WQ0005763_Annual Report_20130228

P_�_
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
• Was a certification form submitted? VeS
• Was distribution conducted during the reported year? qef
• How many drytons were distributed? S I.DT
• Were the distributions within the permitted amount?
• Were recipients information listed?'y-s
• Did it indicate compliance? tefr
• Was form complete? ��eS
• Was it signed by the appropriate people? Y.2J
2. Monitoring
• Were the analyses conducted at the required frequency? ,&J
• Were the metals analyses reported on the Residual. Sampling Summary Form? YIelr
• Were the results reported in mg/kg?ye r
• Were the metals within ceiling concentration permit limits? Y e.S'
• Were the metals within monthly average concentration permit limits? �.-e-F
• If no, were the lab analyses attached?
• Were all the required parameters tested? 1,40 -SAP— iwZ S5 v nJ
• Was TCLP analysis conducted? Y`e3 owns P46,* `r-T
• Were the TCLP contaminants within regulatory limits?7 e—f'
I Pathogen and Vector Attraction Reduction
• Was a signed copy of the Pathogen aOn;Vector Attraction Re(jAction Form submitted? v
• Did the form indicate the �d of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction reduction option used?
• Was the appropriate documentation° show pathogen and vector attraction reduction included in the report?
• Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
4. General
• Was the report in the proper format?
• Were any parts of the annual report missing. N
• Was the report submitted on time? YES'
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Class A Pathogen Review
To be Class A, residuals shall meet either fecal coliform density or salmonella density.
Fec 1 coliform dens'
• Was the sampling conducted at the required frequency? %jam'
• Were multiple samples taken?
• Was each sample less than 1000 MPN/gram of total solids?
Or "
Salmonella density
• Was the sampling conducted at the required frequency?
• Were multiple samples taken?
• Was each sample less than 3 MPN/4 grams of total solids?
To be Class A, residuals shall meet one of the following alternatives:
Alternative 1 - Time/Temperature
• Were the residuals maintained for correct time and temperature?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
Alternative 2 - Alkaline Treatment
• Were logs submitted showing time and temperature?
• Was the pH raised to 12 or greater and maintained for 72 hours or longer?
• Was the temperature 52°C (126°F) for 12 hours or longer white the pH was 12 or greater?
• Were logs submitted showing time and pH?
• Was the temperature corrected to 25°C (77°F)?
Alternative 3 -Prior Testing for Enteric Viruses/Viable Helminth Ova
• Were residuals analyzed prior to the pathogen reduction treatment?
• Prior to treatment were, the density of enteric viruses less than one Plaque -forming Unit per four grams of
total solids; or
was the resultant density after pathogen treatment less than one Plaque -forming Unit per four grams of
total solid?
OR
• Prior to treatment were, the density of viable helminth ova less than one per four grams of total solids; or
was the resultant density after pathogen treatment of viable helminth ova less than one per four grams of
total solids?
• Were the operating parameters documented to the satisfaction of the Division?
Alternative 4 -No Prior Testing for Enteric Viruses/Viable Helminth Ova
• Was the density of enteric viruses less than one Plaque -forming Unit per four grams of total solids at the
time the residuals were prepared for sale or given away?
OR
Was the density of viable helminth ova less than one per four grams of total solids at the time the
residuals were prepared for sale or given away?

Alternative 5 Process To Further Reduce Pathogens
PFRP Composting
. Were the within -vessel method or static aerated pile methods used?
Was the residuals temperature maintained at 55°C (131°F) or higher for three consecutive days or longer
in the within -vessel method or static aerated pile method?
OR
• Was the windrow composting method used?
• Was the residuals temperature maintained at 55°C or higher for 15 consecutive days or longer in the
es during this time?
windrow method, and the windrow turned a minimum of five timrr __ ��` JG 2
PFRP Heat Drvin� hot ases and mpis e c ntent of residuals. reed � �s C-4eck
Was-the-xes duals dried by direct or direct with g , s sQ/.`�s ��e "'� �"��
�a e�jcl� 3/q 1rL c/o S'a/,-dS Zga/G QT� b 1 feck5- — Znd e-A—k h^4P now j�
/ 10% or lower. " • 0
Drd�tlTe %rrip`erature of the residuals- or -the of"tlie-wet~bulb t peratur� of the gas in contact with the
residuals as they leave the dry`r exe teed 80°C (176°F)?
----` ' l z
PFRPHeat'Treatment
® Were the residuals liquid during treatment? °/° 50/: �s ��►{" /°'
Were the residuals heated to a temperature of 180°C (356°F) or higher, for 30 minutes?
PFRP Thermophilic �;erobic Digestion
• Were the residuals liquid during treatment?
Was it an aerobic process with agitation?
Was the mean cell residence time 10 consecutive days at 55°C (131°F) to 60°C (140°F)?
PFRP Beta Rav Irradiation
rays at dosages* at least 1.0 megarad at room temperature
Were residuals radiated with beta
[approximately 20°C (680F)]?
pFup Gamma Rav Irradiation
• Were residuals radiated with gamma rays from certainapp ox mately 20°C (681; at
F)]?and Cesium 137
dosages of at least 1.0 megarad at room temperatur [ PP
PFRP Pasteurization
Was the temperature of the residuals maintained at 700C (158°F) for 30 minutes or longer.

14-Day Aerobic Process
• Were residuals from aerobically digested treatment (Inspection)?
• Were the residuals treated for 14 days?
• Was the residuals temperature higher than 400C (104T) for the 14-day period?
• Was the average residuals temperature higher than 45°C (113°F)?
Alkaline Stabilization f.
• Was the pH of the residuals raised to 12 or higher by the addition of alkali?
• Did the pH of residuals remain at 12 or higher for two hours without the addition
of more alkali?
• Did the pH of residuals remain at 11.5 or higher for an additional twenty-two
hours without the addition of more alkali?
• Was the pH corrected to 250C (770F)?
iniz-of Stabilized Residuals
• Does the residuals contain any unstabilized residuals?
• Were the residuals mixed with any other materials? V 0
• Were the residuals dried to 75% total. solids? Y�JJ -
Drying of Unstabilized Residuals
• Were the residuals mixed with any other materials?
• Were the residuals dried to 90% total solids?.'
Injection
• Was there any significant. amount of residuals on land surface one hour after
injection (Inspection)?
• Was injection done on pasture or hay field?
• Was injection done at time that crop was growing?
• If Class A with respect to pathogen, were residuals injected within eight hours
after discharge from pathogen treatment?
Incorporation
• Were the residuals incorporated into the soil within six hours after application?
• Was incorporation done on pasture'or hay field?
• Was incorporation done at time that crop was growing?
• If Class A with respect to pathogen, were residuals incorporated within eight

Utilization Agreement
(a) By signature and agreeing to accept the bulk class A residuals it is recognized that the
application of Class A residuals is allowed under the conditions of this agreement. The
application of these Class A residuals is considered the beneficial reuse of a waste
under 15A NCAC 02T.1100. The application of these Class A Residuals to the land
has been deemed permitted under 15A NCAC.1103(4) provided the conditions of this
agreement are met. Any action resulting in the damages to surface waters or -
groundwater caused by failure to follow the conditions of the agreement is subject to
enforcement action by the NC Division of Water Quality.
The person or entity accepting the Class A residuals shall to the best of their knowledge meet the
following application requirements: Application of the bulk residuals shall -not be applied to the
land under the following conditions:
a. If it becomes known that the application adversely affects a threatened -or endangered species
listed under section 4 of the Endangered Species Actor its designated critical habitat:
b. If the application causes prolonged nuisance conditions. _ _ --
c. If the land fails to assimilate the bulk residuals or if the application causes the contravention
of surface water or groundwater standards. -
d. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that runoff
of the residuals would occur.
e. Within the 100 tear flood elevation unless the bulk residuals are injected or incorporated
within a 24-hour period following the residuals land application event. Flood elevation information is is available at http://www.ncfloodmgps.com/default swf
f. During a measurable precipitation event (i.e. > .0 P per hour) or within 24 hours following a
rainfall event of 0.5 inches or greater in a 24 hour period. Any emergency residuals land =--
application measures shall first be approved in writing by the Division.
g. If the slope for land is greater than 10 percent when bulk liquid residuals are surface -applied, = and if the slope of the -land is greater than 18 percent when bulk liquid residuals are injected or- -
-incorporated._-
h. If the pH is not maintained in the soil, residuals, and lime mixture, greater than 6.0, on land
application sites onto -which residuals are applied. Residuals may a applied to these sites
provided'that a sufficient amount of lime is also applied to achieve a fmal=pH of the soil
mixture .of at least 6.0, or if an agronomist provides information indicating that the pH of the
soil, residuals, and lime mixture is -suited for the specified crop type.
i. If the land does not have an established vegetative cover in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the -Department of
Agriculture and Consumer Services, the Natural Resource Conservation Service, or other
agronomist unless the bulk residuals are incorporated within a 24-hour period following the
residuals application event or injected.
j. If the vertical separation of the seasonal high water table and the depth of residuals application
is less than one foot.
k. If the vertical separation of the depth to bedrock and the depth of residuals application is less
than one foot.

m. Application of bulk residuals shall not occur within 100 feet of a public or private water
supply source.
n. Application of bulk residuals shall not occur within 25 feet of surface waters.
Signed: for Tuckaseigee Water and Sewer Authority
Date GQ 3
Signed: for
Recipient
Date
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ANNUAL SEWAGE SLUDGE REPORT
OF
TUCKASEIGEE WATER AND SEWER AUTHORITY
PLANT # 1-NPDES # NCO039578 (WQ0005763)- -
for the period of January 1, 2012-December 31, 2012
as required by
RECEIVED
FEB 2 83`2013
WATER DUALI i-! SECTION
INFORMATION PROCESSING UNIT
40 CFR, PART 503
STANDARDS FOR THE USE OR DISPOSAL
SLUDGE
F SEWAGE
lrsA R ® I ^ �
`01 1
Asheville Re9 ioc y
e1®dice
�fi ection.

TABLE OF CONTENTS
(1) REPORTING REQUIREMENTS/PERTINENT INFORMATION
(2) CERTIFICATION
APPENDIX = -
(a) 2012 distrubution and marketing summary
Parts A and B -
(b) 2012 annual sludge production data
(c) Annual Residuals sampling summary form
(d) Residuals Sampling Data
(e) TCLP analysis
(f) Annual Pathogen and Vector Attraction Reduction Forms = _
(g) Daily Dryer record

REPORTING REQUIREMENTS
Facilities responsible for reporting annually are described in the regulations- as:
1. Publicly Owned Treatment Works (POTW) with an average design
influent now rate,equal to or greater than 1.0 MGD.
2'. POTW's serving-a.popul4tion of 10,000 or more.
3. Class I (facilities with an approved pretreatment program) sludge management
facilities.
The Tuckaseigee Water and Sewer Authority Wastewater -Treatment -Plant #1 ds rated as &3.5
mgd facility. The facility also treats the sludge from two additional -plants owned by-the--r-
authority.
Pertinent infi6imation includes:
facility name: Tuckaseigee Water & Sewer' Authority Plant # I
NPDES # NCO039578
correspondence address: 1246 West Main St
Sylva, NC 28779
physical address: 1871 North River Rd
Sylva NC 28779
— facility operator: Stan Bryson
Wastewater Plant Operations Superintendent
ph. 828-586-9318

CERTIFICATION REQUIREMENTS
PART I - POLLUTANT CONCENTRATIONS
Permitted Concentrations
PARAMETER _ _ _ _ 4 A. vg
monthly avg
--- ceiling
Arsenic......:.............0.75 mg/kg :..:..............1.9 mg/kg -
- - =41 mg/kg -
-=75 mg/kg -
Cadmium..................2.10 mg/kg. , ................ 2.6mg/kg
= - -° - 39 mg/kg
85 mg/kg - -
Copper ................ ..... 396 mg/kg mg/kg
1500 mg/kg
4300 mg/kg
Lead ......19.7 mg/kg................. 22.4 mg/kg
:.._ ..................
300 mg/kg
840 mg/kg
- Mercury.....:....: 0.55 mg/kg, ...............0.90 mg/kg
1 - 7�g m :
. -
� - .57 mg/kg
Molybdenum ...............:4.4 m -
- Y g/kg..................5.2 mg/kg -
_ - -
_>_-: -- n/a -
- 75 mg/kg
Nickel ......................13.3 mg/kg................. 15.1 mg/kg :..
_ a . 420 mg/kg
4W mg/kg =
Selenium.....................6.6 m ..
mg/kg ...................7.8 mg/kg
`..
100 mg/kg
100 mg
Zinc ........................1192 mg/kg ................ 1330 mg/kg -
- - --2800 mg/kg
7500 m glkg
PART H -PATHOGEN REDUCTION (40 CFR 501321.-T._
.,
X Class A Class B
PART III VECTOR ATTRACTION (40 CFR 503.33)
_ Option 1 _ Option 2 _ Option 3 _ Option 4
_ Option 5 __Option _6 _ Option 7 X Option 8

PART IV -- CERTIFICATION-
__ I certify under penalty of law, that the Class A pathogen requirements in 40 CFF, Part503. 32 -
have been met and the vector attraction reduction requirement in 40-CFP,-Part [503. 33(b)(6)]==-==-
has been met. I am aware that there are significant penalties for -false certification including fine _--
and imprisonment."_ -
Signed this 28th day of ' January_ , 2013.
Stan Bryson, ewater Superintendent

Appendix A :.
TWSA Plant #1
Distribution and Marketing Summary
Residuals Sources and Volumes

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM. '
PERMIT #: WQ0005763 FACILITY NAME: Tuckaseigee Water and Sewer Auth/TWSA Plant #1
PHONE: [phone] COUNTY: Jackson OPERATOR: Stan Bryson
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? M Yes ❑ No No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Vo me (dry tons
Reci lent Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
January
18.07
0
February
15.59
12.8
March
12.64
15.62
April
13.23
9.94
May
See Appendix A
6.03
7.1
See Appendix A
June
Part A
14.48
19.88
Part B
1
Soil amendment
July
14.56
14.2
August
42.3
41.18
40
Pasture/Hayfields
September
7.86
8.52
October
11.69
11.36
November
26.65
26.9R
I'' i
40
Aac1hrrP/NavfiP.1dr
December
Ir
;
1.71
4.26
-
- -- -- --- -
Totals:
Annual d tons):
0
184.81
171.84
r s _s
81
�
Amenament(s) usea: I u I Bulking Agent(S) used: I u l I 1,,
* If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached
Part C: , 1 -
Facility was compliant during calendar year 2012 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. 51 Yes ❑ No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
r i ,
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
that th re are s' nin nt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permitfee 1 Date i Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)'
it DENR FORM DMSDF (11/2005)

Appendix A
TWSA PLANT # 1
= ANNUAL DISTRIBUTION AND
MARKETING SUMMARY
2012
Part A
Residual
Sources and Volume
Class A
Sludge Volume
Sludge Volume
Residual Volume
P[oduced
Dewatered
Loads
Produced
Month Source
(dry tons
(dry tons)
From Dryer
(dry tons)
January
TWSA Plant # 1 (NC0039578)
18.07
18.07
TWSA Plant # 2 (NC0020214)
0
TWSA Plant # 3 (NC0063321)
0
-
18.07
18.07
0
0
Monthly Total
18.07
February
TWSA Plant # 1 (NC0039578)
8.26
15.59.-
TWSA Plant # 2 (NC0020214)
4.72-
TWSA Plant # 3 (NC0063321)
2.61
15.59
15.59
9
= - 12.8
Monthly Total
March
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
10.33
2.31
0-
12.64
12.64
12.64
11
16.62
April
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
5.80
7.43
0
13.23
13.23
7
9.94
May
TWSA Plant # 1 (NC0039578)
5.82
TWSA Plant # 2 (NC0020214)
0.21
TWSA Plant # 3 (NC0063321)
0
6.03
6.03
5
7.1
Monthly Total
June
TWSA Plant# 1 (NC0039578)
14.48
TWSA Plant # 2 (NC0020214)
1.6
TWSA Plant# 3 (NC0063321)
2.02
-
-
14.48
14.48
14
- _ ,- 19.88
Monthly Total

Part A
Residual
Sources and Volume
Class A
Sludge Volume
Sludge Volume
Sludge Volume
Residual Volume
Produced
Dewatered
Treated
Produced
Month Source
(dry tons)
(dry tons) - .
(dry tons) -- -
- - (dry tons)
July
TWSA Plant # 1-(NC0039578)
11.69
TWSA Plant # 2 (NC0020214)
2.87
TWSA Plant # 3 (NC0063321)
0
14.56
14.56
10
- 14.2
Monthly Total
August
TWSA Plant # 1 (NC0039578)
37.41
-
_
TWSA Plant # 2 (NC0020214)
4.89
TWSA Plant # 3 (NC0063321)
0
-
42.3
42.3
29
41.18
Monthly Total
September
TWSA Plant # 1 (NC0039578)
7.86
TWSA Plant # 2 (NC0020214)
0
TWSA Plant# 3 (NC0063321)
0
-
7.86
7.86
6
- 8.52
Monthly Total
October
TWSA Plant # 1 (NC0039578)
9.04
--
- _
TWSA Plant # 2 (NC0020214) .
0
TWSA Plant # 3 (NC0063321)
2.65
11.69
11.69
8
11.36
Monthly Total
November
TWSA Plant # 1 (NC0039578)
26.65
TWSA Plant # 2 (NC0020214)
0
TWSA Plant # 3 (NC0063321)
0
26.65
26.65
19
26.98
Monthly Total
December
TWSA Plant # 1 (NC0039578)
1.71
TWSA Plant # 2 (NC0020214)
0
TWSA Plant # 3 (NC0063321)
0
1.71
1.71
3
4.26
Monthly Total
Total "sludge" produced by all sources for 2012= 188.43 dry tons
Total "sludge" dewatered by belt press in 2012= 188.43 dry tons---
Total number of dryer loads in 2012= 121 ----- - -___--- - -
Total number of dryer loads x 1.42 dry-tonfload = 171.82 dry tons -
Total "residual" produced for distribution in 2012=171.82 DRY TONS

Appendix A
TWSA PLANT # 1
ANNUAL DISTRIBUTION AND =
MARKETING SUMMARY
2012
Part B
Recipient Information
Est. Volume
Month Name Address wet tons Intended Use
January
Mont hl Total
0
February
Monthly Total
-
0
March
Monthly Totall 0
April
Monthly Totall 0
May
Monthly Total
0
June
Randy Cook
73 Swiftwater Drive
1 ton
soil amendment
Sylva NC 28779
for yard
ph 828-226-9889
Monthly Totall
1 ton
July
Monthly Total
0
August
Tony Collins .
327 Cedar Ridge Rd
pasture/
Franklin NC 28744
20
hayfields
ph 828-421-0140
-
- - --
- Monthly Total
40
September
--
Monthly Total
0
October
Monthly Total
0
1 :71

November
Tony Collins
327 Cedar Ridge Rd
--:-----20
pasture/
Franklin NC 28744
20
hayfields
ph 828-421-0140
Monthly Total
40
December
-, -
Monthly Total
0
Annual Total 81 tons (est.)

Appendix B
Tuckaseigee Water and Sewer- Auth.
2012 Sludge Production

2012 SLUDGE PRODUCTION DATA --
TWSA PLANT # 1 (3.5 mgd) - _ -
NPDES # NC0039578 - -
Sludge dewatered on belt press ........................................................ :........ 2,119,736 gallons
total tons...............................................188.43 tons
total metric tons............................................170.91 dry metric tons
The following residuals were included in the above totals. -- _:
TWSA PLANT # 2 (.5 mgd)
NPDES # NC0020214
Sludge Hauled to Plant # 1 digestor........................................-.-.......... - ...........343,200 gallons
totaltons........................................................................ 27.93 tons .
total metric tons...............................................................25.33 dry metric .tons
TWSA PLANT # 3 (.2 mgd)
NPDES # NCO063321
Sludge Hauled to Plant # 1 digestor............................................................. 75,000 gallons ---
totaltons................................................................................. -7.28 dry tons
total metric tons .................... ............6.60 _dry metric_tons = .
A portion of the sludge that was generated at the Tuckaseigee Water and Sewer Authority during
2012 was hauled by a private contractor to a designated landfill in Georgia.
Landfill: Rand B Landfill
610 Frank Bennett Rd.
Homer, GA 30080
A total of 48.97 tons were hauled to the landfill during 2012.-
Copies of haul tickets can be provided if needed. -- - - - - - _

TWSA Annual Residual
Operation Totals
2012
SLUDGE FEED
DrVer
Run
avg
Total
Total
Total
DATE
% Solids
Gallons
Dry Ton
Days
Loads
Hrs
Jan.
1.74
251,879
18.07
0
0
0
H, fl"!Siilllili!
i,H
Feb.
2.10
178,768
15.59
6
9
35.3
Hid HE,
01 M4:z;!;!P1z-­HH
Mar.
2.14
142,104
12.64
4
11
44.6
Apr.
1.82
174,040
13.23
3
7
29
Ma v
1.30
112,010
6.03
2
5
21.4
Jun.
1.94
2231788
18.10
6
14
60.1
Jul.
2.11
166,569
14.56
4
10
42.7
Aug.
2.38
428,920
42.30
10
29
113.3
Se
2.27
83,313
7.86
2
6
24
K
ilfl 1111, fl i
Oct.
2.74
102,543
11.69
3
8
31.9
U9 i
Nov.
2.89
220,662
26.65
7
19
79.4
Dec.
1.17
351140
1.71
1
3
12.3
Monthl
avgl
2.05
176,645
15.70
4
10
41.2
ytd total
2,11-9,736
188.43
48
121
494.0

2012
TWSA #2 SLUDGE PRODUCTION
MONTH
Date
Gals Hauled To
TWSA # I
% SOLIDS
TOTAL
DRY TON
Hauler
January
IN!
.. .. .......
February
2/16
4,800
0.57
TWSA
2/17
4,800
2.83
0.57
TWSA
2/20
19,200
2.57
2.06
TWSA
2/21
19,200
1.91
1.53
TWSA
NIT
March
3/20
7,200
2.24
0.67
TWSA
3/21
14,400
2.05
1.23
TWSA
3/23
4,800
2.05
0.41
TWSA
'12 '40
-11
April
4/9
4,800
Hi ll",2Q
0.40
TWSA
4/10
9,600
2.00
0.80
TWSA
4/16
21,600
2.00
1.80
TWSA
4/17
14,400
Ilit'llill---i.ililililil-*.Ii,:2100i
1.20
TWSA
4/19
12,000
1.28
0.64
TWSA
4/24
19,200
1.56
1.25
TWSA
4/25
19,200
1.68
1.34
TWSA
May
5/8
9,600
0.53
0.21
TWSA
-1 JH
.. .......
...
June
6/5
16,800
2.28
1.60
TWSA
,rotaI
NN
lil
i fliiw.
..fl'
M, [ill id!
f H
1,411"isfln- 0,
-AM
July
7/23
7,200
1.93
0.58
TWSA
7/24
9,600
1.98
0.79
TWSA
7/25
19,200
1.87
1.50
TWSA
H
Auqust
8/16
7,200
2.19
0.66
TWSA
8/17
12,000
2.19
1.10
TWSA
8/20
16,800
2.11
1.48
TWSA
8/24
21,600
1.85
1.67
TWSA
M
;
fl!fV-7f.
September
-T z
i I 14. i j
October
W"159P
MUM;Ot
ip
November
December
12/19
14,400
2.12
1.27
TWSA
12/20
16,800
2.02
1.41
TWSA
12/21
16,800
1.74
1.22
TWSA
77M,
I H
TOTAL
343,2001
1
27.93
TOTAL 27.93 X .907 metric ton/English Ton
25.33 Dry Metric Tons

2012
TWSA #3 SLUDGE PRODUCTION
MONTH -
Date
Gals Hauled To
TWSA # 1
% SOLIDS
TOTAL
DRY TON
Hauler
January
Mbhthf TT t 1141111H1111111MI
HIN-11-H!
777777r7777=
February
16 th
4,167
2.52
0.44
Cooper
17th
4167
2.61
0.45
Cooper
1 8th
4167
2.56
0.44
Cooper
20th
4167
2.56
0.44
Cooper
21 st
4167
2.62
0.45
Cooper
23rd
4167
2.14
0.37
Coop r
F
March
Mo;:,hthwx,
1 111 6.60
April
Month) j!Total.
Mav
Mbnthl ..Total
ilhiidll. Iffililon; Iii 1ji.,ki ild k1lil! 1.6
June
5th
3,125
2.36
0.31
Cooper
6th
3,125
2.44
0.32
Cooper
7th
3,125
2.49
0.32
Cooper
1 1th
3,125
2.66
0.35
Cooper
12th
3,125
2.26
0.29
Cooper
13th
3,125
0.51
0.07
Cooper
14th
3,125
1.92
0.25
Cooper
15th
3125
0.89
0.12
Coo er
i o' -n- h, t
.... .. 0
IM i : ma -2 2"
HI, '11R."I'liflifi-fil
Julv
RT"i,
A
HV
1i
'1M&tfil .
Auqust
Month)`i , I T.-
R11,11111:11,11
11,1111,114111
00:
--n I IN !'Rl, -till
September
October
8th
3,125
2.83
0.37
Cooper
1 Oth
3,125
2.87
0.37
Cooper
11th
3,125
2.81
0.37
Cooper
14th -
3,125
2.80
0.36
Cooper
1 5th
3,125
2.89
0.38
Cooper
17th
3,125
1.14
0.15
Cooper
18th
3,125
1.78
0.23
Cooper
19th
3125
3.21
0.42
Cooper
November
M: 6 n,,t h W.Hri
M4.14,11
December
TOTAL
75.0001
7.28
TOTAL 7.28 X.907 metric ton/English Ton
= 6.60 Dry Metric Tons
F'I

Tuckaseigee Water and S ewer Auth= T - r
- 20012 Residuals Sampling
Summary Form -r -.

2012
Annual Residual Sampling Summary Form
Permit Number: WQ 0005763
Facility Name: T uckaseigee Water and Sewer Auth
NPDES # NC 0039578
WQ # : WQ 0005763
WWTP Name: TWSA Plant # 1
Sample
:.:,:,;:
f'ii!! HW
Il!
Date
2/14
3/30
6/7
6/28
8114
11/13
Avg.
i; i!I!;!!
Percent Solids
96:4
94.6
96.8
98.2
96.5
Aluminum
19,600
18,900
24,900
24,000
21,850 .
P
✓, Arsenic
1.1
< 0.52
< 0.44 .
1.9
0.75
A
Cadmium
1.9 v
2.0
2.6
1.9
2.10
R
V Calcium
7,990 .,
9,730
10,800
10,700 i
9,805
A
Chromium
25.8
31.0 v
33.6
30.3
30.2
M
copper
330
369 r
472 V
412
396
E
Lead
13.8 ,i
22.4
21.7 ;
2 1. 0 ii
19.7
T
✓ Magnesium
2,970✓
3,070
3,450.v
3,300 j,,
3,198
E
/ Mercury
0.11
0.68
0.90 E/
0.49
0.545
R
Molybdenum
4.2
5.2 ,i
4.4
3.8 .
4.4
S
✓, Nickel
10.2 ,,-
14.3 ,,
15.1 ✓
13.6
13.3
h, s.u.
5.5
6.2 ✓
6.3
5.7 ✓
i 'll!iii'i;'<>iiiiliifi
,/ Potassium
7,090 v
4,100
5,670 1--
4,790 41-11
5,413
1/ Selenium
5.2
7.6
7.8
5.7 i
6.6
Sodium
1000 ",
992
1240
1,120 V
1,088
Zinc
898 ✓
1330
1310 ci
1,230 ✓
1,192
TO
6,680
40,300
49,400
22,800
29,795
mg/
Ammonia -Nitrogen
1020 ,/
1230
81.5 ✓
498
707
kg
,/ Nitrate -Nitrite
ND
< 2.1 .
< 2.0
< 2.0
0.0
Plant Available N
2,210
12,300
14,800
6,940
9,063
i/ Total Phosphorous
21,600
17,100
3500
22,100
16,075
✓ Corrosivi
5.53 s.u.
6.56 s.u.
7.44 s.u.
5.88 s.u.
Ignitability
> 140 F
> 140 F
>.140 F
> 140 F
> 140 F
m
✓ Reactivity, cyanide
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
m
/ Reactivity, sulfide
< 25
< 25
< 25
< 25
< 25
m n/
,/ Fecal Coliform
< 2 v
2
< 2
2
< 2
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

Appendix D
Tuckaseigee Water and Sewer. Auth. -
2012 Residuals Sampling Ddta

aceAnaly. ical
www.pacelabs.com
i
February 29, 2012 -
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NO 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite lob
Huntersville, NC 28078
[phone]
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: Residual2/14.
Pace Project No.: 92112290 _-
Dear Mr. Bryson:
Enclosed are the analytical resuIts'for sam le s received=b thelatiorato - ""a" -` � _' -- ' � p �) y' ry-on February 16, 2012 -
The results relate only to the samples included in this report:" Results-rep.orted he ein=conform to the= - -
most current TN standards and the laboratory's Quality Assurance Manual,'wapplicable,`unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses- have been subcontracted outside of the'Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Si ely,
T Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 15

aCffftlXical
WWW.Paceiabs.com
I l
Project: Lime Residual 2/14
Pace Project No.: 92112290
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
CERTIFICATIONS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001 -
South Carolina Drinking Water Cert. M 99006003
Virginia Drinking Water Certification #: 00213
Connecticut Certification M PH-0-104
Florida/NELAP Certification #: E87627'
Kentucky UST Certification #: 84 -
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification M 357 -
Virg1nia/VELAP Certification #: 460144 _
Asheville Certification IDs =
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648 South Carolina -Certification #: 99030001
Massachusetts Certification #: M-NC030 Virginia Certification #: 00072 -
North Carolina Drinking Water Certification #: 37712 West Virginia Certification M 356 -
North Carolina Wastewater Certification #: 40 Virgina/VELAP Certification #: 460147
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
.[phone]
REPORT OF LABORATORY ANALYSIS
Page 2 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Lime Residual 2/14
Pace Project No.: 92112290
Sample: TWSA DRIED RESIDUAL Lab ID: 92112290001 Collected:--02/14/12 12:00 Received: 02/16/12 11:36 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units Report Limit
DF
- Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
19600 mg/kg
145
20
02/17/12 13:25
0212011218:57
7429-90-5
Arsenic
_ 1.1 mg/kg
0.36
1
02/17/12 13:25
02/18/1217:45
7440-38-2
Cadmium
1.9 mg/kg
0.073
1
02/17/12 13:25
02/18/1217:45
7440-43-9
Calcium
7990 mg/kg
145
20
02/17/12 13:25
02/2011218:57
7440-70-2
Chromium
25.8 mg/kg
0.36
1
02/17/12 13:25
02/18/1217:45
7440-47-3
Copper
330 mg/kg
0.36
1
02/17/12 13:25
02/18/1217:45
7440-50-8
Lead
13.8 mg/kg
0.36
1
02/17/12 13:25
02/18/12 17:45
7439-92-1
Magnesium -
2970-mg/kg
--7.3-
1
02/17/12 13:25
02/18/1217:45
7439-95-4
Molybdenum
4.2 mg/kg
0.36
1
02/17/12 13:25
02/18/1217:45
7439-98-7
Nickel
10.2 mg/kg
0.36
1
02/17/12 13:25
02/18/1217:45
7440-02-0
Potassium
7090 mg/kg
363
1
02/17/12 13:25
02/18/1217:45
7440-09-7
Selenium
5.2 mg/kg
0.73
1
02/17/12 *13:25
02/18/12 17:45
'7782-49-2
Sodium
1000 mg/kg
363
1
02/17/12 13:25
02/18/1217:45
7440-23-5
Zinc
898 mg/kg
14.5
20
02/17/12 13:25
02120/1218:57
7440-66-6
7471 Mercury
Analytical- Method: EPA 7471 Preparation
Method:
EPA 7471
=
-
Mercury
0.11 mg/kg 0.0043
1
02/20/1216:00
02/21/1212:33
7439-97-6
}cent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
2.9 %
0.10
1
02/20/12 16:37
9045 pH Soil
Analytical Method: EPA 9045
PH at 25 Degrees C
5.5 Std. Units
0.10
1
02/24/12 16:00
Plant Available Nitrogen
Analytical Method: 40CFR PART 432.2
Plant Available Nitrogen
2210 mg/kg
1.0
1
02/29/12 12:26
N2 .
Total Nitrogen Calculation
Analytical Method: 40CFR PART 432.2
Nitrogen
6680 mg/kg
40.0
1
02/28/12 16:43
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
1020 mg/kg
10.7
1
02/28/12 15:17
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
6680 mg/kg
240
10
02/26/12 13:14
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
2.0
1
02/21/12 18:57
Nitrogen, Nitrite
ND mg/kg
1.0
1
02/21/12 18:57
Nitrogen, NO2 plus NO3
ND mg/kg
2.0
1
02/21/12 18:57
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
21600 mg/kg
589
200
02/27/1217:52
7723-14-0
i
ate: 02/29/2012 12:26 PM REPORT OF LABORATORY ANALYSIS Page 4 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

11�aceAnalytical
www.pacelabs.com
Project: Lime Residual 2/14
Pace Project No.: 92112290
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content., -
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. -
MDL - Adjusted Method Detection Limit.
- S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. -
Consistent with EPA guidelines, unrounded data are displayed and have been used to -calculate % recovery and RPD values..
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate—
RPD - Relative Percent Difference _-
NC - Not Calculable.
SG - Silica Gel - Clean -Up -
U - Indicates the compound was analyzed for, but not detected. _
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8276-.-The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. = _
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
\BORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TNI accreditation for this parameter.
R1 RPD value was outside control limits.
_ace: 02/29/2012 12:26 PM REPORT OF LABORATORY ANALYSIS Page 14 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

03-16" 12 16:48 FROM -Pace Analytical 8282524618 T-202 P002/004 F-448
Analytical Results
Pace Analytical Asheville - -
2225 Riverside. Drive - -
Asheville NC.- 28804
Entered 2/17/2012 - __ - -•
Reported: 2/22/2012 _
For: 92112290 *sample out of hold time* - -
Sample ID Para -meter Oust ID Result Units= -_-_ Method:-__ Date -Analyzed" Analyst.: _s
120217-3 % Solids ` 92-1122900oi 96.4 - % SM2540B 2/17/12 CL
120217-3 Fecal Colifonn.MTF 9211229OD61 <2--MPN/g SM92210E - 2/17/12 CL
Respectfully submitted,
(Tr
- Dena Myers
.NC Cert #440,
-NCDW Cert #37755,
EPA NC00909.
i G
P.O. ]Box 228 • SEatosville, North Carolina 29687.704/872/4697

03-16-.'12 16:48 FROM -Pace Analytical 8282524618
T-202 P003/004 F-448
STATES'VILLE ANALYTICAL, INC.
STATEMENT OF DATA QUALIFICATION
o
Client Name: 1 U. CC f i� 1 � �1/YQ Laboratory Group ID No. 440
Client Address: �y�U l ��Q EJ' t—' 12 t jc -2U 6
The following analyses are qualified for the reason(s) cited.
Sample No.: 1120 1�_ 1-71 _S Parameter(s):
Explanation:
The indicated condition(s) for the analytical batch, of which your sample(s) -was a part, -or for the sample(s), is outside our
established QA/QC acceptance limits: _
O ' Laboratory Control Standard outside acceptance limits. .
O Sample integrity suspect. (139plain below.)-
O Volatiles vial(s) received with headspace.
O Sample preservation does not meet EPA established sample preservation .
requirements.
O Detection limit(s) elevated due to sample matrix interference,
O Data suspect due to possible laboratory contamination. (Explain below.) -_-- _
O Surrogate/internal standard recovery(s) outside established acceptance
limits.
Analysis performed beyond EPA established allowable holding time. -
Sample Matrix Spikes) outside established acceptance :units. _ --
O Relative Percent Difference for duplicate, analyses outside established
acceptance limits.-
{ .) . Analyte coelutes with the cited compound. Result may represent a
combination of both compounds.
(.) Method Blank results outside established acceptance limits.
/ Sample(s) was analyzed despite the indicated problem: O N/A
Per client's request.
Per Project/Section/QA Manager's requests.
The sample was not reanalyzed due to the following reason: O.NIA
O Insufficient sample received for repeat analysis.
O The . remaining sample not -within the holding limits established by the EPA: .
O The sample's integrity was compromised during the sample storage.
O Per client's instructions - Contact: Date:
O Per Project Manager's/Section Manager's/QA Manager's Bequest. Mgr. Initials:
f) Other -
If you have questions concerning this data qualification report, please contact me at [phone].
Data Reviewed b \ Date: G"
Oug Assuranc Manager
This Statement of Qualification is included as part of the final analytical report for the above referenced. sample(s) and must be
retained as part of that permanent record. u
e

awAnaly ical
wwwPacefabs.com
May 30, 2012
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.,`
1246 West Main Street _ _ -
Sylva, NC 28779
RE: Project: TWSA Dried Sludge -
Pace Project No.: 92117398
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received`by the 'laboratory on Aprif 27,� 2012 ­ fihe
results relate only to the samples included in this report.-__ Result Sreported_herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual; where applicable; `unless
otherwise noted in the body of the report. .
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sc rely,
T Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 1

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
2
Sample Summary
Pace Analytical Service§, Inc.
Order Number: 1209789
Laboratory ID Client ID Matrix Sampling -Date -
1209789-01 Dried Sludge Residual Solid 3/30/2012,
"Analytical Integrity" ! EPA Certified • NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: [phone] • Fax: [phone]
Web Site: wwiv settek. corn

SUMMIT
i ENUIRONIVIENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Report Narrative
Client: Pace Analytical Services, Inc.
Order Number:.-1209789 - -
3
Solid sample results are reported on a wet weight basis except as- noted.-
No problems were -encountered during analysis of this order number; except -as -noted. -
Data Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited. by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting. Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values .are available upon request,
Matrices:
A = Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
SL = Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
WW = Waste Water
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc, is not
responsible for use or interpretation of the data included herein.
1
"Analytical Integrity" • EPA Certified • NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: [phone] , Fax: [phone]
Web Site., www.settek.com

r t UM,'
T
I I
l ENVIRONMENTAL TECHNOLOGIES, INC.
J Analytical Laboratories
Client IN Lab IN Collected Anahte
Dried Sludge 1209789=01 30-Mar-12 pH
Residual
_Client ID#
Lab IN -
Collected Analvse -
Dried Sludge
1209789-01
30-Mar-12 Flash Point
Residual
Client IN
l,ab 1D# . _-'
tiller ed..= Analvle....
Dried Sludge
1209789-01
30-Mar-12 Reactive Cyanide
Residual
Client ID# Lab'JD# Collected .Analvte
Dried Sludge 1209789-01 30=Mar42 Reactive Sulfide
Residual
May 08, 2012
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville, NC 28804
Received: 4/30/2012
Project #: 921173,98
Result Units Matrix Method DF LONG Run Anal ,st
5.53@20.5 C S.U. S SW-846 1 0.01 31-May-12.JRK.
9045 A
Result Units Matrix Method DP LOB, Run Analyst
>140 °F S 1010 1 )I-May-12 TAH
,Result Units_ Matrix_ Method DF _ LOQ Run Analvst
ND ppm S 7.3.3.2 1 0.5 - )I-May-12 TIR
Units Matrix Method DF LOQ Run Analvst
ppm - S - 7.3.4.2 1 25 31-May-12 TIR
Page 4
"Analytical Integrity" - EPA Certified • NELAP Certified
3310 Win Street . Cuyahoga Fa1Is, Ohio 44223 o Phone; 330-253-62 11 • Fax: [phone]
Web Site: iww settek. coin

aceAna1jfta1
www.pacelabs.com
I
July 26, 2012
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street =
Sylva, NC-28779 -_
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
RE: Project: TWSA Dried Residual 6/7/12
Pace Project No.: 92120544-=-
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received-by=the laboratory or -Jtane-07,'2012.--The
results relate only to the samples included in this report.- Results- reported herein --conform to -the -
most" -
current TNI standards and the laboratory's Quality Assurance- Manual °;-where applicable;'unless-
otherwise noted in the body of the report. --
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
-F
Enclosures
[e-mail]
Project Manager
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16

Pace Analytical Services, Inc.
205 East Meadow ® w Road - Suite A
ace�Analytical Eden, NC 27288
www pecerabs:com
[phone]
Project: TWSA Dried Residual 6/7/12
Pace Project No.: 92120544
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs -
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification P 37706
Kentucky UST Certification #: 84 --
North Carolina Field Services Certification M 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12.- - -
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
-- - - -
Asheville Certification IDs-
=
_- 2225 Riverside Dr., Asheville, NC 28804 _ _
North Carolina Wastewater Certification M 40
Florida/NELAP Certification M E87648 _.
South Carolina Certification M 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356 ---
North Carolina Drinking Water Certification M 37712
Virgina/VELAP Certification M 460222
1 ' -
REPORT OF LABORATORY ANALYSIS Page 2 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacefabs.crom:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: TWSA Dried Residual 6/7112
Pace Project No.: 92120544
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TWSA Dried Residual Lab ID: 92120544001 Collected: 06/07/12 11:00 - Received: 06/07/12 13:32 Matrix: Solid'
Results reported on a "dry -weight" basis = -
Parameters Results Units Report Limit DF =-Prepared Analyzed CAS No. Qua]
6010 MET ICP
Analytical Method: EPA 6010 Preparation --Method: EPA 3050
Aluminum
18900 mg/kg
104
10
06/19/12 16:10
06/20/12 14:14
7429-90-5
Arsenic
ND mg/kg
0.52
1
06/19/12 16:10
06/20/12 13:19
7440-38-2
--__Cadmium
_ _ 2.0 mg/kg "
0.10
1
06/19/12 16:10
06/20/12 13:19
7440-43-9
Calcium
9730 mg/kg
10.4
1
06/19/12 16:10
06/20/12 13:19
7440-70-2
Chromium
31.0 mg/kg
0.52
1
06/19/12 16:10
06/20/12 13:19
7440-47-3
Copper
369 mg/kg
0.52
1
06/19/12 16:10
06/20/12 13:19
7440-50-8
Lead.
22.4 mg/kg
0.52
1
06/19/12 16:10
06/20/12 1'3:19
7439-92-1
Magnesium
3070 mg/kg
1.0.4
1
06119/1216:10
06/20/12 13:19
7439-95-4
Molybdenum
5.2 mg/kg
0.52 -
1
06/19/12 16:10
06/20/12 13:19
7439-98-7
Nickel
14.3-mg/kg
0.52
1
06/19/12 16:10
06/20/12 13:19
7440-02-0
Potassium
_-__4100 mg/kg
518
1
06/19/12 16:10
06/20/12 13:19
7440-09-7
Selenium
7.6 mg/kg
1.0
1
06/19/12 16:10
06/20/12 13:19
7782-49-2
Sodium
992 mg/kg
518
1
06/19/12 16:10
06/20/12 13:19
7440-23-5
Zinc
1330 mg/kg
10.4
10
06/19/12 16:10
06/20/12 14:14
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation
Method: EPA 7471
-
- - -
Mercury
0.68 mg/kg
0.045
10
06/20/12 09:00
06/20/12 11:22
7439-97-6
arcent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
5.5 %
0.10
1
06/18/12 09:08
2540G Total Percent Solids
Analytical Method: SM 2540G
Total Solids
94.6 %
0.10
1
06/15/12 14:40
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
6.2 Std. Units
0.10
1
06/08/12 14:00
Plant Available Nitrogen
Analytical Method: 40CFR PART 432.2
Plant Available Nitrogen
12300 mg/kg
1.0
1
06/22/12 14:05
Total Nitrogen Calculation
Analytical Method: 40CFR PART 432.2
Nitrogen
40300 mg/kg
40.0
1
06/22/12 13:58
7727- 37- 9
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
1230 mg/kg
20.2
22
06/12/12 16:03
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
40300 mg/kg
5290
100
06/15/12 14:21
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
2.1
1
06/14/12 21:49
Nitrogen, Nitrite
ND mg/kg
1.1
1
06/14/12 21:49
Nitrogen, NO2 plus NO3
ND mg/kg
2.1
1
06/14/12 21:49
Date: 07/26/2012 08:04 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1g,N2
N2
Page 4 of 16

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
eAnalydcal Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs.com
ac(336)623-8921 [phone] [phone]
ANALYTICAL RESULTS
Project: TWSA Dried Residual 6/ 7 /12
Pace Project No.: 92120544 - .
Sample: TWSA Dried Residual Lab ID: 92120544001 Collected: 06/07/12-1-1:00---- Received:-- 06/07/12 13:32 Matrix: -Solid
Results reported on a "dry -weight" basis
-Parameters --Results = Units- Report Limit DF Prepared Analyzed CAS No: Qua]
365.1 Phosphorus, Total Analytical Method: EPA 365.1 _---
Phosphorus 17100 mg/kg ­529- 100 06112/12 10:45 7723-14-0
Date: 07/26/2012 08:04 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 16

Pace Analytical Services, Inc.
//�� ,,,, // 205 East Meadow Road - Suite A
C�CE+/"1! aIX401 Eden, NC 27288
wwwpacefebs com
[phone]
QUALIFIERS
Project: TWSA Dried Residual 6/7/12
Pace Project No.: 92120544
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or -moisture content.-; - - -
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method -Defection Limit.. - - --
PRL - Pace Reporting_ Limit.: _
-RL - Reporting-.__--
S-- Surrogate -
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used -to calculate % recovery and RPD values. .
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.' -
SG - Silica Gel - Clean -Up -
U - Indicates the compound was analyzed for, but not detected. ---- _ -- - - -
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g SAMPLE ANALYZED OUTSIDE OF EPA RECOMMENDED HOLDING TIME
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TNI accreditation for this parameter.
Date:.07126/2012 08:04 AM REPORT OF LABORATORY ANALYSIS Page 15 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

A 0
S"""U"MMIT
ENVIRONMENTAL,
TECHNOLOGIES, INC.
Analytical 1-aboiatorles;
-LABORATORY REPORT
Client
Pace Analytical Services, Inc.
-2225 Riverside Drive -
Asheville, NC 28804
Order Number
1 -213494
Project Number
92120,544
Issued
Wednesday-, June2-0,, 2012
Total Number of Pages
4 (excluding C.O.C. and. cooler receipt form)
Approved By:
QA Manager
NELAC Accreditation #E87688
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Wire Street - Cuyahoga Falls, Ohio 444223 - Phone: [phone] - Fax: [phone]
Web Site: www.seltek.corn

sum
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboi-ataries
Sample Summary
Client: Pace Analytical Services, -Inc.
Order Number: 1213494
Laboratory ID
1.21,3494-01.
2
Client ID Matrix.-- Sampling Date---
92120544001 Solid 6/7/2012
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Win Street, - Cuyahoga Falls, Ohio 44223 - Phone, 330-253-8211 - Fax: [phone]
Web Site: wwmv.settek.com

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Anaiyticai Laboratdries
Report Narrative
3
Client: Pace Analytical Services, Inc.
Order Number: 1213494
Solid sample results are reported on a wet weight.basis except as -noted. -.
No problems were encountered during analysis of this order.number, except as noted. .
Data Qualifiers:
.B AnalyteJound•in the method blank.
J Estimated concentration of•analyte between MDL (LOD,) and Reporting Limit (LOQ)
C=.Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected atLOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
A=Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
SL = Sludge
SO = Soil
S = Solid
T = Tablet
TO = TCLP Extract.
WW =Waste Water
W = Wipe
The test results meet -the requirements of the NELAC standard, except -where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and -that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client fbr-which this
report.was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
"Analytical Integrity" • EPA Certified • NNELAP Certified
3310 Win Street . Cuyahoga Fails, Ohio 44223 - Phone: [phone] • Fax: [phone]
Web Site: nlwt lvsettck.com

my
ENVIRONMENTAL TECHNOLOGIES, INC.
AnalYlicalaiJaratorle
June 20, 2012
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville, NC 28804
Received: 6/8/2012
Project #: 921*20544
Client [D#
Lab IN
Collected Ana] e
Result
Units
.Matrix Method
DF
LQQ
Run Analyst
92120544001
1213494-61
07 Jun-12 Flash Point,
>140F
S 1010
1
12-Jun-12 TAH
Client.JD#
Lab'TD#
Collected -Analyze
Result
Units
Matrix Method
DF
LQQ
Run Analyst
92120544001
1213494-01
07-Jun-12 pH
6.56@21.6 C
s.u.
S 9040,
1
0.01
11-Jun-12 JRK
Client ID#
Lab ID#
Collected And
Result
Units
Matrix Method
DF
LQQ
Run Analyst
92120544001
1213494-01�07-Jun-12
Reactive Cyanide
ND
ppm
S 7.3.3.2
1
0.5
11-Jun-12 TIR
Client ID#
Lab 1D#.
CollectAnalyte
Result
Units
Matrix Method
DF
LQQ
Run Analyst
92120544001
1213494-01
077Jun-12 Reactive Sulfide
ND. _-
ppm
_ -S 7.3.4.2
1 _
25
11-Jun-12 TIR
Page 4
I I I
"Analytical Integrity„ • EPA Certified • NELAP Certified
3310 Win atreet - Cuyahoga Falls, Ohio 44223 a Phone: [phone] • Fax: [phone]
Web Site: www.settek—rom

c ►�:28 FR09-
T-05i P0002/0002 F-li
A nalytinnl 1D
esults
I ace Analytical . = _ _ _
25 Riverside Dri �Ashevilh
� �5heville Ve - .. N
' D . 28804
En$6od 8/29/2012 _ -
�odp�led: 7/2/2012 -- --

aceAnalytcal
www.pacelab&com
September 20, 2012
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street -i
— -Sylva,-NC-28779 =-- -- - --
RE: Project: Lime Residual 8/14- - - - =
Pace Project No.: 92127855
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received -by -the -laboratory on-August-=14,-2012 =-The-- -:-
results relate only to the samples included in this report ,-Results=reported-l-ereiWconform°to'the`-=-="-
most current TNI standards and the laboratory's Quality -Assurance Manual, —where applicable;=uhle'ss = --_--- -
otherwise noted in the.body of -the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
inc rely,
To i iams
to [e-mail]
Project Manager
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16

aceAnalyfical
wovw.pacelabs.com
Project: Lime Residual 8/14
Pace Project No.: 92127855
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TWSA DRIED RESIDUAL Lab ID:. 92127855001 Collected: 08/14/12 11:50 -- Received: 08/14/12 14:33 Matrix: Solid
Results reported on a "dry -weight' basis -
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
24900 mg/kg
175
20
08/22/12 09:40
08/22/12 18:07
7429-90-5
Arsenic
-ND mg/kg -
0.44
1
08/22/12 09:40
08/22/12 17:03
7440-38-2
Cadmium -
--2.6 mg/kg -
-0.088
1
08/22/12 09:40
08/22/12 17:03
7440-43-9
Calcium - - =
- -10800 mg/kg
175
20
08/22/12 09:40
08/22/12 18:07
7440-70-2
Chromium
33.6 mg/kg
-0.44
1
08/22/12 09:40
08/22/12 17:03
7440-47-3
Copper
472 mg/kg
0.44
1
08/22/12 09:40
08/22/12 17:03
7440-50-8
Lead
21.7 mg/kg
0.44
1
08/22/12 09:40
08/22/12 17:03
7439-92-1
Magnesium _ -'
$450 mg/kg
8.8
1
08/22/12 09:40
08/22/12 17:03
7439-95-4
Molybdenum
4.4 mg/kg
`_- 0.44
1
08/22/12 09:40
08/22/12 17:03
7439-98-7
Nickel
15.1_--m_ g/kg ----0.44
1
08/22/12 09:40
08/22/12 17:03
7440-02-0
Potassium
5670 mg/kg -
- 438
1
08/22/12 09:40
08/22/12 17:03
7440-09-7
Selenium
7.8 mg/kg
- 0.88
1
08/22/12 09:40
08/22/12 17:03
7782-49-2
Sodium
1240 mg/kg-----438
1
08/22/12 09:40
08/22/12 17:03
7440-23-5
Zinc
1310 mg/kg -
17.5
20
08/22/12 09:40
08/22/12 18:07
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation- Method: EPA 7471
- -
-
"4ercury
0.90 mg/kg
0.058
20
08/21/1217:05
08/22/1214:41
7439-97-6
rcent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
3.2 %
0.10
1
08/15/12 15:54
254OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
96.8 % 0.000010
1
08/15/12 11:50
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
6.3 Std. Units
0.10
1
08/23/12 14:30
Plant Available Nitrogen
Analytical Method: 40CFR PART 432.2
Plant Available Nitrogen
14800 mg/kg
1.0
1
08/29/12 15:57
Total Nitrogen Calculation
Analytical Method: 40CFR PART 432.2
Nitrogen
49400 mg/kg
40.0
1
08/24/12 16:47
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
81.5 mg/kg
8.2
1
08/28/12 09:00
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
49400 mg/kg
1290
25
08/21/12 14:39
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
2.0
1
08/23/12 16:27
Nitrogen, Nitrite
ND mg/kg
1.0
1
08/23/12 16:27
Nitrogen, NO2 plus NO3
ND mg/kg
2.0
1
08/23/12 16:27
Date: 09/20/2012 04:01 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
without the written consent of Pace Analytical Services,
Inc..
Qua]
N2
Page 4 of 16

aceAnalj4kal
www.pacetabs.com,
Project: Lime Residual 8/14
Pace Project No.: 92127855
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TWSA DRIED RESIDUAL Lab ID: 92127855001 Collected:-- 08/14/12 11:50 -Received: 08/14/12 14:33 - Matrix: Solid
Results reported on a "dry -weight" basis = -
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 3500 mg/kg 185- 100 08/26/1213:37 7723-14-0
( j
Date: 09/20/2012 04:01 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 16

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Lime Residual8/14 -
Pace Project No.: 92127855 = -
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting) I rn it.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit. - -
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike_.(Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference =
NC - Not Calculable. _
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected. - -
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamirie using Method-8270. The result reported for
each analyte is a combined concentration.
l Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TNI accreditation for this parameter.
t
Date: 09/20/2012 04:01 PM REPORT OF LABORATORY ANALYSIS Page 15 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Analytical Results
Pace -Analytical -Asheville -_
2225 Riverside Drive - -
Asheville NC 28804
Entered 8/15/2012
Reported: 8/22/2012
For: 92127855
Sample ID Parameter Cust ID Result -_ ,Units - Method - Date -Analyzed Analyst - = ----
120815-11 % Solids TWSA-- 99.7 - % SM2540B 8/1'5/12 MD
120815-11 Fecal Coliform MTF TWSA <2 = MPN/g SM92210E 8/15%12 MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA N 000909
P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697

MM ��r
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical L aboraiories
LABORATORY REPORT
Client
Pace Analytical Services, Inc.
2225 Riverside Drive
NC 28804
Order Number
1219249
Project Number
92127855
Issued
Friday, August 24, 2012
Total Number of Pages
4 (excluding C.O.C. and cooler receipt form)
Approved By:
QA Manager
Cbrtifications,;. A2LA/DOD 0724,01, Alabama 41600, Arkansas 88-0735, California 07256CA, 'Colorado, Connecticut PH-0105,
Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho; OH00923, Illinois 200061 and Reg,5, Indiana
C-OH-1 3, Kansas E-1 0347, Kentucky (underground Storage Tank) 3 Kentucky 90146, Louisiana 04061 and
LA1 2004, Maine 2012015, Maryland 339, Massachusetts M-OPH923,:Mlchigan (Reg.5), Minnesota 409711,
Montana CERT0099, New Hampshire 2996, New Jersey QH006, New York 11777, North Carolina 39705 and
631, Ohio 4170, Ohio VAP CI-0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island
LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 5 WG-15J, Region
8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH00923201 1-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 lf[lin Street - Cuyahoga Falls, 01hio 44223 - Phone: [phone], - Fax: [phone]
1111eb Site: iiltmsettek.com

s MMIT
U
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
-Sample Summary
Client Pace Analytical Services, Inc.
Order Number: 1219249
Laboratory ID
1219249-01
Client ID
92127855001
2
Sampling Dafte-
Solid- = = 8/14/2012-
'Analytical Integrity" - EPA Certified - NELAP Certified
'1310 Win Street - (Iuyahoga Fails, C-1hic 44223 . Phone. [phone]"! - Fax: -330-253-4489
Web Site wwwseftek.com,

o MIT
oi
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
3
Report Narrative
Client: Pace Analytical Services, Inc.
Order Number: 1219249
Solid sample results are reported on a wet weight basis except as noted. -
No problems were encountered -during analysis of this order number, except as noted.
Data .Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF =.Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit.(not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
Matrices:
A=Air
C = Cream
DW = Drinking Water
L = Liquid -
O = Oil
SL = Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
VVW = Waste Water
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
"Analytical Integrity" • EPA Certified - NELAIR Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 n hone: S3tt-25S-6211 - Fax: S31tl-25,E-4459
Web Site: wvilvi! settek. corn

y
ENVIRONMENTAL TECHNOLOGIES, INC,
Analytical Laboratories
Client lD#
Lab IN
Collected. AnaWt
92127855001
1219249-01
14-,Aug-12 Flash Point- -
-Client JD#
LablD#
Collected AiWM
92127855001
1219249-01
14-Aug-2 pH'
Client iby Lab l0k Collected Analyte
92127855001 1-219249-01 14-Aug-12,Readive Cyanide
Client ID# LaLlbj Collected_ Analyle
August 24, 2012
Client: Pace Analytical Services, Inc.
Address: 2225,Riverside Drive
Asheville, NC 28804
Received: 8/15/2012
Project #: 92127855
Rmuh 1h1jLs Matrix Method DF LQQ
Run Analyst
>140 . F - --S 1010 - I
16-Aug-12 TAH
Result 11niLs Matrix Method DF 1-00
Run Analyst
7.44-@ 22.2 C s.u. S SW-846 1 0.01
16-Aug-12 NBX
9045 A
Result 11Ui1a---Matrix Method - DF_ _LQQ Run Analyst
ND - - ppm S -7.3.3.2 -1 - 0.5 16-Aug-12 TIR
Result Units -Matrix Method '1317 LQQ Run Analyst
ppm-. --.S -7.3.4,2 ---1,-----25---16-Aug-12TIR
Page 4
Analytical Integrity" - EPA Certified NELAP Certified
3-31OWin Street - CuypJ4_qga_ Falls, Ohio' 44223 - Phone: [phone] . Fax:[phone]
Web Sfte.* wwwsettek.com

aceAnaIXical
wwwparelabs.com
i
November 29, 2012
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
- Sylva, NC 28779 -
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
RE: Project: Dried Residual-11/13
Pace Project No.: 92138358
Dear Mr. Bryson: i = --
Enclosed are the analytical results for sample(s) received_by the laboratoryy--on-November*1-3, 2012: - -
The results relate only to the samples included in this report: -Results=reported herein conform to the- -
most current TNI standards and the laboratory's Quality Assurance Manual; where`applicable,-unless -
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
ly,
Iliams
tom.williams@pacela'bs.com
Project Manager
Enclosures
pcc�
_ REPORT OF LABORATORY ANALYSIS Page 1 of 17
/ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

(:�;a'neAna6dicalo
www.pae.Webs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Dried Residual 11/13
Pace Project No.: 92138358 -
Raleigh Certification IDS
6701 Conference Drive Raleigh, NO 27607
North Carolina Wastewater Certification #: 67 --_
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627 -
Kentucky UST Certification #.' 84 _
West Virginia Certification #: 357 _
Virgin'ia/VELAP Certification #: 460221
Asheville Certification IDS
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West_Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222 f
REPORT OF LABORATORY ANALYSIS Page 2 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnaIXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
[phone]
_ SAMPLE ANALYTE COUNT -
Project: Dried Residual 11/13..-
Pace Project No.: 92138358 = — -- - --
Lab ID - Sample ID
92138358001 TWSA DRIED RESIDUAL
Analytes
Method _
Analysts
Reported
Laboratory
-EPA 6010
_ JDA; JMW '
14
PASI-A
EPA 7471
SH1
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
SM9221C E (MPN) 503
EPJ
1
PASI-R
SM 2540G
TNM
1
PASI-A
EPA 9045
EWS
1
PASI-A
40CFR PART 432.2
EWS
1
PASI-A
40CFR PART 432.2
EWS
1
PASI-A
EPA 350.1
SDH
1
PASI-A
EPA 351.2
JDA
1
PASI-A
EPA 353.2
DMN
3
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 3 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
11�7aceAnalytical ® 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
[phone]
ANALYTICAL RESULTS
Project: Dried Residual 11/13
Pace Project No.: 92138358
Sample: TWSA DRIED RESIDUAL Lab ID: 92138358001 Collected: 11/13/12 10:00 Received: 11/13/12 12:38 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters _ --Results- - - Units Report Limit DF_ Prepared Analyzed CAS No. Qua[
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
24000 mg/kg
62.1
10
11/15/12 18:00 11/18/1217:40 7429-90-5
Arsenic
1.9 mg/kg
0.31
1
11/15/12 18:00 11/17/12 11:02 7440-38-2
Cadmium -
1.9 mg/kg
0.062
1
11/15/12 18:00 11/17/12 11:02 7440-43-9
Calcium __ = _-
_1070Q mg/kg
62.1
10
11/15/12 18:00 11/18/12 17:40 7440-70-2
Chromium
30.3 mg/kg
0.31
1
11/15/12 18:00 11/17/12 11:02 7440-47-3
Copper
412 mg/kg
0.31
1
11/15/12 18:00 11/17/1211:02 7440-50-8
Lead
21.0 mg/kg
0.31
1
11/15/12 18:00 11/17/12 11:02 7439-92-1
Magnesium
3300 mg/kg
6.2
1
11/15/1218:00 11/17/1211'-02 7439-95-4
Molybdenum
3.8 mg/kg
-0.31
1
' 11/15/12 18:00 11/17/12 11:02 7439-98-7
Nickel
- 13.6 mg/kg
- 0.31
1
11/15/12 18:00 11A7/1211:02 7440-02-0
Potassium
4790 mg/kg
310
1
11/15/12 18:00 11 /17/12 11;02 7440-09-7
Selenium
5.7 mg/kg
0.62
1
11/15/12 18:00 11/17/12 11:02 7782-49-2
Sodium
1120 mg/kg
310
1
11/15/12 18:00 11/17/12 11:02 7440-23-5
Zinc
1230 mg/kg
6.2
10
11/15/12 18:00 11/18/1217:40 7440-66-6
7471 Mercury
Analytical Method: EPA 7.471
Preparation Method:
EPA 7471 --
( 7ury
0.49 mg/kg
0.029
10
11/19/1212:10 11/20/121629 7439-97-6
Fercent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
1.8 %
0.10
1
11/14/12 13:29
92210E Fecal Coliform, MPN RAIL
Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN
2.2 MPN/g
0.010
1
11/14/12 10:35 1g,H1
254OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
98.2 %
0.000010
1
11/14/12 09:19
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.7 Std. Units
0.10
1
11/26/12 11:20
Plant Available Nitrogen
Analytical Method: 40CFR PART 432.2
Plant Available Nitrogen
6940 mg/kg
1.0
1
11/29/12 13:53 N2
Total Nitrogen Calculation
Analytical Method: 40CFR PART 432.2
Nitrogen
22800 mg/kg
40.0
1
11/29/12 13:55 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
498 mg/kg
8.6
1
11/14/12 13:35 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
22800 mg/kg
2120
50
11/27/12 16:42 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
jogen, Nitrate
ND mg/kg
2.0
1
11/20/12 23:38
Date: 11/29/2012 01:55 PM REPORT OF LABORATORY ANALYSIS Page 4 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

acekalyiical
www.pacelabs.com
i
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Dried Residual 11/13
—
Pace Project No.: 92138358
= -
Sample: TWSA DRIED RESIDUAL-
Lab ID: 92138358001 Collected:-- 11/13/12 10:00
Received: 11/13/12 12:38 Matrix: Solid -
Results reported on a "dry -weight"
basis
-
Parameters
Results Units
Report Limit DF
Prepared-_,. Analyzed CAS No. Qua[ -
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2-
Nitrogen, Nitrite
ND mg/kg
- 0.99 -1
11/20/12 23:38
Nitrogen, NO plus N63
ND r-bg/kg
2.0 1-
11/20/1223:38
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
-`
Phosphorus
22100 mg/kg
653=. 250
11/27/1211:12 7723-14-0
I
Date: 11/29/2012 01:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceflnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
/ wwwpacelabs.com
t [phone] [phone] [phone]
QUALIFIERS
Project: Dried Residual 11/13
Pace Project No.: 92138358
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution'of
the sample aliquot, or moisture content. -- -
ND - Not Detected at or above adjusted reporting limit. - -
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. -
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit. _
RL - Reporting Limit.
S - Surrogate -
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate) - - -
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference - -
NC - Not Calculable. ---
SG --Silica Gel - Clean-Up=-
U - Indicates the compound was analyzed for, but not detected.--
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for - -
i 1 each analyte is a combined concentration.
/ Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
ig This is a less than value.
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TNI accreditation for this parameter.
Date: 11/29/2012 01:55 PM REPORT OF LABORATORY ANALYSIS Page 16 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

UMM. I
ENVIFiONMENTAL.TI 014NOLOG1ES, INC. -
- - --
Analytical Laborgtories = -
-
::LABORATORY REPORT -- - -� -
- Client
i = --
-- _-_Pace Anafytical Services, Inc.
- 2225 Riverside Drive
- : _. - . Ash ville, NG 28.804
8rder Number
= 1227260 _.
- Project Number
- 921.38358 =
r Issued
- Fridays November 23, 2012
Total Number of Rages:
4 (excluding G:O.G, and cooler receipt form)
Apprwed .
y Ab
a,
Q.-Manager- .�
Certificatlonw. A21AlDOD 0724;01, Alabama 41000, Arkansas a8-b735, Cal(fonria 07256CA, Colorado, Connecticut PH-6105,
Delaara!k Florida NELAC E47688', Georgia E87688 an 949,, Idaho OH00823, IUfnois 200081 and Reg.5, Indiana
C-OH-13, Kansas E-1Q347, Kentucky (underground Storage. Tank) 3, Kentucky 90146, Louisiana 04061 'and
'LA12004, Maine RQ190101 Maryland 339, Massachusetts M-OPH923, AAichip&n (Re46, Louisiana
nta 409711,1'an
Montana CERT0098, New Hainpshin32996. Neer Jersey OH006, New York 11777; Ndrth Caiolina 39705 and
631, Ohio.4170, Ohio VAP• CL0052, Oklahoma. 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island
LAOIID317, South Carolina 8201600-1, Tennessee TN04018, Texas:T104704466-11-6, Region 5 WG1U Region.
a MUS-L,. USDAIAPHIS P32tt=11-00244 Utah OH00923201IA, Vermont VT-87688,. Virginia 00-440 and 15tt1,
Washington C891; .West Virginia 248. and 9957C and E87688,. Wisconsin 399013010
"Analytical lnte9rlty" • EPA Certified NELAP Certified
3310 Win Street. ; GUYS11109a Farts, Ohio 44M • . i2b, e. 33E9-53 82i1 Fax. [phone]
1 WebSite. www..set#ek:Forri

ENVIRONMTAL TEO AI.OLOGIES, 1NC,
— - _ -
frMalkftait'aboratorjes-
2
_ - Sample Summary
Client: Pace Ahalvfical Services Inc -_
Order Number: 1227260
- - -_
La6aratory ID Client ID . Matrix :" -'-= - _-
Sampling Date -_- -
1227260-01 02138358001 Solid 4= - - - _ - 11 /1.3/2012----
"Analytical Integrity" - EPA Certlfied - NELAP Certified
3310 Win Street Cuyahoga Falls, ©hiq 44223 i Phone: [phone] Fax: 330�253-4489
Web Site: ww.settek.csm,

Client#: Pace Analytical gervices. Inc.
Order Number. -1227260 ---
-Solid sample results -are reported: on a wet Weight basis •except as noted. -
No problems were encountered during -analysis of this order number, =excep# as noted.
Data Qualifiers: -
B = Analyte found in the method blank
d Estimated concentration of analyte bet n MDL (LOD) and Reporting Limit (LOQ)`-
C = Analyte. has. been confirmed by another instrument or method
E = Analyte-exceeds the. upper limit of the calibration_ curve. Matrices:
D. = Sample or exttactwas analyzed at a higher dilution q _pin
X = User defined data qualifier. c = Cream
$'= Surrogate out ofcontrof limits DW= Drinking Water
U = Undetected . L =.Ligdid
a = NotAccredited.by NELAC 0 =,O.ir
ND = Non Detected at LOQ
DF = Dilution Factor
Limit.Of QUantitation- (LOQ) = Laboratory Reporting Limit (not adjusted for. dilution factor)
Limit Of Detection (LOD) = Method Detection Limit
Practical Quantitation Limit (PIQL) = (same as LOG)
Method Detection Limit (MDL) = (saffie: as LOD)
Reporting Detection Umit -(RDL) = (same as.LOD)
Estimated uneer ainty values aWavailable upon request. - - -
Thetest results meet the requfrements: of the: NELAG standard, except.where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies. Inc. and that of. the client. Itmannot
be reproduced in any form without the consent of Sdinmit Ehvironrnental Technologies, Inc. or the client for which this
report was issued. The results .*contained in this report are only representative of the samples received. Conditions
can vary at different tunes and at different sampling conditions. Summit Environmental -Technologies,. Inc. is not
responsible fot use or interpretation of the data included herein.
"Analytical )ntegrity" • EPA Certiflect • N)ELAP Oertified
3310 Wirt Street . Cuyahoga Falls, Ohl.6 44223. • Phone: [phone] . Fax! 330-263.4489
We :84e: "ww..settek;com

S-U,
ENVIRONMENTALTECHNOLOGIRS, INC.
Analy tical-Laborat6ries
Climupm Lob ]DO Collected Mo to
92138358001 1227260-01 13-Nov-13. Flash Point
N6vembcr'A 20.12
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville. NC 28864
Received 1If14/20.12
.Pro j edt: #: 9213 83 5 8
nits VJ_1 Method Dh .L00 dnnlvsi
>140 °F S 1010 .1 19-Nov-12 TAH
gient.1MLsblDff
92138358001
-1727260-01-
C to lected Anahl
13-Nov-12 pH
�
Mahkihd
DE
LOO_
1—
5.89 @ 20.6C S.U. S 9M
1
0.01
15AM-12- SMI-
-Ment.IDl
92138358001
LahID#
122726D<OX
Collected nal¢e
13-Nov-12 Reactive Cyanide.
-- - - _
'NO
nits Iytetfiod `
p
LD
Rim Analyst
PPm S 7.3. 3.2'
1.
0.5
15-Nov-12 T1R
C ' t -Lv
9213ti358001
Lab ID#
122726001
Ct9 le - AnAlsResult
18-Nov 12 ReadSuffide
- --- `
- ' at ' t d
p� -
LCg
'n A�
ND ---
Ppm S • 7.3.4.2
1
25
157Nov-12 TIR
Page 4
"Arralytfcal 1J7te9rffy" • EPA Certified - NELAP Certified
3310 Win. Street Cuyahoga falls, Ohio 44223 - Phone: [phone] Pax: 330253-4.489
r i
Web Site: t+utrrtvsettek.eprrr

SunimIt Envirchmental Technologies, -lite. -i
00618ir ftecelpfforM
SIMON 1�11tlipRLs
OrderID: .12,2726o
COOLER
Ord of
1,09 I.nInit
Dale Recaked; Time'RecelvedlCC? _Date 6paried: 1-1
Number of ec
�U-Pe-
N/A
Unpacked
Shipper
U."9Postal
Walk-in Pickup Other.,
P#ftgIng; Pean,6 xtw'e �Wfa —paper-
roam
None Other
Tape an arm,..
N N/A
Custody Seals Intea
by
N NIA
C-0-C in plastic
N
Coolant: 14X'Blue I
Sample Temperature, c
C-0-C filled Out properly
N NA
SOmP]ft Ift separate, begs
R N/A
SSM* containers Intiot
N NIA
Iff no, list brok4n temple
Sample ftVWG (10, data, sic.)
N
-
MIA
Label(s) agree with C-(.:.c
WA
COMI COMIAIMrs used
N
NIA
Suffident UM* received
N
NIA
Sample; at CDffW ON? OW below)
y
Rubbles, absot.from 46'.mL vW10,*
y
N.
"'SoMples with bubbles Ion then the size of a
pea are soo9ptebib.
DateRnle
Comments

Appendix E
TCLP Analysis --

C6Analyt cal
www.pacelabs.com
i -
Pace Analytical Services; Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
June 21, 2012
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street'
Sylva, NC 28779
RE: Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547 -
Pace -Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by=the-laboratory-on=June=07,,2012:- The- -
- results relate only to the samples included in this report: -Results =repo rted-h-erein-conform to the --
most current TNI standards and the laboratory's Quality Assurance Manual; where -applicable; unless
otherwise noted in the body of the report. - _=-----
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
5 c rely,
tom.williams@pacelabs_.com
Project Manager -- _
Enclosures
o REPORT OF LABORATORY ANALYSIS Page 1 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
8':

- Pace Analytical Services, Inc. Pace Analytical Services, Inc.
cal® 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.paceleb:crom
. riP, An6ZI�Is.com -
- - Eden, NC 27288 Asheville, NC 28804
- [phone] [phone]
CERTIFICATIONS
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
Ormond Beach Certification IDs -
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Arizona Certification M AZ0735
-Colorado Certification: FL NELAC Reciprocity
Connecticut Certification M PH 0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate M 05007
Maine Certification #: FLO1264
Massachusetts Certification #: M-FL1264
Michigan Certification M 9911
Mississippi Certification: FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
_ -North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. M 99006003
Virginia Drinking Water Certification #: 00213
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification M 37712
North Carolina Wastewater Certification #: 40
- Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification M 2958
New Jersey Certification #: FL765
New York Certification M 11608
North Carolina Environmental Certificate M 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
U.S.Virgin Islands Certification: FL NELAC Reciprocity
Virginia Certification #: 00432 -
Virginia Environmental Certificate M 460165
Washington Certification M C955
Wyoming Certification: FL NELAC Reciprocity
Wyoming (EPA Region 8): FL NELAC Reciprocity
Connecticut Certification M PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84 -- -
Louisiana DHH Drinking Water-# LA 100031 -
West Virginia Certification M 357
Virginia/VELAP Certification M 460144 - " _
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 17

= - Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® -- 205 East Meadow Road - Suite A _ _ 2225_Biverside Dr.
www.pacelabs.com
aCG'A�la�j/IICc?� - Eden, NC 27288 Asheville, NC 28804
-
- - [phone] [phone]
- SAMPLE SUMMARY
Project: TWSA Dried Residual TCLP _
Pace -Project -No.: - - 92120547 -
Lab ID Sample ID Matrix Date Collected . - Date Received
92120547001 TWSA Dried Residual Water - 106/07/12 11:00 =-' 06/07/12-13:32=-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey-Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17

aceAnalytical
wvmpscelabs:com
Pace Analytical Services, Inc.
- 205 East Meadow Road -Suite A
-- _ _ - - - Eden, NC 27288
— [phone]
Project: TWSA Dried Residual TCLP -,-,--------,Pace Project No.: - 92120547 - -
Lab ID Sample ID
y _92120547001 TWSA Dried Residual
= Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Method -
Analysts
Reported
Laboratory
-" EPA-8081
RES
8
PASI-C
EPA $151
LJM
3
PASI-O
EPA 6010
JMW
7
PASI-A
EPA 7470
SHB
1
PASI-A
EPA 8270
PPM
18
PASI-C
EPA 8260
DLK
15
PASI-C
EPA 9095
LMD
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 4 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
e?CG'A/lc?�yf1Ca� -' Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs.com
[phone] [phone] [phone]
ANALYTICAL RESULTS —
Project:._._ ... TWSA Dried Residual TCLP
Pace -Project No.: 92120547 --
Sample: TWSA Dried Residual Lab ID: 92120547001 Collected: 06/07/12 11:00 Received: 06/07/12 13:32 Matrix: Water
Parameters
8081 GCS Pesticides, TCLP SPE
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP, TCLP
1
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methyl phenol(o-Cresol )
3&4-Methylphenol (m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Results Units Report Limit DF Prepared Analyzed CAS No. Qual -
Analytical Method: EPA 8081 Preparation Method: EPA 3535
Leachate Method/Date: EPA 1311; 06/13/12 16:00
ND ug/L
2.5
5
06/14/12 10:00
06/20/12 14:00
58-89-9
ND ug/L
15.0
5
06/14/12 10:00
06/20/12 14:00
57-74-9
ND _ug/L
2.5
5
06/14/12 10:00
06/20/12 14:00
72-20-8
ND ug/L
2.5
5
06/14/12 10:00
06/20/12 14:00
1024-57-3
ND ug/L
5000 _
5
06/14/12 10:00
06/20/12 14:00
72-43-5
ND ug/L
15.0
5
06/14/12 10:00
06/20/12 14:00
8001-35-2
0 %
10-138
5
06/14/12 10:00
06/20/12 14:00
2051-24-3 D3,S4
0 %
10-110
5
06/14/12 10:00
06/20/12 14:00
877-09-8 S4
Analytical Method: EPA 8151
ND mg/L
0.010
1
06/13/12 07:45
06/14/12 04:11
94-75-7
ND rrig/L
-0.010 -
1
06/13/12 07:45
06/14/12 04:11
93-72-1
106 %
70-130
1
06/13/12 07:45
06/14/12 04:11
19719-28-9
Analytical Method: EPA 6010 Preparation -Method: EPA 3010
Leachate Method/Date: EPA 1311; 06/16/12 16:00
ND mg/L
0.025
1
06/19/12 15:30
06/20/12 16:14
7440-38-2
ND mg/L
0.50
1
06/19/12 15:30
06/20/12 16:14
7440-39-3
ND mg/L
0.0050
1
06/19/12 15:30
06/20/12-16:14
7440-43-9
ND mg/L
0.025
1
06/19/12 15:30
06/20/12 16:14
7440-47-3
ND mg/L
0.025
1
06/19/12 15:30
06/20/12 16:14
7439-92-1
ND mg/L
0.10
1
06/19/12 15:30
06/20/12 16:14
7782-49-2
ND mg/L
0.025
1
06/19/12 15:30
06/20/12 16:14
7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 06/16/12 16:00
ND ug/L
0.20
1
06/20/12 08:40
06/20/12 13:41
7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510--_---
Leachate Method/Date: EPA 1311; 06/13/12 16:00
ND ug/L
50.0
- 1
- 06/14/12 09:00
06/15/12 17:54
106-46-7
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
121-14-2
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
87-68-3
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
118-74-1
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
67-72-1
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
95-48-7
766. ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
98-95-3
ND ug/L
100
1
06/14/12 09:00
06/15/12 17:54
87-86-5
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
110-86-1
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
95-95-4
ND ug/L
50.0
1
06/14/12 09:00
06/15/12 17:54
88-06-2
Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS Page 5 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnaiytical
www.pacelabs.com
Pace Analytical Services, Inc.
- _ 205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
- 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
Sample: TWSA Dried Residual Lab ID: 92120547001 Collected: 06/07/12 11:00 Received: 06/07/12 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV TCLP Sep Funnel Analytical -Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 06/13/12 16:00
Surrogates
Nitrobenzene-d5 (S)
41 %
12-102
1
06/14/12 09:00
06/15/12 17:54
4165-60-0
2-Fluorobiphenyl (S)
41 %
13-107-
1
06/14/12 09:00
06/15/12 17:54
321-60-8
Terpheny1-d14 (S)
54 %
21-132
1
06/14/12 09:00
06/15/12 17:54
1718-51-0
Phenol-d6 (S)
19 %
10-110
1
06/14/12 09:00
06/15/12 17:54
13127-88-3
2-Fluorophenol (S)
26 %
10-110
1
06/14/12 09:00
06/15/12 17:54
367-12-4
2,4,6-Tribromophenol (S)
60 %
27-108
1
06/14/12 09:00
06/15/12 17:54
118-79-6
8260 MSV TCLP
Analytical Method: EPA 8260
- ,
Benzene
ND ug/L
190
38
06/08/12 18:21
71-43-2
2-Butanone (MEK)
ND ug/L
-380
38
06/08/12 18:21
78-93-3
Carbon tetrachloride
ND ug/L
190
38
06/08/12 18:21
56-23-5
Chlorobenzene
ND ug/L
190 ..
38
06/08/12 18:21
108-90-7
Chloroform
ND ug/L
190
38
06/08/12 18:21
67-66-3
1,4-Dichlorobenzene
ND ug/L
190
-38 - -
06/08/12 18:21
106-46-7
1,2-Dichloroethane
ND ug/L
190
--38 -
06/08/12 18:21
107-06-2
1. 1-Dichloroethene
ND ug/L
-190--=38.----
06108/1218:21
75-35-4
.'etrachloroethene
ND ug/L
190
38
06/08/12 18:21
127-18-4
Trichloroethene
ND ug/L
190
38
06/08/12 18:21
79-01-6
Vinyl chloride
ND ug/L
190
38
06/08/12 18:21
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
130 %
70-130
38
06/08/12 18:21
17060-07-0 1 g
Toluene-d8 (S)
102 %
67-135
38
06/08/12 18:21
2037-26-5
4-Bromofluorobenzene (S)
100 %
70-130
38
06/08/12 18:21
460-00-4
Dibromofluoromethane (S)
120 %
70-130
38
06/08/12 18:21
1868-53-7
9095 Paint Filter Liquid Test
Analytical Method: EPA 9095
Free Liquids
0 mL/5min
1.0
1
06/12/12 22:24
Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/�
205 East Meadow Road - Suite A 2225 Riverside Dr.
Analytical Eden, NC 27288 - Asheville, NC 28804
www.pacelabs.com
j [phone] [phone]
i QUALITY CONTROL DATA
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
Pace Analytical Services, Inc.
_- 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: GCSV/8829
Analysis Method: EPA 8151
QC Batch Method: EPA 8151
Analysis Description: 8151 GCS Herbicides TCLP
Associated Lab Samples: 92120547001--
METHOD BLANK: 407955
Matrix: Water- -
Associated Lab Samples: 92120547001
- -
__ _ Blank Reporting
_ Parameter
Units
Result Limit Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
ND 0.010 06/14/12 03:10
2,4-D
mg/L
ND 0.010 06/14/12 03:10
2,4-DCAA (S)
%
84 '70-130 06/14/12 03:10
LABORATORY CONTROL SAMPLE:
407956
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
2,4,5-TP (Silvex)
mg/L
.012 0.012 - 104 70-130
2,4-D,
mg/L
.06 0.058 97 70-130-
2,4-DCAA (S)
%
- - 88 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 407957
407958
-
_ -
T.
MS
MSD
92120547001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
2,4,5-TP (Silvex) mg/L ND
.012
.012
0.012
0.012
104
99
70-130
5 40
2,4-D mg/L ND
.06
.06
0.062
0.058
103
97
70-130
6 40
2,4-DCAA (S) %
112
107
70-1.30
Date: 06/21/2012 06:47 AM
REPORT'OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr.
�?CEIi%�CZIICCZI - Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com
- _ [phone] [phone]
QUALITY CONTROL DATA
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/4307
Analysis Method:
EPA 7470
QC Batch Method: EPA 7470
Analysis Description:
7470 Mercury TCLP
Associated Lab Samples: 92120547001
METHOD BLANK: 781964
Matrix: Water
Associated Lab Samples: 92120547001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
ug/L
ND 0.20 06/20/1213:35 -
LABORATORY CONTROL SAMPLE:
781965
- _-
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
ug/L
2.5 = _ 2.5
99 80-120 - -
MATRIX SPIKE SAMPLE:
781966
92121338001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result— % Rec
Limits Qualifiers
Mercury ---ug/L--
ND-- --2.5
3.1 126
75-125 M1
SAMPLE DUPLICATE: 781967
92121370001 Dup
Max
Parameter
Units
Result Result
RPD RPD
Qualifiers
Mercury
ug/L
ND ND 20
Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

Pace Analytical Services, Inc. Pace
Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical ®
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacelab&com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: TWSA Dried Residual TCLP
Pace Project -No::- 92120547
-
QC Batch: MPRP/10850
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010
MET TCLP
Associated Lab Samples: 92120547001
METHOD BLANK: 781566
Matrix: Water
Associated Lab Samples: 92120547001-
-
'
__._.". Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
Arsenic
mg/L
ND 0.025
06/20/1216:00
Barium
mg/L
ND 0.50
06/20/1216:00
Cadmium
mg/L.
ND -- 0.0050
06/20/1216:00
Chromium
mg/L
ND 0.025
06/20/1216:00
Lead
mg/L
ND 0.025
06120/1216:00
Selenium
mg/L
ND 0.10
06/20/1216:00
Silver
mg/L
ND 0.025
06/20/1216:00
LABORATORY CONTROL SAMPLE:--781567
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Arsenic
- mg/L --
2.5
= 2.6
104
80-120
)arium
mg/L
2.5
- 2.2
89
80-120 -
Cadmium
mg/L
2.5
2.4
98
80-120
Chromium
mg/L
2.5
2.5
101
80-120
Lead
mg/L
2.5
2.3
93
80-120
Selenium
mg/L
2.5
2.6
105
80-120
Silver
mg/L
1.2
1.2
98
80-120
MATRIX SPIKE SAMPLE:
781568
92121338001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.7
108
75-125
Barium
mg/L
ND
2.5
2.7
92
75-125
Cadmium
mg/L
-ND _---2.5
2.5
-102
75-125
Chromium
mg/L
ND
2.5
2.6
105
75-125
Lead
mg/L
ND _
2.5
2.4
- 96
75-125
Selenium
mg/L
ND
2.5
2.7
108
75-125
Silver
mg/L
ND
1.2
1.3
100
75-125
SAMPLE DUPLICATE: 781569
Parameter
92121368001 Dup
Units Result Result RPD
Max
RPD Qualifiers
Arsenic
mg/L
ND ND
20
Barium
mg/L
ND .16J
20
Cadmium
mg/L
3.8 3.8 1
20
Chromium
mg/L
1.1 1.1 1
20
Lead
mg/L
8.5 8.4 1
20
Date: 06/21/2012 06:47 AM
REPORT OF LABORATORY ANALYSIS
Page 9 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc._ Pace Analytical Services, Inc.
5keAnalyfical' 205 East Meadow Road - Suite A _ - _ 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
www.pacefebs.com
------[phone] [phone]
QUALITY CONTROL DATA
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547--
SAMPLE DUPLICATE: 781569
- Parameter Units
Selenium mg/L
Silver mg/L
92121368001 Dup
Result Result
ND ND
ND ND
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD RPD Qualifiers
20
20
Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS Page 10 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

QP
aceAnalyfical
www.pacefabsxom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: TWSA Dried
Residual TCLP
_ Pace Project No.: 92120547
QC Batch: MSV/19379
QC Batch Method: EPA 8260
Associated Lab Samples: 92120547001
METHOD BLANK: 775586
Associated Lab Samples: 92120547001
Parameter
Units
1,1-Dichloroethene
ug/L
1,2-Dichloroethane
ug/L
1,4-Dichlorobenzene
ug/L
2-Butanone (MEK)
ug/L
Benzene
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroform
ug/L
Tetrachloroethene
ug/L
Trichloroethene
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
}oluene-d8 (S)
%
LABORATORY CONTROL SAMPLE:
Parameter
775587
Units
1,1-Dichloroethene
ug/L
1,2-Dichloroethane
ug/L
1,4-Dichlorobenzene
ug/L
2-Butanone (MEK)
ug/L
Benzene
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroform
ug/L
Tetrachloroethene
ug/L
Trichloroethene
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8260 -
Analysis Description: 8260 MSV TCLP
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ND
5.0
06108/1211:43
ND
5.0
06/08/12 11:43
ND
5.0
06/08/12 11:43
ND
10.0
06/08/12 11:43
ND
5.0
06/08/12 11:43
ND
5.0
' 06/08/12 11:43
ND
5.0-
06/08/12 11:43 -
ND
5.0
06/08/12 11:43
ND
-5.0--06/08/12
11:43 -
ND
5.0 -
06/08/12 11:43
ND
5.0
06/0811211:43
109
70-130
06/08/12 11:43
100
-70-130-
06/08/12 11:43
105
70-130:-
06/08/12-11:43
102
67-135
06/08/12 11:43
Pace Analytical Services, Inc.
9800 Kincey Ave.- Suite 100
Huntersville, NC 28078
-[phone]
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
50
55.9
112
70-141
50
56.8
114
70-139
50
46.9
94
70-141
100
109
109
63-150
50
55.8
112 -
70-132
50
53.6
107
70-150
50
52.4-
105
70-134 -
50
55.0 -
110
70-130 - -
50
49.4
99
70-137
50
51.3
103
70-131
50
50.7 -
101
56-144 -
100
70-130
99
70-130
103
70-130
101
67-135
Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS Page 11 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® - - 205 East Meadow Road - Suite A 2225 Riverside Dr.
aceAnalXical Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com
/ /[phone] [phone]
'
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
QC Batch: OEXT/17858
QC Batch Method: EPA 3535
Lab Samples: 92120547001
IAssociated
METHOD BLANK: 778727
Associated Lab Samples: 92120547001
Parameter -
Units
Chlordane (Technical)
ug/L
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
-'
LABORATORY CONTROL SAMPLE:
778728
Parameter
Units
:ndrin
ug/L
gamma-BHC (Lindane),
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
QUALITY CONTROL DATA
Analysis Method: EPA 8081
Analysis Description: 8081 GCS TCLP Pesticides
Matrix: Water
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
ND
= 3.0
06/20/1213:25
ND
- - 0.50
06/20/1213:25
ND
0.50
06/20/1213:25
ND
0.50
06/20/1213:25
ND
1000
06/20/1213:25
ND
3.0
06/20/1213:25
124
- 10-138
-06/20/1213:25
103
10-110
06/20/1213:25
Spike
LCS
LCS % Rec
Conc.
Result
% Rec Limits Qualifiers
1.2
1.6
133
20-134
1.2
1.4
110
20-118
1.2
1.3
109
22-133
3.7
ND
131
44-150
124
10-138
105
10-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
778729
MS
Parameter
92120639001
Units Result
Spike
Conc.
Endrin
ug/L
ND
2.5
gamma-BHC (Lindane)
ug/L
ND
2.5
Heptachlor epoxide
ug/L
ND
2.5
Methoxychlor
ug/L
ND
7.4
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
Date: 06/21/2012 06:47 AM
0
778730
MSD
Spike
MS
MSD
MS
MSD
% Rec
Max
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qua]
2.5
1.6
1.7
66
70
21-133
6 30
54 -"-
56
24-119
3 30
2:5--
----1.3-
= 1.5
52
- 60
50-150
13 30
7.4-"-=
.- ND
ND
61
62
50-150
30
- - -
92
81
10-138
-
92
94
10-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 17

aceAnalXical
www pacefabs.com.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: -- _-_... __TWSA Dried Residual TCLP-
Pace Project No.: 92120547
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
I QC Batch: OEXT/17856
QC Batch Method: EPA 3510
Associated Lab Samples: 92120547001
Analysis Method: EPA 8270
Analysis Description: 8270 TCLP MSSV
METHOD BLANK: 778660
Matrix: Water
Associated Lab Samples: 92120547001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
06/14/12 18:45
2,4,5-Trichlorophenol
ug/L
ND
50.0
06/14/12 18:45
2,4,6-Trichlorophenol
ug/L
ND
50.0
06/14/12 18:45
2,4-Dinitrotoluene
ug/L
ND
50.0
06/14/12 18:45
2-Methyl phenol(o-Cresol)
ug/L
ND
50.0
06/14/12 18:45
3&4-Methylphenol(m&p Cresol)
ug/L
ND
50.0
06/14/12 18:45
Hexachloro-1,3-butadiene
1
ug/L
ND
50.0
06/14/12 18:45
Hexachlorobenzene
ug/L
ND
50.0
06/14/12 18:45
Hexachloroethane
ug/L
ND
50.0-
06/14/12 18:45 -
_
ug/L
ND -
50.0
06/14/12 18:45
'Nitrobenzene
Pentachlorophenol
ug/L
ND
100
06/14/12 18:45
Pyridine
ug/L
ND
50.0
06/14/12 18:45 - -
2,4,6-Tribromophenol (S)
%
58
27-108
06/14/12 18:45
---2-Fluorobiphenyl (S)
%
64
13-107
06/14/12 18:45
-Fluorophenol (5)
%
35
10-110
06/14/12 18:45
Nitrobenzene-d5 (S)
%
65
12-102
06/14/12 18:45
Phenol-d6 (S)
%
24
10-110
06/14/12 18:45
Terphenyl-d14 (S)
%
88
21-132
06/14/12 18:45
L/1DVRH 1 Ur, I IJUPI 1 1111 J/11111LC: 110001
Parameter
1,4-Dichlorobenzene
ug/L
2,4,5-Trichlorophenol
ug/L
2,4,6-Trichlorophenol
ug/L
2,4-Dinitrotoluene
ug/L
2-Methylphenol (o-Cresol)
ug/L
3&4-Methylphenol (m&p Cresol)
ug/L
Hexachloro-1,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachloroethane
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Pyridine
ug/L
'2,4,6-Tribromophenol
(S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
'Nitrobenzene-d5
(S)
Phenol-d6 (S)
%
%
Terphenyl-d14 (S)
%
IDate:
06/21/2012 06:47 AM
Units
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits - Qualifiers
500
337
67
10-110
500
381
76
39-108
500
390
78
40-104
500
316
= 63
42-109
500
341- -
- - ---68
31-110--
500
300
-- � 60 —`
30-110 -
500
328
- - 66
10-110
500
-362 -
72
39-121
500
344
69
10-110
500
351
70
32-101
1000
788
79
18-108
500
229
46
10-110
75
27-108
80
13-107
48
10-110
83
12-102
32
10-110
87
21-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

1 Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr.
aceAnalXical Eden, NC 27288 Asheville, NC 28804
www pecelabs:com
[phone] [phone]
QUALITY CONTROL DATA
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
®
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 778662
92120102001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
778663
MS
Result
MSD
Result
1,4-Dichlorobenzene
ug/L
ND
500
500
334
2,4,5-Trichlorophenol
ug/L
ND
500
500
382
387
2,4,6-Trichlorophenol
ug/L
ND
.500
500
390
390
1
2,4-Dinitrotoluene
ug/L
ND
500
500
326
331
2-Methylphenol(o-Cresol)
ug/L
ND
500
500
367 -
377
3&4-Methylphenol(m&p
ug/L
ND
500
500
343
— 353
Cresol)
a
Hexachloro-1,3-butadiene
ug/L
ND
500
500
333
-323
Hexachlorobenzene
ug/L
ND
500
500
356
353
Hexachloroethane
ug/L
ND
500
500
336
330
Nitrobenzene
ug/L
ND
500
500
-348
337
Pentachlorophenol
ug/L
ND
1000
1000
-801 -
839
Pyridine
ug/L
ND
500
500
252
254
2,4,6-Tribromophenol (S)
1
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
(S)
%
%
—�
Terphenyl-d14
A
1
1
a
i
aDate: 06/21/2012 06:47 AM
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MS
MSD
% Rec-
Max - -
% Rec
% Rec
Limits
RPD
RPD Qual
67
66
30-150
2
30
76
77
30-150
1
30
78
78
30-150
0
30
65
66
30-150
2
30
73
75
30-150
2
30
69
71
30-150
3
30
67-
- 65.
30-150
3
30
71
71
30-150
1
30
67
66
30-150
2
30
70
67
30-150
3
30
80-
- 84
30-150
5
30
50
51
30-150
1
30
73
74
27-108
76
74
13-107
55
54
10-110
81.
80
12-102
41
41
10-110
83
87
21-132
Page 14 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/� ,,CpI�ICaI ® -205 East Meadow Road - Suite A 2225 Riverside Dr.
�Ce/ i! /- - Eden, NC 27288 Asheville, NC 28804
www.pecelabs.crom
[phone] [phone]
j
Project: TWSA Dried Residual TCLP
Pace Project No.: 92120547
fQC Batch: WET/21197
QC Batch Method: EPA 9095
Associated Lab Samples: 92120547001
0
QUALITY CONTROL DATA
Analysis Method: EPA 9095
Analysis Description: 9095 PAINT FILTER LIQUID TEST
SAMPLE DUPLICATE: 777815
92120955001 Dup
Parameter Units Result Result RPD
Free Liquids mL/5min 26 _ 23
I' 1
Date: 06/21/2012 06:47 AM
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers
Page 15 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
- -205 East Meadow Road - Suite A 2225,Riverside Dr.
CeAnalytical Eden, NC 27288 Asheville, NC 28804
www.paceiabs.com
[phone] [phone]
QUALIFIERS
Project: TWSA Dried Residual TCLP -
Pace Project No.: 92120547
Pace Analytical- Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
' the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the.adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit. -
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with -EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
i MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference -
NC - Not Calculable.
SG - Silica Gel - Clean -Up - -
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
1g 8260 results are from a total analysis which show that analytes are not present or that they are present but at such low
levels that the appropriate regulatory levels could not possibly be exceeded, per Section 1.2 of Method 1311.
' D3 Sample was diluted due to the presence of high levels of non -target analytes or other -matrix interference.-- -
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratorycontrol sample-(LCS) recovery.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
I
' Date: 06/21/2012 06:47 AM REPORT OF LABORATORY ANALYSIS Page 16 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

..-Pace Analytical Services, Inc. ._= Pace Analytical Services, Inc. =Pace Analytical'Services, Inc.
' _ _--•-,205 East Meadow Road - Suite A 2225.Riverside Dr. 9800 Kincey-Ave:-Suite 100
- ace naytica - - -----'Eden;
_ . _ "' - , NC 27288 -- ` ' �' Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs:com
[phone] [phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE — = - - _ _ -- == __-
Project:.: _ __-T W.SA Dried Residual TCLP = Pace Project No.: - 92120547 - -
Analytical
Lab ID Sample ID QC Batch Method QC Batch -- Analytical Method Batch---
92120547001 TWSA Dried Residual EPA 3535 - _ " 0EXT/17858 EPA 8081 == GCSV/12213
92120547001 TWSA Dried Residual EPA 8151 GCSV/8829 -EPA 8151.:- =- GCSV/6219
92120547001 TWSA Dried Residual EPA 3010 = MPRP/10850 EPA 6010--:- ICP/9969
' 92120547001 TWSA Dried Residual EPA 7470 _ MERP/4307 _ EPA-7470-_= MERC/4221
92120547001 TWSA Dried Residual EPA 3510 = = _ = OEXT/17856 EPA 8270-- MSSV/6392
92120547001 TWSA Dried Residual EPA 8260 MSV/19379 -
92120547001 TWSA Dried Residual EPA 9095 — --= WET/21197
— - - - -- - - --- - - --
1
Date: 06/21 /2012 06:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 17

//— _US'�y /, yticMegluw0IL Jocument
/ , ,/acehjauoical ® The Chain -of -Custody is a LE JOCUMENT. All relevant fields must be completed accurately. ;
% www.paculabs.com
Section A
Required Client Information:
Section B
Required Project Information:
Section C
Page:
of
C21
invoice Information:
apfC: I
Address:
rt To:
Attention:
1 4 9 0"
�'
Copy To:
Company Name:
to,REGULATORY:
?`
AGENCYAL
Email To:
�22 772
Address:
r NPDES . r GROUND WATER r DRINKING WATER
Purchase Order
No.:
Pece quote
.
Phone:
Project Name:
Reference:
r UST (— RCRA
r OTHER
�6
Pace Project
Manager.
Requested Due l)ate1TAT:
Project Number.
Pace Profile #:Y.
r•.
n
S7`AtE
�%
r Requested AnalysisFiItered
-
Section D
Matrix Codes
i
.—..............
Required Client Information
MATRIX I CODE
m
. o
` - COLLECTED
Preservatives
Z
=
•
Drinki ng Water DNWT
2
o
Sample ID-TWSA Dried Residual (non -discharge permit # WQ 0005763)
-
Water
Waste Water WW
9
v
I
U
COMPOSITE
COMPOSITE
"
Product
SL
START
EN°icRae
,�.•j
Sample date -
pf/ r�
SAMPLE ID
d
oil OL
m
0
�
WP
(A Z' D-g �')
a
z
Analysis Requested:
Sample
mple IDs'MUST BE UNIQUE
Airpa R
Tissue Ts
o
o
w
e
�,
N
Aluminum (Al) Molybdenum (Mo)
Total Nitrogen (N)
Other or
/ ^
RJi
•p�
. w
o; ,
=
o
0
..
Arsenic (Ar) % Total Solids
Total Phosphorous (P)
w
~
a
LL
n
rp�
o
o
L
a,
_.�
Cadmium (Cd) Nickel (Ni)
Ammonia Nitrogen (NH3-N)
u)
. DATE
TIME
AT) •
• TIME
CO
. 4k
D
=
2
=
z
z
2
o
Calcium (Ca) I ` Potassium (K)
Chromium (Cr) Selenium (Se)
Total Kjeldahl Nitrogen (TKN)
Corrosivity
::
l ' l .
Copper (Cu) Sodium (Na)
Lead (Pb) Zinc (Zn)
Ignitability
Reactivity
Magnesium (Mg) ph
TCLP (Full Scan)
'A:
Mercury (Hg) Fecal Coliform mpn/g
r
,"5
Plant Available Nitrogen (PAN) Surface
applied
W.
._iI
{
10
}
11:
:12'
ADDITIONAL COMMENTS
LINQl11SHEDBY%%►FFILIATIO
ArErTJME
qC CEFTED,BYIAFFILIATION
DATE
;!'TIME
1
SAMPLE CONDITIONS
i
I
SAMPLER NAME AND SIGNATURE t ' ; I �'
ORIGINAL
e7
0 ^
PRINT Name of SAMPLER:
S
d
o ci
SIGNATURE of SAMPLER:
f
DATE Signed
m
(MWDDIYY):
rn
C/)
- _ , - - rev. - ay- 007

Appendix F =
Annual Pathogen and Vector.---.,--.
Attraction Reduction

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Tuckaseigee Water and Sewer Auth. - Permit Number: , WQ 00005763
WWTP Name: TWSA Plant #1 NPDES Number: NC 0039578
Monitoring Period: From 1/1/2012 To - 12/31/2012
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑'_
Alternative 40 Alternative 5 ® Alternative 6 ❑"
If applicable to alternative perftirmed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying $1 Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B:
Alternative 10
Alternative 2 ❑
Alternative 3 ❑21
If applicable to 'alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens" -.—
Lime Stabilization` ' ❑
-"'""Air -"Air Diying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion[]r
'� � ` t,� ,�, n, .
oM...�,...xAe,
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level
; _; - = =- = -Pathogen Density
Number of
Frequency
Sample
Analytical
Parameter
in Sludge .
Excee-
of
Type
`- Tech-
Minimuir
Geo. Mean
Maximurr
Units
__,Z x.10 to the 6th..,...,
_...
..power MPN per
=gram of total: <.
-solids or 2 x 10 to
Fecal Coliform
-. -'Ahe 6th power-
_- -
_1000 mpnper- ...
gram of total solid
< 2
< 2
2
mpn/g
--0. -
quarterly
grab
S►�'1
q�aICE
weight)
Salmonella bacteria
3 WN per 4
(in lieu of fecal
grams total solid
coliform
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑
Option 2 ❑
Option 3 ❑
Option 4
❑
Option 5 ❑
❑ � s
❑ Option 10�
Option 6 ❑
P
O lion 7 ❑
P
Option 8 ®
P
Option 9
P
No vector attraction reduction options were performed
1133
- CERTIFICATION STATEMENT (please check the appropriate statement)
-.
® "I certify; -under penalty of law, that the pathogen requirements-in-40 CFR-503.32 and the vector
attraction -reduction requirement in 40 CFR 503.33 have been met"-
❑ "I certify, under -penalty of law, that the pathogen requirements in-40 CFR.503.32 and the vector
attraction reduction.requirement in 40 CFR 503.33 have not been met.""Please note if you check
this statement attach an explanation why you have not met -one -or both of the requirements.) -
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Stan Bryson, WWTP Supt.
Preparer Name and Title (type or print)
1 I
Signature of Pr er Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier ("%93M) RF (5/2003) Date

DRYER OUTPUT % SOLID
Dish. Wgt
rams
Wet Sample +Dish , '
rams
:: Dried Sample+ Dish."
rams

1st Dryer Batch v.
Fill�Cycle Started @ Dry Cycle Started @ 3 Discharge Cycle Started @ .S
Temperatures
�r
DRYER OUTPUT_/. Soug
os Dish•W t
:........
vvet Sample + Dish
TDried Sample +Dish
..
rams
rams
, ----- -
rams
v2v3
_
137-��`7 ;
:...
x100= ,
T otaf Solids
Li-%
:2nd Dryer Batch-
Fill Cycle Started ',@
DryCycle Started @
Discharge Cycle Started @
Discharge
Time Exhaust
Discharge.
roduct
eratures
Dry
ry ' ChamberEChamber Rotor ROtOf
Timer
. _
n
RYER OUTPUT %.
x100=
Total Solids

TWSA DRYER OPERATIONS
DAILY RECORD
3rd Dryer Batch ..
Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started ,@ _
Tem eratu' es
Time
Discharge
Exhaust
Discharge:..
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor.:.
Out
Operator
DRYER OUT PUT % SOLID , Dish Wgt Wet Sample., Dish Dried Sample +_ Dish-
rams rams `- rams

' TWSA., DRYER. OPERATIONS
- -
DAILY RECORD
-
DATE
START` STOP ,. TOTAL - - - -
RUN.TIME, HRS.
1 st Dryer Batch
Fill, Cycle Started @
I • J�
Dry Cycle Started :@. - �'- 3 Discharger Cycle Started @
Tem eratures -- -
- __ _ -_
a Discharge Discharge Dry - Chamber' Chamber . Rutor':
.
_ 'Rotor -
Time Exhaust
Product
Timer In Out. -- -In',
Out'- O erator
15
o g
DRYER ouTPUT io ouos - Dish W t
Wet. Sample +Dish Dried Sample;+ Dish:
-
-
:
rams
ms ...
rams
ni1,:
x 100
:..
tt
otaf Solids
end Dryer Batch
:.
Fill Cycle Started @
Dry Cycle Started @ Discharge Cycle Started @
Tem eratures '. '
Rotor
Discharge'
i Time Exhaust
Discharge
Product
Dry. Chamber Chamber Rotor
"timer '" 1n'
Out �n
but,. O erator,
1RYER OUTPUT %SouD .
Dish. Wgt
Wet Sample + Dish. Dried Sample +Dish
.
rams
rams rams
,'..'
X 100 ='
I
%Total Solids
uo712

DRYER ouTPUT Rio soua
Dish 1Ngf
"
Wet Sample +Dish ,
Dried Sample +Dish
- -
rams
rams .
rams
to
35.3fS1:
x'100 , Q.
o otal, Solids:
:2nd :Dryer Batch
:
Fill Cycle Started @
Dry Cycle Started @
pischarge Cycle Started
Discha . e
Time:Exhaust
Tem eratures :'
Discharge Dry:Chamber...chamber Rotor
:
-
Rotor
"
:limer.
..OutIn'
..
"O erator-
iRYER OUTPUT % souo
:
Dish Wgt
Wet Sample +.Dish.
Dried Sample .+Dish
rams
rams
rams
%
Total. Solids I
0602

Time
Discharge
Exhaust
Discharge
Product
Dry .
Timer.
Chamber
In
. Chamber
Out
Rotor
In
Rotor,
Out
Operator

Time
Discharge
Exhaust
Discharge
Product--_.
Dry _
-- Timer
Chamber
In,
.Chamber
Out
Rotor
In -
Rotor
Out
Operator

TWSA DRYER. OPERATIONS
DAILY RECORD
DATE-17
STOP O- ...;
START', TTAL
- - -
RUNTIME, HRS
-1 St Dryer Batch.
Fill Cycle Started @ Dry Cycle Started .6 Discharge Cycle Started @
Tem eratures
-Discharge
Discharge Dry . - Chamber.' Chamber Rotor -Rotor
Time Exhaust Product Timer 16 Out In^ Out
O erator
04
o
DJRYER 6 UTPII Soubs Dish'Wgt Wet Sample t Dish Dried Sample fDish
rams rams ' rams
- -
t.i� �-
:.. g . X oo�l
%`T oa' of s
2nd Dryer.Batch y'
t Fill Cycle Started @ ; Dry Cycle Started @
c7 scharge Cycle Started
y
Tern eratures
n erator
Discharge
Time Exhaust
Discharge Dry. enamber Chamber : Rotor Rotor
Product' ' ; Timer r In Out : '_'.. In '.. • . `::..Out-'
y�.3
')RYER OUTPUT °i° souD
.Dish-Wgt .: Wet Sample +Dish Dried Sample-t`Dish .
rams rams rams
76
Q/ �f
b ��
% Total Solids
2/6Y(2

Dry Cycle Started @ Discharge Cycle Started
Temperatures
Discharge
Exhaust
Discharge.
Product
Dry
Timer
Chamber
In
Chamber
Out
. Rotor
In
Rotor -Time
Out
Operator
DRYER OUTPUT % SOLID
Dish Wgt .
rams
Wet Sample 4-,Dish
rams `
Dried --Sample + Dish
rams

`
TWSA DRYER. -OPERATIONS
-
•DAILY.RECORD
DATE -.. .91
START ' STOP : "TOTAL
RUN TIME, HRS
1 St Dryer Batch
Fill Cycle Started @ 3
Dry Cycle Started @ a
- Discharge Cycle Started @
Tem eratures
_
Discharge' Discharge
Dry . ... Chamber .Chamber Rotor
-Rotor
Time - Exhaust Product
Timer' In Out, . In
Out O erator
0 :
f,
..
7: = -
a��3 3�,�,
q 3 ,-� - 3
DRYER OUTPUT Rio SOLIDS
Dish Wgt:
rams
Wet Sample + Dish Dried Sample + Dish
rams ' ' `'
rams
1,D15q
�i59c,
a3.29"oo
%Total Solids :-
2nd Dryer Batch
Fill Cycle Startetl @ J :Dry Cycle Started @ .1� f ►9. y ��.
. -. Dis' .h e C cle Started. @
Tem eratures
Rotor,
`erator,
Discharge Discharge
Time "Exhaust: .'Product :
Dry: :Chamber Chamber : Rotor
Timer 1n Out' In
Out O _
26
.. .:.
a �
1RYER OUTPUT %SOLID Dish Wgt
Wet Sample +:Dish . Dried Sample _+ Dish
rams
rams . rams
I• .
%Total Solids I
i

TWSA DRYER OPERATIONS -
DAILY RECORD
3rd Dryer Batch
Fill Cycle Started @ Dry Cycle Started @ Discharge _Cycle Started.@
Tem eratures
Time
Discharge
Exhaust
Discharge
`Product
Dry
Timer
Chamber -
In
Chamber
Out
Rotor- -
In
Rotor
Out
Operator
Jc
: 5
A c
an 7
1(
4 tz
.1-4.
46
S'. q
Z
a-,9L
3to
3_�4
913
S-
A Lo -
7
q3 6,
3 7.E
dd

Time .
Discharge
Exhaust
Discharge.
- Product
.Dry
Timer -
= Chamber
In '
Chamber
Out -
Rotor- .7--
An
'Rotor...
Out
-
Operator
GlV.
.goy
aJy
� 9
o
0
.VVy
- 36
yes
SP
DRYER OUTPUT % SOLID
Dish Wgt..
rams
Wet Sampie +.Dish
-rams
Dried.Samrle,+ Dish_
rams

Discharge: Dis , charge D r*y
Dry
Char'ber Chamber
amber
Rotor
Rotor Rotor
Rotor
Time Exhaust
P roduct
Ti mer
. Timer-
O
Out
In Out in Out
in Out
3 3 3 �a. Ra- --112-
0
0 erato
c;Vaq
a bb
01
*bb
.
D
DRYER OUTPUT.%. SOLLI 'Dish Wgt
Wet Sample
a +'bish .Dried Sample.+ Dis
rams'- -
rams (grams),
w.
lgrg�q
,
x.1.0 0
.
i
a a Solids
..'�2nd Dryer Batch
'Fill Started .15­[�L;P!3. Cycle. Staed Dry C Ycle Started 0- -
Dischar ge Cycle Start6d, (d-)
Tem'6' tures,
0 e r`at6r
Time
DischargeDischarge
Exhaust: *P rod'u,ct
Dry. a
Timer
:'Chamber..- ..Chamber -
In Out
Roti:!ii, Rotor
An
_7
3 Vf
�4 9.
32
e1V
)RYER-OUTPUT %
I - f vu- (0. .A, %J
yq
0a, X1001=..
.0611.2
%Total Solids

Time
Discharge
Exhaust
Discharge
'Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor---.
Out
Operator
3?
9
'e/V'
40 g'
-VV,
773
7.37
1136-
'VY6
3 Zzl
f51-°

Fill Cycle'Started @ • �j G C cie Started a� % 3
ry. y Discharge Cycle Started @
0 o y .{3
7.:fAf7
3gDea41
-
VIlet Sample + Dish
Dned:Sample + is
rams
rams ....
!�
x,00 @
Tetal
l
% Solids
)ry Cycle Started @ 3 / Discharge G��cle Started
;:Tem eratures-�
- -
Dry :>Chamber
Timer In:::
Chamber° ` Rofior
:;Out . ' _ >In :::...
'Rotor
;Out. O erator
3

-- , TVVSA `DRYER.OPERATIONS
. DAILrRECORD
TART:.. STOP TOTAL
RUN TIME, FIRS
1st.Dryer Batch
: FiIL Cycie Started @ . r 1C G Cycle �.y ' `� E�ischarg Cycle Started
-mac- ry y _
@
Tc� i ! perat
Mires
Dlschame Discharge Chamber
Time Exhaust Product Timer - In Out Ift
Out O erator:..'
6:o
a og ND y 3&-4
3 :.
s,4�--F14 3 '4
: 3g
DRYERoUrPvT %soclDs Dish Wgt, VI/et Sample +Dish Dned:Sample +
rams rams
`ski e�O3S�{
r
100
2nd Dryer Batch I 11
" FIII Cycle Started @ [ r L Dry Cycle Started @ 1 :a D ischarge Cycle Started @—
', . Tem eratures , 3
.
Discharge Discharge Dry .,Chamber Chamber. ; Rotor
'rime `Exhaust --product.": Timer In • :.:OUt In
Rotor
Out. iQ erator
..
_ -
DRYER, OUTPUT °lo SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + prsh ..
rams .. rams . rams :. .
CQ
-00
a O77t'' i '/ lD %Total
. .
Solids

Time.
Discharge]
Exhaust
Discharge,
Product
I Dry.
Timer
Chamber
in
Chamber
Uut
Rotor
in
Rotor.. ._
Out
Ci eraior
Z-7o-2
sa
6o7
21 6e
.?0,3
JOO
tly,1, i.
y37
32-
,5-510
4- 5
;735-
' .V'/v ..
l50
C/ ys
�3�
y5
3� .
: 537/0
39�_�s

Iao�r5 1139:
7
as ;
�3 a as a =s o.
=
a
a:
a L E
aa� ate- icy ; �:�
:�_ .3�
����:
���,.
10 % a 3 d.: a t' [o O ` ;�= qs
` �3ur
f �f �f,
3'(oaf `. ,1
.
lDRYER OUTPUT % souDs Dish Wgt Wet Sample +Dish
Dried Sample + Dtsh
=
`- rams : .: rams . .:
rams-
�aiG
2 ��3
e
d
O%o T
:. ,. 2nd Dryer Batch
Fill C cle Started Dry Cycle Started @
4_
Discharge Cycle Started @ o�J. "
77
Tem eratures ­::
Rotor
Discharge Discharge Dry :Chamber chamber:.. Rotor
1 Tmie Exhaust Product Timer In'::;Out
In
Out n erator
a;
sy :
yess
DRYERAUTPUT /° SOLIDS Dlsh W t-: Wet Sam le
g . p +Dish
Dried Sample + Dish
rams grams ..
rams-
�Oay„.
o
9
^
x 1`00 -
Total Solids
2I61-12

TVVSA, DRYER -OPERATIONS
DAILY RECORD
3rd Dryer Batch
'Fill Cycle Started @ Dry Cycle. Started @ . Discharge Cycle Started @
Tem eratures ..
Discharge Discharge I _= Dry- _ chamber chamber Rotor Rotor„ - =
Time Exhaust Product Timer in Out in Out Operator

Tirne
. ixhaust
Product
Timer In
out
In
r�
�
3�
R.
e
j DRYER ouTPur Rio soiiDs
Dish V11gt
Wet Sample +`Dish Dned.Sample + Dis
-
rams
rams : • .
grams)* `
a•
2nd Dryer Batch
I FdLcvria• Sfiarfgwi rni

tern eratures.
Discharge I Discharge, I DryChamber Chamber Rotor Rotor.,
Time. Exhaust Product Timer in (-)ut in Out Ca eraior

Time Exhaust
Product
T iner In
Out
Iri Out
O erator-
r
�; a.
�
- -
-
PT
:DRYER OUTPUT % sows
Dish Wgt.
Wet Sample +Dish
Dned:Sample + Dish
- ...
rams .
:_ .. rams '` .:.
rams
J.
.. .�
-
�aao�.T
o otal<Solids.:.
2nd Dryer Batch
Fil{ Cycle Started @
Dry Gycle 5iarted @
Discharge Cycle Started
}
Tem eratures `
y
Dlscharg�
Tmie `Exhaust
Discharge.:
Product -
Dry Chamber
Timer In
cnamber.
: Out
Rotor Rotor
(n Out .
C� erator
i
DRYER OUTPUT /u SOLIDs :Dish
Dried Sample .+. Dish ;
Wgt : ;'
Wet Sample + Dish .
:. :..
rams
rams
ra, Ms
...
x:1`00 =
..
%
Total Solids
I

Fill' Cycle Started;@ Dry Cycle Started @ Discharge Cycle Started @
i em eratures
Discharge I Discharge: I Dry Chamber Chamber Rotor. I Rotor,
Time. Exhaust Product Timer in Uut in I UU1 O erator

DRYER ouTPur soLiDs Dish Wgt Wet Sample + ♦Dish
bried '8ampI + Dish.-
._
rams :
rams :
rams':
.z
x 100
✓o Tota I Solids -
_
z
2nd Dryer Batch
; �
_
{ Fill Cycle Started @
I � .
Dry Cycle Started @
Y t
Discharge G��cle Started @
;
Tem p eratures'
Discharge
Discharge Dry ,chamber
Chamber: Rotor Rotor
rme Exhaust
Producf Timer In
Qut : In Out.
--Operator
Dried .Sample + Drsh
I DRYER-ourPur r s(?'Lipsj.
Dish. Wgt .; : Wet Sample + Dish - ,
rams rams
rams. `
x.100'-;
% Total Solids

. 1 ern eratures
Discharge I Discharge: I Dry. Chamber .Chamber Rotor_ Rotor..
Time. Exhaust Product rimer I in Out in Out Operator

TWSA DRYER.OPERA -IONS
`DAILY -RECORD_
DATE
ISTART`-
STOP TOTAL
RUB! TIME,.HRS
�7
a r,
1st Dryer Batch
Fill Cycle Started @
O Dry Cycle Stained @ i ti Discharge Cycle Started L /Zi D
Im
era_eUreS
Discharge JISChargG ui y CI -nb . chamber' :O ar (�O`►Eir
ITime Exhaust
Product Timer In Out In Out
O erator
1 (�
2 (p'.
3 w Zoe . ` '-/2
DRYER OUTPUT % soLIDs
Dish Wgt Vllet Sample + Dish DnedSample + Dish
Vss
r
rams rams ` . rams :
1 3 Vva
40
%Total Solids
k
2nd Dryer Batch
Fill Cycle Started @ / Dry Cycle Started @ d�' c5 3 .y Discharge Cslcie Started @'�9
Temperatures
jjPisb0airS(e'-*.Discharge,: Chamber chamber.'.' Rotor Rotor
Time ''Exhaust
Product Timer In Out < - :.'ln Out O erator
r�
DRYER:OUTPUT %SOLIDS
Dish Wgt„ Wet Sample +Dish Dried Sample .+ Dish
rams rams L V
rams
777
7(t 171�
x' 100
% Total Solids
2J6h12

%Vr9 f�. DRYER OPERATIONS .
DAILY RECORD
3rd Dryer Batch
Fill C ,cle'Started �� Dry Cycle Started Discharge Cycle Started V
Temperatures,
-Discharge I Discharge: I Dry chamber -
Time.
Exhaust
Product
l imer
in
:chamber,
uut
:Rotor_,
to
_Rotor:.::.
uut
O erator
air
�0-7.
, 50
���
��
3
-7 S'
.
��
237
aoS
/00
V37
yy4�
3?2-:53r°

TWSA DRYER. OPERATIOf�S . . ,.. .
.;
DAILY".RECORD
DATE Lo 14 J
1
STARTSTOP . :.TOTAL
----------------
RON TIME, HRS
1st Dryer Batch
Fill Cycle Started @
Dry y Cr? 1 Discharge Cycle Started @ cq Z
G C cie Started r� -� 1�_
i em craturas
Discharge Discharge a Di •^= ^
�� -� y %namber, :Chari.4,berv�tJi :oior
Ti. e "Exhaust Product
Timer In OIn Out rator
g� as T
aD%j
apt
:, 0 qab. 108 .'+ao- _
a �
a a5
:... DRYER OUTPUT Rio soiios Dish Wgt Wet Sample +Dish, Dried Sample + Dish
_
rams '
rams rants '
wa3
/yo3
1
y
x 100
a-os ;o;
_ o Total Solids .
2nd Dryer Batch
FiII Cycle Started @' •�
Dry C cle Started
Y @ • JrJY Discharge :Cycle `Started @ /✓
Tem eratures
Discharge
Discharge
Dry chamber Chamber' Rotor Rotor
Time Exhaust
Product
Timer :.` , ..'In :.: Qui In Out O erator
3 -
aDE
�100 445 39 -�y - 3$
3: o�ca �>
DRYER.OUTPUT pia SouDSF0O3
,
Wet Sample + Dish Dried Sample .+ Dish
rams ..rams
./�
9,c/�'7
.1�b
93 9- 4`7? 26
a
1743- D
x,100 = p. 9
3 9 h 7 71> % Total Solids

Fill Cycle Started:@ 'x Dry Cycle Started @ SOO Discharge Cycle Started @
.... Tamnarafi irac .
Time
Discharge
Exhaust
I Discharge
Product
I : Dry..
Timer
Chamber
in
Chamber
out
Rotor
in
Rotor.. .
Out
Operator
2
.s-
'���
2��
�o�
.:foo���
��/�
��7
S�
e ra
-23 ..
;;7��

TWSA DRYER.OPERATIONS ..
DATE
I'
START -STOP STOP TOTAL
RUN TIME, HRS
1 1 st Dryer Batch
Fill Cycle Started @
q
01 Dry Cycle Started @a l•� Discharge Cycle Stariea @ ,6157.
ITern
eratt gyres
Dlschai-c g Discharge DP y Chamber. Chamber Rolor „uivr
ITime ExhaUSt
Product Timer In Out. In Out O eretor
-
- - (0_ a �
.� q' . 3� EJO.. _
ri�,'c�,&�
- .alp
DRYER'OUTPUT % soups Dish Wgt Wet Sample+..Dish - Dried Sample f Dish
rams : rams rams
` °� TO OIIdS
2nd Dryer Batch
Fill C cle Started • S t 2 (o t.
Y @ Dry Cycle Started @ Discharge Started
.
Cycle @•
Tem •'eratures:'
Discharge:' Dry ;.-chamber Chamber Rotor Rotor
Discharge
Time Exxhaust
: Product Timer=::'In; Oufi In Out.. O erator,
off. �� �.
�o . • , .D yy� 3_��.qy­�� ..
01
DRYER OUTPUT %SOLID
Dish Wgt .. '. Wet Sample +Dish . Dried Sample +Dish
rams :. rams rams. ':
x1.00=
a rr b (2 : �P % Total Solids
1P

I ern eratures
Discharge I Discharge I . Dry. Chamber Chamber Rotor Rotor.
Time. Exhaust Product T-imer I in I Out I in Out Operator
DRYER OUTPUT%'sotlDs..Dish Wgt
: Wet Sample.... Dish,
-Dried:Sample i. Dish.
rams
rams
rams
.x 'l oo
Total Solids
,Alarms or CommentsG i I
f.-:f.� b't� r ..��—�,'
I I
• � •s
-
Gam'
,. .Q,'ain
.
�-;
..� G
C 0:1/1 .
C' BTi `ill T"a.` i 6VL
S
Gta
IL
IF

Disci urge
Disclarge
Di y
ihamrer
I Charnher
r:viar
� ( uiUr
TFj iie E haust
Product
Timer
In
Out
In
Out
O erator
0
L.
DRYER OUTPUT % SOLIDS DishKvo
Wet Sample + Dish
Dried Sample + Dish-
- - ...
ra
rams .
rams
to
�.�,.��
x100= e}%
:. ,D /a:: oho Total Solids•
2nd DryeCBatch
FIII C cle Started
I Y.. @
s.
-
�'.
Dry Cycle Started @ `� Discharge Cycle Started @ ��Q
4.
Tem 'eratures
Discharge
Time ' Exhaust
Discharge
',,Product
Dry ;Chamber
Timer .` In:
Chamber. Rotor
.Out- : ` In
Rotor
Out _.. O erator
ao-
7
1®0
'�
755
DRYER OUTPUT %'SOLIDS
Dish Wgt ; .
Wet Sample + Dish .
Dried Sample _+ Dish
rams
rams
rams
�g/'7 :.
:. ' � •.. ..
3
„� �)
.V (d % Total Solids

Tem eratures
Discharge . Discharge: I Dry chamber chamber Rotor Rotor. -
Time. Exhaust i'roduct Timer In Out in Out O erator

DISCtiar'geLDisrdl
a
�� y
Chamber.
ChamUel'
MvivrTime
Exhaustduct
Timer
In
out
In
dut
d erator
�
n
C'
R
7
IM . zi
me
:
o :.
�Go�S"36
3 �....
I27z2
t
ll
IDRYER' OUTPUT % souDs 'Dish Wgf Wet Sample +_ Dish
.. Dried Sample +Dish
-
rams
rams
rams.....Q
6.:
a3;3g a
I
o Total Solids .
.2nd. Diyer Batch ! P
Fill C cle Started ;
y @ Dry Cycle Started @ �� D Discharge dvcle Started @ 51" '
'Tempera`tures
Discharge:
Discharge
Dry
Chamber
Chamber.
Rotor`
Rotor
Time
:'Exhaust
" ".Product":
Timer':`
In
:. Qut.
_In.
Out
O erator
_
_��.
:
�..
-
50,
•
DRYER.OUTPUT % SOLIDS
Dried Sam ple..+ Dish
Dish .Wgt " Wet Sample + Dish
rams rams
rams `
S-
x 1:00 = qq
Sa v
% Total
Solids
2/6/•I2

em eratures
Discharge Discharge.I Dry I Chamber Chamber Rotor. Rotor... -
Time Exhaust' Product Timer 6n taut in Oui Operator

Discharge Diswiargc ems- ^i Ch I3` tom'
Y
t,amre, .
am Cr
.v. i
.uLuF
Time
Exhaust
Product
Timer
In
Out
In
Out
Operator
Of
" :
',' f ' e/ �
✓
� l✓�%
, . r� .:.
, •+mow `�%
�
��
..�, : %
•o
c.
�
.
`
Z
- .
t
o
.: DRYER OUTPUT % SOLIDS
Dish 1Ngt
Wet Sample +Dish
Dned.Sample + Dlsh
rams
' rams '
rams
�
n
x100-
o� TotaGSo(ids.:`
2nd DryerBatch
Fill C cle Started " D C cfe 5iarted Dischar e:C �cle Started'
Y- @ rY Y @ 1
9 @
Tem 'eratures
Time .. [:'E�,habsf-
Discharge
_
Discharge!
'Product ' :
D.ry
Timer
Chamber
In'.
Chamber:
::Out -
Rotor
In
Rotor
Out
Operator
-
.
T.
5-
bD
DRYER OUTPUT % sOLlos
:• Dried Sample ,+ Dish,
_Dish Wgt-,:
Wet Sample +. Dish . _
rams -,
rams .
rams :.
J
x .100
% Tofal'Solids'.
-1' .
J6112 '

Fill Cycle.Startedl c/11:5:
Dry Cycle Started @
Discharge Cycle.Started �
Temperatures
,.
Discharge
Discharge; I
. Dry
Time
Exhaust
Prod ct
-timer
-Chamber
in
.Chamber
Out -
; .Rotor
- in
Rotor..: ,.
Ou
u eraior
s_2^7
a 30
d .
i .5-o
y-7
y3
yV9
, 303
6-1-7
goy
10a
-Wo
yes
3,;13
v'�S
7-07
211
-150,
any
V3&
1
s
go
o
��6 .-
5 �) -,
.

Time
Dischwge
Exhaust
Discharge
Product
u; y
Timer
Chainber
In
'
Chanber v�Or
out In
:vI�Jr
out
D erator
8'33
cgb
b.
3..
DRYER OUTPUT % SOLIDS , Dlsh Wgt
Dried Sample +Dish -
VVet Sample + Dish,
rams
: rams :
grams .
x 10�
Total Solids.
l
2oyc
nd Diver Batch
Fill C cle Started r! s�
I y @
."
Dry Cycle Started @ 3 Discharge Cycle Started
R � Tem eratures
Discharge
Discharge;'
Dry Chamber
,chamber Rotor
Rotor
Time
=.'Exhaust
Product
Timer . In
..
Out : - In
Out
0 erator
-
ZM
A. A if
I
All
dos ..
® owl �y�
�31
DRYER:OUTPUT'%SOLIDS
Dried Sample+ Dish
Dish VUgt ;
. Wet Sample + Dish
rams
rams .
rams
1
IS�
x1.00-q
% Total Solids

Temperatures
Discharge Discharge:) Dry I: chamber chamber, Rotor. Rotor„
Time Exhaust Product Timer in Out in out Operator
DRYER. OU-T ?UT %'SOLID
Di.sh:W.gt :
;.filet Sample. =Dish
(grams)'
Dried Sample.. -. Dishhs
rams

-
TVVsA:DRYER.OPERATIQNS ;
F '
DAILY -RECORD ' -
DATE
START' STOP .. " TOT '.
RUN TIME, HRSf `7
`� pptt
1st Dryer Batch +
Fill Cycle Started cx O o1 Dry Cycle Started @ D �'`{ Discharge Cycle Started
1- ---- T!E�mc%tL•r$S -.
1
Discharge Diisciarge
Time . Exhaust Product
r�� y . Chamber
Timer In
Chamber
Out
;uiar
I In
Out
Operator
�-f J
co
o�� 3 a6
a4457
q3
-
14,3'77-
DRi(ER OUTPUT % souDs: _ Dish 1Ngt
Dried .Sample +Dish
Samp
1Nefi le +. Dish,
rt -
rams(grams)rants
J.ly , :Jr ��
:3
.x 100
% Total Solids
2nd Dryer Batch :. _
1 .Fill C cle Started .2
y @
�� . -,
Dry Cycle Started @ Discharge Cycle Started
`Tem `eratures
Discharge
Discharge
Dry Chamber
Chamber; Rotor Rotor
Time Exhaust
Product
Timer. :In
°' Out O erator _ -
�,� : c� o ...:
d•
• •:.. - j : "
1
.., ;tom . .+ -
V
q, : ',: -� .
O
, -�
_ ;
.10
DRYER.OUTPUT:% SOLIDs
Dried Sample +.Dish
Dish Wgt .
Wet Sample + Dish,
rams
: rams
rams
x1,00=
% Total Solids

T VVSA DRYER OPERATIONS
DAILY RECORD
3rd Dryer Batch
Fill Cycle Started: D C cie_Started Sy Discharge Cy le Started
Y @ ry 1+ @. g_ @
Temperatures.
Time.
Discharge
Exhaust
I Discharge:
I Product
I , Dry .
7-imer
Chamber
in
,chamber
I Out
;Rotor
I in
Rotor.
Out
Operator
30
0,!';'
So
41 ?V7
Vim;
-29�
J y
WO5
/oa
SIySj(JW7
-Vtl,3
150
.7 T3
7v
� )0
Vim.%
DRYER OUTPUTWsOL=fls. Dish.\hVgt . WetSample :.,Dish Dried Sarnple s_:Dish.,
rams rams rams

DRYER 6UTPUT Rio saLiDs
Dish Wgt Wet Sample
;. +:bish,
. Dned.Sample + Dish
rams -..
j.
- r
;2nd Dryer Batch
Fill C cle Started �� D C cle Started
Y @ ry y @ Discharge Cycle Started
,....
:.. :Tem eratu'ies
Discharge Dry _ Chamber Chamber Rotor Rotor
Discharge
Tmie
Exhaust
,Product: - r .Timer .:
. : In
: Out
- In .
Out ..
O erator
3
as
DRYER.OUTPtlT �o SOLlD
Dned Sample .+ Dish
Dish Wgt Wet Sample + Dish ..
.
rams rams
:..
:: rams : :. ,
/°Total Solids

em eratures
rge Discharg: Chamberhambe
.Discha: Dry.:. Rotor Rotor,.=
Time Exhaust Product Timer in Out in CJui G erator
'DRYER OUTPUT % SOLIDS
Dish f';gi :
rams
'fat :Sample.-., Disl-i
rains -
Dried. Sample + Dish
rams
0

TWSA DRYER OP:ERATEOkS
- -
=
DAIL Y"RECORD '
DATE .:
START::'.' -STOP
TOTAL
RUN TIME, HRS
,/.-
�] :n`7 [Q ..
✓ , a`�
_ -
1st Dryer Batch.
- -Fill Cycle Started @
Dry Cycle. Started @ �� Jr
Dischairge Cycle Started Q• C�
I.
Teri eratu s
Dis&.arc3. e
Discharge
L. y
Chamber.
Chamber.
4:uf�r
" R0t0r
Time .
Exhaust
Product
Timer
In
Out
In
Out
Operator
l:
pia
DRYER OUTPUT soups
Dish VNgt
Wet Sample +Dish
Dried.Samp!e
+Dish
-
_
p
rams :
rams).", ram
�`'/
0�3
_
'
x 100
,, b
% Totaf Solids
rted @� Discharge Cycle 8
tarted`@02
27
y
IDRYER.OUTPUT % souDs
Dish Wgt;::.:'Wet
Sample +Dish ...
Dried Sample ,+ Dish
rams
gams
rams
a.
x:1.00 -
%'Total Solids

1 em eratures .....
Discharge . Discharge. I . Dry chamber chamber Rotor Rotor..- .
Time Exhaust Product Timer In Out in uut iJ
FZYER,OUTPUT % SOLID
©ish Ut��t
:)J et Sample: `Dish .
rams
_Dried.Sample � Dishcams
rams

Time
Discharge
Exhaust
DISCharge .
Product
- . Did .
Timer
Chamber
Chamber.
Out
RotGr
In
Rotor
Out
Operator
/
^�IInnJ
9-"73

Time
Discharge
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor .
Out
Operator
y'
5 :
a09
0 :
V05
3q3
;7,1.z
Z 07'
50
VV5
C1J �/
1111`�
�2 /-/0
/00
,&�
9
v �?4'
30V
.200
vvq
v0
V
��,�

Time
Discharge.
Exhaust
Discharge
Product
Dry •. -
Timer
Chamber
In.
Chamber.
Out.
Roto
'-.in
P.otor_
:Out
Operator
�0'7
; 0
3 88
-34`26
-��
a ��.
a off'
, 50 : ,
.�� l
�f3� _:
.��1.
��►-:� -
'��0
b
g

Time
Discharge
Exhaust
Discharge.
Product
Dry
Timer
chamber
In
Chamber
Out
Rotor
In
Rotor -
Out
Operator
.20
aoq
n
i0
�109..
V//'
say
�23 :�
.20-7
Sd
6
C/y
3�.�
/
"V
.20.2
:2e9.,
%av
yy4(.,
yj 9 .
yy
t13s
-VVS
�5p
ago
DRYER OUTPUT %.SOLID . Dish Wgt. ; Wet Sample. ried Sample + Dish
. rams rams rams

.usi�z

TWSA.. DRYER OPERATIONS
DAILY RECORD
3rd Dryer Batchjq
Fill Cycle Started @ _7 Dry Cycle Started@ y Discharge Cycle Started,@
Tem eratures
Discharge Discharge - -Dry=_-T> Chamber- Chamber- Rotor-
Rotor
Time
Exhaust
Product--
-- --Timer=
=- In
Out
In
Out
Operator
o-5
9
vo�
393
�'6 '
0?4�11
.207'
50
VV5
y3
j119
3AI
jgv°9
�7,- j9
;20g.
15-c
VV4
V05
/��
,703 9
9
0 y
a o
vvy'
vo a-
V V15
C/o

_ Time
Discharge
Exhaust
Discharge
Product
-.'Dry
.Timer
Chamber
In
Chamber _
Out
Rotor
In
Rotor ' -
Out -
Operator
:
- -o
��
o'
a�
O
�..P-No
�b
DD
$
3
5�
,35g=.
: ;�5'
;2
3as,"I:=
77.E
Lt4f

TWSA DRYER OPERATIONS
-
DAILY RECORD
3rd Dryer Batch
Fill Cycle Started @ 3
DryCycle Started @/
Discharge Cycle Started @
_
Tem eratures
... -
Discharge
Discharge,
Dry
Chamber
Chamber
Rotor:
Rotor ---
"
Time
Exhaust
Product
Timer
In
Out
In
Out
Operator
�o
aa4
0
�a
voq
W
�-2�
sa y
.20
Sb
yy9
y�
y6
S,V
_20.2
--2671.o,
1 av
y3-V
yel.
3
S
73y�l
3D5
moo
.
y��
911/%
.

Time
Discharge
Exhaust
Discharge
Product
Dry ,
Timer,
Chamber
Ih
Chamber
Out
Rotor
.'In -
Rotcr
Out
Operator
I
(0
o:14-4
9
3 a
6
-a
a�.�f
ao7
03
14419
1446
39
.�4k
3
c
I D I,pl
� (eD
30;
-
:4 -1-
a
3

Time
Discharge
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor -
Out
Operator
_
a ..
7-7 Z
..t
Sl
2Z S
zo
G�
S
3�'
qqs
3 .
DRYER OUT PUT % SOLID
Dish.Wgt
rams
- Wet Sample. +-Dish Dried Sample + Dish
(grams)' rams
.
.Iq

-PRYER OUTPUT % so :ifls °'Dish Wgt
Wet Sample +Dish
Dried .$ample.+,Dish
O rams '
rams
rams
7e
x` 100
% Total Solids .:
.
2nd Dryer Batcf�
Fill Cycle Started @ Dry Cycle Started @ I -3a
:.
Discharge Cycle Started,.@ 332
Tern eiatures
�"m a
Discharge
::'Exhaust
Discharge::
. ;Product ':'
Dry
... Timer ..
Chamber
::. Jn.` .
Chamber.
`.:Out
Rotor
= In'Qut
Rotor
O erator
-
-14
;..-
3oSD
y3�/;
DRYER OUTPUT, io SOUb
,.
. Dish W.9t .
-. Wet Sample +.Dish ,
Dried Sample +.Dish
rams
rams '
-63
r
��%.
X100=
.
GG
/°Total Solids'...'

Time
Discharge
Exhaust
Discharge;
Product
Dry
Timer =
Chamber
- '...In
Chamber'
Out .
Rotor
� In -
Rotor: _>
Out , _
Operator
s10�2:boo
.27�05
DRYER OUTPUT % SOLID
V
Dish' Wgt
rams
Wet Sam le. j-..:Dish :Dried :Sam{�Ie y Dish
rams -, rams
o/v
,3G S

Time
Discharge
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor -
In
Rotor - .
Out
Operator
229
3�17
Z2 y
Sn
4/y7
cl�S
�3
�30 .
.7,o
1:37,9
��7
�7y
305
-19G
�O
y4e?,
yy,5
j9 -
.5O
DRYER ou T PUT % soup .:Diish W. t: Wet. Sample Dish Dried Sample + Dish
rams rams rams
fob ®�.. b , = _

_- ,°•
=T1NSA: DRYER OPERATIONS. -.
DAILY- RECORD
DATE
START: " - STOP .; .::` TOTAL
RUN-TIME, HRS
1st.Dryer Batch .
FIII Cycle Started.
. "
Dry -Cycle Started @` %/ Discharge Cycle Started @%
Temperatures '
Disbhai c
DIS01 large
u; y; ..
Cii2i716er
Cia ber
�:�tor - _
R- ��
w4v
..
Exhaust---
._ Product
Timer
In
Out
In= - --
Out'
Operator
_
0 3
��'7.
• - , ---
s
3
as
sa
g,58
a�4.
ao14P
lla
-DRYER OUTPUT °io SOLio
Dish Wgt
Wet Sample + Dish-Dried-8ample:+:Dish
rams `rams rams
_
oZt.e Sy'79 3g
e.
0�7 115� X.100
`
,
b ` Solids %Total
2nd Dryer Batch
FIII`Cycle Started @ ! �' 33 ,Dry Gycle Started @ 1J �P Discharge cycle Started @.0.
Temperatures.'.
Time
Discharge
. "Exhaust
Discharge;
: Product-'."-:.
Dry
Tinier
chamber
_ to ';
Cnamber.
Out ':.
Rotor
:. In : ,;
Rotor
Out
'Operator'
;.
i S
b LP:
t
3`
Eb
5�
a
-;446
Dr
��
a -a
off:. -•al.
-
:._ . a.
6 `6,b:
DRYER.OUTPUT %SOLID
Dish-, Wgt
Wet Sample +.Dish.. Dried Sample +Dish
rams
rams :: rams .
=•.
y i9o3
w.
..oi
9
x1o0=
p 1 t� -
�_
%•Total Solids
2J t2 - . .

Time
Discharge..
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
'Rotor .
Out
Operator
DRYER OUTPUT % SOLID"
Dish W t
_ iams
Wet Sample -i:� Dish
rams
-,Dried Sample + Dish'.
rams
x 100

' TWSA. DRYER.OPERATIONS-'::
r '
' DAILY RECORD
DATE
START ` : STOP ." - . TOTAL* :
RUN.TIME; HRS ..
fo.3 V :., ..,
�1 .�13..._
_-
1st.Dryer Batch
`.
Fill C cle Started .. t� 5 D �C cle Started , L
Y @ ry_ y @. `o� Discharge Cycle SLarted @ -
Tern eratures
D1S�fiargE
�ISCi iargc
.:C�.y
Ch6rnber.
ihanber
Ri7tvr
r:vt.''.r
_ Time
Exhaust*
.Product
-- Timer
In
Out
In
Out
O erator .
-DRYER OUTPUT 9i.'SouoS
:-.Dish .Wgt
_ Wet Sample + Dish Dried Sample.+ Dish.
- - -
::
rams
:. rams rams
3
'
r
Total Solids
2nd Dryer Batch _
FIII Cycle Started @ �.. Dry Cie Started @ Discharge Cycle Started
Tem eratures
Time
Discharge:
Exhaust
Discharge
Product"'.
Dry
,.`...Timer
Chamber
In:..
Cnarmber.
`:.Oat
Rotor. :
In.
':Rotor
:`Out
O'erator,
�
��►'�-
b�.�_
.moo ::�t3�
-��13
�3a�
338::E
:_ :-
-,. .:: •- .
r
43 ° :
.6a
DRYER OUTPU % SouD .;
Dish Wgt°
Wet Sample.+.Dish Dried SampEta)
le +Dish
rams
rams . . rams :.
x 1.00
''
u ..
%=Total
..
Solids.

y
T Time
Discharge
Exhaust
Discharge:
Product
Dry . -
Timer
-Chamber
In
Chamber.
Out
Rotor .
In..
'Rotor..
Out
O erator .
l v
. 3
ja
yl,ly
2��-
"y�.8'_
:317-
s�
/.
3
dos
/00
Z22 . .
3w =
5.�

Fill' Cycle Started @ L p Dry Cycle Started @ Discharge Cycle Started @ S yrio
Tem eratures
Time
Discharge:
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor. .
Out
Operator
3 s
Z? 7
:�o�
SO
spy/
y .�
y�0 .
3�3
ASP
y.25
-25'
2q6
160
11y5
1135.
VV5-
-3 _
.15
D
yy5.
Y ye
05"
3 y,7
S
3�05
g/j?
7
y y�
y�/�
.39
�5P
DRYER OUIMPUT % SOUD
. Dish Wgt
: Wet Sample
�- Dish
Dried Sample 1 Dish
-
rbms •
rams
rams
X 'oo q
Total. Solids
Alarms or Comments
_

TWSA . DRYER OPERATIONS
DAILY_ RECORD :.
3rd Dryer Batch �7
Fill; Cycle Started@ ��2 Dry Cycle Started @ w�1 Discharge Cycle Started @ -sib/
Temperatures
Time
Discharge.
Exhaust
Discharge
Product
Dry
Timer
Chamber
In
Chamber
Out
Rotor---
In -
. Rotor. .
Out
Operator
as
o
1
oa
c
�.��s�
aG
/9
�Oy
1450
: 41yS
y3�
VV5
.3Go
SJ� •
��� -
�/�3.
Aso.
yS�S
���
y�5 -
3�3
.� 92
s
ram/
/,,33
eI34(:,
OW
e7- 99
S S/7" .

Time
Discharge
Exhaust
Dlscliar.ge
Product •
ut;y.
Timer
iilaill6Er
In
Chamber
Out
Motor
In
;;iOr
Out
Operator
39
3)
a a&
tm
liq
a
6-a..�3.�.79:--
-
l3
3-q 1'-
. a•% .�
�� �::
36.E
1$�-
�`-�
. �� l
���
� � 9' g
�
-DRYER OUTPUT % SOLIDSp:Dish:Wgt
Wet Sample + Dish
Dried Sample +Dishrarris
rams
rams
Z 33
x r
' .
_
��- ... -
U o Total'solids
2nd Dryer Batch
a ea`
Fill C cle Started �. D C cle Started �' Dischar e.0 cle Started• Y . @ rY Y @
J.
.Tem eratares : .
Discharge
Discharge.--Dry;,;;*­,chamber
chamber.,
Rotor
_ Rotor
° .Time
Exhaust
Product •'
:` Timer
In
Out '.
In . :
Out
`O' erator
23`
:apes;
"
�:3
6 Fl.

T_ WSA -DRYER OPERATIONS -
..:'.. .
DAILY RECORD.
3rd Dryer Batch
Fill Cycle Started@
Dry Cycle. Started @ OqDischarge
Cycle Started.@
Temperatures
Discharge
Discharge
Dry
Chamber
Chamber
Rotor
Rotor..:
Time
Exhaust
Product
Timer
In
Out
In
out,
Operator
c�Za
E
`.o
x,3 4P
v.S
f?
, -0
43
4,5-0
1 3 z 3
'14 .
Z� 2
l ��
4_
437

I�ffm
IFMIM
'f 44S
42 l{,4
Temperatures
Time
Discharge
Exhaust
Disc hargc
Product,
-i]�y
Timer'.
Dha�rri7er
in
:,ia���aer .
Out `'
i : �tc^.r
-in
:�D+nr
Out..
Operator
gip-
Z1b:
11444 't,q8
.3,2.3
..:.. : ;
IIM�14
F Mow �v
- DRYER:OUTPUT %.SOL'IM
Ity
DRYER OUTPUT % Souos...Dish
1Ngt
Wet Sample +Dish
Dried Sample_+ Dish
'
rams
rams
rams .
f. .
. :.
X.
-
v %Total Solids
2/6/12

Time
Discharge
Exhaust.
Discharge
Product
Dry
Timer
Chamber
in
- chamber.
Out
Rotor
in
-Rotor,
Out
Operator
�Fs
. Viz- 7....
%to. C�
. ibo
�3 7 _-
.. ,`�
3 7 . •
� /�
DRYER' CCITPLIT %o..SOLID Dish Wgt Wet Sample + Dish, Dried Sample +Dish .
rams rams rams

DRYER OUTPUT %SOLIDS" Dish Wgt .. Wet Sample +Dish.
Dried Sample.+ Dish
_
rams : ,
:: rams),:. , ..
�i3 l
q.
x oo
Total "Solids
2nd Dryer Batch-,;, :. `,-
;Fill Cycle Started @: DryCycle Started Discharge Cycle tailed
Tein eratares
Discharge
Discharge;
Dry
; chamber
chamber
Rotor
"ln
Rotor
EJ< t
Product':
Timer..
Out
Out
"O' erator
4146,
NU
F
,.
��
� � :
;.y�s
s:
Sys-�
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. •
.:�
.
DRYER OUTPUT %SOLIDS Dish VUgt. Wet.Sample + Dish
'ramsgrams)rams
Dried Sample + Dish
i�i '�/ /
�/ ����
:
�� . a'�c Pf
. �
.. lX.100
6
. _ .
x 100
%Total So �ds
Solids

TWSA DRYER OPERATIONS
DAILY RECORD -
3rd Dryer Batch
FillCycle Started@ Dry Cycle. Started @ S.U Discharge Cycle Started @ 2 w '
Tem peratures
Time
Discharge
Exhaust
Discharge
Product
Dry ..
Timer
Chamber
In
Chamber
Out
Rotor
In
' Rotor
Out
Operator
5 o
: 21 3
a.a
pro
z
Z3
{
5 ,
33
ao
o
43G'4q
31
2 L
.ZO ��
/b d
Sr
`7
2 .
A 3
D
o
4 qS
'� 3
VS
3 ��
//�
5,�...3
o -1 -
1
14 qs�
DRYER OU TPU T %SOUC Di.sh Wgi Wet Sample = Dish Dried Sample.-s Dish
rams :: rams . rams

i em eratures
Discharge Disu-ha! uiy inaiiiC7BC Chamber RCtCr, RctOr
Time
Exhaust
Product
Timer
In
Out
"in
taut.
O erator-
C)a
3
43
aAA
; O
a
g - - -
'DRYER ouTPUT °i° soi iD
'Dish Wgt
rams
Wet Sample+ Dish
rams ,, : .
Dried .Sample +Dish
,:. :::> rams
Io
L� %` Total,Sohds
2nd Dryer Batch n
FIII C cle Started t
Y @
;.:
D C cle Started ` Dlscharge.Cycie Started:%.
ry y @ @
Tem` F.
eratures`
Time
Discharge
Exfiatast
Discharge
Product <
Dry
` :Tmer :.
.chamber
In'
Chamber:"
Out
Rotor
"-In
_Rotor
Out
O' erator
P131
�a
-
f
ao3
a�
DRYER:OUTPUT.I° SOLIDS:,
°.
Dish 1/Ugt
Wet Sample + Dish .
Dried Sample+`Dish ..
rams ..
rams
(grams):'.
(Q ( `x.100=
;- .IP •
%Total Solids:
7J61j2 . `c

_
Time '
Discharge
Exhaust
Discharge,
Product
_ Dry
Timer
cfiamber
In
:chamber
Out
,Rotor'==.
In .
_' Rotor..
Out
Operator
y/
yak
�s
doe,
5 0
cos
o .
9�09 :
DR ER ou �u °�o_soi�fl _ Dish Wyt
Dried Sample + rJst
; Mt SamFle Dish :
,.
rams .
... rams
rams
_..:.
7.
X,oa-
Total Solids-
Alarms or Comments
ass::`
�tl/� CYI�� '-icr©i c�c►:�-c. `` 'a�'
f
.

Time
DISCI �art3c
1=; haust
Disci iai yc
Product
Di q
ilmer
inai7fuer
In
Cilai7{3Ef
Out
Rotor
In
Ron+M.
Out
Operator
1?Y
3 (7g '
39f__
`(
aq,:
.
:.::
DRYER OUTPUT % SOLIDS.. Dish Wgt
Wet Sample + Dish .
Dried Sample+ Dish
rams)'
rams
rams
f -
1 '
x 100
%Total Solids
2nd Dryer Batch /nn
:Fill C cle Started ! V �'�'::
y @ Dry Cycle Started @. - Discharge Cycle Started @•• .off
_.
Tem eiatures' .
'i ime
Discharge
Exhaust
Discharge
Product '
Dry
`Timer ;:
chamber
In
Chamber.
Out =
Rotor: =
: In
Rotor
Out
`
O' erator
44
a56
: �
abo
`ba
f._
E
off: (o •
'-(o�
1'a':33"
s :-
.44
:
DRYER,OUTPUT % SOLIDS,, Dish Wgt
Wet Sample +.Dish
Dried Sample +. Dish
rams(grams)rams
% C 7
x 1'00
otal Solids
21611

TWSA DRYER. OPERATIONS
DAILY RECORD' - -
3rd' Dry er;Batch
.
FiII Cycle Started @ _ Dry Cycle Started r��Discharge Cycle Started.@. 7y
-Tamnarafir rrac . .
Time.
Discharge
Exhaust
Discharge
Product
Dry
Timer
Chamber .
In.
' Chamber .
Out
Rotor
In
Rotor . .
Out
Operator
�-?33
�6/s
:------aaacR.cu: uT %° souas Dish U�lgt Wet Sample Dish Dried Samgl� � Dish; -
: rams rams grams).

-DRYER OUTPUT % SOLIDS

term erasures
Discharge Discharge, Dry chamber chamber Rotor Rotor. .
Time Exhaust Product Timer In Out In Out Operator
DRYER.OUTPUT, % SOLID
Dish Wgt
tarns
Wet Sample + Dish ,
rams
- Dried Sample.+ Dish
, rams
x 16o =

Time .
iiSCiiai yc
Exhaust
�iSi ia!- ge
Product
D. y _.
Timer .
Chamber.
in
Chamber
Out
P:vt-r
in
RG+nr
Out
Operator
AO
Po.
E'h
D
as
a
o
3
431a
JJ 43
3-) �

Time
Discharge.
Exhaust
Discharge
Product
Dry
Timer
Chamber .
in
Chamber
Out
Rotor
In
Rotor..
Out
Operator
Rio
o`er
207 :...
0
3 ;F
V00
20-7
50 ..
I -IV
y13-5
%y7...
?q
yso
2�2 7
-,703
/00
yyy
y37-
yyy
-2
Sp
yS73
3S
ASP
iv
�3 05
9.� :
'WO
yy
DRYER, OUTPUT % SOLID
Dish Wgt
rams
Wt-Sample + Dish .. Dried Sample + Dish
rams yams ,

.,LTi'me
I]iSc}iaFyc
Exhaust
Dis--6large ury' -
: Product Timer
ChazrGer
In
CilaiTiaEf
Out
`:otc^.r Rotor
In Out
O erator

Time.
Discharge
Exhaust'
Discharge.
Product
Dry ..
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor. .
Out
Operator
DRYER. O.UTr UT % SOLID
Dish Wgt
-(drams
"Wet Sample = Dish
rams
Dried Sample 1_ Dish
rams

4
TWSA.,,RR YER. OPERATIONS
DAILYRECORD
DATE
START STOP '
TOTAL _.
RUN-TIME, HRS
.d : ...
S
;1st Dryer Batch
y �..
Fill Cycle Started -
Dry'Cycle Started @ ��
Discharge Cycle Started
Temperatures
DischameDiS
a
•D
01m,
lvLeni
aaIII vtvr
-
Time
E3chaust
Product '
.Timer
In
Out :
in
` Out
Operator
�f3�.'
.
r�
f
;-
✓^�
RX�
//��
!`fir'
DRYER ouTPUT !i. Souos
`: Dish VVgt
Wet Sample + Dish
Dried Sample +. Dish
r_-
:.(grams)'
rams rams
-
Ir6MC�
4
l: �6 %Total Solids
2nd Dryer Bkch
rill Cycle Started @ Dry Cycle Started' @. o
Discharge Cycle ;Started_ @ f
Tem erature's.:
Discharge
Discharge'
Dry
Chamber
Chamber
Rotor '.
Rotor
:
Tirrae
;Exhaust
Product.'
.`. Timer..
:: ,,. In
:Out. -=.
In
Out
O` erator
C1
DRYER OUTPUT ,% SOLIDS:,
,
Dish Wgt= ,Wet,Sam.ple.+ Dish. _ Dried SampEe:,Dish.
rams ..
rams ram
' �c.100 =
..

i
Time.
Discharge
Exhaust
Discharge
Product
Dry
Timer
chamber
In
chamber
Out
Rotor
In
Rotor.
Out
Operator
311
V 3.7
✓13
yN
,
�a
�o�
DR%R.CUTr^UT%:SOLIDS,Dish U1lg#. Wet SamPla?.- Dish Dried Sample_+ Dish L —
(grams): .. rams rams
'0.3 .

Time
Disci urge
Discharge
-Exhaust
h...-
Disci large
Product
-Il..
u� y.
Timer
chamber
In
chambei
Out
Q. L
.acr
In
.:a,�.
r4..::«..
Out
O erator
cTiq
_Z�
�g
cl�Cfj
(�

Time
Discharge
Exhaust
Discharge
Product
Dry.
Timer
Chamber
In
. Chamber
Out
Rotor
In
Rotor
Out
Operator
4135
20
� o
0.
9
9
�'o ..
/v o
yyy
y��
/c/S
3G;g53-159
70vy3v3
7 �
9 �
30�
/ 9
10 S7
cl39
DRYER -OUTPUT "lo SOLID . Dish Wgt Wet Sample - Dish. Dried Sample L Di®h
W.cams rams rams .
19..-
%oiia

Time
Discharge
Exhaust
Discharge
Product
Diy
Timer
Chamber
in
Chamber
Out
Rotor
in
ROLcr
Out
O erator
Tem. eratares
Tffne
Discharge
'Exhaust
Discharge
Product'::
Dry
..` Timer
.:Chamber
- in
:-.Chamber
Out' _;
Rotor'.'
°.In ::".
Rotor
Out
O' erator

i em eratures
Discharge Discharge Dry Chamber. Chamber Rotor Rotor
'Time Exhaust Product Timer In Out In Out Operator

. TWSA DRYER OPERATIQNS
-
DjAILY:RECORD
-
DATE /. ` 2 Q
START STOP
TOTAL:
- .
TIME; HRS
.7.TRUN
:`::.
Ist.Dryer Batch
FillCycle Started 'Z
@ �-
0(. Discharge C cle Started !� 3
Dry Cycle Started @ • , 9 Y @
Term eratures
Discharge
Dischar.gc•
�-11Y -
.Cii2mber
i..ilarnbei.
Qct.'-+r
'.,Time .
"Exhaust
Product-
Timer
In
Out
in
'Out
Operator
L/
2- y.2
717
!,
c�, f
� ��-
:Zvi. •
,�-5 � ::
y y:-
:L/3 �
-. y.�--.-.:
3 � � ..���
_
fi
_ _
`DRYER' OUTPUT % SOLIDS
Dish'Wgt
rarns
Wet Sample + Dish Dried Sample + Dish-
rams rams

Time
Discharge
Exhaust
Discharge...
Product
:Dry.
Timer
Chamber
In
Chamber
Out
Rotor
In
Rotor..
Out
Operator
qO '
VO5"
�?3/
��'�
V36
Vy7
�
`O.o
DRYER' OU.1PU% % SOLID
Dish VYgt
rams .
Wet_Sarnple.+ Dish
..rams
Dried Sample 1 Dish
(grams)., .

TWSA-DRYER.OPERATIONS
= `
_ • DAILY RECORD
•
I � � ��^
•
DATE - •
START STOP ' .. TOTAL
RUN-TIME, HRS
Fn 77 bw
: '`- tQ
1st Dryer Batch
'7
.-'FillCycle Started @ Dry Cycle Started @ Discharge .Cycle Started
ried @
Tem eratures.
t...,.
Disc hcrge.
t y,
DIS�r�a��, c
Di �
y
iilBiTibeP
'er
Vlaiiluc�
Rot
t..�
Ro+ yr
Time
Exhaust
Product
Timer
In
Out
In
Out
O erstor
Jed0.
_ •
04
DRYER OUTPUT %.SOLIDS "Dish Wgt Wet Sample + Dish . Dried •Sample:+'Dish _
d
rams : rams
q x . 00 r
Total Solids '
H
,t
2nd Dryer Ba#ch s ti �ti;ti w r }
Fill Cycle Started @ U Dry Cycle Started` @. Discharge. Cycle Started@
.,
:Tem eratures :
Discharge
Discharge.
Dry.'.:::.Chamber
chamber.
C
:Rotor _
:: Rotor
Time
_
Exhaust'
.:.'
`'Producf:
`' .Timer
Im
".Out
,
` In `
Out
:: 0` erator
WA
a�
o
a
y
:.:
-DRYER:OUTPUT % SOLID
.Dish Wgt . Wet Sample +.. Dish Dried Sample + Dish
:...... ... :. . ... . • . - ; . -
rams ' rams rams
x100- 5
% Total Solids
..2/6/12 `.. .-
� J... .

Time
Discharge
Exhaust
Discharge:
Product
Dry ..
Timer
Chamber'
In
chamber
Out
Rotor-
In
Rotor,., _
out,
Operator
51
P 7,
570:
5
s�3S"
Ow
��
3�
��