NC0088692_Renewal (Application)_20220926

Ms.STATE Q'' ,
ROY COOPER ` j.
Governor t' I
ELIZABETH S.BISER C
Secretary
RICHARD E.ROGERS,JR. NORTH CAROLINA
Director Environmental-Quality-
September 26, 2022
Sparks Oil Company
Attn: Jerry Sparks, President
412 N Scales St
Reidsville, NC 27320
Subject: Permit Renewal
Application No. NC0088692
J.W. Smith/ Camp Spring 76
Caswell County
Dear Applicant:
The Water Quality Permitting Section acknowledges the September 26, 2022, receipt of your permit renewal application
and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 150E-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
r4ciSincerelyjcio
ld/n
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
cc: Mika Trifunovic-PYRAMID
ec: WQPS Laserfiche File w/application
E Q N Carolina part Environmental Quality I i of aoue
Worthmston-Salem DeReglonalOfmentflceof 1450vironmentaWestHanesMillRoadDivis,Suitone300Wter I Wlnston-SResrcs
alem;North Carolina 27105
m� ti�\ 336.776.9800

PYRAMID
ENVIRONMENTAL&ENGINEERING,P.C.
September 20, 2022
Attention: Wren Thedford
NCDEQ/DWR/SWPS/Point Source Branch
NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: NPDES Permit Renewal Request for RECEIVED
JW Smith/Camp Springs 76 Groundwater Remediation System
8920 Cherry Grove Road SEP 216 2022
Reidsville, Caswell County, NC
NPDES Permit#NC0088692 NCDEQ/DWR/NPDES
NCDEQ Groundwater Incident#21685
Dear Mr.Thedford:
Mr.Joe R. Corporon of NCDEQ/DWR/NPDES Permitting informed me that this NPDES permit renewal request for
the above-referenced remediation system and associated documentation must be submitted to you by mail.
Initially, I sent the electronic renewal application to Mr. Kent Wiggins.
As requested by Sparks Oil Company, Pyramid Environmental & Engineering, PC has prepared the NPDES permit
renewal request package for the JW Smith/Camp Springs 76 petroleum-impacted groundwater remediation system
holding NPDES Permit # NC0088692. As instructed by Mr. Kent Wiggins, the renewal package includes EPA NPDES
Forms 1 & 2C as well as the remediation system outfall topographic map, three most recent remediation system
influent and effluent analytical reports, the remediation system diagram showing flow rates, and a copy of the
current NPDES permit.
If you have any questions or need any additional information regarding this permit renewal request, please let me
know.
Sincerely,
*1#-/A0We;
Mika Trifunovic
Project Manager
[e-mail]
office 336.335.3174
mobile [phone]
Enclosures:NPDES Permit Renewal Package
P.O.Box 16265•Greensboro,NC 27416
503 Industrial Ave•Greensboro,NC 27406
Phone[phone]•Fax[phone]•Toll Free(866)545-9507
Email:[e-mail]
www.pyramidenvironmental.com

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
Form U.S.Environmental Protection Agency
1 EPA Application for NPDES Permit to Discharge Wastewater
NPDES GENERAL INFORMATION
SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1))
1.1 Applicants Not Required to Submit Form 1
Is the facility a new or existing publicly owned Is the facility a new or existing treatment works
1.1.1 1
treatment works? 1. .2 treating domestic sewage?
If yes, STOP. Do NOT complete El No If yes,STOP. Do NOT 0 No
Form 1.Complete Form 2A. complete Form 1. Complete
Form 2S.
1.2 Applicants Required to Submit Form 1
1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing,
g. operation or a concentrated aquatic animal commercial, mining,or silvicultural facility that is
n production facility? currently discharging process wastewater?
o ❑ Yes-* Complete Form 1 ❑✓ No ✓0 Yes 4 Complete Form El No
a and Form 28. 1 and Form 2C.
0 1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing,
mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that
commenced to discharge? discharges only nonprocess wastewater?
❑ Yes 4 Complete Form 1 ✓❑ No ❑ Yes 4 Complete Form 1=1 No
ce and Form 2D. 1 and Form 2E.
1.2.5 Is the facility a new or existing facility whose
discharge is composed entirely of stormwater
associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
❑ Yes 4 Complete Form 1 ✓❑ No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x)or
b 15 .
SECTION 2.NAME,MAILING ADDRESS,AND LOCATION (40 CFR 122.21(f)(2))
2.1 Facility Name
J.W.Smith/Camp Springs 76(GW-REM)-PC-1
0 2.2 EPA Identification Number
U
0 NC0088692
2.3 Facility Contact
Name(first and last) Title Phone number
Jerry Sparks President of Sparks Oil Company [phone]
Email address
[e-mail]
2.4 Facility Mailing Address
Street or P.O. box
412 N.Scales Street
City or town State ZIP code
Reidsville NC 27320
EPA Form 3510-1(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
im
tic d 2.5 Facility Location
Street,route number,or other specific identifier
0 8920 Cherry Grove Road
rn
c c County name County code(if known)
3 Caswell
City or town State ZIP code
z Reidsville NC 27320
SECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3))
3.1 SIC Code(s) Description(optional)
NA This facility is a petroleum-impacted groundwater remediation system
m
0
0
co
3.2 NAICS Code(s) Description(optional)
NA This facility is a petroleum-impacted groundwater remediation system
SECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4))
4.1 Name of Operator
Pyramid Environmental&Engineering,P.C. Mika Trifunovic is the facility/project manager.
4.2 Is the name you listed in Item 4.1 also the owner?
o ❑ Yes ❑✓ No
4.3 Operator Status
`o
❑ Public—federal ❑ Public—state ❑ Other public(specify)
❑✓ Private ❑ Other(specify)
4.4 Phone Number of Operator
[phone]
4.5 Operator Address
Street or P.O. Box
y 503 Industrial Ave.
o
c w City or town I State ZIP code
o V Greensboro NC 27406
03
n Email address of operator
[e-mail]
SECTION 5. INDIAN LAND(40 CFR 122.21(f)(5))
c 5.1 Is the facility located on Indian Land?
c VS
❑Yes ❑✓ No
EPA Form 3510-1(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
SECTION 6.EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6))
6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each)
m NPDES(discharges to surface ❑ RCRA(hazardous wastes) ❑ UIC(underground injection of
water) fluids)
O
NC0088692
Li)
a ❑ PSD(air emissions) El Nonattainment program(CM) ❑ NESHAPs(CM)
❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) ❑ Other(specify)
SECTION 7. MAP(40 CFR 122.21(f)(7))
7.1 Have you attached a topographic map containing all required information to this application?(See instructions for
specific requirements.)
0 Yes ❑ No ❑ CAFO—Not Applicable(See requirements in Form 2B.)
SECTION 8. NATURE OF BUSINESS(40 CFR 122.21(f)(8))
8.1 Describe the nature of your business.
The facility is a petroleum-impacted groundwater remediation system.
in
U)
U)
ca
0
0
40
SECTION 9.COOLING WATER INTAKE STRUCTURES(40 CFR 122.21(f)(9))
9.1 Does your facility use cooling water?
❑ Yes ✓❑ No 4 SKIP to Item 10.1.
15
co9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at
2 40 CFR 125, Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your
NPDES permitting authority to determine what specific information needs to be submitted and when.)
0
tp
v c
SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10))
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that
apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and
d when.)
❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section
cc Section 301(n)) 302(b)(2))
a)
❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a))
Section 301(c)and(g))
❑✓ Not applicable
EPA Form 3510-1(revised 3-19) Page 3
1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 + OMB No.2040-0004
SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
11.1 In Column 1 below,mark the sections of Form 1 that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to provide attachments.
Column 1 Column 2
❑✓ Section 1:Activities Requiring an NPDES Permit ❑ w/attachments
❑✓ Section 2:Name, Mailing Address, and Location ❑ w/attachments
❑✓ Section 3:SIC Codes 0 w/attachments
❑✓ Section 4:Operator Information ❑ wl attachments
❑✓ Section 5: Indian Land ❑ w/attachments
❑� Section 6:Existing Environmental Permits 0 w/attachments
0Section 7: Map ❑ map pographic ❑ w/additional attachments
c 0Section 8: Nature of Business ❑ w/attachments
❑✓ Section 9: Cooling Water Intake Structures ❑ w/attachments
GP
GP
El Section 10:Variance Requests
❑ wl attachments
❑ Section 11:Checklist and Certification Statement ❑ w/attachments
Y 11.2 Certification Statement
U
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system,or those persons
directly responsible for gathering the information, the information submitted is,to the best of my knowledge and
belief, true,accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Jerry Sparks President of Sparks Oil Company
Signatur) Date signed
(7-711/1/
4/2 l'/ q. ?-
EPA Form 3510-1(revised 3-19) Page 4

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River Basin:Roanoke HITC:030101040202 SCALE NC Grid:B21 SW
County:Caswell 1:24,000 USGS Quad:Cherry Grove,NC
,

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
Form U.S.Environmental Protection Agency
2C \—/EPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
c Outfall Receiving Water Name Latitude Longitude
Number
0
001 Country Line Creek 36° 17' 46" N -79° 29' 31" W
Ta
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SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
a, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
balance?(See instructions for drawing requirements.See Exhibit 2C-1 at end of instructions for example.)
J �
❑✓ Yes ❑ No
SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1,provide average flow and treatment information.Add additional sheets if
necessary.
"Outfall Number"
Operations Contributing to Flow
Operation Average Flow
Petroleum-impacted groundwater remediation system 0.002 mgd
c -
mgd
is
mgd
-a
40 mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
air stripping of petroleum VOCs 1-K
multimedia filtration 1-Q
carbon adsorption 2-A
discharge to surface water 4-A
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
3.1 **Outfall Number"
cont. Operations Contributing to Flow
Operation Average Flow
mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size.flow rate through each treatment unit. Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
d
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U
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E
ra
N
H
- **Outfall Number**
N Operations Contributing to Flow
Operation Average Flow
rn mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
3.2 Are you applying for an NPDES permit to operate a privately owned treatment works?
❑ Yes ✓❑ No 4 SKIP to Section 4.
Nn 3.3 Have you attached a list that identifies each user of the treatment works?
❑ Yes ❑ No
EPA Form 3510-2C(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
SECTION 4.INTERMITTENT FLOWS(40 CFR 122.21(g)(4))
4.1 Except for storm runoff,leaks,or spills,are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑ Yes ❑✓ No 4 SKIP to Section 5.
4.2 Provide information on intermittent or seasonal flows for each applicable outfall.Attach additional pages,if necessary.
Outfall Operation Frecuency Flow Rate
Number (list) Average Average Long-Term Maximum Duration
Days/Week MonthslYear Average Daily
days/week months/year mgd mgd days
30 days/week months/year mgd mgd days
u_
c days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
SECTION 5.PRODUCTION(40 CFR 122.21(g)(5))
5.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under Section 304 of the CWA apply to your facility?
❑ Yes A No 4 SKIP to Section ..
5.2 Provide the following information on applicable ELGs.
w ELG Category ELG Subcategory Regulatory Citation
as
5.3 Are any of the applicable ELGs expressed in terms of production(or other measure of operation)?
❑ Yes ❑ No 4 SKIP to Section 6.
5.4 Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
Outfall Unit of
Number Operation,Product,or Material Quantity per Day Measure
CO
CO
CO
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0
a
EPA Form 3510-2C(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
SECTION 6.IMPROVEMENTS(40 CFR 122.21(g)(6))
6.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing,
upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes 12 No 4 SKIP to Item 6.3.
6.2 Briefly identify each applicable project in the table below.
Affected Final Compliance Dates
Brief Identification and Description of Outfalls Source(s)of -
o Project (list outfall Discharge Required Projected
number)
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6.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects
that may affect your discharges)that you now have underway or planned?(optional item)
❑ Yes ❑ No ✓❑ Not applicable
SECTION 7.EFFLUENT AND INTAKE CHARACTERISTICS(40 CFR 122.21(g)(7))
See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must
complete. Not all applicants need to complete each table.
Table A.Conventional and Non-Conventional Pollutants
7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑ Yes 0 No 4 SKIP to Item 7.3.
7.2 If yes,indicate the applicable outfalls below.Attach waiver request an. o er required information to the application.
Outfall Number Outfall Number Outfall Number
7.3 Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application ackage?
Permit NC0088692 only requires monifonng No;a waiver has been requested from my NPDES
i ❑ Yes of Flow and TSS from TableA pollutants ❑ permitting authority for all pollutants at all outfalls.
ES Table B.Toxic Metals,Cyanide,Total Phenols,and Organic Toxic Pollutants
. 7.4 Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
listed in Exhibit 2C-3?(See end of instructions for exhibit.)
❑ Yes ✓❑ No 4 SKIP to Item 7.8
7.5 Have you checked"Testing Required"for all toxic metals,cyanide,an.total pneno s in Section 1 of Table B?
❑ Yes ❑ No
7.6 List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s)identified
in Exhibit 2C-3.
Primary Industry Category Required GC/MS Fraction(s)
(Check applicable boxes.)
❑Volatile ❑Acid ❑Base/Neutral ❑Pesticide
❑Volatile ❑Acid 0 Base/Neutral ❑ Pesticide
❑Volatile ❑Acid ❑Base/Neutral 0 Pesticide
EPA Form 3510-2C(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
7.7 Have you checked"Testing Required"for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
O Yes 0 No
7.8 Have you checked`Believed Present"or"Believed Absent"for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
❑ Yes 0 No
7.9 Have you provided(1)quantitative data for those Section 1,Table B,pollutants for which you have indicated testing is
required or(2)quantitative data or other required information for those Section 1,Table B, pollutants that you have
indicated are"Believed Present"in your discharge?
Q Yes 0 No
7.10 Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes 4 Note that you qualify at the top of Table B, ❑✓ No
d then SKIP to Item 7.12.
7.11 Have you provided(1)quantitative data for those Sections 2 through 5,Table B,pollutants for which you have
c determined testing is required or(2)quantitative data or an explanation for those Sections 2 through 5,Table B,
pollutants you have indicated are"Believed Present"in your discharge?
p Yes ❑ No
a; Table C.Certain Conventional and Non-Conventional Pollutants
12 7.12 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C
s for all outfalls?
Y ❑ Yes ❑ No
c 7.13 Have you completed Table C by providing(1)quantitative data for those pollutants that are limited either directly or
indirectly in an ELG and/or(2)quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present"?
❑✓ Yes 0 No
w Table D.Certain Hazardous Substances and Asbestos
7.14 Have you indicated whether pollutants are`Believed Present"or"Believed Absent"for all pollutants listed in Table D for
all outfalls?
✓❑ Yes 0 No
7.15 Have you completed Table D by(1)describing the reasons the applicable pollutants are expected to be discharged
and(2)by providing quantitative data,if available?
❑✓ Yes ❑ No
Table E.2,3,7,8-Tetrachlorodibenzo-p-Dioxin(2,3,7,8-TCDD)
7.16 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions,or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. ❑✓ No-4 SKIP to Section 8.
7.17 Have you completed Table E by reporting qualitative data for TCDD?
❑ Yes ❑ No
SECTION 8.USED OR MANUFACTURED TOXICS(40 CFR 122.21(g)(9))
8.1 Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
r ❑ Yes 51 No 4 SKIP to Section 9.
8.2 List the pollutants below.
1. 4. 7.
2. 5. 8.
3. 6. 9.
EPA Form 3510-2C(Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on(1)any of your discharges or(2)on a receivin• water in relation to your discharge?
❑ Yes 0 No 4 SKIP to Section 10.
9.2 Identify the tests and their purposes below.
Test(s) Purpose of Test(s) Submitted to NPDES Date Submitted
o Permitting Authority?
❑ Yes ❑ No
15)
❑ Yes ❑ No
❑ Yes ❑ No
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
✓❑ Yes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm
Pace Analytical Services,LLC
N
Laboratory address 9800 Kincey Ave.Suite 100
Huntersville,NC 28078
[phone]
0 Phone number
[phone]
Pollutant(s)analyzed Total Suspended Solids
Phenolics,Total
Lead
VOCs
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
❑ Yes ✓❑ No 4 SKIP to Section 12.
0
E 11.2 List the information requested and attach it to this application.
1. 4.
0
2. 5.
V
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number I Facility Name Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
SECTION 12.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
12.1 In Column 1 below, mark the sections of Form 2C that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note
that not all applicants are required to complete all sections or provide attachments.
Column 1 Column 2
✓❑ Section 1:Outfall Location ❑Q w/attachments
❑✓ Section 2:Line Drawing 0 w/line drawing 0 w/additional attachments
Section 3:Average Flows and w/list of each user of
❑✓ Treatment 0 w/attachments 0 privately owned treatment
works
❑ Section 4: Intermittent Flows ❑ w/attachments
❑ Section 5: Production ❑ w/attachments
w/optional additional
❑ Section 6: Improvements 0 w/attachments 0 sheets describing any
additional pollution control
plans
❑ w/request for a waiver and ❑ wl explanation for identical
supporting information outfalls
0
wl small business exemption
request El w/other attachments
`° Section 7: Effluent and Intake
c ✓❑ Characteristics ❑✓ w/Table A ❑✓ w/Table B
0
✓❑ w/Table C ❑✓ w/Table D
cI) El w/Table E ❑ w/analytical results as an
attachment
R ❑ Section 8: Used or Manufactured
H Toxics 0
w/attachments
Section 9: Biological Toxicity
t ❑ Tests ❑ w/attachments
U
D Section 10:Contract Analyses 0 w/attachments
❑ Section 11:Additional Information ❑ wl attachments
✓❑ Section 12: Checklist and ❑ wl attachments
Certification Statement
12.2 Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is. to the best of my knowledge and belief,true,
accurate,and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Jerry Sparks President of Sparks Oil Company
Sig�ture Date signed
i�/Iiii_.,‘ 9r/9
EPA Form 3510-2C(Revised 3-19) Page 7

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EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 001 OMB No.2040-0004
TABLE A.CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1
Effluent Intake
Waiver (Optional)
Pollutant Requested Units Maximum Maximum Long-Term
(if applicable
ste (specify) Daily Monthly Average Daily Number of Long-Term Number of
Discharge Discharge Discharge Analyses Average Value Analyses
(required) (if available) Of available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for al/of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand Concentration
1 (BOD5) ❑ Mass
Chemical oxygen demand Concentration
2' El(COD) Mass
Concentration
3. Total organic carbon(TOC) ❑
Mass
Concentration mg/L 20.0 <2.6 Monthly
4. Total suspended solids(TSS) ❑
Mass
Concentration
5. Ammonia(as N) ❑
Mass
6. Flow ❑ Rate MGD 0.008 0.002 Continuous
Temperature(winter) ❑ °C °C
7.
Temperature(summer) ❑ °C °C
pH(minimum) ❑ Standard units s.u.
8.
pH(maximum) ❑ Standard units s.u.
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 9

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EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Di eqh aruidge) Df availabischarg e) De ischarge Analyses AValuee Analyses
r (if available)
❑ Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table. Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Antimony,total Concentration
1.1 (7440-36-0) Mass
Arsenic,total Concentration
1.2 (7440 38 2) 0 0 0Mass
Beryllium,total Concentration
1.3 (7440-41-7) El 0 Mass
Cadmium,total Concentration
1.4 (7440-43-9) Mass
Chromium,total Concentration
1.5 (7440-47-3) Mass
Copper,total Concentration
1.6 (7440-50-8) Mass
Lead,total ❑ Concentration Monitor <1 Quarterly
1.7 (7439-92-1) Mass
•
Mercury,total Concentration
1.8 (7439 97 6) ❑ ❑ -
Mass
Nickel,total ❑ Concentration
1'9 (7440-02-0) Mass
1.10 Selenium,total 0 0 Concentration
(7782-49-2) Mass
1.11 Silver,total 0 Concentration
i (7440-22-4) Mass
EPA Form 3510-2C(Revised 3-19) Page 11

EPA Identification Number T NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Maximum Maximum Long-Term Long-
(and CAS Number,if available) Required Believed Believed (specify) Number
Daily Monthly Average Number Term
Present Absent Daily of of
D(sc fired) Discharge)available ge Analyses AverageValue Analyses
required
(ifDischar available)
1.12 Thallium,total 0 Concentration
0 El
(7440-28-0) Mass
Zinc,total Concentration
1.13 (7440 66 6) 0
Mass
1.14 Cyanide,total 0 Concentration
0 0
(57-12-5) Mass
1.15 Phenols,total 0 Concentration ug/L 150 <20 Monthly
Mass
Section 2.Organic Toxic Pollutants(GC/MS Fraction—Volatile Compounds)
Acrolein Concentration
2.1 —
(107-02-8) Mass
Acrylonitrile 0 Concentration
2.2 El 0
(107-13-1) Mass
Benzene O Concentration ug/L 0.6 <0.5 Monthly
2.3 El El
(71-43-2) Mass
Bromoform 0 Concentration
2.4 (75-25-2) Mass
Carbon tetrachloride El El 12 Concentration
2.5 (56-23-5) Mass
Chlorobenzene El � Concentration
2.6 El
(108-90-7) Mass
Chlorodibromomethane El 01:1 Concentration
2.7 (124-48-1) Mass
Chloroethane 1=1 Concentration
2.8 El 0
(75-00-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) (if available) Value
2.9 2-chloroethylvinyl ether ❑ ❑ ❑ Concentration
(110-75-8) Mass
Concentration
2.10 Chloroform(67-66-3) 0 El
2.11 Dichlorobromomethane ❑ ❑ ❑✓ Concentration
(75-27-4) Mass
212 11-dichloroethane ❑ ❑ ❑✓ Concentration
(75-34-3) Mass
1,2-dichloroethane El ❑ ❑ Concentration ug/L 5 <0.5
2.13 (107-06-2) Mass Monthly
2.14 1,1-dichloroethylene ❑ ❑ ❑✓ Concentration
(75-35-4) Mass
1,2-dichloropropane ❑ ❑ ❑ Concentration
2.15 (78-87-5) Mass
2.16 1,3-dichloropropylene ❑ ❑ ❑✓ Concentration
(542-75-6) Mass
2.17 Ethylbenzene El 0 ❑✓ Concentration ug/L _ 48.5 <0.5
(100-41-4) Mass Monthly
Methyl bromide 0 ❑ ❑ Concentration
2.18 (74-83-9) Mass
2.19 Methyl chloride El 0 ✓❑ Concentration
(74-87-3) Mass
2.20 Methylene chloride ❑ ❑ ✓❑ Concentration
(75-09-2) Mass
221 1,1,2,2-tetrachloroethane ❑ 0
ElConcentration
(79-34-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
PollutantlParameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge q Dd) f ava labs) Discharge Analyses ischarg AValuee Analyses
(if available)
2.22 Tetrachloroethylene ❑ Concentration
El 0
(127-18-4) Mass
2.23 Toluene 0Concentration ug/L 5.5 <0.5 Monthly
13 El
(108-88-3) Mass
2 24 1,2-trans-dichloroethylene 0Concentration
El El
(156-60-5) Mass
2.25 1,1,1-trichloroethane ❑ Concentration
El 0(71-55-6) Mass
2.26 1,1,2-trichloroethane 1=1 0Concentration
(79-00-5) Mass
2.27 Trichloroethylene 0Concentration
(79-01-6) Mass
—
2.28 Vinyl chloride El
Vinyl
(75-01-4) Mass
Section 3.Organic Toxic Pollutants(GCIMS Fraction—Acid Compounds)
3.1 2-chlorophenol ❑ 0Concentration
(95-57-8) Mass
3.2 2,4-dichlorophenol 0Concentration
ID El
(120-83-2) Mass
2,4-dimethylphenol ❑ Concentration
3.3 El El
(105-67-9) Mass
3.4 4,6-dinitro-o-cresol El0Concentration
El
(534-52-1) Mass
2,4-dinitrophenol El Concentration
3.5 (51-28-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge rfavailablle) Discharge Analyses AverageValue Analyses
(required)
(if available)
2-nitrophenol ❑ Concentration
3.6 El El
(88-75-5) Mass
4-nitrophenol ❑ Concentration
3.7 El 0
(100-02-7) Mass
p-chloro-m-cresol El Concentration
3.8 El
(59-50-7) Mass
Pentachlorophenol ❑ ❑ Concentration
3.9 (87-86-5) Mass
3.10 Phenol 0Concentration
El El
(108-95-2) Mass
3.11 2 4,6-trichlorophenol Concentration
(88-05-2) Mass
Section 4.Organic Toxic Pollutants(GC/MS Fraction—Base/Neutral Compounds)
Acenaphthene 0 ❑ Concentration
4.1 (83-32-9) Mass
Acenaphthylene El Concentration
4.2 El
(208-96-8) Mass
4.3 Anthracene 0Concentration
El El
(120-12-7) Mass
Benzidine ❑ Concentration
4.4 (92-87-5) Mass _
Benzo(a)anthracene El El Concentration
4.5 (56-55-3) Mass
4.6 Benzo(a)pyrene ElConcentration
(50-32-8) Mass
EPA Form 3510-2C(Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant'Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long Number
Present Absent Daily Monthly Term
of of
Discharge Discharge DisDcharge Analyses Average Analyses
(required) (if available) Value
(if available)
4.7 3,4-benzofluoranthene ❑ 0Concentration •
(205-99-2) Mass
4.8 Benzo(ghi)perylene 0Concentration
(191-24-2) Mass
Benzo(k)fluoranthene ❑ ❑ Concentration
4.9 (207-08-9) Mass
Bis(2-chloroethoxy)methane ❑ ❑ Concentration
4.10 (111-91-1) Mass
Bis(2-chloroethyl)ether ❑ Concentration
4.11 (111-44-4) Mass
4.12 Bis(2-chloroisopropyl)ether ❑ 0Concentration
(102-80-1) Mass
4.13 Bis(2-ethylhexyl)phthalate 0Concentration
0 El
(117-81-7) Mass
4-bromophenyl phenyl ether ❑ Concentration
4.14 0 El
(101-55-3) Mass
Butyl benzyl phthalate ❑ Concentration
4.15 0 El
(85-68-7) Mass
2-chloronaphthalene 0 Concentration
4.16 El El
(91-58-7) Mass
4-chlorophenyl phenyl ether 0 Concentration
4.17 (7005-72-3) Mass
Chrysene 0 Concentration
4.18 (218-01-9) Mass
Dibenzo(a,h)anthracene ❑ Concentration
4.19 (53-70-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 16

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC •XIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
4.20 1,2-dichlorobenzene ❑ 0Concentration
(95-50-1) Mass
4.21 1,3-dichlorobenzene ❑ 0Concentration
(541-73-1) Mass
4.22 1,4-dichlorobenzene ❑ El Concentration
(106-46-7) Mass
4.23 3,3-dichlorobenzidine El ✓3 Concentration
(91-94-1) Mass
4.24 Diethyl phthalate ✓❑ Concentration
(84-66-2) Mass
4.25 Dimethyl phthalate 0 ❑ ✓❑ Concentration
(131-11-3) Mass
4.26 Di-n-butyl phthalate 0 0 ElConcentration
(84-74-2) Mass
4.27 2 4-dinitrotoluene ❑ ❑ © Concentration
(121-14-2) Mass
4.28 2,6-dinitrotoluene 0 Concentration
(606-20-2) Mass
4.29 Di-n-octyl phthalate 0 ✓❑ Concentration
(117-84-0) Mass
1,2-Diphenylhydrazine Concentration
4.30 (as azobenzene)(122-66-7) Mass
4.31 Fluoranthene � ❑ Concentration
0(206-44-0) Mass
4.32 Fluorene ✓❑ Concentration
0 El -
(86-73-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 17

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
D(reguired)arge D(f available)ischarge
Discharge Analyses AValuee Analyses
(if available)
Hexachlorobenzene ElConcentration
4.33 0 El
(118-74-1) Mass
4.34 Hexachlorobutadiene � a Concentration
(87-68-3) Mass
4.35 Hexachlorocyclopentadiene 0 El 0 Concentration
(77-47-4) Mass
4.36 Hexachloroethane El0 Concentration
(67-72-1) Mass
4.37 Indeno(1,2,3-cd)pyrene 0 Concentration
0 El
(193-39-5) Mass
4.38 Isophorone 0 Concentration
0 El
(78-59-1) Mass
4.39 Naphthalene 0 Concentration ug?I 6 <2 Monthly
(91-20-3) Mass
4.40 Nitrobenzene 0 Concentration
El 0
(98-95-3) Mass
4.41 N-nitrosodimethylamine 0 0 Concentration
El
(62-75-9) Mass
N-nitrosodi-n-propylamine � � Concentration
4.42 El
(621-64-7) Mass
4.43 N-nitrosodiphenylamine 0 Concentration
(86-30-6) Mass
Phenanthrene 0 Concentration
4.44 0 El
(85-01-8) Mass
4.45 Pyrene Concentration
(129-00-0) Mass
EPA Form 3510-2C(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
4.46 1,2,4-trichlorobenzene ❑ 0 ❑✓ Concentration
(120-82-1) Mass
Section 5.Organic Toxic Pollutants(GC/MS Fraction—Pesticides)
Aldrin Concentration
5.1 (309-00-2) ❑ 0 0 Mass
a-BHC Concentration
5.2 (319-84-6) 0 0 .
Mass
(3-BHC Concentration
5.3 (319-85-7) 0 ❑ U Mass
y-BHC Concentration
5.4 (58 89 9) El 0 0 Mass
6-BHC Concentration
5.5 (319-86-8) 0 El Mass
5.6 Chlordane 0
❑ 0 Concentration
(57-74-9) Mass
4,4'-DDT ❑ ❑ 0 Concentration
5.7
(50-29-3) Mass
5.8 4,4'-DDE 0 ❑ ❑ Concentration
(72-55-9) Mass
4,4'-DDD 0 ❑ ❑ Concentration
5.9 (72-54-8) Mass
Dieldrin Concentration
5.10 (60-57-1) 0 0 ❑
Mass
5.11 a-endosulfan ❑ ❑ 0 Concentration
(115-29-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No,2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Temp of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
R-endosulfan Concentration
5.12 El El El
(115-29-7) Mass
Endosulfan sulfate Concentration
5.13 (1031 07 8) El El ❑
Mass
5.14 Endrin Concentration
(72-20-8) Mass
Endrin aldehyde Concentration
5.15 (7421-93-4) Mass
Heptachlor Concentration
5.16 (76-44-8) Mass
Heptachlor epoxide Concentration
5.17 (1024-57-3) 0 ❑ 0 Mass
PCB-1242 Concentration
5.18 (53469-21-9) 0 0 0 Mass
PCB-1254 Concentration
5.19 (11097-69-1) 0 El El Mass
PCB-1221 Concentration
5.20 (11104-28-2) 0 0 ✓❑ Mass
PCB-1232 Concentration
5.21 (11141-16-5) 0 0 0 Mass
PCB-1248 Concentration
5.22 (12672-29-6) ❑ 0 ✓❑ Mass
PCB-1260 Concentration
5.23 (11096-82-5) 0 0 ✓0 Mass
PCB-1016 Concentration
5.24 (12674-11-2) 0 0 ✓❑ Mass
EPA Form 3510-2C(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 0.001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
Toxaphene Concentration
5.25 (8001-35-2) ❑ ❑ ✓❑ Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 21

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall.You need not complete the'Presence or Absence"column of Table C for
each pollutant.
✓❑ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall.You need not complete the`Presence or Absence"column of Table C for
each pollutant.
1 Bromide 0 0 Concentration
(24959-67-9) Mass
2 Chlorine,total ❑ 0 Concentration
residual Mass
3. Color 0 0 Concentration
Mass
Concentration
4. Fecal coliform 0 0 Mass
5 Fluoride ❑ ❑ Concentration
(16984-48-8) Mass
Concentration
6 Nitrate-nitrite ❑ 0 Mass
Nitrogen,total Concentration
7' organic(as N) El ElMass
Concentration
8. Oil and grease ❑ 0 Mass
Phosphorus(as Concentration
9. P),total(7723-14-0) ❑ 0 Mass _
10. Sulfate(as SO4) ❑ ❑ Concentration
-
(14808-79-8) Mass
Concentration
11. Sulfide(as S) 0 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 23

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent
(Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum DailyLon -Term
Monthly Average Daily Number of Average Number of
Present Absent Discharge
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
12. Sulfite(as S03) ❑ 0 Concentration
(14265-45-3) Mass
Concentration
13. Surfactants 0 0 Mass
14. Aluminum,total ❑ ❑ Concentration
(7429-90-5) Mass
15.
Barium,total
❑ ❑ Concentration
(7440-39-3) Mass
Boron,total El El Concentration
16. (7440-42-8) Mass
17. Cobalt,total ❑ ❑ Concentration
(7440-48-4) Mass
Iron,total El Concentration
18' (7439-89-6) Mass
Magnesium,total ❑ El Concentration
19. (74 9-95-4) Mass
Molybdenum, Concentration
20. total 0 0 Mass
(7439-98-7)
21 Manganese,total ❑ 0 Concentration
(7439-96-5) Mass
Tin,total 0 0 Concentration
22. (7440-31-5) Mass
23.
Titanium,total 0 0 Concentration
(7440-32-6) Mass
EPA Form 3510-2C(Revised 3-19) Page 24

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Dail Long Term
Present Absent Discharge y Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses • Analyses
(required) Value
(if available) (if available)
24. Radioactivity
Concentration
Alpha,total ❑ 0 Mass
Concentration
Beta,total 0 0 Mass
Concentration
Radium,total ❑ 0 Mass
Concentration
Radium 226,total ❑ 0 Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 25

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EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
1. Asbestos ❑ ✓❑
2. Acetaldehyde ❑ ✓❑
3. Ally'alcohol ❑ ✓❑
4. Ally!chloride 0 ✓❑
5. Amyl acetate 0 0
6. Aniline 0 0
7. Benzonitrile 0 0
8. Benzyl chloride ❑ 0
9. Butyl acetate 0 ✓❑
10. Butylamine 0 0
11. Captan 0 ✓❑
12. Carbaryl 0 0
13. Carbofuran 0 ✓❑
14. Carbon disulfide ❑ ❑✓
15. Chlorpyrifos 0 ✓❑
16. Coumaphos 0 ❑✓
17. Cresol 0 ✓❑
18. Crotonaldehyde 0 ✓❑
19. Cyclohexane ❑ ✓❑
EPA Form 3510-2C(Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
20. 2,4-D(2,4-dichlorophenoxyacetic acid) ❑ ❑✓
21. Diazinon ❑ ❑✓
22. Dicamba ❑ ❑✓
23. Dichlobenil ❑ ✓❑
24. Dichlone ❑ ✓❑
25. 2,2-dichloropropionic acid ❑ ❑✓
26. Dichlorvos ❑ ❑✓
27. Diethyl amine ❑ 0
28. Dimethyl amine ❑ ❑✓
29. Dintrobenzene ❑ ❑✓
30. Diquat ❑ 0
31. Disulfoton ❑ ❑�
32. Diuron ❑ ❑✓
33. Epichlorohydrin ❑ ❑✓
34. Ethion ❑ ❑✓
35. Ethylene diamine ❑ ❑✓
36. Ethylene dibromide ❑ ❑✓
37. Formaldehyde ❑ ❑✓
38. Furfural ❑ ❑✓
EPA Form 3510-2C(Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
39. Guthion 0 ❑✓
40. Isoprene 0 ❑✓
41. Isopropanolamine 0 ❑✓
42. Kelthane 0 ❑✓
43. Kepone 0 ✓❑
44. Malathion ❑ ❑
45. Mercaptodimethur 0 p
46. Methoxychlor 0 ✓❑
47. Methyl mercaptan 0 ✓❑
48. Methyl methacrylate 0 ✓❑
49. Methyl parathion 0 ✓❑
50. Mevinphos 0 ✓❑
51. Mexacarbate ❑ ❑
52. Monoethyl amine ❑ ❑
53. Monomethyl amine 0 ✓❑
54. Naled 0 ✓❑
55. Naphthenic acid 0 ✓❑
56. Nitrotoluene 0 ✓❑
57. Parathion 0 ✓❑
EPA Form 3510-2C(Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
58. Phenolsulfonate 0 0
59. Phosgene 0 0
60. Propargite 0 0
61. Propylene oxide 0 0
62. Pyrethrins 0 0
63. Quinoline 0 0
64. Resorcinol 0 0
65. Strontium 0 0
66. Strychnine 0 0
67. Styrene 0 0
68. 2,4,5-T(2,4,5-trichlorophenoxyacetic 0 0
acid)
69. TDE(tetrachlorodiphenyl ethane) 0 0
70. 2,4,5-TP[2-(2,4,5-trichlorophenoxy) 0 0
propanoic acid]
71. Trichlorofon 0 0
72. Triethanolamine 0 0
73. Triethylamine 0 0
74. Trimethylamine 0 0
75. Uranium 0 0
76. Vanadium 0 0
EPA Form 3510-2C(Revised 3-19) Page 30

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
77. Vinyl acetate ❑ ✓❑
78. Xylene ❑ ✓❑
79. Xylenol ❑ ❑✓
80. Zirconium ❑ ✓❑
Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 31

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EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0088692 NC0088692 J.W.Smith/Camp Springs 76 OMB No.2040-0004
TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii))
TCDD Presence or
Congeners Absence
Pollutant Used or (check one) Results of Screening Procedure
Manufactured Believed Believed
Present Absent
2,3,7,8-TCDD El El
EPA Form 3510-2C(Revised 3-19) Page 33

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Influent from SVE knock-out
Max.Flew:50 GPO(0.03 GPM)
Insignificant amount of water Expected Avg.no.:<0.003 GPM < CD
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
June 30, 2022
Mr. Mika Trifunovic
Pyramid Environmental
P.O. Box 16265
Greensboro, NC 27416
RE: Project: JW SMITH
Pace Project No.: 92610954
Dear Mr. Trifunovic:
Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
nicole.d'[e-mail]
[phone]
Project Manager
Enclosures
\ i` REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 20

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacslabs.com [phone]
CERTIFICATIONS
Project: JW SMITH
Pace Project No.: 92610954
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville, NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 20

Pace Analytical Services,LLC
aceAnalytical/1
9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacdabs.eam [phone]
SAMPLE ANALYTE COUNT
Project: JW SMITH
Pace Project No.: 92610954
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92610954001 INF EPA 6020B DBB1 4 PASI-A
SM 6200B SAS 63 PASI-C
SM 2540D-2015 ZMC 1 PASI-A
EPA420.4 Rev 1.0 1993 NDS 1 PASI-A
92610954002 EFF EPA 6020B CRW,DBB1 4 PASI-A
SM 6200B SAS 63 PASI-C
SM 2540D-2015 ZMC 1 PASI-A
EPA 420.4 Rev 1.0 1993 NDS 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 20

Pace Analytical Services,LLC
e 9800 Kincey Ave. Suite 100
aceAna/ ical Huntersville,NC 28078
www.pecelebs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92610954
Sample: INF Lab ID: 92610954001 Collected: 06/20/22 14:00 Received: 06/21/22 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method:EPA 6020E Preparation Method:EPA 3010A
Pace Analytical Services-Asheville
Hardness,Calcium(SM 2340B) 17800 ug/L 500 1 06/28/22 11:46 06/28/22 23:16
Hardness,Magnesium(SM 2340B) 16900 ug/L 41.2 1 06/28/22 11:46 06/28/22 23:16
Lead ND ug/L 1.0 1 06/28/22 11:46 06/28/22 23:16 7439-92-1
Hardness,Total(SM 2340B) 34700 ug/L 541 1 06/28/22 11:46 06/28/22 23:16
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene 80.9 ug/L 2.0 4 06/24/22 14:46 71-43-2
Bromobenzene ND ug/L 2.0 4 06/24/22 14:46 108-86-1 i
Bromochloromethane ND ug/L 2.0 4 06/24/22 14:46 74-97-5
Bromodichloromethane ND ug/L 2.0 4 06/24/22 14:46 75-27-4
Bromoform ND ug/L 2.0 4 06/24/22 14:46 75-25-2
Bromomethane ND ug/L 20.0 4 06/24/22 14:46 74-83-9
n-Butylbenzene ND ug/L 2.0 4 06/24/22 14:46 104-51-8
sec-Butylbenzene ND ug/L 2.0 4 06/24/22 14:46 135-98-8
tert-Butylbenzene ND ug/L 2.0 4 06/24/22 14:46 98-06-6
Carbon tetrachloride ND ug/L 2.0 4 06/24/22 14:46 56-23-5
Chlorobenzene ND ug/L 2.0 4 06/24/22 14:46 108-90-7
Chloroethane ND ug/L 4.0 4 06/24/22 14:46 75-00-3
Chloroform ND ug/L 2.0 4 06/24/22 14:46 67-66-3
Chloromethane ND ug/L 4.0 4 06/24/22 14:46 74-87-3
2-Chlorotoluene ND ug/L 2.0 4 06/24/22 14:46 95-49-8
4-Chlorotoluene ND ug/L 2.0 4 06/24/22 14:46 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 4.0 4 06/24/22 14:46 96-12-8
Dibromochloromethane ND ug/L 2.0 4 06/24/22 14:46 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 2.0 4 06/24/22 14:46 106-93-4
Dibromomethane ND ug/L 2.0 4 06/24/22 14:46 74-95-3
1,2-Dichlorobenzene ND ug/L 2.0 4 06/24/22 14:46 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 4 06/24/22 14:46 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 4 06/24/22 14:46 106-46-7
Dichlorodifluoromethane ND ug/L 2.0 4 06/24/22 14:46 75-71-8
1,1-Dichloroethane ND ug/L 2.0 4 06/24/22 14:46 75-34-3
1,2-Dichloroethane 3.7 ug/L 2.0 4 06/24/22 14:46 107-06-2
1,1-Dichloroethene ND ug/L 2.0 4 06/24/22 14:46 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 4 06/24/22 14:46 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 4 06/24/22 14:46 156-60-5
1,2-Dichloropropane ND ug/L 2.0 4 06/24/22 14:46 78-87-5
1,3-Dichloropropane ND ug/L 2.0 4 06/24/22 14:46 142-28-9
2,2-Dichloropropane ND ug/L 2.0 4 06/24/22 14:46 594-20-7
1,1-Dichloropropene ND ug/L 2.0 4 06/24/22 14:46 563-58-6
cis-1,3-Dichloropropene ND ug/L 2.0 4 06/24/22 14:46 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 4 06/24/22 14:46 10061-02-6
Diisopropyl ether 2.8 ug/L 2.0 4 06/24/22 14:46 108-20-3
Ethylbenzene 78.3 ug/L 2.0 4 06/24/22 14:46 100-41-4
Hexachloro-1,3-butadiene ND ug/L 8.0 4 06/24/22 14:46 87-68-3
Isopropylbenzene(Cumene) 6.1 ug/L 2.0 4 06/24/22 14:46 98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 20

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelibs.com [phone]
i
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92610954
Sample: INF Lab ID: 92610954001 Collected: 06/20/22 14:00 Received: 06/21/22 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Methylene Chloride ND ug/L 8.0 4 06/24/22 14:46 75-09-2
Methyl-tert-butyl ether 327 ug/L 2.0 4 06/24/22 14:46 1634-04-4
Naphthalene 67.2 ug/L 8.0 4 06/24/22 14:46 91-20-3
n-Propylbenzene 7.6 ug/L 2.0 4 06/24/22 14:46 103-65-1
Styrene ND ug/L 2.0 4 06/24/22 14:46 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 2.0 4 06/24/22 14:46 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 2.0 4 06/24/22 14:46 79-34-5
Tetrachloroethene ND ug/L 2.0 4 06/24/22 14:46 127-18-4
Toluene 546 ug/L 2.0 4 06/24/22 14:46 108-88-3
1,2,3-Trichlorobenzene ND ug/L 8.0 4 06/24/22 14:46 87-61-6
1,2,4-Trichlorobenzene ND ug/L 8.0 4 06/24/22 14:46 120-82-1
1,1,1-Trichloroethane ND ug/L 2.0 4 06/24/22 14:46 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 4 06/24/22 14:46 79-00-5
Trichloroethene ND ug/L 2.0 4 06/24/22 14:46 79-01-6
Trichlorofluoromethane ND ug/L 4.0 4 06/24/22 14:46 75-69-4
1,2,3-Trichloropropane ND ug/L 2.0 4 06/24/22 14:46 96-18-4
1,2,4-Trimethylbenzene 109 ug/L 2.0 4 06/24/22 14:46 95-63-6
1,3,5-Trimethylbenzene 93.4 ug/L 2.0 4 06/24/22 14:46 108-67-8
Vinyl chloride ND ug/L 4.0 4 06/24/22 14:46 75-01-4
m&p-Xylene 332 ug/L 4.0 4 06/24/22 14:46 179601-23-1
o-Xylene 459 ug/L 2.0 4 06/24/22 14:46 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 82 % 70-130 4 06/24/22 14:46 17060-07-0
4-Bromofluorobenzene(S) 96 % 70-130 4 06/24/22 14:46 460-00-4
Toluene-d8(S) 103 % 70-130 4 06/24/22 14:46 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 3.7 mg/L 3.3 1 06/22/22 14:56
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable 0.055 mg/L 0.020 1 06/30/22 13:50 06/30/22 16:31 64743-03-9 M1,R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 20

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite Huntersville,NC 2807878
www.pacalabs.eom [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92610954
Sample: EFF Lab ID: 92610954002 Collected: 06/20/22 14:30 Received: 06/21/22 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method:EPA 6020E Preparation Method:EPA 3010A
Pace Analytical Services-Asheville
Hardness,Calcium(SM 2340B) 57600 ug/L 5000 10 06/28/22 11:46 06/29/22 14:44
Hardness,Magnesium(SM 2340B) 63200 ug/L 412 10 06/28/22 11:46 06/29/22 14:44
Lead ND ug/L 1.0 1 06/28/22 11:46 06/28/22 23:20 7439-92-1
Hardness,Total(SM 2340B) 121000 ug/L 5410 10 06/28/22 11:46 06/29/22 14:44
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 06/24/22 13:52 71-43-2
Bromobenzene ND ug/L 0.50 1 06/24/22 13:52 108-86-1
Bromochloromethane ND ug/L 0.50 1 06/24/22 13:52 74-97-5
Bromodichloromethane ND ug/L 0.50 1 06/24/22 13:52 75-27-4
Bromoform ND ug/L 0.50 1 06/24/22 13:52 75-25-2
Bromomethane ND ug/L 5.0 1 06/24/22 13:52 74-83-9
n-Butylbenzene ND ug/L 0.50 1 06/24/22 13:52 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 06/24/22 13:52 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 06/24/22 13:52 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 06/24/22 13:52 56-23-5
Chlorobenzene ND ug/L 0.50 1 06/24/22 13:52 108-90-7
Chloroethane ND ug/L 1.0 1 06/24/22 13:52 75-00-3
Chloroform ND ug/L 0.50 1 06/24/22 13:52 67-66-3
Chloromethane ND ug/L 1.0 1 06/24/22 13:52 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 06/24/22 13:52 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 06/24/22 13:52 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 06/24/22 13:52 96-12-8
Dibromochloromethane ND ug/L 0.50 1 06/24/22 13:52 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 06/24/22 13:52 106-93-4
Dibromomethane ND ug/L 0.50 1 06/24/22 13:52 74-95-3
1,2-Dichlorobenzene ND ug/L 0.50 1 06/24/22 13:52 95-50-1
1,3-Dichlorobenzene ND ug/L 0.50 1 06/24/22 13:52 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 06/24/22 13:52 106-46-7
Dichlorodifluoromethane ND ug/L 0.50 1 06/24/22 13:52 75-71-8
1,1-Dichloroethane ND ug/L 0.50 1 06/24/22 13:52 75-34-3
1,2-Dichloroethane ND ug/L 0.50 1 06/24/22 13:52 107-06-2
1,1-Dichloroethene ND ug/L 0.50 1 06/24/22 13:52 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 06/24/22 13:52 156-59-2
trans-1,2-Dichloroethene ND ug/L 0.50 1 06/24/22 13:52 156-60-5
1,2-Dichloropropane ND ug/L 0.50 1 06/24/22 13:52 78-87-5
1,3-Dichloropropane ND ug/L 0.50 1 06/24/22 13:52 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 06/24/22 13:52 594-20-7
1,1-Dichloropropene ND ug/L 0.50 1 06/24/22 13:52 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 06/24/22 13:52 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 06/24/22 13:52 10061-02-6
Diisopropyl ether ND ug/L 0.50 1 06/24/22 13:52 108-20-3
Ethylbenzene ND ug/L 0.50 1 06/24/22 13:52 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 06/24/22 13:52 87-68-3
lsopropylbenzene(Cumene) ND ug/L 0.50 1 06/24/22 13:52 98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 20

Pace Analytical Services,LLC
e 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacalabs.com [phone]
I
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92610954
Sample: EFF Lab ID: 92610954002 Collected: 06/20/22 14:30 Received: 06/21/22 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Methylene Chloride ND ug/L 2.0 1 06/24/22 13:52 75-09-2
Methyl-tert-butyl ether 0.90 ug/L 0.50 1 06/24/22 13:52 1634-04-4
Naphthalene ND ug/L 2.0 1 06/24/22 13:52 91-20-3
n-Propylbenzene ND ug/L 0.50 1 06/24/22 13:52 103-65-1
Styrene ND ug/L 0.50 1 06/24/22 13:52 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 06/24/22 13:52 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 06/24/22 13:52 79-34-5
Tetrachloroethene ND ug/L 0.50 1 06/24/22 13:52 127-18-4
Toluene ND ug/L 0.50 1 06/24/22 13:52 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2.0 1 06/24/22 13:52 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2.0 1 06/24/22 13:52 120-82-1
1,1,1-Trichloroethane ND ug/L 0.50 1 06/24/22 13:52 71-55-6
1,1,2-Trichloroethane ND ug/L 0.50 1 06/24/22 13:52 79-00-5
Trichloroethene ND ug/L 0.50 1 06/24/22 13:52 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 06/24/22 13:52 75-69-4
1,2,3-Trichloropropane ND ug/L 0.50 1 06/24/22 13:52 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 06/24/22 13:52 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 06/24/22 13:52 108-67-8
Vinyl chloride ND ug/L 1.0 1 06/24/22 13:52 75-01-4
m&p-Xylene ND ug/L 1.0 1 06/24/22 13:52 179601-23-1
o-Xylene ND ug/L 0.50 1 06/24/22 13:52 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 84 % 70-130 1 06/24/22 13:52 17060-07-0
4-Bromofluorobenzene(S) 99 % 70-130 1 06/24/22 13:52 460-00-4
Toluene-d8(S) 102 % 70-130 1 06/24/22 13:52 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 06/22/22 14:56
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.020 1 06/30/22 13:50 06/30/22 16:33 64743-03-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 20

Pace Analytical Services,LLC
s 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacslabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
QC Batch: 707124 Analysis Method: EPA 6020E
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92610954001,92610954002
METHOD BLANK: 3688722 Matrix: Water
Associated Lab Samples: 92610954001,92610954002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hardness,Calcium(SM 2340B) ug/L ND 500 06/28/22 22:11
Hardness,Magnesium(SM 2340B) ug/L ND 41.2 06/28/22 22:11
Hardness,Total(SM 2340B) ug/L ND 541 06/28/22 22:11
Lead ug/L ND 1.0 06/28/22 22:11
LABORATORY CONTROL SAMPLE: 3688723
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Hardness,Calcium(SM 2340B) ug/L 6250 6210 99
Hardness,Magnesium(SM 2340B) ug/L 10300 10300 100
Hardness,Total(SM 2340B) ug/L 16500 16500 100 80-120
Lead ug/L 50 50.6 101 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3688724 3688725
MS MSD
92611576001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Hardness,Calcium(SM ug/L 1540 6250 6250 7710 7830 99 101 2
234013)
Hardness,Magnesium(SM ug/L 4680 10300 10300 15300 15600 103 106 2
2340B)
Hardness,Total(SM 2340B) ug/L 6220 16500 16500 23000 23500 102 104 75-125 2
Lead ug/L ND 50 50 51.8 53.4 103 106 75-125 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 20

Pace Analytical Services,LLC
or
aceAnalytical 9800 neyAve Suite 100
Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
QC Batch: 706793 Analysis Method: SM 62008
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92610954001,92610954002
METHOD BLANK: 3687194 Matrix: Water
Associated Lab Samples: 92610954001,92610954002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/24/22 13:17
1,1,1-Trichloroethane ug/L ND 0.50 06/24/22 13:17
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/24/22 13:17
1,1,2-Trichloroethane ug/L ND 0.50 06/24/22 13:17
1,1-Dichloroethane ug/L ND 0.50 06/24/22 13:17
1,1-Dichloroethene ug/L ND 0.50 06/24/22 13:17
1,1-Dichloropropene ug/L ND 0.50 06/24/22 13:17
1,2,3-Trichlorobenzene ug/L ND 2.0 06/24/22 13:17
1,2,3-Trichloropropane ug/L ND 0.50 06/24/22 13:17
1,2,4-Trichlorobenzene ug/L ND 2.0 06/24/22 13:17
1,2,4-Trimethylbenzene ug/L ND 0.50 06/24/22 13:17
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/24/22 13:17
1,2-Dibromoethane(EDB) ug/L ND 0.50 06/24/22 13:17
1,2-Dichlorobenzene ug/L ND 0.50 06/24/22 13:17
1,2-Dichloroethane ug/L ND 0.50 06/24/22 13:17
1,2-Dichloropropane ug/L ND 0.50 06/24/22 13:17
1,3,5-Trimethylbenzene ug/L ND 0.50 06/24/22 13:17
1,3-Dichlorobenzene ug/L ND 0.50 06/24/22 13:17
1,3-Dichloropropane ug/L ND 0.50 06/24/22 13:17
1,4-Dichlorobenzene ug/L ND 0.50 06/24/22 13:17
2,2-Dichloropropane ug/L ND 0.50 06/24/22 13:17
2-Chlorotoluene ug/L ND 0.50 06/24/22 13:17
4-Chlorotoluene ug/L ND 0.50 06/24/22 13:17
Benzene ug/L ND 0.50 06/24/22 13:17
Bromobenzene ug/L ND 0.50 06/24/22 13:17
Bromochloromethane ug/L ND 0.50 06/24/22 13:17
Bromodichloromethane ug/L ND 0.50 06/24/22 13:17
Bromoform ug/L ND 0.50 06/24/22 13:17
Bromomethane ug/L ND 5.0 06/24/22 13:17
Carbon tetrachloride ug/L ND 0.50 06/24/22 13:17
Chlorobenzene ug/L ND 0.50 06/24/22 13:17
Chloroethane ug/L ND 1.0 06/24/22 13:17
Chloroform ug/L ND 0.50 06/24/22 13:17
Chloromethane ug/L ND 1.0 06/24/22 13:17
cis-1,2-Dichloroethene ug/L ND 0.50 06/24/22 13:17
cis-1,3-Dichloropropene ug/L ND 0.50 06/24/22 13:17
Dibromochloromethane ug/L ND 0.50 06/24/22 13:17
Dibromomethane ug/L ND 0.50 06/24/22 13:17
Dichlorodifluoromethane ug/L ND 0.50 06/24/22 13:17
Diisopropyl ether ug/L ND 0.50 06/24/22 13:17
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 20

Pace Analytical Services,LLC
9800 Kinsey Ave. Suite
aceAnalyfical
Huntersville,NC 28078078
www.pacslabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
METHOD BLANK: 3687194 Matrix: Water
Associated Lab Samples: 92610954001,92610954002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylbenzene ug/L ND 0.50 06/24/22 13:17
Hexachloro-1,3-butadiene ug/L ND 2.0 06/24/22 13:17
lsopropylbenzene(Cumene) ug/L ND 0.50 06/24/22 13:17
m&p-Xylene ug/L ND 1.0 06/24/22 13:17
Methyl-tert-butyl ether ug/L ND 0.50 06/24/22 13:17
Methylene Chloride ug/L ND 2.0 06/24/22 13:17
n-Butylbenzene ug/L ND 0.50 06/24/22 13:17
n-Propylbenzene ug/L ND 0.50 06/24/22 13:17
Naphthalene ug/L ND 2.0 06/24/22 13:17
o-Xylene ug/L ND 0.50 06/24/22 13:17
sec-Butylbenzene ug/L ND 0.50 06/24/22 13:17
Styrene ug/L ND 0.50 06/24/22 13:17
tert-Butylbenzene ug/L ND 0.50 06/24/22 13:17
Tetrachloroethene ug/L ND 0.50 06/24/22 13:17
Toluene ug/L ND 0.50 06/24/22 13:17
trans-1,2-Dichloroethene ug/L ND 0.50 06/24/22 13:17
trans-1,3-Dichloropropene ug/L ND 0.50 06/24/22 13:17
Trichloroethene ug/L ND 0.50 06/24/22 13:17
Trichlorofluoromethane ug/L ND 1.0 06/24/22 13:17
Vinyl chloride ug/L ND 1.0 06/24/22 13:17
1,2-Dichloroethane-d4(S) % 82 70-130 06/24/22 13:17
4-Bromofluorobenzene(S) % 98 70-130 06/24/22 13:17
Toluene-d8(S) % 103 70-130 06/24/22 13:17
LABORATORY CONTROL SAMPLE: 3687195
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L 50 48.5 97 60-140
1,1,1-Trichloroethane ug/L 50 49.7 99 60-140
1,1,2,2-Tetrachloroethane ug/L 50 42.6 85 60-140
1,1,2-Trichloroethane ug/L 50 49.8 100 60-140
1,1-Dichloroethane ug/L 50 46.0 92 60-140
1,1-Dichloroethene ug/L 50 53.3 107 60-140
1,1-Dichloropropene ug/L 50 47.1 94 60-140
1,2,3-Trichlorobenzene ug/L 50 50.8 102 60-140
1,2,3-Trichloropropane ug/L 50 42.9 86 60-140
1,2,4-Trichlorobenzene ug/L 50 50.7 101 60-140
1,2,4-Trimethylbenzene ug/L 50 46.6 93 60-140
1,2-Dibromo-3-chloropropane ug/L 50 45.5 91 60-140
1,2-Dibromoethane(EDB) ug/L 50 48.4 97 60-140
1,2-Dichlorobenzene ug/L 50 47.0 94 60-140
1,2-Dichloroethane ug/L 50 45.5 91 60-140
1,2-Dichloropropane ug/L 50 54.6 109 60-140
1,3,5-Trimethylbenzene ug/L 50 48.3 97 60-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 20

Pace Analytical Services,LLC
(1 ?eAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
1
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
LABORATORY CONTROL SAMPLE: 3687195
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,3-Dichlorobenzene ug/L 50 47.4 95 60-140
1,3-Dichloropropane ug/L 50 46.6 93 60-140
1,4-Dichlorobenzene ug/L 50 46.9 94 60-140
2,2-Dichloropropane ug/L 50 46.4 93 60-140
2-Chlorotoluene ug/L 50 44.2 88 60-140
4-Chlorotoluene ug/L 50 44.1 88 60-140
Benzene ug/L 50 47.1 94 60-140
Bromobenzene ug/L 50 46.8 94 60-140
Bromochloromethane ug/L 50 45.7 91 60-140
Bromodichloromethane ug/L 50 43.7 87 60-140
Bromoform ug/L 50 47.3 95 60-140
Bromomethane ug/L 50 41.9 84 60-140
Carbon tetrachloride ug/L 50 56.6 113 60-140
Chlorobenzene ug/L 50 47.1 94 60-140
Chloroethane ug/L 50 48.8 98 60-140
Chloroform ug/L 50 41.1 82 60-140
Chloromethane ug/L 50 60.6 121 60-140
cis-1,2-Dichloroethene ug/L 50 48.7 97 60-140
cis-1,3-Dichloropropene ug/L 50 49.8 100 60-140
Dibromochloromethane ug/L 50 47.2 94 60-140
Dibromomethane ug/L 50 51.9 104 60-140
Dichiorodifluoromethane ug/L 50 67.3 135 60-140
Diisopropyl ether ug/L 50 55.0 110 60-140
Ethylbenzene ug/L 50 46.1 92 60-140
Hexachloro-1,3-butadiene ug/L 50 56.1 112 60-140
Isopropylbenzene(Cumene) ug/L 50 47.5 95 60-140
m&p-Xylene ug/L 100 92.4 92 60-140
Methyl-tert-butyl ether ug/L 50 45.9 92 60-140
Methylene Chloride ug/L 50 45.9 92 60-140
n-Butylbenzene ug/L 50 48.2 96 60-140
n-Propylbenzene ug/L 50 45.4 91 60-140
Naphthalene ug/L 50 49.1 98 60-140
o-Xylene ug/L 50 46.0 92 60-140
sec-Butylbenzene ug/L 50 48.5 97 60-140
Styrene ug/L 50 46.4 93 60-140
tert-Butylbenzene ug/L 50 40.1 80 60-140
Tetrachloroethene ug/L 50 53.2 106 60-140
Toluene ug/L 50 46.1 92 60-140
trans-1,2-Dichloroethene ug/L 50 52.4 105 60-140
trans-1,3-Dichloropropene ug/L 50 48.3 97 60-140
Trichloroethene ug/L 50 58.2 116 60-140
Trichlorofluoromethane ug/L 50 50.8 102 60-140
Vinyl chloride ug/L 50 63.1 126 60-140
1,2-Dichloroethane-d4(S) % 86 70-130
4-Bromofluorobenzene(S) % 96 70-130
Toluene-d8(S) % 97 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 20

Pace Analytical Services,LLC
aceAnalytical® 9800 neyAve. Suite 100
Huntersville,NC 28078
www.pacslabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3687196 3687197
MS MSD
92611150006 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane ug/L ND 1000 1000 1040 980 104 98 60-140 6
1,1,1-Trichloroethane ug/L ND 1000 1000 1140 1040 114 104 60-140 9
1,1,2,2-Tetrachloroethane ug/L ND 1000 1000 949 893 95 89 60-140 6
1,1,2-Trichloroethane ug/L ND 1000 1000 1120 1020 112 102 60-140 9
1,1-Dichloroethane ug/L ND 1000 1000 1080 982 108 98 60-140 9
1,1-Dichloroethene ug/L ND 1000 1000 1230 1120 123 112 60-140 9
1,1-Dichloropropene ug/L ND 1000 1000 1070 1000 107 100 60-140 7
1,2,3-Trichlorobenzene ug/L ND 1000 1000 925 1030 93 103 60-140 11
1,2,3-Trichloropropane ug/L ND 1000 1000 978 893 98 89 60-140 9
1,2,4-Trichlorobenzene ug/L ND 1000 1000 931 1020 93 102 60-140 9
1,2,4-Trimethylbenzene ug/L 1200 1000 1000 2210 2270 101 107 60-140 3
1,2-Dibromo-3-chloropropane ug/L ND 1000 1000 923 850 92 85 60-140 8
1,2-Dibromoethane(EDB) ug/L ND 1000 1000 1060 985 106 98 60-140 7
1,2-Dichlorobenzene ug/L ND 1000 1000 1000 986 100 99 60-140 2
1,2-Dichloroethane ug/L 82.1 1000 1000 1160 1040 108 96 60-140 11
1,2-Dichloropropane ug/L ND 1000 1000 1230 1130 123 113 60-140 9
1,3,5-Trimethylbenzene ug/L 397 1000 1000 1440 1450 104 105 60-140 1
1,3-Dichlorobenzene ug/L ND 1000 1000 1030 988 103 99 60-140 4
1,3-Dichloropropane ug/L ND 1000 1000 1030 926 103 93 60-140 11
1,4-Dichlorobenzene ug/L ND 1000 1000 1000 978 100 98 60-140 3
2,2-Dichloropropane ug/L ND 1000 1000 935 837 93 84 60-140 11
2-Chlorotoluene ug/L ND 1000 1000 1030 967 103 97 60-140 7
4-Chlorotoluene ug/L ND 1000 1000 966 940 97 94 60-140 3
Benzene ug/L 6690 1000 1000 7910 8140 122 145 60-140 3 M1
Bromobenzene ug/L ND 1000 1000 1050 991 105 99 60-140 6
Bromochloromethane ug/L ND 1000 1000 1030 939 103 94 60-140 10
Bromodichloromethane ug/L ND 1000 1000 950 865 95 86 60-140 9
Bromoform ug/L ND 1000 1000 895 828 90 83 60-140 8
Bromomethane ug/L ND 1000 1000 816 883 82 88 60-140 8
Carbon tetrachloride ug/L ND 1000 1000 1220 1130 122 113 60-140 8
Chlorobenzene ug/L ND 1000 1000 1070 1010 107 101 60-140 6
Chloroethane ug/L ND 1000 1000 1290 1170 129 117 60-140 10
Chloroform ug/L ND 1000 1000 861 794 86 79 60-140 8
Chloromethane ug/L ND 1000 1000 1400 1310 140 131 60-140 7
cis-1,2-Dichloroethene ug/L ND 1000 1000 1140 1040 114 104 60-140 9
cis-1,3-Dichloropropene ug/L ND 1000 1000 1060 959 106 96 60-140 10
Dibromochloromethane ug/L ND 1000 1000 953 876 95 88 60-140 8
Dibromomethane ug/L ND 1000 1000 1150 1050 115 105 60-140 10
Dichlorodifluoromethane ug/L ND 1000 1000 1510 1380 151 138 60-140 9 M1
Diisopropyl ether ug/L 117 1000 1000 1340 1240 122 112 60-140 8
Ethylbenzene ug/L 726 1000 1000 1730 1740 101 102 60-140 1
Hexachloro-1,3-butadiene ug/L ND 1000 1000 1010 1050 101 105 60-140 3
Isopropylbenzene(Cumene) ug/L 29.0 1000 1000 1090 1060 107 103 60-140 3
m&p-Xylene ug/L 3510 2000 2000 5490 5600 99 104 60-140 2
Methyl-tert-butyl ether ug/L 397 1000 1000 1450 1370 106 98 60-140 6
Methylene Chloride ug/L ND 1000 1000 1000 904 100 90 60-140 10
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 20

Pace Analytical Services,LLC
s 9800 Kincey Ave. Suite 100
aceAnal ical
Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3687196 3687197
MS MSD
92611150006 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
n-Butylbenzene ug/L ND 1000 1000 977 1030 98 103 60-140 5
n-Propylbenzene ug/L 69.3 1000 1000 1050 1040 98 97 60-140 2
Naphthalene ug/L 402 1000 1000 1360 1510 96 111 60-140 10
o-Xylene ug/L 1610 1000 1000 2640 2640 104 103 60-140 0
sec-Butylbenzene ug/L ND 1000 1000 1010 1020 101 102 60-140 2
Styrene ug/L ND 1000 1000 1040 997 104 100 60-140 5
tert-Butylbenzene ug/L ND 1000 1000 857 850 86 85 60-140 1
Tetrachloroethene ug/L ND 1000 1000 1180 1130 118 113 60-140 5
Toluene ug/L 6870 1000 1000 7810 8080 94 121 60-140 3
trans-1,2-Dichloroethene ug/L ND 1000 1000 1190 1090 119 109 60-140 9
trans-1,3-Dichloropropene ug/L ND 1000 1000 995 910 100 91 60-140 9
Trichloroethene ug/L ND 1000 1000 1350 1230 135 123 60-140 9
Trichlorofluoromethane ug/L ND 1000 1000 1230 1140 123 114 60-140 8
Vinyl chloride ug/L ND 1000 1000 1420 1300 142 130 60-140 9 M1
1,2-Dichloroethane-d4(S) % 87 86 70-130
4-Bromofluorobenzene(S) % 95 97 70-130
Toluene-d8(S) % 96 96 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 20

Pace Analytical Services,LLC
aceAnalytical® 9800 Ki ncey Ave. Suite100
Huntersville,NC 28078078
www.pacalabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
QC Batch: 706060 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92610954001,92610954002
METHOD BLANK: 3683770 Matrix: Water
Associated Lab Samples: 92610954001,92610954002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 06/22/22 14:51
LABORATORY CONTROL SAMPLE: 3683771
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 246 98 90-110
SAMPLE DUPLICATE: 3684640
92610747001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 210 212 1
SAMPLE DUPLICATE: 3684641
92610802001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 543 500 8
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 20

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacolabs.eom [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92610954
QC Batch: 708025 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92610954001,92610954002
METHOD BLANK: 3692593 Matrix: Water
Associated Lab Samples: 92610954001,92610954002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L ND 0.020 06/30/22 16:27
LABORATORY CONTROL SAMPLE: 3692594
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.051 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3692595 3692596
MS MSD
35724070002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L 0.0076 0.05 0.05 0.041 0.045 73 80 90-110 7 M1
U
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3692597 3692598
MS MSD
92610954001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L 0.055 0.05 0.05 0.084 0.098 56 85 90-110 16 M1,R1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
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Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.paealabs.com [phone]
QUALIFIERS
Project: JW SMITH
Pace Project No.: 92610954
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 20

aceAna/ytical®
www.pacslabs.com Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JW SMITH
Pace Project No.: 92610954
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92610954001 INF EPA 3010A 707124 EPA 6020E 707488
92610954002 EFF EPA 3010A 707124 EPA 6020E 707488
92610954001 INF SM 6200B 706793
92610954002 EFF SM 6200B 706793
92610954001 INF SM 2540D-2015 706060
92610954002 EFF SM 2540D-2015 706060
92610954001 INF EPA 420.4 Rev 1.0 1993 708025 EPA 420.4 Rev 1.0 1993 708078
92610954002 EFF EPA 420.4 Rev 1.0 1993 708025 EPA 420.4 Rev 1.0 1993 708078
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/30/2022 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 20

Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville❑ Eden❑ Greenwood 0 Huntersvilie 0 Raleigh Mechanicsville❑ Atlantan] Kernersville❑
Sample Condition al Name:
Upon Receipt WOE ���
Courier: run'Atek [-)0tJortmayitteo' 610954
�❑,�f ❑ups ❑uses ❑Client
❑Commercial Once ❑Other: 1111/I illI'll+1111111
92610,�54
Custody Seal Present? Oyes �No Seals intact? Oyes No
Date/Initials Person Examining Conten : __ Ii ++ 1
Packing Material: ❑Bubble Wrap ]Bubble Bags ❑None CO l Z.1 '2 Z
Other Biological Tissue Frozen?
Thermometer: c nJ,1 Oyes ❑No Dili t
0 IR Gun ID: ll Z.TC)t k'�.
Type of Ice: n/et DOlue (]None
Correction Factor: •
Cooler Temp: l Add/Subtract('C)
Temp should be above freezing to 6'C
Cooler Temp Corrected('C: 2_ , \ °Samples out of temp criteria.Samples on ice,cooling process
USDA Regulated Soil( N/A,water sample) has begun
Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally,
(check maps)?Dyes ❑No inducing Hawaii and Puerto Rico)?Des ONo
Chain of Custody Present? ,-,EI� Comments/Discrepancy:
es QNo ON/A 1.
Samples Arrived within Hold Time? es ONo —
ON/A z
I .
Short Hold Time Analysis(<72 hr.)?
Dyes ON/A 3.
Rush Turn Around Time Requested? Oyes Bit o ON/A 4.
Sufficient Volume? Yes ❑No ON/A 5.
Correct Containers Used? Qr s ONo ON/A 6.
-Pace Containers Used? [�/Ss ONo ON/A
Containers Intact? Yes ONo ON/A 7.
Dissolved analysis:Samples Field Filtered? QYes ONo �/A _8
Sample.Labels Match COC? ISes ONo ON/A 9.
-Includes Date/Time/ID/Analysis Matrix: l"L i
Headspace in VOA Vials(>5-6mm)? Des 6lo ON/A 10.
Trip Blank Present? Oyes ONo ON/A 11.
Trip Blank Custody Seals Present? Oyes ElNo ON/A
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? [Yes ONo
Lot ID of splitcontalners:
Person contartpd
Project Manager SCURF Review:
Date:
Pro14aklanager_SREReview: --.______- -_--------_-,-
-
Date: --
Qualtrax ID:69614
Page 1 of 2 Page 18 of 20
1

Effective Date: 05/12/202205/12/2022
•'Check mark top half of box if pH and/or dechlorination is verified and Project N WO# 92610954
within the acceptance range for preservation samples. PM: NMI Due Date: 07/06/22
ExceptlonsiVOA,Coliform,TOC._Oil_and_Grease,DRO/8015(water).DOC,atig CLIENT: 92-Pyramid
"Bottom half of box is to!1st number of bottles
L'**Check all unpreserved Nitrates for chlorine -�
m v
v 0 a'
F. . u O v y ¢ n ¢ z
a v a ? V N 0 N C 2 a 74 v -- Z m N M ? W
L 4 y V V A 7 _ y Z.
2 a aai 2 . a m n i i' rr w z t Z• v Y ¢ ¢ e a' z a�i
v d 111 e a M v °: z a z z u 4 m z z O2 U N i_
o. n a O O ¢ 0 A d a n g p ` 0 u ? qz i " " N �' > m
O 7 C = = N Z C U O N I Z z VNI V O 8 t ,O A 2 C c
9 Y. 9 Y. v X 2 y 2 ,. N U ry cm ,/� ii. d 2 O .. c
N re A to N �' N ti n A �EE 2 2 ] 2 N y ti v u N 7EE
a a 0. m a a a, 0-rl c a E Q E Q d O 0 0 O 0 `p . a E o E
E E E v` E E E E € v d E a E E - --+ ; - N � 1 J 6. J H
a o _ N 0 N - = = Vol o c E E E ppE E 3 E E E sE E E
!t N .'r N N $ O V y N tOn YOI `7. O O
> > N > 2 N m 6 5 5 �r .i N ce 6 N 6
Y a. a. a. i a o a. a. t9 t~9 O 15 O1 m o~i CI m a0r 0 F h C 3 3
m in m m m m m m 3 a a a a a 4 8 > > o $ > w Ni rn it, a " a
1 \ _ \ .---
XL/ \ . &,1
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4
lik
\ --
6 \
I\' 't
7 \ \ _
ISk _____
g ` ` _
9 \
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10 \ \
11
- )--------\\.\\ _____
12
pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot A
adjusted added
aCt i"Wiw vuver t , d d, pancy a ec mg art., aroma compliance iampies,a copy of this form will be sent to the North C7mlins DEMR Cr_rrincatiu0 Ofliie(i.e.
Out of nose,incorrect preservative,out of temp,incorrect containers.
Qualtrax ID:69614 Page 2 of 2
Page 19 of 20

0
,7. ace Analytical' CHAIN-OF-CUSTODY/Analytical Request Document
.rr rrcnn:.co. The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed apcuratel .
Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info.pacelabs com/hubfs/pas�standard-terms.pdf N
Section A O
Section B Section C tT
Required Client Information: I m
Required Project Information: d
.,ompany: Pyramid EnvironmentalInvoice Information:
Report To Trifunovrq Mika Page: 1
4ddress. 503 Industrial Avenue Copy To Attention
9 �f 1
3reensboro,NC 27416 Company Name.
=mar. Purchase Order#: Address ( Regulatory Agency
Pace Quote A ryA en
'horn. [phone] 'Fax Project Name i Trust Fund Rates
JW Smith#202.-378 NPDES Pace Protect Manager. an.brumfield
fequnsled Due Date: .',,wyjA � Project# ery (a)pacelabs coat. State/Location
Pace Profile#. 3498-2
NC
Requested Analysis Altered(YIN)
MATRIX CODE OU COLLECTED Z
Dr eking Water OW 2O Preservatives
Ware; w g u —
Weat.Water Ww __ a w
Product P C
m
SAMPLE ID Seri/Sole SL t, o �, Z
Oil Ot i? START END m ro Y
One Character per box. we, wP .. ¢ w I- werr
(A-Z,0-9 r,-) A.r AR o a a z D o a u a •
c
Sample Ids must be unique a�°;,, �T w o 7,-
m ° r_ic zt0 °
F- - ii m O = a rl A
a rn O O ry t Q g o o -a
cc
S t DATE TIME DATE TIME w w n i = = z z 2 p ry ti o m
m o m .
2 frf irb' /410 7 ✓ter✓ i , r���
3 •
`
4
5
6
7
8
•
10
1'
12
ADDITIONAL COMMENTS RI-LW NISt1ED t3YIAFFILIATION DATE TIMET
ACCEPTED BY I AFFILIATION
DATE TIME SAMPLE CONDRIONS
Z f L t_
SAMPLER NAME AND SIGNATURE j
PRINT Name of SAMPLER: tl P
SIGNATURE of SAMPLER:(4�1/��yyy�``,,���,� "1 /�/ I DATE Si ned� �%r 2 m _ ,m
v 9 Li m Z °Z F�
- m> U�OY fn=`>

Pace Analytical Services,LLC
ace A nal tical® 9800 Kincey Ave. Suite 78
l�liHll ,IJ/`T U Huntersville,NC 28078
/ www.pacelabs.com [phone]
I
July 21, 2022
Mr. Mika Trifunovic
Pyramid Environmental
P.O. Box 16265
1 Greensboro, NC 27416
RE: Project: JW SMITH
Pace Project No.: 92614625
Dear Mr. Trifunovic:
Enclosed are the analytical results for sample(s) received by the laboratory on July 13, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
nicole.d'[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
0 This report shall not be reproduced,except in full,
11 without the written consent of Pace Analytical Services,LLC. Page 1 of 19
`,V •/

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacslibs.cam [phone]
CERTIFICATIONS
Project: JW SMITH
Pace Project No.: 92614625
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 19

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.paeol�bs.eom [phone]
SAMPLE ANALYTE COUNT
Project: JW SMITH
Pace Project No.: 92614625
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92614625001 INF. SM 6200B SAS 63 PASI-C
SM 2540D-2015 MAB2 1 PASI-A
EPA 420.4 Rev 1.0 1993 NDS 1 PASI-A
92614625002 EFF. SM 6200B SAS 63 PASI-C
SM 2540D-2015 MAB2 1 PASI-A
EPA420.4 Rev 1.0 1993 NDS 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 19

Pace Analytical Services,LLC
a 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.cam [phone]
1
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92614625
Sample: INF. Lab ID: 92614625001 Collected: 07/12/22 14:30 Received: 07/13/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene 70.6 ug/L 2.0 4 07/14/22 15:25 71-43-2
Bromobenzene ND ug/L 2.0 4 07/14/22 15:25 108-86-1
Bromochloromethane ND ug/L 2.0 4 07/14/22 15:25 74-97-5
Bromodichloromethane ND ug/L 2.0 4 07/14/22 15:25 75-27-4
Bromoform ND ug/L 2.0 4 07/14/22 15:25 75-25-2
Bromomethane ND ug/L 20.0 4 07/14/22 15:25 74-83-9
n-Butylbenzene ND ug/L 2.0 4 07/14/22 15:25 104-51-8
sec-Butylbenzene ND ug/L 2.0 4 07/14/22 15:25 135-98-8
tert-Butylbenzene ND ug/L 2.0 4 07/14/22 15:25 98-06-6
Carbon tetrachloride ND ug/L 2.0 4 07/14/22 15:25 56-23-5
Chlorobenzene ND ug/L 2.0 4 07/14/22 15:25 108-90-7
Chloroethane ND ug/L 4.0 4 07/14/22 15:25 75-00-3
Chloroform ND ug/L 2.0 4 07/14/22 15:25 67-66-3
Chloromethane ND ug/L 4.0 4 07/14/22 15:25 74-87-3
2-Chlorotoluene ND ug/L 2.0 4 07/14/22 15:25 95-49-8
4-Chlorotoluene ND ug/L 2.0 4 07/14/22 15:25 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 4.0 4 07/14/22 15:25 96-12-8
Dibromochloromethane ND ug/L 2.0 4 07/14/22 15:25 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 2.0 4 07/14/22 15:25 106-93-4
Dibromomethane ND ug/L 2.0 4 07/14/22 15:25 74-95-3
1,2-Dichlorobenzene ND ug/L 2.0 4 07/14/22 15:25 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 4 07/14/22 15:25 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 4 07/14/22 15:25 106-46-7
Dichlorodifluoromethane ND ug/L 2.0 4 07/14/22 15:25 75-71-8
1,1-Dichloroethane ND ug/L 2.0 4 07/14/22 15:25 75-34-3
1,2-Dichloroethane 4.0 ug/L 2.0 4 07/14/22 15:25 107-06-2
1,1-Dichloroethene ND ug/L 2.0 4 07/14/22 15:25 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 4 07/14/22 15:25 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 4 07/14/22 15:25 156-60-5
1,2-Dichloropropane ND ug/L 2.0 4 07/14/22 15:25 78-87-5
1,3-Dichloropropane ND ug/L 2.0 4 07/14/22 15:25 142-28-9
2,2-Dichloropropane ND ug/L 2.0 4 07/14/22 15:25 594-20-7
1,1-Dichloropropene ND ug/L 2.0 4 07/14/22 15:25 563-58-6
cis-1,3-Dichloropropene ND ug/L 2.0 4 07/14/22 15:25 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 4 07/14/22 15:25 10061-02-6
Diisopropyl ether 2.8 ug/L 2.0 4 07/14/22 15:25 108-20-3
Ethylbenzene 61.4 ug/L 2.0 4 07/14/22 15:25 100-41-4
Hexachloro-1,3-butadiene ND ug/L 8.0 4 07/14/22 15:25 87-68-3
lsopropylbenzene(Cumene) 4.9 ug/L 2.0 4 07/14/22 15:25 98-82-8
Methylene Chloride ND ug/L 8.0 4 07/14/22 15:25 75-09-2
Methyl-tert-butyl ether 428 ug/L 2.0 4 07/14/22 15:25 1634-04-4
Naphthalene 78.2 ug/L 8.0 4 07/14/22 15:25 91-20-3
n-Propylbenzene 6.0 ug/L 2.0 4 07/14/22 15:25 103-65-1
Styrene ND ug/L 2.0 4 07/14/22 15:25 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 2.0 4 07/14/22 15:25 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 2.0 4 07/14/22 15:25 79-34-5
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 19

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacalabs.cam [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92614625
Sample: INF. Lab ID: 92614625001 Collected: 07/12/22 14:30 Received: 07/13/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 2.0 4 07/14/22 15:25 127-18-4
Toluene 408 ug/L 2.0 4 07/14/22 15:25 108-88-3
1,2,3-Trichlorobenzene ND ug/L 8.0 4 07/14/22 15:25 87-61-6
1,2,4-Trichlorobenzene ND ug/L 8.0 4 07/14/22 15:25 120-82-1
1,1,1-Trichloroethane ND ug/L 2.0 4 07/14/22 15:25 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 4 07/14/22 15:25 79-00-5
Trichloroethene ND ug/L 2.0 4 07/14/22 15:25 79-01-6
Trichlorofluoromethane ND ug/L 4.0 4 07/14/22 15:25 75-69-4
1,2,3-Trichloropropane ND ug/L 2.0 4 07/14/22 15:25 96-18-4
1,2,4-Trimethylbenzene 93.3 ug/L 2.0 4 07/14/22 15:25 95-63-6
1,3,5-Trimethylbenzene 106 ug/L 2.0 4 07/14/22 15:25 108-67-8
Vinyl chloride ND ug/L 4.0 4 07/14/22 15:25 75-01-4
m&p-Xylene 278 ug/L 4.0 4 07/14/22 15:25 179601-23-1
o-Xylene 490 ug/L 2.0 4 07/14/22 15:25 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 96 % 70-130 4 07/14/22 15:25 17060-07-0
4-Bromofluorobenzene(S) 101 % 70-130 4 07/14/22 15:25 460-00-4
Toluene-d8(S) 98 % 70-130 4 07/14/22 15:25 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 5.8 mg/L 2.8 1 07/15/22 11:27
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable 0.055 mg/L 0.020 1 07/20/22 12:00 07/20/22 18:57 64743-03-9
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 19

Pace Analytical Services,LLC
e 9800 Kince Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacslabs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92614625
Sample: EFF. Lab ID: 92614625002 Collected: 07/12/22 15:00 Received: 07/13/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 07/14/22 13:54 71-43-2
Bromobenzene ND ug/L 0.50 1 07/14/22 13:54 108-86-1
Bromochloromethane ND ug/L 0.50 1 07/14/22 13:54 74-97-5
Bromodichloromethane ND ug/L 0.50 1 07/14/22 13:54 75-27-4
Bromoform ND ug/L 0.50 1 07/14/22 13:54 75-25-2
Bromomethane ND ug/L 5.0 1 07/14/22 13:54 74-83-9
n-Butylbenzene ND ug/L 0.50 1 07/14/22 13:54 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 07/14/22 13:54 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 07/14/22 13:54 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 07/14/22 13:54 56-23-5
Chlorobenzene ND ug/L 0.50 1 07/14/22 13:54 108-90-7
Chloroethane ND ug/L 1.0 1 07/14/22 13:54 75-00-3
Chloroform ND ug/L 0.50 1 07/14/22 13:54 67-66-3
Chloromethane ND ug/L 1.0 1 07/14/22 13:54 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 07/14/22 13:54 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 07/14/22 13:54 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 07/14/22 13:54 96-12-8
Dibromochloromethane ND ug/L 0.50 1 07/14/22 13:54 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 07/14/22 13:54 106-93-4
Dibromomethane ND ug/L 0.50 1 07/14/22 13:54 74-95-3
1,2-Dichlorobenzene ND ug/L 0.50 1 07/14/22 13:54 95-50-1
1,3-Dichlorobenzene ND ug/L 0.50 1 07/14/22 13:54 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 07/14/22 13:54 106-46-7
Dichlorodifluoromethane ND ug/L 0.50 1 07/14/22 13:54 75-71-8
1,1-Dichloroethane ND ug/L 0.50 1 07/14/22 13:54 75-34-3
1,2-Dichloroethane ND ug/L 0.50 1 07/14/22 13:54 107-06-2
1,1-Dichloroethene ND ug/L 0.50 1 07/14/22 13:54 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 07/14/22 13:54 156-59-2
trans-1,2-Dichloroethene ND ug/L 0.50 1 07/14/22 13:54 156-60-5
1,2-Dichloropropane ND ug/L 0.50 1 07/14/22 13:54 78-87-5
1,3-Dichloropropane ND ug/L 0.50 1 07/14/22 13:54 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 07/14/22 13:54 594-20-7
1,1-Dichloropropene ND ug/L 0.50 1 07/14/22 13:54 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 07/14/22 13:54 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 07/14/22 13:54 10061-02-6
Diisopropyl ether ND ug/L 0.50 1 07/14/22 13:54 108-20-3
Ethylbenzene ND ug/L 0.50 1 07/14/22 13:54 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 07/14/22 13:54 87-68-3
Isopropylbenzene(Cumene) ND ug/L 0.50 1 07/14/22 13:54 98-82-8
Methylene Chloride ND ug/L 2.0 1 07/14/22 13:54 75-09-2
Methyl-tert-butyl ether 1.4 ug/L 0.50 1 07/14/22 13:54 1634-04-4
Naphthalene ND ug/L 2.0 1 07/14/22 13:54 91-20-3
n-Propylbenzene ND ug/L 0.50 1 07/14/22 13:54 103-65-1
Styrene ND ug/L 0.50 1 07/14/22 13:54 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 07/14/22 13:54 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 07/14/22 13:54 79-34-5
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 19

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pecelebs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92614625
Sample: EFF. Lab ID: 92614625002 Collected: 07/12/22 15:00 Received: 07/13/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
P P Y
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 0.50 1 07/14/22 13:54 127-18-4
Toluene ND ug/L 0.50 1 07/14/22 13:54 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2.0 1 07/14/22 13:54 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2.0 1 07/14/22 13:54 120-82-1
1,1,1-Trichloroethane ND ug/L 0.50 1 07/14/22 13:54 71-55-6
1,1,2-Trichloroethane ND ug/L 0.50 1 07/14/22 13:54 79-00-5
Trichloroethene ND ug/L 0.50 1 07/14/22 13:54 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 07/14/22 13:54 75-69-4
1,2,3-Trichloropropane ND ug/L 0.50 1 07/14/22 13:54 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 07/14/22 13:54 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 07/14/22 13:54 108-67-8
Vinyl chloride ND ug/L 1.0 1 07/14/22 13:54 75-01-4
m&p-Xylene ND ug/L 1.0 1 07/14/22 13:54 179601-23-1
o-Xylene ND ug/L 0.50 1 07/14/22 13:54 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 100 % 70-130 1 07/14/22 13:54 17060-07-0
4-Bromofluorobenzene(S) 97 % 70-130 1 07/14/22 13:54 460-00-4
Toluene-d8(S) 99 % 70-130 1 07/14/22 13:54 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.7 1 07/15/22 11:27
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.020 1 07/20/22 12:00 07/20/22 18:58 64743-03-9
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 19

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacdabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
QC Batch: 710512 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92614625001,92614625002
METHOD BLANK: 3704788 Matrix: Water
Associated Lab Samples: 92614625001,92614625002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/14/22 11:09
1,1,1-Trichloroethane ug/L ND 0.50 07/14/22 11:09
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/14/22 11:09
1,1,2-Trichloroethane ug/L ND 0.50 07/14/22 11:09
1,1-Dichloroethane ug/L ND 0.50 07/14/22 11:09
1,1-Dichloroethene ug/L ND 0.50 07/14/22 11:09
1,1-Dichloropropene ug/L ND 0.50 07/14/22 11:09
1,2,3-Trichlorobenzene ug/L ND 2.0 07/14/22 11:09
1,2,3-Trichloropropane ug/L ND 0.50 07/14/22 11:09
1,2,4-Trichlorobenzene ug/L ND 2.0 07/14/22 11:09
1,2,4-Trimethylbenzene ug/L ND 0.50 07/14/22 11:09
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/14/22 11:09
1,2-Dibromoethane(EDB) ug/L ND 0.50 07/14/22 11:09
1,2-Dichlorobenzene ug/L ND 0.50 07/14/22 11:09
1,2-Dichloroethane ug/L ND 0.50 07/14/22 11:09
1,2-Dichloropropane ug/L ND 0.50 07/14/22 11:09
1,3,5-Trimethylbenzene ug/L ND 0.50 07/14/22 11:09
1,3-Dichlorobenzene ug/L ND 0.50 07/14/22 11:09
1,3-Dichloropropane ug/L ND 0.50 07/14/22 11:09
1,4-Dichlorobenzene ug/L ND 0.50 07/14/22 11:09
2,2-Dichloropropane ug/L ND 0.50 07/14/22 11:09
2-Chlorotoluene ug/L ND 0.50 07/14/22 11:09
4-Chlorotoluene ug/L ND 0.50 07/14/22 11:09
Benzene ug/L ND 0.50 07/14/22 11:09
Bromobenzene ug/L ND 0.50 07/14/22 11:09
Bromochloromethane ug/L ND 0.50 07/14/22 11:09
Bromodichloromethane ug/L ND 0.50 07/14/22 11:09
Bromoform ug/L ND 0.50 07/14/22 11:09
Bromomethane ug/L ND 5.0 07/14/22 11:09
Carbon tetrachloride ug/L ND 0.50 07/14/22 11:09
Chlorobenzene ug/L ND 0.50 07/14/22 11:09
Chloroethane ug/L ND 1.0 07/14/22 11:09
Chloroform ug/L ND 0.50 07/14/22 11:09
Chloromethane ug/L ND 1.0 07/14/22 11:09
cis-1,2-Dichloroethene ug/L ND 0.50 07/14/22 11:09
cis-1,3-Dichloropropene ug/L ND 0.50 07/14/22 11:09
Dibromochloromethane ug/L ND 0.50 07/14/22 11:09
Dibromomethane ug/L ND 0.50 07/14/22 11:09
Dichlorodifluoromethane ug/L ND 0.50 07/14/22 11:09
Diisopropyl ether ug/L ND 0.50 07/14/22 11:09
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 19

Pace Analytical Services,LLC
at 9800 Kincey Ave. Suite 100
aceAnalytical
Huntersville,NC 28078
www.pacalabs.com [phone]
I
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
METHOD BLANK: 3704788 Matrix: Water
Associated Lab Samples: 92614625001,92614625002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylbenzene ug/L ND 0.50 07/14/22 11:09
Hexachloro-1,3-butadiene ug/L ND 2.0 07/14/22 11:09
Isopropylbenzene(Cumene) ug/L ND 0.50 07/14/22 11:09
m&p-Xylene ug/L ND 1.0 07/14/22 11:09
Methyl-tert-butyl ether ug/L ND 0.50 07/14/22 11:09
Methylene Chloride ug/L ND 2.0 07/14/22 11:09
n-Butylbenzene ug/L ND 0.50 07/14/22 11:09
n-Propylbenzene ug/L ND 0.50 07/14/22 11:09
Naphthalene ug/L ND 2.0 07/14/22 11:09
o-Xylene ug/L ND 0.50 07/14/22 11:09
sec-Butylbenzene ug/L ND 0.50 07/14/22 11:09
Styrene ug/L ND 0.50 07/14/22 11:09
tert-Butylbenzene ug/L ND 0.50 07/14/22 11:09
Tetrachloroethene ug/L ND 0.50 07/14/22 11:09
Toluene ug/L ND 0.50 07/14/22 11:09
trans-1,2-Dichloroethene ug/L ND 0.50 07/14/22 11:09
trans-1,3-Dichloropropene ug/L ND 0.50 07/14/22 11:09
Trichloroethene ug/L ND 0.50 07/14/22 11:09
Trichlorofluoromethane ug/L ND 1.0 07/14/22 11:09
Vinyl chloride ug/L ND 1.0 07/14/22 11:09
1,2-Dichloroethane-d4(S) % 95 70-130 07/14/22 11:09
4-Bromofluorobenzene(S) % 96 70-130 07/14/22 11:09
Toluene-d8(S) % 96 70-130 07/14/22 11:09
LABORATORY CONTROL SAMPLE: 3704789
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L 50 57.7 115 60-140
1,1,1-Trichloroethane ug/L 50 46.9 94 60-140
1,1,2,2-Tetrachloroethane ug/L 50 51.6 103 60-140
1,1,2-Trichloroethane ug/L 50 49.2 98 60-140
1,1-Dichloroethane ug/L 50 40.9 82 60-140
1,1-Dichloroethene ug/L 50 44.3 89 60-140
1,1-Dichloropropene ug/L 50 46.5 93 60-140
1,2,3-Trichlorobenzene ug/L 50 54.2 108 60-140
1,2,3-Trichloropropane ug/L 50 49.8 100 60-140
1,2,4-Trichlorobenzene ug/L 50 59.0 118 60-140
1,2,4-Trimethylbenzene ug/L 50 52.5 105 60-140
1,2-Dibromo-3-chloropropane ug/L 50 60.0 120 60-140
1,2-Dibromoethane(EDB) ug/L 50 55.9 112 60-140
1,2-Dichlorobenzene ug/L 50 55.1 110 60-140
1,2-Dichloroethane ug/L 50 40.1 80 60-140
1,2-Dichloropropane ug/L 50 46.4 93 60-140
1,3,5-Trimethylbenzene ug/L 50 54.1 108 60-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 19

Pace Analytical Services,LLC
e 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacolabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
LABORATORY CONTROL SAMPLE: 3704789
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,3-Dichlorobenzene ug/L 50 55.9 112 60-140
1,3-Dichloropropane ug/L 50 49.8 100 60-140
1,4-Dichlorobenzene ug/L 50 51.7 103 60-140
2,2-Dichloropropane ug/L 50 46.7 93 60-140
2-Chlorotoluene ug/L 50 51.8 104 60-140
4-Chlorotoluene ug/L 50 51.6 103 60-140
Benzene ug/L 50 45.3 91 60-140
Bromobenzene ug/L 50 53.3 107 60-140
Bromochloromethane ug/L 50 45.9 92 60-140
Bromodichloromethane ug/L 50 50.7 101 60-140
Bromoform ug/L 50 51.6 103 60-140
Bromomethane ug/L 50 54.3 109 60-140
Carbon tetrachloride ug/L 50 55.4 111 60-140
Chlorobenzene ug/L 50 51.6 103 60-140
Chloroethane ug/L 50 39.3 79 60-140
Chloroform ug/L 50 43.8 88 60-140
Chloromethane ug/L 50 40.9 82 60-140
cis-1,2-Dichloroethene ug/L 50 42.8 86 60-140
cis-1,3-Dichloropropene ug/L 50 50.4 101 60-140
Dibromochloromethane ug/L 50 57.7 115 60-140
Dibromomethane ug/L 50 54.9 110 60-140
Dichlorodifluoromethane ug/L 50 41.0 82 60-140
Diisopropyl ether ug/L 50 40.1 80 60-140
Ethylbenzene ug/L 50 50.3 101 60-140
Hexachloro-1,3-butadiene ug/L 50 64.0 128 60-140
Isopropylbenzene(Cumene) ug/L 50 52.0 104 60-140
m&p-Xylene ug/L 100 102 102 60-140
Methyl-tert-butyl ether ug/L 50 39.4 79 60-140
Methylene Chloride ug/L 50 40.4 81 60-140
n-Butylbenzene ug/L 50 55.3 111 60-140
n-Propylbenzene ug/L 50 51.5 103 60-140
Naphthalene ug/L 50 56.4 113 60-140
o-Xylene ug/L 50 52.8 106 60-140
sec-Butylbenzene ug/L 50 53.5 107 60-140
Styrene ug/L 50 54.3 109 60-140
tert-Butylbenzene ug/L 50 45.6 91 60-140
Tetrachloroethene ug/L 50 56.6 113 60-140
Toluene ug/L 50 47.4 95 60-140
trans-1,2-Dichloroethene ug/L 50 43.1 86 60-140
trans-1,3-Dichloropropene ug/L 50 50.1 100 60-140
Trichloroethene ug/L 50 52.7 105 60-140
Trichlorofluoromethane ug/L 50 46.0 92 60-140
Vinyl chloride ug/L 50 45.5 91 60-140
1,2-Dichloroethane-d4(S) % 77 70-130
4-Bromofluorobenzene(S) % 97 70-130
Toluene-d8(S) % 97 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 19
I

Pace Analytical Services,LLC
9800 Kincey Ave. Suite100
aceAnalytical®
Huntersville,NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3704790 3704791
MS MSD
92614625002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane ug/L ND 20 20 24.1 23.8 121 119 60-140 1
1,1,1-Trichioroethane ug/L ND 20 20 21.6 22.2 108 111 60-140 3
1,1,2,2-Tetrachloroethane ug/L ND 20 20 20.9 20.2 105 101 60-140 3
1,1,2-Trichioroethane ug/L ND 20 20 20.7 20.3 103 102 60-140 2
1,1-Dichloroethane ug/L ND 20 20 18.7 18.8 94 94 60-140 0
1,1-Dichloroethene ug/L ND 20 20 19.9 20.0 100 100 60-140 1
1,1-Dichloropropene ug/L ND 20 20 21.1 21.5 106 108 60-140 2
1,2,3-Trichlorobenzene ug/L ND 20 20 21.6 22.3 108 112 60-140 3
1,2,3-Trichloropropane ug/L ND 20 20 19.2 18.7 96 93 60-140 3
1,2,4-Trichlorobenzene ug/L ND 20 20 22.8 22.8 114 114 60-140 0
1,2,4-Trimethylbenzene ug/L ND 20 20 20.8 21.3 104 107 60-140 2
1,2-Dibromo-3-chloropropane ug/L ND 20 20 22.3 21.9 111 109 60-140 2
1,2-Dibromoethane(EDB) ug/L ND 20 20 22.9 22.8 115 114 60-140 1
1,2-Dichlorobenzene ug/L ND 20 20 21.5 22.1 108 110 60-140 2
1,2-Dichloroethane ug/L ND 20 20 17.9 18.1 89 90 60-140 1
1,2-Dichloropropane ug/L ND 20 20 19.6 20.4 98 102 60-140 4
1,3,5-Trimethylbenzene ug/L ND 20 20 21.6 22.2 108 111 60-140 3
1,3-Dichlorobenzene ug/L ND 20 20 21.4 22.0 107 110 60-140 3
1,3-Dichloropropane ug/L ND 20 20 20.8 20.6 104 103 60-140 1
1,4-Dichlorobenzene ug/L ND 20 20 20.5 21.2 103 106 60-140 3
2,2-Dichloropropane ug/L ND 20 20 20.0 20.8 100 104 60-140 4
2-Chlorotoluene ug/L ND 20 20 20.9 21.0 104 105 60-140 1
4-Chlorotoluene ug/L ND 20 20 20.2 20.7 101 104 60-140 3
Benzene ug/L ND 20 20 19.4 19.6 97 98 60-140 1
Bromobenzene ug/L ND 20 20 21.8 22.1 109 110 60-140 1
Bromochloromethane ug/L ND 20 20 22.1 23.2 111 116 60-140 5
Bromodichloromethane ug/L ND 20 20 21.0 21.2 105 106 60-140 1
Bromoform ug/L ND 20 20 20.1 19.8 100 99 60-140 1
Bromomethane ug/L ND 20 20 24.7 24.1 123 121 60-140 2
Carbon tetrachloride ug/L ND 20 20 22.4 22.5 112 112 60-140 0
Chlorobenzene ug/L ND 20 20 21.9 21.7 109 109 60-140 1
Chloroethane ug/L ND 20 20 18.5 19.1 93 96 60-140 3
Chloroform ug/L ND 20 20 19.5 19.9 98 99 60-140 2
Chloromethane ug/L ND 20 20 18.8 17.1 94 86 60-140 9
cis-1,2-Dichloroethene ug/L ND 20 20 19.1 19.7 95 98 60-140 3
cis-1,3-Dichloropropene ug/L ND 20 20 20.5 21.0 103 105 60-140 2
Dibromochloromethane ug/L ND 20 20 23.1 22.6 116 113 60-140 2
Dibromomethane ug/L ND 20 20 22.5 23.2 112 116 60-140 3
Dichlorodifluoromethane ug/L ND 20 20 19.1 19.1 95 96 60-140 0
Diisopropyl ether ug/L ND 20 20 18.1 18.4 91 92 60-140 1
Ethylbenzene ug/L ND 20 20 21.7 21.6 109 108 60-140 0
Hexachloro-1,3-butadiene ug/L ND 20 20 25.7 25.9 129 130 60-140 1
Isopropylbenzene(Cumene) ug/L ND 20 20 21.9 21.9 110 110 60-140 0
m&p-Xylene ug/L ND 40 40 43.3 42.8 108 107 60-140 1
Methyl-tert-butyl ether ug/L 1.4 20 20 18.9 19.4 88 90 60-140 2
Methylene Chloride ug/L ND 20 20 14.8 14.9 74 74 60-140 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville,NC 28078
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I
QUALITY CONTROL DATA i
Project: JW SMITH
Pace Project No.: 92614625
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3704790 3704791
MS MSD
92614625002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
n-Butylbenzene ug/L ND 20 20 21.9 22.1 110 111 60-140 1
n-Propylbenzene ug/L ND 20 20 20.9 21.0 105 105 60-140 1
Naphthalene ug/L ND 20 20 21.0 21.1 105 105 60-140 0
o-Xylene ug/L ND 20 20 21.9 21.9 109 110 60-140 0
sec-Butylbenzene ug/L ND 20 20 21.6 22.2 108 111 60-140 3
Styrene ug/L ND 20 20 21.5 21.3 108 106 60-140 1
tert-Butylbenzene ug/L ND 20 20 18.8 19.1 94 95 60-140 1
Tetrachloroethene ug/L ND 20 20 23.8 24.1 119 120 60-140 1
Toluene ug/L ND 20 20 19.8 20.3 99 101 60-140 2
trans-1,2-Dichloroethene ug/L ND 20 20 19.7 19.8 98 99 60-140 1
trans-1,3-Dichloropropene ug/L ND 20 20 20.2 20.3 101 101 60-140 0
Trichloroethene ug/L ND 20 20 23.0 23.2 115 116 60-140 1
Trichlorofluoromethane ug/L ND 20 20 18.2 18.9 91 94 60-140 4
Vinyl chloride ug/L ND 20 20 21.7 22.1 109 110 60-140 2
1,2-Dichloroethane-d4(S) % 84 85 70-130
4-Bromofluorobenzene(S) % 100 100 70-130
Toluene-d8(S) % 95 95 70-130
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aeAnalytical® Huntersville,NC 28078
/ www.pacslabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
QC Batch: 710825 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92614625001,92614625002
METHOD BLANK: 3706461 Matrix: Water
Associated Lab Samples: 92614625001,92614625002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 07/15/22 11:23
LABORATORY CONTROL SAMPLE: 3706462
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 251 236 94 90-110
SAMPLE DUPLICATE: 3706674
92614700001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 168 192 13
SAMPLE DUPLICATE: 3706675
92614597002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 79.8 80.4 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
® 9800 Kinsey Ave. Suite100
aceAnalytical
Huntersville,NC 28078078
www.pacalabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92614625
QC Batch: 711662 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92614625001,92614625002
METHOD BLANK: 3710960 Matrix: Water
Associated Lab Samples: 92614625001,92614625002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L ND 0.020 07/20/22 17:50
LABORATORY CONTROL SAMPLE: 3710961
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.053 107 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3710962 3710963
MS MSD
35729882001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L 0.16 0.05 0.05 0.16 0.19 -13 53 90-110 19 M1,R1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3710964 3710965
MS MSD
92614943002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L <0.020 0.05 0.05 0.057 0.055 82 77 90-110 4 M1
Results presented on this page are in the units indicated by the"units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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Huntersville,NC 28078078
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[phone]
i
QUALIFIERS
Project: JW SMITH
Pace Project No.: 92614625
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kinsey Ave. Suite100
Huntersville,NC 28078078
www.pacslabs.com [phone]
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JW SMITH
Pace Project No.: 92614625
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92614625001 INF. SM 6200B 710512
92614625002 EFF. SM 6200B 710512
92614625001 INF. SM 2540D-2015 710825
92614625002 EFF. SM 2540D-2015 710825
92614625001 INF. EPA 420.4 Rev 1.0 1993 711662 EPA420.4 Rev 1.0 1993 711845
92614625002 EFF. EPA420.4 Rev 1.0 1993 711662 EPA420.4 Rev 1.0 1993 711845
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/21/2022 07:11 AM without the written consent of Pace Analytical Services,LLC. Page 16 of 19

uC#_Title: ENV-FRM-HUN1-0083 v01—Sample Condition Upon Receipt
-Pace
Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville ElEden❑ Greenwood❑ Hunt rsville Raleigh❑ Mer"'�irsvillel-1 Atlanta❑ Kernersville❑
Sample Condition Client Name: 1 ('',�(y r t1V r r d GAP / WO# : 926
Upon Receipt / Project M: (�1�625
Courier: ❑Fed E ❑UPS Rhe5r:
❑Client IIIII1 IIIII IIIIII1 I'II
92814625
Custody Seal Present? Dyes ,d 'o Seals Intact? Oyes No
�7
Date/Initials Person Examining Canlents�� / 3/2
,
Packing Material: &I/Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Fro n?
Thermome r: Oyes ❑Na
IR Gun ID: I 2,1--0 6 L' Type of Ice: et ❑Blue ❑None
Correction Factor:
Cooler Temp: ` Add/Subtract(°C) 0 Temp should be above freezing to 6°C
Cooler Temp Corrected °C) , Z ❑Samples out of temp criteria.Samples on ice,cool'ng process
has begun
USDA Regulated Soil( /A,w ter sample)
Did samples originate in a qu antine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(i ern ionally,
(check maps)?Dyes including Hawaii and Puerto Rico)?Oyes o
Comments/Discrepancy:
Chain of Custody Present? es ❑No ON/A 1.
Samples Arrived within Hold Time? Yes ON/A 2.
Short Hold Time Analysis(<72 hr.)? Oyes ON/A 3.
Rush Turn Around Time Requested? ❑Y s zit. o ON/A 4.
Sufficient Volume? es ❑No ❑N/A 5.
Correct Containers Used? es ONo ON/A 6.
-Pace Containers Used? es ❑No ON/A
Containers Intact? es ONE ON/A 7
Dissolved analysis:Samples Field Filtered? Oyes o ON/A 8.
Sample Labels Match COC? Riles ❑No ON/A 9.
-Includes Date/Time/ID/Analysis Matrix: `v�
Headspace in VOA Vials(>5.6mm)? Yes ❑ o ON/A 10.
Trip Blank Present? Oyes No ON/A 11.
Trip Blank Custody Seals Present? Oyes ON/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
PfojecLAAanaget SRF Review: Date: — -- - -
Page 17 of 19
Qualtrax ID:69614 Page 1 of 2

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—? CHAIN-OF-CUSTODY/Analytical Request Document °'
Pace The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. co
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Submitting a sample via this chain Cl custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info.pacelabs.comlhubfs/pas-standard-terms.pdf. d
Section A Section B Section C
Required Client information: Required Project Information: Invoice Information: Page: 1 Of 1
Cemoany pyramid Environmental Report To Tnfunovic.Mika Attention
Address t'p3 Industrial Avenue Copy To Company Name
Greensboro.NC 2741E Address
Regulatory Agency
Email: Purchase Order n Pace Quote
Phone. i.336)335-3174 IFaa Project Name ,1W Smith(2022-180 NPDESI Pace Protect Manager nicole.d'[e-mail]. State/Location
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite Huntersville,NC 2807878
www.pacelabs.cam [phone]
September 07, 2022
Mr. Mika Trifunovic
Pyramid Environmental
P.O. Box 16265
Greensboro, NC 27416
RE: Project: JW SMITH
Pace Project No.: 92622459
Dear Mr.Trifunovic:
Enclosed are the analytical results for sample(s)received by the laboratory on August 25, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
D ' -
Nicole D'Oleo
nicole.d'[e-mail]
[phone]
Project Manager
Enclosures
0%:0j► REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 1 of 19

Pace Analytical Services,LLC
i ®aceAnalytcal 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
I
CERTIFICATIONS
Project: JW SMITH
Pace Project No.: 92622459
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville, NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#: LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.cam [phone]
I
SAMPLE ANALYTE COUNT
Project: JW SMITH
Pace Project No.: 92622459
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92622459001 INF SM 6200B SAS 63 PASI-C
SM 2540D-2015 MAB2 1 PASI-A
EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A
92622459002 EFF SM 6200B SAS 63 PASI-C
SM 2540D-2015 MAB2 1 PASI-A
EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92622459
Sample: INF Lab ID: 92622459001 Collected: 08/24/22 15:00 Received: 08/25/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene 101 ug/L 2.0 4 08/27/22 08:00 71-43-2
Bromobenzene ND ug/L 2.0 4 08/27/22 08:00 108-86-1
Bromochloromethane ND ug/L 2.0 4 08/27/22 08:00 74-97-5
Bromodichloromethane ND ug/L 2.0 4 08/27/22 08:00 75-27-4
Bromoform ND ug/L 2.0 4 08/27/22 08:00 75-25-2
Bromomethane ND ug/L 20.0 4 08/27/22 08:00 74-83-9
n-Butylbenzene ND ug/L 2.0 4 08/27/22 08:00 104-51-8
sec-Butylbenzene ND ug/L 2.0 4 08/27/22 08:00 135-98-8
tert-Butylbenzene ND ug/L 2.0 4 08/27/22 08:00 98-06-6
Carbon tetrachloride ND ug/L 2.0 4 08/27/22 08:00 56-23-5
Chlorobenzene ND ug/L 2.0 4 08/27/22 08:00 108-90-7
Chloroethane ND ug/L 4.0 4 08/27/22 08:00 75-00-3
Chloroform ND ug/L 2.0 4 08/27/22 08:00 67-66-3
Chloromethane ND ug/L 4.0 4 08/27/22 08:00 74-87-3
2-Chlorotoluene ND ug/L 2.0 4 08/27/22 08:00 95-49-8
4-Chlorotoluene ND ug/L 2.0 4 08/27/22 08:00 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 4.0 4 08/27/22 08:00 96-12-8
Dibromochloromethane ND ug/L 2.0 4 08/27/22 08:00 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 2.0 4 08/27/22 08:00 106-93-4
Dibromomethane ND ug/L 2.0 4 08/27/22 08:00 74-95-3
1,2-Dichlorobenzene ND ug/L 2.0 4 08/27/22 08:00 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 4 08/27/22 08:00 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 4 08/27/22 08:00 106-46-7
Dichlorodifluoromethane ND ug/L 2.0 4 08/27/22 08:00 75-71-8
1,1-Dichloroethane ND ug/L 2.0 4 08/27/22 08:00 75-34-3
1,2-Dichloroethane 3.7 ug/L 2.0 4 08/27/22 08:00 107-06-2
1,1-Dichloroethene ND ug/L 2.0 4 08/27/22 08:00 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 4 08/27/22 08:00 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 4 08/27/22 08:00 156-60-5
1,2-Dichloropropane ND ug/L 2.0 4 08/27/22 08:00 78-87-5
1,3-Dichloropropane ND ug/L 2.0 4 08/27/22 08:00 142-28-9
2,2-Dichloropropane ND ug/L 2.0 4 08/27/22 08:00 594-20-7
1,1-Dichloropropene ND ug/L 2.0 4 08/27/22 08:00 563-58-6
cis-1,3-Dichloropropene ND ug/L 2.0 4 08/27/22 08:00 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 4 08/27/22 08:00 10061-02-6
Diisopropyl ether 2.9 ug/L 2.0 4 08/27/22 08:00 108-20-3
Ethylbenzene 36.9 ug/L 2.0 4 08/27/22 08:00 100-41-4
Hexachloro-1,3-butadiene ND ug/L 8.0 4 08/27/22 08:00 87-68-3
Isopropylbenzene(Cumene) 4.4 ug/L 2.0 4 08/27/22 08:00 98-82-8
Methylene Chloride 33.2 ug/L 8.0 4 08/27/22 08:00 75-09-2 C9
Methyl-tert-butyl ether 321 ug/L 2.0 4 08/27/22 08:00 1634-04-4
Naphthalene 54.9 ug/L 8.0 4 08/27/22 08:00 91-20-3
n-Propylbenzene 2.9 ug/L 2.0 4 08/27/22 08:00 103-65-1
Styrene ND ug/L 2.0 4 08/27/22 08:00 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 2.0 4 08/27/22 08:00 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 2.0 4 08/27/22 08:00 79-34-5
REPORT OF LABORATORY ANALYSIS
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Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 19

Pace Analytical Services,LLC
9800 100
aceAnalytical nceyAve. Suite
Huntersville,NC 28078078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92622459
Sample: INF Lab ID: 92622459001 Collected: 08/24/22 15:00 Received: 08/25/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 2.0 4 08/27/22 08:00 127-18-4
Toluene 361 ug/L 2.0 4 08/27/22 08:00 108-88-3
1,2,3-Trichlorobenzene ND ug/L 8.0 4 08/27/22 08:00 87-61-6
1,2,4-Trichlorobenzene ND ug/L 8.0 4 08/27/22 08:00 120-82-1
1,1,1-Trichloroethane ND ug/L 2.0 4 08/27/22 08:00 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 4 08/27/22 08:00 79-00-5
Trichloroethene ND ug/L 2.0 4 08/27/22 08:00 79-01-6
Trichlorofluoromethane ND ug/L 4.0 4 08/27/22 08:00 75-69-4
1,2,3-Trichloropropane ND ug/L 2.0 4 08/27/22 08:00 96-18-4
1,2,4-Trimethylbenzene ND ug/L 2.0 4 08/27/22 08:00 95-63-6
1,3,5-Trimethylbenzene 111 ug/L 2.0 4 08/27/22 08:00 108-67-8
Vinyl chloride ND ug/L 4.0 4 08/27/22 08:00 75-01-4
m&p-Xylene 273 ug/L 4.0 4 08/27/22 08:00 179601-23-1
o-Xylene 393 ug/L 2.0 4 08/27/22 08:00 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 83 % 70-130 4 08/27/22 08:00 17060-07-0
4-Bromofluorobenzene(S) 97 % 70-130 4 08/27/22 08:00 460-00-4
Toluene-d8(S) 103 % 70-130 4 08/27/22 08:00 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 4.8 mg/L 2.7 1 08/28/22 14:28
420.4 Phenolics,Total Analytical Method: EPA420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable 0.043 mg/L 0.020 1 09/07/22 09:50 09/07/22 13:01 64743-03-9 M1
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92622459
Sample: EFF Lab ID: 92622459002 Collected: 08/24/22 15:30 Received: 08/25/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 08/27/22 07:42 71-43-2
Bromobenzene ND ug/L 0.50 1 08/27/22 07:42 108-86-1
Bromochloromethane ND ug/L 0.50 1 08/27/22 07:42 74-97-5
Bromodichloromethane ND ug/L 0.50 1 08/27/22 07:42 75-27-4
Bromoform ND ug/L 0.50 1 08/27/22 07:42 75-25-2
Bromomethane ND ug/L 5.0 1 08/27/22 07:42 74-83-9
n-Butylbenzene ND ug/L 0.50 1 08/27/22 07:42 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 08/27/22 07:42 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 08/27/22 07:42 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 08/27/22 07:42 56-23-5
Chlorobenzene ND ug/L 0.50 1 08/27/22 07:42 108-90-7
Chloroethane ND ug/L 1.0 1 08/27/22 07:42 75-00-3
Chloroform ND ug/L 0.50 1 08/27/22 07:42 67-66-3
Chloromethane ND ug/L 1.0 1 08/27/22 07:42 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 08/27/22 07:42 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 08/27/22 07:42 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 08/27/22 07:42 96-12-8
Dibromochloromethane ND ug/L 0.50 1 08/27/22 07:42 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 08/27/22 07:42 106-93-4
Dibromomethane ND ug/L 0.50 1 08/27/22 07:42 74-95-3
1,2-Dichlorobenzene ND ug/L 0.50 1 08/27/22 07:42 95-50-1
1,3-Dichlorobenzene ND ug/L 0.50 1 08/27/22 07:42 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 08/27/22 07:42 106-46-7
Dichlorodifluoromethane ND ug/L 0.50 1 08/27/22 07:42 75-71-8
1,1-Dichloroethane ND ug/L 0.50 1 08/27/22 07:42 75-34-3
1,2-Dichloroethane ND ug/L 0.50 1 08/27/22 07:42 107-06-2
1,1-Dichloroethene ND ug/L 0.50 1 08/27/22 07:42 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 08/27/22 07:42 156-59-2
trans-1,2-Dichloroethene ND ug/L 0.50 1 08/27/22 07:42 156-60-5
1,2-Dichloropropane ND ug/L 0.50 1 08/27/22 07:42 78-87-5
1,3-Dichloropropane ND ug/L 0.50 1 08/27/22 07:42 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 08/27/22 07:42 594-20-7
1,1-Dichloropropene ND ug/L 0.50 1 08/27/22 07:42 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 08/27/22 07:42 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 08/27/22 07:42 10061-02-6
Diisopropyl ether ND ug/L 0.50 1 O8/27/22 07:42 108-20-3
Ethylbenzene ND ug/L 0.50 1 08/27/22 07:42 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 08/27/22 07:42 87-68-3
Isopropylbenzene(Cumene) ND ug/L 0.50 1 08/27/22 07:42 98-82-8
Methylene Chloride ND ug/L 2.0 1 08/27/22 07:42 75-09-2
Methyl-tert-butyl ether 1.3 ug/L 0.50 1 08/27/22 07:42 1634-04-4
Naphthalene ND ug/L 2.0 1 08/27/22 07:42 91-20-3
n-Propylbenzene ND ug/L 0.50 1 08/27/22 07:42 103-65-1
Styrene ND ug/L 0.50 1 08/27/22 07:42 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 08/27/22 07:42 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 08/27/22 07:42 79-34-5
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 ncey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: JW SMITH
Pace Project No.: 92622459
Sample: EFF Lab ID: 92622459002 Collected: 08/24/22 15:30 Received: 08/25/22 09:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 0.50 1 08/27/22 07:42 127-18-4
Toluene ND ug/L 0.50 1 08/27/22 07:42 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2.0 1 08/27/22 07:42 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2.0 1 08/27/22 07:42 120-82-1
1,1,1-Trichloroethane ND ug/L 0.50 1 08/27/22 07:42 71-55-6
1,1,2-Trichloroethane ND ug/L 0.50 1 08/27/22 07:42 79-00-5
Trichloroethene ND ug/L 0.50 1 08/27/22 07:42 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/27/22 07:42 75-69-4
1,2,3-Trichloropropane ND ug/L 0.50 1 08/27/22 07:42 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 08/27/22 07:42 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 08/27/22 07:42 108-67-8
Vinyl chloride ND ug/L 1.0 1 08/27/22 07:42 75-01-4
m&p-Xylene ND ug/L 1.0 1 08/27/22 07:42 179601-23-1
o-Xylene ND ug/L 0.50 1 08/27/22 07:42 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 84 % 70-130 1 08/27/22 07:42 17060-07-0
4-Bromofluorobenzene(S) 99 % 70-130 1 08/27/22 07:42 460-00-4
Toluene-d8(S) 104 % 70-130 1 08/27/22 07:42 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.6 1 08/28/22 14:29
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.020 1 09/07/22 09:50 09/07/22 13:05 64743-03-9
REPORT OF LABORATORY ANALYSIS
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Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 19

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelahs.com [phone]
I
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
QC Batch: 719936 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92622459001,92622459002
METHOD BLANK: 3752098 Matrix: Water
Associated Lab Samples: 92622459001,92622459002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/27/22 03:31
1,1,1-Trichloroethane ug/L ND 0.50 08/27/22 03:31
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/27/22 03:31
1,1,2-Trichloroethane ug/L ND 0.50 08/27/22 03:31
1,1-Dichloroethane ug/L ND 0.50 08/27/22 03:31
1,1-Dichloroethene ug/L ND 0.50 08/27/22 03:31
1,1-Dichloropropene ug/L ND 0.50 08/27/22 03:31
1,2,3-Trichlorobenzene ug/L ND 2.0 08/27/22 03:31
1,2,3-Trichloropropane ug/L ND 0.50 08/27/22 03:31
1,2,4-Trichlorobenzene ug/L ND 2.0 08/27/22 03:31
1,2,4-Trimethylbenzene ug/L ND 0.50 08/27/22 03:31
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/27/22 03:31
1,2-Dibromoethane(EDB) ug/L ND 0.50 08/27/22 03:31
1,2-Dichlorobenzene ug/L ND 0.50 08/27/22 03:31
1,2-Dichloroethane ug/L ND 0.50 08/27/22 03:31
1,2-Dichloropropane ug/L ND 0.50 08/27/22 03:31
1,3,5-Trimethylbenzene ug/L ND 0.50 08/27/22 03:31
1,3-Dichlorobenzene ug/L ND 0.50 08/27/22 03:31
1,3-Dichloropropane ug/L ND 0.50 08/27/22 03:31
1,4-Dichlorobenzene ug/L ND 0.50 08/27/22 03:31
2,2-Dichloropropane ug/L ND 0.50 08/27/22 03:31
2-Chlorotoluene ug/L ND 0.50 08/27/22 03:31
4-Chlorotoluene ug/L ND 0.50 08/27/22 03:31
Benzene ug/L ND 0.50 08/27/22 03:31
Bromobenzene ug/L ND 0.50 08/27/22 03:31
Bromochloromethane ug/L ND 0.50 08/27/22 03:31
Bromodichloromethane ug/L ND 0.50 08/27/22 03:31
Bromoform ug/L ND 0.50 08/27/22 03:31
Bromomethane ug/L ND 5.0 08/27/22 03:31
Carbon tetrachloride ug/L ND 0.50 08/27/22 03:31
Chlorobenzene ug/L ND 0.50 08/27/22 03:31
Chloroethane ug/L ND 1.0 08/27/22 03:31
Chloroform ug/L ND 0.50 08/27/22 03:31
Chloromethane ug/L ND 1.0 08/27/22 03:31
cis-1,2-Dichloroethene ug/L ND 0.50 08/27/22 03:31
cis-1,3-Dichloropropene ug/L ND 0.50 08/27/22 03:31
Dibromochloromethane ug/L ND 0.50 08/27/22 03:31
Dibromomethane ug/L ND 0.50 08/27/22 03:31
Dichlorodifluoromethane ug/L ND 0.50 08/27/22 03:31
Diisopropyl ether ug/L ND 0.50 08/27/22 03:31
Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
®aceAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
METHOD BLANK: 3752098 Matrix: Water
Associated Lab Samples: 92622459001,92622459002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylbenzene ug/L ND 0.50 08/27/22 03:31
Hexachloro-1,3-butadiene ug/L ND 2.0 08/27/22 03:31
Isopropylbenzene(Cumene) ug/L ND 0.50 08/27/22 03:31
m&p-Xylene ug/L ND 1.0 08/27/22 03:31
Methyl-tert-butyl ether ug/L ND 0.50 08/27/22 03:31
Methylene Chloride ug/L ND 2.0 08/27/22 03:31
n-Butylbenzene ug/L ND 0.50 08/27/22 03:31
n-Propylbenzene ug/L ND 0.50 08/27/22 03:31
Naphthalene ug/L ND 2.0 08/27/22 03:31
o-Xylene ug/L ND 0.50 08/27/22 03:31
sec-Butylbenzene ug/L ND 0.50 08/27/22 03:31
Styrene ug/L ND 0.50 08/27/22 03:31
tert-Butylbenzene ug/L ND 0.50 08/27/22 03:31
Tetrachloroethene ug/L ND 0.50 08/27/22 03:31
Toluene ug/L ND 0.50 08/27/22 03:31
trans-1,2-Dichloroethene ug/L ND 0.50 08/27/22 03:31
trans-1,3-Dichloropropene ug/L ND 0.50 08/27/22 03:31
Trichloroethene ug/L ND 0.50 08/27/22 03:31
Trichlorofluoromethane ug/L ND 1.0 08/27/22 03:31
Vinyl chloride ug/L ND 1.0 08/27/22 03:31
1,2-Dichloroethane-d4(S) % 84 70-130 08/27/22 03:31
4-Bromofluorobenzene(S) % 100 70-130 08/27/22 03:31
Toluene-d8(S) % 105 70-130 08/27/22 03:31
LABORATORY CONTROL SAMPLE: 3752099
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L 50 49.4 99 60-140
1,1,1-Trichloroethane ug/L 50 49.0 98 60-140
1,1,2,2-Tetrachloroethane ug/L 50 45.8 92 60-140
1,1,2-Trichloroethane ug/L 50 50.1 100 60-140
1,1-Dichloroethane ug/L 50 44.9 90 60-140
1,1-Dichloroethene ug/L 50 43.9 88 60-140
1,1-Dichloropropene ug/L 50 44.2 88 60-140
1,2,3-Trichlorobenzene ug/L 50 35.8 72 60-140
1,2,3-Trichloropropane ug/L 50 43.0 86 60-140
1,2,4-Trichlorobenzene ug/L 50 39.0 78 60-140
1,2,4-Trimethylbenzene ug/L 50 42.9 86 60-140
1,2-Dibromo-3-chloropropane ug/L 50 45.7 91 60-140
1,2-Dibromoethane(EDB) ug/L 50 52.3 105 60-140
1,2-Dichlorobenzene ug/L 50 41.4 83 60-140
1,2-Dichloroethane ug/L 50 42.7 85 60-140
1,2-Dichloropropane ug/L 50 52.4 105 60-140
1,3,5-Trimethylbenzene ug/L 50 44.0 88 60-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
LABORATORY CONTROL SAMPLE: 3752099
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,3-Dichlorobenzene ug/L 50 42.0 84 60-140
1,3-Dichloropropane ug/L 50 50.7 101 60-140
1,4-Dichlorobenzene ug/L 50 42.5 85 60-140
2,2-Dichloropropane ug/L 50 46.0 92 60-140
2-Chlorotoluene ug/L 50 42.8 86 60-140
4-Chlorotoluene ug/L 50 41.8 84 60-140
Benzene ug/L 50 48.0 96 60-140
Bromobenzene ug/L 50 43.9 88 60-140
Bromochloromethane ug/L 50 50.4 101 60-140
Bromodichloromethane ug/L 50 46.4 93 60-140
Bromoform ug/L 50 44.8 90 60-140
Bromomethane ug/L 50 41.9 84 60-140
Carbon tetrachloride ug/L 50 45.6 91 60-140
Chlorobenzene ug/L 50 45.4 91 60-140
Chloroethane ug/L 50 35.1 70 60-140
Chloroform ug/L 50 44.3 89 60-140
Chloromethane ug/L 50 42.3 85 60-140
cis-1,2-Dichloroethene ug/L 50 46.1 92 60-140
cis-1,3-Dichloropropene ug/L 50 51.0 102 60-140
Dibromochloromethane ug/L 50 48.3 97 60-140
Dibromomethane ug/L 50 47.9 96 60-140
Dichlorodifluoromethane ug/L 50 36.1 72 60-140
Diisopropyl ether ug/L 50 47.2 94 60-140
Ethylbenzene ug/L 50 43.8 88 60-140
Hexachloro-1,3-butadiene ug/L 50 39.9 80 60-140
lsopropylbenzene(Cumene) ug/L 50 42.8 86 60-140
m&p-Xylene ug/L 100 88.0 88 60-140
Methyl-tert-butyl ether ug/L 50 41.2 82 60-140
Methylene Chloride ug/L 50 47.5 95 60-140
n-Butylbenzene ug/L 50 42.3 85 60-140
n-Propylbenzene ug/L 50 41.9 84 60-140
Naphthalene ug/L 50 40.0 80 60-140
o-Xylene ug/L 50 45.9 92 60-140
sec-Butylbenzene ug/L 50 41.7 83 60-140
Styrene ug/L 50 47.5 95 60-140
tert-Butylbenzene ug/L 50 35.8 72 60-140
Tetrachloroethene ug/L 50 43.9 88 60-140
Toluene ug/L 50 42.7 85 60-140
trans-1,2-Dichloroethene ug/L 50 47.7 95 60-140
trans-1,3-Dichloropropene ug/L 50 49.4 99 60-140
Trichloroethene ug/L 50 53.5 107 60-140
Trichlorofluoromethane ug/L 50 34.4 69 60-140
Vinyl chloride ug/L 50 44.3 89 60-140
1,2-Dichloroethane-d4(S) % 85 70-130
4-Bromofluorobenzene(S) % 99 70-130
Toluene-d8(S) % 95 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
9800 Kincey Ave. Suite100
aceAnalytical Huntersville,NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3752100 3752101
MS MSD
92622299002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane ug/L ND 800 800 843 808 105 101 60-140 4
1,1,1-Trichloroethane ug/L ND 800 800 867 838 108 105 60-140 3
1,1,2,2-Tetrachloroethane ug/L ND 800 800 781 751 98 94 60-140 4
1,1,2-Trichloroethane ug/L ND 800 800 872 826 109 103 60-140 5
1,1-Dichloroethane ug/L ND 800 800 800 784 100 98 60-140 2
1,1-Dichloroethene ug/L ND 800 800 804 791 101 99 60-140 2
1,1-Dichloropropene ug/L ND 800 800 793 762 99 95 60-140 4
1,2,3-Trichlorobenzene ug/L ND 800 800 676 674 85 84 60-140 0
1,2,3-Trichloropropane ug/L ND 800 800 749 722 94 90 60-140 4
1,2,4-Trichlorobenzene ug/L ND 800 800 714 725 89 91 60-140 2
1,2,4-Trimethylbenzene ug/L 2380 800 800 3230 3400 107 128 60-140 5
1,2-Dibromo-3-chloropropane ug/L ND 800 800 742 715 93 89 60-140 4
1,2-Dibromoethane(EDB) ug/L ND 800 800 869 820 109 102 60-140 6
1,2-Dichlorobenzene ug/L ND 800 800 790 778 99 97 60-140 1
1,2-Dichloroethane ug/L ND 800 800 746 708 93 88 60-140 5
1,2-Dichloropropane ug/L ND 800 800 912 879 114 110 60-140 4
1,3,5-Trimethylbenzene ug/L 616 800 800 1480 1510 108 112 60-140 2
1,3-Dichlorobenzene ug/L ND 800 800 800 772 100 97 60-140 3
1,3-Dichloropropane ug/L ND 800 800 833 786 104 98 60-140 6
1,4-Dichlorobenzene ug/L ND 800 800 798 780 100 97 60-140 2
2,2-Dichloropropane ug/L ND 800 800 712 703 89 88 60-140 1
2-Chlorotoluene ug/L ND 800 800 838 820 105 102 60-140 2
4-Chlorotoluene ug/L ND 800 800 804 784 100 98 60-140 2
Benzene ug/L 388 800 800 1300 1290 113 113 60-140 0
Bromobenzene ug/L ND 800 800 848 817 106 102 60-140 4
Bromochloromethane ug/L ND 800 800 888 832 111 104 60-140 6
Bromodichloromethane ug/L ND 800 800 808 792 101 99 60-140 2
Bromoform ug/L ND 800 800 680 667 85 83 60-140 2
Bromomethane ug/L ND 800 800 587 653 73 82 60-140 11
Carbon tetrachloride ug/L ND 800 800 837 841 105 105 60-140 0
Chlorobenzene ug/L ND 800 800 837 809 105 101 60-140 3
Chloroethane ug/L ND 800 800 700 676 87 84 60-140 3
Chloroform ug/L ND 800 800 770 728 96 91 60-140 6
Chloromethane ug/L ND 800 800 728 720 91 90 60-140 1
cis-1,2-Dichloroethene ug/L ND 800 800 823 786 103 98 60-140 5
cis-1,3-Dichloropropene ug/L ND 800 800 828 792 103 99 60-140 4 1
Dibromochloromethane ug/L ND 800 800 753 740 94 92 60-140 2
Dibromomethane ug/L ND 800 800 862 838 108 105 60-140 3
Dichlorodifluoromethane ug/L ND 800 800 732 709 92 89 60-140 3
Diisopropyl ether ug/L 18.9J 800 800 830 778 101 95 60-140 7
Ethylbenzene ug/L 1240 800 800 2090 2110 105 108 60-140 1
Hexachloro-1,3-butadiene ug/L ND 800 800 726 746 91 93 60-140 3
Isopropylbenzene(Cumene) ug/L 54.5 800 800 845 835 99 98 60-140 1
m&p-Xylene ug/L 5490 1600 1600 7140 7270 103 111 60-140 2
Methyl-tert-butyl ether ug/L ND 800 800 676 627 85 78 60-140 8
Methylene Chloride ug/L 153 800 800 924 867 96 89 60-140 6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 19

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3752100 3752101
MS MSD
92622299002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
n-Butylbenzene ug/L ND 800 800 861 877 108 110 60-140 2
n-Propylbenzene ug/L 161 800 800 943 955 98 99 60-140 1
Naphthalene ug/L 1020 800 800 1840 1910 103 111 60-140 3
o-Xylene ug/L 1890 800 800 2690 2730 100 104 60-140 1
sec-Butylbenzene ug/L ND 800 800 800 807 100 101 60-140 1
Styrene ug/L ND 800 800 868 818 109 102 60-140 6
tert-Butylbenzene ug/L ND 800 800 681 682 85 85 60-140 0
Tetrachloroethene ug/L ND 800 800 839 811 105 101 60-140 3
Toluene ug/L 4380 800 800 4910 5070 66 86 60-140 3
trans-1,2-Dichloroethene ug/L ND 800 800 853 816 107 102 60-140 4
trans-1,3-Dichloropropene ug/L ND 800 800 773 756 97 94 60-140 2
Trichloroethene ug/L ND 800 800 969 927 121 116 60-140 4
Trichlorofluoromethane ug/L ND 800 800 686 679 86 85 60-140 1
Vinyl chloride ug/L ND 800 800 807 779 101 97 60-140 4
1,2-Dichloroethane-d4(S) % 88 89 70-130
4-Bromofluorobenzene(S) % 97 95 70-130
Toluene-d8(S) % 97 99 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 19

Pace Analytical Services,LLC
9800 Kincey Ave. Suite100
aceAnalytical
Huntersville,NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
QC Batch: 720027 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92622459001,92622459002
METHOD BLANK: 3752442 Matrix: Water
Associated Lab Samples: 92622459001,92622459002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 08/28/22 14:27
LABORATORY CONTROL SAMPLE: 3752443
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 249 248 100 90-110
SAMPLE DUPLICATE: 3752478
92622413001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 1120 1070 5
SAMPLE DUPLICATE: 3752479
92622469001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 64.0 64.6 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 19

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
1
QUALITY CONTROL DATA
Project: JW SMITH
Pace Project No.: 92622459
QC Batch: 721701 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92622459001,92622459002
METHOD BLANK: 3760162 Matrix: Water
Associated Lab Samples: 92622459001,92622459002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L ND 0.020 09/07/22 12:45
LABORATORY CONTROL SAMPLE: 3760163
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.049 98 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3760164 3760165
MS MSD
92622664005 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L <0.0076 0.05 0.05 0.051 0.047 97 91 90-110 7
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3760166 3760167
MS MSD
92622459001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L 0.043 0.05 0.05 0.086 0.090 86 93 90-110 4 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 19

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.cam [phone]
QUALIFIERS
Project: JW SMITH
Pace Project No.: 92622459
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 19

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.cem [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JW SMITH
Pace Project No.: 92622459
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92622459001 INF SM 6200E 719936
92622459002 EFF SM 6200B 719936
92622459001 INF SM 2540D-2015 720027
92622459002 EFF SM 2540D-2015 720027
92622459001 INF EPA420.4 Rev 1.0 1993 721701 EPA420.4 Rev 1.0 1993 721769
92622459002 EFF EPA 420.4 Rev 1.0 1993 721701 EPA 420.4 Rev 1.0 1993 721769
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/07/2022 03:16 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 19

IJt•M_1 Itie. GIV v-r ruvi-nui I-uuoo vu l aampie s..onaition upon Keceipt
jPace
Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Ashevlfle❑ Eden[1] Greenwood❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name: �, om Lt n�k i s,�ntvnrrlitA�, I
Upon Receipt ro ect#: WO# : 92622459
Courier: fed e ❑UPS ❑Other. ❑Client 1111111111111111111111
❑Commercial
92S22459
Custody Seal Present? UYes Seals Intact/ Dyes No '1�/
Date/Initials Person Examining Contents: ✓� r (1L—
Packing Mater I: Bubble Wrap OBubble Bags ❑None ❑ Other Biological Tissu Froz ?
Thermome r: / _ / Dyes ONo
IR Gun ID: (� �, (.� Type of Ice: \I WVet ❑Blue ❑None
_I Correction Factor:
Cooler Temp: Add/Subtract(°C) 6 Temp should be above freezing to 6°C
❑Samples out of temp criteria.Samples on ice,cooling process
Cooler Temp Corrected VC) �3 has begun
USDA Regulated Soil /A, ter sample)
Did samples originate in a qu rantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(i ernat ally,
(check maps)?❑Yes including Hawaii and Puerto Rico)?❑Yes 1101!K
Comments/Discrepancy:
Chain of Custody Present? �Yes ONo ON/A 1.
Samples Arrived within Hold Time? s ONo ON/A 2.
Short Hold Time Analysis(<72 hr.)? Oyes "�No ON/A 3.
Rush Turn Around Time Requested? ❑Yes \'No ON/A 4.
Sufficient Volume? ses ONO ❑N/A 5.
Correct Containers Used? 'Yes ❑No ON/A 6.
-Pace Containers Used? QY s ONo ON/A
Containers Intact? gYes ONo ON/A 7.
Dissolved analysis:Samples Field Filtered? Dyes I c o ON/A 8.
Sample Labels Match COC? \Yes ONo ON/A 9.
-Includes Date/Time/ID/Analysis Matrix: V V
Headspace in VOA Vials(>5-6mm)? ['Yes "o ON/A 10.
Trip Blank Present? Oyes ' No ON/A 11.
Trip Blank Custody Seals Present? Dyes v`t om ON/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
•
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Managar SRF
Qualtrax ID:69614 Page 1 of 2 Page 17 of 19

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1
°�' CHAIN-OF-CUSTODY/Analytical Request Document
Pat }G The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately
Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info.pacelabs.com/hubfs/pasistandard-erms.pdf.
Section A Se tion B Section C I
Required Client Infor,nation: Required Project Information: Invoice Information: Pape: 1l Of
Company. Pyramr.Environmental Report To. Trdunooc,Mika Attention.
Address 503 Inc(steal Avenue Copy To Company Name
Greensboro,NC 2741' Address'
egulatory Agency
Ema,, Purchase Ordere Pace Ouote.
Phone. 133613:5-3174 lFax Project Name JW Smith(2022-180.NPDESI Pace Protect Manager nicole d'oleo@'pacelabs corn, State I Loeltion
Requested Due Date.•rAiioembe4 Project a Pace Profile a 3498-2 NC
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NC Department of r'
Environmental Quality if
(�
Received
NOV u 2017 Governor
ROY COOPER
Winston-Salem MICHAEL S. REGAN
Secretary
Water Resources Regional Office S. JAY ZIMMERMAN
Environmental Quality Director
October 13,2017
Mr.Jerry Sparks,President
Sparks Oil Company
412 N.Scales Street
Reidsville,North Carolina NC 27320-2909
Subject: Issuance of NPDES Permit NC0088692
J.W. Smith/Camp Springs 76(GW-REM)—PC-1
8920 Cherry Grove Road,Reidsville 27320
Caswell County
Dear Mr. Sparks:
The Division of Water Resources(the Division)hereby issues the attached NPDES permit for the subject
facility.This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and
the Memorandum of Agreement between North Carolina and the U.S.Environmental Protection Agency
dated October 15,2007,or as subsequently amended.
We have made the following updates to your previous permit:
1. The facility map has been updated.The location of Outfall 001 is corrected to the following:
Latitude: 36° 17' 46"(36.296111)
Longitude-79°29' 31"(-79.491944)
2. Regulatory citations have been added.
3. Effluent quarterly monitoring for Total Hardness has been added.Please see discussion below for
more information. Effluent hardness sampling should be performed in conjunction with sampling for
hardness dependent metals(Lead).Please note that since the outfall location is under zero flow
conditions,no instream hardness sampling will be required.
4. For all parameters with limits both monthly average limits and daily maximum limits have been
applied.The US EPA requires both a Monthly Average and a Daily Maximum for parameters that are
limited[40 CFR 122.45(d.)].
5. The limits for Isopropyl Ether(µg/L), 1,2-Dichloroethane(µg/L)and Naphthalene(µg/L)have been
updated to 10 mg/L,5 µg/L and 6 µg/L,respectively.
6. Monitoring of Phenol has been changed to Total Recoverable Phenolics(parameter code 32730).
7. Electronic reporting of discharge monitoring reports(eDMR)has been added in Section A.(2.).
• We have made the following updates for the final permit:
8. The flow limit of 0.009 MGD was corrected to be a monthly average limit.
The NC 2007-2014 Water Quality Standard(WQS)Triennial Review was approved by the NC
Environmental Management Committee(EMC) on November 13,2014.The US EPA subsequently approved
the WQS revisions on April 6, 2016 with some exceptions.The NC Division of Water Resources NPDES
Permitting Unit is required to implement the new dissolved metal standards in all permits public noticed after
Apri16, 2016.
State of North Carolina I Environmental Quality
1617 Mail Service Center I Raleigh,North Carolina 27699-1617
919-707-9000

Mr. Sparks
October 13,2017
Page 2 of 2
The new standards for most metals include acute standards.The freshwater standards for several metals are
expressed as the dissolved form of the metals,and seven metals have hardness-dependent equations.As a
result,the NPDES Permitting Unit will need site-specific effluent hardness data and instream hardness data,
upstream of the discharge, for each facility monitoring these metals in order to calculate permit
limitations. Effluent hardness has been added to this permit at a monitoring frequency of quarterly.No
instream monitoring will be required due to zero flow conditions. See Section A.(1.)Effluent Limitations and
Monitoring Requirements.
If any parts,measurement frequencies,or sampling requirements contained in this permit are
unacceptable,you have the right to an adjudicatory hearing,upon written request submitted within thirty
(30)days after receiving this letter.Your request must take the form of a written petition conforming to
Chapter 150B of North Carolina General Statutes,and you must file it with the Office of Administrative
Hearings,6714 Mail Service Center,Raleigh,North Carolina 27699-6714.Unless such a demand is
made,this permit shall remain final and binding.
Please note that this permit is not transferable except after notice to the Division.The Division may
require modification or revocation and reissuance of the permit.This permit does not affect the legal
requirements to obtain other permits which may be required by the Division of Water Resources or any
other Federal, State,or Local governmental permits that may be required.
If you have questions,or if we can be of further service,please contact Derek Denard at
[[e-mail]]or call(919)807-6307.
•
Respe6tfully, A:if
S.Jay Zimmerm c,D
Division of Water Resources,NCDEQ
Enclosure:NPDES Permit NC0088692(Issuance Final)
hc: Central Files
NPDES Program Files
WSRO Files/Attn:George Smith
ec: Jerry Sparks,Sparks Oil Company [e-mail]]

NPDES Permit NC0088692
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
NPDES
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Sparks Oil. Company
is hereby authorized to discharge wastewater from a facility located at the
J.W. Smith/Camp Springs 76 (GW-REM)
8920 Cherry Grove Road, Camp Springs 27320-0227
Caswell County
to receiving waters designated as a designated as an unnamed tributary to Country Line Creek in the
Roanoke River Basin in accordance with effluent limitations,monitoring requirements, and other
conditions set forth in Parts I, II, III and IV hereof.
This permit shall become effective November 1, 2017.
This permit and authorization to discharge shall expire at midnight on October 31, 2022.
Signed this day October 13,,201 .
/*/
S4'ay Zimmerman, P.G., Diree ....,"
Division of Water Resources
By Authority of the Environmental Management Commission
Page 1of6

NPDES Permit NC0088692
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility,whether for operation or discharge are hereby
revoked. As of this permit issuance, any previously issued permit bearing this number is no longer
effective. Therefore,the exclusive authority to operate and discharge from this facility arises under the
permit conditions,requirements, terms, and provisions included herein.
•
Sparks Oil Company
is hereby authorized to:
1. Continue to operate a 0.009 MGD Groundwater Remediation System/Soil—Vapor Extraction
System consisting of the following components;
• three(3)recovery wells
• an 80-gallon 7.5 Hp air compressor
• a 235-gallon oil-water separator
• a 65-gallon sump tank with a 1 Hp centrifugal pump
• a shallow 5 tray low profile air stripper with a 7.5 Hp air stripper blower
• a 0.5 Hp air stripper discharge centrifugal pump
• a 160-gallon sump pump with two(2) centrifugal pumps
• a bag filter
• one multimedia aggregate filter
• hydro-solenoid backwash system with a backwash trickle filter
• four(4)high pressure carbon filters
• a totalizing meter for system discharge
• a soil vapor extraction well converted from an existing monitoring well
• a soil vapor extraction knock out drum with a 10 Hp blower and 0.5 Hp centrifugal
pumps
located at the W. Smith/Camp Springs 76 Petroleum Contaminated Groundwater Remediation Site
(GW-REM), 8920 Cherry Grove Road,Reidsville, Caswell County; and
2. discharge from said treatment works at the location specified on the attached mapinto an unnamed
g p
tributary to Country Line Creek, currently classified WS-II; HQW within Subbasin 03-02-04 [HUC:
030101040202] of the Roanoke River Basin.
Page 2 of 6

I
NPDES Permit NC0088692
PARTI
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
[15A NCAC 02B .0400 et seq., 02B .0500 et seq.]
During the period beginning on the effective date of this permit and lasting until expiration,the
Permittee is authorized to discharge filter backwash from outfall 001. Such discharges shall be limited,
monitored and reported'by the Permittee as specified below:
LIMITS MONITORING REQUIREMENTS1
EFFLUENT CHARACTERISTICS -
[PARAMETER CODES] Monthly Daily r Measurement Sample Sample 1
Averate _Maximum •Frequenc Type Location
Flow(MGD)2 50050 0.009 MGD Continuous 2 Recording 2 Effluent
Total Suspended Solids(TSS)(mg/L) C0530 20.0 mg/L 20.0 mg/L Monthly Grab Effluent
MTBE(µg/L) 22417 9.5 µg/L 9.5 µg/L Monthly Grab Effluent
Benzene(µg/L) 34030 0.60 µg/L 0.60 µg/L Monthly Grab Effluent
Toluene(µg/L) 34010 5.5 µg/L 5.5 µg/L Monthly Grab Effluent
Ethylbenzene(µg/L) 34371 4 48.5 µg/L 48.5 µg/L Monthly Grab Effluent
-
Total.Xylenes(µg/L) 81551 335 µg/L 335 µg/L Monthly Grab Effluent
Isopropyl Ether(µg/L) 77117 10 mg/L 10 mg/L Monthly Grab Effluent
1,2-Dichloroethane(µg/L) 32103 5 µg/L 5 µg/L, Monthly Grab Effluent
Ethylene Dibromide(µg/L) 77651 Quarterly Grab Effluent
r 1,2,4-Trimethylbenzene(µg/L) 77222 195 µg/L 195 µg/L Monthly Grab Effluent
1,3,5-Trimethylbenzenejtg/L) 77226 315 µg/L 315 µg/L Monthly Grab Effluent
~
n-Propyl Benzene(µg/L) 77224 Quarterly Grab Effluent
Naphthalene(µg/L) 34696 6 µg/L 6 µg/L Monthly Grab Effluent
—
Total Recoverable Phenolics(µg/L) 32730 150 µg/L 150 µg/L Monthly Grab Effluent
Hardness-Total as
[CaCO3 or(Ca+Mg)](mg/L)3 00900 Monitor&Report Quarterly Grab Effluent
Lead(µg/L)3 01051 Quarterly Grab Effluent
Footnotes:
1. The Permittee shall begin submitting Discharge Monitoring Reports electronically using NC DWR's eDMR
application system. See Condition A.(2.).
2. Flow maybe measured using a totalizing flow meter.
3. Effluent hardness sampling should be performed in conjunction with sampling for hardness dependent
metals(Lead).
Conditions:
There shall be no discharge of floating solids or visible foam in other than trace amounts.
Page 3 of 6

NPDES Permit NC0088692
A. (2.) ELECTRONIC REPORTING OF MONITORING REPORTS
{G.S. 143-215.1(b)]
Federal regulations require electronic submittal of all discharge monitoring reports(DMRs)and program
reports.The final NPDES Electronic Reporting Rule was adopted and became effective on December 21,2015.
NOTE: This special condition supplements or supersedes the following sections within Part II of this permit
(Standard Conditions for NPDES Permits):
• Section B. (11.) Signatory Requirements
• Section D. (2.) Reporting
• Section D. (6.) Records Retention
• Section E.(5.) Monitoring Reports
1. Reporting_Reauirements [Supersedes Section D. (2.)and Section E.(5.)(a))
The permittee shall report discharge monitoring data electronically using the NC DWR's Electronic
Discharge Monitoring Report(eDMR)internet application.
Monitoring results obtained during the previous month(s)shall be summarized for each month and
submitted electronically using eDMR. The eDMR system allows permitted facilities to enter monitoring
data and submit DMRs electronically using the internet. Until such time that the state's eDMR application
is compliant with EPA's Cross-Media Electronic Reporting Regulation(CROMERR),permittees will be
required to submit all discharge monitoring data to the state electronically using eDMR and will be required
to complete the eDMR submission by printing,signing,and submitting one signed original and a copy of the
computer printed eDMR to the following address:
NC DEQ/Division of Water Resources/Water Quality Permitting Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
If a permittee is unable to use the eDMR system due to a demonstrated hardship or due to the facility being
physically located in an area where less than 10 percent of the households have broadband access,then a
temporary waiver from the NPDES electronic reporting requirements may be granted and discharge
monitoring data may be submitted on paper DMR forms (MR 1, 1.1,2, 3)or alternative forms approved by
the Director. Duplicate signed copies shall be submitted to the mailing address above. See"How to
Request a Waiver from Electronic Reporting"section below.
Regardless of the submission method,the first DMR is due on the last day of the month following the
issuance of the permit or in the case of a new facility,on the last day of the month following the
commencement of discharge.
Starting on December 21,2020,the permittee must electronically report the following compliance
monitoring data and reports,when applicable:
• Sewer Overflow/Bypass Event Reports;
• Pretreatment Program Annual Reports; and
• Clean Water Act(CWA) Section 316(b)Annual Reports.
Page 4 of 6

i
NPDES Permit NC0088692
The permittee may seek an electronic reporting waiver from the Division(see"How to Request a Waiver
from Electronic Reporting"section below).
2. Electronic Submissions
In accordance with 40 CFR 122.41(1)(9),the permittee must identify the initial recipient at the time of each
electronic submission. The permittee should use the EPA's website resources to identify the initial recipient
for the electronic submission.
Initial recipient of electronic NPDES information from NPDES-regulated facilities means the entity(EPA or
the state authorized by EPA to implement the NPDES program)that is the designated entity for receiving
electronic NPDES data[see 40 CFR 127.2(b)].
EPA plans to establish a website that will also link to the appropriate electronic reporting tool for each type
of electronic submission and for each state. Instructions on how to access and use the appropriate electronic
reporting tool will be available as well. Information on EPA's NPDES Electronic Reporting Rule is found
at: http://www2.epa.gov/compliance/final-national pollutant-discharge-elimination-system-npdes-
electronic-reporting-rule.
Electronic submissions must start by the dates listed in the"Reporting Requirements"section above.
3. How to Request a Waiver from Electronic Reporting
The permittee may seek a temporary electronic reporting waiver from the Division. To obtain an electronic
reporting waiver,a permittee must first submit an electronic reporting waiver request to the Division.
Requests for temporary electronic reporting waivers must be submitted in writing to the Division for written
approval at least sixty(60)days prior to the date the facility would be required wider this permit to begin
submitting monitoring data and reports. The duration of a temporary waiver shall not exceed 5 years and
shall thereupon expire. At such time,monitoring data and reports shall be submitted electronically to the
Division unless the permittee re-applies for and is granted a new temporary electronic reporting waiver by
the Division. Approved electronic reporting waivers are not transferrable. Only permittees with an
approved reporting waiver request may submit monitoring data and reports on paper to the Division for the
period that the approved reporting waiver request is effective.
Information on eDMR and the application for a temporary electronic reporting waiver are found on the
following web page:
http://deq.nc.gov/about/divisions/water-resources/ednu-
4. Sianatory Requirements Supplements Section B.(11.)(b)and Supersedes Section B.(11.) (d)1
All eDMRs submitted to the permit issuing authority shall be signed by a person described in Part U,Section
B.(11.)(a)or by a duly authorized representative of that person as described in Part II,Section B.(11.)(b).
A person, and not a position,must be delegated signatory authority for eDMR reporting purposes.
For eDMR submissions,the person signing and submitting the DMR must obtain an eDMR user account
and login credentials to access the eDMR system. For more information on North Carolina's eDMR system,
registering for eDMR and obtaining an eDMR user account,please visit the following web page:
Page5of6

NPDES Permit NC0088692
http://deq.nc.gov/about/divisions/water-resources/edmr
Certification. Any person submitting an electronic DMR using the state's eDMR system shall make the
following certification[40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE
ACCEPTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief true, accurate, and complete.I am aware that there are significant penalties for
submitting false information, including the possibility offines and imprisonment for knowing violations."
5. Records Retention[Supplements Section D.(6.)i
The permittee shall retain records of all Discharge Monitoring Reports, including eDMR submissions.
These records or copies shall be maintained for a period of at least 3 years from the date of the report. This
period may be extended by request of the Director at any time[40 CFR 122.41].
Page 6 of 6

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County:Caswell 1:24,000 USGS Quad:Cherry Grove,NC

{ PDES Permit Standard Conditions
Page 1 of 18
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.These samples shall be
representative of the wastewater discharged during the sample period.
3/Week
Samples are collected three times per week on three separate calendar days.These samples shall be representative of
the wastewater discharged during the sample period.
Act or"the Act"
The Federal Water Pollution Control Act,also known as the Clean Water Act(CWA),as amended,33 USC 1251, et.
seq.
Annual Average
The arithmetic mean of all"daily discharges"of a pollutant measured during the calendar year. In the case of fecal
coliform,the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system,which is
not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day.However,for purposes of this permit,any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Week
The period from Sunday through the following Saturday.
Calendar Quarter
One of the following distinct periods:January through March,April through June,July through September,and
October through December.
Composite Sampl
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 mL in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period.The
Director may designate the most appropriate method(specific number and size of aliquots necessary,the time interval
between grab samples,etc.)on a case-by-case basis. Samples may be collected manually or automatically.Composite
samples may be obtained by the following methods:
(1) Continuous:a single,continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume:a series of grab samples collected at equal time intervals over a 24 hour period
of discharge and combined proportional to the rate of flow measured at the time of individual sample
collection,or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period with
the time intervals between samples determined by a preset number of gallons passing the sampling point.Flow
measurement between sample intervals shall be determined by use of a flow recorder and totalizer,and the
preset gallon interval between sample collection fixed at no greater than 1/24 of the expected total daily flow at
the treatment system,or
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(4) Constant time/constant volume:a series of grab samples of equal volume collected over a 24-hour period at a
constant time interval.Use of this method requires prior approval by the Director.This method may only be
used in situations where effluent flow rates vary less than 15 percent.The following restrictions also apply:
➢ Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters
> Influent samples shall not be collected more than once per hour.
> Permittees with wastewater treatment systems whose detention time<24 hours shall collect effluent grab
samples at intervals of no greater than 20 minutes apart during any 24-hour period.
> Pernuttees with wastewater treatment systems whose detention time exceeds 24 hours shall collect effluent
grab samples at least every six hours;there must be a minimum of four samples during a 24-hour sampling
period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility.Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling.For pollutants measured in units of mass,the"daily discharge"is calculated as
the total mass of the pollutant discharged over the day.For pollutants expressed in other units of measurement,the
"daily discharge"is calculated as the average measurement of the pollutant over the day. (40 CFR 122.2;see also
"Composite Sample,"above.)
Daily Maximum
The highest"daily discharge"during the calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. Sampling shall be conducted on weekdays except where holidays or other disruptions of normal operations
prevent weekday sampling. If sampling is required for all seven days of the week for any permit parameter(s),that
requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWR or"the Division"
The Division of Water Resources,Department of Environment and Natural Resources.
Effluent
Wastewater discharged following all treatment processes from a water pollution control facility or other point source
whether treated or untreated.
,EMC
The North Carolina Environmental Management Commission
EPA
The United States Environmental Protection Agency
Facility Closure
Cessation of all activities that require coverage under this NPDES permit.Completion of facility closure will allow this
permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N=the number of individual values.For purposes of
calculating the geometric mean,values of"0"(or"<[detection level]")shall be considered=1.
Grab Sample
Individual samples of at least 100 mL collected over a period of time not exceeding 15 minutes.Grab samples can be
collected manually.Grab samples must be representative of the discharge(or the receiving stream,for instream
samples).
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PDES Permit Standard Conditions
Page 3 of 18
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the CWA.
Instantaneous flow measurement
The flow measured during the minimum time required for the flow measuring device or method to produce a result in
that instance.To the extent practical,instantaneous flow measurements coincide with the collection of any grab
samples required for the same sampling period so that together the samples and flow are representative of the discharge
during that sampling period.
Monthly Average(concentration limit)
The arithmetic mean of all "daily discharges"of a pollutant measured during the calendar month. In the case of fecal
coliform or other bacterial parameters or indicators,the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Resources.
Quarterly Average(concentration Imit)
The arithmetic mean of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property,damage to the treatment facilities which causes them to become inoperable,or
substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1)of the CWA.
Upset
An incident beyond the reasonable control of the Pennittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements.An upset does not include noncompliance caused by
operational error,improperly designed treatment facilities,inadequate treatment facilities,lack of preventive
maintenance,or careless or improper operation.
Weekly Average(concentration limit)
The arithmetic mean of all"daily discharges"of a pollutant measured during the calendar week.In the case of fecal
coliform or other bacterial parameters or indicators,the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Comply
The Permittee must comply with all conditions of this permit.Any permit noncompliance constitutes a violation of
the CWA and is grounds for enforcement action;for permit termination,revocation and reissuance,or
modification;or denial of a permit renewal application[40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a)of the
CWA for toxic pollutants and with standards for sewage sludge use or disposal established under section -
405(d)of the CWA within the time provided in the regulations that establish these standards or prohibitions or
standards for sewage sludge use or disposal,even if the permit has not yet been modified to incorporate the
requirement.
b. The CWA provides that any person who violates section[s] 301,302,306,307,308,318 or 405 of the Act,or
any permit condition or limitation implementing any such sections in a permit issued under section 402,or any
requirement imposed in a pretreatment program approved under sections 402(a)(3)or 402(b)(8)of the Act,is
subject to a civil penalty not to exceed$37,500 per day for each violation. [33 USC 1319(d)and 40 CFR
122.41(aX2)]
c. The CWA provides that any person who negligently violates sections 301,302,306,307,308,318,or 405 of
the Act,or any condition or limitation implementing any of such sections in a permit issued under section 402
of the Act,or any requirement imposed in a pretreatment program approved under section 402(a)(3)or
402(bX8)of the Act,is subject to criminal penalties of$2,500 to$25,000 per day of violation,or
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imprisonment of not more than 1 year,or both.In the case of a second or subsequent conviction for a negligent
violation,a person shall be subject to criminal penalties of not more than$50,000 per day of violation,or by
imprisonment of not more than 2 years,or both. [33 USC 1319(c)(1)and 40 CFR 122.41(a)(2)]
d. Any person who knowingly violates such sections,or such conditions or limitations is subject to criminal
penalties of$5,000 to$50,000 per day of violation,or imprisonment for not more than 3 years,or both.In the
case of a second or subsequent conviction for a knowing violation,a person shall be subject to criminal
penalties of not more than$100,000 per day of violation,or imprisonment of not more than 6 years,or both.
[33 USC 1319(c)(2)and 40 CFR 122.41(a)(2)]
e. Any person who knowingly violates section 301,302,303,306,307,308,318 or 405 of the Act,or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,and
who knows at that time that he thereby places another person in imminent danger of death or serious bodily
injury,shall,upon conviction,be subject to a fine of not more than$250,000 or imprisonment of not more than
15 years,or both.In the case of a second or subsequent conviction for a knowing endangerment violation,a
person shall be subject to a fine of not more than$500,000 or by imprisonment of not more than 30 years,or
both.An organization,as defined in section 309(c)(3)(B)(iii)of the CWA,shall,upon conviction of violating
the imminent danger provision,be subject to a fine of not more than$1,000,000 and can be fined up to
$2,000,000 for second or subsequent convictions. [40 CFR 122.41(a)(2)]
f. Under state law,a civil penalty of not more than$25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms,conditions,or requirements of a permit. [North
Carolina General Statutes§ 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301,302,
306,307,308,318 or 405 of this Act.,or any permit condition or limitation implementing any of such sections
in a permit issued under section 402 of this Act.Administrative penalties for Class I violations are not to
exceed$16,000 per violation,with the maximum amount of any Class I penalty assessed not to exceed
$37,500.Penalties for Class II violations are not to exceed$16,000 per day for each day during which the
violation continues,with the maximum amount of any Class U penalty not to exceed$177,500. [33 USC
1319(g)(2)and 40 CFR 122.41(a)(3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit with a reasonable likelihood of adversely affecting human health or the environment[40
CFR 122.41(d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on"Bypassing"(Part II.C.4),"Upsets"(Part H.C.5)and"Power Failures"
(Part lI.C.7),nothing in this permit shall be construed to relieve the Permittee from any responsibilities,liabilities,
or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of the Federal Act,33 USC
1319.Furthermore,the Permittee is responsible for consequential damages,such as fish kills,even though the
responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities,liabilities,or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq.or Section 311 of the Federal Act,33 USG 1321.Furthermore,the Permittee is responsible for
consequential damages,such as fish kills,even though the responsibility for effective compliance may be
temporarily suspended.
5. PropertyRights
The issuance of this permit does not convey any property rights in either real or personal property,or any exclusive
privileges,nor does it authorize any injury to private property or any invasion of personal rights,nor any
infringement of Federal, State or local laws or regulations[40 CFR 122.41(g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
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7. Severability
The provisions of this permit are severable.If any provision of this permit,or the application of any provision of
this permit to any circumstances,is held invalid,the application of such provision to other circumstances,and the
remainder of this permit,shall not be affected thereby[NCGS 150B-23].
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority,within a reasonable time,any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying,revoking and reissuing,or
terminating this permit or to determine compliance with this permit.The Permittee shall also furnish to the Permit
Issuing Authority upon request,copies of records required by this permit[40 CFR 122.41(h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit,the
Permittee must apply for and obtain a new permit[40 CFR 122.41(b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date.In order to receive automatic authorization to
discharge beyond the expiration date,the Permittee shall submit such information,forms,and fees as are required
by the agency authorized to issue permits no later than 180 days prior to the expiration date unless permission for a
later date has been granted by the Director. (The Director shall not grant permission for applications to be
submitted later than the expiration date of the existing permit.)[40 CFR 122.21(d)]Any Permittee that has not
requested renewal at least 180 days prior to expiration,or any Permittee that does not have a permit after the
expiration and has not requested renewal at least 180 days prior to expiration,will subject the Permittee to
enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications,reports,or information submitted to the Permit Issuing Authority shall be signed and certified[40
CFR 122.41(k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section,a responsible
corporate officer means: (a)a president,secretary,treasurer or vice president of the corporation in charge
of a principal business function,or any other person who performs similar policy or decision making
functions for the corporation,or(b)the manager of one or more manufacturing,production,or operating
facilities,provided,the manager is authorized to make management decisions which govern the operation
of the regulated facility including having the explicit or implicit duty of making major capital investment
recommendations,and initiating and directing other comprehensive measures to assure long term
environmental compliance with environmental laws and regulations;the manager can ensure that the
necessary systems are established or actions taken to gather complete and accurate information for permit
application requirements;and where authority to sign documents has been assigned or delegated to the
manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,respectively;or
(3) For a municipality,State,Federal,or other public agency: by either a principal executive officer or
ranking elected official[40 CFR 122.22].
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a.above or by a duly authorized representative of that person.A
person is a duly authorized representative only if
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for the overall operation
of the regulated facility or activity,such as the position of plant manager,operator of a well or well field,
superintendent,a position of equivalent responsibility,or an individual or position having overall
responsibility for environmental matters for the company.(A duly authorized representative may thus be
either a named individual or any individual occupying a named position.);and
(3) The written authorization is submitted to the Permit Issuing Authority[40 CFR 122.22]
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c. Changes to authorization:If an authorization under paragraph(b)of this section is no longer accurate because
a different individual or position has responsibility for the overall operation of the facility,a new authorization
satisfying the requirements of paragraph(b)of this section must be submitted to the Director prior to or
together with any reports,information,or applications to be signed by an authorized representative[40 CFR
122.22]
d. Certification.Any person signing a document under paragraphs a.orb.of this section shall make the following
certification[40 CFR 122.22].NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted Based on my inquiry of the person or persons who manage the system,or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief true, accurate, and complete.I am aware that there are significant penalties for
submitting false information, including the possibility offines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified,revoked and reissued,or terminated for cause.The filing of a request by the
Permittee for a permit modification,revocation and reissuance,or termination,or a notification of planned changes
or anticipated noncompliance does not stay any permit condition[40 CFR 122.41(f)].
13. Permit Modification,Revocation and Reissuance,or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the permit,
revoking and reissuing the permit,or terminating the permit as allowed by the laws,rules,and regulations
contained in Title 40,Code of Federal Regulations,Parts 122 and 123;Title 15A of the North Carolina
Administrative Code,Subchapter 02H.0100;and North Carolina General Statute 143.215.1 et.al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division.Failure to pay the fee in a timely manner in accordance with 15A NCAC 02H.0105(b)(2)
may cause this Division to initiate action to revoke the permit.
Section C. Operation and Maintenance of Pollution Controls
1. Certified Operator
Owners of classified water pollution control systems must designate operators,certified by the Water Pollution
Control System Operators Certification Commission(WPCSOCC),of the appropriate type and grade for the
system,and,for each classification must[T15A NCAC 08G.0201]:
a. designate one Operator In Responsible Charge(ORC)who possesses a valid certificate of the type and grade at
least equivalent to the type and grade of the system;
b. designate one or more Back-up Operator(s)in Responsible Charge(Back-up ORCs)who possesses a valid
certificate of the type of the system and no more than one grade less than the grade of the system,with the
exception of no backup operator in responsible charge is required for systems whose minimum visitation
requirements are twice per year,and
c. submit a signed completed"Water Pollution Control System Operator Designation Form"to the Commission
(or to the local health department for owners of subsurface systems)countersigned by the designated certified
operators,designating the Operator in Responsible Charge(ORC)and the Back-up Operator in Responsible
Charge(Back-up ORC):
(1) 60 calendar days prior to wastewater or residuals being introduced into a new system;or
(2) within 120 calendar days following:
➢ receiving notification of a change in the classification of the system requiring the designation of a new
Operator in Responsible Charge(ORC)and Back-up Operator in Responsible Charge(Back-up ORC)
of the proper type and grade;or
➢ a vacancy in the position of Operator in Responsible Charge(ORC)or Back-up Operator in
Responsible Charge(Back-up ORC).
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(3) within seven calendar days of vacancies in both ORC and Back-up ORC positions replacing or designating
at least one of the responsibilities.
The ORC of each Class I facility(or the Back-up ORC,when acting as surrogate for the ORC)must:
> Visit the facility as often as is necessary to insure proper operation of the treatment system;the treatment
facility must be visited at least weekly
➢ Comply with all other conditions of 15A NCAC 08G .0204.
The ORC of each Class II,Ill and IV facility(or the Back-up ORC,when acting as surrogate for the ORC)must:
➢ Visit the facility as often as is necessary to insure proper operation of the treatment system;the treatment
facility must be visited at least five days per week,excluding holidays
➢ Properly manage and document daily operation and maintenance of the facility
> Comply with all other conditions of 15A NCAC 08G.0204.
2. Proper Operation and Maintenance
The Permittee shall at all times properly operate and maintain all facilities and systems of treatment and control
(and related appurtenances)which are installed or used by the Permittee to achieve compliance with the conditions
of this permit.Proper operation and maintenance also includes adequate laboratory controls and appropriate quality
assurance procedures.This provision requires the Permittee to install and operate backup or auxiliary facilities only
when necessary to achieve compliance with the conditions of the permit[40 CFR 122.41(e)].
NOTE: Properly and officially designated operators are fully responsible for all proper operation and maintenance
of the facility,and all documentation required thereof, whether acting as a contract operator[subcontractor]or a
member of the Permittee's staff.
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit[40 CFR 122.41(c)].
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations[40 CFR 122.41(m)(2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded,but
only if it also is for essential maintenance to assure efficient operation.These bypasses are not subject to the
provisions of Paragraphs b.and c.of this section.
b. Notice[40 CFR 122.41(m)(3)]
(1) Anticipated bypass.If the Permittee knows in advance of the need for a bypass,it shall submit prior notice,
if possible at least ten days before the date of the bypass;including an evaluation of the anticipated quality
and effect of the bypass.
(2) Unanticipated bypass.The Permittee shall submit notice of an unanticipated bypass as required in Part
II.E.6. (24-hour notice).
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass,unless:
(A) Bypass was unavoidable to prevent loss of life,personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime.This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance;and
(C) The Permittee submitted notices as required under Paragraph b.of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system-wide collection system
permit associated with the treatment facility.
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(3) The Permit Issuing Authority may approve an anticipated bypass,after considering its adverse effects,if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1)of this section.
5. Upsets
a. Effect of an upset[40 CFR 122.41(n)(2)]: An upset constitutes an affirmative defense to an action brought for
noncompliance with such technology based permit effluent limitations if the requirements of paragraph b.of
this condition are met.No determination made during administrative review of claims that noncompliance was
caused by upset,and before an action for noncompliance,is fmal administrative action subject to judicial
review.
b. Conditions necessary for a demonstration of upset:Any Pennittee who wishes to establish the affirmative
defense of upset shall demonstrate,through properly signed,contemporaneous operating logs,or other relevant
evidence that:
(1)An upset occurred and that the Pennittee can identify the cause(s)of the upset;
(2)The Permittee facility was at the time being properly operated;and
(3)The Permittee submitted notice of the upset as required in Part II.E.6.(b)of this permit.
(4)The Permittee complied with any remedial measures required under Part II.B.2.of this permit.
c. Burden of proof[40 CFR 122.41(n)(4)]: The Permittee seeking to establish the occurrence of an upset has
the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids,sludges,filter backwash,or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States except as permitted
by the Commission.The Permittee shall comply with all applicable state and Federal regulations governing the
disposal of sewage sludge,including 40 CFR 503,Standards for the Use and Disposal of Sewage Sludge;40 CFR
Part 258,Criteria For Municipal Solid Waste Landfills;and 15A NCAC Subchapter 2T,Waste Not Discharged To
Surface Waters.The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards(as required by 15A NCAC 02H.0124)to
prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by means
of alternate power sources,standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
I. Representative Sampling
Samples collected and measurements taken,as required herein,shall be representative of the permitted discharge.
Samples collected at a frequency less than daily shall be taken on a day and time that is representative of the
discharge for the period the sample represents.All samples shall be taken at the monitoring points specified in this
permit and,unless otherwise specified,before the effluent joins or is diluted by any other wastestream,body of
water,or substance.Monitoring points shall not be changed without notification to and the approval of the Permit
Issuing Authority[40 CFR 122.41(j)1.
2. Reporting
Monitoring results obtained during the previous month(s)shall be summarized for each month and reported on a
monthly Discharge Monitoring Report(DMR)Form(MR 1, 1.1,2,3)or alternative forms approved by the
Director,postmarked no later than the last calendar day of the month following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility,on the last day of the month following the commencement of discharge.Duplicate signed copies of these,
and all other reports required herein,shall be submitted to the following address:
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NC DENR/Division of Water Resources/Water Quality Permitting Section
ATTENTION:Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges.The
devices shall be installed,calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device.Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10%from the true discharge rates throughout the range of expected discharge
volumes.Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once-through condenser cooling water flow monitored by pump logs,or pump hour meters as specified in Part I of
this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Laboratories used for sample analysis must be certified by the Division.Permittees should contact the Division's
Laboratory Certification Section(919 733-3908 or http://portal.ncdenr.org/web/wq/lab/cert)for information
regarding laboratory certifications.
Facilities whose personnel are conducting testing of field-certified parameters only must hold the appropriate field
parameter laboratory certifications.
Test procedures for the analysis of pollutants shall conform to the EMC regulations(published pursuant to NCGS
143-215.63 et.seq.),the Water and Air Quality Reporting Acts,and to regulations published pursuant to Section
304(g),33 USC 1314,of the CWA(as amended),and 40 CFR 136;or in the case of sludge use or disposal,
approved under 40 CFR 136,unless otherwise specified in 40 CFR 503,unless other test procedures have been
specified in this permit[40 CFR 122.41].
To meet the intent of the monitoring required by this permit,all test procedures must produce minimum detection
and reporting levels that are below the permit discharge requirements and all data generated must be reported down
to the minimum detection or lower reporting level of the procedure.If no approved methods are determined
capable of achieving minimum detection and reporting levels below permit discharge requirements,then the most
sensitive(method with the lowest possible detection and reporting level)approved method must be used.
5. Penalties for Tampering
The CWA provides that any person who falsifies,tampers with,or knowingly renders inaccurate,any monitoring
device or method required to be maintained under this permit shall,upon conviction,be punished by a fine of not
more than$10,000 per violation,or by imprisonment for not more than two years per violation,or by both.If a
conviction of a person is for a violation committed after a first conviction of such person under this paragraph,
punishment is a fine of not more than$20,000 per day of violation,or by imprisonment of not more than 4 years,
or both[40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge use
and disposal activities,which shall be retained for a period of at least five years(or longer as required by 40 CFR
503),the Permittee shall retain records of all monitoring information,including:
➢ all calibration and maintenance records
➢ all original chart recordingsfor continuous monitoring instrumentation
strip
➢ copies of all reports required by this permit
➢ copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement,report or application.This period may be extended by request of the Director at any time[40 CFR
122.411.
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7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit,the Permittee shall record the
following information[40 CFR 122.41]:
a. The date,exact place,and time of sampling or measurements;
b. The individual(s)who performed the sampling or measurements;
c. The date(s)analyses were performed;
d. The individual(s)who performed the analyses;
e. The analytical techniques or methods used;and
f. The results of such analyses.
8. Inspection and Entry
The Pennittee shall allow the Director,or an authorized representative(including an authorized contractor acting as
a representative of the Director),upon the presentation of credentials and other documents as may be required by
law,to;
a. Enter,at reasonable times,upon the Permittee's premises where a regulated facility or activity is located or
conducted,or where records must be kept under the conditions of this permit;
b. Have access to and copy,at reasonable times,any records that must be kept under the conditions of this permit;
c. Inspect at reasonable times any facilities,equipment(including monitoring and control equipment),practices,
or operations regulated or required under this permit;and
d. Sample or monitor at reasonable times,for the purposes of assuring permit compliance or as otherwise
authorized by the CWA,any substances or parameters at any location[40 CFR 122.41(i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit.The discharge of
any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall constitute
a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or additions
to the permitted facility[40 CFR 122.41(1)].Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29(b);or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged.This notification applies to pollutants subject neither to effluent limitations in the permit,nor to
notification requirements under 40 CFR 122.42(a)(1);or
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,and
such alteration,addition or change may justify the application of permit conditions that are different from or
absent in the existing permit,including notification of additional use or disposal sites not reported during the
permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit[40 CFR 122.41(1)(2)].
4. Transfers
This permit is not transferable to any person without prior written notice to and approval from the Director in
accordance with 40 CFR 122.61.The Director may condition approval in accordance with NCGS 143-215.1,in
particular NCGS 143-215.1(b)(4)b.2.,and may require modification or revocation and reissuance of the permit,or
a minor modification,to identify the new permittee and incorporate such other requirements as may be necessary
under the CWA[40 CFR 122.41(1)(3), 122.61]or state statute.
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5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit[40 CFR 122.41(1)(4)].
a. Monitoring results must be reported on a Discharge Monitoring Report(DMR)(See Part H.D.2)or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit using test procedures
approved under 40 CFR Part 136 and at a sampling location specified in this permit or other appropriate
instrument governing the discharge,the results of such monitoring shall be included in the calculation and
reporting of the data submitted on the DMR.
6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment.Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances.The written submission
shall contain a description of the noncompliance,and its cause;the period of noncompliance,including exact
dates and times,and if the noncompliance has not been corrected,the anticipated time it is expected to
continue;and steps taken or planned to reduce,eliminate,and prevent reoccurrence of the noncompliance[40
CFR 122.41(1)(6)].
b. The Director may waive the written report on a case-by-case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at(800)662-7956,[phone] or(919)733-3300.
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported under Part II.E.5 and 6.of this permit at the
time monitoring reports are submitted. The reports shall contain the information listed in Part II.E.6. of this permit
[40 CFR 122.41(1)(7)J.
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application,or submitted
incorrect information in a permit application or in any report to the Director,it shall promptly submit such facts or
information[40 CFR 122.41(1)(8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the Division
as soon as possible,but in no case more than 24 hours or on the next working day following the occurrence or first
knowledge of the occurrence of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic,such as the dumping of the contents of a sludge
digester;the known passage of a slug of hazardous substance through the facility;or any other unusual
circumstances.
b. Any process unit failure,due to known or unknown reasons,that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps,aerators,compressors,etc.
c. Any failure of a pumping station,sewer line,or treatment facility resulting in a by-pass without treatment of all
or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.Also see reporting requirements for municipalities in Part IV.C.2.c.of this permit.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2)or Section 308 of the Federal Act,33
USC 1318,all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division.As required by the Act,effluent data shall not be considered confidential.Knowingly making any
false statement on any such report may result in the imposition of criminal penalties as provided for in NCGS 143-
215.1(b)(2)or in Section 309 of the Federal Act.
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•
11. Penalties for Falsification of Reports
The CWA provides that any person who knowingly makes any false statement,representation,or certification in
any record or other document submitted or required to be maintained under this permit,including monitoring
reports or reports of compliance or noncompliance shall,upon conviction,be punished by a fine of not more than
$25,000 per violation,or by imprisonment for not more than two years per violation,or by both[40 CFR 122.41].
12. Annual Performance Reports
Permittees who own or operate facilities that primarily collect or treat municipal or domestic wastewater and have
an average annual flow greater than 200,000 gallons per day shall provide an annual report to the Permit Issuing
Authority and to the users/customers served by the Permittee(NCGS 143-215.1C).The report shall summarize the
performance of the collection or treatment system,as well as the extent to which the facility was compliant with
applicable Federal or State laws,regulations and rules pertaining to water quality.The report shall be provided no
later than sixty days after the end of the calendar or fiscal year,depending upon which annual period is used for
evaluation.
The report shall be sent to:
NC DENR/Division of Water Resources/Water Quality Permitting Section
ATTENTION:Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
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PART III
OTHER REQUIREMENTS
Section A. Construction
a. The Permittee shall not commence construction of wastewater treatment facilities,nor add to the plant's treatment
capacity,nor change the treatment process(es)utilized at the treatment plant unless(1)the Division has issued an
Authorization to Construct(AtC)permit or(2)the Permittee is exempted from such AC permit requirements
under Item b.of this Section.
b. In accordance with NCGS 143-215.1(a5)[SL 2011-394],no permit shall be required to enter into a contract for the
construction,installation,or alteration of any treatment work or disposal system or to construct,install,or alter any
treatment works or disposal system within the State when the system's or work's principle function is to conduct,
treat, equalize,neutralize, stabilize,recycle, or dispose of industrial waste or sewage from an industrial facility and
the discharge of the industrial waste or sewage is authorized under a permit issued for the discharge of the
industrial waste or sewage into the waters of the State. Notwithstanding the above,the permit issued for the
discharge may be modified if required by federal regulation.
c. Issuance of an AC will not occur until Final Plans and Specifications for the proposed construction have been
submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall,upon written notice from the Director, conduct groundwater monitoring as may be required to
determine the compliance of this NPDES permitted facility with the current groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe(40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge,on a routine or frequent basis,of
any toxic pollutant which is not limited in the permit,if that discharge will exceed the highest of the following
"notification levels";
(1) One hundred micrograms per liter(100 µg/L);
(2) Two hundred micrograms per liter(200 µg/L)for acrolein and acrylonitrile; five hundred micrograms per liter
(500 µg/L)for 2,4-dinitrophenol and for 2-methyl-4,6-dinitrophenol;and one milligram per liter(1 mg/L)for
antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge,on a non-routine or infrequent
basis,of a toxic pollutant which is not limited in the permit,if that discharge will exceed the highest of the
following"notification levels";
(1) Five hundred micrograms per liter(500 µg/L);
(2) One milligram per liter(1 mg/L)for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system covered
by this permit.The Division may require specific measures during deactivation of the system to prevent adverse
impacts to waters of the State.This permit cannot be rescinded while any activities requiring this permit continue at the
permitted facility.
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PART IV
SPECIAL CONDITIONS FOR MUNICIPAL FACILITIES
Section A. Definitions
In addition to the defmitions in Part II of this permit,the following definitions apply to municipal facilities:
Indirect Discharge or Industrial User
Any non-domestic source that discharges wastewater containing pollutants into a POTW regulated under section
307(b),(c)or(d)of the CWA. [40 CFR 403.3 (i)and(j)and 15A NCAC 02H.0903(bX11)]
Interference
Inhibition or disruption of the POTW treatment processes;operations;or its sludge process,use,or disposal which
causes or contributes to a violation of any requirement of the Pertnittee's(or any satellite POTW's if different from the
Permittee)NPDES,collection system,or non-discharge permit or prevents sewage sludge use or disposal in
compliance with specified applicable State and Federal statutes,regulations,or permits. [15A NCAC 02H
.0903(b)(14)]
Pass Through
A discharge which exits the POTW into waters of the State in quantities or concentrations which,alone or with
discharges from other sources,causes a violation,including an increase in the magnitude or duration of a violation,of
the Permittee's(or any satellite POTW's,if different from the Permittee)NPDES,collection system,or non-discharge
permit. [15A NCAC 02H.0903(b)(23)]
Publicly Owned Treatment Works(POTW)
A treatment works as defined by Section 212 of the CWA,which is owned by a State or local government organization.
This definition includes any devices and systems used in the storage,treatment,recycling and reclamation of municipal
sewage or industrial wastes of a liquid nature.It also includes the collection system,as defined in 15A NCAC 2T
.0402,only if it conveys wastewater to a POTW treatment plant.The term also means the local government
organization,or municipality,as defined in section 502(4)of the CWA,which has jurisdiction over indirect discharges
to and the discharges from such a treatment works.In this context,the organization may be the owner of the POTW
treatment plant or the owner of the collection system into which an indirect discharger discharges.This second type of
POTW may be referred to as a"satellite POTW organization." [15A NCAC 02H.0903(b)(26)]
"Significant Industrial User"or"SIU"
An Industrial User that discharges wastewater into a publicly owned treatment works and that[15A NCAC 02H
.0903(b)(33)]:
1. Discharges an average of 25,000 gallons per day or more of process wastewater to the POTW(excluding sanitary,
noncontact cooling and boiler blowdown wastewaters);or
2. Contributes process wastewater which makes up five percent or more of the NPDES or non-discharge permitted
flow limit or organic capacity of the POTW treatment plant.In this context,organic capacity refers to BOD,TSS
and ammonia;or
3. Is subject to categorical standards under 40 CFR Part 403.6 and 40 CFR Parts 405-471;or
4. Is designated as such by the Permittee on the basis that the Industrial User has a reasonable potential for adversely
affecting the POTW's operation or for violating any pretreatment standard or requirement,or the POTW's effluent
limitations and conditions in its NPDES or non-discharge permit,or to limit the POTW s sludge disposal options;
5. Subject to approval under 15A NCAC 02H.0907(b),the Permittee may determine that an Industrial User meeting
the criteria in paragraphs 1 or 2 of this definition above has no reasonable potential for adversely affecting the
POTW's operation or for violating any pretreatment standard or requirement,the POTW's effluent limitations and
conditions in its NPDES or non-discharge permit,or to limit the POTW's sludge disposal options,and thus is not a
Significant Industrial User(SIU);or
6. Subject to approval under 15A NCAC 02H.0907(b),the Permittee may determine that an Industrial User meeting
the criteria in paragraph 3 of this definition above meets the requirements of 40 CFR Part 403.3(v)(2)and thus is a
non-significant categorical Industrial User.
Section B. Publicly Owned Treatment Works(POTWs)
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All POTWs must provide adequate notice to the Director of the following[40 CFR 122.42(b)]:
1. Any new introduction of pollutants into the POTW from an indirect discharger,regardless of the means of
transport,which would be subject to section 301 or 306 of CWA if it were directly discharging those pollutants;
and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger as
influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph,adequate notice shall include information on(1)the quality and quantity of effluent
introduced into the POTW,and(2)any anticipated impact that may result from the change of the quantity or
quality of effluent to be discharged from the POTW.
Section C. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit.Other pollutants attributable to inputs from Industrial Users
discharging to the POTW may be present in the Permittee's discharge.At such time as sufficient information
becomes available to establish limitations for such pollutants,this permit may be revised to specify effluent
limitations for any or all of such other pollutants in accordance with best practicable technology or water quality
standards.
2. Prohibited Discharges
a. The Permittee shall develop and enforce their Pretreatment Program to implement the prohibition against the
introduction of pollutants or discharges into the waste treatment system or waste collection system which
cause or contribute to Pass Through or Interference as defined in 15A NCAC 02H.0900 and 40 CFR 403.[40
CFR 403.5(a)(1)]
b. The Permittee shall develop and enforce their Pretreatment Program to implement the prohibitions against the
introduction of the following wastes in the waste treatment or waste collection system[40 CFR 403.5(b)]:
(1) Pollutants which create a fire or explosion hazard in the POTW,including,but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees Centigrade
using the test methods specified in 40 CFR 261.21;
(2) Pollutants which cause corrosive structural damage to the POTW,but in no case discharges with pH lower
than 5.0,unless the works is specifically designed to accommodate such discharges;
(3) Solid or viscous pollutants in amounts which cause obstruction to the flow in the POTW resulting in
Interference;
(4) Any pollutant,including oxygen demanding pollutants(BOD,etc.)released in a Discharge at a flow rate
and/or pollutant concentration which will cause Interference with the POTW;
(5) Heat in amounts which will inhibit biological activity in the POTW resulting in Interference,but in no
case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C(104°F)
unless the Division,upon request of the POTW,approves alternate temperature limits;
(6) Petroleum oil,non-biodegradable cutting oil,or products of mineral oil origin in amounts that will cause
Interference or Pass Through;
(7) Pollutants which result in the presence of toxic gases,vapors,or fumes within the POTW in a quantity that
may cause acute worker health and safety problems;or
(8) Any trucked or hauled pollutants,except at discharge points designated by the POTW.
c. The Permittee shall investigate the source of all discharges into the POTW,including slug loads and other
unusual discharges,which have the potential to adversely impact the Permittee's Pretreatment Program and/or
the operation of the POTW.
The Permittee shall report such discharges into the POTW to the Director or the appropriate Regional Office.
Any information shall be provided orally within 24 hours from the time the Permittee became aware of the
circumstances.A written submission shall also be provided within 5 days of the time the Permittee becomes
aware of the circumstances.The written submission shall contain a description of the discharge;the
investigation into possible sources;the period of the discharge, including exact dates and times;if the
discharge has not ceased,the anticipated time it is expected to continue;and steps taken or planned to reduce,
eliminate,and prevent reoccurrence of the noncompliance,
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3. With regard to the effluent requirements listed in Part I of this permit,it may be necessary for the Permittee to
supplement the requirements of the Federal Pretreatment Standards(40 CFR,Part 403)to ensure compliance by
the Permittee with all applicable effluent limitations. Such actions by the Permittee may be necessary regarding
some or all of the industries discharging to the municipal system.
4. The Permittee shall require any Industrial User(IU)discharging to the POTW to meet Federal Pretreatment
Standards developed under Section 307(b)of the Act as amended(which includes categorical standards and
specific local limits,best management practices and narrative requirements).Prior to accepting wastewater from
any Significant Industrial User(SIU),the Permittee shall either develop and submit to the Division a new
Pretreatment Program or,as necessary,a modification of an existing Pretreatment Program,for approval as
required under section D below as well as 15A NCAC 02H.0907(a)and(b). [40 CFR 122.44(j)(2)]
5. This permit shall be modified,or alternatively,revoked and reissued,to incorporate or modify an approved POTW
Pretreatment Program or to include a compliance schedule for the development of a POTW Pretreatment Program
as required under Section 402(b)(8)of the CWA and implementing regulations or by the requirements of the
approved State pretreatment program,as appropriate.
Section D. Pretreatment Programs
Under authority of sections 307(b)and(c)and 402(b)(8)of the CWA and implementing regulations 40 CFR 403,
North Carolina General Statute 143-215.3(14)and implementing regulations 15A NCAC 02H.0900,and in accordance
with the approved pretreatment program,all provisions and regulations contained and referenced in the pretreatment
program submittal are an enforceable part of this permit. [40 CFR 122.44(j)(2)]
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8)of the CWA,40
CFR 403, 15A NCAC 02H.0900,and the legal authorities,policies,procedures,and fmancial provisions contained in
its pretreatment program submission and Division approved modifications thereof. Such operation shall include but is
not limited to the implementation of the following conditions and requirements.Terms not defined in Part II or Part IV
of this permit are as defined in 15A NCAC 02H.0903 and 40 CFR 403.3.
1. Sewer Use Ordinance(SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program. [15A
NCAC 02H.0903(b)(32),.0905 and.0906(b)(1);40 CFR 403.8(f)(1)and 403.9(b)(1)and(2)]
2. Industrial Waste Survey(IWS)
The Permittee shall implement an IWS consisting of the survey of users of the POTW collection system or
treatment plant,as required by 40 CFR 403.8(f)(2)(i-iii)and 15A NCAC 02H.0905 [also 40 CFR 122.44(j)(1)],
including identification of all Industrial Users that may have an impact on the POTW and the character and amount
of pollutants contributed to the POTW by these Industrial Users and identification of those Industrial Users
meeting the definition of SIU.Where the Permittee accepts wastewater from one or more satellite POTWs,the
IWS for the Permittee shall address all satellite POTW services areas,unless the pretreatment program in those
satellite service areas is administered by a separate Permittee with an approved Pretreatment Program.The
Permittee shall submit a summary of its IWS activities to the Division at least once every five years,and as
required by the Division.The IWS submission shall include a summary of any investigations conducted under
paragraph C.2.c.of this Part.[I5A NCAC 02H.0903(b)(13),.0905 and.0906(b)(2);40 CFR 403.8(f)(2)and 403.9]
3. Monitoring Plan
The Permittee shall implement a Division-approved Monitoring Plan for the collection of facility specific data to
be used in a wastewater treatment plant Headworks Analysis(HWA)for the development of specific pretreatment
local limits.Effluent data from the Plan shall be reported on the DMRs(as required by Parts Il.D and II.E.5.). [15A
NCAC 02H.0903(b)(16),.0906(b)(3)and.0905]
4. Headworks Analysis(HWA)and Local Limits
The Permittee shall obtain Division approval of a HWA at least once every five years,and as required by the
Division.Within 180 days of the effective date of this permit(or any subsequent permit modification)the
Permittee shall submit to the Division a written technical evaluation of the need to revise local limits(i.e.,an
updated HWA or documentation of why one is not needed)[40 CFR 122.44].The Permittee shall develop,in
accordance with 40 CFR 403.5(c)and 15A NCAC 02H.0909,specific Local Limits to implement the prohibitions
listed in 40 CFR 403.5(a)and(b)and 15A NCAC 02H.0909.Pursuant to 40 CFR 403.5,local limits are
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enforceable Pretreatment Standards as defined by 40 CFR 403.3(1). [15A NCAC 02H.0903(b)(10),.0905,and
.0906(b)(4)]
5. Industrial User Pretreatment Permits(IIJP)&Allocation Tables
In accordance with NCGS 143-215.1,the Permittee shall issue to all Significant Industrial Users,permits for
operation of pretreatment equipment and discharge to the Permittee's collection system or treatment works.These
permits shall contain limitations,sampling protocols,reporting requirements,appropriate standard and special
conditions,and compliance schedules as necessary for the installation of treatment and control technologies to
assure that their wastewater discharge will meet all applicable pretreatment standards and requirements.The
Permittee shall maintain a current Allocation Table(AT)which summarizes the results of the HWA and the limits
from all IUPs.Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA. [15A NCAC 02H.0906(b)(6),.0909,.0916,and.0917;40 CFR 403.5,403.8(f)(1)(iii);
NCGS 143-215.67(a)]
6. Authorization to Construct(AtC)
The Permittee shall ensure that an Authorization to Construct permit(AtC)is issued to all applicable Industrial
Users for the construction or modification of any pretreatment facility.Prior to the issuance of an AtC,the
proposed pretreatment facility and treatment process must be evaluated for its capacity to comply with all
Industrial User Pretreatment Permit(IUP)limitations. [15A NCAC 02H.0906(b)(7)and.0905;NCGS 143-
215.1(a)(8)]
7. POTW Inspection&Monitoring of their IUs
The Permittee shall conduct inspection,surveillance,and monitoring activities as described in its Division
approved pretreatment program in order to determine,independent of information supplied by Industrial Users,
compliance with applicable pretreatment standards. [15A NCAC 02H.0908(e);40 CFR 403.8(f)(2)(v)] The
Permittee must:
a. Inspect all Significant Industrial Users(SIUs)at least once per calendar year;
b. Sample all Significant Industrial Users(SIUs)at least once per calendar year for all SIU permit-limited
parameters.including flow except as allowed under 15A NCAC.0908(e);and
c. At least once per year,document an evaluation of any non-significant categorical Industrial User for
compliance with the requirements in 40 CFR 403.3(v)(2),and either continue or revoke the designation as non-
significant.
8. IU Self Monitoring and Reporting
The Permittee shall require all Industrial Users to comply with the applicable monitoring and reporting
requirements outlined in the Division-approved pretreatment program,the industry's pretreatment permit,or in 15A
NCAC 02H.0908. [15A NCAC 02H.0906(b)(5)and.0905;40 CFR 403.8(t)(1)(v)and(2)(iii);40 CFR
122.44(j)(2)and 40 CFR 403.12]
9. Enforcement Response Plan(ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b)and(c)of the CWA(40 CFR 405 et.seq.),prohibitive discharge standards
as set forth in 40 CFR 403.5 and 15A NCAC 02H.0909, specific local limitations, and other pretreatment
requirements.All remedies,enforcement actions and other,shall be consistent with the Enforcement Response
Plan(ERP)approved by the Division. [15A NCAC 02H.0903(b)(7),.0906(b)(8)and.0905;40 CFR 403.8(0(5)1
10. Pretreatment Annual Reports(PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 02H.0908.In lieu of submitting annual
reports,Modified Pretreatment Programs developed under 15A NCAC 02H.0904(b)may be required to submit a
partial annual report or to meet with Division personnel periodically to discuss enforcement of pretreatment
requirements and other pretreatment implementation issues.
For all other active pretreatment programs,the Permittee shall submit two copies of a Pretreatment Annual Report
(PAR)describing its pretreatment activities over the previous calendar year to the Division at the following
address:
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NC DENR/Division of Water Resources/Water Quality Permitting Section
Pretreatment,Emergency Response,and Collection Systems(PERCS)Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
These reports shall be submitted by March 1 of each year and shall contain the following:
a. Narrative
A narrative summary detailing actions taken,or proposed,by the Permittee to correct significant non-
compliance and to ensure compliance with pretreatment requirements;
b. Pretreatment Program Summary(PPS)
A pretreatment program summary(PPS)on forms or in a format provided by the Division;
c. Significant Non-Compliance Report(SNCR)
A list of Industrial Users(Ms)in significant noncompliance(SNC)with pretreatment requirements,and the
nature of the violations on forms or in a format provided by the Division;
d. Industrial Data Summary Forms(IDSF)
Monitoring data from samples collected by both the POTW and the Significant Industrial Users(SIUs).These
analytical results must be reported on Industrial Data Summary Forms(1DSF)or on other forms or in a format
provided by the Division;
e. Other Information
Copies of the POTW's allocation table,new or modified enforcement compliance schedules,public notice of
Ills in SNC,a summary of data or other information related to significant noncompliance determinations for
IUs that are not considered SIUs,and any other information,upon request,which in the opinion of the Director
is needed to determine compliance with the pretreatment implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Industrial Users(ills)that were in significant noncompliance(SNC)
as defined in the Permittee's Division-approved Sewer Use Ordinance with applicable pretreatment requirements
and standards during the previous twelve month period.This list shall be published within four months of the
applicable twelve-month period. [15A NCAC 02H.0903(b)(34),.0908(b)(5)and.0905 and 40 CFR
403.8(f)(2)(viii)]
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results,along with
support information including general records,water quality records,and records of industrial impact on the
POTW and shall retain all other Pretreatment Program records as required by 15A NCAC 02H.0908(f). [15A
NCAC 02H.0908(f);40 CFR 403.12(o)]
13. Pretreatment Program Resources
The Permittee shall maintain adequate funding and qualified personnel to accomplish the objectives of its approved
pretreatment program.and retain a written description of those current levels of inspection. [15A NCAC 02H
.0906(b)(9)and(10)and.0905;40 CFR 403.8(f)(3),403.9(b)(3)]
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits modifications,POTW
monitoring of their Significant Industrial Users(Sills),and Monitoring Plan modifications,shall be considered a
permit modification and shall be governed by 40 CFR 403.18, 15 NCAC 02H .0114 and 15A NCAC 02H.0907.
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