WQ0004268_More Information (Requested)_20180123

,ROY COOPER
gollfq1710r.
cMIIAEL S. REGAN
Secretary
Warer Resources LINDA CULPEPPER
VIRONMENIAL CUALrrY Interim Director
January 23, 2018
JOAN LEE — SENIOR VICE
, Mumiy-pRoyiN, LLC
POST OFFICE BOX 856
WAR8AW, NORTH CAROLINA 28398
Subject: Application No. WQ0004268
Additional Information Request
Murphy -Brown WWIS
Wastewater Irrigation System
Sampson County
Dear Ms. Lee:
Division of Water Resources' 'Central and Regional staff has reviewed -the application package received
November 2, 2017. However, 'additional information is required before the review may be completed.
Please address the items on the attached pages no later than the close of business on Febniary.23, 2018.
Please be aware that you are responsible for meeting all requirements set forth in North Carolina rules and
regulations. Any oversights that occurred in the review of the subject application package are, still the
Applicant's responsibi[ity In addition, any omissions made in responding to the outstanding items in
SeetidnA.
Please reference the subject application:nuniber when providing the requested inforniation. All.revised
and/or additional documentation shall be signed, sealed and dated (where needed), with three copies
submitted to my attentionat the address below.
Tf yon. have any questiOns regarding this request, please do hot hesitate to contact Me .at [phone] or
ashley.kabat®hedermgov. Thank you for your cooperation.
J
Sincerely;
Athley. Kabat, EnVitonmental Engineer
Division of Water Resources
cc: Fayetteville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Permit Application File WQ0004268
Compares.7„
State cif North Carolina I EnvironmentatQuality I Water Resources I Water Quality Permitting I Non -Discharge i'ermining
1617 MailService Center I Raleigh, North Carolina 27699-1617
919-807-6332 -
l';-4tRAP

Ms: Joan Lee
January 23, 2018,
Page 2 of 3
A. Site Maps:
1.
Pleasesubmit a site map showing the redUced irrigation fields redrawni,the following,setbacks from
themost recent permit iapance, amilhe revlew and:compliance boundaries:,
a. The setbacks for iirigation.sites permitted under 15A NCAC 02H 0200 (i.e., Fields A, B, C-
andt0:shali beaslollows distances in. feet):
i. Any habitable residence or place ofpublic assembly under ownership:
ii. Surface waters:
iii. Any well with exception of monitoring wells:
iv. Any property
v. Fublic right nf way:
[15A NCAC:02H .0219.0A
b. The setbacks for irrigation -sites permitted under 15A NCAC 02T .0500 (i.e., Zonesi. through
18A) shall beas fpllows (all distances in feet):
Any habitable residence or place Orpublienasernbly under separate oWnetahip!, 400
ii. Any habitable residence or place of publinassembly owned by the Permittee 200
iii. Any priyateOr public water supply source: Igo
iv.. water: 100.
v. Groundwater lowering ditches : .100
vi.. Surface water diversions: 25
Anywell with exteptidn of raonitoring:wells: 100
viu Any property line 150
ix Top of slope of emhankments or cuts,:oftwo feet or More in;vertiOal height 15
x. Any water line from a disposal system: 10
xi Subsurface groundwater lowering drainage systems 100
Any Swimming pOol: 100
,xiii,Public right ofway 50
'xiv. Nitrification field: 20
xv: Any building foundation or -basement:. 15
[15ANCAC 02'1%0506(0]
c. The setbacks for Storage and treatment Units permitted under 15A NCAC '0211 0200 shall he
,as follows distances infeet):
i. Any. well with exception of monitoring wells:
ii. Any property line:
[15A NCAC 02H .02190)]
d. The setbacks for storage and treatment Unitspermitted under 15A NCAC 02T ,:0500 (i.e.,
•screening facility, etc.) shall be as follows (all distances in feet):
i. Any habitable residence or place of public assembly under separate ownership:.
.ii. Any private .or public water supply source:
iii. Surface waters:
400
.100.
tog
.150
50
100
50

Ms . Joan Lee
January 23, 2018
Page 3 of 3
iv. Any well with exception of monitoring wells:
v. Any property line:
[15A NCAC 02T .0506(01
100
50
2 A map Is attached (Figure 1) showing the sitomap forTields A-D provided to the division with
current Sampson County GIS data for parcel lines and property Ownership. The parcel shape of
the ,property formerly owned by Sager Creek Foods, Inc. has changed and may have resulted in
setback violations from property lines and/or public right of ways. This can he addressed hi one
thefolloviing.ways:
a. Propose the field area be :reduced by capping spray heads and/or reducing_the wetted area by
reducing the area of influence of certain 'spray heads.
b. Record a. setback waiver (attached) with the Sampson County Register of Deeds for each
property which setbacks will not be -met., A copy of the setback waiver after it has been
recorded with the Sanipson County Register cifteeds shoUldha submitted to theDivision.
3. A map is attached (Figure 2). showing the site map for Fields 1-18A provided in the last permit
issuance with current Sampson County GIS data for parcel lines and property ownerShip. These
fields look to be in conapliandelVith the setbacks listed above from the last permit issuance. Verify
the attached map is still accurate and there are no proposed changes to Fields 1-18A.

egend , F =
•A ineiB Fatiticith..
Butteitiall;LLC
arroll •Matthieviis Baggett
Earl Benny King
KAMCP,:,LLC`'''
Maria:'F Baena
Goog(e earth
(c 2018 Googpe

State of North Carolina
Department of Environmental Quality
Division of Water Resources
NON -DISCHARGE WASTWATER SYSTEM 'WAIVER
• AGREEMENT TO:WAIVE: SETBACKS AS REQVIREDi BY
j5A NCAC-02r.050kaj, .0500(b), :0606(a), .0706(9 AND .1006(0
, certify', that I am Adeeded•owner of the property located' at.:
Address:: Parcel No.:
City: State: Zip Code: 'County:
'Furthermore, I certify that I. am authorized to make decisions regarding this property, and that Edo hereby
agree that the setback distances cited below be granted to the Applicant/Ptiiiiittee:listedon the following
,page.
O I Understand the:Setback requirements, set forth In 15A. 'NCAC '01T. For the parcel identified
Above,I vonsentto a -reduced: setback from feet feet, t thereby allowing the,
application of wastewater effluent as near as feet frOnintyproperty line.
0 I understand the setback !TOO:ernpits set forth in 15A NCAC l02T. For the parcel identified
above; I 0000 to a reduced 'setback tom feet, to ( feet, thereby allowing• the
Application Of_wasteWiter effluent as,nearas feettrommty residence.
.1 understand the ,setback requirements set forth in iSA NCAC 92T. For the parcel identified
_ .
above, , I consent to a reduced setback • from feet feet, -thereby allowing the
constructionOf wastewater treatment and storage units as near as feet from my property line
„
understand the setbackrequirements set forth in 15A NCAC 021% For, the. parcel identified
above, 1 vonsent, to a reduced .setback from 'feet :feet; thereby allowing the
construction of wastewatettreatment andstorage units as flOgy feet front my residence.
Signature : Date:
F0104t NPWSW..03-17 ,P'age -of,2

Applicant/Pennittee:
Address: . Parcel No::
City: State: Zip Code: County:,
NORTH CAROLINA, COUNTY
,.a Notary Publie"for COtinty, North Carolina,
do hereby certify that, personally appeared:beforeme this day
and acknowledged the due execution of the foregoing
Witneas iny,hand, and official seal, this the day of
SEAL
Signature,of Notaly Pnblic
MY commission expires
• Once notarized, this form shall be recorded at the Register of Deeds ir .the county or
counties in which the described properties are located. A copy of the recorded
waiver shall be sent to the following address:
Division of Water Resources
Water Quality Permitting Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617-
FORK NDWsw 03-17
P4ge2 of 2

pz-1 dwr
f'
oo' IeEar h
018 000.21,3
grow crop fields (corm. si>>wheat'rot
r, _f �1
surfafe �a dir4r--
Legend
x olvv•2

}
Sager Creek/Delmonte, Pre -Ditch Discharge to Six Run Creek
Compound
Mo i ng Well
)sJo71-
Background (Mill
Run)
Downgradient
(Rowan Rd. Bridge)
Field Parameters
Temp (°C)
19.7
9.6.
11.1
pH (SU)
4.15
7.43
6.67
Cond. (µmhos/cm)
611
106.4 _
175.2
DO (mg/I)
4.21
4.22
9.78
Bacterial (CFU/100m1) ,
Fecal Coliform ,
NA
19
130
Total Coliform
NA
500
520.
Nutrients (mg/L)
TKN
6.8
0.60
0.72
NH3
6.8 -
0.05
. 0.07
KN
0
0.55
0.65
NO Z & NO3
<0.02
0.08
<0.02
P
<0.02
; 0.10.
0.08
Metals (µg/L) " -_
Al .
2,000 .
190
<50.
As
<2
<2 '
<2
Ba
52
21
26
Ca
930 .
7,900
11,000
Cd
<0.5.
<0.5
<0.5
Cr
<5
<5
<5,
Cu
5.3
<2
<2
Fe
4,800
1,900
610
K
17,000
, . 3,800
15,000
Mg
1,300
2,600
'4,400
Mn
45
, 33
30
Na
83,000
5,700
8,600
Ni
3.4
<2
<2
Pb
<2
<2
.. <2
$e
<1
<1
<1
'Sr
<10
29
39
V
<10
<10 -•
<10
Zn
88
<12
<12
Note: Samples collected on 04-Dec-2017 (prior to construction of the ditch)

FIELD DATA FORM •
SAMPLING LOCATION: S1 A4i A/ ('gyp, / 7t%LNt /0-
COLLECTORS: )G• tnl F-)1i e / J J3/he-27L?.
METER USED:
�A/1
STATION
% 41j21201
)LL. p UN
r � 0�
DATE
yymmdd
TIME
24 hr
hhmm
DEPTH
m
x.x
H2O TEMP
°C
x.x -
Atm
Pressure
mmHg
xooc
DO Sat %
x.x
DO mgll
x.xx
COND uS/cm
x.x
pH
x.x
•SECCHI m
x.xx
COMMENTS .
UP i AI 3 0*
r'‘6 20P-
1v4o
9.Vc
6,. )-
3 ?:sZ
4, 22
ca(9:4
7 4-3
AM -
Co uN G goo -Ai
)
iv45
II,) °G
b.0
6947,
--3
175
6.
r✓'-
1-•
.)
5 7,
4.21
4.15
NA-
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A-CA-7-
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P
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•
•
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FieldDataForm Rev0715.xlsx
07/2015

L. i'AC45659
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
FIIBLLCDELMONTE
SAMPSON Collector
FRO Report To
CFR Collect Date:
Collect Time:
Sample Depth
K WHITE
FRO
1 /04/2017 %
13:25
VisitlD
Location ID:
Priority
Sample Matrix:
Loc. Type:
Final Report
If this report is labeled preliminary report, the results have not been validated.
Result/
CAS # Analyte Name PQL Qualifier
LAB
Sample temperature at receipt by lab 2.4
6P082WQ0004268
ROUTINE
(GROUNDWATER
WATER SUPPLY
p�,-I
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC45659
12/05/2017
08_15
MSWIFT
NC Courier
1 /24/18
01/24/2018
Do not use for Regulatory purposes.
Method Analysis
Units
oD
Reference Date
Validated by
12/5/17 PGAUTHIER
NH3 as N in liquid
0.02
NUT
6.8
mg/L as N
EPA 350.1 REV 2 12/7/17
CGREEN
NO2+NO3 as N in liquid
0.02
10:02 fJ
mg/Las N
EPA 353.2 REV 2 12/12/17 • CGREEN
Phosphorus total as P in liquid
0.02
0.02 U
mg/L as P
EPA 365.1 REV 2 12/13/17 CGREEN
Total Kjeldahl N as N in liquid
0.2
1Imo.-s,1
'g--:-
mg/L as N
EPA 351.2 REV 2 12/8/17 CGREEN
7429-90-5 Al by ICP
50
MET
2000
ug/L
EPA200.7 Rev4.4 / 1/12/18 ESTAFFORDI
7440-38-2 As by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7440-38-3 Ba by ICP
10
52
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10
085
mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-43-9 Cd by ICPMS
0.50
0.50 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7440-47-3 Cr by ICPMS
5.0
5.0 U
ug/L
EPA 200.8 Rev5:4 1/4/18 ESTAFFORD1
7440-50-8 Cu by ICPMS
2.0
5.3
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORDI
7439-89-6 Fe by ICP
50
4800
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-09-7 K by ICP
0.10
17
mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7439-95-4 Mg by ICP
0.10
'WA mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7439-96-5 Mn by ICP
10
45
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-23-5 Na by ICP
0.10
831pnt7 mg/L
•
EPA 200.7 Rev4.4 1/19/18 ESTAFFORD1
7440-02-0 Ni by ICPMS
2.0
3.4
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7439-92-1 Pb by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7782-49-2 Se by ICPMS
1.0
1.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7440-24-6 Sr by ICPMS
10
10 U
ug/L
EPA 200.8 Rev5.4
1/5/18 ESTAFFORD1
7440-62-2 V by ICP
10
10 U
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-66-6 Zn by ICPMS
10
88
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
AC45659
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outine
❑Stor water
lis
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yyf
Compliance
❑ COC
I: Ground
L!S
❑ Waste
Monitoring Well
Effluent
Water Supply
Influent❑
a f'
}:'if:l
} . n �`a
LlState Couner
,(i�q:. +, ❑Hand Delivery
4. Other
Notes
�,
nit
FF ' i/>~ '
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�"
❑ Chlorinated ❑De -chlorinated in Field
LL- ` Grab Li Composite
�� i . F . ,: +
7t
t , , t;• . 4 ❑ Other
❑ Emergency❑
❑oA
❑ Blank
❑Solution
Field Blank
Trip Blank
p
❑Filter Blank
❑Other
. "
� (jt# y"
li 3
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Dissolved analysis Enter "NS
❑ Filtered in Field in check -boxes for parameters
•
": /
w y ulf S gELot'
• y. a.FIt ' • /
'� 1,`
; 4.
Imo. , iimitc'' :4:b. ,i,ti
MBAS (surfactants) mg/L
4k,ligOtta'!R 0t'r4II?$5Vr 'fY . M
Tin (Sn) pg/L
Acidity, as CaCO3, to pH 4 5/8 3 mg/L
Oil and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L -
(Ti) - pg/L
Alkalinity, as CaCO3, to pH 4 5/8 3 mg/L
Phenols, Total Recoverable-- pg/L
pg
Antimony (Sb) pg/L
� rrTitanium
Y
anadium (V) pg/L
BOD Biochemical Oxygen Demand, 5-day mg/L
Residue Total (Total-Sohds) mg/L
Arsenic (As) pg/L
Zinc
(Zn) pg/L
cBOD Carbonaceous BOD, 5-day mg/L
Residue. Volatile/Fixed, Total mg/L
Barium (Ba) pg/L
Conform Fecal MF /100m1
Residue Suspended (Suspended Solids) mg/L
Beryllium (Be) pg/L
Boron (B), Total pg/L
Conform Total MF /100m1
Residue Volatile/Fixed, Suspended mg/L
admium (Cd) pg/L
Mercury 1631, low-level ng/L
Conform Tube Fecal /100m1
TOS-Total Dissolved Solids mg/L
alcium(Ca) mg/L
Conform Tube Total /100m1
Silica mg/L
Chromium (Cr), Total pg/L
I)ti t'•t 1 ' ` WA
Specific Conductance, at 25 °C umhos/cm
Sulfide mg/L
Cobalt (Co) pg/L
Acid Herbicides
TOC- Total Organic Carbon mg/L
Tannin & Lignin mg/L
Copper (Cu) pg/L
Organochlonne Pesticides
Turbidity NTU
ron (Fe) pg/L
Organonitrogen Pesticides
09
(j`@ i'�iet 'VOA'
Lead (Pb) pg/L
r
Organophosphorus Pesticides
W
pH s u
Lithium (Li) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Magnesium (Mg) mg/L
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAS)
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
Sulfate mg/L
A. ,
Too " • p >; ,
Molybdenum (Mo) pg/L
Chlorophyll a pg/L
mmonia as N (NH3-N) mg/L
ickel (Ni) pg/L
Volatile Organics (VOA)
Color ADMI c u
itrate-Nitrite as N (NO3+NO2-N) mg/L
•otassium (K) mg/L
Color Platinum Cobalt c u
fTotal
Kjeldahl Nitrogen as N (TKN) mg/L
Selenium (Se) pg/L
TPH Gasoline Range
COD Chemical Oxygen Demand mg/L
'/
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
Cyanide, Total mg/L
1
Nitrite as N (NO2-N) mg/L
V
:.drum (Na) mg/L
ei
o(a' $xy>
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton /Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS •
•may-
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.'AC45660
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
MILL RUN AT ROWAN RD
SAMPSON .
FRO
CFR
Collector:
Report To
Collect Date:
Collect Time:
Sample Depth
K WHITE
FRO
12/04/2017
12_40
0.1
Visit1D
Location ID: 6P082WQ0004268
Priority ROUTINE
Sample Matrix: GROUNDWATER
Loc. Type: ` WATER SUPPLY
Final Report
If this report is labeled preliminary report, the results have not been validated. Donot use for Regulatory purposes.
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC45660
12/05/2017
•08_15
MSWIFT
NC Courier
1/24/18
01/24/2018
CAS # Analvte Name
Sample temperature at receipt by lab
PQL
Result/ r,
Qualifier
LAB •
2.4 • `C
Units
Method Analysis
Reference . Date
Validated by
12/5/17 PGAUTHIER
Coliform, MF Fecal in liquid
1
MIC
19 BIQ1
CFU/100m1
SM 9222 D-1997
12/5/17 ESTAFFORD1
Coliform, MF Total in liquid
1
500 Q1 CFU/loom)
SM 9222 B-1997
12/5/17 ESTAFFORDI
NH3 as N in liquid
0.02
NUT
0.05
mglL as N
EPA 350.1 REV 2 12/7/17 CGREEN
NO2+NO3 as N in liquid
0`.02
0.08
mg/L as N
EPA 353.2 REV 2 12/12/17 CGREEN
Phosphorus_total as P in liquid
0.02
0.10
mg/L as P
EPA 365.1 REV 2 12/13/17 CGREEN
Total Kjeldahl N as N in liquid
0.2
0.60
mg/L as N
EPA 351.2 REV 2 - 12/8/17 CGREEN
7429-90-5 Al by ICP
50
MET
190
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7,440-38-2 As by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7440-38-3 Ba by ICP
10
21
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10
7
mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-43-9 Cd by ICPMS
0.50
0.50 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7440-47-3 • Cr by ICPMS
5.0
5.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7440-50-8 Cu by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7439-89-6 Fe by ICP
50
1900 '
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-09-7 K by ICP
J
0.10
36380 mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7439-95-4 Mg by ICP
0.10
2 mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7439-96-5 Mn by ICP
10
33
ug/L
EPA200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-23-5 Na by ICP
0.10
mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-02-0 Ni by ICPMS
- 2.0
2.0 U ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORDI
7439-92-1 Pb by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7782-49-2 Se by ICPMS
1.0 1.0 U ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7440-24-6 Sr by ICPMS
10
29
ug/L
EPA 200.8 Rev5.4
1/5/18 ESTAFFORDI
7440-62-2 V by ICP
10
10 U
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-66-6 Zn by ICPMS
10
12 U
ug/L
EPA200.8 Rev5.4 1/4/18 ESTAFFORDI
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

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--AF45661
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
North Carolina Division of Water Resources Water Sciences Section LaboratoryResults
SIX RUNS AT ROWAN RD
SAMPSON
FRO
CFR
Collector: K WHITE
Report To FRO
Collect Date: 12/04/2017
Collect Time: 12_45
Sample Depth 0.1
VlsitID
Location ID:
Priority
Sample Matrix:
Loc. Type:
Final Report
if this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
6P082WQ0004268
ROUTINE
SURFACEWATER
RIVER/STREAM
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC45661
12/05/2017
08_15
MSWIFT
NC Courier
1/24/18
01/24/2018
CAS # Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
2.4
Units
'C
Method Analysis
Reference Date Validated by
12/5/17 PGAUTHIER
Coliform, MF Fecal in liquid
MIC -
130 Q1 CFU/1o0m1
SM 9222 D-1997
12/5/17 ESTAFFORDI
Coliform, MF Total in liquid /
1
520 Q1 CFU/1o0m1
SM 9222 B-1997
12/5/17 ESTAFFORDI
NH3 as N in liquid
0.02
NUT
0.07
mg/L as N
EPA 350.1 REV 2 12/7/17 CGREEN
NO2+NO3 as N in liquid
0.02
0.02 U
mg/L as N
EPA 353.2 REV 2 12/12/17 CGREEN
Phosphorus total as P in liquid
0.02
0.08
mg/L as P
EPA 365.1; REV 2
12/13/17 CGREEN
Total Kjeldahl N as N in liquid
0.2
0.72
mg/L as N
EPA 351.2 REV 2 12/8/17 CGREEN
7429-90-5 Al by ICP
50
MET
50 U
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-38-2 As by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORD1
7440-38-3 Ba by ICP
10
26
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10
11 446 mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-43-9 Cd by ICPMS
0.50
0.50 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
7440-47-3 Cr by ICPMS
5.0
5.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
7440-50-8 Cu by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7439-89-6 Fe by ICP
50
610
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-09-7 K by ICP
0.10
15A0 mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7439-95-4 Mg by ICP
0.10
44 o d
mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7439-96-5 Mn by ICP
10
30
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-23-5 Na by ICP
0.10
8 6 mg/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-02-0 Ni by ICPMS
2.0
2.0 U
ug/L •
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
7439-92-1 Pb by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
7782-49-2 Se by ICPMS
1.0
1.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7440-24-6 Sr by ICPMS
10
39
ug/L
EPA 200.8 Rev5.4
1/5/18 ESTAFFORD1
7440-62-2 V by ICP
10
10 U
ug/L
EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-66-6 Zn by ICPMS
10
12 U
ug/L
EPA 200.8 Rev5.4 1/4/18 ESTAFFORDI
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
AC45661
,1:141.
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MBAS (surfactants) mg/L
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414IPBrdh!6t'efc�fa(✓)' +"itysl,;w #1, 7m it?ti-,
Tin (Sn) µg/L
Acidity, as CaCO3, to pH 4 5/8 3 mg/L
Oil and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L
Titanium (Ti) µg/L
Alkalinity, as CaCO3, to pH 4 5/8 3 mg/L
Phenols, Total Recoverable pg/L
• ntimony (Sb) pg/L
Vyanadiurh
(V) µg/L
BOD Biochemical Oxygen Demand, 5-day mg/L
Residue Total (Total Solids) mg/L
• senic (As) pg/L
V
Zinc (Zn) µg/L
cBOD Carbonaceous BOD, 5-day mg/L
Residue. Volatile/Fixed, Total mg/L
Barium (Ba) pg/L
Coliform Fecal MF /100m1
Residue Suspended (SuspendedSokds) mg/L
:eryllium (Be) pg/L
Boron (B),Total µg/L
r/Conform
Total MF /100m1
Residue Volatile/Fixed, Suspended mg/L
Cadmium (Cd) pg/L
Mercury 1631, low-level ng/L
Coliform Tube Fecal /100m1
TDS -Total Dissolved Solids mg/L
t/
alcium (Ca) mg/L
Conform Tube Total /100m1
Silica mg/L
Chromium (Cr), Total pg/L
al,
diganit p„dia'diet¢js`ji'rt ,"f( ptu;a, L9'.,/
Specific Conductance, at 25 °C umhos/cm
Sulfide mg/L
.
Cobalt (Co) pg/L
Acid Herbicides
TOC - Total Organic Carbon mg/L
Tannin & Lignin mg/L
Copper (Cu) pg/L
Organochlorine Pesticides
Turbidity NTU
on (Fe) pg/L
Organonitrogen Pesticides
:r',
aallirakifS:(IuS;.' 1114•111',�°,c',il.I"'„ 'MitillI, tP 'f
Lead (Pb) pg/L
Organophosphorus Pesticides
601410
01.f f%1l rya ..ggti ° eegiAl.{llgi
PH s u
Lithium (Li) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Z/
Magnesium (Mg) mg/L
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAs)
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
Sulfate mg/L
10.
ai i 44 10, % IJ " 4fJ t U'+ i ;{ay, Y
Molybdenum (Mo) pg/L
Chlorophyll a pg/L
Vt
mmonia as N (NH3-N) mg/L
ickel (Ni) ug/L
Volatile Organics (VOA)
Color ADMI c u
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
Potassium (K) mg/L
Color Platinum Cobalt c u
Total Kjeldahl Nitrogen as N (TKN) mg/L
r,
Selenium (Se) pg/L
TPH Gasoline Range
COD Chemical oxygen Demand mg/L
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
Cyanide, Total mg/L
Nitrite as N (NO2-N) mg/L
tr.
Sodium (Na) mg/L
'(
01bldg( jr;((t" 0rBfi "t'fi VM-TO
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton / Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS .
to"
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Revision 2/06/2015

AC4 4. 0
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
SIXRUN{a�HWY241UP)= •
Sampson Collector:
FRO
CPR
K WHITE
Report To FRO
Collect Date: 01/29/2018
r Collect Time: 12 5
Sample Depth 0_6
VisitlD
Location ID: 6P082WQ0004268
Priority ROUTINE
Sample Matrix:S RU FACEWATER)
Loc. Type: River/Stream
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC47310
01/30/2018
08_15
MSWIFT
NC Courier
3122/18
03/22/2018
CAS # Analyte Name.
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
2.4
Units
°C
Method
Reference
Analysis
Date ' Validated by
1/30/18 PGAUTHIER
NH3 as N in liquid
0.02
NUT
0.02 U
mg/L as N
EPA 350.1 REV 2 2/9/18
CGREEN
NO2+NO3 as N in liquid
0.02
0.08
mg/Las N
EPA 353.2 REV 2 2/9/18
CGREEN
Phosphorus_total as P. in liquid
0.02
0.08
mg/Las P
EPA 365.1 REV 2 2/6/18
CGREEN
Total Kjeldahl N. as N in liquid
0.2
0.63 r
mg/Las N
EPA 351.2 REV 2 2/2/18
CGREEN
Bromide
0.4
WET
0.4 U
mg/L
EPA 300.0 rev2.1
2/1/18
CGREEN
Chloride
1.0
20
mg/L
EPA 300.0 rev2.1
2/1/18
CGREEN
Fluoride
0.4
0.4 U
mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
Sulfate
2.0
12
mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
7429-90-5 Al by ICP
50
MET
95
ug/L
EPA 200.7 Rev4.4
2/9/18 ESTAFFORD1
7440-38-3 Ba by ICP
10
25
ug/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10
9.7
mg/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-50-8 Cu by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4 2/26/18 ESTAFFORD1
7439-89-6 Fe by ICP
50
650
ug/L
- EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-09-7 K by ICP
0.10
11
mg/L
EPA200.7 Rev4.4 2/9/18 ESTAFFORD1
7439-95-4 Mg by ICP
0.10
3.7
mg/L
EPA 200.7 Rev4.4
2/9/18 ESTAFFORD1
7439-96-5 Mn by ICP•
10
20
ug/L
EPA200.7,Rev4.4 2/9/18 ESTAFFORD1
7440-02-0 Ni by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 2/26/18 ESTAFFORD1
7440-24-6 Sr by ICPMS
10
35
ug/L
EPA 200.8 Rev5.4 2/16/18 ESTAFFORD1
7440-66-6 Zn by ICPMS
10
10 U
ug/L
EPA 200.8 Rev5.4 2/26/18 ESTAFFORD1
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Caroh a Division of Water Resources
Water Sample Collection & Submittal Form
Central Laboratory(Water Sciences Section
r
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Acidity, as CaCO3, to pH 4.5/8.3 mg/L
011 and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) ` , pg/L
Titanium (Ti) pg/L
Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L
Phenols; Total Recoverable pg/L
Antimony (Sb) pg/L
Vanadium (V) pg/L
BOD: Biochemical Oxygen Demand, 5-day mg/L
Residue:. Total (Total Solids) i mg/L
Arsenic (As) pg/L
X
Zinc (Zn) pg/L
cBOD: Carbonaceous BOD, 5-day mg/L
Residue: Volatile/Fixed, Total mg/L
X
Barium (Ba) pg/L
Coliform: Fecal MF /100m1
Residue: Suspended (Suspended Solids) mg/L
Beryllium (Be) pg/L
Boron (B), Total pg/L
Coliform: Total MF /100m1
Residue: Volatile/Fixed, Suspended mg/L •
Cadmium (Cd) )lg/L
Mercury 1631, low-level ng/L
Coliform: Tube Fecal /100m1
TDS -Total Dissolved Solids mg/L
X
Calcium (Ca) mg/L
-
Coliform: Tube Total _ /100m1
Silica .. mg/L
Chromium (Cr), Total pg/L
Mg
Li ,i p ' s fL ;: a i
Specific Conductance, at 25 °C _, umhos/cm
Sulfide mg/L
Cobalt (Co) -- ug/L
Acid Herbicides -
TOC -Total Organic Carbon mg/L
Tannin & Llgnln mg/L
X
Copper (Cu) pg/L
organochlorine Pesticides
Turbldity ' NTU
X-
Iron (Fe) IJg/L
Organonitrogen Pesticides
,jags
d,i,L( .4; T aU.rJ'J.; 1 If i ;,, ilMett
Lead (Pb) pg/L
Organophosphorus Pesticides •
°
pH ) s.u.
Lithium Li ( ) Ug/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Magnesium (Mg) mg/L
X.
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAs)
Fluoride mg/L
-
Mercury (Hg) pg/L
TPH Diesel Range
'A,
Sulfate mg/L
z...4
?OD.; J; --- ;. 1 _
Molybdenum (Mo) pg/L
Chlorophyll a - Ng/L.
Ammonia as N (NH3-N) • mg/L
X
Nickel (Ni) . pg/L
Volatile Organics' (VOA)
Color: ADMI _ - c.u. .
(
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
X
Potassium (K) mg/L
Color: Platinum Cobalt c.u.
)r
Total Kjeldahl Nittrogen as N (TKN) mg/L
Selenium (Se) - pg/L
TPH Gasoline Range'
COD: Chemical oxygen Demand mg/L
X
Total Phosphorus as P (TP) mg/L
Silver (Ag) - fig/L
Cyanide, Total ' mg/L
Nitrite as N (NO2-N) mg/L
Sodium (Na) mg/L
jl.��hr'�
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
X
:Strontium (Sr) pg/L
Phytoplankton /Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) • pg/L
LAB COMMENTS :
14-9.5
pINt
Revision: 2/06/2015

A'47311
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
=SIX RUN (aTROWANRD ib01
Sampson Collector: K WHITE
FRO Report To FRO
CPR Collect Date: T01/29/2018.1
i, CollebNine: 14_15)
Sample Depth 0.5
VisitlD
Location ID:
Priority
Sample Matrix:
Loc. Type:
Final Report
6P082WQ0004268
ROUTINE
SURFACEWATER
River/Stream
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC47311
01/30/2018
08_15
MSWIFT
NC Courier
3/22/18
03/22/2018
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Analysis
CAS # Analvte Name PQL Date
Sample temperature at receipt by lab
Result/
Qualifier
- LAB
2.4
Units
'C
Method
Reference
Validated b
1/30/18 PGAUTHIER
NH3 as N in liquid
0.02
NUT
0.03
mg/Las N'
EPA 350.1 REV 2 2/9/18
CGREEN
NO2+NO3 as N in liquid 0.02
0.30
mg/L as N
EPA 353.2 REV 2 2/9/18
CGREEN
Phosphorus_total as P in liquid 0.02
0.12
mg/Las P
EPA 365.1 REV 2 2/6/18
CGREEN
Total Kjeldahl N as N in liquid
0:2(
0.79
mg/L as N
EPA 351.2 REV 2 2/2/18
CGREEN
Bromide
0.4
WET
0.4 U
mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
Chloride
1.0
19
mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
Fluoride
0.4
0.4 U
mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
Sulfate
2.0
13 mg/L
EPA 300.0 rev2.1 2/1/18
CGREEN
7429-90-5 Al by ICP
50
MET
560
ug/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-38-3 Ba by ICP
10
26
• ug/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10 \, 9.5
mg/L
EPA 200.7 Rev4.4
2/9/18 ESTAFFORD1
7440-50-8 Cu by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 2/26/18 ESTAFFORD1
7439-89-6 Fe by ICP
50
910
ug/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORD1
7440-09-7 K by ICP
0.10
9.9
mg/L
EPA 200.7 Rev4.4 2/9/18 ESTAFFORDI
7439-95-4' Mg by ICP
0.10
3.5
mg/L
EPA200.7 Rev4.4 2/9/18 ESTAFFORD1
7439-96-5 Mn by ICP
10-
32
ug/L
EPA 200.7 Rev4.4
2/9/18 ESTAFFORDI
7440-02-0 Ni by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 2/26/18 ESTAFFORDI
7440-24-6 Sr by ICPMS
10
34
ug/L
EPA 200.8 Rev5.4 2/16/18 ESTAFFORDI
7440-66-6 Zn by ICPMS
10
10 U
ug/L
EPA 200.8 Rev5.4 2/26/18 ESTAFFORD1
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

s1
North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
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Notes:
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it 'W t
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tf YJ°U' ^°y
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A.f?,'
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r
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Dissolved analysis: Enter"DIS
❑ Filtered in Field
in check -boxes for parameters
4 5 ® '
rJ ,
�" r� e:;` `
e:Civ !
aOr 6e- 1)�/
lal
.r.„. • ,6::t., i a.Ab (P!,Ni[, aP0`ita
MBAS(surfactants). mg/L
g • ii•Ppi
Tin (Sn) pg/L
Acidity, as CaCO3, to pH 4.5/8.3 mg/L
011 and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L
Titanium (Ti) pg/L
Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L
Phenols, Total Recoverable pg/L
Antimony (Sb) ' pg/L
Vanadium (V) pg/L
BOD: Biochemical Oxygen Demand, 5-day mg/L
Residue: Total (Total Solids) mg/L
Arsenic (As) • pg/L
A
Zinc (Zn) pg/L
cBOD: Carbonaceous BOD, 5-day mg/L
Residue: Volatile/Fixed, Total mg/L
(
Barium (Be) pg/L
Coliform: Fecal MF /100m1
Residue: Suspended (Suspended Solids) mg/L
Beryllium (Be) (lg/L
Boron (B), Total pg/L
Coliform: Total MF /100m1
Residue: Volatile/Fixed, Suspended mg/L
Cadmium (Cd) pg/L
Mercury 1631, low-level ng/L
Collform: Tube Fecal /10om1
TDS -Total Dissolved Solids mg/L
`(
Calcium (Ca) mg/L
Coliform: Tube Total /100m1
Silica • mg/L
Chromium (Cr), Total - pg/L
yi5;.`/ja
:,-.1, , Atfietenatelft,nT
Add Herbicides
Specific Conductance, at 25 °C umhos/cm
Sulfide mg/L
Cobalt (Co) • Ug/L
TOC - Total Organic Carbon mg/L
Tannin & Lignin mg/L
X
Copper (Cu) pg/L
orgenochlorine Pesticides
TLirbidity • NTU
I
X
Iron (Fe) pg/L
Organonitrogen Pesticides
I :;;Nina
n, ti' -u� (�i 4��
Lead (Pb) pg/L
Organophosphorus Pesticides
°7',ti
.�7
iP :n1T.L Mli(°1 °ra<"ri)it ..1.at44•'i raima,'",}iZ:'.
pH s,u.
Lithium (LI) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
%
Magnesium (Mg) mg/L
Chloride mg/L
-
94
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAs)
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
X
Sulfate mg/L
,r1J:,a;
a7a:: tt)SP r.r°,."
Molybdenum (Mo) pg/L
Chlorophyll a pg/L.
'
Ammonia as N (NH3-N) • mg/L
iG
Nickel (Ni) pg/L
Volatile Organics (VOA)
Color: ADMI c.u.
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
)[
Potassium (K) mg/L
Color: Platinum Cobalt c.u.
X
Total Kjeldahl Nitrogen as N'(TKN) mg/L
Selenium (Se) pg/L
TPH Gasoline Range.
COD: Chemical. Oxygen Demand mg/L
Total Phosphorus as P (TP) mg/L
Silver.(Ag) pg/L
Cyanide, Total mg/L
Nitrite as N (NO2-N) mg/L
Sodium (Na) mg/L
,11,*,,
(; • „w ? 14],,g,, ,(,'l1'4i? I'rx;1r n; xr
Phytopiankton / Algae
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
)(
Strontium (Sr) pg/L
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS :
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Revision: 2/06/2015

AC47308
Loc. Descr.: CANAL
County: am son
Region: FRO
River Basin CP13
Emergency
COC YeslNo
North Carolina. Division of Water Resources Water Sciences Section Laboratory Results
Collector: K WHITE
Report To FRO
ColleciDat� e: " 01/2972018
Collect Time: 14`00j
Sample Depth 0_5
VlsitID
Location ID: 6P082W00004268
Priority ROUTINE
Sample Matrix: SURFACEWATER
lion c. Type: River/Stream
CAVA'
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC47308`
01/30/2018
08;15
MSWIFT
NC Courier
2/16118
02/16/2018
CAS # Analvte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
2.4
Units
Method
Reference
Analysis
Date Validated by
1/30/18 PGAUTHIER
t NF3as YNlin;ligyid
NO2+1103 iCN.inaiguidd
NUT
0.02
mg/L as N
0.02 2J . mg/Las N
EPA 350.1 REV 2 '2/9/18
EPA 353.2 REV 2 2/9/18
CGREEN
CGREEN
Phosphorus total as P in liquid
0.02
0.10
mg/Las P
EPA 365.1 REV 2 2/6/18
CGREEN
`Tgf'ahKJeldahL_N'as;N^,in_liquid,�
Bromide
0.2
1 f2.)
mg/L as N
EPA 351.2 REV 2 2/2/18
CGREEN
WET
0.4 0.4 U mg/L
EPA 300.0 rev2.1
2/1/18
CGREEN
Chloride
1.0
100
mg/L
EPA 300.0 rev2.1
2/1/18
CGREEN
Fluoride
0.4 0.4 U mg/L
EPA 300.0 rev2.1
2/1/18
CGREEN
Sulfate
2.0 18 mg/L
EPA 300.0 rev2.1
'2/1/18
CGREEN
WSS Chemistry Laboratory» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample Is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
0-0
Notes.
❑ Chlorinated ❑De-chlonnated in Field
Dissolved analysis Enter"DIS"
❑ Filtered in Field
, In check -boxes for parameters
Water Sample Collection & Submittal Form
IL•�IT
Zy SA-;‘) 2018 -
rab [Composite
Other
0,5'
❑Amblent
Routine
❑Compliance
❑ COC
•
['Emergency
❑DA
&Pon wttoco+-Us1s
111. River/Stream Dlake
Surface • Estuary ['Canal
❑Stormwater
❑ Ground ❑Monitonng Well ❑Water Supply
['Waste ❑Effluent :Influent
❑ Blank 9;::r:
❑Trip Blank
nk
OSolution ❑Other
(2 Ow EVCAir
741;?��e
Acidity, as CaCO3, to pH 4 5/8 3 mg/L
Alkalinity, as CaCO3, to pH 4 5/8 3 mg/L
BOD Biochemical oxygen oemand,5-day mg/L
cB00 Carbonaceous BOD, 5-day
Cohform Fecal MF
Cohform Total MF
Cohform Tube Fecal
Cohform Tube Total
mg/L
/100m1
/100m1
/loomI
/100m1 1
Specific Conductance, at 25 °C umhos/cm.
TOC - Total Organic Carbon
Turbldity
mg/L
NTU
Nv'r .(/-1'122.6D
MBAS (surfactants)
011 and Grease, HEM, Total Recoverable
Phenols, Total Recoverable
Residue Total (Total Saris)
Residue Volatile/Fixed, Total
Residue Suspended (Suspended Solids)
Residue Volatile/Fixed, Suspended
TDS -Total Dissolved Solids
Silica
Sulfide
Tannin & Lignin
,v,,WW
Ate
x
Bromide
Chloride
Fluoride
Sulfate
Chlorophyll a
Color ADMI
mg/L
mg/L
mg/L
mg/L
pg/L
cu
mg/L
mg/L
pg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
me/L
mg/L
su
orsanordwavatteste
Aluminum (Al)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Calcium (Ca)
Chromium (Cr), Total
Cobalt (Co)
Copper (Cu)
Iron (Pe)
Lead (Pb)
Ng/L
pg/L
pg/L
pg/L
pg/L
pg/L
mg/L
pg/L
µg/L
pg/L
pg/L
pg/L
Tin (Sn)
Titanium (Ti)
Vanadium (V)
Zinc (Zn)
Boron (8), Total
Mercury 1631, low-level
iinEWN
Acid Herbicides
Organochlonne Pesticides
Organonitrogen Pesticides
Organophosphorus Pesticides
pg/L
µg/L
pg/L
pg/L
pg/L
ng/L
Lithium (LI)
pg/L
PCBs (polychlonnated biphenyls)
Magnesium (Mg)
Manganese (Mn)
Mercury (Hg)
Molybdenum (MO
mg/L
pg/L
pg/L
pg/L
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TPH Diesel Range
X_-
Color Platinum Cobalt
COD Chemical Oxygen Demand
Cyanide, Total
Formaldehyde
cu
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mg/L
Hexavalent Chromium (Cr6+)
LAB COMMENTS t
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mg/L
Ammonia as N (NH3-N)
1 Total Kjeldahl Nitrogen as N (TKN) mg/L
mg/L
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
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Nitrate as N (NO2-N)
Nitrate as N (NO3-N calculated)
Orthophosphate as.P (PO4)
Nickel (Ni)
Potassium (K)
PBX
mg/L
mg/L
mg/L
mg/L
mg/L
Selenium (Se)
Silver(Ag)
Sodium (Na)
Strontium (Sr)
Thallium (TI) _
pg/L
Volatile Organics (VOA)
pg/L
mg/L
pg/L
TPH Gasoline Range
pg/L
Phytoplankton / Algae
Revision 2/06/2015
9.3
4410.7.
N41
pH
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North Carolina Division of Water Resources
Water Sample Collection & Submittal Form
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.
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IColor:Total
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Silver (Ag) µei-
Cyanide, Total mg/L
Nitrite as N (NO2-N) mg/L
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Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton / Algae
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS :
U4�Azr�r�'i•L�iU'�t'
Revision: 2/06/2015
9.3
/v/11

North Carolina Division of Water Resources'
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
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,
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Boron (B), Total pg/L
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Cadmium (Cd) pg/L,.
Mercury 1631, low-level ng/L
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Magnesium (Mg) .4 .-- hg/L
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Hexavalent Chromium (Cr6+) mg/L
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Thallium (TI) j": - + r Ng/L '
-- _
LAB COMMENTS :
Revision: 2/06/2015
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Aluminum (Al) pg/L
Titanium (Ti) pg/L
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Vanadium (V) pg/L
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Semi -Volatile Organics (BNAs)
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)}rt:•.:''
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•
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t/
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Potassium (K) , mg/L
..
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TPH Gasoline Range
• • • • , . -
,
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Silver (Ag) ' ' pg/L
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Ig.
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Strontium (Sr) pg/L
Phytoplankton / Algae
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) ( mg/L
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) Ng/L
'
LAB COMMENTS :
Revision: 2/06/2015

FIELD DATA FORM W6tooa42128
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07/20.15

Barber, Jim
From: Barber, Jim
Sent Wednesday, December 13,.2017 4:07 PIVI
To: 'Elkin, Dave'; Kraig Westerbeek ([e-mail])
Cc: Allen, Trent; White, Kenneth B
Subject RE: [External] FW: Elliot Site.121317
Attachments:. PZ 1 16 Nov 2017 sample data and well schematic.pdf Field data PZ 1 & surface water
and maps. with MW1&MW2 charts.pdf; Former Del Monte MB LLC plant site MWs & PZ
1 jpg; ORC'& BU. ORC designation form.pdf . -
Dave Elkin;
Attached are several. documents for field visits made recently to the former Sager Creek/Del Monte site. A well
schematic for PZ-1 and lab datafrom the sample taken on 16 November2017 is also provided. Hopefully after the first.
of the year we will have the second sample result for PZ-1 taken on 4 Dec. 2017. I don't think we'Il see much of a change.
in the water quality of the second sample since the field parameters from 16 Nov. (watersample in bottle) and the field
parameters directly taken from the well are similar:. I've also:providedsome historical data from our database for MW-1
and MW-2.
Based on the information from field measurements at PZ-1-on 16 Nov. and 4 Dec.; it appears that if you construct a
surface water cut-off ditch to a depth,of 5' or less.below ground surface you willcapture surface water and probably
won't get an appreciable; amount of shallow groundwater. The depths to shallow groundwater belowground surface at
PZ-1 were 6.30' and 6.20' on 17 Nov. and 4 Dec. Unless we have above normal rainfall during the winter and early
spring, I wouldn't think that the seasonal high water table at PZ-1 would rise more than a foot (again,. based on normal
winter rainfall). I placed a note on.the worksheets we used in the field that soil mottling occurred around 5'_ below grade
at PZ-1 (indicative of historical seasonal high water table) and we advanced the borehole approximately 3' beyond the
mottled soil horizon:
I've also attached the webpage example and a copy of the ORC and Back. Up ORC designation forms that need to be
executed (if not already) to designate who/whom will be the new .ORC and ;BU ORC for MB LLC.
I will be out of the office starting 14 Dec. 2017 and will return on 3 Jan. 2018. If you have any questions or need
additionalassistance, give Kent White a call at 910-433-3338 orTrent.Allen at901-433-3336:
Jim Barber
Environmental Engineer
NCDEQ-DWR-WQRO
Fayetteville Regional Office
910-433-3340 voice`
910-486-0707 fax
iim.barber at ncdenr.gov
E-mail correspondence to and from this address may be`subject to the North Carolina Public Records Law and
may. be disclosed to third parties.
A Go Green! Print this email only when necessary. Thank you for helping.NCDENR be environmentally responsible.
1

AC44846 North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.:
County:
Region:
River Basin
Emergency
COC Yes/No
x-MBLLrcTb I: O
amoson
FRO
CPR
YES
Collector:,
Report To
Collect Date:
Collect Time:
Sample Depth
J BARBER
FRO
11/16/2017
13:45
VisitlD
Location ID:-6P082WQ0004268
Priority EMERGENCY
Sample Matrix: �GROUNDWATEJ
Loc. Type: WATER SUPPLY
Final Report62.16).
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC44846
11/17/2017
08_45
MSWIFT
NC Courier
11/29/17
11/29/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Method
CAS # Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
1.0
Units
°C
Reference
Analysis
Date
Validated by
11/17/17 PGAUTI-IIER
NH3 as N in liquid
0.02
NUT
6.3
mg/L as N
EPA 350.1 REV 2 11/20/17 CGREEN-
NO2+NO3 as N in liquid
-0.02
0:02�U
mg/L as N
EPA 353.2 REV 2 11/20/17 CGREEN
Phosphorus total as P in liquid
0.02
0.02 U
mg/L as P
EPA 365.1 REV 2 „ 11/20/17 CGREEN
Total Kjeldahl N as N in liquid
0.2
�s•:`si
mg/L as N
EPA 351.2 REV 2 11/21/17 CGREEN
Bromide.
1J5 0.4
WET
0.91
mg/L
EPA 300.0 rev2.1
11/17/17 CGREEN
Chloride
.2S0
1.0
12
Fluoride
0.4
0.4 U
mg/L
mg/L
EPA 300.0 rev2.1
11/17/17 CGREEN
EPA 300.0, rev2.1
11/17/17 CGREEN
S;uffatej
S0
2.0
tie
mg/L
EPA 300.0 rev2.1
11/17/17 CGREEN
7429-90-5 Al by ICP
/a5
50
MET '
2400
ug/L
EPA 200.7 Rev4.4 11/27/17 ESTAFFORDI
7440-38-2 As by ICPMS
/0
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 11/28/17 ESTAFFORD1
7440-38-3 Ba by ICP
700
10
69
ug/L
EPA 200.7 Rev4.4 11/28/17 ESTAFFORDI
7440-70-2 Ca by ICP
N5
0.10
1.7
mg/L
EPA 200.7 Rev4.4 11/28/17 ESTAFFORDI
7440-43-9 Cd by ICPMS
2
0.50
0.50 U
ug/L
EPA 200:8 Rev5.4 11/28/17 ESTAFFORDI
7440-47-3 Cr by ICPMS
/0
5.0
5.0 U
ug/L
EPA 200.8 Rev5.4 - 11/28/17 ESTAFFORD1
7440-50-8 Cu by ICPMS
/000
2.0
6.5 -
ug/L
EPA 200.8 Rev5.4 11/28/17 ESTAFFORDI
7439-89-6 Fe by ICP
300
50
:5400`
ug/L
EPA 200.7 Rev4.4 11/27/17 ESTAFFORD1
7440-09-7 K by ICP
N5
0.10
17
mg/L
EPA 200.7 Rev4.4 11/28/17 ESTAFFORDI
7439 95-4 Mg by ICP
NS
0.10
1.6
mg/L
( EPA200.7 Rev4.4 11/28/17 ESTAFFORDI
7439-96-5 Mn by ICP
So
,10
ug/L
EPA 200.7 Rev4.4 11/27/17 ESTAFFORDI
7440-23-5 Na by ICP
7440-02-0 Ni by ICPMS
1QS
/00
0.10 , reij
2.0
3.9
mg/L ,
ug/L
EPA 200.7 Rev4.4 11/28/17 ESTAFFORDI
EPA 200.8 Rev5.4 11/28/17 ESTAFFORDI
7439-92-1
Pb by ICPMS
/5-
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4 11/28/17 ESTAFFORDI
7782-49-2 Se by ICPMS
7440-24-6 Sr by ICPMS
aO
1.0
1.0 U
ug/L
EPA 200.8 Rev5.4 11/28/17 ESTAFFORDI
AI5
10
12
ug/L
EPA 200.8 Rev5.4
11/28/17 ESTAFFORDI
7440-62-2 V by ICP
Ars
10 -
10 U
ug/L
EPA200.7 Rev4.4 11/27/17 ESTAFFORDI -
7440-66-6 Zn by ICPMS
/000
10
84
ug/L
EPA 200.8 Rev5.4 11/28/17 ESTAFFORD1
N'5 = No Z L. 5T APNt=1 Z�
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

Monitoring Well Schematic, Submerged Screen _
WeII ID P�--
Date /G' itlov. .2017 1
Project Name ())a �� C /5Acrs1L CREEIc/DEL (y1 o,t�TE C u/� 00d Liz 4 8
Project Location C G/,u TOL') -5AM P.501) CO U417
Hieght of Casing
Depth to Top of
Gravel Pack
Depth to Top of
Screen
$.io"
Depth to Bottom of
Well Casing
y.
/, GO
l9.1 771rE41UEPVC.
Grout 3,g u 0 136.tfTei!/M Atc_
Screen / t1' X 0. 0/0 "$t.tT Pvc_
2,50/
Gravel Pack ,J0, / P 5AND
Screen
or 70 SC446

AC45659
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.: MBLLCDELMONTE
County: SAMPSON Collector: K WHITE
Region: FRO Report To FRO
River Basin CFR Collect Date; - 12/0412017
Emergency Collect Time:-"13_25
COC Yes/No Sample Depth
VlsitID
Location ID:
Priority ROUTINE
:Sample Matrix: �GRUUNDWATE�
Loc. Type: WATER SUPPLY
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
6P082WQ0004268
Sample ID: AC45659
PO Number #
Date Received: 12/0512017
Time Received: 08,_15
Labworks LoginID MSWIFT
Delivery Method NC Courier
Final Report Date: 1/24/18
Report Print Date: 01/24/2018
CAS # Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
2.4
Units
'C
Method
Reference
Analysis
Date Validated by
12/5/17 PGAUTHIER
E ,.NH•3_as: N in ligiiid
cT10+NO3T670:N=in liquid3
NUT
0.02
mg/Las N EPA 350.1 REV 2 12/7/17 CGREEN
0.02 0:021J mg/Las N EPA 353.2 REV 2 12/12/17 CGREEN
Phosphorus_total as P in liquid
0.02 0.02 U mg/L as P EPA 365.1 REV 2 12/13/17 CGREEN
Total Kjeldahl"N_as Nsn;llquitlj
0.2
mg/Las N EPA 351.2 REV 2 12/8/17 CGREEN
7429-90-5 Al by ICP
50
MET
2000
ug/L EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-38-2 As by ICPMS
2.0
7440-38-3 Ba by ICP
2.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
10 52 ug/L EPA200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-70-2 Ca by ICP
0.10
0.93
mg/L EPA 200.7 Rev4.4 1/12/18 ESTAFFORDI
7440-43-9 Cd by ICPMS
0.50
0.50 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
7440-47-3 Cr by ICPMS
5.0 5.0 U ug/L EPA200.8 Rev5.4 1/4/18 ESTAFFORDI
7440-50-8 Cu by ICPMS
2.0
5.3
ug/L EPA 200.8 Rev5.4 1/4/18 ESTAFFORDI
7439-89-6 Fe by ICP
50 4800 ug/L EPA200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-09-7 K by ICP
0.10 17 mg/L EPA200.7 Rev4.4 1/12/18 ESTAFFORDI
7439-95-4 Mg by ICP
0.10 1.3 mg/L EPA200.7 Rev4.4 1/12/18 ESTAFFORD1
7439-96-5 Mn by ICP
10
45
ug/L EPA200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-23-5 Na by ICP
0.10 83 mg/L EPA200.7 Rev4.4 1/19/18 ESTAFFORDI
7440-02-0 Ni by ICPMS
2.0
3.4
ug/L EPA 200.8 Rev5.4 1/4/18 ESTAFFORDI
7439-92-1 Pb by ICPMS
2.0
2.0 U
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORDI
7782-49-2 Se by ICPMS
7440-24-6 Sr by ICPMS
1.0 1.0 U ug/L EPA200.8 Rev5.4 1/4/18 ESTAFFORDI
10
10U
ug/L
EPA 200.8 Rev5.4
1/5/18 ESTAFFORD1
7440-62-2 V by ICP
10
10 U
ugfL EPA 200.7 Rev4.4 1/12/18 ESTAFFORD1
7440-66-6 Zn by ICPMS
10
88
ug/L
EPA 200.8 Rev5.4
1/4/18 ESTAFFORD1
WSS Chemistry Laboratory» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample Is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
AC45659
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f c L0k%`
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MBAs (surfactants) mg/L
t 11'.
flw^r4.s'vF Y
i ' ;, MIZait : r.`fi' ie ,xa -zs.5r ATZ
Tin (Sn) pg/L
Acidity, as CaCO3, to pH 4 5/8 3 . mg/L
-
Oil and Grease, HEM, Total Recoverable mg/L
4
Aluminum (Al) pg/L -
Titanium (Ti) NA
Alkalinity, as CaCO3, to pH 4 5/8 3 mg/L
Phenols, Total Recoverable pg/L
Antimony (Sb) pg/L
anadlum (V) pg/L
BOD Biochemical Oxygen Demand, 5-day mg/L
-
Residue Total (TotalSolyds) mg/L
4
Arsenic (As) pg/L
4
Zinc (Zn) - pg/L
cBOD Carbonaceous BOD, 5-day mg/L
-
Residue' Volatile/Fixed, Total mg/L
4
Barium (Ba) - pg/L
Conform Fecal MF /100m1
Residue Suspended (SuspendedSohds) mg/L
Beryllium (Be) pg/L
Boron (B),Total pg/L
Coliform Total MF /100m1
-
Residue Volatile/Fixed, Suspended mg/L
J
admium (Cd) pg/L
Mercury 1631, low-level ng/L
Conform Tube Fecal /100m1
-
TDS -Total Dissolved Solids mg/L
4.
alcium (Ca) mg/L
'Conform Tube Total /100m1
-
Silica mg/L
A
Chromium (Cr), Total pg/l-
= :,'j
ry,�,
�y �r 2 `Wi <t
Specific Conductance, at 25 °C umhos/cm
-
Sulfide mg/L
Cobalt (Co) pg/L
Acid Herbicides
TOC- TotalOrganicCarbon mg/L
-
Tannin & Lignin mg/L
,A
copper (Cu) pg/L
OrganochlormePesticides
Turbidity NTU
J
ron (Fe) pg/L
Organonitrogen Pesticides
lTMEMyEF
EVMMyri�+'N,0"'
�
Lead (Pb) pg/L
Organophosphorus Pesticides
,' +
t+�;��y
Y 1• IE rr y+rrr �rrZ• tali,, ,�i FI4?S +^ ''�`C"F (. •;(
j3;��,:'i � l,uaS.�.k��,<<�h�.9�.° (,i)�,iKf�?1,'i>;;,;,
-
pH s u
Lithium (Li) pg/L
)
PCBs of chlorinated bi hen Is
(polychlorinated P y )
Bromide mg/L
-
Hardness, Total asCaCO3-by titration mg/L
Magnesium (Mg) 'mg/L
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAs)
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
Sulfate mg/L
TI StT .
�;i��'n�4t���!�5:;��:,�
A1; ,.,.�.' I T i R-fIY,M' uL'v� YSfjj'Y�
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Molybdenum (Mo) pg/L
Chlorophyll a pg/L
n/
mmonia as N (NH3-N) mg/L
d
ickel (Ni) pg/L
Volatile Organics (VOA)
Color ADM1 c u
IMAI
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
'otassium (K) mg/L
Color Platinum Cobalt c u
-
Total Kleldahl Nitrogen as N (TKN) mg/L
4
Selenium (Se) pg/L
TPH Gasoline Range
COD Chemical Oxygen Demand mg/L
trA
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
-.
Cyanide, Total mg/L
-
Nitrite as N (NO2-N) mg/L
:. dium (Na) mg/L
%
; 1.:...i{t ,y" tl WP: 1.
Formaldehyde mg/L
-
Nitrate as N (NO3-N calculated) mg/L
4
Strontium (Sr) pg/L
Phytoplankton /Algae
Hexavalent Chromium (Cr6+) mg/L
-
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS •
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Revision 2/06/2015

-
AC46585
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.: DIVERSION CANALISAGER CREEK
County: Sampson Collector: K WHITB
Region: FRO Report To
River Basin CPF "'Collect=oate:- u-'01112/2018
Emergency .`CollecfTiine: T12:00
COC Yes/No Sample Depth
VlsitID
Location ID: FRO NLC
Priority ROUTINE
Sample Matrix: SURFACEWATER
)- yTYPe:- al'
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Method Analysis
CAS # Analvte Name PQL Qualifier Units Reference Date Validated by
LAB
1/17/18 PGAUTHIER
Sample ID: AC46585
PO Number #
Date Received: 01/17/2018
Time Received: 08_30
Labworks LoginlD MSWIFT
Delivery Method NC Courier
Final Report Date: 1/31/18
Report Print Date: 01/31/2018
Sample temperature at receipt by lab
1.3
"C
Bromide
0.4
WET
0:62
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
Chloride
1,0'
130
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
Fluoride
0.4 0.4 U mg/L
EPA300.0 rev2.1 1/25/18 CGREEN
Sulfate
2.0
14
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
WSS Chemistry Laboratory» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample Is analyte free but that the analyte Is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection az Submittal Form i
Dx
t»•.:r wars �,
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in check -boxes tor parameters
4. t1'�' -
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Tin (Sn)
A
Acidity, as CaCO3, to pH 4 5/8.3 mg/L
Oil and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L
pg/L
Titanium (Ti)
A
Alkalinity, as CaCO3, to pH 4 5/8 3 mg/L
Phenols, Total Recoverable pg/L
Antimony (Sb) pg/L
pg/L
Vanadium (V)
B
BOD Biochemical Oxygen Demand, 5-day mg/L
Residue Total (Total Solids) mg/L
Arsenic (As) pg/L
pg/L
Zinc (Zn)
cBOD Carbonaceous BOD, 5-day mg/L
Residue. Volatile/Fixed, Total mg/L
Barium (Ba) pg/L
pg/L
C
Coliform Fecal MF /100m1
Residue. Suspended (Suspended Solids) mg/L
Beryllium (Be) pg/L
Boron (B), Total
Coliform Total MF /10om1
Residue Volatile/Fixed, Suspended mg/L
Cadmium (Cd) pg/L
pg/L
Mercury 1631, low-level ng/L
Coliform Tube Fecal /100m1
TDS -Total Dissolved Solids mg/L
Calcium (Ca) mg/L
Coliform Tube Total /100m1
Silica mg/L
Chromium (Cr), Total pg/L
Qrkiikli Fdtartf et6;3t •d y > ;..5
Specific Conductance, at 25 °C umhos/cm
Sulfide mg/L
Cobalt (Co) pg/L
Acid Herbicides
T
TOC-Total Organic Carbon mg/L
Tannin & LIgnln mg/L
Copper (Cu) pg/L
Organochlorine Pesticides
Turbidity NTU
Iron (Fe) pg/L
Organonitrogen Pesticides
r
�p3bli'M�ttigrAK
AriV-'a.`'S: s.-i '.,SA, t '�:'%r°
Lead (Pb) pg/L
Organophosphorus Pesticides
a'1��` iN.e . ie ktf; 'it'bedr ate1k`f4 ", Nq« A.
pH s u.
Lithium (Li) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Magnesium (Mg) mg/L
'S
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile Organics (BNAs)
F
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
l'
Sulfate mg/L
NAtk(ft
eift era itti S ,S0c t; q ;rVt "(, w;gs a
Molybdenum (Mo) pg/L
C
Chlorophyll a pg/L
Ammonia as N (NH3-N) mg/L
Nickel (NI) pg/L
Volatile Organics (VOA)
C
Color ADMI c u
Nitrate -Nitrite as N (NO3+NOZ-N) mg/L
PotassnJm (K) mg/L
Color. Platinum Cobalt c u.
Total KJeldahl Nitrogen as N (TKN) mg/L
Selenium (Se) pg/L
TPH Gasoline Range
COD. Chemical Oxygen Demand - mg/L
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
C
Cyanide, Total mg/L
Nitrite as N (NO2-N) mg/L
Sodium (Na) mg/L
„ .,,;tBio'041
'�(;; '• 1;i„i,,t7 WVrt:I^ Jt
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton / Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (T1) pg/L
LAB COMMENTS .
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1

AC46586 North Carolina. Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.: DIVERSION CANAL/SAGER CREEK
County: Sampson Collector: JC WHITE VisitID
Region: ERQ Report To FRO Location ID: FRO NLC
jcT. cYtµ
River Basin CPF 1.35111edt Date: " Oil 2/2018 j Priority ROUTINE
Emergency Collect Time: 12_30 Sample Matrix: SURFACEWATER
COC Yes/No Sample Depth Loc. Type: [gag
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Sample ID: AC46586
PO Number #
Date Received: 01/17/2018
Time Received: 08_30
Labworks LoginlD MSWIFT
Delivery Method NC Courier
Final Report Date: 1/31/18
Report Print Date: 01/31/2018
Result/
CAS # Analyte Name PQL Qualifier
LAB
Sample temperature at receipt by lab
Units
1.3 °C
Method Analysis
Reference Date
1/17/18
Validated by
PGAUTHIER
NUT
mg/L as N EPA 350.1 REV 2 . 1/23/18 CGREEN
trNN3-as L1afiJiquid 0.02 Q 84;
NO2+NO3 as N Ir►ligtiid-J 0.021 2; ] mg/Las N EPA 353.2 REV 2 1/25/18 CGREEN
0.02 0.31 mg/L as P EPA 365.1 REV 2 1/26/18 CGREEN
Phosphorus_ total as P in liquid
Total K eld`ahl N as N m hguid J 0.2 E52:1J mg/Las N EPA 351.2 REV 2 1/23/18 CGREEN
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample Is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
2
095
4CA-,l4HL
AC46586
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Acidity, as CaCO3, to pH 4 5/8 3 mg/L
Oil and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L
Titanium (Ti) pg/L
Alkalinity, as CaCO3, to pH 45/8,3 mg/L
Phenols, Total Recoverable Ng/L
Antimony (Sb) pg/L
Vanadium (V) pg/L
BOD. Biochemical oxygen Demand,5-day mg/L
Residue Total (Total Solids) mg/L
Arsenic (As) pg/L
Zinc (Zn) pg/L
cBOD• Carbonaceous BOD, 5-day mg/L
Residue. Volatile/Fixed, Total mg/L
Barium (Ba) pg/L
Conform Fecal MF /100m1
Residue. Suspended (Suspended Solids) mg/L
Beryllium (Be) pg/L
Boron (B), Total pg/L
Cohform _Total MF /100m1
Residue Volatile/Fixed, Suspended mg/L
Cadmium (Cd) - pg/L
Mercury 1631, low-level ng/L
Conform. Tube Fecal /100m1
TDS -Total Dissolved Solids mg/L
Calcium (Ca) mg/L
Conform Tube Total /100m1
Silica mg/L
Chromium (Cr), Total pg/L
1 txr t)(etals ?tis k'°f"s •;-)st4
Specific Conductance, at25 °C umhos/cm
Sulfide mg/L
Cobalt (Co) _ pg/L
Acid Herbicides
TOC - Total Organic Carbon mg/L
Tannin & Lignin mg/L
Copper (Cu) pg/L
Organochlorine Pesticides
Turbidity NTU
I
Iron (Fe) pg/L
Organonitrogen Pesticides
tiiNAar3. '010/Peiaral" t
Lead (Pb) lig/L
Organophosphorus Pesticides
�ti,'v.";. If 6lrllagglFe)Ib Enid, .f 1« tetite03
pH s u
Lithium (Lc) - pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Magnesium (Mg) mg/L
Chloride mg/L
Manganese (Mn) pg/L
Semi -Volatile organics.(BNAs)
Fluonde mg/L
Mercury (Hg) pg/L
TPH Diesel Range
Sulfate mg/L
L i.,1,
e'`t
Molybdenumit (Mo)
Chlorophyll a pg/L
Ammonia as N (NH3-N) mg/L
Nickel (NI) pg/L
Volatile Organics (VOA)
Color ADMI c u
)(
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
PotassiUm (K) mg/L
Color Platinum Cobalt c.0
Total Kjeldahl Nitrogen as N (TKN) mg/L
Selenium (Se) pg/L�TPH
Gasoline Range
COD. Chemical oxygen Demand mg/L l
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
Cyanide, Total mg/L
Nitnte as N (NO2-N) mg/L
Sodium (Na) mg/L
, ,.,
CQto'j} gi;? L ekr ; '; i3,•;r'a` „d,. :i
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton / Algae
,
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) pg/L
LAB COMMENTS
evision

. k465e6 North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr DIVERSION+CANAL`ISAGER CEEK.
County: Sampson Collector: K WHITE VisitlD
Region: FRO Report To ' FRO Location ID: FRO NLC
River Basin CPF Collect Date: tto1/12/2018 Priority ROUTINE
Emergency Collect Time: 12:30 Sample Matrix: SURFACEWATER
CDC Yes/No Sample Depth Loc. Type: Canal
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Sample ID:, AC46586
PO Number #'
Date Received: 01/17/2018
Time Received: 08_30
Labworks LoginiD MSWIFT
Delivery Method = NC Courier
Final Report Date: 1/31/18
Report Print Date: 01/31/2018
Result/
CAS # Analyte Name PQL Qualifier
LAB
Sample temperature at receipt by lab 1.3
Units
-c
Method Analysis
Reference Date Validated by
1/17/18 PGAUTHIER
NH3 as N in liquid
NUT
0.02 0.84 mg/L as N EPA 350.1 REV 2 1/23/18 CGREEN
NO2+NO3 as N in liquid
0.02 :2' mg/Las N EPA 353.2 REV 2 1/25/18 CGREEN
Phosphorus total as P in liquid
0.02. 0.31 mg/L as P EPA 365.1 REV 2 1/26/18 CGREEN
Total Kjeldahl N as N in liquid-.
0.2 2.1 mg/L as N EPA 351.2 REV 2 1/23/18CGREEN
4
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC46585
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.:;DIVERSION.CANAL/SAGER CREEK
County: Sampson Collector:
Region: FRO
River Basin CPF
Emergency
COC Yes/No
K WHITE
Report To FRO
Collect Date: 4- '01/12/2018,
Collect Time: 12:00
Sample Depth
VisitlD
Location ID:
Priority
Sample Matrix:
Loc. Type:
Final Report
FRO NLC
ROUTINE
SURFACEWATER
Canal
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Delivery Method
Final Report Date:
Report Print Date:
AC46585
01/17/2018
08_30
MSWIFT
NC Courier
1/31/18
01/31/2018-
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
CAS # Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
LAB
1.3
Units
'C
Method Analysis
Reference Date Validated by
1/17/18 PGAUTHIER
Bromide
0.4
WET
0.62
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
Chloride
1.0
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
Fluoride
0.4
- 0.4 U
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
Si lfatQ
2.0
"14 1
mg/L
EPA 300.0 rev2.1 1/25/18 CGREEN
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
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Oil and Grease, HEM, Total Recoverable mg/L
Aluminum (Al) pg/L
Titanium (Ti) µg/L
Alkalinity, as CaCO3,'to pH.4.5/8.3 mg/L
Phenols, Total Recoverable pg/L
Antimony (Sb) pg/L
Vanadium (V) µg/L
B
BOD: Biochemical Oxygen Demand, 5-day mg/L
Residue: Total (Total Solids) mg/L
Arsenic (As) pg/L
Zinc (Zn) µg/L
cBOD: Carbonaceous BOD, 5-day mg/L
Residue: Volatile/Fixed, Total mg/L
Barium (Ba) pg/L
Coliform: Fecal MF •/100m1
Residue: Suspended (Suspended Solids) mg/L
Beryllium (Be) pg/L
Boron (B), Total µg/L
Coliform: Total MF /100m1
Residue: Volatile/Fixed, Suspended mg/L
Cadmium (Cd) . pg/L
Mercury 1631, low-level ng/L
C
Coliform: Tube Fecal /100m1
TDS -Total Dissolved Solids mg/L
Calcium (Ca) mg/L
C
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Silica mg/L
Chromium (Cr), Total , pg/L
`^.OrganjcsParametets
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Sulfide mg/L
Cobalt (Co) pg/L
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T
TOC - Total Organic Carbon mg/L
Tannin & Lignin • mg/L
Copper (Cu) µg/L
Organochlorine Pesticides
Turbidity NTU
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( ) pg/L
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;;"tithe[
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., r . WetCheptistly.P,arametet's: ri+; i MGM, ;,ti":
pH s.u.
-Lithium (Li) pg/L
-PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration mg/L
Magnesium (Mg) mg/L
Chloride mg/L
Manganese (Mn) pg/L
-
Semi -Volatile Organics (BNAs)
Fluoride mg/L
Mercury (Hg) pg/L
TPH Diesel Range
Sulfate mg/L
t utrientsf?arameters'fia,.; 'iK,,x:.: KrR €:r
Molybdenum (Mo) pg/L
Chlorophyll a pg/L
2(
Ammonia as N (NH3-N) mg/L
Nickel (Ni) pg/L
Volatile Organics (VOA)
Color: ADMI c.u.
)(
Nitrate -Nitrite as N (NO3+NO2-N) mg/L
Potassium (K) mg/L
Color: Platinum Cobalt c.u.
Total Kjeldahl Nitrogen as N (TKN)- mg/L
Selenium (Se) pg/L
TPH Gasoline Range
COD: Chemical Oxygen Demand mg/L
Total Phosphorus as P (TP) mg/L
Silver (Ag) pg/L
Cyanide, Total mg/L
Nitrite as N (NO2-N) • mg/L
Sodium (Na) mg/L
Bjojogical,fi �y * _:,; g rs „ :.1
Formaldehyde mg/L
Nitrate as N (NO3-N calculated) mg/L
Strontium (Sr) pg/L
Phytoplankton / Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4) mg/L
Thallium (TI) • pg/L
LAB COMMENTS :
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Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
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pg/L
Titanium (Ti)
µg/L
Alkalinity, as CaCO3,'to pH.4.5/8.3 • mg/L
Phenols, Total Recoverable
pg/L
Antimony (Sb)
pg/L
Vanadium (V)
µg/L
BOD: Biochemical Oxygen Demand, 5-day mg/L
. Residue: Total (Total Solids)
mg/L
Arsenic (As)
pg/L
Zinc (Zn)
pg/L
cBOD: Carbonaceous BOD, 5-day mg/L .
Residue: Volatile/Fixed, Total
mg/L
Barium (Ba)
pg/L
Coliform: Fecal MF-/100m1
Residue: Suspended (Suspended Solids)
mg/L
Beryllium (Be)
pg/L
Boron (B), Total
RA
Coliform: Total MF /100m1
Residue: Volatile/Fixed, Suspended
mg/L
Cadmium (Cd)
pg/L
Mercury 1631, low-level •
ng/L
Coliform: Tube Fecal /100m1
TDS -Total Dissolved Solids
mg/L
• Calcium (Ca)
mg/L
Coliform: Tube Total /100m1
Silica
mg/L
Chromium (Cr), Total
pg/L
Organk0 Parameters
Specific Conductance, at 25 °C umhos/cm
Sulfide
mg/L
Cobalt (Co)
pg/L
Acid Herbicides
TOC - Total. Organic Carbon mg/L
Tannin & Lignin •
mg/L,
Copper (Cu) •
Ng/1-
Organochlorine Pesticides
Turbidity NTU
Iron (Fe)
pg/L
Organonitrogen Pesticides
Ryg
O hef P ra,11>iete.►.. ;f en ?, , t f ,,,,;£ F f i. j {e,''
Lead (Pb)
Ng/L
Organophosphorus Pesticides
Wetchem0st6Parett►ete60.:' k OM.,.2,i , : :„t,'x :.-
pH
s.u.
•Lithium (Li)
pg/L
PCBs (polychlorinated biphenyts)
Bromide mg/L
Hardness, Total as CaCO3 - by titration
mg/L
Magnesium (Mg)
mg/L
%'
Chloride mg/L
Manganese (Mn)
pg/L
Semi -Volatile Organics (BNAs)
mg/L
Mercury (Hg)
pg/L
TPH Diesel Range
7Fluoride
-
Sulfate mg/L
;'
i Ut grit *iiiii*,ls ,r ,.: ;; r • i , ; :
,
Molybdenum (Mo)
pg/L
Chlorophyll a pg/L
Ammonia as N (NH3-N)
mg/L
-
Nickel (Ni) •
pg/L
Volatile Organics (VOA)
Color: ADMI c.u.
Nitrate -Nitrite as N (NO3+NO2-N)
mg/L
Potassium (K)
mg/L
Color: Platinum Cobalt c.u.
Total Kjeldahl Nitrogen as N (TKN)
mg/L
Selenium (Se)
•Ng/L
TPH Gasoline Range
COD: Chemical Oxygen Demand mg/L
Total Phosphorus as P (TP)
mg/L
Silver (Ag)
pg/L
Cyanide, Total mg/L
Nitrite as N (NO2-N)
mg/L
Sodium (Na)
mg/L
,
81ological,, ,.,, . ,;
Formaldehyde mg/L
Nitrate as N (NO3-N calculated)
mg/L
Strontium (Sr)
pg/L
Phytoplankton / Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4)
mg/L
Thallium (TI)
•
pg/L
LAB COMMENTS :
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Information
Parcels (Yellow)
Tax Bill
Deed
XY
.11
PIN: 18022726002
OWNER: FAIRCLOTH, ANNE B
OWNER ADDRESS:
207 N CHESTNUT ST
OWNER CITY: CLINTON 1
OWNER STATE: NC
OWNER ZIP: 28328
ACREAGE: 84.56
APN: 2435-#051
BK PG: .1800/383
DATE RECORDED: • 6/9/2011
LAND TAX DEFERRED: 145781
ASSESSED VALUE: 74899
TOTAL TAX VALUE: 74899
SITE ADDRESS: TURKEY HWY
TWP CODE: , 18
TAX CODE: F10
SEG TYPE: RESIDUALIRESIDENTILOT
CONSIDERATION: 0
APPR SEG VALUE:
$50,3461$150,3401$20,000
Null
AGRICULTURE
2435-00-6640
2435006640
82.251721
Orphaned Parcel
Null
-ODESSEY\RSiwiec
18022726002 L.
N10 100AAA •
' Null .
Null
Null
Null
Null ,
Null
Null
V
Null
USE DESC: ,
PARCEL CLASS:
GIS_APN:
GEO_PIN:
CALC_ACRES:
STATUS:
CREATEDBY:
MODIFIEDBY:
PIN_1:
MAPSHEET:
STYLE:
YEAR_BUILT:
HEAT:
SYSTEM:
ROOF:
FOUNDATION:
BEDROOMS:
FULL BATH:
Legend
Display Labels Display 50 Results
13— Pt- r/0 ye PN` 4:84-1-wg
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North Carolina Division of Water Resources
Water Sample Collection &Submittal
Central Laboratory (Water Sciences Section)
Form
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, u�a
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MBAS (surfactants)
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Tin (Sn) pg/L
Acidity, as CaCO3, to pH 4.5/8.3 mg/L
011 and Grease, HEM, Total Recovelrable
mg/L
%
Aluminum (Al) pg/L
Titanium (Ti) pg/L
Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L
Phenols, Total Recoverable
pg/L
Antimony (Sb) pg/L
anadium (V) pg/L•
BOD: Biochemical oxygen Demand, 5-day mg/L
Residue: Total (Total Solids)
mg/L
Arsenic (As) pg/L
inc (Zn) µg/L
cBOD: Carbonaceous BOD, 5-day mg/L
Residue: Volatile/Fixed, Total
mg/L
Barium (Ba) pg/L
Coliform: Fecal MF /100m1
Residue: Suspended (Suspended Solids)
mg/L
Beryllium (Be) pg/L
Boron (B), Total pg/L
Collform: Total MF /100ml
Residue: Volatile/Fixed, Suspended
mg/L
admium (Cd) pg/L
Mercury 1631, low-level ng/L
Coliform: Tube Fecal /100m1
TDS - Total Dissolved Solids
mg/L
alcium (Ca) mg/L
-
Coliform: Tube Total /100m1
Silica
mg/L
Chromium (Cr), Total pg/L
Tr��H".XNkWSMP}"C'
WOO
•1fl b
Specific Conductance, at 25 °C umhos/cm
Sulfide
mg/L
Cobalt (Co) pg/L
Acid Herbicides
TOC - Total Organic Carbon mg/L
Tannin & Lignin
mg/L
Copper (Cu) pg/L
Organochlorine Pesticides
Turbidity NTU
Iron (Fe) pg/L
Organonitrogen Pesticides
''i'�
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Lead (Pb) pg/L
Organophosphorus Pesticides
10i
�
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pH
s.u.
_Lithium (Li) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness, Total as CaCO3 - by titration
mg/L
✓
Magnesium (Mg) mg/L
Chloride • mg/L
.Manganese (Mn) - pg/L
Semi -Volatile Organics (BNAs)
,Fluoride mg/L
Mercury (Hg) • pg/L
TPH Diesel Range
Sulfate mg/L
SIR
AIWA ! et , 1li'
(, . Salt �. r
.�'�lu�>���5
Molybdenum
Y (Mo) pg/L
Chlorophyll a pg/L
Ammonia as N (NH3-N)
mg/L
ickel (Ni) pg/L
Volatile Organics (VOA)
Color: ADMI c.u.
Nitrate -Nitrite as N (NO3+NO2-N)
mg/L
otassium (K) mg/L
Color: Platinum Cobalt c.u.
Total Kjeldahl Nitrogen as N (TKN)
mg/L
Selenium (Se) pg/L
TPH Gasoline Range •
COD: Chemical Oxygen Demand mg/L
Total Phosphorus as P (TP)
mg/L
Silver (Ag) • pg/L
Cyanide, Total mg/L
Nitrite as N (NO2-N)
mg/L
dium (Naj mg/L
k y;" nl(t]yi
i4k"ti
Formaldehyde mg/L
Nitrate as N (NO3-N calculated)
mg/L
Strontium (Sr) pg/L
Phytoplankton /Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate as P (PO4)
mg/L
Thallium (TI) pg/L
LAB COMMENTS :
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Revision: 2/06/2015

North Carolina Division of Water Resources
Central Laboratory (Water Sciences Section)
Notes:
Water Sample Collection &
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n(1204
❑ Chlorinated• ❑De -chlorinated in Field
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Grab UCom
❑ Other:
Submittal Form
osite
T�4
El Ambient
Routine
❑ Compliance
❑ c0c
❑ Emergency
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❑ Waste
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Solution
River/Stream
❑Estuary
❑Stormwater
Monitoring Well
❑Effluent
❑Field Blank
❑Filter Blank
❑Other:
Lake
❑Can'ai
Water Supply
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UState Courier
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?
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RA
clmty, as CaLu3, to pH 4.5/B.
Alkalinity, as CaCO3, to pH 4.5/8.3
BOD: Biochemical Oxygen Demand, 5-day
cBOD: Carbonaceous BOD, 5-day
mg/L
mg/L
mg/L
mg/L
II and Grease, HEM, local Recoverable
Phenols, Total Recoverable
Residue: Total (Total Solids)
Residue: Volatile/Fixed, Total
mg/L 4/ Aluminum (A
pg/L Antimony (Sb)
mg/L Arsenic (As)
mg/L V Barium (Ba)
pg/L Titanium (Ti)
pg/L 1„6enadium (V)
pg/L
pg/L
Zinc (Zn)
pg/L
pg/L
pg/L
oliform: Fecal MF
� Coliform: Total MF
Coliform: Tube Fecal
Coliform: Tube Total
Specific Conductance, at 25 °C
TOC - Total Organic Carbon
/100ml
/100m1
/100m1
/100m1
umhos/cm
mg/L
Residue: Suspended (Suspended Solids)
Residue: Volatile/Fixed, Suspended
TDS -Total Dissolved Solids
Silica
Sulfide
Tannin & Lignin
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
eryllium (Be)
Cadmium (Cd)
,/Calcium (Ca)
'Chromium (Cr), Total
Turbidity
Bromide
Chloride
Fluoride
Sulfate
Chlorophyll a
Color: ADMI
Color: Platinum Cobalt
COD: Chemical Oxygen Demand
Cyanide, Total
Formaldehyde
NTU
mg/L
mg/L
mg/L
pg/L
mg/L
mg/L
mg/L
HexavalentChromium (Cr6+) mg/L
.vjR,,
IW OMENDhis" W'r MPLIOr
pH
Hardness, Total as CaCO3 - by titra
grij;j0.0?* CMKONWIW
Vic Ammonia as N (NH3-N)
�/ otal Kjeldahl Nitrogen as N (TKN)
3
Nitrate -Nitrite as N.(NO3+NO2-N)
Total Phosphorus as P (TP)
Nitrite as N (NO2-N)
Nitrate as N (NO3-N calculated)
Orthophosphate as P (PO4)
:ion
s.u.
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Cobalt (Co)
,' Copper (Cu)
V - Iron (Fe)
Lead (Pb)
pg/L
11g/L
mg/L
Pg/L
pg/L
pg/L
Boron (B), Total
Mercury 1631, low-level
Acid Herbicides
Organochlorine Pesticides
g/L
ng/L
Lithium (Li)
,✓ Magnesium (Mg)
Manganese (Mn)
Mercury (Hg)
Molybdenum (Mo) •
1'lickel (Ni)
potassium (K)
Selenium (Se)
Silver (Ag)
,/r5bdlum (Na)
// Strontium (Sr)
pg/L
pg/L
pg/L
mg/L
ijg/L
pg/L
pg/L
pg/L
mg/L
pg/L
pg/L
mg/L
pg/L
Thallium (TI) pg/L
Organonitrogen Pesticides
Organophosphorus Pesticides
PCBs (polychlorinated biphenyls)
Semi -Volatile Organics (BNAs)
TPH Diesel Range
Volatile Organics (VOA)
TPH Gasoline Range
Phytoplankton / Algae
iG
LAB COMMENTS :
Oie
5
Revision: 2/06/2015
I (�
7, L)

North Carolina Division of Water Resources
Water Sample Collection &
Central Laboratory (Water Sciences Section)
Submittal Form
It
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osite
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❑ Filtered in Field
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1
li
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bu'�'r5ty�.J
i Y"xs?
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VitrilW0
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40
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Tin (Sn) µg/L
Acidity, as CaCO3, to pH 4.5/8.3 mg/L
Oil and Grease,
HEM, Total Recoveirable
mg/L
luminum (Al) pg/L
Titanium (Ti) pg/L
Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L
Phenols, Total
Recoverable
pg/L
ntimony (Sb) pg/L
Arsenic
p
nadium (V) µg/L
BOD: Biochemical oxygen Demand, 5-day mg/L
Residue: Total
(Total Solids)
mg/L
�
(As) pg/L
Zinc (Zn) pg/L
cBOD: Carbonaceous BOD, 5-day mg/L
Residue: Volatile/Fixed,
Total
mg/L
%/Barium
(Ba) • fig/L
,Coliform: Fecal MF /100m1
Residue: Suspended
(Suspended Solids)
mg/L
,,Beryllium (Be) I1g/L
Boron (B), Total pg/L_
V
Coliform: Total MF /100m1
Residue: Volatile/Fixed,
Suspended
mg/L
Cadmium (Cd) pg/L
Mercury 1631, low-level ng/L
Coliform: Tube Fecal /100m1
TDS -Total
Dissolved Solids
mg/L
(Ca) mg/L
Coliform: Tube Total /100m1
Silica
mg/L
,alcium
Chromium (Cr), Total hg/L
*
Specific Conductance, at 25 °C - umhos/cm
Sulfide
mg/L
.
Cobalt (Co) pg/L
Acid Herbicides
TOC - Total Organic Carbon mg/L
Tannin &
Lignin
mg/L
r7Copper
(Cu) IJg/L
Organochlorine Pesticides
Turbidity NTU
on (Fe) Jg/L
Organonitrogeh Pesticides
i il o�.
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Lead Pb pg/L
OrganophosphorusPesticldes
3 "
40410 0110' f `MO{ C r air
pH
s.u.
Lithium (Li) pg/L
PCBs (polychlorinated biphenyls)
Bromide mg/L
Hardness,
Total asCaCO3-bytitraltion
mg/L
,JMagnesium(Mg)
mg/L
_
Chloride mg/L
Manganese (Mn) pg/L '
Semi -Volatile Organics (BNAs)
.Fluoride -mg/L
Mercury (Hg) Ilg/L
TPH Diesel Range
Sulfate mg/L
"`4
0 'r
tm.
t r ;
"ar % .'
jr,Imonia
Molybdenum (Mo)
Chlorophyll a hg/L
Nitrate
as N (NH3 N)
mg/L
ickel (Ni) _ hg/L
Volatile Organics (VOA)
Color: ADMI c.u.
-Nitrite
as N (NO3+NO2-N) I
mg/L
,�
/Potassium
(K) mg/L
Color: Platinum Cobalt c.u.
/
.Total Kjeldahl
Nitrogen as N (TKN) I
mg/L
Selenium (Se) IJg/L
TPH Gasoline Range
COD: Chemical Oxygen Demand mg/L
/
Total Phosphorus
as P (TP)
mg/L
Silver (Ag) pg/L
_
Cyanide, Total mg/L
Nitrite as
N-(NO2-N)
mg/L
V Sodium (Na) mg/1-
010VAI3NI„}�,�
Formaldehyde mg/L
Nitrate as
N (NO3-N calculated) I
- mg/L
kr-Strontium (Sr) pg/L
Phytoplankton /Algae
Hexavalent Chromium (Cr6+) mg/L
Orthophosphate
as P (PO4)
mg/L
• Thallium (TI) Jg/L
LAB COMMENTS :
.
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PERMIT: WQ0004268
FACILITY: Sager Creek Foods Inc - Allens, Inc. - Plant #7
PARAMETER: 00680 - Carbon, Tot Organic (TOC)
240
200
160
T
- MW1
- MW _1
MW2
120 - BMW-2
- MW3
- ®- MW-3
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From: Elkin, Dave [mailto:[e-mail]]
Sent Wednesday, December 13, 201710:18 AM
To: Barber, Jim <[e-mail]> .
Cc: Nordin, David <[e-mail]>; Miller, Thad'<[e-mail]>
Subject: [External]FW: Elliot Site 121317 .
iCAUTION: External email. Do not click links or open attachments unless verified. Send all suspicious email as an attachment to
report'.spam @ nc.gov.
Good morning Jim;
We are getting'more anxiouswith: our. desire to divert surface water away from our large lagoon at the Elliot site ( see
below email). Can you give me anindication where your thinking is on this. I would like to have equipment Tined up to
move as soon as we can.
Thanks,
Dave
From: Nordin, David.
Sent: Wednesday, December 13, 2017 10:00 AM
To: Westerbeek, Kraig; Elkin, Dave; Weston, Kevin
Cc: Norris, Michael
Subject: Elliot Site 121317
There was 2.8 inches of rainfall at the Elliott site.Iast week. The lagoon appears to have risen `10"inches last week from
the rain. Derek has checked several times the level. Michaelhas asked: Thad to check the staff guage to ensure the level
is correct.
David Nordin
Environmental Systems Director'
Hog Production Division - Corporate
Eastern Operations
Smith iel4
oa4,{oi5 ;o `Rtspoi s{b.tg
[phone] office PO Box 856/2822 NC Hwy 24 West
(910) 290 - 0231 mobile Warsaw, NC 28398
[e-mail] www.smithfieldfoods.com
•
This communication (including any attachments) is confidential and is intended to be privileged pursuant to applicable law.. if you are not the intended,
recipient or the employee or agent responsible for delivering it to the intended recipient then you are hereby notified that the dissemination, distribution
-or copying of this communication is-prohibited.Ifyou received this communication in error,; please notify Smithfield Foods, Inc. immediately by'telephone
([phone]) and then delete this comrnunication and destroy all copies thereof.

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(c) Except for tracers used in concentrations which have been determined by the Division of Public Health to be protective of
human health, and the use of which has been permitted by the Division, substances which are not naturally occurring and for
which no standard is specified shall not be permitted in concentrations at or above the practical quantitation limit in Class GA
or Class GSA groundwaters. Any person may petition the Director to establish an interim maximum allowable concentration
for a substance for which a standard has not been established under this Rule. The petitioner shall submit relevant
toxicological and epidemiological data, study results, and calculations necessary to establish a standard in accordance with
Paragraph (d) of this Rule. Within three months after the establishment of an interim maximum allowable concentration for a
substance by the Director, the Director shall initiate action to consider adoption of a standard for that substance.
(d) Except as provided in Paragraph (f) of this Rule, groundwater quality standards for substances in Class GA and Class
GSA groundwaters are established as the least of:
(1) Systemic threshold concentration calculated as follows: [Reference Dose (mg/kg/day) x 70 kg (adult body
weight) x Relative Source Contribution (.10 for inorganics; .20 for organics)] / [2 liters/day (avg. water
consumption)];
(2) Concentration which corresponds to an incremental lifetime cancer risk of 1x10-6;
(3) Taste threshold limit value;
(4) Odor threshold limit value;
(5) Maximum contaminant level; or
(6) National secondary drinking water standard.
(e) The following references, in order of preference, shall be used in establishing concentrations of substances which
correspond to levels described in Paragraph (d) of this Rule.
(1) Integrated Risk Information System (U.S. EPA).
(2) Health Advisories (U.S. EPA Office of Drinking Water).
(3) Other health risk assessment data published by the U.S. EPA.
(4) Other relevant, published health risk assessment data, and scientifically valid peer -reviewed published
toxicological data.
(f) The Commission may establish groundwater standards Less stringent than existing maximum contaminant levels or
national secondary drinking water standards if it finds, after public notice and opportunity for hearing, that:
(1) more recent data published in the EPA health references listed in Paragraph (e) of this Rule results in a
standard which is protective of public health, taste threshold, or odor threshold;
(2) the standard will not endanger the public health and safety, including health and environmental effects
from exposure to groundwater contaminants; and
(3) compliance with a standard based on the maximum contaminant level or national secondary drinking water
standard would produce serious hardship without equal or greater public benefit.
(g) Groundwater quality standards specified in Paragraphs (h) and (i) of this Rule and interim maximum allowable
concentrations established pursuant to Paragraph (c) of this Rule shall be reviewed by the Director on a triennial basis.
Appropriate modifications to established standards shall be made in accordance with the procedure prescribed in Paragraph
(d) of this Rule where modifications are considered appropriate based on data published subsequent to the previous review.
(h) Class GA Standards. Unless otherwise indicated, the standard refers to the total concentration in micrograms per liter of
any constituent in a dissolved, colloidal or particulate form which is mobile in groundwater. This does not apply to sediment
or .other particulate matter which is preserved in a groundwater sample as a result of well construction or sampling
procedures. The Class GA standards are:
(1) Acenaphthene: 80;
(2) Acenaphthylene: 200;
(3) Acetone: 6 mg/L;
(4) Acrylamide: 0.008;
(5) Anthracene: 2 mg/L;
(6) Arsenic: 10;
(7) Atrazine and chlorotriazine metabolites: 3;
(8) Barium: 700;
(9) Benzene: 1;
(10) Benzo(a)anthracene (benz(a)anthracene): 0.05;
(11) Benzo(b)fluoranthene: 0.05;
(12) Benzo(k)fluoranthene: 0.5;
(13) Benzoic acid: 30 mg/L;
(14) Benzo(g,h,i,)perylene: 200;
(15) Benzo(a)pyrene: 0.005;
NORTH CAROLINA ADMINISTRATIVE CODE
Amended April 1, 2013 16

(16) Bis(chloroethyl)ether: 0.03;
(17) Bis(2-ethylhexyl) phthalate (di(2-ethylhexyl) phthalate): 3;
(18) Boron: 700;
(19) Bromodichloromethane: 0.6;
(20) Bromoform (tribromomethane): 4;
(21) n-Butylbenzene: 70;
(22) sec-Butylbenzene: 70;
(23) tert-Butylbenzene: 70;
(24) Butylbenzyl phthalate: 1 mg/L;
(25) Cadmium: 2;
(26) Caprolactam: 4 mg/L;
(27) Carbofuran: 40;
(28) Carbon disulfide: 700;
(29) Carbon tetrachloride: 0.3;
(30) Chlordane: 0.1; 4
(31) Chloride: 250 mg/L;
(32) Chlorobenzene: 50;
(33) Chloroethane: 3,000;
(34) Chloroform (trichloromethane): 70;
(35) Chloromethane (methyl chloride): 3;
(36) 2-Chlorophenol: 0.4;
(37) 2-Chlorotoluene (o-chlorotoluene): 100;
(38) Chromium: 10;
(39) Chrysene: 5;
(40) Coliform organisms (total): 1 per 100 mL;
(41) Color: 15 color units;
(42) Copper: 1 mg/L;
(43) Cyanide (free cyanide): 70;
(44) 2, 4-D (2,4-dichlorophenoxy acetic acid): 70;
(45) DDD: 0.1;
(46) DDT: 0.1;
(47) Dibenz(a,h)anthracene: 0.005;
(48) Dibromochloromethane: 0.4;
(49) 1,2-Dibromo-3-chloropropane: 0.04;
(50) Dibutyl (or di-n-butyl) phthalate: 700;
(51) 1,2-Dichlorobenzene (orthodichlorobenzene): 20;
(52) 1,3-Dichlorobenzene (metadichlorobenzene): 200;
(53) 1,4-Dichlorobenzene (paradichlorobenzene): 6;-
(54) Dichlorodifluoromethane-(Freon-12; Halon): 1 mg/L;
(55) 1,1-Dichloroethane: 6;
(56) 1,2-Dichloroethane (ethylene .dichloride): 0.4;
(57) 1,2-Dichloroethene (cis): 70;
(58) 1,2-Dichloroethene (trans): 100;
(59) 1,1-Dichloroethylene (vinylidene chloride): 350;
(60) 1,2-Dichloropropane: 0.6;
(61) 1,3-Dichloropropene (cis and trans isomers): 0.4;
(62) Dieldrin: 0.002;
(63) Diethylphthalate: 6 mg/L;
(64) 2,4-Dimethylphenol (m-xylenol):.100;
(65) Di-n-octyl phthalate: 100;
(66) 1,4-Dioxane (p-dioxane): 3;
(67) Dioxin (2,3,7,8-TCDD): 0.0002 ng/L;
(68) 1,1— Diphenyl (1,1,-biphenyl): 400;
(69) Dissolved solids (total): 500 mg/L;
(70) Disulfoton: 0.3;
(71) Diundecyl phthalate (Santicizer 711): 100;
NORTH CAROLINA ADMINISTRATIVE CODE
Amended April 1, 2013 17

(72) Endosulfan: 40;
(73) Endrin, total (includes endrin, endrin aldehyde and endrin ketone): 2;
(74) Epichlorohydrin: 4;
(75) Ethyl acetate: 3 mg/L;
(76) Ethylbenzene: 600;
(77) Ethylene dibromide (1,2-dibromoethane): 0.02;
(78) Ethylene glycol: 10 mg/L;
(79) Fluoranthene: 300;
(80) Fluorene: 300;
(81) Fluoride: 2 mg/L;
(82) Foaming agents: 500;
(83) Formaldehyde: 600;
(84) Gross alpha (adjusted) particle activity (excluding radium-226 and uranium): 15 pCi/L;
(85) Heptachlor: 0.008;
(86) Heptachlor epoxide: 0.004;
(87) Heptane: 400;
(88) Hexachlorobenzene(perchlorobenzene): 0.02;
(89) Hexachlorobutadiene: 0.4;
(90) Hexachlorocyclohexane isomers (technical grade): 0.02;
(91) n-Hexane: 400; -
(92) Indeno(1,2,3-cd)pyrene: 0.05;
(93) Iron: 300;
(94) Isophorone: 40;
(95) Isopropylbenzene: 70;
(96) Isopropyl ether: 70;
(97) Lead: 15;
(98) Lindane (gamma hexachlorocyclohexane): 0.03;
(99) Manganese: 50;
(100) Mercury: 1;
(101) Methanol: 4 mg/L;
(102) Methoxychlor: 40;
(103) Methylene chloride (dichloromethane): 5;
(104) Methyl ethyl ketone (2-butanone): 4 mg/L;
(105) 2-Methylnaphthalene: 30;.
(106) 3-Methylphenol (m-cresol): 400;
(107) 4-Methylphenol (p-cresol): 40;
(108) Methyl tert-butyl ether (MTBE): 20;
(109) Naphthalene: 6;
(110) Nickel: 100;
(111) Nitrate (as N): 10 mg/L;
(112) Nitrite (as N): 1 mg/L;
(113) N-nitrosodimethylamine: 0.0007;
(114) Oxamyl: 200;
(115) Pentachlorophenol: 0.3;
(116) Petroleum aliphatic carbon fraction class (C5 - C8): 400;
(117) Petroleum aliphatic carbon fraction class (C9 - C18): 700;
(118) Petroleum aliphatic carbon fraction class (C19 - C36): 10 mg/L;
(119) Petroleum aromatics carbon fraction class (C9 - C22): 200;
(120) pH: 6.5 - 8.5;
(121) Phenanthrene: 200;
(122) Phenol: 30;
(123) Phorate: 1;
(124) n-Propylbenzene: 70;
(125) Pyrene: 200;
(126) Selenium: 20;
(127) Silver: 20;
NORTH CAROLINA ADMINISTRATIVE CODE
Amended April 1, 2013 18

(128) Simazine: 4;
(129) Styrene: 70;
(130) Sulfate: 250 mg/L;
(131) 1,1,2,2-Tetrachloroethane: 0.2;
(132) Tetrachloroethylene (perchloroethylene; PCE): 0.7;
(133) 2,3,4,6-Tetrachlorophenol: 200;
(134) Toluene: 600;
(135) Toxaphene: 0.03;
(136) 2,4,5-TP (Silvex): 50;
(137) 1,2,4-Trichlorobenzene: 70;
(138) 1,1,1-Trichloroethane: 200;
(139) Trichloroethylene (TCE): 3;
(140) Trichlorofluoromethane: 2 mg/L;
(141) 1,2,3-Trichloropropane:.0.005;
(142) 1,2,4-Trimethylbenzene: 400;
(143) 1,3,5-Trimethylbenzene: 400;
(144) 1,1,2-Trichloro-1,2,2-trifluoroethane (CFC-113): 200 mg/L;
(145) Vinyl chloride: 0.03;
(146) Xylenes (o-, m-, and p-): 500; and
(147) Zinc: 1 mg/L. -
(i) Class GSA Standards. The standards for this class are the same as those for Class GA except as follows:
(1) chloride: allowable increase not to exceed 100 percent of thenatural quality concentration; and
(2) dissolved solids (total): 1000 mg/L.
(j) Class GC Standards.
(1) The concentrations of substances that, at the time of classification, exceed the standards applicable to Class
GA or GSA groundwaters shall not be caused to increase, nor shall the concentrations of other substances
be caused to exceed the GA or GSA standards as a result of further disposal of contaminants to or beneath
the surface of the land within the boundary of the area classified GC.
(2) The concentrations of substances that, at the time of classification, exceed the standards applicable to GA
or GSA groundwaters shall not be caused_ to migrate as a result of activities within the boundary of the GC
classification, so as to violate the groundwater or surface water quality standards in adjoining waters of a.
different class.
(3) Concentrations of specific substances, that exceed the established standard at the time of classification, are
listed in Section .0300 of this Subchapter.
History Note: Authority G.S. 143-214.1; 143B-282(a) (2);
Eff. June 10, 1979;
Amended;Eff. November 1, 1994; October 1, 1993; Septeinber,l, 1992; August 1, 1989;
Temporary Amendment Eff. June 30, 2002;
Amended Eff. August 1, 2002;
Temporary Amendment Expired February 9, 2003;
Amended Eff. April 1, 2013; January 1, 2010; April 1, 2005.
NORTH CAROLINAADMINISTRATIVE CODE
Amended April 1', 2013 19

ACME Mapper 2.1 - 14.3 km SW of Warsaw NC

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9.2 km ExNE of Clinton NC, 12.9 km WxNW of Warsaw NC
13.2 km SW of Faison NC,169 km ERNE of Sampson County NC
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Waterbodies Tree
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Cape Fear
Name of Stream
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18 - Cape Fear Drainage Area
six runs
L
Turtle Branch
Six Rini s Creek
H
0-111
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From source to Great Coharie Creek II 18-68-1-19
'Fromsouuce to Quewiffle SviarrT
Kings Branch
Clifton Branch
Hoe Swamp
Mill Swamp
Gillmore Swamp
Tenmile Swamp
Beaverc]arn Swamp
Turkey Creek
Hicks Branch
Mill Run
18-68-2-(0 3)
From source to Six Runs Creek
Rowans Branch (Chestnt
Bull Branch
Stewarts Creek
L
Buckhall Creek
Carlton Mill Run
Bakers Branch
From source to King Branch
From source to Six Runs Creek
From source to Six Runs Creek
From source to Six Runs Creek
From source to Six Runs Creek
From source to Six Runs Creek
From source to Six Runs Creek
From source to Turkey Creek
From source to Six Runs Creek
From source to Six Runs Creek
From source to Six Runs Creek
From soruce to Six Runs Creek
From source to Stewarts Creek
From source to Stewarts Creek
Beck
18-68-2-0.5
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CSw
18-68-2-0.5-1
18-68-2-1
18-68-2-2
18-68-2-3
18-68-2-4
18-68-2-5
18-68-2-6
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From source to Carltons Mill Run
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Active
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04/01/1959
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15A NCAC 02B .0211 FRESH SURFACE WATER QUALITY STANDARDS FORcCLASS C WATERS
General. The water quality standards for all fresh surface waters shall be the basic standards applicable to Class C waters.
Water quality standards for temperature and numerical water quality standards for the protection of human health applicable
to all fresh surface waters are in Rule .0208 of this Section. Additional and more stringent standards applicable to other
specific freshwater classifications are specified in Rules .0212, .0214, .0215, .0216, .0218, .0219, .0223, .0224 and .0225 of
this Section. fActioi n Levels for purposes of National Pollutant Discharge Elimm ion System=(NPDES) permitting areJ
specif d`in t m (22) of this Rule. f
(I)TB`est Usage of Waters: aquatic Life propagation and maintenance of biological integrity (including fishing
and fish), wildlife, secondary recreation, agriculture, and any other usage except for primary recreation or
as a source of water supply for drinking, culinary, or food processing purposes;
(2) Conditions Related to Best Usage: the waters shall be suitable for aquatic life propagation and
maintenance of biological integrity, wildlife, secondary recreation, and agriculture. Sources of water
pollution that preclude any of these uses on either a short-term or long-term basis shall be considered to be
violating a water quality standard;
(3) ' Ch orml e, total residual': 17 ug/1;
(4) Chlorophyll a (corrected)' notgreater than 40 u gor lakes, reservoirs, and other waters subject to growths
of macroscopic or microscopic vegetation ton designated as trout waters, and not greater than 15 ug/1 for
lakes, reservoirs, and other waters subject to growths of macroscopic or microscopic vegetation designated
as trout waters (not applicable to lakes or reservoirs less than 10 acres in surface area). The Commission or
its designee may prohibit or limit any discharge of waste into surface waters if the surface waters
experience or the discharge would result in growths of microscopic or macroscopic vegetation such that the
standards established pursuant to this Rule would be violated or the intended best usage of the waters
• would be impaired;
(5) Cyanide, total:, 5.0'ug/L]
(6) Dissolved oxygenjnot less than 6.0 mg/1 for trout waters; for non -trout waters, -not less than a dailyaverage
of 5.0 mg/41 pwith a minimum instantaneous value of not less than 4.0 mg/1; swamp waters lake coves or
ackwaters and lake bottom waters -inay have lower values if caused by natural conditions;
(7) Fecal col shall not exceed a geometric mean of1200/100m11(MF count)} based upon at least five
consecutive samples examined during any 30 day period, nor exceefi 400/100m1 zn more than 20 percent of
the samples examined during such period. Violations of the fecal coliform standardare expected during
rainfall events and, in some cases, this violation is expected to be caused by uncontrollable nonpoint source
pollution. All coliform concentrations shall be analyzed using the membrane filter technique, unless high
turbidity or other adverse conditions necessitate the tube dilution method. In case of controversy over
results, the MPN 5-tube dilution technique shall be used as the reference method;
(8) Floating solids, settleable solids, or sludge deposits: only such amounts attributable to sewage, industrial
wastes, or other wastes as shall not make the water unsafe or unsuitable for aquatic life and wildlife or
impair the waters for any designated uses;
(9) Fluoride: 1.8 mg/1;
(10) Gases, total dissolved: not greater than 110, percent of saturation;
(11) etals:
(a) - With the exception of mercury and selenium, freshwater aquatic life standards for metals shall be
based upon measurement of the dissolved fraction of the metal. Mercury and selenium water
quality standards shall be based upon measurement of the total recoverable metal;
(b) Freshwater metals standards that are not hardness -dependent shall be as follows:
(i) Arsenic, dissolved, acute: WER• 340 ug/1;
(ii) Arsenic, dissolved, chronic: WER 150 ug/1;
(iii) Beryllium, dissolved, acute: WER 65 ug/1; -
(iv) Beryllium, dissolved, chronic: WER• 6.5 ug/1;
(v) Chromium VI, dissolved, acute: WER• 16 ug/1;
(vi) Chromium VI, dissolved, chronic: WER• 11 ug/1;
(vii) Mercury, total recoverable, chronic: 0.012 ug/1;
(viii) Selenium, total recoverable, chronic: 5 ug/1;

(ix) Silver, dissolved, chronic: WER. 0.06 ug/1;
With the exception of mercury and selenium, acute and chronic freshwater aquatic life standards
for metals listed in this Subparagraph apply to the dissolved form of the metal and apply as a
function of the pollutant's water effect ratio (WER). A WER expresses the difference between the
measures of the toxicity of a substance in laboratory waters and the toxicity in site water. The
WER shall be assigned a value equal to one unless any person demonstrates to the Division's
satisfaction in a permit proceeding that another value is developed in accordance with the "Water
Quality Standards Handbook: Second Edition" published by the US Environmental Protection
Agency (EPA-823-B-12-002), free of charge, at
http://water.epa.gov/scitech/swguidance/standards/handbook/, hereby incorporated by reference
including any subsequent amendments. Alternative site -specific standards may also be developed
when any person submits values that demonstrate to the Commissions' satisfaction that they were
derived in accordance with the "Water Quality Standards Handbook: Second Edition,
Recalculation Procedure or the Resident Species Procedure", hereby incorporated by reference
including subsequent amendments at
http ://water.ep a.gov/scitech/swguidance/stand ards/handbook/.
This material is available free of charge.
Hardness -dependent freshwater metals standards are located in Sub -Item (c) and (d) of this Rule
and in Table A: Dissolved Freshwater Standards ,for Hardness -Dependent Metals;
(c) CHardness-dependent freshwater metals standards_ shall be,as follows
(i) H ardness-dependent metals standards shall be derived using the equations specified in
Table A: Dissolved Freshwater Standards for Hardness -Dependent Metals. If the actual
instream hardness (expressed as CaCO3 or Ca+Mg) is less than 25 milligrams/liter
(mg/1), standards shall be calculated based upon 25 mg/1 hardness. If the actual instream
hardness is greater than 25 mg/1 and less than 400 mg/1, standards shall be calculated
based upon the actual instream hardness. If the instream hardness is greater than 400
mg/1, the maximum applicable hardness shall be 400 mg/1;
(ii) Hardness -dependent metals in NPDES permitting: for NPDES permitting purposes,
application of the equations in Table A: Dissolved Freshwater Standards for Hardness -
Dependent Metals shall have hardness values (expressed as CaCO3 or Ca+Mg)
established using the median of instream hardness data collected within the local US
Geological Survey (USGS) and Natural Resources Conservation Service (NRCS) 8-digit
Hydrologic Unit (HU). The minimum applicable instream hardness shall be 25 mg/1 and
the maximum applicable instream hardness shall be 400 mg/1, even when the actual
median instream hardness is less than 25 mg/1 and greater than 400 mg/1;
(d) Alternatives:
Acute and chronic freshwater aquatic life standards for metals listed in Table A apply to the
dissolved form of the metal and apply as a function of the pollutant's water effect ratio (WER),
which is set;forth in Sub -Item (b) of this Rule. Alternative site -specific standards may also be
developed as set forth in Sub -Item (b) of this Rule;
Table A: Dissolved Freshwater Standards for Hardness -Dependent Metals
Numeric standards calculated at 25 mg/I hardness are listed below for illustrative purposes. The Water Effects Ratio
(WER) is equal to one unless determined otherwise under Sub -Item (d) of this Rule.
Metal
Equations for Hardness -Dependent Freshwater Metals (ug/1)
Standard at
25 mg/1
hardness
(ug/I)
Cadmium,
Acute
WER. [{1.136672-[In hardness](0.041838)} • e^{0.9151 [In hardness]-3.1485}]
0.82
Cadmium,
Acute,
Trout waters
WER. [{1.136672-[/n hardness](0.041838)} • e^{0.9151[In hardness]-3.6236}} -
0.51
Cadmium,
WER [{1.101672-[ln hardness](0.041838)) • e^{0.7998[In hardness]-4.4451 } ]
0.15

• Chronic
Chromium
III, Acute
WER• [0.316 • e^{0.8190[ln hardness]+3.7256}]
180
Chromium
III, Chronic
WER• [0.860 • e^{0.8190[In hardness]+0.6848}]
24 '
Copper,
Acute
WER• [0.960 • e^{0.9422[In hardness]-1.700}]
Or,
Aquatic Life Ambient Freshwater Quality Criteria -Copper 2007 Revision
(EPA-822-R-07-001)
3.6
NA
Copper,
Chronic
WER• [0.960 • e^{0.8545[In hardness]-1.702}]
Or,
Aquatic Life Ambient Freshwater Quality Criteria -Copper 2007 Revision
(EPA-822-R-07-001)
2.7
NA
Lead,
Acute
WER• [{1.46203-[ln hardness](0.145712)} • e^{1.273[In hardness]-1.460}]
14
Lead,
Chronic
WER• [{1.46203-[ln hardness](0.145712)) • e^{1.273[In hardness]-4.705}]
0.54
Nickel,
Acute
WER• [0.998 • e^{0.8460[ln hardness]+2.255}]
140
Nickel,
Chronic
WER• [ 0.997 • e^{0.8460[In hardness]+0.0584}]
16
Silver,
Acute
WER• [ 0.85 • e^{1.72[In hardness]-6.59}]
0.30
Zinc, Acute
WER• [0.978 • e^{0.8473[In hardness]+0.884}1
36
Zinc,
Chronic
WER• [ 0.986 • e^{0.8473[In hardness]+0.884}]
36
(e)
Compliance with acute instream metals standards shall only be -evaluated using an average of two
or more samples collected within one hour. Compliance with chronic instream metals standards
shall only be evaluated using an average of a minimum of four samples taken on consecutive days,
or as a 96-hour average;
(f) Metals criteria shall be used for proactive environmental management. An instream exceedence of
the numeric criterion for metals shall not be considered to have caused an adverse impact to the
instream aquatic community without biological confirmation and a comparison of all available
monitoring data and applicable water quality standards. This weight of evidence evaluation shall
take into account data quality and the overall confidence in how representative the sampling is of
conditions in the waterbody segment before an assessment of aquatic life use attainment, or non -
attainment, shall be made by the Division. Recognizing the synergistic and antagonistic
complexities of other water quality variables on the actual toxicity of metals, with the exception of
mercury and selenium, biological monitoring will be used to validate, by direct measurement,
whether or not the aquatic Life use is supported;
(12) Oils, deleterious substances, colored, or other wastes: only such amounts as shall not render the waters
injurious to public health, secondary recreation, or to aquatic life and wildlife, or adversely affect the
palatability of fish, aesthetic quality, or impair the waters for any designated uses. For the purpose of
implementing this Rule, oils, deleterious substances, colored, or other wastes shall include substances that
cause a film or sheen upon or discoloration of the surface of the water or adjoining shorelines pursuant to
40 CFR 110.3(a)-(b) which are hereby incorporated by reference including any subsequent amendments
and additions. This material is available, free of charge, at: http://www.ecfr.gov/;
(13�}`- �esticides:l
(a) Aldrin: 0.002 ug/I;
(b) Chlordane: 0.004 ug/1;
(c) DDT: 0.001 ug/1;
(d) Demeton: 0.1 ug/1;

(e) Dieldrin: 0.002 ug/1;
(f) Endosulfan: 0.05 ug/1;
(g) Endrin: 0.002 ug/1;
(h) Guthion: 0.01 ug/1;
(i) Heptachlor: 0.004 ug/1;
(j) Lindane: 0.01 ug/1;
(k) Methoxychlor: ' 0.03 ug/1;
(1) Mirex: 0.001 ug/1;
Parathion: 0.013 ug/1; and
(m)
(n) Toxaphene: 0.0002 ug/1;
(14) pH: shall be normal for the waters in the area, which range between 6.0 and 9.0 except that swamp waters
may have a pH as low as 4.3 if it is the result of natural conditions;
(15) Phenolic compounds: only such levels as shall not result in fish -flesh tainting or impairment of other best
usage;
(16) dL Polychlorinated biph, gills (total of all PCBs and congeners identified): 0.001 ug/1;
(17) Radioactive substances:
(a) Combined radium-226 and radium-228: the average annual activity level (based on at least one
- sample collected per quarter) for combined radium-226 and radium-228 shall not exceed five
picoCuries per liter;
(b) Alpha Emitters: the average annual gross alpha particle activity (including radium-226, but
excluding radon and uranium) shall not exceed 15 picoCuries per liter;
(c) Beta Emitters: the average annual activity level (based on at least one sample collected per
quarter) for strontium-90 shall not exceed eight picoCuries per liter; nor shall the average annual
gross beta particle activity (excluding potassium-40 and other naturally occurring radionuclides)
exceed 50 picoCuries per liter; nor shall the average annual activity level for tritium exceed
20,000 picoCuries per liter;
(18) Temperature: not to exceed 2.8 degrees C (5.04 degrees F) above the natural water temperature, and in no
case to exceed 29 degrees C (84.2 degrees F) for mountain and upper piedmont waters. and 32 degrees C
(89.6 degrees F) for lower piedmont and coastal plain Waters; the temperature for trout waters shall not be
increased by more than 0.5 degrees C (0.9 degrees F) due to the discharge of heated liquids, but in no case
to exceed 20 degrees C (68 degrees F);
(19) (Toluene: 11 ug/1 or 0.36 ug/1 in trout classified waters;
(20) Trialkylt compounds: 0.07 ug/1 expressed as tributyltin;
(21) Turbidity the turbidity in the receiving water shall not exceed SO-Nepfi"elo em tric Turbidity Units(NTU) .J
{streams not designated as trout waters and-10 NTU in streams, lakes, or reservoirs designated as trout
waters; for lakes and reservoirs not designated as trout waters, the turbidity shall• not exceed 25 NTU; if
turbidity exceeds these levels due to natural background conditions, the existing turbidity level shall not be
increased. Compliance with this turbidity standard can be met when land management activities employ
Best Management Practices (BMPs) [as defined by Rule .0202 of this Section] recommended by the
Designated Nonpoint Source Agency [as defined by Rule .0202 of this Section]. BMPs shall be in full
compliance with all specifications governing the proper design, installation, operation, and maintenance of
such BMPs;
_(22)-_—Action Levels for Toxic Substances Applicable to NPDESPermits J
(a) Copper, dissolved, chronic: 2.7 ug/1;
(b) Silver, dissolved, chronic: 0.06 ug/1;
(c) Zinc, dissolved, chronic: 36 ug/1; and
(d) Chloride: 230 mg/1;
The hardness -dependent freshwater action levels for copper and zinc, provided here for illustrative
purposes, corresponds to a hardness of 25 mg/l. Copper and zinc action level values for other instream
hardness values shall be calculated per the chronic equations specified in Item (11) of this Rule and in
Table A: Dissolved Freshwater Standards for Hardness -Dependent Metals. If the action levels for any of
the substances listed in this Item (which are generally not bioaccumulative and have variable toxicity to
aquatic life because of chemical form, solubility, stream characteristics or associated waste characteristics)
are determined by the waste load allocation to be exceeded in a receiving water by a discharge under the
specified 7Q10 criterion for toxic substances, the discharger shall monitor the chemical or biological

effects of the discharge; efforts shall be made by all dischargers to reduce or eliminate these substances
from their effluents. Those substances for which action levels are listed in this Item shall be limited as
appropriate in the NPDES permit if sufficient information (to be determined for metals by measurements of
that portion of the dissolved instream concentration of the action levels parameter attributable to a specific
NPDES permitted discharge) exists to indicate that any of those substances may be a causative factor
resulting in toxicity of the effluent.
History Note: Authority G.S. 143-214.1; 143-215.3(a)(1);
Eff. February 1, 1976;
Amended Eff. January 1, 2015; May 1, 2007; April 1, 2003; August 1, 2000; October 1, 1995; August 1,
1995; April 1, 1994; February 1, 1993.
15A NCAC 02B .0212 FRESH SURFACE WATER QUALITY STANDARDS FOR CLASS WS-I WATERS
The following water quality standards apply to surface waters within water supply watersheds classified as WS-I. Water
quality standards applicable to Class C waters as described in Rule .0211 of this Section shall also apply to.Class WS-I
waters.
(1) The best usage of WS-I waters shall be as follows: a source of water supply for drinking, culinary, or
food -processing purposes for those users desiring maximum protection of their water supplies; waters
located on land in public ownership; and any best usage specified for Class C waters;
(2) The conditions related to the best usage shall be as follows: waters of this class are protected water
supplies within essentially natural and undeveloped watersheds in public ownership with no permitted point
source dischargers except those specified in Rule .0104 of this Subchapter; waters within this class shall be
relatively unimpacted by nonpoint sources of pollution; land use management programs are required to
protect waters from nonpoint source pollution; the waters, following treatment required by the Division,
shall meet the Maximum Contaminant Level concentrations considered safe for drinking, culinary, and
food -processing purposes that are specified in the national drinking water regulations and in the North
Carolina Rules Governing Public Water Supplies, 15A NCAC 18C .1500. Sources of water pollution that
preclude any of these uses on either a short-term or long-term basis shall be considered to be violating a
water quality standard. The Class WS-I classification may be used to protect portions of Class WS-II, WS-
III, and WS-IV water supplies. For reclassifications occurring after the July 1, 1992 statewide
reclassification, the more protective classification requested by local governments shall be considered by
the Commission when all local governments having jurisdiction in the affected area(s) have adopted a
resolution and the appropriate ordinances to protect the watershed or the Commission acts to protect a
watershed when one or more local governments has failed to adopt necessary protection measures;
(3) Quality standards applicable to Class WS-I Waters shall be as follows:
(a) MBAS (Methylene -Blue Active Substances): not greater than 0.5 mg/1 to protect the aesthetic
qualities of water supplies and to prevent foaming;
(b) Nonpoint Source Pollution: none shall be allowed that would adversely impact the waters for use
as a water supply or any other designated use;
(c) Organisms of coliform group: total coliforms not to exceed 50/100 ml (MF count) as a monthly
geometric mean value in watersheds serving as unfiltered water supplies;
(d) Chlorinated phenolic compounds: not greater than 1.0 ug/1 to protect water supplies from taste
and odor problems from chlorinated phenols;
(e) Sewage, industrial wastes: none shall be allowed except those specified in Item (2) of this Rule or
Rule .0104 of this Subchapter;
(f) Solids, total dissolved: not greater than 500 mg/1;
(g) Total hardness: not greater than 100 mg/1 as calcium carbonate (CaCO3 or Ca + Mg);
(h) Toxic and other deleterious substances:
(i) Water quality standards (maximum permissible concentrations) to protect human health
through water consumption and fish tissue consumption for non -carcinogens in Class
WS-I waters:
(A) Barium: 1.0 mg/1;
(B) Chloride: 250 mg/1;
(C) Nickel: 25ug/1;
(D) Nitrate nitrogen: 10.0 mg/I;

ATTACHMENT A — LIMITATIONS: AND 1VIONITORING REQUIREMENTS
PPI 001— WWTF Effluent
Permit Number: WQ0004268
Version: 3.0
EFFLUENT CHARACTERISTICS
EFFLUENT LIMITS
MONITORING REQUIREMENTS
:PCS
Code
01002'
00310
01027
Parameter Description
Arsenic, Total (as As)
BOD, 5-Day (20 °C)
Cadmium, Total (asCd)
Units of
Measure
mg/L
mg/L
mg/L
Monthly
Average
Monthly DailyMinimum gaily Maximum
Geometric Mean
'Measurement
Frequency
3 x Year'
Monthly
3 x Year'
Sample
Type
Grab
Grab
Grab
00916
Calcium, Total (as Ca)
mg/L
Monthly
Grab
00940
Chloride (as C1)
mg/L
3 x Year'
Grab
01034
Chromium, Total (as Cr)
mg/L.
3 x Year'
Grab
31616
Coliform, Fecal MF,1VI-FC Broth, 44. °C
#/100 mL
Monthly
Grab
50050
01051
00927
71900
Flow, in Conduit or thru Treatment Plant
Lead, Total (as Pb)
Magnesium, Total (as Mg)
Mercury, Total (as Hg)
GPD
mg/L
mg/L
mg/L
415;000
Continuous
3 x Year'
3 x Year'
3 x Year
Recorder
Grab,
Grab.
Grab
01067
Nickel, Total (as Ni)
mg/L
'3 k Year'
Grab
00610.
Nitrogen, Ammonia Total. (as N)
mg/L
Monthly
Grab
00625
Nitrogen, Kjeldahl, Total (as N)
ing/L
Monthly,
Grab
00620 '
Nitrogen, Nitrate Total (as N)
mg/L
Monthly
Grab
00600
Nitrogen, Total (as N).
mg/L
Monthly
Grab -
00400
pH.
su
Per Event
Grab
00665
Phosphorus, Total (as P)
mg/L
Monthly
Grab
WQ09C
Plant Available Nitrogen,; Concentration
mg/L
Monthly
Calculated
00929
Sodium, Total (as Na)
mg/L
Monthly
Grab
00931
Sodium Adsorption Ratio
ratio
Monthly
Calculated
70300
00530
01092
Solids, Total Dissolved— 180 °C
Solids, Total Suspended,
Zinc, Total (as Zn)
mg/L
mg/L
mg/L
1. 3 -x Year sampling shall be conducted in March, July and November.
3 x Year'
Monthly
3xYear'
Grab
Grab
Grab
WQ0004268 Version 3.0
Attachment A
Page 1 of 1

ATTACHMENT C — GROUNDWATER MONITORING AND LIMITATIONS Permit Number: WQ0004268
Monitoring wells: MW-1, MW-2, MW-3, MW-4, R-1, R-2A, R 3, R 4, R-5A, R 6, R 7, R-8 and R-9
Version: 3.0
GROUNDWATER CHARACTERISTICS
GROUNDWATER STANDARDS
MONITORING REQUIREMENTS
PCS Code
Parameter Description
Daily Maximum
Frequency Measurement
Sample Type
Footnotes
00680
Carbon, Tot Organic (TOC)
mg/L
3 x Year
Grab
1, 6
00940
Chloride (as Cl)
250
mg/L
3 x Year
Grab
1
31616
Coliform, Fecal MF, M-FC Broth, 44.5 °C
#/100 mL
3 x Year
Grab
1
00610
Nitrogen, Ammonia Total (as N)
1.5
mg/L
3 x Year
Grab
1
00620
Nitrogen, Nitrate Total (as N)
10
mg/L
3 x Year
Grab
1
00400
pH
6.5-8.5
su
3 x Year
Grab
1, 2
00665
Phosphorus, Total (as P)
mg/L
3 x Year
Grab
1
70300
Solids, Total Dissolved - 180 °C
500
mg/L
3 x Year
Grab
1
00945
Sulfate, Total (as SO4)
250
mg/L
3 x Year
Grab
1
82546
Water Level, Distance from measuring point
feet
3 x Year
Calculated
I, 2, 3
1. 3 x Year monitoring shall be conducted in March, July & November; Annual monitoring shall be conducted every November.
2. The measurement of water levels shall be made prior to purging the wells. The depth to water in each well shall be measured from the surveyed point on the top of the casing. The measurement of
pII shall be made after purging and prior to sampling for the remaining parameters.
3. The measuring points (top of well casing) of all monitoring wells shall be surveyed to provide the relative elevation of the measuring point for each monitoring well. The measuring points (top of
casing) of all monitoring wells shall be surveyed relative to a common datum.
4. If TOC concentrations greater than 10 mg/L are detected in any downgradient monitoring well, additional sampling and analysis must be conducted to identify the individual constituents comprising
this TOC concentration. If the TOC concentration as measured in the background monitor well exceeds 10 mg/L, this concentration will be taken to represent the naturally occurring TOC
concentration. Any exceedances of this naturally occurring TOC concentration in the downgradient wells shall be subject to the additional sampling and analysis as described above.
5. Monitoring wells shall be reported consistent with the nomenclature and location information provided in Figure 1 and this attachment.
WQ0004268 Version 3.0 Attachment C Page 1 of 1

0<0rn
0 0 , a;
F
R
a
'1
'1
i0
a
EXPLANATION
6 Permanent Compliance Well
Abandoned Compliance Well
Issued Permit Compliance Boundary
Issued Permit Review. Boundary
- .Permitted Irrigation Zones
500 -250 0 , ;500 1,000 1,500 , 2,000
Basemp: Drawing A30701: Owens Surveying
Feet
wc. _ 'tea'= ••
R=2A•
141
Wel No.
MW-1
Status
. Active
Fasting
Northing
Top Casing,
,Elevation
Land.
Surface ,
Elevation
Ord Wet
No.
MW-1
NAD83 Ft.
4231,662"
NAD83 Ft.
449,058
NAVD88 Ft.
131.63
NAVD88 FL
129,55
MW-2
Active,
2,232,183
.448,411
111.90
110.74
MW-2
MW-3
Active
2,233 475
447,089
91.18
89.53
' MW3 .
MW-4
Active
2,234,885
449,861
133.75.
131.18
'MW-4.
R-1
Active
2,228,891
. 445,636
90.47
• 87.20
CW-7
R 2
Abandoned
2,229,383
' • 445,196
' 89.09.
86.05
• CW-6
R-2A
Active.
2,229,518
445,191
88.32
85.02
None •
R 3'
• Active
• 2,230,053
444,685
89.96
86.98
CW-5 '
R-4
Active
.2,229,492
' 443,682,
92.03
88.52
CW-4-
R-5
Abandoned.
2,227,878
' 443,978
97.62
95A2
CW-1E
• R-5A
Active
2,227,812
..444,03T"
95.53
93.48.
None
R-6
Active
2,226,727
444,187
• 95,81
• 93.22
CW-3
R-7
Active
• 2,226,250
' '444,901
' ' 107,38
•104.36
CS-8 •
R-8
Active '
. 2,226,467
• 446,134
• 121:68.
118.65
CW-1
R-9.
Active
2,228,097
• 445,830
.100.00
. 97.07
None

15A NCAC 02B .0213 REVISIONS TO DISSOLVED OXYGEN STANDARDS
History Note:
Authority G.S. 143-214.1;
Eff December 14, 1978;
Amended Eff. July 1, 1988;
Repealed Eff October 1, 1989.
15A NCAC 02B .0214 FRESH SURFACE WATER QUALITY STANDARDS FOR CLASS WS-II WATERS
The following water quality standards apply to surface waters within water supply watersheds that are classified WS-II. Water
quality standards applicable to Class C waters as described in Rule .0211 of this Section also apply to Class WS-II waters.
(1) The best usage of WS-II waters are as follows: a source of water supply for drinking, culinary, or
food -processing purposes for those users desiring maximum protection for their water supplies where a
WS-I classification is not feasible and any best usage specified for Class C waters;
(2) The conditions related to the best usage are as follows: waters of this class are protected as water supplies
which are in predominantly undeveloped watersheds and meet average watershed development density
levels as specified in Sub -Items (3)(b)(i)(A), (3)(b)(i)(B), (3)(b)(ii)(A) and (3)(b)(ii)(B) of this Rule;
discharges which qualify for a General •Permit pursuant to 15A NCAC 2H .0127, trout farm discharges,
recycle (closed loop) systems that only discharge in response to 10-year storm events and other stormwater
discharges are allowed in the entire watershed; new domestic and industrial discharges of treated wastewater
are not allowed in the entire watershed; the waters, following treatment required by the Division of
Environmental Health, shall meet the Maximum Contaminant Level concentrations considered safe for
drinking, culinary, and food -processing purposes which are specified in the national drinking water
regulations and in the North Carolina Rules Governing Public Water Supplies, 15A NCAC 18C .1500.
Sources of water pollution which preclude any of these uses on either a short-term or long-term basis shall
be considered to be violating a water quality standard. The Class WS-II classification may be used to
protect portions of Class WS-III and WS-IV water supplies. For reclassifications of these portions of Class
WS-III and WS-IV water supplies occurring after the July 1, 1992 statewide reclassification, the more
protective classification requested by local governments shall be considered by the Commission when all
local governments having jurisdiction in the affected area(s) have adopted a resolution and the appropriate
ordinances to protect the watershed or the Commission acts to protect a watershed when one or more local
governments has failed to adopt necessary protection measures;
(3) Quality standards applicable to Class WS-II Waters are as follows:
(a) Sewage, industrial wastes, non -process industrial wastes, or other wastes: none shall be allowed
except for those specified in either Item (2) of this Rule and Rule .0104 of this Subchapter; none
shall be allowed that have an adverse effect on human health or that are not effectively treated to
the satisfaction of the Commission and in accordance with the requirements of the Division of
Environmental Health, North Carolina Department of Environment and Natural Resources. Any
discharger may be required upon request by the Commission to disclose all chemical constituents
present or potentially present in their wastes and chemicals which could be spilled or be present in
runoff from their facility which may have an adverse impact on downstream water quality. These
facilities may be required to have spill and treatment failure control plans as well as perform
special monitoring for toxic substances;
(b) Nonpoint Source and Stormwater Pollution: none that would adversely impact the waters for use
as a water supply or any other designated use;
(i) Nonpoint Source and Stormwater Pollution Control Criteria for Entire Watershed:
(A) Low Density Option: development density must be limited to either no more
than one dwelling unit per acre of single family detached residential
development (or 40,000 square foot lot excluding roadway right-of-way) or 12
percent built -upon area for all other residential and non-residential development
in the watershed outside of the critical area; stormwater runoff from the
development shall be transported by vegetated conveyances to the maximum
extent practicable;
NORTH CAROLINAADMINISTRATIVE CODE
Eff Mav 1, 2007 Page 26

(3)
Quality standards applicable to Class WS-I Waters are as follows:
(a) MBAS (Methylene -Blue Active Substances): not greater than 0.5 mg/1 to protect the aesthetic
qualities of water supplies and to prevent foaming;
(b) Nonpoint Source Pollution: none shall be allowed that would adversely impact the waters for use
as a water supply or any other designated use;
(c) Organisms of coliform group: total coliforms not to exceed 50/100 ml (MF count) as a monthly
geometric mean value in watersheds serving as unfiltered water supplies;
(d) Chlorinated phenolic compounds: not greater than 1.0 ug/1 to protect water supplies from taste and
odor problems from chlorinated phenols;
(e) Sewage, industrial wastes: none shall be allowed except those specified in Subparagraph (2) of
this Paragraph or Rule .0104 of this Subchapter;
(f) Solids, total dissolved: not greater than 500 mg/1;
(g) Total hardness: not greater than 100 mg/1 as calcium carbonate;
(h) Toxic and other deleterious substances:
(i) Water quality standards (maximum permissible concentrations) to protect human health
through water consumption and fish tissue consumption for non -carcinogens in Class
WS-I waters:
(A) Barium: 1.0 mg/1;
(B) Chloride: 250 mg/I;
(C) Manganese: 200 ug/1;
(D) Nickel: 25 ug/1;
(E) Nitrate nitrogen: 10.0 mg/1;
(F) 2,4-D: 100 ug/1;
(G) 2,4,5-TP (Silvex): 10 ug/1;
(H) Sulfates: 250 mg/1;
(ii) Water quality standards (maximum permissible concentrations) to protect human health
through water consumption and fish tissue consumption for carcinogens in Class WS-I
waters:
(A) Aldrin: 0.05 ng/1;
(B) Arsenic: 10 ug/1;
(C) Benzene: 1.19 ug/1;
(D) Carbon tetrachloride: 0.254 ug/1;
(E) Chlordane: 0.8 ng/1;
(F) Chlorinated benzenes: 488 ug/1;
(G) DDT: 0.2 ng/1;
(H) Dieldrin: 0.05 ng/1;
(I) Dioxin: 0.000005 ng/1;
(J) Heptachlor: 0.08 ng/1;
(K) Hexachlorobutadiene: 0.44 ug/1;
(L) Polynuclear aromatic hydrocarbons (total of all PAHs): 2.8 ng/1;
(M) Tetrachloroethane (1,1,2,2): 0.17 ug/1;
(N) Tetrachloroethylene: 0.7 ug/1;
(0) Trichloroethylene: 2.5 ug/I;
(P) Vinyl Chloride: 0.025 ug/1.
History Note: Authority G.S. 143-214.1; 143-215.3(a)(1);
Eff. February 1, 1976;
Amended Eff. May 1, 2007; April 1, 2003; October 1, 1995; February 1, 1993; March 1, 1991; October 1,
1989.
NORTH CAROLINAADMINISTRATIVE CODE
Eff May 1, 2007 Page 25

w
(xv) Trialkyltin compounds: 0.07 ug/1 expressed as tributyltin;
(4) Action Levels for Toxic Substances:
(a) Copper: 7 ug/1;
(b) Iron: 1.0 mg/1;
(c) Silver: 0.06 ug/1;
(d) Zinc: 50 ug/1;
(e) Chloride: 230 mg/1;
If the Action Levels for any of the substances listed in this Subparagraph (which are generally not
bioaccumulative and have variable toxicity to aquatic life because of chemical form, solubility, stream
characteristics or associated waste characteristics) are determined by the waste load allocation to be
exceeded in a receiving water by a discharge under the specified low flow criterion for toxic substances
(Rule .0206 in this Section), the discharger shall monitor the chemical or biological effects of the discharge;
efforts shall be made by all dischargers to reduce or eliminate these substances from their effluents. Those
substances for which Action Levels are listed in this Subparagraph shall be limited as appropriate in the
NPDES permit based on the Action Levels listed in this Subparagraph if sufficient information (to be
determined for metals by measurements of that portion of the dissolved instream concentration of the Action
Level parameter attributable to a specific NPDES permitted discharge) exists to indicate that any of those
substances may be a causative factor resulting in toxicity of the effluent. NPDES permit limits may be
based on translation of the toxic form to total recoverable metals. Studies used to determine the toxic form
or translators must be designed according to "Water Quality Standards Handbook Second Edition"
published by the Environmental Protection Agency (EPA 823-B-94-005a) or "The Metals Translator:
Guidance For Calculating a Total Recoverable Permit Limit From a Dissolved Criterion' published by the
Environmental Protection Agency (EPA 823-B-96-007) which are hereby incorporated by reference
including any subsequent amendments. The Director shall consider conformance to EPA guidance as well
as the presence of environmental conditions that limit the applicability of translators in approving the use of
metal translators.
For purposes other than consideration of NPDES permitting of point source discharges as described in this
Subparagraph, the Action Levels in this Rule, as measured by an appropriate analytical technique, per 15A
NCAC 02B .0103(a), shall be considered as numerical ambient water quality standards.
History Note: Authority G.S. 143-214.1; 143-215.3(a)(1);
Eff. February 1, 1976;
Amended Eff May 1, 2007; April 1, 2003; August 1, 2000; October 1, 1995; August 1, 1995; April 1, 1994;
February 1, 1993.
15A NCAC 02B .0212 FRESH.SURFACE WATER QUALITY STANDARDS FOR CLASS WS-I WATERS
The following water quality standards apply to surface waters within water supply watersheds that are classified WS-I. Water
quality standards applicable to Class C waters as described in Rule .0211 of this Section also apply to Class WS-I waters.
(1) The best usage of WS-I waters are as follows: a source of water supply for drinking, culinary, or
food -processing purposes for those users desiring maximum protection of their water supplies; waters
located on land in public ownership; and any best usage specified for Class C waters;
(2) The conditions related to the best usage are as follows: waters of this class are protected water supplies
within essentially natural and undeveloped watersheds in public ownership with no permitted point source
dischargers except those specified in Rule .0104 of this Subchapter; waters within this class must be
relatively unimpacted by nonpoint sources of pollution; land use management programs are required to
protect waters from nonpoint source pollution; the waters, following treatment required by the Division of
Environmental Health, shall meet the Maximum Contaminant Level concentrations considered safe for
drinking, culinary, and food -processing purposes which are specified in the national drinking water
regulations and in the North Carolina Rules Governing Public Water Supplies, 15A NCAC 18C .1500.
Sources of water pollution which preclude any of these uses on either a short-term or long-term basis shall
be considered to be violating a water quality standard. The Class WS-I classification may be used to protect
portions of Class WS-II, WS-III and WS-IV water supplies. For reclassifications occurring after the July 1,
1992 statewide reclassification, the more protective classification requested by local governments shall be
considered by the Commission when all local governments having jurisdiction in the affected area(s) have
adopted a resolution and the appropriate ordinances to protect the watershed or the Commission acts to
protect a watershed when one or more local governments has failed to adopt necessary protection measures;
NORTH CAROLINAADMINISTRATIVE CODE
EffMay 1, 2007 Page 24

d-
(i) Arsenic: 50 ug/1;
(ii) Beryllium: 6.5 ug/1;
(iii) Cadmium: 0.4 ug/1 for trout waters and 2.0 ug/1 for non -trout waters; attainment of these
water quality standards in surface waters shall be based on measurement of total
recoverable metals concentrations unless appropriate studies have been conducted to
translate total recoverable metals to a toxic form. Studies used to determine the toxic
form or translators must be designed according to the "Water Quality Standards
Handbook Second Edition" published by the Environmental Protection Agency (EPA
823-B-94-005a) or "The Metals Translator: Guidance For Calculating a Total
Recoverable Permit Limit From a Dissolved Criterion" published by the Environmental
Protection Agency (EPA 823-B-96-007) which are hereby incorporated by reference
including any subsequent amendments. The Director shall consider conformance to EPA
guidance as well as the presence of environmental conditions that limit the applicability
of translators in approving the use of metal translators;
(iv) Chlorine, total residual: 17 ug/1;
(v) Chromium, total recoverable: 50 ug/1;
(vi) Cyanide, 5.0 ug/1, unless site -specific criteria are developed based upon the aquatic life
at the site utilizing The Recalculation Procedure in Appendix B of Appendix L in the
Environmental Protection Agency's Water Quality Standards Handbook hereby
incorporated by reference including any subsequent amendments;
(vii) Fluorides: 1.8 mg/I;
(viii) Lead, total recoverable: 25 ug/1, collection of data on sources, transport and fate of lead
shall be required as part of the toxicity reduction evaluation for dischargers who are out
of compliance with whole effluent toxicity testing requirements and the concentration of
lead in the effluent is concomitantly determined to exceed an instream level of 3.1 ug/1
from the discharge;
(ix) Mercury: 0.012 ug/1;
(x) Nickel: 88 ug/I, attainment of these water quality standards in surface waters shall be
based on measurement of total recoverable metals concentrations unless appropriate
studies have been conducted to translate total recoverable metals to a toxic form. Studies
used to determine the toxic form or translators must be designed according to the "Water
Quality Standards Handbook Second Edition" published by the Environmental Protection
Agency (EPA 823-B-94-005a) or "The Metals Translator: Guidance For Calculating a
Total Recoverable Permit Limit From a Dissolved Criterion" published by the
Environmental Protection Agency (EPA 823-B-96-007) which are hereby incorporated
by reference including any subsequent amendments. The Director shall consider
conformance to EPA guidance as well as the presence of environmental conditions that
limit the applicability of translators in approving the use of metal translators;
(xi) Pesticides:
(A) Aldrin: 0.002 ug/1;
(B) Chlordane: 0.004 ug/1;
(C) ` DDT: 0.001 ug/1;
(D) Demeton: 0.1 ug/1;
(E) Dieldrin: 0.002 ug/1;
(F) Endosulfan: 0.05 ug/1;
(G) Endrin: 0.002 ug/1;
(H) Guthion: 0.01 ug/1;
(I) Heptachlor: 0.004 ug/1;
(J) Lindane: 0.01 ug/I;
(K) Methoxychlor: 0.03 'ug/1;
(L) Mirex: 0.001 ug/1;
(M) Parathion: 0.013 ug/1;
(N) Toxaphene: 0.0002 ug/1;
(xii) Polychlorinated biphenyls: (total of all PCBs and congeners identified) 0.001 ug/1;
(xiii) Selenium: 5 ug/1;
(xiv) Toluene: 11 ug/1 or 0.36 ug/I in trout waters;
NORTH CAROLINAADMINISTRATIVE CODE Eff Mav 1, 2007 Page 23

Barber, Jim
From: Barber, Jim
Sent: Friday, December 08,20173:43 PM
To: Pointer, Brian
Subject: ambient stations on Six Runs,Creek
Attachments: MB LLC Del Monte surface data locations four jpg
Brian;
I'm working with a permittee that is working to close a spray irrigation permit that has a large storage lagoon that may
discharge to Six Runs Creek. The permittee is going to establish two sampling points just upstream and downstream of
the lagoon to get a current picture on surface water quality. 1 would like to get data from the following two ambient
sites. The first station is Six Runs Creek at SR 1919 (Sta. # B8679500) which is not being sampled and the last hard copy
data we have in Fayetteville is from Dec. 2005. The second station is Six Runs Creek at SR 1960 (Sta. # B8725000) which
is currently being sampled. If I can, I would like to get the last three years of data for each station tohave a historical
background to compare to the data the permittee is going to have from sampling the two locations near the lagoon.
I've'provided a map for reference. Thanks for the help.
Jim Barber
Environmental Engineer
NCDEQ-DWR-WQRO
Fayetteville Regional Office
910-433-3340 voice
910-486-0707 fax
iim.barber(Wncdenr.uov
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and
may be disclosed to third parties.
' ` Go Green! Print this email only when necessary. Thank you for helping NCDENR be environmentally responsible:
*******************

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North Carohna Division of Water Resources
Central Laboratory (Water Sciences Section)
Water Sample Collection & Submittal Form
Vlsttti: r
_(optional 402
Tor
ID •
. 'II4,cation Descriptlon• ; • SIX RUNS CRK AT SR 1980 NR TAYLORS BRIDGE
Location Code. B8725000
County:.
Sampson
• DWR Region:: •
• , Owedegcaliriryj_ • • FRO
.; Collector: 14r WN1'ic.
• DWROfce: FRO
(or agency name)
River Basin: N CPF19
• Date:
101717
' Notes:
Time:
.5
Chlonnated De-chlonnated in Field
- Dissolved analysis Enter"DIS"
El Filtered in Field
in check -boxes for parameters
: Drab 0 Composite
%Method •'' I (Other
•
SampleeDeptln
•
, 01
Priority:
. AMBIENT
❑ Ambient
Routine
Compliance
COC
Emergency
❑ OA
Secchl Depth: • ,-
Water Matrbc
SURFACEWATER
❑ Surface
❑ Ground
Waste
▪ Blank
❑ Solution
Location Type
RIVERISTREAM
❑RrverlStream ❑ Lake
▪ Estuary
El
❑ Stonnwater ❑
❑ Monitonng Well ❑
❑ Effluent ❑
❑ Field Blank
Water Supply
❑ Other
Canal
Influent
Filter Blank
Tnp Blank
Collector's Comments:
login Fife: '
FRO 102017
''Lab Use Only: •
Laboriacory `' AC43083
SompieNo:
DateRecelved:
. • •
10(/$//7
Thne Re'crelved:
Received By: -
s--
•' •`
QNC Courier
Delivery' -
Method: '
❑Hand Delivered
❑Other
kmperatirre
( l)on Arrlvah i
•
I ,5
Lab Comments.
Field Parameters) I Water Temp (ol,
1?t7
Atm Press (mmHg)
Analysis Requested
-7(v'8
%Sat (%)
D0 (ppm)
glog
:end (umhos/cm)
171+3
Analysis Requested -
,H(su)
to t f
7 I Salinity (ppt)
MIC
Coliform; MF Fecal in liquid
Turbidity -
NUT
NH3 as N in liquid
NO2+NO3 as N in liquid
Phosphorus total as Pin liquid
Total K)eldahl N as N in liquid
COLIFFECMF_LIQ
TURBIDITY
NH3N_L(Q
NO2&NO3_LIQ
PHOSTOTP_LIQ
TKNN_LIQ
`J A /'')142G 64.
•
d-jrly/, ) D i�

AC43083 North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Loc. Descr.: SIX RUNS CRK AT SR 1960 NR TAYLORS BRIDGE
County: Sampson Collector: H WHITE VlsitlD 402
Region: FRO Report To FRO Location ID: B 78 25000
River. Basin CPF 9 Collect Date: 10/17121 0Priority AMBIENT
Emergency Collect Time: 11:45 Sample Matrix: SURFACEWATER
COC Yes/No Sample Depth 04 Loc. Type: RIVER/STREAM
Final Report
If this report is labeled preliminary report the results have not been validated. Do not use for Regulatory purposes.
Sample ID: AC43083
PO Number#
Date Received: 10 8/2017
Time Received: 08_00
Labworks LoginiD BPOINTER
Delivery Method NC Courior
Final Report Date: 1116/17
Report Print Date: 11 /06/2017
CAS # Analvte Name
Sample temperature at receipt by lab
Result/
PQL Qualifier
LAB
1.5
Units
°C
Method Analysis
Reference Date Validated by
10/18/17 PGAUTHIER
MIC
Coliform, MF Fecal in liquid 1 320 13441
CFU/100m1 SM'9222 D-1997 10/18/17 ESTAFFORD1
Turbidity 1.0 5.8 NTU SM 2130 B-2001 10/18/17 ESTAFFORD1
NH3 as N in liquid
NUT
0.02 0.02 mg/L as N EPA 350.1 REV 2
10/19/17 CGREEN
NO2+NO3 as N in liquid
0.02 0.32 mg/Las N EPA353.2 REV 2 10/19/17 CGREEN
Phosphorus total as P in liquid
0.02 0.20 mg/L as P EPA365.1 REV 2 10/24/07 CGREEN
Total Kjeldahl N as, N in liquid
0.2 0.83 mg/L as EPA3512 REV 10/20/17 CGREEN
WSS Chemistry Laboratory» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
°Not Detected" or°U° does not indicate the sample is analyte tree but that the analyte is not detected at or above the POL.
Page 1 of 1

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PERMIT: WQ0004268
FACILITY: Sager Creek Foods Inc - Sager Creek Vegetable Company
PARAMETER: 00610 - Nitrogen, Ammonia Total (as N)
5.0
4.5
4.0
3.5
3.0
2.5
2.0
1.5
1.0
0.5
0.0
70
761
GW59 Date

1 c e in c , u y an November.
WQ0004268 Version 3.0
Pi-fhA I!) EaPF P ts,Aw....E.W.wi. 5 ;
ATTACHMENT A — LIMITATIONS AND MONITORING REQUIREMENTS
PPI 001 — WWTF Effluent
Permit Number: WQ0004268
Version: 3.0
EFFLUENT CHARACTERISTICS
EFFLUENT LIMITS
MONITORING REQUIREMENTS
PCS
Code
Parameter Description
Units of
Measure
Monthly
Average
Monthly
Geometric Mean
Daily Minimum
•
Daily Maximum
Measurement
Frequency
Sample
Type
01002
Arsenic, Total (as As)
mg/L
A d,,
ar,..i. -
.,;*. .• ,t:- t
•.!:;::: ' , .1.. '
';'::' -:'. : • ..:.-.::
;f , :.i.,' .',., . .!:'Y .
• •-!-
.. :
3 x Year '
Grab
JF 00310
BOD, 5-Day (20 °C)
mg/L
"
' -
' : .:
• 1 : , o , , .
Monthly
Grab
01027
Cadmium, Total (as Cd)
InWL
A r•%& 1
, ..
3 x Year 1
Grab
4c-00916
Calcium, Total (as Ca)
mg/L
skir
'::: -= :'.. :,..Z:.; ..-, ,
., , .. :
', '
. _,
•
,. .
Monthly
Grab
00940
Chloride (as Cl)
mg/L
,
,...',--;. f -,:i,...;:....,:‘-
. , , .
. - ,..,
. ,...
3 x Year'
Grab
01034
Chromium, Total (as Cr)
mg/L
A
Aive,- 6
.. ;:-. ::::,.;:',,;:::
"_ -,..
:....-;,,:'!. ,._: .„ .
3 x Year 1
Grab
01616
Coliform, Fecal MF, M-FC Broth, 44.5 °C
#/100 mL
_ i)./..',:,".-Att.:-:
.'.
:
Monthly
Grab
6/50050
Flow, in Conduit or thru Treatment Plant
GPD
415,000 p
csatintrairs CUT
Recorder
01051
Lead, Total (as Pb)
mg/L
4,..,e, . tik,/,,,,.....
.).-is y. ::,.',-..,,:L-
,:y• -. -
:,:. ....::: :;.: ::: :
3 x Year 1
Grab
00927
Magnesium, Total (as Mg)
mg/L
O. ,
, •? '!. :"f'.:' '''
`, , • ,.
3 x Year I
Grab
71900
Mercury, Total (as Hg) - .
mg/L
A th, a - QJ /
. t , ,
. ,
- -. ...,..,:"
3 x Year 1
Grab
01067
Nickel, Total (as Ni)
mg/L
4 N . clrlil
:,,.. :•::.:::...,:::,:::
, . .,
. ,
3 x Year'
Grab
(41%19
lj\litrogen, Ammonia Total (a-ST-s,i)
mg/L
A
A r36 • cilif
.::•:::::*. n.:' :: ..':1:
r.' ' , .. ' ' '
,,. .. :
Moethly 3xyg
Grab
ef0665 JRNitrcigiii,-KjelOal,
Total (as Kii)
mg/L
„,,,,. 6,,..
,_.
,, .., ,
,,,-.-:;
maaftthiy 3 s yg-
Grab
,i7-00620)
'Nitic;gen'Nitrate Total (9.1)
mg/1,
"'
" f
Meittrly3x VZ
Grab
r 00600
Nitrogen, Total (as N)
mg/L
'',..:N•:.:',:,.:..'. , .,.''-',,,,'...?
,.• . : -
Monthly 3y, yit
Grab
/00400
LpH
-Phos—phorus,
su
„
_
P...e1-rwer1t3x Vfz.
Grab
00665 )
Total (as P)i
mg/L
4th3 _
10etfit, SA..
Grab
(WQ09C
Plant Available Nitrogen, Concentration
mg/L
..;;'''''';'..,.
, .., . : ,,,,
-;;,:'- ,...-
?.: e - ' ,
::::-;:l.;;
Monthly
Calculated
e-00929
)
Sodium, Total (as Na)
mg/L
: , , ,'
.,..
, :.,.:..'-‘.
...i.'" ‘- .•°!::'''
: ' :
Monthly
Grab
(00931
Sodium Adsorption Ratio
ratio
-''''''
Monthly
Calculated
70300
Solids, Total Dissolved- 180 °C
mg/L
' ;44'
' ' • ,'2 ;''
3 x Year 1
Grab
r;00530
Solids, Total Suspended
mg/L
Ari
. .„., . .... , .,
Monthly
Grab
01092
Zinc, Total (as Zn)
mg/L
A Ivt-(1
..,-, ,.... : -.:.::-;::. :::7 1 -
, . , ,.
- ,.
..",' " .- ..:::.
" .
3 x Year I
Grab
Attachment A
Page 1 of 1
A LAIN\ U