 12/12/11 lag metals see attached voc see attached LOG ID: 1112-179 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor :i LfiJ .Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Coats America (MW#13) COLLECTION DATE: 12/6/2011 PERMIT #: COLLECTION TIME: 09:00 ADDRESS: Coats America (Wells) RECEIVED DATE: 12/6/2011 P.O. Box 368 Marion, NC 28752 RECEIVED TIME: 13:45 REPORTED. 12/29/2011 LOG ID., 1112-180 REPORTED BY: NBC. CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor rm6rrcH Lass. -Inc POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS. NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 12/6/2011 _ PERMIT #. COLLECTION TIME: 10:00 ADDRESS., Coats America (Wells) RECEIVED DATE: 12/6/2011 P.O. Box 368 RECEIVED TIME: 13:45 Marion, NC 28752 REPORTED: 12/29/2011 - ANALYSIS ANALYSIS - _:RESULTS UNITS ;DATE �4NALYST --'Sulfate <10.0 mg/L 12/8/11 - .%Chlodde <2.5 mg/L 12/15/11 lag T. Phosphorus <0.16 mg/L 12/13/11 jdg toc 2.82 mg/L 1219111 `/`IDS 441 mg/L 12/12/11 lag metals see attached voc see attached LOG 1D: 1112-182 REPORTED BY: NBC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor mqrER6rjrcHL1fAfi.1nc. POST OFFICE BOX 1056 • 45 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28830 (828)396-4444 SAMPLE. Coats America (MW#15) COLLECTION DATE: 12/6/2011 PERMIT A COLLECTION TIME: 10:30 ADDRESS., Coats America (Wells) RECEIVED DATE: 12/6/2011 P.O. Box 368 RECEIVED TIME., 13:45 Marion, NC 28752 REPORTED., 12/29/2011 ANALYSIS ANAtYS/S RESULTS UIyITS DATE ANALYST ✓Sulfate 29.0 mg/L 12/8111 ✓Chloride <2.5 mg/L 12/15/11 lag T. Phosphorus <0.16 mg/L 12/13/11 jdg- toc 2.56 mg/L 1219/11 ,4DS 382 mg/L 12/12/11 metals see attached voc see attached LOG ID: 1112-183 REPORTED 3Y: Nff� CCERTIFIED LAB # 50 Tony Gragg, Lab Supervisor RF-SEARCh- & ANALYTICAL • LA ORATORIES/ INC. Analytical/Process Consultations December 21, 2011 Water Tech Labs P.O. Box 1056 Granite Falls, NC 28630 Attention: Joe Gragg, Project Name: Coats American II. Miscellaneous MW2 MW10 MW11 MW12 MW13 MW14 MW15 Parameters Unit Results Results Results Results Results Results Results. Aluminum, Total mg/L 3.39 0.073 0.272 0.093 <0.025 2.44 <0.025 ✓Arsenic, Total mg/L 0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 ✓�arium, Total mg/L 0.136 0.018 0.076 0.096 0.046 0.140 0.123 Vtadmium, Total mg/L <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 .,chromium; Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 Calcium, Total mg/L 27.7 0.221 13.3 483 14.0 76.3 73.7 Lead, Total mg/L 0.04D yvt <0.005 <0.005 <0.005 <0.005 OA3 <0.005 Magnesium, Total mg/L = ;��u,l 1�' 0 <0.500 :. 4 > ~.10y 10. ] , .iJj X Manganese, Total mg/L 1. 4 <0.005 0. 62 0 2. 0 Q:V: . 94 Nickel, Total mg/L 0.012 <0.005 <0.005 0.007 0.006 <0.005 <0.005 -,Selenium, Total mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 Sodium, Total mg/L 11.5 34.2 23.0 143 134 26.3 16.2 ,-91fate mg/L 10.1 14A 23.9 <10.0 <10.0 <10.0 29.0 ,Sample Number 719754 719755 719756 719757 719758 719759 719760 Sample Date 12/06/11 12/06/11 12/06/11 12/06/11 12/06/11 12/06/11 12/06/11 Sample Time 0700 0730 0800 0830 0900 0930 1000 mg/L = milligrams per Liter = parts per million (ppm) < = Less than or below detection limit w r3 C a m w C O — z••-ir)wton_ Hte•"-HntoCc)C7C7 S,�WgrTn�'Oiva tz cr o m A 5 Coo°oE 9rocaoc�cc� •,p `Ab c pa �, Cx� cAoWr r b o• o+ o' :-I `CJ •t V fP •-' N IJ IJ IN W . � SI 8 CD ~ H 4+ r.. 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Code: WATERT Granite Falls, NC 28630 Cust. P.O.#i INCL TOC RESULTS No. Sample ID 001 MONITORING WELL #2 Date Sampled 12/6/2011 Time Sampled Matrix 7:00 GW Sample Type Grab Condition 4 +/- 2 deg C Test Performed Method Results — Anal zed Lab Loc atey Time Qualifier Total Organic Carbon 5310C <1.0 mg/L R 1219111 9.10 No. Sample ID 002 MONITORING WELL #10 Date Sampled 12/6/2011 Time Sampled Matrix 7:30 GW Sample Type Grab Condition 4 +/- 2 deg C Test Performed Method Results Lab Loc DnaVzedTime Qualifier Total Organic Carbon 5310C <1.0 mg/L R 12/9/11 9:10 No. Sample ID 003 MONITORING WELL #11 Date Sampled 12/612011 Time Sampled Matrix 8:00 GW Sample Type Grab Condition 4 +/- 2 deg C Test Performed Method Results lyzed Lab Loc Date Time Qualifier Total Organic Carbon 5310C 4.08 mg/L R 1219111 9:10 No. Sample ID 004 MONITORING WELL #12 Date Sampled 12/612011 Time Sampled Matrix 8:30 GW Sample Type Grab Condition 4 +1- 2 deg C Test Performed Method Results Lab Loc DaTyzed Time Qualifier Total Organic Carbon 5310C 2.76 mg/L R 1219/11 9:10 No. Sample ID 005 MONITORING WELL #13 Date Sampled 1216/2011 Time Sampled Matrix 9:00 GW Sample Type Grab Condition 4 +1- 2 deg C Test Performed Method Results nal ed Lab Loc Date' Time Qualifier Total Organic Carbon 5310C 4.02 mg/L R 1219/11 9:10 "TROYEST 6701 Conference Drive Page 2 of 2 Raleigh, NC 27607 Telephone: (919) 834-4984 Telephone: (919) 834-4984 Fax: (919) 834-6497 NCIWW Cert. #: 067 Fax: (919) 834-6497 NCIDW Cert. M 37731 Laboratory Report Work Order m 1112-00431 No. Sample ID 006 MONITORING WELL #14 Date Sampled 12/6/2011 Time Sampled Matrix 9:30. GW Sample Type Grab Condition 4 +/- 2 deg C Test Performed Method Results zed Lab Loc D,Ty Time Qualifier Total Organic Carbon 5310C 2.82 mg/L R 12/9111 9:10 No. Sample ID 007 MONITORING WELL #15 Date Sampled 12/612011 Time Sampled Matrix 10:00 GW Sample Type Grab Condition 4 +1- 2 deg C Test Performed Method Results Lab Loc Date ed Time Qualifier Total Organic Carbon 5310C 2.56 mg/L R 12/9111 9:10 Reviewed by: i for Tritest, Inc. 'SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: L O H t_5 1-1 in t r ! r f}yj Permit Name (if different): Facility Address: 6 (1 0 3 Yh I4 r • o V (St(eet) 2 $,tz (City) Stale) (zip) County � G --.Wet C Contact Person: 1 ll t �►� ►`) r` Telephone #: SZg-9d-G - 4// 1 Well Location/ Site Name:.5elail- I;C EX Grdury No. of Wells to be Sampled: �_ [tram Permit) Well Identification Number (from Permit): M&I- 2-- For GroundwaterTreatment Systems Well Depth: 76' it. Well Diameter /2 in. Check One: ❑ Influent (98) Screened Interval: '"A+ it. to .11/4 ft. ❑ Effluent (99) Depth to Water Level: 39.6 It. below measuring point. . Measuring Point (M.P.) is: 2,3 It. above land surface. Relative M.P. Elevation MR.: Gallons of water pumped/bailed before sampling: 7/•2.f Date sample collected: Field analysis: pH , Specific Conductance ' uMhos Temp. I6 °C, Odor Appearance 9-11 DEPARTMENT OF ENVIRONMENT & NATURAL RE40URCES WATER QUALITY DIVISION, GROUNDWATER SECT ON- 1636 MAIL SERVICE CENTER PERMIT #: 418 o005G q5EXPIRATION DATE: CV' ?2`80 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 13 ID Lagoon Remedialion: Infiltration Galle 0` Spray Field Remediation: I �_ CM Rotary Distributor Land Application of Other: Sludge NOTE: Values should reflect dissolved and . E- E f V E D colloidal concentrations. Date sample analyzed: t-=E /Vc I/d k/ Laboratory Name: W14 '7-Pc/, Certification No. 6-0 ation Processing nt /BOG PARAMETERS (Samples for metals were collected unfiltered_Y YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P_V'16-11 0.21 mn/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 8•io-ii /aZ mg/I pH (when analyzed) 919 // •b units TOC mg/I Chloride 8-2-1-11 Zs'o mg/I Arsenic S-f2-li 50.004;' mg/I Grease and Oils mg/I Phenol mg/I Sulfate 8-12-11 X-C) mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 GW-59 R Vj. 03/2000 Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium V- l2-t t 0, 127 mg/I Ca - Calcium _ Y- I?- 2S• y mg/I . Cd-Cadmium V-12" Zb.00t mg/I Chromium: Total 41-t2- I1 4 6.00C mg/I Cu - Copper mg/I Fe - Iron mg/I Hg ,- Mercury mg/I K - Potassium mg/I Mg -Magnesium fI-12-11 13.7 mg/I Mn-Manganese t3-t 2-li 0432- mQ/1 X_ YES Ni -Nickel 13-►2- Pb - Leart Zn - Zinc Ammonia Nitroge Other (Specify Com NO) n pounds and Concert -0-1 J -lz- n9 mg/1 mg/I — mg/1 mg/I ation Units) O, o�G• O,G n,oii ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #.'Attach la report.) ReportAttached? Yes (1) o (0) VOC method # = method # = method # = 11ti,"t.L1 KT'1'an q w O f G Permittee (orpArthbfized Agent) name and I e - PI ase print or type -��W Signature of ermittee (or A ho(zed Agent) (Dale) 0 G CJ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Co (,4+- s Vn l: r "G A ry Permit Name (if differe t): Facility Address: �U �O 3fo Yh in C AJ (slreeq tv` 7-V MS ljowel't (Cil ) ( ale) Rip) County Contact Person:�+,tt 4 P'i4Vh A- A i+l� �✓ Telephone #: Well Location/ Site Name: 540it,111456 °"' No. of Wells to be Sampled: T_ (Irani Permll) Well Identification Number (from Permit): 0741- /d For Groundwater Treatment Systems Well Depth: 1 it. Well Diameter. 2- in. Check one: ❑ Influent (98) Screened Interval: it. to wA" ft: ❑ Effluent (99) Depit� to Water Level: fib•/ fl. below measuring point. Measuring Point (M.P.) is: Z,3 ft. above land surface. Relative M.P. Elevation In ft.: Gallons of water pumped/bailed before sampling: 3 Date sample collected: _ Field analysis: pH '�/S Specific Conductance uMhos Temp. 2 / °C, Odor Appearance PERMIT #: w Non -Discharge DEPARTMENT OF ENVIRONMENT & NATURAL RE OURCES WATER QUALITY DIVISION, GROUNDWATER SEC ION 1636 MAIL SERVICE CENTER b+ooB5Goc3 EXPIRATION DATE: RAJ/ UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITOR[ _ Lagoon Remedialion: Infiltration Ga Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. EI`v ED REC Date sample analyzed: Sew /3•t%/o rr/ Laboratory Name: W d y"e r TPc n Certification No. S"a Information Processing Unit PARAMETERS (Samples for metals were collected unfiltered X YES NO 'and field acidified COD mg/I Nitrite (NO2) as N - mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phnsnhnrus- Tntal as P SI-Id-1l LO,/6 mn/1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 5-16-11 116' mg/I pH (when analyzed) (?-?-It G.y3" units TOC $-14-t / t ►.D mg/I Chloride 9- 21-11 mg/I Arsenic 9-12- 11 Co.00S mg/I Grease and Oils mg/I Phenol mg/I Sulfate g-12-11 32. mg/I Specific Conductance - uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium S- ►2- If a.oZb mg/I Ca - Calcium_9-12-11 40.saa mg/I Cd - Cadmium 9-12-11 40.1001 mg/I Chromium: Total o,00s mg/I Cu - Copper trig/l Fe - Iron rng/I Hg - Mercury mg/I K -- Potassium g Mg - Magnesium 9,12'1 I o •s a0 mg/I Mn - Manqanese_ 5-12-rf' 40,00s' m❑/I X -YES NO) l wunsvu Ni - Nickel-1z-1► 46oaf mg/I Pb - Lea 5'•/Z- 11 .00Smg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Conce tration Units) o iu - 2-i , ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes (1) o (0) VOC : method # = method # = method # = (or Aul ari ed AV gent) Name and T411a 7 Prase print or tvoe L GW-59 �� O./e-�/ Rev. 03/2000 Signature of Fwfmillee (or „ulWrized Agent) (Dale) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: %o AfS on, c r i c 4& Permit Name (if differ nt): Facility Address: t, 6 3 £� dr ON (Streeq Icily) stale) 2$%!iot County l�/ Our el G Contact Person: 'ji Pli,nro,c rI+ 1�u �.Y5 Telephone Well Location/ Site Name: SkvitF / 195h No. of Wells to be Sampled: 7 (Irom P.—II)Well Identification Number (from Permit): Mlr! For Groundwater Treatment Systems Well Depth: ft. Well Diameter: 2--in- Check One: ❑ Influent (98) Screened Interval:/j4 ft. to ^'/A ft. 11 Effluent 99 Depth to Water Level: 14,9 ft. below measuring point. Measuring Point (M.P.) ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _ Date sample collected: ?-q-// Field analysis: pH , Specific Conductance ' uMhos . Temp. %9 -C, Odor Appearance PERMIT #: U, Non -Discharge NPDES DEPARTMENT OF ENVIRONMENT & NATURAL RE 3OURCES WATER QUALITY DIVISION, GROUNDWATER SECI ION 1636 MAIL SERVICE CENTER RALEIG'H, NC 27699-1636 Phone: 191 )733-39: EXPIRATION DATE: UIC TYPE F PERMITTED OPERATION BEING MONITOREI Lagoon - Remedialion: Infiltration Galli Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. RE Date sample analyzed: S 4-oOF &rrl e W Laboratory Name: W W7 it ?;mac _h Sj Certification No. SS 6 PARAMETERS (Samples for metals were collected unfiltered_X YES NO and field acidified COD mg/I Nitrite (NO2) as N m /I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P lb-lf -10.14 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate m /I Dissolved Solids: Total 51-to-jr 244 mg/I AlAI -Aluminum mg/I pH (when analyzed) F-?-// G•/y units Ba -Barium 2-11 6.107 mg/I TOC mg/I Ca - Calcium E t2.-a 237, 3 mg/I Chloride g`21-t1 Arsenic 53-f2-rl /[o mg/I Co•oo5 mg/I Cd - Cadmium 8-12 -►1 Chromium: Total.8-a-•r► ' 'Zn,00 1 mg/I m /I g Zo.00s Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate 8- IZ--ft mg/I 1Z9 mg/f Fe - Iron Hg -Mercury mg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia TKN as N mg/I Mg - Magnesium 9"12-11 W-82 mg/I mg/I Mn-Manganese 9-12-it O,1,3% mg/I ;` l'ermittee (or A thor' ed Agent) GW-59 Rev. 03/2000 Signature o ermit ee (orA 1 A YES NO) Ni -Nickel S-12-11 46 Pb- Lead SLIL-11 to Zn - Zinc Ammonia Nitrogen Other (Specify Compounds and Concen -2611 EI V ED Oil os mg/I os mg/I mg/I .— mg/I ition Units) ORGANICS: (GC,GC/MS,HPLC,) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) NO (0) VOC : method # and TiI!l." Pleaseprini or Woe method # method # A // Unit.: SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: ' - • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES . WATER QUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM 1636.MAIL SERVICE CENTER FACILITY INFORMATION Please Print Clearly or Type RALEIGH NC 27699-1636 Phone: 91 733-3221 PERMIT #: 600 S G d EXPIRATION DATE: cS Non -Discharge UIC FacilityName: �b 14 �S /� N1 >= ►^ C{ /�- -241 Permit Name (if differept): Facility Address: i' �0 �e G NPDES M $4 r 1 O rV (Street) _ N C Stale) 297'Z,c) County INN po w e t l .. Contact Person �'h l,1 ?74'Imo- / 9APk Nud�_ - 14 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Well Location/ SF / fF/ Telephone #: R241-7S6 )11 —X Remediation: Infiltration Galle Site Name: v r'� ,f vE,.i No. of Wells to be Sampled: �_ Spray Field Remediation: (from pemll) Rotary Distributor Land Application of Sludge Other: Well Identification Number (from Permit): In&)-12 For Groundwater Treatment Systems 13 Well Depth: ft. Well Diameter•: 1 Screened Interval; 1 ft. to `V00— it. in. Check One: ❑ Influent (98) Effluent 99 Depth to Water Level: /D•I ft. below measuring point. TE NOTE, �� Values should reflect dissolved and . colloidal FOE�/ ���a'� Measuring Point (M.P.) is: ?•b ft. above land surface. Relative M.P. Elevation in ft.: concentrations. Gallons of water pumped/bailed before sampling: _�_ Date sample collected: - 9-// 640 Date sample analyzed: .5 ,F ,BAe /d kr SF P 29 7 2011 Field analysis: pH , Specific Conductance uMhos Laboratory. Name taAfAr 'c Temp. 1C 'C, Odor Appearance Certification No. Sl1 nor hV Unit tD woeo� /Boo PARAMETERS (Samples for metals were collected unfiltered_ X _YES NO and field acidified _YES NO) COD mg/I Coliform: MF Fecal /100mf Nitrite (NO2) as N Nitrate (NO3) as N mg/I Ni - Nickel P/2-11 /I �- mg/I Coliform: MF Total /100m1 m I?b -Lea z-ll g ee- . Phosphorus: Total as P. S Z0,16 mg/I Zn - Zinc oS mg/I (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total `/0-/1 s 9,f mg/I Orthbphosphate Al - Aluminum mg/I Ammonia Nitrogen mg/I mg/I pH (when analyzed) - -// .G units Ba - Barium R-IZ-U mg/I Other (Specify Compounds and. Concen 01126 mg/I S /4" - 2-11 ration Units) - TOC _ $- lb `1( 3.19 mg/I Ca -Calcium 9112-1) An e• fl rn 9 /I d;0 M ZOO Chloride _S -2EI f 2 mg/I Cd -Cadmium 9-12- If -.54 Z n, 1101 mg/I Arsenic _ 9-12-u 6.00! mg/I Chromium: Total S-lz-)I 46,005 mg/I Grease and Oils. mg/I Cu - Copper mg/I Phenol mg/I Sulfate -12-II /1.1 mg/I Fe - Iron Hg - Mercury mg/I ORGANICS: GC,GC/MS,HPLC ( ) Specific Conductance P uMhos K - Potassium mg/I 9 (Specify test and method #, Attach la mg/I Report Attached? Yes report.) Total Ammonia mg/I Mg - Magnesium gl-12-1=i 1 /0.3 mg/I VOC 0 0 ( ) TKN as N mg/I Mn-Manganese V-12-j1 method #)= 2.13 mg/I :method # method # = Au or type C., GW-59 Rev. 0312000 Agen SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM 1636 MAIL SERVICE CENTER FACILITY INFORMATION Please Print Clearly or Type RALEIGH NC 27699-1636 Phone:91733-3221 n Facility Name: 1.oA'(5 A0%EriC_Aw 2a�/ PERMIT #:W906OSG03 EXPIRATIONDATE: Non -Discharge UIC Permit Name (if different): Facility Address: P O X 2 6 t3. NPDES it A C I D n- vU c 2 � Z c ICnY) (Sireeq Y r1i c- 6o to e t l (rP) Count TYPE OF PERMITTED OPERATION BEING MONITORED Conta& Person?h;tt; ? f vn,4 r$(A ria i - Telephone #: �a8-7S6 ' N// % — Lagoon Remediation: Infiltration Galley Well Location/ Site Name: 51V • N /v,t Kf No. of Wells to be Sampled: 7 --mil) Spray Field Remediation: (Uom Rotary Distributor Land Application of Sludge Other: Well Identification Number (from Permit): YYl W ` 13 For Groundwater Treatment Systems Well Depth: 1.5 it. Well Diameter. 2 in. Check One: ❑ Influent (98) �—. Values should reflect dissolved and . Screened Interval: ""/A ft. to r`/A El ft. �Effluent (99) Depth io Water Level: 13•7 ft, below a measuring point. Measuring Point (M.P.) is: 21ft. above land surface. Relative M.P. Elevation in ft.: colloidal concentrations. '(�' 'VE® Gallons of water pumped/bailed before sampling: - Date sample collected: -4 '/I Date sample analyzed: ,$,EE a ie&r k) s a P Field analysis: pH 6.3.5 , Specific Conductance uMhos Laboratory Name: W.4�Er P0A ' Temp. Z n °C, Odor Appearance Certification No. 6' Information Processing t1nR PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified COD mg/I Nitrite (NO2) as N m /1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total _ /I00Ml Phnsnhnrnic• Tntal ac 17 II (Note: Use MPN method for highly turbid samples Dissolved Solids: Total 8-40•-it X7l •mg/l pH (when analyzed) 9-11 L.3S units TOC __ g-lb-fl 3 .a$ mg/I Chloride 8 -Z 1- 11 j 23 mg/I Arsenic 9-1Z~11 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1?-12-1f mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum - mg/I Ba - Barium 9-1 Z-1 0.01.1 mg/I Ca - Calcilam -1I 2 239 . mg/I Cd - Cadmium `) L-1 '44001 mg/I Chromium: Total 9-)Z-/r- 40,006- mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium m g/I Mg - Magnesium -12 �J/ /d•z mg/I Mn - Manganese. 01757 mn/I I2A K YES NO) Ni - Nickel Pb-- Lea Zn - Zinc Ammonia Nitrogen_ Other (Specify Compound S,E/EwiG�► 8�1Z` LO• o g/ Go, OS mg/I mg/1 mg/I and Conce tration Units) 1 o d,57- I .,ac— ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach I b report.) Report Attached? Yes (1) o (0) VOC : method # = C method # = method # = GW-59 Rev. 0312000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM t-AUILI I Y trot-unmH I [UN Please Print Clearly or Type Facility Name: CO' -AS 4 yh•Er-1CAA— Permit Name (if diffe�g nt): Facility Address: NO f3a X' 36 8 (Street) 1ti, t4 ni >7rl/ ,t� c 2��SZ County ^ /0.010A 6G tac -i.: l: .% , -now �a�e rA //4 .Nz'°' Telephone #: _�Li�'7,s6 Contact Person: Well Location/ Site Name: r 1,66 / ti No. of Wells to be Sampled:_ (from ermlt) Well Identification Number (from Permit): For Groundwater Treatment Systems Well Depth: IS S it. Well Diameter-2 in. Check One: ❑ Influent (98) Screened Interval: '1/'F ft. to � it. I-] Effluent (99) Depth io'Waler Level: 9.1 It. below measuring point. Measuring Point (M.P.) is:-2.12_ ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 'Z Date sample collected: Field analysis: pH li ./ Specific Conductance uMhos Temp. /7 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RE OURCES WATER QUALITY DIVISION, GROUNDWATER SEC ION 1636 MAIL SERVICE CENTER PERMIT #: w EXPIRATION DATE Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITOREC A Lagoon Remediation: Infiltration Galle Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE` QE/ Laboratory Name: —,4 -1,CP 7" Certification No. . S- D PARAMETERS (Samples for metals were collected unfiltered-_A_YE5 NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P- A'// . CG•/G m9 /I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total Jo-J/ W mg/I Al - Aluminum mg/I pH (when analyzed) f4- /1 "1& `/1 4-7/ units Ba - Barium 6-12 t f D•/2Z mg/I TOC _ y 2y mg/I Ca - CaIcItim f2,-11 7q 2- rng/I Chloride 4n mg/I Cd - Cadmium " 2-11 m /I Arsenic 9`12-1 f �d.6o5 mg/I Chromium: Total `/2`►t Lb�oaS mg/I Grease and Oils mg/I Cu - Copper mg/l Phenol Sulfate S3-2t'II mg/I <B.t7 / mg/I Fe - Iron Hg -Mercury m /I g mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia rrlg/I Mg -Magnesium _ 8-12` // y/•3 mg/I TKN as N mg/I Mn - Manganese_ 2'1/' /.a>' m9 /I _YES NO) Ni - Nickel k-/2-11 Pb - Lead 8-/4-/1 Zn - Zinc Ammonia Nitrogen - Other �-'���(Specify Compounds and ���N:Gzn V-/2-/I =Z6/ SFP T, 7 `1011 mation Processing Uni Z o•e1os- <o mg/I mg/I mg/I mg/I Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach IE b report.) Report Attached? Yes (1) o (0) VOC : method # _ method # method # = e, Pe/_ O!`C • GW-59 ' Rev. 0312000 Signature of Per ttee (or Aulhorized ent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY r DEPARTMENT OF ENVIRONMENT & NATURAL RE 3OURCES GROUNDWATER QUALITY MONITORING: WATER QUALITY DIVISION, GROUNDWATER SEC1 ION COMPLIANCE REPORT FORM 1636MAIL SERVICE CENTER RALEIGH NC 27699-1636 Phone: 91 733-32, ACILITY INFORMATION n Please Print Clearly or Type Facility Name: l , o (1tzT.5 IV /// E' r' r' C q. In, Permit Name, (if differe t : Facility Address: IF M04 n 1 a 4 ) (streeq/�"� 0 (City) s at IZip) County Contact Person: l: • a• NN ti Telephone #: 929- 76 Well Location/ Site Name: S-!G. " r % WSA No. of Wells to be Sampled: Well Identification Number (from Permit): W- / For Groundwater Treatment Systems Well Depth: % ft. Well Diameter•: in. Check One: ❑ Influent (98) Screened Interval: / lo/ it_ to '-/'N ft. ❑ Effluent (99) Depth to Water Level: _/A3 ftbelow measuring point. Measuring Point (M.P.) is:_5 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: Y2 Date sample collected: Field analysis: pH •L/ Specific Conductance . uMhos Temp. 19! °C, Odor Appearance PERMIT #: m EXPIRATION DATE: Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _K_ Lagoon - Remedialion: Infiltration Galle Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and .��� colloidal concentrations.RECoE Date sample analyied: S Sr '2?.F16 •J 1w '1011 Laboratory Name:. wid-1 ✓ Te Certification No. st7 tntforma +on pe�nessing Unit PARAMETERS (Samples for metals were collected unfiltered_ X YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phnsnhnri is• Tntal ac P f-lb-11 Z-A./6 rr -/l (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total .0 mg/I pH (when analyzed) 6•,2 units TOC 9-16 -1/ IV-mg/I Chloride _ R-W - Il -'' .0 mg/I Arsenic 0-12-)1 mg/I Grease and Oils mg/I Phenol mg/I Sulfate -12-11 mg/I _/�G Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum mg/1 Ba - Barium Vf Z - f 1 O./y a mg/I Ca - Calcium 91-U-lf b-y mg/I admium i?• ►Z�-I/ Cd - Cadmium— Ld•oo f mg/I Chromium: Total 9-12-11 ' � � •o os mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium g Mg : Magnesium I2-4/ 31• 2, mg/I Mn - Manqanese "f2-(1 /49 rrin/I Permittee r A 1 orize n GW-s9 Rev. 03/2000 Signature of er inee orAull —L_YES NO) Ni - Nickel •iz_r < mg/I Pb -'Lead t'12-/l co-605 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/1 Other (Specify Compounds and Cancer tration Units) SELEoit,m V-r2,-11 6.0t7�i ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) NO (0) VOC method # = method # = method # = i // rl GW-49A COMPLIANCE REPORT FORM Permit # 1�&66OS 4c 3 (Submit one each monitoring period with GiV-59 forms.) 1 Enter date monitoring results were due. ( t/ - `3. o- tt) Will this monitoring report (GW-59 and GW-59A) be. submitted after the established due date? YES NO X 2 Was any required information missing on the GW-59 report forms? YES NO iF the answer to question 1 or 2 is "YES', list in the space provided below the welt identification numbers) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing Identification plate, area overgrown, etc.)? If the answer is "1'es ", contact the Regional Office for guidance. YES NO 4 Are any monitored constituents equal to or above the established standards? YE NO if the answer to question 4 is "NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s) exceeding standards in the space provided below. -% jo s W 1 'L :fin ;.tu5 t-' ffipxygns e a i•.13ar�°%i 5> zl � �' i�'�'�%� 5 For the constituents identified in question'4 above, have standards e-en exceeded previously for the same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is 'NO" skip to section 8. If the answer to question 5 is "YES'; fist in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). YES NO Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring, CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO', monitoring wells maybe improperly located; contact the Regional Office. X 7 is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO if the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. RECEWPD SEA 2 7 2013 'nfoi7n8tion Pmce 9 Unit 8 The person completing this portion (GW-59A) o t itoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 hereliyackrio a that;the}above information was evaluated and the inforanationsubniltfed_Tnfhis Sign re of Permittee Authorized Agent) Date GW-59A 12/8/2003 A r; WRTER POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE F.=%L.LS. NORTH CA,ROLiNA 28630 (828)396-4444 SAMPLE: Coats America (MW#02) COLLECTION DATE: 8/9/2011 PERMIT #: COLLECTION TIME: 09:00 ADDRESS: RECEIVED DATE: 8/9/2011 RECEIVED TIME: 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST ` Sulfate <10.0 mg/L 8112/11 Chloride <5.0 mg/L 8/21/11 jmf T. Phosphorus 0.28 mg/L 8/16/11 jdg toc <1.0 mg/L 8/16/11 TDS 102 mg/L 8/10/11 lag metals see attached MCCENE SEP Wo aWn processing unit DWQ150 LOG ID: 1108-135 REPORTED BY: NC CERTIFIED LAB # 50 fm * I Tony Gragg, Lab Supervisor k _ ._ ._ ._ :___ --. ./nc. POST CI :iCE SOX 1056 • #5 PINEWOOD PLAZA DR. t RAI IITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Coats America (MW#1-0) COLLECTION DATE: 8/9/2011 PERMIT #: COLLECTION TIME., 09:15 ADDRESS: RECEIVED DATE: 8/9/2011 RECEIVED TIME., 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST' Sulfate 32.6 mg/L 8/12/11 Chloride 7 mg/L 8/21/11 jmf T. Phosphorus <0.16 mg/L 8/16/11 jdg toc <1.0 mg/L 8/16/11 TDS 115 mg/L 8/10/11 lag metals see attached LOG ID: 1108-136 REPORTED BY: NC CERTIFIED LAB # 50 l i Tony Gragg, Lab Supervisor 94 8-inc, 05 POST OFFICE BOX 1056 5 PINEWOOD PLAZA DR. GRANITE FALLS. iti1ORTH CAROLINA 28630 (828)396-4444 SAMPLE: Coats America (MW#11) COLLECTION DATE: 8/9/2011 PERMIT # COLLECTION TIME: 09:30 ADDRESS: RECEIVED DATE., 8/9/2011 RECEIVED TIME: 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Sulfate 128 mg/L 8/12/11 Chloride 16 mg/L 8121/11 jmf T. Phosphorus <0.16 mg/L 8/16/11 jdg toc 2.35 mg/L 8/16/11 TDS 299 mg/L 8/10/11 lag metals see attached LOG ID: 1108-137 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor t POST OFFICE BOX. ': 56 • 115 PINEWOOD PLAZA DR. GRAM T = FALLS. NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Coats America (MW#12) COLLECTION DATE: 8/9/2011 PERMIT #: COLLECTION TIME: 09:45 ADDRESS: RECEIVED DATE: 8/9/2011 RECEIVED TIME: 13:25 REPORTED: 8/30/2011. ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Sulfate 11.1 mg/L 8/12/11 Chloride 8 mg/L 8121/11 jmf T. Phosphorus <0.16 mg/L 8/16/11 jdg toc 3.19 mg/L 8/16/11 TDS 595 mg/L 8/10/11 lag metals see attached LOG ID: 1108-138 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor ;4 _ - _ _ . __ __ .inc. TECH POST OFFICE BOX 1056 ° #5 PINEWOOD PLAZA DR, GRANITE FALLS. NORTH CAROLINA 28630 (828)396-4444 SAMPLE. Coats America (MW#13) COLLECTION DATE: 8/9/2011 PERMIT* COLLECTION TIME: 10:00 ADDRESS: RECEIVED DATE., 8/9/2011 RECEIVED TIME: 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Sulfate <10.0 mg/L 8/12/11 Chloride 123 mg/L 8/21/11 jmf T. Phosphorus . <0.16 mg/L 8/16/11 jdg toc 3.08 mg/L 8/16/11 TDS 471 mg/L 8/10/11 lag metals see attached LOG ID: 1108-139 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor Y, ,COST OF=ICE BOX -L55 a #5 PINEWOOD PLAZA DR. GRANITE: FALLS. NORTH CAR UNA 29630 (828)396-4444 SAMPLE: Coats America (MW#14) COLLECTION DATE: 8/9/2011 PERMIT #: COLLECTION TIME: 10:15 ADDRESS: RECEIVED DATE: 8/9/2011 RECEIVED TIME: 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Sulfate <10.0 mg/L 8/12/11 Chloride <5.0 mg/L 8/21/11 jmf T. Phosphorus <0.16 mg/L 8/16/11 jdg toc 4.24 mg/L 8/16/11 TDS 457 mg/L 8/10/11 lag metals see attached LOG ID: 1108-140 REPORTED BY: NC CERTIFIED LAB # 50 fo Tony Gragg, Lab Supervisor 4 WHTER°:. ECH ln,`. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORT! i CAROLINA 2863E (828)396-4444 SAMPLE: Coats America (MW#15) PERMIT #. ADDRESS: COLLECTION DATE: 8/9/2011 COLLECTION TIME: 10:30 RECEIVED DATE: 8/9/2011 RECEIVED TIME. 13:25 REPORTED: 8/30/2011 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST -Sulfate 156 mg/L 8/12/11 Chloride <5.0 mg/L 8/21/11 jmf T. Phosphorus <0.16 mg/L 8/16/11 jdg toc 3.52 mg/L 8/16/11 TDS 460 mg/L 8/10/11 lag metals see attached LOG 1D: 1108-141 REPORTED BY: NC CERTIFIED LAB # 50 foot 3 Tony Gragg, Lab Supervisor Method SM 20Ed 4500-H PH WORKSHEET Analysis Date Time Sample ID Collection Date Time Results SU's Analyst -4— / ,3o Buffer4.00 **** ***** 2, Buffer 10.00 ***** ***** Of Ch 63 Buffer 7.00 QC ***** ***** f0o ***** Slope Efficiency ***** ***** 6 3 Am A J-2 l q Ga S, 6 3X �`� 7.v- -( I t9930 0. 3 W- 106b (0.3 6 Eb Z630 , LSZ ,01 BUFFERS: Fisher 4.00 LOT # 1,05314 EXP 08/2012 7.00 LOT # 104056 EXP 06/2012 NON REPORTABLE FOR NPDES !` - -T T A 1 - A - T TT /1 Tl T\ T !1 10.00 LOT 9 104216 EXP 07/2012 —T TT T T! A TT In i n 1 CST T]n a O Page 1 of 2 UROUTEST Laboratory Report Lab Location R' - Lab,Location 'C' Lab Location 'W NC/WV Cert.#: 067 NC/DW Cert.#: 37731 NC/WV Cert.#: 103 NC/DW Cert.#: 37733 NCM/W Cert.#: 075 NC/DW Cert.#: 37721 6701 Conference Dr, Raleigh, NC 27607 8300 Ramada Dr, Suite C2, Clemmons, NC 27012 6624 Gordon Rd, Unit G, Wilmington, NC28411 Ph: (919) 8344984 Fax: (919) 834-6497 Ph: (336) 766-7846 Fax: (336) 766-2514 Ph: (910) 763-9793 Fax: (910) 343-9688 3 Project No.: 01 Project ID: COATS AMERICA MONITORING WELLS --- Prepared for --- Jon Gragg Water Tech Labs PO Box 1056 Granite Falls, NC 28630 Report Date: 8/19/2011 Date Received: 8/10/2011 Work Order #: 1108-00759 Cust. Code: WATERT Cust. P.O.#: INCL TOC RESULTS No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 001 MONITORING WELL #2 8/9/2011 9:00 GW Grab 4 +1- 2 deg C Test Performed Method Results ------------ Analyzed T----- Lab Loc Date Time Qualifier Total Organic Carbon 5310C <1.0 mg/L R 8/16111 10:43 No. Sample ID 002 MONITORING WELL #10 Date Sampled 819/2011 Time Sampled Matrix 9:15 GW Sample Type Grab Condition 4 +1- 2 deg C Test Performed Method Results ------------ Analyzed Lab Loc Date -------- Time Qualifier Total Organic Carbon 5310C <1.0 mg1L R 8/16111 10:43 No. Sample ID 003 MONITORING WELL #11 Date Sampled 8/9/2011 Time Sampled Matrix 9:30 GW Sample Type Grab Condition 4 +/- 2 deg C - - - - --- Analyzed -------- Test Performed Method Results Lab Loc Date Time Qualifier Total Organic Carbon 5310C 2.35 mg/L R 8116/11 10:43 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 004 MONITORING WELL #12 8/9/2011 9:45 GW Grab 4 +1- 2 deg C - - - - --- Analyzed -------- Test Performed Method Results Lab Loc Date Time Qualifier Total Organic Carbon 5310C 3.19 mg/L R 8116111 10:43 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition nns MONITORING WFI 1 #13 819/9011 10.00 rW Grab 4 +l- 2 deg C - - - --- Analyzed -------- Test Performed Method Results Lab Loc Date Time Qualifier Total Organic Carbon 5310C 3.08 mg1L R 8116/11 10:43 0 0 Telephone: (919) 834-4984 Fax: (919) 834-6497 iIG`'TEST 6701 Conference Drive Raleigh, NC 27607 Telephone: (919) 834-4984 Fax: (919) 834-6497 Laboratory Report Page 2 of 2 NC/WW Cert. #: 067 NC/DW Cert. #: 37731 Work Order #: 1108-00759 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 006 MONITORING WELL #14 8/9/2011 10:15 GW Grab 4 +/- 2 deg C Test Performed Method - - --- Analyzed Results Lab Loc Date -------- Time Qualifier Total Organic Carbon 5310C 4.24 mg/L R 8/16/11 10:43 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 007 MONITORING WELL #15 8/9/2011 10:30 GW Grab 4 +/- 2 deg C - - - --- Analyzed --- ---- Test Performed Method Results Lab Loc Date Time Qualifier Total Organic Carbon 5310C 3.52 mg/L R 8116/11 10:43 Reviewed by: r for Tritest, Inc. e+���eoa®atttP�i RESEARCH ArNAlyTICAI ,,,`�`G��' z. UbORAT®RiES INC. rNC Analytical/Process Consultations • Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by SK -JC Lab Sample Number --------------------- 710003 Parameter Storet # Results Sulfate (00945) <10.0 mg/l Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.107 mg/l Cadmium,Tot (01027) <0.001 mg/1 Chromium, Tot (01034) <0.005 mg/1 Calcium,Tot (00916) 25.4 mg/l Lead,Tot (01051) 0.029 mg/1 Magnesium, Tot (00927) 13.7 mg/l Manganese,Tot (01055) 0.832 mg/l Nickel,Tot (01067) 0.009 mg/l Selenium,Tot (01147) <0.005 mg/1 Sodium,Tot (00929) 10.6 mg,/l Clients Sample Source Coats American MW2 Number Time Collected (Hrs) 0900 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com ®'t�mesa'�e�etee aw RESEARCh 6&ANA1YTiCA[..eG`�F`.....�,rr�. I-AbORATO&S, INC. cc NC #34 z - Analytical/Process Consultations s CTO !PIE0 AN�4� Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by SK -JC Lab Sample Number -------------------- 710004 Parameter Storet # Results Sulfate (00945) 32.6 mg/l Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.026 mg/l Cadmium,Tot (01027) <0.001 mg/1 Chromium,Tot (01034) <0.005 mg/1- Calcium,Tot (00916) <0.500 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) <0.500 mg/1 Manganese,Tot (01055) <0.005 mg/1 Nickel,Tot (01067) <0.005 mg/1 Sel.enium,Tot (01147) <0.005 mg/l Sodium,Tot (00929) 43.6 mg/1 Clients Sample Source Number Time Collected (Hrs) Coats American MW10 0915 P.O. Box 473 • 106 Short Street ^ Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com- ,�+s0e m, uo�awi F RESEARCH LANA1YTiCA1 .�``c,� trT���♦ LAb®RA►TORIES INC.0. NC #34 Zs ' Analytical/Process Consultations Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by Lab Sample Number ----------------- 710005 Parameter Storet # Results Sulfate (00945) 128 mg/1 Arsenic,Tot (01002) Barium,Tot (01007) Cadmium,Tot (01027) =T Chromium, Tot (01034) Calcium,Tot (00916) Lead,Tot (01051) Magnesium,Tot (00927) Manganese,Tot (01055) Nickel,To.t (01067) Selenium; Tot (011.47) Sodium,Tot (00929) <0.005 mg/1 0.107 mg/l <0.001 mg/l <0.005 mg/l • 25.3 mg/l Number Time Collected (Hrs) 0930 <0.005 mg/l 8.82 mg/l 0.639 mg/1 <0.005 mg/1 <0.005 mg/l 69.1 mg/l 0 P.O. Box 473 • 1.06 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 . www.randalabs.com RESEARCh & ANA1YTiCA1 �e�G�............ cly Atyp����i� LAbORATOMESO INC. = C'2 -fie •— o:CA NO Analytical/Process Consultations +, i� rFD AJANo-`� Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by SK -JC Lab Sample Number -------------------- 71000G Parameter Storet # Results Sulfate (00945) 11.1 mg/1 Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.120 mg/1 Cadmium,Tot (01027) <0.001 mg/l Chromium,Tot (01034) <0:0'05`,mg/1 Calcium,'Tot (00916) 50.8 mg/l , Lead,Tot (01051) <0.005 mg/1 -Magnesium,Tot (00927) 10.3 mg/1 Manganese,Tot (01055) 2.43 mg/l Nickel,Tot (01067) 0.010 mg/1 Selenium,Tot (01147) <0.005 mg/1 Sodium,Tot (00929) 184 mg/1 -------------------- Clients Sample Source Coats American MW12 NUMber Time Collected (Hrs) 0945 P.D. Box 473 • 106 Short Street , Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.rand.alabs.com ' �e44�asaeaUaP�i RESEARCh ANA[yTiCA UbORATORiES, INC. NC �'`bc��' •• �T��,°`a JY �a � • O M Analytical/Process Consultations e V Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by SK -JC Lab Sample Number -------------------- 710007 Parameter Storet # Results Sulfate (00945) <10.0 mg/1 Arsenic,Tot (01002) <0.005 mg/1 Barium,Tot (01007) 0.073 mg/l Cadmium,Tot (01027) <0.001 mg/1 Chromium,Tot (01034) <0.005 mg/l • Calcium,Tot (00916) 23.9 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 16.2 mg/1 Manganese,Tot (01055•) 0.757 mg/l Nickel,Tot (01067) <0.005 mg/1 Selenium,Tot .(01147) <0.005 mg/1 Sodium,Tot (00929) 105 mg/1 Clients Sample Source u e Time Collected (Hrs) -------------------- Coats American MW13 1000 P.O. Box 473 • 106 Short Street . Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com RESEARCh 8L ANA1YTiCA[ I-AbORATORVS, INC. Analytical/Process Consultations .sv1111811"4 Ojai co ®✓� �{�y4 .U) rys r i 4 ���',9;o PEED ANP`, •`9 Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056, Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26/11 Analyses Performed by SK -JC Lab Sample Number -------------------- 710008 Parameter Storet # Results Sulfate (00'945) <10.0 mg/1 Arsenic,Tot (01002) <0.005 mg/l Barium,Tot (01007) 0.122 mg/l Cadmium,Tot (01027) <0.001 mg/l Chromium,Tot (01034) <0.005 — /1 -_-' Calcium,Tot (00916) 74.2 mg/1 Lead,Tot (01051) <0.005 mg/l Magnesium,Tot (00927) 41.5 mg/l Manganese,Tot (01055) 1.05 mg/l Nickel,Tot (01067) <0.005 mg/l Selenium,Tot (0.1147) <0.005 mg/l Sodium,Tot (00929) 57.7 mg/1' Clients Sample Source Nuffiber Time Collected (Hrs) -------------------- Coats American MW14 1015 P.O. Box 473 ® 106 Short Street . Kernersville, North Carolina 27284 • 336-996-2841 • Fax 336-996-0326 www.randalabs.com 6 RESEARC & ANAlyTICAI LkORATWEs, INC. Analytical/Process Consultations ;%`rv431112,f14, ♦�,,�6 . �.chlto sue._ :cam. NC Qooi Water Tech Labs. Inc. Date Sample Collected 08/09/11 P.O. Box 1056 Date Sample Received 08/12/11 Granite Falls, NC 28630 Date Sample Analyzed 08/12/11 Attn: Joe Gragg Date of Report 08/26./11 Analyses Performed by SK -JC Lab Sample Number ----------------- 710009 Parameter Storet # Results Sulfate (00945) 156 mg/l Arsenic,Tot (01002) <0.005 mg/l Barium,Tot (01007) 0.140 mg/l Cadmium,Tot (01027) <0.001 mg/l �CYiromium,�Tot (01034) <0.005 mg/1 Calcium,Tot (00916) 73.4 mg/l Lead,Tot (01051) <0.005 mg/1 Magnesium,Tot (00927) 31.2 mg/l Manganese,Tot (01055) 1.49 mg/l. Nickel,Tot (01067) <0.005 mg/l ScicniUM, Tot (011=7i <0.00S mg/1 Sodium,Tot (00929) 61.7 mg/1 -------------------- ien s Sample Source Number Time Collected (Hrs) 1030 P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841• Fax 336-996-0326 www.rsndalabs.com G CLIENT rr a 5 Pinewood Plaza Drive • P.O. Ix 1056 Granite Falls, NC 28630 Phone (828) 396-4444 • Fax (828) 396-5761 PHONE: A� o,6 tj C IS7S 2 TYPE SAMPLE: No. LOCATIONS: $2S'766-V/)1 6 X 3 3 f g SAMPLER NAME: OtA PLE LOCATION FACILITY NAME SAMPLE COLLECTION SAMPLE TYPE CONTAINERS ANALYSIS REQUIRED DATE TIME TEMP °C GRAB / COMPOSITE NO. PLASTIC I GLASS G 7 • -,PG- I% Zd ► �( �"1 �f /�3a G- L P4' V _ e/ G- 7 P4- G. AA) , 13 16;oD C%- 7 P-4 RELINQUISHED BY: DATE: TIME: RECEIVED BY: u �� �a �rv��i`l DATE: � i l TIME: 2 00 RELINQUISHED BMY: DATE: TIME: REC ED BY: .o,�-�� DATE: TIME: PRESERVATION: [ ] Cool 4°C - BOD, TSS [ ] Cool 40C - pH<2 w/ H2SO4- NH3 1 2 [ ] Cool 40C - Na2S203 - Coliform Bacteria, NH3 Sample Temperature at Lab (°C) 1 - Chlorine Residual mg/I 2 - Chlorine Residual mg/I NC CERTIFIED LAB # 50 GROUNDWATER QUALITY MONI COMPLIANCE REPORT FORM Facility Name: k �s fH>�E r?'SEU JFgOlfR ° SUBM T FOFTM �ON YELL W PAPER ONLY RING: 2,L Q 5 21 Well Identification Number (from Permit): M 60" z- For Groundwater Treatment Systems Well -Depth: "l�7 it. Well Diameter-: in. Check One: ❑ Influent (+a8) Screened Interval: �/ft it. to //n' l�3 it. ❑ Effluent {J9) Depth to Water Level: 2 fr % ft. below measuring point. Measuring Point (M.P.) It. above land surface. � Relative M.P. Elevation in fit.: (' Gallons of water pumped/bailed before sampling: Date sample collected: Field analysis: pH— _ , Specific Conductance- ' umhos . Temp. C, Odor Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC27699-1636 Phone: (919) 733-39: PERMIT#: W 060©-S(-O' EXPIRATION )ATE: J_-2 61/ Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED < Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other:' NOTE: Values should reflect dissolved and . colloidal concentrations. -// Dale sample analyzed: . 5C A= 13 ct n t j Laboratory Name:—Zd,4+e,- —T c A Certification No. 1; "d PARAMETERS (Samples for metals were collected unfiltered _X_YES ta0 and field acidified COD mg/I Nitrite (NOZ) as N m /I Coliform: MF Fecal g /100m1 Nitrate (NO3) as N _mg/I Coliform: MF Total /100ml Phnsnhnri,s• Tntal ac / 7/ . _/l (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total q-2o- /1 hb mg/I pH (when analyzed) units TOC y-25-- /1 1-6 mg/1 Chloride L4-2o-11 S-, ce? mg/I Arsenic •1•-Ig•- I-J 0.©/ mg/I a Grease nd Oils mg/l Phenol mg/I Sulfate mg/I C�/-L2-/1 ,L3c/ Specific onductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum — mg/I Ba - Barium y-19 0.397 mg/I Ca - Calcium -1 •-f / mg/I Cd - Cadmium'_-( `1={I 4 6.662- mg/I Chromium: Total-T.- 0.012- mg/I Cu - Copper m9 /I Fe - Iron ,� _•__ .1:.:W. mg/I Hg - Mercury ?U1f mg/I K - Potassium!F->,,-.-- - mg/I Mg -Magnesium �� _�/:.�. ;,F. {lrCj, / mg/I Mn - Manganese -1/ 11, 35' ma/I X YES NO) Ni - Nickel /9 -T/ 0.0 / mg/I Pb - Lead-z!-/9J/ a i5+% mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) T F"v, uon �/_1 G-// G U, Od ` !h5/Z ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM r—iA% r j j , nir r,mA i t�ry n s Please. Print Clearly or Type Facility Name o >=6&) Permit Name (if differ t): Facility Address: 1O & 3 fi7 City) (Street) 2 Y �SZ (t r � ,v Count fYi 1 ! l 1 , _((State) tZip) y Contact Person: ' \ �! w' `' Telephone #: 2 S6 ­ 9 /i I _ Well Location/ Site Name: 5 +� 64 _,,, No. of Wells to be Sampled;__. _ Well Identification Number (from Permit): For Groundwater Treatment Systems to Well Depth: / II. Wel�Diameter•: 2 in. Check One: ❑ Influent- (013) Screened Interval: ' / ft. U�f} it. I] Effluent (g9) Depth to Water Level: L% ft. below measuring point. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: S Date sample collected: Field analysis: pH ?, 2- Specific Conductance uMhos Temp. °C, Odor Appearance DEPARTMENT of ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WC9CsQCS�y �,0 EXPIRATION DATE: 15 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: + (= 6 to Laboratory Name: 4 E r^ Tee h Certification No. PARAMETERS (Samples for metals were collected unfiltered_ A YES _f <O and field acidified COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N. Nitrate (NO3) as N � mg%I mg/I Coliform: MF Total /100ml Phosphorus: Total as P.1-5 l 1 r 0, lf` mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate _ m /I 9 Dissolved Solids: Total 4l 20 // I(�S mg/I Al -Alum Aluminum � mg/C pH (when analyzed) TOC �j-2S-ll units Z- to 0 Ba - Barium q::-L 'I - f i `- ct-il LD-e2(3mg/I Chloride L1-26-11 mg/I I 53 mg Ca - Calcitam' _ Cd - Cadmium.'-►9-(_.L_, 0,500 m /I 40,002mg/I g Arsenic q-1 •- f 1 ,—�', <10, aos mg/l Ll Chromium: Tota11�_i 1_' L�, 00,E mg/1 Grease and Oils mg/I Cu.- Copper___ mg/I Phenol Sulfate 22-1l �` mg/I % 3,(� mg/I Fe - Iron __. Hg -Mercury m /I g m /I Specific Conductance uMhos K - Potassium----mg/I Total Ammonia mg/I Mg - Magnesium �._1`j._Il 0,221 mg/I TKN as N mg/I Mn - Manganese --- I```f'l �<0'005' mg/1 A YES NO) Ni - Nickel!cJ-1/ 4.6,66 mg/I Pb - Lead_y'1mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units ,jLc E'I7ii 'I9? �/-1��// L C? �r� iv,y� ��-r-i9•-r� �2, y ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method# certifv that. t0 the hest of MW knnwlarfna and hatiof it,o :nf,..... ,►a.,....,,�. «:.a .� :_ .�:_ __ p ►" C rermittee (or Authorized Ag t) N me and Title - Please print ar Rev. 0312000 Signature of Peutriiles (o ulhorized Agen (Date) 0 GROUNDWATER COMPLIANCE RI Facility Name: t 0 Permit Name (if diff _ ent): Facility_Adoress:� Contact Person: 114 Well Location/ Site Name: - �jh.e N JO, "SUBMIT FORM ON YELLOW PAPER ONLY - Print Clearly or Type r. Telephone #: IE2 W-- `7,, `'b :l i j J =A No. of Wells to be Sampled: ,—_'Z:, Well Identification Number (from_ Permit): -/ For Groundwater Treatment Systems Well Depth: ft. Well Diameter: 2 in. ,t r, Check One: ❑ Influel (98) Screened Interval: / ft. to _ ft. ❑ Effluent i99) Depth to Water Level: __L5-6 ft. below measuring point. _ Measuring Point (M.P_) is: 3y1_ ft. above land surface. Relative M.P. Elevation in ft.:'y Gallons of water pumped/bailed before sampling: �_ Date sample collected: Field analysis: pH --�<`7—, Specific Conductance uMhas ,[� Temp. °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATERSECTION 1636 MAIL SERVICE CENTER PERMIT #: 0 0660S 6 Non -Discharge NPDES EXPIRATION DATE: --,5 La TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 1 p iLJ Laboratory Name: GJ r T-c h _ Certification No. S 6 PARAMETERS (Samples for metals were collected unfiltered--X_YE5 __._8t0' and field acidified COD mg/I Nitrite (NO2) as N m /I Coliform: MF Fecal g /100m1 Nitrate (NO3) as N m /I Coliform: MF Total _ /100m1 Phnsnhnnrc• TnfnI /' ,76--/l (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total 1-715`// mg/I pH (when analyzed) units TOC I-f ` 2.5-11 'm 9 /I Chloride �,1` 2 0 -1 f �J. 3 mg/I Arsenic ��-19- 11 . mg/I Grease and Oils mg/I Phenol mg/I Sulfate !1-22-- I I mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate _ mg/I Al -Aluminum mg/I Ba - Barium ` ` 1 / Ca - Calcium )9'-%/ /1, Z mg/I _ Cd - Cadmium_ CD •OOZ mg/I Chromium: Total `-I�%_:_'.! ��:oos mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium-­mg/I Mg - Magnesiumf•� mg/I Mn - Manganese J_/ - 6,05t/ _ ma/I Signalure of Pem-Iitiee ,A —YES NO) Ni - Nickel' -/9`1/ c .moo mg/I Pb - Lead 19 2'-// mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) l iviy,7 c. /) -9e) ,Sep r .`[� v✓L % � � Z. ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = method # = GROUNDWj < j I Fa-,4<. 15 COMPLIANT FACILITY INFORf� Facility Name: Permit Name.(if difl Facility Address: ' ConIcnr)tact Person: Well Location/ Site Name: S -4'v 1,61 r FF l ,1,ol�, SUBMIT FORM ON YELLOW PAPER ONLY )RING: Please Print CIE C I%.- ry pZ County ? Telephone #: No. of Wells to be A) Co�t`✓t,t�w- Well Identification Number (from Permit): a 40 - / 2- _ Well Depth: {=.2 ft. Well Diameter: '� in. For Ground,_ Check One: ❑ IntlUetzt_� Screened Interval: "'f4- It. to---=-fL—fL [] Effluent (39) ` Depth to Water Level: 1., ft. below measuring point. Measuring Point (M.P.) is: 2- Cw It. above land surface. Relative M.P. Elevation in fit.: Gallons of water pumped/bailed before sampling: l n1 Date sample collected: Field analysis: pH 6 '69 , Specific Conductance ' uMhos . Temp. >'7 °C, Odor Appearance 'Vf Cb. 4 1eaa rge DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: +ZO UIC OPERATION BEING MONITORED n Remedialion: Infiltration Gallery Field Remedialion: Distributor Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. y 1 Date sample analyzed: Laboratory Name: LJ' 4+c'r 7F, Certification No. PARAMETERS (Samples for metals were collected Unfiltered YES. : fC) and field acidified COD mg/I Nitrite (NO2) as N _. _._ mg/I Coliform: MF Fecal /100ml Nitrate N as N _. mg/I Coliform: MF Total /100m1 (01 Total as i 5-.h'lI f}��fmg/I (Note: Use MPN method for highly turbid samples) Orthophosphate _-_ _ mg/I Dissolved Solids: Total yt-2bfil LO mg/I Al - Aluminum m /I pH (when analyzed) `t �-2-S- units Ba - Barium 4 -/9--1 O, r�i mg/I TO t I 2 4E) mg/I Ca - Calcidm 19-•1 J _ S3 mg/I Chloride mg/I Cd - rtltri �,/- I�-! �- _ �a "e2-mg/I Arsenic y-J�r -I ! .� -Oc mg/I �C far,r ifa ,: Total 9 : L en, ob6- mg/I Grease and Oils mg/I Cu - Copper mg/I Ph _.- -_. —YES. NO) Ni - t t?a'''l`) li d►,��, tv mg/I Pb Zn - ZIn mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ��� iy:yi �/ •19 J/ / 7 � eno Sulfate 'L1�"22: ►i %"- mg/I Fe - Iron -- m9/I ORGANICS: (GC,GC/MS,HPLC) Specific Conductance g/I uMhos Hg - Mercury K - Potassium mg/I mg/I (Specify test and method #. Attach lab report.) Report Total Ammonia mg/I Mg- Magnesium r{�t` �i l%-T mg/I Attached? Yes1 No (0) VOC TKN as N mg/I Mn - mg/I :method #)_ method # = method # = r ► . _ . ... -.._ _.. ..21- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM rsAi,lu r T rrvr r+mfa i iUry Please Print Clearly or Type Facility Name: l• �s Z mIrr/tC4 Permit Name (if different Facility Address: 6 BOX 34 Se 4/, iO-L (Street) � --- (City) ai) ZL Z--Rip) County 9 ) Contact Person: ` - _ 1''L • Telephone #:' Z%' Well Location/ Site Name: 2.A—P161 No. of Wells to be Sampled: — Well Identification Number (from Permit): filzc) / For Groundwater Treatment ::yslems Well Depth: 1 ft. Well Diameter 2 in. Check One: E] lnfluen; (98) Screened Intel: ft. to ft. E] Effluent 99 Depth rva th to Water Level: `�' �/ ff. below measuring point. Measuring Point (M.P.) is: 4J_4 it. above land surface. Relative M.P. Elevation in ft.:'_ Gallons of water pumped/bailed before sampling: 2. r7, Date sample collected: Field analysis: pH A y Specific Conductance uMhos Temp. °C, Odor Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: (91.91733-39: PERMIT #: j��EXPIRATION DATE: Jam` L'6 i Non -Discharge UJC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED V Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: - -5A Laboratory Name: WA 01, Certification No. - PARAMETERS (Samples for metals were collected unfiltered_A YES ?•f0 and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as i,_ mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total L/­?&-J1 D1 mg/I Al - Aluminum - mg/I pH (when analyzed) TOC y' 1 / units Z.3C► mg/I Ba - Barium 4/ -1 -1 % Ca - Calcium ` `/ ` i/_...__ c�•a'3 smg/I /�L Chloride it mg/I Cd - Cadmium -1/ ._._.: mg/I &,a2-mg/I Arsenic _ V -19 -1 1 -e66- C6 r I Chromium: Total �I -/`i_ !_ t6,c}�"mg/l Grease and Oils mg/I Cu - Copper __ _ • mg/I Phenol Sulfate '�j.• 2 2- g - Z-mg/I __..__ Hg = (Mercury mg/I mg/I Specific Conductance uMhos K - Potassium--,mg/I Total Ammonia mg/I Mg - Magnesium [ j :_. 1 _ /b, Jr mg/I TKN as N mg/I Mn - Manganese LT;-_. 0 �. oz>f� mg/I GW-59 Rev. 03/2000 Signature of r Authsrize 1K YES NO) Ni -Nickel. mg/I Pb - Lead �1-19-1-/ �L r�cS mg/I Zn -Zinc • mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration �Units) far ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : method # = or C method # = method # _ 'SUBMIT FORM ON YELLOW PAPER ONLY - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION j Please Print Clearly or Type Facility Name: C (1 K _ Permit Name (if differe Facility Address: (Street) —�-- 9 County (city) r /. ` i 7 to e) aim (Zip) Contact Person: Telephone #: P2V' f Well Location/ Site Name: S�µt'rl+�t�rd /t+ No. of Wells to be Sampled:,.✓� ({ruin Pump)__ Well Identification Number (from Permit): Mk)-) i For Groundwater Treatment Systems Well Depth: it. Well Diameter: in. Check One: ❑ lnfluetat (98) Screened Interval: y'��f ft. Co 'rfr9- ft. ❑ Effluent (09) Depth to Water Level: `��� ft. below measuring point. Measuring Point (M.P.) is: ?4 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling:_ Date sample collected:.l' Field analysis: pH— , Specific Conductance umhos Temp. -°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: &)600EXPIRATION DATE: S- :E)ll Non -Discharge U IC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon Remedialfon: Infiltration Gallery Spray Field Remediation: Rolary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: - LSC,r Air/ 4 uJ Laboratory Name: 011 e `TEc Certification No. .Sr PARAMETERS (Samples for metals were collected unfiltered_OYES -._?':O and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N _ mg/I Coliform: MF Total /100ml Phosphorus: Total as i'_ =S`/' 0.2mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total y-25-tI 33 2 mg/I Al - Aluminum __ mg/I pH (when analyzed) units Ba - Barium -1 -1 / mg/I TOC `�`2;5=// Z.r'12- mg/I Ca - Calcium �r­ /y-ll mg/I Chloride q-2D--11 mg/I Cd - Cadmium �_1 6 `!� �r°�� mg/I Arsenic -1!3 -1% mg/I Chromium: Total `_�=__ �•�o mg/1 Grease and Oils mg/I Cu - Copper ____. mg/I Phenol Sulfate tf '- �2� 1 mg/I -K16 mg/I Fe - Iron Hg - Mercury rhg/I mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia m h 9 M Magnesium ;�ti 9 - 9 Y3r 2 mg/I TKN as N mg/I Mn - Manganese -,Uf-rr' Ga% 63 mg/I GW-59 Rev. 0312000 Permittee (or t Signature of Peuailic;e lie - —YES NO) Ni- Nickel V -1 mg/I Pb-Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) S'(-' ,"Vff7 Iv i 460&-1f'%jL ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC : 'method # = */(-- U t" method # _ method # _ ~9f/ n GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if diff Facility Address:- 01;4rt6A, Contact Person: Yh, I Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY - Please Print Clearly or Type r iCt+ %Sz County - (zip) Telephone #: No. of Wells to be Sampled:�;� Well Identification Number (from Permit): /ram/rl `/r7 For Groundwater Treatment Syslems Well Depth: l it. Well Diameter. '2- in. Check One: ❑ Influen'i (98) Screened Interval. ✓`bf- it. to ✓"0 it. p Effluent (99) Depth to Water Level: 3 fi. below measuring point. Measuring Point (M.P.) is: A✓6'^ft. above land surface. Relative M.P. Elevation in ft.: _ Gallons of water pumped/bailed before sampling: d7iDate sample collected: Field analysis: pH , Specific Conductance ' uMhos . Temp. __1__1C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phnna• 14101 719_'lo- PERMIT#:Gc��OO�rS/r'� EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X_ Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. J Date sample analyzed: 5 Ak s- 6 -/ 0 Laboratory Name: - Ll rw,F1 v TecA Certification No. !i PARAMETERS (Samples for metals were collected unfiltered_X YES ;:() and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Coliform: MF Total /100ml Phosphorus: Total as r. ->-SIl L6,11, mnn (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total �1-26=11 36b mg/I pH (when analyzed) units TOC _4` 2,5 -1 i /• 83 mg/I Chloride it`20-)l /,<-,6 mg/I Arsenic -f5"`II Ze.156s, mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific onductance LiMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate _ mg/I Al - Aluminum mg/I Ba - Barium L? �5�-I•/ 6.123 mg/I Ca - Calcium "� /✓ __.•_ _ gY, i mg/1 Cd - Cadmium t ` 9-Il____ _ �6•�o a mg/I Chromium: Total_t; �d•oa5 mg/1 Cu - Copper _.__ : mg/I Fe - Iron - mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium Ir _ 444C4s mg1l _ Mn - Manganese�. _. .:7S -'1 ma/I Signature of PeIiisiltee YES NO) Ni - Nickel_ `l �� ✓/ �- ycf� mg/I Pb -Lead ze.,-e — mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) - �zry ►rr -� - /� �d1 ��� of>: L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = method # = Li W-:t0A [ O MPLL&NCE REPORT FORM Permit # W& OL051 (Submit one each monitoring period with GW-59 forms) 1 Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) YES NO be. submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 9 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? Ifthe answer is -Yes'; contact the Regional Ofce forguidance. / 4 Are any monitored constituents equal to or above the established standards? YE> NO If the answer to question 4 is NO; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentrations) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO" skip to section B. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding j standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility- Failure to do -so may subject the pennittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. i hereby acknowledge that a above irifoFrr�iatlon yvas,evalWAR- Ind nfo—dWon-5ubmitted .the. report (Gompi , Report GUY 59A,,,�f-' '. s and.:.complete�o�Fie�est of my kriowlec}ge ;�. .� Signat of Permittee r AutHorrized Agent) Date G«'-59A 12/8/2003