WQ0004268_2014 Annual Agronomist Report_20150227

February 27, 2015
Mr. Tony Honeycutt
NCDENR - Division of Water Quality
Aquifer Protection Section
225 Green Street, Suite 714
Fayetteville, NC 28301
RE: Sager Creek Vegetable Company (formerly dba Allens, Inc.) —Turkey, NC
Annual Agronomist Report
Dear Mr. Honeycutt:
As required under Condition 10 under Part IV of Permit No. WQ-0004268, Sager Creek
Vegetable Company (Sager Creek) is providing an Annual Agronomist Report prepared by our
consultant, Soil & Environmental Consultants, PA (S&EC).
The S&EC Report makes some recommendations for soil amendments (potassium, magnesium,
and sulfur) is some fields and resampling of soil in one area. Sager Creek is making plans to
proceed with these recommendations in the spring.
Please let us know if you have any questions or concerns. Thank you!
Sincerely,
Sager Creek Vegetable Company
Laura J. Mushinski, CHMM
Director — Environmental Quality
cc: Reid Wells, Sager Creek —Turkey
Warren Wojiski, Sager Creek —Turkey
[phone] • 305 East Main Street • PO Box 250 • Siloam Springs AR 72761-0250 • www.sagercreekveggies.com

S&
EC
Soil & Environmental Consultants, PA
8412 Falls of Neuse Road, Suite 104, Raleigh, NC 27615 • Phone: (919) 84C6-5900 ! Fax: [phone]
sandec.com
February 24, 2015
Project #10977.S10
Sager Creek Vegetable Company
Attn: Laura Mushinski
PO Box 250
Siloam Springs, AR 72761
Re: Annual Agronomist Report for Wastewater Irrigation Spray Fields Located at Sager Creek
Vegetable Company (Formally Aliens, Inc: Plant #7) —Sampson County, NC.
I. Introduction
Soil & Environmental Consultants, PA, (S&EC) has completed an annual agronomic
evaluation for the continued operation of the spray irrigation fields for the site referenced
above. This report addresses the permit conditions set forth by NC-DWQ permit number
WQ0004268 concerning the annual agronomic evaluation for each spray field currently in
operation. The purpose of this report is to evaluate current site management practices and
agronomic conditions that contribute to the ability of the established crops to assimilate
nutrients in an efficient manner. As part of the study, S&EC evaluated irrigation zones 1-18
(and 18A) located approximately 2 miles southwest of the existing canning facility on Rowan
Road as well as Zones A-D, located directly south and southwest of the facility. Fieldwork
forthis-current-studylwas. cornpetedin:Febniary 2015 by NC Licensed Soil Scientist Ricky
Pontello.
II. Evaluation Methods and Observations
In order to accommodate high rates of wastewater application, Coastal bermudagrass serves
as the warm season receiver crop. Coastal bermudagrass, a hybrid bermudagrass variety, is a
wann season perennial that grows quickly in the summer months and has a high capacity to
assimilate plant nutrients, making it well -suited for wastewater disposal applications. Since
bermudagrass goes dormant in the late fall, wintertime wastewater application is
accommodated by over -seeding the bermudagrass. with winter annual ryegrassor oats. ~ s dr
on interviei s-with site m. gers, ay is cut; baled and removed off -site on an:_`asvne
S&EC traversed the individual spray zones and observed current site management practices as
well as current cropping conditions. At the time of the evaluation, S&EC observed that Zones
1-18 and Zones A, B and C had actively growing ryegrass interspersed with various weeds.
-Zo e D is a seasonal field, so the bermudagrass was dernnant at tlhe time: ofinspectior. S&EC
oe,‘

observed-a-few-areaswhere bare spots -are present in Zone C and in Zones l8: In Zone -48
Zone t;, ryegrass yellow_appearancc on..the-tips Inter-views-with_field
" g p_P gr� p
managers revealed"that�the3%e11Q vrn than eared in the, ye ass-was�also- resentin the
bermudagrass in-Summer-2014; 1thou7i to -a -lesser extenta
At the time of the field visit, S&EC observed localized" areas of ponding across the site.
However, it should be noted that significant snowmelt largely contributed to the saturated
conditions. S&EC did not observe significant signs of runoff from the fields (i.e. gullies,
drainage patterns, etc.). In addition, S&EC observed that vegetated buffers were well -
maintained around each spray field.
Sager Creek Vegetable Company provided S&EC with soil .fertility laboratory data for all
irrigation zones. In irrigation Zones A-D and 1-18, soil samples were collected by Crop
Production Services and analyzed by Waters Agricultural Laboratories, Inc. Soil fertility lab
analyses results are included in Attachment 1 for reference. Monthly and annual nitrogen
loading rates for individual spray zones were provided to S&EC by the client`-§ EC -used
these figures -to verify annual-nitrogenwloing rates are within permit -limits -set forth for
individual irrigation zone
III. Soil Sample Results and Recommendations
According to the nitrogen loading data provided to S&EC, the application rates for each zone
appear to be within permit limits, while also providing adequate plant available nitrogen
(PAN) for Coastal bermudagrass and winter ryegrass/oats production.
Based on a review of the soil sample lab results, the soils at this site generally have adequate
soil fertility conditions to support growth of bermudagrass and annual winter ryegrass with a
few exceptions.,As noteTin`the soil`fertilitytest results, curt_ent_soiLtestpotassiwn_(K)- else
in Zones-l=1"3`are categorized as "Lad would benefit fr m fertilizer-K additions�?�S&E j
ceeondrthat fertilizer a j hcations if K-be made afthe re ate Of 100 ib K2O/air°e to
Ries 1, 2, 3A, 3B;4, 5 and 13 to ensure sufficient K fertility. In addition,_1801b
cKzO/acre-should-be-appliedli Zones 6:12. Y
Ai February 2014, S&EC observed-someyelliAVi g chlorosis) of the winter oats Burin
fie1d1 isit. In order to a ine-if the -yellowing was a nutrient -induced deficiency,
vegetative leaf samples were collected and analyzed by A&L Eastern Laboratories
(Attachment 2). Results'indicathat he -submitted -leaf -sample -showed -a -deficiency implant
sulfur:--Soil-sam les-from- Oct ober2D14indicate-that soil magnesium -(Mg) and-sul�fur(S)
levels remain -low in some areas, S&EC recommends that fertilizer ap lications_of
MgSO-be-ntede at;the rate of 45 I1Zacre to Zones 4-12 to elevat se oil'magnesium-an
{sulfur _Vets: or the remaining zones, soil phosphorus, potassium, calcium and magnesium
are present at levels sufficiently high to support the wastewater receiver crops.
According to the soil sample data, soil pH is slightly higher than optimal in Zones C, D, 1,
3A, 5, 6, 7, 9, 10, 14, 15 and 18A, but does not warrant remedial action at this time. Soil pH
values for these zones varied from 7.3-7.5. Because maintaining a pH of 6.0-7.0 is important
Page 2 of 5

for ensuring optimal nutrient availability, soil pH should be monitored on an annual basis.
[Since soils withpHiaiues.iaboy"_e.8 ican-lead-to-micro u rent (i C Zn)-deficiencies,
fti,tureeleme ital sulfa addiiions'would.be,appropriate to low` :ei he.soil pH if values -ever
exxceedt 8 0/ An ap licattiono f 100 1-ZO lbs S°7acre_wouldbeYs f cent to acAfy the_soil-to-
target'Hp 9:7:0-and-wouldliave the added benefit of adding' sulfur to.�thhe_soi1. In order to
Abe effective, sulfur applications rnu"st also be mcorporated by disking or other means. Since
the acidification process is mediated by soil bacteria, total reaction time could range from a
few weeks to several months, depending on the soil temperature. Generally, soil temperatures
must be higher than 50° F for the microbial transformation of S to sulfuric acid.
Since the wastewater source has an elevated sodium adsorption ratio (SAR)(there is a slight
risk of developing sodium related problems in the soils, particii1atlyin zo ere soli pHis)
C7 S or above.j Soils with pH values above 8.5 and with high —levels of soil sodium are
classified as sodic soils, which"can have major limitations to the surface infiltration_capacity
of the soil. ccording to the soil fertility analysis, the soil exchangeable_sodium percentage
[(ESP) for the fields ranges from 0 to 16% (Ta61e 1). Ierigati Q e_Z.is s1i A above°the,
action Ievel (>15%)-for-sodic soil remediation. S&EC recomurensls_collectiug-and"
�analyzirtg additions I soil samples, ondthis-field to. confirm_whether_or.not_elev to ed_levels
Cofsodi'umatruly-exis If the additional samples confirm an ESP above 15%, additional
remedial action should be taken by applying gypsum (CaSO4) to the surface soil horizons in
order to prevent the development of sodic conditions. application rate of 800-to=1 000-1b
CaSO Id -be appropriate_to reduce soaum levels in the soil:�In adciiton by following -the-,
abovestated recommendation of.applying 45.1bMgSO4/ac to Zone 7, the -magnesium wily
_elp-tocounteract'the negativezffects,of sodium saturation.in-the-soil] S&EC recommends
that annual soil samples should continue to include an analysis of Exchangeable Sodium
Percentage (ESP) to monitor sodium levels.
Zones A-D and Zones 1-18 are all categorized as "Very High" in teens of soil phosphorus.
An index value of "Very High" indicates that there will be no crop yield response with
additional P applications. Although applying additional phosphorus to these spray areas does
not pose any agronomic issues, the high soil P levels may pose an environmental conceal if
significant runoff and/or, soil erosion occurs. Considering the current cover crops and their
beneficial erosion control properties, as well as stream and waterway buffers, additional
wastewater-P application should not pose a high risk of P-loss. However, irrigation schedules
should be closely monitored to avoid over -saturating irrigation zones, which could lead to
excessive runoff.
Page 3 of 5

Table 1. Approximate Exchangeable Sodium Percentage (ESP) for all irrigation zones.
Irrigation Zone
Exchangeable sodium % (ESP)
A
3.4
B
3.7
C
2.4
D
8.7
1
5.6
2
5.3
3A
•<-9;7
3B
8.2
4T0.4.h
5
6.5
6
4.7
7
(-16A
8
1.7
9
r11,1--- ,,
10
6.0
11
3.0
12
4.3
13
0.0
14
2.4
15
1.5
16
4.0
17
0.7
18
2.2
1BA
2.3
Crop Management Considerations
[There were some bares op its that ere_obser !ed_across the site that sheuld-be reseede ,a�v�tih
ber nudagrass.' Weeds should also be controlled using appropriate selective herbicides.
poastal-bermudagr sa sh u1d be u 416:5 weeks -or -when igrow t1Kinchesja11
Once beimu ak ass is overseeded with winter rye or oats in the fall, grass should be cut to a
height of 3 inches or less to encourage rye estabiishment.LSB EC re oc nmmends-that-fall 7
'everseedmg should be accomph'shedb3 dfilling he seed instead of broadcastingio encourage
biter �eed/soil contact and protection fromearly frosts.._ the early spring, approximately
two weeks before bermudagrass is expected to turn green, mowing height should be reduced
to 3/ to 1-inch to alp l bermudagrass to recover and out -compete the winter rye. —Since
:hermudageassais very-mtelerant to s ade; latespring-cutting-of winter- -rye-shoulbided
waftmay severel limitbermudagra ss recovery:
Page 4 of 5

If not already in place, a harvest management plan should be integrated into the current
irrigation scheme in order to maximize the nutrient removal capabilities of the cover crops
and minimize the "downtime" required by drying, cutting, baling and removal of the hay.
arvesting grass as_ silage l be-a-more-efficient-metthod=forcrop-removal-b-y reduc rigthe1
timerequired`for hary ng a ictivities.) ( $ f !/)
S&EC is pleased to serve you in this manner. If you have any questions or require additional
information then please give us a call.
Ricky Pontello
NC Licensed Soil Scientist
Mark Allen
ARCPACS Certified Professional Soil
Scientist
Page 5 of 5

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
OMICROBAC® RIoeilS@ScVe-5C%)
Fayetteville Division
Certificate of Analysis
Project: Wastewater Sample - Mthly
Date Reported: 01/22/15
Date Received: 12/15/14
• ate Sampled: 12/•1504.,
Samp ed By: Wells
Effluent sample
K4L0481-01
Analyte •
Result
Units
Analyzed Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Sbdtu ffi5rr
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
BOD
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Total Suspended Solids
Total Kjeldahl Nitrogen
1.17
1520
0.906
<0.0500
10.9
340
32.4
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Phosphorus, Total 1.97
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
pH Units
mg/L
mg/L
12/19/14 16:06
12/22/14 12:44
12/29/14 12:35
12/15/14 11:25
12/19/14 16:45
12/19/14 16:45
12/30/14 21:42
12/15/14 16:20
12/17/14 09:00
12/30/14 09:08
AG
AG
JAO
DSK
NCH
NCH
BKS
DSK
SW
SW
mg/L 12/30/14 10:18 DCM
QC Batch Run - (Microbac Laboratories, Inc - Cbicagoland)
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
SM 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 2540 D-1997
SM 4500-Norg C-1997
E365.4
Analyte
. Result
Units
Source
RPD Limit
Calcium
Sodium
55.9
35.5
mg/L
mg/L
•14L0692
14L0692
QC Batch Run - (Microbac Laboratories, Inc - Fayetteville)
1.12
0.814
20
20
Analyte
Result
Units
Source
RPD Limit
Nitrate as N
Nitrite as N
Nitrite as N
Nitrite as N
Nitrate as N
Total Suspended Solids
Nitrate as N
BOD
11.2 mg/L
0.247 mg/L
0.604 mg/L
0.156 mg/L
19.0 mg/L
13.2 mg/L
1.69 mg/L
1520 mg/L
K4L0518
K4L0616
K4L0527
K4L0518
K4L0527
K4L0440
K4L0616
K4L0481
24
8
1
0.2
0.09
6
0.2
0
Microbac Laboratories, Inc.
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com
200
200
200
200
200
5
200
20
Page.1. of 3.

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
Certificate of Analysis
• Project: Wastewater Samples - Mthly/3yr
Date Rd: 11/21/14
Date Received: 11/03/14
Sampled; 11 0301
Sampled By: Poythress
Effluent, grab
K4K0039-01
Analyte
Result
Units
Analyzed Analyzed By
Method
Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Cadmium
111 �a1"cium
.Lead
agn"`esiuth
Sodium
_ Mercury
<0.0020
,23
<0.0075
1'60,
<0.00020
Analyzed by: Microbac Laboratories, Inc. - Fayetteville "
Ammonia as N <0.100
Arsenic <0.00200
BOD 87.9
Ct1orid 167
Chromium <0.002
Nickel 0.0500
Nitrate as N 0.302
Nitrite as N <0.0500
Plant Available Nitrogen 7.55
Phosphorus, Total
Total Dissolved Solids
Total Suspended Solids
Total Kjeldahl Nitrogen
Zinc
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
pH Units
7.2 mg/L
788 mg/L
356 mg/L
24.0 mg/L
0.0950 mg/L
11/11/14 12:35
11/11/14 12:35
11/11/14 12:35
11/11/14 12:35
11/11/14 12:35
11/10/14 12:20
11/07/14 09:37
11/13/14 09:38
11/05/14 10:14
11/05/14 08:55
11/20/14 20:17
11/20/14 15:43
11/05/14 08:55
11/05/14 08:55
11/04/14 17:05
11/11/14 08:20
11/07/14 08:00
11/04/14 09:20
11/05/14 15:00
11/11/14 08:04
11/20/14 16:54
AG
AG
AG
AG
AG
AG
SW
JAW
DSK
NCH
JAW
JAW
NCH
NCH
JMO
DSK
JAO
JAO
SW
SW
JAW
QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland)
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 245.1 Rev 3.0
SM 4500 NH3 C-1997
SM 3113 B-2004
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
SM 3113 B-2004
SM 3111 B-1999
EPA 300.0, Rev. 2.1 (1993) B
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 4500-P F-1999
SM 2540 C-1997
SM 2540 D-1997
SM 4500-Norg C-1997
SM 3111 B-1999
Analyte Result
Units
Source
RPD Limit
Mercury
Sodium
Magnesium
Lead
0.00186
194
61.4
2.01
mg/L
mg/L
mg/L
mg/L
K4K0039
14K0220
14K0220
14K0220
1.19
0.463
0.0978
0.798
20
20
20
20
Page 1 of 4

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393 .
4r1
MICROBAC®
Fayetteville Division
Certificate of Analysis.
Project: Wastewater Sample - Mthly
Date Reported: 11/14/14
Date Received: 10/22/14
` DateySamwmra 19fi22%1'4
Sampled By: Wells
Effluent, Grab
K4J0688-01 •
Analyte
Result
Units
Analyzed Analyzed By
Method •
Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Calciumt
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
BOD
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus, Total
Total Suspended Solids
Total Kjeldahl Nitrogen
13.7
76.0
<0.0500
<0.0500
10.2
C7.2-3
9.9
191
24.4
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
10/27/14 14:52
10/27/14 14:52
10/29/14 15:47
10/22/14 15:10
10/23/14 17:11
10/23/14 17:11
11/04/14 18:17
10/27/14 13:30
10/31/14 07:40
10/23/14 09:45
10/24/14 07:32
AG
AG
SW
DSK
NCH
NCH
BKS
DSK
JAO
JAO
SW
QC Batch Run - (Microbac Laboratories, Ina - Chicagoland)
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
SM 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2:1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 4500-P F-1999
SM 2540 D-1997
SM 4500-Norg C-1997
Analyte
Result
Units
Source
RPD Limit
Calcium.
Sodium
66.3 mg/L
36.6 mg/L
QC Batch Run -
14J1009
14J1009
Microbac Laboratories, Inc - Fayetteville)
1.41
2.60
20
20
Analyte
Result
Units
Source
BOD
Nitrite as N
Total Suspended Solids
Nitrate as N
Total Suspended Solids
Anunonia as N
Ammonia as N
Phosphorus, Total
Total Kjeldahl Nitrogen
785 mg/L
8.45 mg/L
25.2 mg/L
1.21 mg/L
46.9 mg/L
ND mg/L
2.43 mg/L
K4J0595
K4J0603
K4J0677
K4J0603
K4J0702
K4J0732
K4J0732
5.8 mg/L K4J0834
375 mg/L K4J0549
Microbac Laboratories, Inc.
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1 910.864.8774 f J www.microbac.com
RPD Limit
2
0.5
5
1
10
46
3
10
20
200
5
200
5
20
20
10
20
Page 1_of'3 :.I

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
(MICROBAC@
Fayetteville Division
Certificate of Analysis
Project: Wastewater Sample - Mthly
Date Reported: 10/12/14
Date Received: 09/24/14
DateSampl' a 09/24/14
Sampled By: Wells
Effluent sample, grab
K4I0735-01
Analyte
Result
Units Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
*atcium
ALB
Sodium. 60
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
BOD
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus, Total
Total Suspended Solids
Total Kjeldahl Nitrogen
9.13
70.8
0.724
0.642
14.9
12
176
39.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
09/29/14 15:39
09/29/14 15:39
10/01/14 15:30
09/24/14 15:45
09/25/14 10:30
09/25/14 10:30
10/03/14 16:34
09/29/14 10:45
09/30/14 08:25
09/25/14 07:40
09/30/14 08:02
AG
AG
SW
DSK
JAW
JAW
BKS
DSK
JAO
JAO
SW
QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland)
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
SM 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 4500-P F-1999
SM 2540 D-1997
SM 4500-Norg C-1997
Analyte
Result
Units
Source
RPD Limit
Calcium
Sodium
64.3
36.2
mg/L
mg/L
14I1151
14I1151
QC Batch Run - (Microbac Laboratories, Inc -Fayetteville)
0.295
0.0828
20
20
Analyte
Result
Units
Source
RPD Limit
BOD
Nitrite as N
Total Suspended Solids
Nitrate as N
Total Suspended Solids
Total Suspended Solids
Phosphorus, Total
Phosphorus, Total
Ammonia as N
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
K4I0655
K4I0725
K4I0706
K4I0725
K4I0744
K410757
K4I0695
mg/L K4I083 8
mg/L K4I0672 0
Microbac Laboratories, Inc.
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com
0
2
2.08
ND
47.7
0.702
128
9.50
5.0
0.95
1.22
21
3
4
2
20
200
5
200
5
5
10
10
20
Page.1 of 3

Aliens, Inc \
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
(}MICROBAC'
Fayetteville Division
Certificate of Analysis
Project: Wastewater Sample - Mthly
Effluent sample, grab
K4H0833-01
Date Reported: 09/12/14
Date Received: 08/26/14
Date Sampled: 08126/.14
Sampled By: Wells
Analyte
Result
Analyzed by: Miaobac Laboratories, Inc. - Qiicagoland
rale111117)
Sodium
7
0b
Units Analyzed Analyzed By Method Qualifier •
mg/L 09/02/14 16:35 AG
mg/L 09/02/14 16:35 AG
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
Analyzed by: Miaobac Laboratories, Inc. - Fayetteville
Ammonia as N 23.3 mg/L 09/04/14 09:30 JAO SM 4500 NH3 C-1997
BOD 73.1 mg/L 08/27/14 12:00 DSK SM 5210 B-2001
Nitrate as N 0.764 mg/L 08/29/14 15:21 JAW EPA 300.0, Rev. 2.1 (1993)
Nitrite as N 0.568 mg/L 08/29/14 15:21 JAW EPA 300.0, Rev. 2.1 (1993)
Plant Available Nitrogen 18.7 mg/L 09/12/14 18:08 JMO Calculation
Phosphorus, Total
Total Suspended Solids
Total Kjeldahl Nitrogen
15
81.0
42.4
pH Units 09/04/14 14:20 DSK SM 4500 H+B-2000 H
mg/L 08/29/14 07:50 JAO
mg/L 08/28/14 07:50 JAO
mg/L 08/29/14 07:30 JAO
QC Batch Run (Microbac Laboratories, Inc. - Chicagoland)
(Aqueous)
SM 4500-P F-1999
SM 2540 D-1997
SM 4500-Norg C-1997
Analyte
Result Units
Sodium
Calcium
Sodium
Calcium
39.5
58.9
33.0
154
mg/L
mg/L
mg/L
mg/L
Source
14H1436
14H1436
14H1436
14H1436
QC Batch Run - (Microbac Laboratories, Inc -Fayetteville)
RPD Limit
0.756
0.407
0.786
0.455
20
20
20
20
Analyte
Result Units
Nitrate as N ND mg/L
BOD 440 mg/L
Nitrite as N ND mgfL
Nitrite as N ND mgfL
Nitrate as N 8.94 mg/L
Total Kjeldahl Nitrogen 12.4 mg/L
Total Suspended Solids 13.2 mg/L
Microbac Laboratories, Inc.
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com
Source
K4H0821
K4H0808
K4H0863
K4H0821
K4H0863
K4H0816
K4H0819
RPD Limit
4
15
2
2
200
20
200
200
200
20
5
I Page 1 of 3 I

OMICROBAC®
Ammonia as N
Arsenic
BOD
Chromium
Lead
Nickel
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus, Total
Total Dissolved Solids
Total Suspended Solids
Total Kjeldahl Nitrogen
Zinc
Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
Certificate of Analysis
Project: Wastewater Samples - Mthly/3yr
Date Reported: 08/08/14
Date Recei ed: 07/14/14
. Date Sampled. 07/d_4 44
Sampled By: Poythress
Effluent, grab
K4G0455-01
Analyte
Field Data
pH
Temperature
Result
Units
Analyzed Analyzed By
8.3 pH Units 07/14/14 11:05 • Poythress
31.3 °C 07/14/14 11:05 Poythress
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Cadmium
C+alcium
aagtresiu(Aani
ium 4.
Mercury
<0.0020
.190,,`
<0.00020
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
41.2
<0.00200
69.3
<0.002
0.0208
<0.0500
0.659
<0.0500
26.4
16
972
53.0
58.2
0.0244
mg/L 07/21/14 12:19 AG
mg/L 07/21/14 12:19 AG
mg/L 07/21/14 12:19 AG
mg/L 07/21/14 12:19 AG
mg/L 07/22/14 16:19 AG
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
mg/L
mg/L
07/16/14
08/07/14
07/16/14
07/29/14
08/07/14
08/05/14
07/31/14
07/20/14
07/20/14
08/08/14
07/16/14
08:50
01:48
11:00
16:20
01:54
18:54
14:30
22:26
22:26
12:08
15:45
07/16/14 07:30
07/15/14 10:45
07/17/14 07:40
07/18/14 07:20
07/31/14 15:21
JAO
JAW
DSK
JAW
JAW
JAW
MSL
MSL
MSL
JMO
DSK
JAO
JAO
JAO
JAO
JAW
QC Batch Run - (Microbac Laboratories, Inc - Chicagoland)
Method
pH
Field
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 245.1 Rev 3.0
Qualifie 1
SM 4500 NH3 C-1997
SM 3113 B-2004
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
SM 3113 B-2004
SM 3113 B-2004
SM 3 111 B-1999
EPA 300.0, Rev. 2.1 (1993) B
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 4500-P F-1999
SM 2540 C-1997 S 1
SM 2540 D-1997
SM 4500-Norg C-1997
SM 3111 B-1999
Analyte
Result
Units Source
RPD
Limit
Mercury
0.00208
14G0855
3.07
20
Page 1 of 4
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com
mg/L
Microbac Laboratories, Inc.

r.
Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fryetteviiie Division
Certificate of Analysis
Project: Wastewater Sample - Mthly
Date Reported: 07/17/I4
Date Received: 06/25/14
Da c S:,,r3lcd: r 25/I,0
Sampled By: Wc1Ts
Effluent sample, grab
1406909-01
Analyte
Result"
Unit;
A nal_lzrd
Analyzed By
Method
Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagolara
Wal .
S�diutrl
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Aimnonia as N
BOD
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus, Total
Total Suspended Solids
Total Kjeldah! Nitrogen
27.
135
0.440
,•),-.
71
16
139
51.5
mg/L
nig/L
r±g/L
t,
nzr-L
pll Units
nmg/L
07/07/14 14:54
07/07/14 14:54
07.101/1z 09:10
06/251k. 15:35
06r•27/14 20:28
06/271!4 70:28
17/10 I 08:13
06130/1" 15:25
07/97/' L• 08:00
06/26/14 07:45
06/27/ i L• 07:35
AG
AG
JAO
DSK
MSL
MSL
BKS
DSK
JAO
JAO
JAO
QC F.-
Bi•. t;,h' sin=C - (:Yfiernbac J.c.h•vrm.•rFcc. Ina - C%ricvin/m!ral
EPA 200.7 Rev 4.4
EPA 200.7Rev 4.4
S1V4 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 } [
(Aqueous)
SM 4500-P F-1999
SM 2540 D-1997
SM 4500-Norg -1 99•7
Analyte
Calcium
Sodium.
Source
!=E0140
i4C:(:!40
QC Batch RAI n - (rl ficrnbrre Lerhd`ntnriex, inc. - flo'elteril' )
RPD Limit
1.14 20
1.5 20
Analyte
BOD
Total Suspended Solids
Total Suspended Solids
Nitrite as N
Total Suspended Solids
Nitrate as,N
Ammonia as N
Total Kjeldahl Nitrogen
Ammonia as N
Result
183
7.00
Units
mg/L
Souris
1406326
1406896
irg/L. 1406833
i406)04
RPD
7
5
n1,,L 1:09I2 17
717cr/!_ 1406904
n w L 1406912 5
t;tg,`L 1406546
rrc; t. KAGOOl5
: ),)ac. Loburata. i, s, i±ii.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 910.864.1920 p 1910.864.8774• f I vinrivv.rrlicrobac.com
Limit 1
20
5
5
200
1.25
794)
491
N L'
N:10
10
200
10

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC. 28393
K
Fayetteville Division
Certificate of Analysis
Project: Wastewater: Sample - Mthly
Date Rcpor'ed: 06/12/14
Date R ', 29/ 14
®DateS_Mcd' it7.9;hIl
Sampled By: Wells
Effluent, Grab
1405727-01
Analyte
Result
Units ..ual.+zce Analyzed By
Method - Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
1111141
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
BOD
Nitrate as N
Nitrite as N
PlantAvailab1;- Nitrr,l*es
pl1
Phosphorus, Total
Total Suspended Solids
Total Kjeldahl Nitrogen
29.4
1860
0.851
0.4 I !•
14
47.3
46.1
mg/L
nig/L
mg/I.
mg/L
mg/L
m iL_
g/L
mg/L
mg/L
06/09/14 18:24
06/09/14 18:24
05/30/14 08:50
05/29/14 13:40
.05/29/14 22:40
05129/14 22:40
2::09
05/30/14 14:45
05/30/;2- 07:51
05/30/14 07:55
05/30/ 4 07:40
AG
AG
JAO
DSK
MSL
MSL
P.KS
DSK
JAO
JAO
JAO
QC Batch R'..'G - (.rficrrhuc• r,t&uritici:es, Me. - Clricagaiend)
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
Sly' 4500 NH3 C-1907
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 45001-1+B-2000 H
(Aqueous)
SM 4500-P F-1990
SIv12540 D-1997
SM 4500-Norg -1997
Analyte
Sodium
Calcium
Calcium
Sodium
Result
37.0
33.4
159
470
Units
mg/1..
rogi
rngiL
QC Batch Run -
Source
14F0285
1.:F0285
14170232
14F0282
it-ierobar Latorrc• Ties, ',,c- - Fayers i'J ei
RPD Li:nit
2.74 20
2.77
0.18?
0.657
20
20
20
nalytc
Nitrite as N
BOB
Nitrate as N
Total Suspended Soiidt.
Total Suspended Solids
Total Suspended Solids
Phosphorus, Total
Result
ND
594
7.19
9.70
28si
23.0
5.1
1 •nits
ing%L
ug/L
Source • RPD Limit
1405 730 200
1405719
1405730
'.c05677
i405 75
1405742
1405655
0
17
3
20
200
5
5
ti
10
of 3
2592 Hope 1Jills Road 1 Fayeti:eville. NC 28306 1 i3'ii.I.t'64.,920 p 1910.tiC44 3774 f www.rnscrobac.comp�a�
ric;iL
tlrS%�
tru4.'L
ivircrobac i_aboratories. Inc.

Allcns, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 2i2393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phonc
910.864.8774 Fax
Certificate of Analysis
Project: Wastewater Sample - Mthly
Date Reported: May 21, 2014
Dat. Received. April 28, 0.
p
Sampled By: Wells
Effluent sample, grab
1404561-01
Analytc.
Result
Analyzed by: Microbac - Fayetteville Division
Ammonia as N
BOD
Nitrate as N
Nitrite as
Plant Available Nitrogen
Phosphorus, Total
Total Suspended Solids
Total Kjeldahl Nitrogen
Units Analyzed
26.1 mg/L
1980 mg/L
1.16 mg/L
0.676 mg/L
16.2 mg/L
4r6 pH Units
11 mg/L
43.6 mg/L
30.3 mg/L
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Sodium 1"7tt
t alctum
State Certifications:
NCDNR 4I I
NCDOH #37714
USDA #3787
mg/L
rng/
Analyzed By
Mcthod Qualifier
4/29/14 9:25
4/30/14 10:10
4/29/14 23:08
4/29/14 23:08
4/29/14 21:53
4/29/14 9:35
4/30/14 7:50
4/30/14 9:30
4/30/14 7:35
5/2/14 9:23
5/2/14 9:23
JAO
DSK
JAW
JAW
BKS
DSK
JAO
JTL
JAO
SA
SA
SM 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 11+B-2000 . H
(Aqueous)
SM 4500-P F-1999
SM 2540 D-1997
SM 4500-Norg C-1997
EPA 200.7 Rev 4.4
EPA.200.7 Rev 4.4
Respectfully Submitted
Bonnie K. Sanders, Senior Pr kite' Manager
Page 1 of 2

Aliens, Inc
Mr. Reid Wells
5900 Turkcy Highway
Turkey NC, 28393
Fayetteville Division
2592 Hopc Mills Rd
Fayetteville, NC 28306
910.864.1920 Phonc
910.864.8774 Fax
Certificate of Analysis
Project: Wastewater Samples - Mthly/3yr
Date Reported: April 22, 2014
Date Received: March 24, 2014
Lf Sampled: March 24 20a14
Sampled By: Davidson
Effluent, grab
1403522-01
Analytc
Analyzed by: Microbac - Fayetteville Division
Ammonia as N
Arsenic
BOD
I or; e
Chromium
Lead •
Nickel
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus, Total
'total Dissolved Solids
Total Suspended Solids
Total Kjeldahl Nitrogen
Zinc
Result
6.67
<0.00200
1930
19'
0.004
<0.00100
<0.0100
1.13
1.72
11.8
.40
Units Analyzed Analyzed By
mg/L 3/28/14 8:15 MO
mg/L 4/9/14 22:21 JAW
mg/L 3/26/14 9:40 DSK
mg/L 3/27/14 13:3 ! JAW
mg/L 3/31/14 4:47 JAW
mg/L 4/14/14 1:34 JAW
mg/L 3/26/14 20:51 MSL
mg/L 3/25/14 3:42 JAW
mg/L 3/25/14 12:04 JAW
mg/L 4/9/14 11:46 BKS
pH Units 3/28/14 13:30 DSK
8.7 mg/L 3/31/14 8:00 J AO
1140 mg/L 3/27/14 14:20 JAO
31.0 mg/L 3/27/14 10:16 JTL
25.5 mg/L 3/27/14 7:30 JAO
0.169. mg/L 3/26/14 16:13 MSL
Analyzed by: Microbac Laboratories, Inc. - Chicagoiand
E 1i i m • <0.0020 •
Mercury
State Certifications:
NCDNR #I1
NC'D011 #37714
USDA #3787
<0.00020
mg/L 3/31/14 14:31 SA
mg/L 3/31/14 14:31 SA
mg/L 3/31/14 14:31 SA
mg/L 3/31/14 14:31 SA
mg/L 3/27/14 15:56 RPL
• Method
Qualifier
SM 4500 NH3 C-1997
SM 3113 B-2004
SM 5210 B-2001
EPA 300.0, Rev. 2.1 (1993)
SM 3113 B-2004
SM 3113 B-2004
SM 3111 B-1999
EPA 300.0, Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (! 993)
Calculation
SM 45001-1+13-2000
(Aqueous)
SM 4500-P F-1999
SM 2540 C-1997
SM 2540 D-1997
SM 4500-Norg C-1997
SM 3111 B-1999
ERA. 200.7 Rev 4.4
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4.
EPA 200.7 Rev 4.4
EPA 245.1 Rev 3.0
Al2. S1
Rcspci;ttully Submitted
n0
Bonnie K. Sanders, Senior Project Manager
Pag� e 1 of 4�

Aliens, Inc
Mr. Reid Wells
5900 Turkey I liehway
Turkey NC, 28393
Fayetteville Division
25921-lope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: Wastewater Sample - 11thty
Date Reported: February 28, 2014
Date Received: February 17..2014;
Sample"d Fcbtuai
Sampled By: "ci a We is
7/,
20
1 Analytc
Effluent sample, grab
1402289-01
Analyzed by: Microbac - Fayetteville Division
Ammonia as N
EIOD
Nitrate as N
Nitrite as N
Plan Available Nitrogen
Phosphorus. Total
Total Suspended Solids
Total Kjeldahl Nitrogen
Result
7.53
1.840
0.446
0..304
10.3
9.3
C
26.7
Analyzed by: Microbac Laboratories, Inc. - Cnicagoianu
0
State Certificaucns:
NCDNR :.' I
NCD(31-I P37714
USDA #3787
Units Analyzed
mg/L
mg/L
rng/L
Ing/1.,
pfl Units
mg/L
in all,
mg/L
. Analyzed By
2/24/ 44 9:22 JAO
2/19/14 9:58 DSK
2/19/14 1:35 • JAW
2/19'14 1:35 .1AW
2/28/14 0:16 BKS
2/21/14 15:15 DSK
2/21/14 7:45 JAO
2/18/14 9:15 .IAO '
2/25/14 7:35 JAO
!PO, 2/25/14 11:13 SA
g/_, • 2/25/ 1'4 11:13 . SA
Method
Qualifier
SM 4500 NH3 C-1997
SM 5210 B-2001
EPA 300.0. Rev. 2.1 (1993)
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 H+B-2000 H
(Aqueous)
SM 4500-P F-1999
SM 2540-D-1997
SM 4500-Norg C-1997
EPA 200.7 Rev 4.4
EPA 200.7 Rev 4.4
Respectfully Submiuea
, . '� a
- 2Ln�
Bonnie K. Sanders. Senior Project Manager
Page 1 of 3

Allan, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: Wastewater Sample-1llthly
Date Reported: January 29. 2014
Date Received: January 16, 20IA
Dtt e Sampled: January p&RL4, ,
S to pled By: Client
iAnalyte
Effluent, Grab
1401316-01
Analyzed by: Microbac - Fayetteville Division
Ammonia as N
BUD
Nitrate as N
Nitrite as N
Plant Available Nitrogen
Phosphorus. 'Total
Total Suspended Solids
Total Kje(dab( Nitrogen
Result
6.06
1630
0.705
. 0.530
10.8_
tr -
7 7. •)
Analyzed by: Microbac Laboratories, Inc. - Lhicagoland
Cale rn 40'
Sodium • i170:
Suer_ Certifications:
NCDKR i
NCDOtI 437714
USDA P37•:7
Units
mg/L
m g/L
mgiL
mg!L
ntg/L.
p11 Units
mg/L
mg/L
nig/L
mg/L
mg/L
Analyzed Analyzed By
1/21/14 9:30
1/16/14 16:33
1/17/14 17:11
1/17, 4 17:11
I /29/ 14 19:3 7 •
1/23/14 11:20
1/21/14 8:04
1/22/14 9:20
1/17/14 7:50
,IAO
DSK
IMISL
MSL
BKS
DSK
JAO
JAO
JAO
Method Qualifier
SM 4500 NI-13 C-1997
SM 5210 B-2001 G5
EPA 300.0, Rev. 2.1 (1993) B
EPA 300.0, Rev. 2.1 (1993)
Calculation
SM 4500 1I+B-2000 I-1,
(Aqueous)
SM 4500-P F-1999 A 12
SM 2540 D-97
SM 4500-Norg C-1997
1/24/14 10:17 SA EPA 200.7' Rev 4.4
1 /24/ 14 10:17 SA EPA 200.7 Rev 4.4
Respectfully Submitted
7)
-1I�11
Bonnie K. :Sanders, Senior Project Manager
Page 1 of 2