NC0081957_Permit (Issuance)_20000619

NPDES DOCUHENT $CANNINO COVER SHEET
NC0081957
Narrows Powerhouse
NPDES Permit:
Document Type: ,Permit
Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Engineering Alternatives (EAA)
Report
Instream Assessment (67b)
Speculative Limits
Environmental Assessment (EA)
Document Date:
June 19, 2000
This document is printed on reuse paper - impiore any
content on the rezrerse side

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
June 19, 2000
Mr. William L. McCaskill
c/o Yadkin, Inc.
P.O. Box 576
Badin, North Carolina 28009
A&VA
NCDENR
Subject: NPDES Permit Issuance
Permit No. NC0081957
Narrows Powerhouse
Stanly County
Dear Mr. McCaskill:
The Division has modified the permit in accordance with the May 2, 2000, settlement
meeting. The changes include modification of the sampling frequency to require annual
monitoring. As discussed at the meeting samples may be obtained anytime during the
calendar year, with the Discharge Monitoring Report (DMR) due every year on January 30th for
the previous years monitoring.
Attached is the NPDES permit No NC0081957 issued June 19, 2000, based on your
March 1, 1999 application and addendums. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between
North Carolina and the US Environmental Protection Agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty
(30) days following receipt of this letter. This request must be in the form of a written petition,
conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of
Administrative Hearings (6714 Mail Service Center, Raleigh, North Carolina 27699-6714). Unless such
demand is made, this decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division
may require modification or revocation and reissuance of the permit. This permit does not affect the
legal requirements to obtain other permits which may be required by the Division of Water Quality or
permits required by the Division of Land Resources, the Coastal Area Management Act or any other
Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Michael Myers at telephone
number [phone], extension 508.
Sincerely,
Original Signed By
David A. Goodrich
Kerr T. Stevens
cc: Mooresville Regional Office - Water Quality Section
Central Files
NPDES Files
Point Source Compliance/Enforcement Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer Internet: http://h2o.enr.state.nc.us/

Permit No. NC0081957
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Yadkin, Inc.
is hereby authorized to discharge wastewater from a facility located at
Narrows Powerhouse
on NCSR 1704
Stanly County
to receiving waters designated as Yadkin River in the Yadkin -Pee Dee River Basin in accordance
with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV hereof.
This permit shall become effective August 1, 2000.
This permit and authorization to discharge shall expire at midnight on January 31, 2004.
Signed this day June 19, 2000.
Original Signed By
David A. Goodrich
Kerr T. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

SUPPLEMENT TO PERMIT COVER SHEET
Yadkin, Inc.
is hereby authorized to:
Permit No. NC0081957
1. Continue to discharge once -through cooling waters from outfalls 001, 002, 005, 006, and 007 and
water from a sump drain (Outfall 003) located at Narrows Powerhouse, on NCSR 1704, Stanly
County, and
Discharge from said treatment works at the location specified on the attached map into the Yadkin
River which is classified as class WS-IV and B waters in the Yadkin -Pee Dee River Basin

Latitude:
Longitude:
Quad #:
Stream Class:
Receiving Stream
Permitted Flow:
Facility Information
35°25' 09" Sub -Basin
80°05' 32"
F17NE
WS-IV and B
Yadkin River
N/A
Facility
Location
Yadkin, Inc.
NC0081957
Nartows Powerhouse

A (1). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - Final
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge once -through cooling water from outfall(s)
serial number 001, 002, 005, 006 and 007. Such discharges shall be limited and monitored by the Permittee as specified below:
Permit No. NC0081957
EFFLUENT CHARACTERISTICS
DISCHARGE LIMITATIONS
MONITORING REQUIREMENTS
Monthly Average
Weekly Average
Daily Maximum ,,
Effluent Measurement
Frequency
Sample Type
Sample
Location*
Flow (MGD)
Annual
Estimate
E
Temperature'
1
1
Annual
Grab
E
pH2
Annual
Grab
E
NOTES:
* Sample Location: E — Effluent or at the point closest to discharge where a representative sample of the discharge can feasibly be obtained.
1 The temperature of the effluent will be regulated so that the temperature of the receiving stream does not increase by more than 2.8 °C above the natural water
temperature. In no case should the receiving stream temperature exceed 32 °C due to the facility's operation. Temperature of the effluent may be obtained anywhere
downstream of the heat exchanger effluent that is representative of the discharge.
2 The pH of the effluent shall not be less than 6.0 standard units nor greater than 9.0 standard units, unless ambient river conditions prevent compliance with this range.
The Permittee shall obtain authorization from the Division prior to the use of any chemical additive in the discharge. The permittee shall notify the Director in
writing at least ninety (90) days prior to instituting the use of any additional additive in the discharge, which may be toxic to aquatic life (other than additives
previously approved by the division). Such notification shall include the completion of a Biocide Worksheet Form 101 (if applicable), a copy of the MSDS for the
additive, and a map indicating the discharge point and receiving stream.
Monitoring results obtained during the calendar year shall be recorded and reported on a Discharge Monitoring Report (DMR) form and postmarked no later than January 30th
following the completed reporting period. The first DMR is due January 30' 2001. Samples obtained for monitoring purposes may be collected anytime during the calendar
year.
There shall be no discharge of floating solids or visible foam (other than trace amounts) in the effluent, unless ambient river conditions prevent compliance.

A (2). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - Final
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number 003 — Sump
Drain. Such discharges shall be limited and monitored by the Permittee as specified below:
Permit No. NC0081957
EFFLUENT CHARACTERISTICS
DISCHARGE LIMITATIONS
MONITORING REQUIREMENTS
Monthly Average
Weekly Average
Daily Maximum
Effluent Measurement
Frequency
Sample Type
Sample
Location*
Flow
Annual
Estimate
E
Oil and Grease'
15 mg/I
20 mg/I
Annual
Grab
E
pH2 _
Annual
Grab
E
NOTES:
* Sample Locations: E — Effluent or at the point closest to discharge where a representative sample of the discharge can feasibly be obtained.
1 The tailrace shall be visually inspected for oil sheen attributed to facility operations on a weekly basis in conjunction with inspections of the floor sump and rope skimmer.
Confirmation that a visual inspection was conducted shall be recorded in the operating log for the facility and provided to the Division upon request.
2. The pH of the effluent shall not be less than 6.0 standard units or greater than 9.0 standard units, unless ambient river conditions prevent compliance with this range.
3. If the parameter has not be detected above the quantitation level for the respective parameter then the permittee may request that this parameter be removed from the permit.
4. Applies to total PCBs present and includes PCB 1242, 1254, 1221, 1232, 1248, 1260, and 1016.
Best Management Practices (BMPs) must be employed to ensure that excessive pollutants are not discharged to the surface water of the state. These practices should
include as a minimum, routine maintenance of the rope skimmer type oiUwater separator and cleaning accumulated sediment in the bottom of the sump annually.
Chemical wheel pit cleaning is permitted on a monthly basis. When wheel pit cleaning occurs, the tailrace shall be inspected visually for foam and oil. Cleaning shall be
conducted only with pre -approved solvents. Should the Permittee wish to change solvents, a written request should be made to the Division including the MSDS for the
proposed solvent.
Mechanical cleaning operations, which do not contribute any wastewater to the discharge are not limited by this permit. Non -discharging cleaning operations may be conducted
as often as necessary to ensure safety and proper facility operation.
The Permittee shall obtain authorization from the Division prior to the use of any chemical additive (i.e. biocides) in the discharge. The permittee shall notify the
Director in writing at least ninety (90) days prior to instituting the use of any additional additive in the discharge, which may be toxic to aquatic life (other than
additives previously approved by the division). Such notification shall include the completion of Biocide Worksheet Form 101 (if applicable), a copy of the MSDS for
the additive, and a map indicating the discharge point and receiving stream.
Monitoring results obtained during the calendar year shall be recorded and reported on a Discharge Monitoring Report (DMR) form and postmarked no later than January 30th
following the completed reporting period. The first DMR is due January 30' 2001. Samples obtained for monitoring purposes may be collected anytime during the calendar
year.
There shall be no discharge of floating solids or visible foam (other than trace amounts) in the effluent, unless ambient river conditions prevent compliance.

Permit No. NC0081957
SUPPLEMENT TO EFFLUENT LIMITATIONS
AND MONITORING REQUIREMENTS
SPECIAL CONDITIONS
A(3) Penstock Sump Drains — CORRECTIVE ACTION CONDITION
Issuance of this permit is conditional upon the permitees adherence to the provisions contained in the
corrective action letter concerning the clean out of the penstock sump drains. The permittee shall notify
the Division no later than 90 days after completion of the provisions of this letter.

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
February 14, 2000
Mr. William L. McCaskill
c/o Yadkin, Inc.
P.O. Box 576
Badin, North Carolina 28009
NCDENR
Subject: Permit No. NC0081957
Narrows Powerhouse
Stanly County
Dear Mr. McCaskill:
The Division has reviewed the Yadkin Inc. comments received February 1, 2000 in response to the draft
NPDES permit. The Division has considered the concerns raised and has modified the permit in
accordance with current Division policy, all responses to concerns and revisions made to draft permit,
NC0081957, are explained below:
Comment #1: Yadkin Inc. request clarification regarding the Corrective Action Letter related to the
discharge of sump water.
Comment #2: Yadkin Inc. request clarification on the basis for discharge limits during both active and
passive discharge of the sump water.
Response to Comments 1 and 2: To clarify, the Corrective Action Letter addresses the situation where
active pumping is used to remove sump water prior to discharging to a surface water body. Under normal
operating conditions were sump water is passively discharging to the Yadkin River, the limitations and
monitoring requirements stipulated on page A(2) for outfall 003 shall be followed.
The basis for the limitations stipulated in the Corrective Action Letter are as follows: The limitations
stipulated for lead, Cadmium, Chromium, Zinc, and Copper represent the r the Final Acute Values.
These limitations were derived from the criteria developed by the EPA for protection of aquatic
organisms to acute toxicity resulting from exposure to these toxicants.
The PCB limitation was derived from the chronic standard established by the North Carolina
Environmental commission. The Division has taken an environmentally conservative position by
applying this chronic standard as an acute standard, not taking dilution into consideration. The reason for
implementing the standard in this manner is the fate of PCBs in the environment. PCBs in soil and water
are extremely slow to degradeYith no known processes other than slow degradation by microbial
breakdown. Any PCBs discharged to the river are likely to be transported downriver or deposited onto
the sediment at the bottom of the river where they are likely to remain and accumulate.
The Yadkin River at the Falls Powerhouse has a classification of WS-IV and B CA. This classifications
resulted because this reach of the Yadkin River is used for both water supply and primary recreation.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer Internet: http://h2o.enr.state.nc.us/

Yadkin, Inc.
Permit No. NC0081957
Narrows Powerhouse
Page 2
Because there is a high risk of human exposure, the Division has used an environmentally conservative
approach to establishing the conditions under which the discharge may occur.
Comment #3: The Effluent Limitations and Monitoring Page A(1) only references outfalls 001, 002 and
005, but does not include cooling water outfalls 006 and 007.
Response: The outfalls referenced on the Effluent Limitations and Monitoring Page A(1) in the draft
permit, represent the actual physical outfalls present at the facility. The final permit has been modified to
include outfalls 006 and 007 this will to allow Yadkin Inc. to obtain samples at a location other than at the
actual outfall, since sample retrieval at the outfall is not practical.
Comment #4: Clarification of the pH monitoring requirement, since Yadkin Inc. does not add
any chemical additives to the source water.
Response: The hydrogen ion content of water is considered a generic measurement of water quality and
as such is included as a condition of the general permit for hydroelectric facilities. Since the conditions of
the general permit are considered minimum requirements, the semi-annual monitoring of pH, for outfalls
001, 002, 005, 006 and 007, and the quarterly monitoring of outfall 003, will remain as a condition for
this permit.
Comment #5: No monitoring frequencies for pH on the page A(2).
Response: This was an oversight and the final permit has been corrected to include quarterly pH
monitoring of water discharged through outfall 003.
Comment #6: Clarification of the temperature monitoring requirement. The maximum temperature
change across the generator is 25 °C with a ratio of cooling water discharge to generator discharge of
1:30,000. Therefore, the worst case temperature rise of the Yadkin River due to cooling water discharge
would be 0.0083 °C, assuming an ambient water temperature of 20 °C.
Response: As with pH, temperature is considered a generic measurement of water quality and as such is
included as a condition of the general permit for hydroelectric facilities. Since the conditions of the
general permit are considered minimum requirements, the semi-annual monitoring of temperature will
remain as a condition for this permit.
Comment #7: Yadkin Inc. request clarification as to the basis for establishing discharge limits for oil
and grease at outfall 003.
Response: The Narrows Powerhouse, like most hydroelectric facilities, incorporates lubrication into the
routine maintenance for the facility. Because lubrication is common to hydroelectric facilities an oil and
grease limit has been included as a condition of the general permit for hydroelectric facilities. Since the
conditions of the general permit are considered minimum requirements, the oil and grease limit for outfall
003 will remain in the permit.
Comment #8: The boiler plate language relating to increases in stream temperature on the Effluent
Limitations and Monitoring Requirements Page A(1) needs to be prefaced with a footnote that instream
monitoring is not required.
Response: The intent of this limitation is not to require instream monitoring of temperature for reporting
purposes. As with all limited and monitored parameters the required sampling location is specified in the

Yadkin, Inc.
Permit No. NC0081957
Narrows Powerhouse
Page 3
permit. Please note that the Effluent Limitations and Monitoring Requirements Page specifies that
temperature monitoring be conducted on the effluent and does not indicate that upstream or downstream
sampling is required. Therefore, the facility is only required to monitor the temperature of the effluent for
the outfalls referenced on the page A(1).
Comment #9: Yadkin Inc. request that Discharge Monitoring Reports (DMR) submittal be waived.
Response: Since Yadkin, Inc. request coverage under an individual NPDES permit, DMR reporting is
required.
Comment #10: Since it is impractical to obtain samples at the point of discharge, Yadkin Inc. request
approval for sampling at the closest point to discharge where a representative sample can practically be
obtained.
Response: The Division agrees that this is a reasonable request and included the phrase, "E — Effluent or
the point closest to discharge where a representative sample of the discharge can feasibly be obtained." to
allow for sampling at the sump upstream of the discharge.
Comment #11 and #12: On the Effluent Limitations and Monitoring Page A(1) there is no sample type
listed for flow monitoring and Effluent Limitations and Monitoring Page A(2) has no monitoring
frequency or sample type listed for flow monitoring.
Response: These errors have been corrected in the final permit.
Comments received other than those from the Permittee:
Comment #13: The question was raised to the absence of individual toxicant monitoring during passive
discharge from the sump.
Response: The Division has found that there is no reasonable potential for the Narrows Powerhouse to
exceed the chronic standard for lead, chromium, chromium, and PCBs or the action level for copper and
Zinc. A limit for these parameters will not be included as a condition for the permit. However, it is
Division policy to include monitoring as a condition for the permit. Therefore, monitoring of the
toxicants listed above will be required as a condition for the permit. If after one year the listed parameters
have not been detected then Yadkin Inc. may request that these parameters be removed from the permit.
Attached is the NPDES permit No NC0081957 issued February 14, 2000. This permit is issued pursuant
to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between North Carolina and the US Environmental Protection Agency dated December 6, 1983.
Please take notice that this permit is not transferable. Part II, E.4. addresses the requirements to be
followed in case of change in ownership or control of this discharge. This permit does not affect the legal
requirement to obtain other permits which may be required by the Division of Water Quality or permits
required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local
government permit that may be required.
If any parts , measurement frequencies or sampling requirements contained in this permit modification are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30)
days following receipt of this letter. This request must be a written petition conforming to chapter 150E
of the North Carolina General Statutes, filed with the Office of Administrative Hearings, Post Office

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens. Director
February 3, 2000
Larry McCaskill
Yadkin Inc.
P.O. Box 576
Badin, North Carolina 28009
AlirA
NCDENR
Subject: Corrective Action Letter
Permit No. NC0081957
Narrows Powerhouse
Stanly County
Dear Mr. McCaskill:
The purpose of this letter is to clarify the Division's position regarding the discharge of the sump water at
the Narrows Powerhouse. The Narrows Powerhouse is a hydroelectric facility located in Stanly County
North Carolina. Stormwater, which is deposited on the penstocks, collects in sumps located along the
east foundation of the hydroelectric facility. Water samples collected February 26, 1999 and March 15,
1999 revealed that the sediment deposited in the sumps contain levels of PCBs and heavy metals.
Samples were also collected on the water above the sediment and revealed the presence of heavy metals
(i.e. Pb). A subsequent analysis of the water above the sediment, collected on September 21,1999,
detected lead and PCB at 0.045 mg/I and 0.357 ug/l, respectively.
Based on the latest findings, the Division suggests that Yadkin Inc. evaluate disposal methods other than
discharge. The Division recognizes that the cost associated with alternative disposal methods make
discharging an attractive alternative and the Division may permit the discharge provided that either of the
following two options are followed.
Option One:
Prior to discharge Yadkin Inc. must obtain two samples from the sump. One sample shall represent the
upper third of the water column and one sample shall represent the bottom third of the water column.
Analysis results must demonstrate that the listed metals and PCB concentrations are below the following
levels:
Lead (Pb) = 33.78 ug/l
Cadmium (Cd) = 5 ug/I
Chromium (Cr) = 984.3 ug/1
Zinc (Zn) = 65 ug/I
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 - TELEPHONE [phone]/FAX [phone]
AN EQUAL OPPORTUNITY AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/ 1 0% POST -CONSUMER PAPER
VISIT US ON THE INTERNET @ http://h2o.enr.state.nc.us/NPDES

Yadkin Inc.
Permit No. NC0081957
Narrows Hydroelectric Facility
Page 2
Copper (Cu) = 9.2 ug/I
Total PCBs = 0.000079 ug/I
The Permittee shall determine the concentration of the listed metals in the sump water using either EPA
Method 200.7, EPA Method 200.9, or 3113B (Standard Methods). The concentration of PCB in the sump
water shall be determined using either EPA Method 8082 or EPA Method 608.
Upon determination that the contaminant levels are below those listed above, the sump water may be
discharged until the water level in the lower sump is'h the full water level.
Option Two:
Prior to discharge the sump water shall receive appropriate treatment to remove the contaminants
previously mentioned. The treatment technology employed shall be a proven technology for removal of
the listed contaminants and approved by the Division prior to implementation. After receiving the
appropriate treatment, discharge of the sump water is permitted until the water level in the lower sump is
depressed to'h the full water level. The remainder of the water contained in the sump must be disposed
of by an alternative other than discharge.
lease any comments you have regar.' _ this letter or NPDES • mit to DE► — DWQ
PD,E'Unit no ter than amu y 23, 2000. If you - e a• quest •ns ce cernin• • .raft permit for
r facility, please • ichael 1 yers4t [phone], extension
Sincerely,
Kerr T. Stevens
Division of Water Quality
enta
cc: Mooresville Regional Office Regional Office / Water Quality Section
Central Files
NPDES Files

A
Aluminum Company of America
ALCOA
2000 January 21
N. C. Department of Environment
and Natural Resources
Division of Water Quality
Post Office Box 29535
Raleigh, North Carolina 27626-0535
CERTIFIED MAIL
RETURN RECEIPT
Z 411 371 081
Attn: Michael J. Myers
RE: COMMENTS ON DRAFT NPDES PERMIT - YADKIN INC
Narrows Powerhouse - NC0081957
Dear Mr. Myers:
L
w i _!TY J
a ol.sr SOOROE 111;-:iCH
Alcoa is providing the following written comments to the above referenced document on
behalf of Yadkin, Inc.. On behalf of Alcoa and Yadkin, I would like to thank you for your
time and consideration of the issues and comments which follow.
If you should have any questions regarding these matters, please don't hesitate to contact
me.
Yours Very Truly,
f - cam `/ 2-_
William L. McCaskill
Senior Environmental Specialist
Alcoa - Badin Works
Cc:email
S. H. Myers
B. A. Cox
H. J. van der Meyden
J. D. Morton - PGH - NAEHS
J. J. Lettrich - PGH - Legal
M. A. Ross — PGH - Legal
G. J. Ott - Yadkin
K. G. Hunsucker - Yadkin
P. J. Poplin - Yadkin
P:\WINWORD\ENVIRON\WATER\YADKIN\YADKIN NARROWS DRAFT PERMIT COMMENTS.DOC
P.O. Box 576 Badin, North Carolina 28009 USA

NPDES Draft Permit Comments
Yadkin, Inc
Yadkin, Inc has applied for coverage under an individual NPDES permit for this facility
rather than a general permit because of conditions in the general permit which they feel
are unwarranted for this operation.
The following summarizes the comments, as well as, our understanding of the agencies
position based on our discussions during our 10/19/99 meeting, as well as, subsequent
phone conversations.
Ji. Yadkin requests clarification regarding the corrective action letter dated 12/23/99
related to the discharge of sump water. There are two potential scenarios for
discharging the sump water:
A) Actively pumping the water with a sump pump directly to the river
B) Passively discharging the water via gravity flow through the draft tube inlet into
the Unit #4 penstock. (i.e. — stormwater causing intermittent discharges of sump
water.)
As per my 1/4/99 phone conversation with Mr. Mike Myers, it is our understanding
that the letter is addressing scenario A) whereby we would be actively pumping the
water and have to meet the conditions stated in the letter, and not scenario B) which
is occurring on an ongoing basis, for which the stated conditions in the letter do not
apply.
12. Yadkin requests clarification as to the basis for established discharge limits during
circumstances in which active pumping of sump water directly to the river occurs.
Similarly, Yadkin requests clarification as to the requirements which have to be met
.�� under circmstances in which sump water is passively discharged via gravity flow
through the draft tube inlet into the Unit #4 penstock. The stated limits or
requirements to treat the water are overly restrictive and apparently do not take into
consideration reasonable expectations of instream concentrations.
The effluent limitations and monitoring requirements page A(1) only reference
cooling water outfalls 001, 002, & 005, but do not include cooling water outfalls
006 & 007. You will recall that cooling water from from Unit 1(Outfall 001) & Unit 2
(Outfall 006) discharge at a common point, however, since they flow from different
sources until they discharge outside the powerhouse, we listed them as different
outfalls for purposes of clarity. The same situation exists with Unit 3 (Outfall 005) &
Unit 4 (Outfall 007). They are generated from different sources, but exit the
powerhouse at a common point. The reason for listing them as different outfalls is
because the combined discharge cannot be accessed for monitoring purposes if
monitoring is required. Can these outfalls be granted representative outfall status such
that we only have to permit and/or monitor 1 or 2 of the discharges? If not, then they
also need to be reflected on this page as permitted discharges.
2

cp)1/
NPDES Draft Permit Comments
Yadkin, Inc
N4. Yadkin requests clarification egarding the requirements to monitor the pH of cooling
water and sump water. Sinc there are no chemical additives added to these sources,
what is the basis for reque ing that the pH of non -contact cooling water and/or sump
water be monitored?
• Based on our discussions during our 10/19/99 meeting, it is our understanding
that the division understands our position on the above issue and does not
necesarily see the need for monitoring the pH of these discharges.
fluent Limitations and Monitoring Requirements Pages A(2), there is no
oring frequency listed for pH. If pH monitoring is required, then a specified
mYnitoring frequency needs to be indicated on this page.
Yadkin requests clarification regarding the basis of requirements to monitor the
temperature of the cooling water discharges. In the schematic diagrams which were
submitted as part of the application, there is data which indicates that the volume of
generator discharge water relative to the cooling water discharge is proportionally, at
a minimum, a 3000:1 ratio. Operating data indicates there is only an average increase
of 4° - 5° C across the heat exchangers. The maximum increase before a genearator
will trip off-line due to insufficient cooling capacity is 20° — 25°C.
The following thermodynamic equation related to temperature & volume can be used
to show what the resulting temperature would be from combining the cooling water
discharge with the generator discharge.
T(3) = (V(,) X T(») + V(2) X T(2) ) / (V(1) + V(2) )
For Yadkin's case, assuming a water temperature of 20°C, and a cooling water rise of
worst case 25°C, then the resulting water temperature would be:
T(3) _ (3000 x 20) + (1 x 45)) / (3000 + 1 )
_ (60000 + 45) / 3001
= 20.0083
The resulting increase in the receiving water of .0083 degrees is well below the 2.8
degree threshold of allowable temperature rise above background.
• Based on our discussions during our 10/19/99 meeting, it is our understanding
that the division understands our position on the above issue and does not
necessarily see the need for monitoring the temperature of these discharges.
7. Yadkin requests clarification as to the basis for establishing discharge limits
for oil & grease at Outfall 003. There was no fact sheet or waste load allocation
sheets included with the draft permit to support the discharge limits of 15 mg/1
(monthly average) and 20 mg/1 (daily maximum) for this discharge.
d
Per V jc
47
04 el
3 "

NPDES Draft Permit Comments
Yadkin, Inc
The boiler plate language relating to increases in stream temperature on the Effluent
Limitations and Monitoring Requirements page A(1) needs to be prefaced with a
footnote that instream monitoring is not required. _ ---
• Based on our discussions during our 10/19/99 meeting, it is our understanding
that the division understands our position on this issue. Since the boiler plate
language related to instream temperature increases cannot be removed, the
agency is willing to modify the language on the Effluent Limitations and
Monitoring Requirements Page to indicate that instream monitoring is not
required..
9. Yadkin requests that DMR reporting as specifies' in the Effluent Limitations and
Monitoring Requirements page be waived. B...ed on our discussions during our
10/19/99 meeting, it is our understanding t s . t hydroelectric facilities permitted under
the N. C. general permit NC500000. are •llecting similar data and are not required to
°`( • submit these reports.
At)/ • Based on our discussions during our 10/19/99 meeting, it is our understanding
that the division understands the above issue and will consider our request, but
may expect that we provide the DMR as a part offacilitating the divisions needs
for acquisition of data regarding these discharges.
10. Yadkin requests approval that y required sampling is allowed to be performed at
the closest point to the disch ge, which is representative of such discharge, as is
feasible based on the d sig and accessibility of the particular discharge. In a lot of
cases, it is impracticabl o collect samples from the end of the pipe for a particular
discharge due to it bein submerged, elevated, or located in a hazardous or
inaccessible area on the downstream side of the facilities. / _ 4
•�, It is our understanding that the division understands our position on the above
issue and does not see any problems associated with this request.
11. On the Effluent Limi ions and Monitoring Requirements Page A(2), the monitoring
frequency for Oil d Grease references footnote #1 which discusses inspections of
the tailrace. he onitoring frequency for Oil & Grease needs to be specified in the
monitoring r irements sectio s of this page.
rj'
` 12. On the Effluent Limitat
is no sample typ list
powerhouses, th
ns and Monitoring Requirements Pages A(1) & A(2), there
for flow monitoring. On the draft permits for the other three
ple type listed for flow monitoring was specified as
"estimated". The sample type needs to be listed as "estimated" to be consistent with
the other draft permits.
C/v or
4

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Govemor
Bill Holman, Secretary
Kerr T. Stevens, Director
December 23, 1999
Larry McCaskill
Yadkin Inc.
P.O. Box 576
Badin, North Carolina 28009
ATA
NCDENR
Subject: Corrective Action Letter
Permit No. NC0081957
Narrows Powerhouse
Stanly County
Dear Mr. McCaskill:
The purpose of this letter is to clarify the Division's position regarding the discharge of the sump water at
the Narrows Powerhouse. The Narrows Powerhouse is a hydroelectric facility located in Stanly County
North Carolina. Stormwater, which is deposited on the penstocks, collects in sumps located along the
east foundation of the hydroelectric facility. Water samples collected February 26, 1999 and March 15,
1999 revealed that the sediment deposited in the sumps contain levels of PCBs and heavy metals.
Samples were also collected on the water above the sediment and revealed the presence of heavy metals
(i.e. Pb). A subsequent analysis of the water above the sediment, collected on September 21,1999,
detected lead and PCB at 0.045 mg/1 and 0.357 ug/1, respectively.
Based on the latest findings, the Division suggests that Yadkin Inc. evaluate disposal methods other than
discharge. The Division recognizes that the cost associated with alternative disposal methods make
discharging an attractive alternative and the Division may permit the discharge provided that either of the
following two options are followed.
Option One:
Prior to discharge Yadkin Inc. must obtain two samples from the sump. One sample shall represent the
upper third of the water column and one sample shall represent the bottom third of the water column.
Analysis results must demonstrate that the listed metals and PCB concentrations are below the following
levels:
Lead (Pb) = 33.78 ug/1
Cadmium (Cd) = 5 ug/1
Chromium (Cr) = 984.3 ug/1
Zinc (Zn) = 65 ug/1
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 - TELEPHONE [phone]/FAX [phone]
AN EQUAL OPPORTUNITY AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/ 10% POST -CONSUMER PAPER
VISIT US ON THE INTERNET @ http://h2o.enr.state.nc.us/NPDES

Yadkin Inc.
Permit No. NC0081957
Narrows Hydroelectric Facility
Page 2
Copper (Cu) = 9.2 ug/1
Total PCBs = 0.000079 ug/1
The Permittee shall determine the concentration of the listed metals in the sump water using either EPA
Method 200.7, EPA Method 200.9, or 3113B (Standard Methods). The concentration of PCB in the sump
water shall be determined using either EPA Method 8082 or EPA Method 608.
Upon determination that the contaminant levels are below those listed above, the sump water may be
discharged until the water level in the lower sump is'h the full water level.
Option Two:
Prior to discharge the sump water shall receive appropriate treatment to remove the contaminants
previously mentioned. The treatment technology employed shall be a proven technology for removal of
the listed contaminants and approved by the Division prior to implementation. After receiving the
appropriate treatment, discharge of the sump water is permitted until the water level in the lower sump is
depressed to' the full water level. The remainder of the water contained in the sump must be disposed
of by an alternative other than discharge.
Please provide any comments you have regarding this letter or your NPDES permit to DENR — DWQ
NPDES Unit no later than January 23, 2000. If you have any questions concerning the draft permit for
your facility, please call me at [phone], extension 508.
Sincerely,
Michael J. Myers, MS E
NPDES Unit
cc: Mooresville Regional Office Regional Office / Water Quality Section
Central Files
NPDES Files

DENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0081957
Facility Information
Applicant/Facility Name:
Yadkin, Inc. /Narrows Powerhouse
Applicant Address:
PO Box 576, Badin, NC 28009-0576
Facility Address:
On NCSR 1704
Permitted Flow
N/A — Daily Average —1,903,280 gpd
Type of Waste:
Once -through cooling water.
Facility/Permit Status:
Renewal
County:
Stanly
Miscellaneous
Receiving Stream:
Yadkin River
Regional Office:
Mooresville
Stream Classification:
WS-IV & B CA
USGS Topo Quad:
F 18 NE
303(d) Listed?:
NO
Permit Writer:
Michael Myers
Subbasin:
03-07-08
Date:
October 5,1999
Drainage Area (mi2):
''
Summer 7Q10 (cfs)
Winter 7Q10 (cfs):•
Average Flow (cfs):
IWC (%):
Primary SIC Code:
4911
SUMMARY
This facility maintains four outfalls (001, 002, 003and 005). The source of wastewater for outfalls 001,002,
and 005 is once through cooling water, outfall 004 is a sump drain collecting runoff. The old permit stipulates
that outfalls 001 through 003 be monitored (with no limits) for flow, temperature and total residual chlorine.
No discharge monitoring reports have been required because of the use of BMPs.
Outfall, 004, which collects runoff from the site has recently been found to contain elevated levels of heavy
metals. The sediment that has accumulated in the sump has been analyzed and found to contain PCBs in
addition to heavy metals. Because the discharge from this outfall is low and the receiving stream flow is large
use of the mass balance equation allows large concentrations of the toxicants of concern. The '/z FAV values
therefore govern the concentration of the pollutants in the discharge. The discharge of the contaminated
sump water will be cover under a corrective action letter to Yadkin, Inc.
The latest analytical data provided by Yadkin Inc. indicates that PCBs are also contained in the water. The
latest analysis indicates that the concentration of PCBs in the sump water is 0.357 ug/1 with an freshwater
human health standard of 0.000079 ug/1. Because of this most recent data, it is recommended that Yadkin Inc
evaluate methods of disposal other than discharging.
Available/ FAV s:
Cd = 5 ug/I
Cr = 984.3 ug/1
Cu = 9.2 ug/I
Pb = 33.8 ug/l
Hg = 2.4 ug/1
Zn = 65 ug/1
Yadkin Inc. has requested that monitoring be replaced by implementation of BMPs. Additionally, Yadkin
Inc. requested that the pH and temperature "Boiler Plate" language be excluded from the permit. This plant
is eligible for coverage under general permit NCG50000, however, they prefer the individual permit because
the general permit does not provide a provision for BMP practices in lieu of monitoring. In the next renewal
of the general permit the viability of providing such a provision into the permit should be examined. For all
Yadkin. Inc. — Narrows Hydroelectric Powerhouse Fact Sheet
NPDES Renewal
Page 1

hydroelectric facilities that request individual permits in lieu of the general permit, it is the Division's position
that these facilities should be permitted consistently statewide. Therefore, permit NC0027332 and general
permits NCG500000 were used in developing this draft permit for the hydroelectric plants owned by Yadkin,
Inc. in the Yadkin River basin.
The receiving stream (Yadkin River) is classified as WS-IV and B CA waters from Badin dam to a point 0.5
miles upstream of Falls dam. This reach is not listed on the 303(d) list as impaired water. According to the
May 1998 Yadkin -Pee Dee River Basinwide Water Quality management Plan this reach has been classed as
supporting its designated uses.
TOXICITY TESTING:
Current Requirement: N/A
Recommended Requirement: N/A
COMPLIANCE SUMMARY:
To date this facility has not been required to submit Discharge Monitoring Reports (DMR) because of the
implementation of Best Management Practices. However a historical review of inspection reports was
conducted and Mike Parker (Mooresville Regional Office) was contacted regarding compliance issues. With
the available information it was concluded that this facility has no compliance issues.
INSTREAM MONITORING:
This facility is not required to perform any instream monitoring.
PROPOSED CHANGES:
Outfalls 001, 002, and 005 — Monitoring and/or permit limits have been set for flow and temperature as
outlined on the Effluent Limitations page.
DMR submittal - DMRs will need to be submitted quarterly for all outfalls.
Total Residual Chlorine (TRC) - Total residual chlorine monitoring will be removed from the permit, since
chlorine is not utilities at this facility.
Chromium, zinc, and cooper restriction - The chromium, zinc, and copper excerpt will be excluded since this is
adequately addressed in the notification requirement if any toxicants are to be added.
Temperature - Temperature requirement will reflect the situation if natural conditions raise the ambient temp
above 32°C.
PROPOSED SCHEDULE FOR PERMIT ISSUANCE:
Draft Permit to Public Notice:
Permit Scheduled to Issue:
STATE CONTACT:
If you have any questions on any of the above information or on the attached permit, please contact Michael
Myers at [phone] ext. 508.
REGIONAL OFFICE COMMENT: This is a minor permit renewal therefore the regional office comments
will be solicited during the public comment period.
Copies of the following are attached to provide further information on the permit development:
• Reasonable Potential Analysis (majors only)
• Existing permit effluent sheets with changes noted (existing facilities only)
• Draft Permit
NPDES Recommendation bv:
Date
Y iclkin. Inc. — Narrows Hydroelectric Powerhouse Fact Sheet
NPDES Renewal
Page 2

Regional Office Comments
am/ c„/ /di ?adiGL
Yit.e. Ale -ad slo •vial ff ...�
-06 eg7-71-2
/4/,
Regional Recommendation by:
Signature
Reviewed and accepted by:
Date
Regional Supervisor:
Signature
Date
NPDES Unit Supervisor:
Signature
Date
Yadkin. Inc. — Narrows Hydroelectric Powerhouse Fact Sheet
NPDES Renewal
Page 3

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
MEMORANDUM
To:
From:
Subject:
Britt Setzer
NC DENR / DEH /
Mooresville Regional
Michael J. Myers
NPDES Unit
November 9, 1999
•
Tonal Engineer
face
Review of Draft NPDES Permit NC0081957
Yadkin Inc. — Narrows Powerhouse
Stanly County
A7A
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Please indicate below your agency's position or viewpoint on the draft permit and return this form by
December 17, 1999. If you have any questions on the draft permit, please contact me at the
telephone number or e-mail address listed at the bottom of this page.
nNwIivIiv, n%NVANNANiNwIivIiVANANwAN/VVNV NANANivIw�iNViANANNVnAivnAN MINIM ANANNVAANINV/WivANA/ViV/VVN ANi
RESPONSE: (Check one)
Vr."'
Concur with the issuance of this permit provided the facility is operated and maintained
properly, the stated effluent limits are met prior to discharge, and the discharge does not
contravene the designated water quality standards.
Concurs with issuance of the above permit, provided the following conditions are met:
Opposes the issuance of the above permit, based on reasons stated below, or attached:
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 919 733-5083, extension 508 (fax) 919 733-0719
VISIT US ON THE INTERNET @ http://h2o.enr.state.nc.us/NPDES
Mike.myers@ ncmail.net

r\Lis
North Carolina } ss
Mecklenburg County}
The Knight Publishing Co., Inc.
Charlotte, NC
Affidavit of Publication
THE CHARLOTTE OBSERVER
NCDENR/DWQ/BUDGET OFFICE
CHRISTIE JACKSON
1617 MAIL SERVICE CENTER
RALEIGH NC 27699-1617
REFERENCE: 30019881
3454987 Wastewater Permit
Before the undersigned, a Notary Public of said
County and State, duly authorized to administer
oaths affirmations, etc., personally appeared,
being duly sworn or affirmed according to law,
doth depose and say that he/she is a
representative of the Knight Publishing Company a
corporation organized and doing business under the
laws of the State of Delaware, and publishing a
newspaper known as The Charlotte Observer in the
city of Charlotte, County of Mecklenburg and State
of North Carolina and that as such he/she is
familiar with the books, records, files and
business of said Corporation and by reference to
the files of said publication
the attached advertisement was inserted. The
following is correctly copied from the books and
files of the aforesaid Corporation and
Publication.
PUBLISHED ON: 11/13
AD SPACE:
FILED ON:
NAME:
70 LINE
11/18/99
TITLE:
DATE:
In Testimony Whereof I have hereunto set my hand and
day and y a aforesaid.
S
Notary:
►7
My Commission
PUBLIC NOTICE
STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION/NPDES UNIT
1617 MAIL SERVICE CENTER
RALIGH271617
NFICATION OF INTENT ISSUE AN NNP
OTIPOES WASTEWATER PERMfT
On the basis of thWou h staff review and application of NC General Statute
143.21, Pudic Law 92-500 and other lawful standards and regulations, the North
Carolina Environmental Management Commission proposes to issue a National
Pollutant Discharge Elimination System (NPDES) wastewater discharge permit to
the person(s) listed on the attached pages, effective 45 days from the publish
date of this notice.
Wrdten comments regarding the proposed permit will be accepted until 30 days
aftconsidered heredbin tt eat nab determinations e of si All comments
regreceived prior arding t t0 that date are
Ureclor of the NC Division of Water Goal proposed public bme The
for the proposed permit should the Division receive a s ne to iantld a egreef public
interest. significant degree of public
Copies of the draft permit and other scowling information on file used to deter-
mine conditions present in the draft permit are available upon request and pay-
mentto NCecosts of Division of ater Quality at thuction. Mail e aeabbovve addts ress or or call Msf information
Jackson at [phone]. extension 538. Please include the NPDES permit
number (attached) in any communication. Interested persons may also visit the
Division of Water Quality at 512 N. Salisbury Street. Raleigh. NC 2760e-1148
between the hours of 800 a.m. and 600 p.m. to review information on file.
NPDES Permit Number NC0081957, Yadkin Inc.. Narrows Powerhouse, P.O.
Box 576, Badin, NC 28009 has applied for a permit renewal for a facility
located In Stanly County discharging Treated wastewater into Yadkin River in
the Yadkin Pee -Dee River Basin. Currently, no parameters are water quality
limited. This discharge may affect future allocations in this portion of the
receiving stream.
LP3454987
itQ
OIL,
affixed my seal, the
Expires: _I /6X`-.5

T fk Stanly News and Press
a
P.O. Box 488
Albemarle, NC 28002
[phone]
STARTDATE CLASS DESCRIPTION WORDS INS CHG
MURPHY, KIM
NCDENRIDWQIBUDGET OFFICE
RALEIGH,NC 27626-0535
PO BOX 29535
11/14/99 300 PUBLIC NOTICE STATE 324
NORTH CAROLINA, STANLY COUNTY
AFFIDAVIT OF PUBLICATION
Before the undersigned, a Notary
Public of said County and State, duly
commissioned, qualified, and authorized by
law to administer oaths, personally appeared:
LaJeune Waggoner, who being first duly sworn,
deposes and says: that he is Publisher of a
newspaper known as THE STANLY NEWS AND PRESS,
published, issued, and entered as second class mail
in the City of Albemarle, in said County and State;
that he is authorized to make this affidavit and sworn
statement; that the notice or other legal advertisement,
a true copy of which is attached hereto, was published
in THE STANLY NEWS AND PRESS on the dates
specified on the copy attached and that the said
newspaper in which such notice, paper, document, or
legal advertisement was published was, at the time of
each and every such publication, a newspaper meeting
all of the requirements and qualifications of Section 1-597
of the General Statures of North Carolina and was a
qualified newspaper within the meaning of Section 1-597
of the General Statures of North Carolina.
AFFIDAVIT OF INSERTION
Date: 11/15/99
1
DEC 1 61999
POINT SOURCE BRANCH
1 68.04
Sworn 1
this _I!
My
PUBLIC NOTICE
STATE Of NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT
COMMISSION/NPDES UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA
27699-1617
NOTIFICATION OF INTENT TO ISSUE A
NPDES WASTEWATER PERMIT
On the basis of thorough staff review and appli-
cation of NC General Statute 143.21, Public
Law 92.500, and other lawful standards and reg-
ulations, the North Carolina Environmental Man-
agement Commission proposes to issue a
National pollutant Discharge Elimination System
(NPDES) wastewater discharge to the person(s)
listed on the attached pages effective'45 days
from the publish date of this notice.
Written comments regarding the proposed permit
will be accepted until 30 days after the publish
date of this notice. All comments received prior to
that date are considered in the final determina-
tions regarding the proposed permit. The Director
of the NC Division of Water Quality may decide to
hold a public meeting for the•proposed permit
should the division receive a significant degree of
public interest.
Copies of the draft permit :5End other supporting
information on file used to etermine conditions
e
a
present in the draft permiare available upon
request and payment of thcosts of reproduc-
above address o� ca, "Pst$ forinforma-
[phone], etensl�nn38.�Pleaseckncludet.
the NPDES permit number (attached) in any
communication. interested persons may also visit
the Division of Water Quality at 512 North Salis-
bury Street, Raleigh, NC 27604-1148 between
the hours of 8:OOam-5:00pm to review informa-
tion on tile.
Z'DES Permit NC0081957, Yadkin Inc., Nar-
rows Powerhouse, PO Box 576 Badin, NC 28009
has applied for a permit renewal for a facility
located in Stanly County. discharging treated
wastewater into Yadkin River in the Yadkin Pee
Dee River Basin. Currently no parameters are
water quality limited. This discharge may effect
future allocations in this portion of the receiving
stream.
Dated November 10, 1999
David A. Goodrich )
Kerr T. Division of Environmental Directorvens,
Management
November 14, 1999

Stanly News Press
237 W. North St.
P.O. Box 488
Albemarle, NC 28002
Phone: [phone]
Fax: [phone]
Ad Number: 12772
Ad Classification: 300
Ad Type: Legal
Payment Method: Billed
Customer: KIM MURPHY
NCDENR/DWQ/BUDGET OFFICE
PO BOX 29535
RALEIGH, NC 27626-0535
Customer Phone: [phone]
orm
o(v-V-v'
Original Salesperson: MANDAS
Salesperson Generating Bill: MANDAS
Initial text: PUBLIC NOTICE STATE
Start: 11/14/99 Stop: 11/14/99 Total inserts: 1
Publication: Start: Stop: Inserts:
Stanly NewsPress 11/14/99 11/14/99 1
Gross:
Surcharge:
Total:
Credits:
Amt paid:
Amt due:
$ 68.04
0.00
68.04
0.00
0.00
68.04
RECEIVED
NOV 15 1999
DWQ BUDGET OFFICE

PUBLIC NOTICE
STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT
COMMISSION/NPDES UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA
27699-1617
NOTIFICATION OF INTENT TO ISSUE A
NPDES WASTEWATER PERMIT
On the basis of thorough staff review and appli-
cation of NC General Statute 143.21, Public Law
92-500, and other lawful standards and regula-
tions, the North Carolina Environmental Manage-
ment Commission proposes to issue a National
pollutant Discharge Elimination System (NPDES)
wastewater discharge to the person(s) listed on
the attached pages effective 45 days from the
publish date of this notice.
Written comments regarding the proposed permit
will be accepted until 30 days atter the publish
date of this notice, All comments received prior to
that date are considered in the final determina-
tions regarding the proposed permit. The Director
of the NC Division of Water Quality may decide to
hold a public meeting for the proposed permit
should the division receive a significant degree of
public interest.
Copies of the draft permit and other supporting
information on file used to determine conditions
present in the draft permit are available upon
request and payment of the costs of reproduction.
Mail comments and/or requests for information to
the NC Division of Water Quality at the above
address or call Ms. Christie Jackson at (919)733-
5083, extension 538. Please include the NPDES
permit number (attached) in any communication.
interested persons may also visit the Division of
Water Quality at 512 North Salisbury Street,
Raleigh, NC 27604-1148 between the hours of
8:00am-5:00pm to review inf rmation on file.
NPDES Permit dkin Inc., Nar-
rows Powerhouse, PO Box 576 Badin, NC 28009
has applied for a permit renewal for a facility
located in Stanly County. discharging treated
wastewater into Yadkin River in the Yadkin Pee
Dee River Basin. Currently no parameters are
water quality limited. This discharge may effect
future allocations in this portion of the receiving
stream.
Dated November 10, 1999
David A. Goodrich
Kerr T. Stevens, Director
Division of Environmental Management
November 14, 1999

To: Permits and Engineering Unit
Water Quality Section
Attention: Charles Weaver
SOC Priority Project: No
Date: June 4, 1999
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Stanly
NPDES Permit No.: NC0081957
MRO No.: 99-65
PART I - GENERAL INFORMATION
1. Facility and Address: Narrows Powerhouse
c/o Yadkin, Inc.
Post Office Box 576
Badin, N.C. 28009
2. Date of Investigation: May 27, 1999
3. Report Prepared By: Michael L. Parker, Environ. Engr. II
4. Person Contacted and Telephone Number: Mr. Ronny Pickier, [phone]
5. Directions to Site: From the junction of SR 1704 and SR 1719 (Falls Road) in the Town of
Badin, travel northeast on SR 1704 to the end of the road. The Narrows Powerhouse is
located at the end of SR 1704.
6. Discharge Point(s), List for all discharge Points: -
Latitude: 35 ° 25' 09"
Longitude: 80° 05' 32"
Attach a USGS Map Extract and indicate treatment plant site and discharge point on map.
USGS Quad No.: F 18 NE
7. Size (land available for expansion and upgrading): There is little, if any, area available for
the construction of wastewater treatment facilities, if necessary.
8. Topography (relationship to flood plain included): The Powerhouse is located on the main
segment of the Yadkin River; however, the hydroelectric generation facilities are not subject
to flooding.

Page Two
9. Location of Nearest Dwelling: The nearest dwelling is at least one mile from the
Powerhouse site.
10. Receiving Stream or Affected Surface Waters: Yadkin River
a. Classification: WS-III and B
b. River Basin and Subbasin No.: Yadkin 03-07-08
c. Describe receiving stream features and pertinent downstream uses: The Yadkin
River is used for primary and secondary recreation and electricity generation. There
are no known water intakes for a distance of several miles below this Powerhouse.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of Wastewater: * MGD
Outfalls*:
001 002 003 004 005 006 007
0.432 0.172 0.00288 Intermittent 0.432 0.432 0.432
* Intermittent based on electricity needs and power production.
b. Types and quantities of wastewater:
Outfall 001, 005, 006, 007: Generator Cooling water
Outfall 002: Thrust bearing cooling water.
Outfall 003: Turbine wheelpits, floor drains, powerhouse sumps, and powerhouse
sumps.
c. Prevalent toxic constituents in wastewater: None. There are no biocides added to the
cooling water at this facility.
2. Production Rates (industrial discharges only) in Pounds: N/A
3. Description of Industrial Process (for industries only) and Applicable CFR Part and Subpart:
N/A
4. Type of Treatment (specify whether proposed or existing): There are no existing treatment
facilities for the proposed outfalls. For domestic wastewater disposal, employees must either
return to ALCOA's plant or use a portable toilet, which is provided.
5. Sludge Handling and Disposal Scheme: Sludge generation is not expected from any outfall.

Page Three
6. Treatment Plant Classification: N/A
7. SIC Code(s): 4911
Wastewater Code(s): 48
MTU Code(s): N/A
PART III - OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grants Funds (municipals only)? No
2. Special monitoring requests: None at this time.
3. Additional effluent limits requests: None at this time.
4. Air Quality and/or Groundwater concerns or hazardous materials utilized at this facility that
may impact water quality, air quality or groundwater? No AQ or GW concerns nor are
hazardous materials utilized at this facility.
PART IV - EVALUATION AND RECOMMENDATIONS
The applicant, Yadkin, Inc. (a subsidiary of ALCOA), operates a powerhouse (dam) on the
Yadkin River known as Narrows Powerhouse, which generates hydroelectric power used in
ALCOA's aluminum manufacturing process. The dam was constructed in the early 1900s. Complex
electrical generation machinery exist at this facility that requires cooling water during operation.
There have been no changes to this facility with regards to the permitted outfalls since the Permit
was last issued.
One important change that should be included in the subject permit is the existence of an
additional discharge from the sumps located along the east foundation of the hydroelectric
generation building. These sumps receive stormwater that collects along the building's foundation
and pumps the water into the process water stream that feeds Narrows Generator Unit No. 4. The
stormwater comes into contact with the penstocks that serve the dam with water for electrical
generation. Through the years, routine maintenance of the penstocks has included painting, which
up until the past 2-3 decades involved the use of lead -based paint. Over time, this paint has
continually flaked off, and was carried to the sumps during storm events. In a recent analysis,
elevated levels of lead were found in analysis of the sump water and sludges that had settled into the
bottom of the sumps. In addition to the existence of lead, PCBs and other constituents were found in
the sludges as well. Yadkin proposes to remove the sludges for disposal in a hazardous waste
landfill, however, the water located in the sumps must be removed before the sumps can be cleaned
of the sludges. Therefore, prior to renewal of this permit, it will be necessary to determine whether
or not this outfall can be effectively permitted considering the current layout of the site, the lack of
available treatment, and the potential for elevated levels of pollutants to enter surface waters.

Page Four
Pending receipt and approval of the WLA and a decision made by the NPDES Unit
regarding the ability to permit the recently discovered sump water discharge, it is recommended that
the NPDES Permit be reissued as requested.
Signature of Report Preparer Date
ts,
Water Quality Regional Su ► - rvisor Date
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NOV 1 ly/y,
Aluminum Company of America
1999 October 27
Mr. Dave Goodrich
N. C. Division of Water Quality
P. O. Box 29535
Raleigh, N. C. 27626-0535
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Z 493 673 006
RE: ADDENDUM #2 - NPDES PERMIT APPLICATION - YADKIN, INC
NARROWS POWERHOUSE NC 0081957
Dear Mr. Goodrich:
On behalf of Yadkin, Inc., Alcoa is submitting the attached analytical data as addendum #2 to
the NPDES permit application which was recently submitted by Yadkin, Inc. for the Narrows
Powerhouse. The attached analytical data is for a recently discovered discharge from the
Narrows Powerhouse which was identified just prior to submitting the permit application,
and for which we did not have any data at the time the application was submitted.
The discharge consists primarily of stormwater that collects in sumps along the outside of the
east foundation of the hydroelectric generation building. In order to prevent structural
problems with the building and penstock foundations, the water has historically been
removed by aspirating it into the process water stream which feeds the Narrows Unit #4
generator.
The attached data are for a water sample which was collected on 9/21/99 from standing water
in the Penstock Sumps. It should be noted that there was no discharge occurring at the time of
sampling, so samples were not collected from an actual discharge, but rather from standing
water which accumulates beneath the Penstocks. The data indicate that there are PCB's
present at a concentration of 0.357 ug/1 and total lead at a concentration of 0.045 mg/l.
A copy of this information was provided to Mr. Mike Myers of the Division during his
10/19/99 visit to Badin to discuss the draft NPDES permit for the Narrows Powerhouse.
If you should have additional questions or would like to discuss this further, please don't
hesitate to contact me.
Very Truly Yours,
William L. McCaskill
Senior Environmental Specialist
Alcoa - Badin Works
\\BAD_SERVICES\MCCASWLSIWINWORD\ENVIRON\WATER\NC-DEM\YADKIN NPDES PERMIT APP
ADDENDUM#2.DOC
P.O. Box 576 Badin, North Carolina 28009 USA
1

Attachments - Analytical reports
email: B. A. Cox
J. E. Adams - Tapoco
B. J. Polk
G. J. Ott
K. G. Hunsucker
H. J. van der Meyden
cc: S. H. Myers - attachment (analytical data)
J. D. Morton - attachment (analytical data)
Rex Gleason - NCDWQ - Mooresville - Certified Mail - Z 493 673 007
attachment (analytical data)
ABAD_SERVICESIMCCASWLSMINWORDIENVIRONIWATERINC-DEMWADKIN NPDES PERMIT APP
ADDENDUM#2.DOC
2

SEP-30-1999 17:34 SAVANNAH LABS
EL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
714 JAG YJ10' r . wv L r
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.saviabs.com
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Kadin, NC 28009
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
16269-5 NARROWS PENSTOCK
PARMIETER
LOG NO: S9-16269
Received: 22 SEP 99
Reported: 30 SEP 99
Client Po. No.: BA14 9 6 2 6BA
Project: ALCOA-BADIN
Sampled By: Client
Code: 172990930
Page 8
DATE/
TIME SAMPLED
09-21-99/13:00
Lead (6010)
Lead, mg/1
Dilution Factor
Prep Date
Analysis Date
Analyei8 Time
Batch ID
Analyst
16269-5
0.045
1.0
09.23.99
09.23.99
2128
0923H
JRF

-23u • Sr?(,
1
ALCOA CHEMICAL LABORATORY
MASSENA OPERATIONS
ANALYTICAL REPORT
SAMPLE NUMBER: 99005987
SAMPLE DATE: 15:00:00 9/21/1999
SAMPLED BY: D.HEFNER
SAMPLE DESCRIPTION: Narrows Penstock
SOURCE ID: COC#
TEST NAME ANALYSIS
PCB_608
PCB_SURR
T0'd 1d101
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Tetrachloro-m-xylene
Decachlorobiphenyl
ANALYSIS
RESULTS UNITS
< 0.065 ppb
< 0.065 ppb
• 0.065 ppb
c 0.065 ppb
< 0.065 ppb
< 0.065 ppb
0.357 ppb
81.222 t
130.300 t
PREPARATION
DATE
9/28/1999
ANALYSIS
DATE
10/07/1999
10/07/1999
666T-zT-100
S6Z7 092, ST£

-2 3V - S-774
1
ALCOA CHEMICAL LABORATORY
MASSENA OPERATIONS
ANALYTICAL REPORT
SAMPLE NUMBER: 99005987
SAMPLE DATE: 15:00:DO 9/21/1999 °.'
SAMPLED BY: D.HEFNER
SAMPLE DESCRIPTION: Narrows Penstock
SOURCE ID: COC#
ANALYSIS PREPARATION ANALYSIS
TEST NAME ANALYSIS RESULTS UNITS DATE DATE
PCB_608 Aroclor 1016 < 0.065 ppb
Aroclor 1221 . < 0.065 ppb
Aroclor 1232 < 0.065 ppb
Aroclor 1242 < 0.065 ppb
Aroclor 1248 < 0.065 ppb
Aroclor 1254 < 0.065 ppb
Aroclor 1260 0.357 ppb
PCB _BURR Tetrachloro-m-xylene 81.222
Decachlorobiphenyl 130.300 t
Z0'd 113101
9/28/1999 10/07/1999
10/07/1999
Z0'd S6M7 092, St£

" SEP-30-1999 17:34 SRUHNNHH LHIiS
BL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
71G 'MG 101bD r.V_I7/1f
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.savlabs.com
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-16269
Received: 22 SEP 99
Reported: 30 SEP 99
Client PO. No.: BA349626BA
Project: ALCOA-BADIN
Sampled By: Client
Code: 172990930
Page 8
DATE/
TIME SAMPLED
16269-5 NARROWS PENSTOCK
09-21-99/13:00
PARAMETER
Lead (60.0)
Lead, mg/1
Dilution Factor
Prep Date
Analysis Date
Analysis Time
Batch ID
Analyst
. 16269-5
0.045
1.0
09.23.99
09.23.99
2128
0923E
JRF

Aluminum Company of America
1999 March 29
Mr. Dave Goodrich CERTIFIED MAIL
N. C. Division of Water Quality RETURN RECEIPT REQUESTED
P. O. Box 29535 Z 276 262 578
Raleigh, N. C. 27626-0535
RE: ADDENDUM TO NPDES PERMIT APPLICATION - YADKIN, INC
NARROWS POWERHOUSE NC 0081957
Dear Mr. Goodrich:
On behalf of Yadkin, Inc., Alcoa is submitting the attached analytical data as an addendum to
the NPDES permit application which was recently submitted by Yadkin, Inc. for the Narrows
Powerhouse. The attached analytical data is for a recently discovered discharge from the
Narrows Powerhouse which was identified just prior to submitting the permit application,
and for which we did not have any data at the time the application was submitted.
The discharge consists primarily of stormwater that collects in sumps along the outside of the
east foundation of the hydroelectric generation building. In order to prevent structural
problems with the building and penstock foundations, the water has historically been
removed by aspirating it into the process water stream which feeds the Narrows Unit #4
generator. The data consists of two separate water samples which were collected from the
sumps beneath the Narrows penstocks, as well as, a sludge sample which was collected from
sludge which was removed from the sumps beneath the penstocks.
The first water sample collected on 2/26/99 was collected st bsequent to the sludge having
been removed from the sumps. The water level in the sumps at that time was — 12". It is
important to note that because of the low water level at the time of sampling, there was no
discharge occurring, so the 2/26/99 sample was taken from standing water in the sump
beneath the Unit #4 penstock, and not from the pump discharge.
The second water sample collected on 3/15/99 was collected subsequent to a storm when the
sumps were full with — 3 - 5 feet of standing water. Again, it is important to note that the
sample was collected from standing water beneath the Unit #4 penstock, and not from the
pump discharge since active pumping of the water has not occurred since the original
discovery of contaminants in the water.
You will note that the 3/15/99 water sample was also analyzed for Polychlorinated Biphenyls
(PCB's) with concentrations detemined to be below the reported PQL's of 1.0 and 2.0 ug/1
for respective arochlors. The decision to analyze the water for PCB's was made after
receiving the analytical results for the sludge which had been removed from the sumps and
determined to have a PCB concentration of 22.4 mg/kg. You will also note that both of the
P.O. Box 576 Badin, North Carolina 28009 USA

water samples contained lead, as well as, other trace metals which has resulted from
historical painting activities associated with the penstocks which have been maintained since
the facility installation in the early 1900's. The water which is currently standing in the
sumps gravity flows to the river through the aspiration inlet into the Unit #4 generator every
time there is additional water deposited in the sumps from stormwater infiltration.
In order to facilitate further cleaning of the sumps, Yadkin is requesting permission to pump
the remaining water in the sumps to the river which is estimated to be — 30,000 - 50,000
gallons. Once this accomplished, an attempt will be made to further clean sediment from the
sumps in an effort to reduce or eliminate any further contamination in this discharge.
Additionally, Yadkin is requesting permission to continue to routinely pump accumulated
stormwater from the sumps to the river to prevent any future structural problems with the
foundations of the building and penstocks.
We request you consider this matter on an expedited basis as 1) we have a Federal Energy
Regulatory Commission (FERC) requirement that this water not be allowed to cover the
penstock foundations as is the present condition and 2) we want to expedite removal of the
remaining sediment to ensure the cleanest water possible be discharged to the stream.
If you should have additional questions or would like to discuss this further, please don't
hesitate to contact me.
Very Truly Yours,
1,4e.A0,.... .>,AveZid
William L. McCaskill
Senior Environmental Specialist
Alcoa - Badin Works
Attachments - Analytical reports (S9-11332 & S9-11667)
email: B. A. Cox
J. E. Adams - Tapoco
cc: S. H. Myers - attachment (analytical data)
B. J. Polk - attachment (analytical data)
G. J. Ott - attachment (analytical data)
K. G. Hunsucker - attachment (analytical data)
H. J. van der Meyden - attachment (analytical data)
J. D. Morton - attachment (analytical data)
Certified Mail - Z 276 262 577
Rex Gleason - N. C. DWQ - Mooresville - attachment (analytical data)
P:IWINWORDIENVIRONIWATERINC-DEMINARROWS PENSTOCKS.DOC
2

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 1
DATE/
TIME SAMPLED
11332-1 Penstock Sludge
02-26-99/1300
PARAMETER
11332-1
Metals in TCLP Extract (6010)
Arsenic (TCLP-6010), mg/1
Barium (TCLP-6010), mg/1
Cadmium (TCLP-6010), mg/1
Chromium (TCLP-6010), mg/1
Lead (TCLP-6010), mg/1
Selenium (TCLP-6010), mg/1
Silver (TCLP-6010), mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Mercury in TCLP Extract (7470)
Mercury (TCLP-7470), mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.20
<1.0
<0.10
<0.20
69
<0.50
<0.10
03 01.99
03 02.99
EM
03 04.99
2004
03020
1.0
<0.020
03.01.99
03.03.99
BJB
03.03.99
0912
0303R
1.0
Esc: s, 4045-
/14,42,_
,J D jx Dx:/f,'
G, 1445ac,---e/Z yaD/CiAl
b

•
.,
• B L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 2
DATE/
TIME SAMPLED
11332-1 Penstock Sludge
02-26-99/1300
PARAMETER
11332-1
Antimony (TCLP) (6010)
Antimony (TCLP) , mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (TCLP)
Nickel (TCLP-6010) , mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.020
03.01.99
03.02.99
EM
03.04.99
2004
03020
1.0
<0.040
03.01.99
03.02.99
EM
03.04.99
2004
03 020
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 3
DATE/
TIME SAMPLED
11332-1 Penstock Sludge
02-26-99/1300
PARAMETER
11332-1
Beryllium (TCLP)
Beryllium (TCLP-6010), mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Thallium in TCLP Extact (6010)
Thallium (TCLP) ,
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
mg/1
<0.0040
03.01.99
03.02.99
EM
03.04.99
2004
03020
1.0
0.010
03.01.99
03.02.99
EM
03.04.99
2004
03020
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 4
DATE/
SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES TIME SAMPLED
11332-1
Penstock Sludge 02-26-99/1300
PARAMETER 11332-1
Vanadium (TCLP) (6010)
Vanadium (TCLP-6010), mg/1 <0.010
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.02.99
Analyst EM
Analysis Date 03.04.99
Analysis Time 2004
Batch ID 03020
Dilution Factor 1.0
Zinc (TCLP)
Zinc (TCLP), mg/1 9.3
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.02.99
Analyst EM
Analysis Date 03.04.99
Analysis Time 2004
Batch ID 03020
Dilution Factor 1.0

• S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 5
DATE/
TIME SAMPLED
11332-1 Penstock Sludge
02-26-99/1300
PARAMETER
11332-1
Semivolatiles in TCLP Extract (8270)
Cresol (ortho) (TCLP), mg/1
Cresol m & p (TCLP) , mg/1
Cresol o,m,p (TCLP), mg/1
1,4-Dichlorobenzene (TCLP), mg/1
2,4-Dinitrotoluene (TCLP), mg/1
Hexachlorobenzene (TCLP), mg/1
Hexachiorobutadiene (TCLP), mg/1
Hexachloroethane (TCLP), mg/1
Nitrobenzene (TCLP), mg/1
Pentachlorophenol (TCLP), mg/1
2,4,5-Trichlorophenol (TCLP), mg/1
2,4,6-Trichlorophenol (TCLP), mg/1
Pyridine (TCLP) , mg/1
Surrogate-2FP
Surrogate-PHL
Surrogate-NBZ
Surrogate-2FBP
Surrogate-TBP
Surrogate-TPH
TCLP (1311) Sec. 7.2 Extraction Date
Extraction Date (Extract)
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.25
<0.050
<0.050
<0.25
80 %
84 %
80 %
84 %
92 *
104 %
03.01.99
03.02.99
03.02.99
CJR
03.05.99
0737
0302C
1.0

a
5
B L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 6
DATE/
TIME SAMPLED
11332-1 Penstock Sludge
02-26-99/1300
PARAMETER
11332-1
Volatiles in TCLP Extract (8260)
Benzene (TCLP), mg/1
Carbon tetrachloride (TCLP), mg/1
Chlorobenzene (TCLP), mg/1
Chloroform (TCLP) , mg/1
1,2-Dichloroethane (TCLP), mg/1
1,1-Dichloroethylene (TCLP), mg/1
Methyl ethyl ketone (TCLP), mg/1
Tetrachloroethylene (TCLP), mg/1
Trichloroethylene (TCLP), mg/1
Vinyl chloride (TCLP), mg/1
Surrogate - Toluene-d8
Surrogate - 4-Bromofluorobenzene
Surrogate - Dibromofluoromethane
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.020
<0.020
<0.020
<0.020
<0.020
<0.020
<0.10
<0.020
<0.020
<0.040
100 %
95 Is
110 %
ES
03.05.99
1536
1L0305
1.0

S
L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 7
DATE/
SAMPLE DESCRIPTION , SOLID OR SEMISOLID SAMPLES TIME SAMPLED
11332-1
Penstock Sludge 02-26-99/1300
PARAMETER
11332-1
PCB's (8082)
Aroclor-1016, ug/kg dw <4900
Aroclor-1221, ug/kg dw <10000
Aroclor-1232, ug/kg dw <4900
Aroclor-1242, ug/kg dw <4900
Aroclor-1248, ug/kg dw 8700
Aroclor-1254, ug/kg dw 7200
Aroclor-1260, ug/kg dw 6500
Surrogate - TCX *F33
Prep Date 03.01.99
Analyst SG
Analysis Date 03.05.99
Analysis Time 1137
Batch ID 0301Q
Dilution Factor 100.0

•,.
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 8
DATE/
TIME SAMPLED
11332-2
Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Biochemical Oxygen Demand (5-Day) (405.1)
Biochemical Oxygen Demand (5 Day), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Suspended Solids (160.2)
Suspended Solids, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
pH (150.1)
pH, units
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution
Date
Time
Factor
5.5
02.28.99
JE
02.28.99
1205
0228A
410
03.02.99
JH
03.03.99
1000
0303B
2.0
6.7
02.28.99
JE
02.28.99
1120
0228A
1.0

S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 9
DATE/
SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
11332-2
Penstock Sump 02-26-99/1130
PARAMETER 11332-2
Settleable Matter (Imhoff), ml/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Oil & Grease (Hexane Extractable Material) (1664)
Oil & Grease (Hexane Extractable Material), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Total Recoverable Phenolics (420.2)
Phenolics, Total Recoverable, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
15
03.03.99
PB
03.03.99
1000
0303A
1.0
45
03.03.99
LG
03.04.99
0900
0303A
1.0
<0.050
03.03.99
WB
03.04.99
1635
0303A
1.0

A .�.
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 10
DATE/
TIME SAMPLED
11332-2 Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Chemical Oxygen Demand (410.2)
Chemical Oxygen Demand, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Ammonia-N (350.1)
Ammonia-N, mg/1
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution
Date
Time
Factor
Cyanide (335.4)
Cyanide, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
84
03.03.99
RD
03.04.99
1710
0303B
1.0
0.39
03.02.99
DM
03.02.99
0807
0302B
1.0
<0.010
03.04.99
LH
03.04.99
1856
0304S
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 11
DATE/
TIME SAMPLED
11332-2 Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Aluminum (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Beryllium (200.7),
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cadmium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
mg/1
16
03.01.99
CK
03.02.99
2011
0301H
1.0
<0.0040
03.01.99
CK
03.02.99
2011
0301H
1.0
0.013
03.01.99
CK
03.02.99
2011
0301H
1.0

•Ai
.1•
a r
S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 12
DATE/
TIME SAMPLED
11332-2 Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Chromium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Copper (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
0.16
03.01.99
CK
03.02.99
2011
0301H
1.0
0.25
03.01.99
CK
03.02.99
2011
0301H
1.0
<0.040
03.01.99
CK
03.02.99
2011
0301H
1.0

P,
Y
L.
• •
-SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 13
DATE/
TIME SAMPLED
11332-2 Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Selenium (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Zinc (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Mercury (245.1)
Mercury, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.01.99
CK
03 .02 .99
2011
0301H
1.0
2.7
03.01.99
CK
03.02 .99
2011
0301H
1.0
0.00082
03.03.99
BJB
03.03.99
0853
0303R
1.0

-SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 14
DATE/
TIME SAMPLED
11332-2 Penstock Sump
02-26-99/1130
PARAMETER
11332-2
Lead (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Lead (Dissolved) (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
7.4
03.01.99
CK
03.02.99
2011
0301H
1.0
0.22
03.01.99
CK
03.02.99
2016
0301H
1.0

{ t~
4 f
SI SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR S
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 15
DATE/
OLID/SEMISOLID TIME SAMPLED
11332-3
11332-4
11332-5
11332-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-3
11332-4 11332-5 11332-6
PCB's (8082)
Aroclor-1016,
Aroclor-1221,
Aroclor-1232,
Aroclor-1242,
Aroclor-1248,
Aroclor-1254,
Aroclor-1260,
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Surrogate - TCX
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
dw
dw
dw
dw
dw
dw
dw
<33 67
<67
<33
<33
<33
<33
<33 80
76 % 101 %
03.01.99 03.01.99
SG SG
03.03.99 03.03.99
1242 1416
0301Q 0301Q
1.0 1.0
2.0
6.0
5.6
2.5
5.6
6.3
1.7
33
67
33
33
33
33
33
SG SG

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 16
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 11332-7
Metals in TCLP Extract (6010)
Arsenic (TCLP-6010), mg/1 <0.20
Barium (TCLP-6010), mg/1 <1.0
Cadmium (TCLP-6010), mg/1 <0.10
Chromium (TCLP-6010), mg/1 <0.20
Lead (TCLP-6010), mg/1 <0.20
Selenium (TCLP-6010), mg/1 <0.50
Silver (TCLP-6010), mg/1 <0.10
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.02.99
Analyst EM
Analysis Date 03.04.99
Analysis Time 1957
Batch ID 03020
Dilution Factor 1.0
Mercury in TCLP Extract (7470)
Mercury (TCLP-7470), mg/1 <0.020
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.03.99
Analyst BJB
Analysis Date 03.03.99
Analysis Time 0907
Batch ID 0303R
Dilution Factor 1.0

t.
•
• f
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 17
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 11332-7
Antimony (TCLP) (6010)
Antimony (TCLP) , mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (TCLP)
Nickel (TCLP-6010) , mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.020
03.01.99
03.02.99
EM
03.04.99
1957
03 020
1.0
<0.040
03.01.99
03.02.99
EM
03.04.99
1957
03020
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 18
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 11332-7
Beryllium (TCLP)
Beryllium (TCLP-6010), mg/1 <0.0040
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.02.99
Analyst EM
Analysis Date 03.04.99
Analysis Time 1957
Batch ID 03020
Dilution Factor 1.0
Thallium in TCLP Extact (6010)
Thallium (TCLP), mg/1 <0.010
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Prep Date 03.02.99
Analyst EM
Analysis Date 03.04.99
Analysis Time 1957
Batch ID 03020
Dilution Factor 1.0

S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 19
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 11332-7
Vanadium (TCLP) (6010)
Vanadium (TCLP-6010), mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Zinc (TCLP)
Zinc (TCLP), mg/1
TCLP (1311) Sec. 7.2 Extraction Date
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.01.99
03.02.99
EM
03.04.99
1957
03020
1.0
<0.020
03.01.99
03.02.99
EM
03.04.99
1957
03020
1.0

` S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 20
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 11332-7
Semivolatiles in TCLP Extract (8270)
Cresol (ortho) (TCLP), mg/1 <0.050
Cresol m & p (TCLP) , mg/1 <0.050
Cresol o,m,p (TCLP), mg/1 <0.050
1,4-Dichlorobenzene (TCLP), mg/1 <0.050
2,4-Dinitrotoluene (TCLP), mg/1 <0.050
Hexachlorobenzene (TCLP), mg/1 <0.050
Hexachlorobutadiene (TCLP), mg/1 <0.050
Hexachloroethane (TCLP), mg/1 <0.050
Nitrobenzene (TCLP), mg/1 <0.050
Pentachlorophenol (TCLP), mg/1 <0.25
2,4,5-Trichlorophenol (TCLP), mg/1 <0.050
2,4,6-Trichlorophenol (TCLP), mg/1 <0.050
Pyridine (TCLP), mg/1 <0.25
Surrogate-2FP 84 %
Surrogate-PHL 86 %
Surrogate-NBZ 80
Surrogate-2FBP 84
Surrogate-TBP 80 %
Surrogate-TPH 108 %
TCLP (1311) Sec. 7.2 Extraction Date 03.01.99
Extraction Date (Extract) 03.02.99
Prep Date 03.02.99
Analyst CJR
Analysis Date 03.05.99
Analysis Time 0806
Batch ID 0302C
Dilution Factor 1.0

B L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 21
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11332-7 TCLP Extraction Fluid Blank
PARAMETER 113 3 2 - 7
Volatiles in TCLP Extract (8260)
Benzene (TCLP), mg/1 <0.020
Carbon tetrachloride (TCLP), mg/1 <0.020
Chlorobenzene (TCLP), mg/1 <0.020
Chloroform (TCLP) , mg/1 <0.020
1,2-Dichloroethane (TCLP), mg/1 <0.020
1,1-Dichloroethylene (TCLP), mg/1 <0.020
Methyl ethyl ketone (TCLP), mg/1 <0.10
Tetrachloroethylene (TCLP), mg/1 <0.020
Trichloroethylene (TCLP), mg/1 <0.020
Vinyl chloride (TCLP), mg/1 <0.040
Surrogate - Toluene-d8 101 %
Surrogate - 4-Bromofluorobenzene 98 6
Surrogate.- Dibromofluoromethane 112 %
Analyst ES
Analysis Date 03.05.99
Analysis Time 1609
Batch ID 1L0305
Dilution Factor 1.0

1'
SI SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 10519039
Page 22
DATE/
IQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard Is Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9 11332-10 11332-11
Biochemical Oxygen Demand (5-Day) (405.1)
Biochemical Oxygen Demand (5 Day), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Suspended Solids (160.2)
Suspended Solids, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<2.0 92 %
02.28.99 02.28.99
JE JE
02.28.99 02.28.99
1205 1205
0228A 0228A
<5.0 106 Is
03.02.99 03.02.99
JH JH
03.03.99 03.03.99
1000 1000
0302B 0302B
1.0 1.0
02.28.99
JE
02.28.99
1205
0228A
2.0
02.28.99
JE
02.28.99
1205
0228A
5.0
RD RD

S I SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR LIQUID
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 23
DATE/
SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9 11332-10 11332-11
pH (150.1)
pH, units
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution Factor
Oil & Grease (Hexane Extractable Material)
Oil & Grease (Hexane Extractable
Material), mg/1
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution Factor
Date
Time
Date
Time
JE
(1664)
<5.0
03.03.99
LG
03.04.99
0900
0303A
1.0
112 %
02.28.99
JE
02.28.99
1120
0228A
1.0
102
03.03.99
LG
03.04.99
0900
0303A
1.0
JE JE
40
0.55 5.0
03.03.99
LG
03.04.99
0900
0303A
1.0
03.03.99
LG
03.04.99
0900
0303A
1.0

B L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 24
DATE/
LIQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER 11332-8
11332-9 11332-10 11332-11
Total Recoverable Phenolics (420.2)
Phenolics, Total Recoverable, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Chemical Oxygen Demand (410.2)
Chemical Oxygen Demand, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.050 112 % 0.0090
03.03.99 03.03.99
WB WB WB
03.04.99 03.04.99
1635 1635
0303A 0303A --
1.0 1.0
<20 88 * 9.6
03.03.99 03.03.99
RD RD RD
03.04.99 03.04.99
1710 1710 --
0303B 0303B
1.0 1.0
0.050
WB
20
RD

� rr
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 25
DATE/
LIQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9 11332-10 11332-11
Ammonia-N (350.1)
Ammonia-N, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cyanide (335.4)
Cyanide, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.030-
03.02.99
DM
03.02.99
0801
0302B
1.0
<0.010
03.04.99
LH
03.04.99
1856
0304S
1.0
103 % 0.015 0.030
03.02.99 03.02.99 03.02.99
DM DM DM
03.02.99 03.02.99 03.02.99
0800
0302B 0302B 0302B
1.0 1.0 1.0
107 * 0.0013 0.010
03.04.99 ---
LH LH LH
03.04.99 ---
1856 0304S
1.0

.SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 26
DATE/
IQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard 1 Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9
11332-10 11332-11
Aluminum (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Beryllium (200.7),
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cadmium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
mg/1
<0.20.
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.0040
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.0050
03.01.99
CK
03.02.99
1835
0301H
1.0
110 1
03.01.99
CK
03.02.99
1840
0301H
1.0
106 1
03.01.99
CK
03.02.99
1840
0301H
1.0
109 1
03.01.99
CK
03.02.99
1840
0301H
1.0
0.027 0.20
CK CK
0.00054 0.0040
CK CK
0.00071 0.0050
CK CK

•
y • i
SI SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 27
DATE/
IQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9 11332-10 11332-11
Chromium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Copper (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.020.
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.040
03.01.99
CK
03.02.99
1835
0301H
1.0
108 %
03.01.99
CK
03.02.99
1840
0301H
1.0
106 %
03.01.99
CK
03.02.99
1840
0301H
1.0
108
03.01.99
CK
03.02.99
1840
0301H
1.0
0.0017 0.010
CK CK
0.00090
CK
0.020
CK
0.0047 0.040
CK CK

* 4'
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
•
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 28
DATE/
IQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard W Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9 11332-10 11332-11
Selenium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Zinc (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Mercury (245.1)
Mercury, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.020
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.00020
03.03.99
BJB
03.03.99
0842
0303R
1.0
106 W
03.01.99
CK
03.02.99
1840
0301H
1.0
110 %
03.01.99
CK
03.02.99
1840
0301H
1.0
0.0042 0.010
CK CK
0.0059 0.020
CK CK
<0.00020 0.000072 0.00020
03.03.99
BJB BJB BJB
03.03.99
0850
0303R
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11332
Received: 27 FEB 99
Reported: 08 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 13549038
Page 29
DATE/
IQUID SAMPLES TIME SAMPLED
11332-8
11332-9
11332-10
11332-11
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11332-8
11332-9
11332-10 11332-11
Lead (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Lead (Dissolved) (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.0050..
03.01.99
CK
03.02.99
1835
0301H
1.0
<0.0050
03.01.99
CK
03.02.99
1845
0301H
1.0
106 1
03.01.99
CK
03.02.99
1840
0301H
1.0
106 1
03.01.99
CK
03.02.99
1840
0301H
1.0
0.0015 0.0050
CK CK
0.0015 0.0050
CK CK
Methods: EPA SW-846, Update III.
Methods: EPA 40 CFR Part 136
*F33 = Because the sample was diluted prior to analysis, surrogate recoveries
are not reported.
5(:^P.e-/q
Steven J. Whit Project Manager
Final Page Of Report

Serial Number 1.1, v U ( i
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SLSAVANNAH LABORATORIES O 5102 LaRoche Avenue, Savannah, GA 31404 Phone: [phone] Fax: [phone],
O 2846 Industrial Plaza Drive, Tallahassee, FL 32301 Phone: [phone] Fax: [phone]
SERVICES, INC.
& ENVIRONMENTAL O 414 SW 12th Avenue, Deerfield Beach, FL 33442 Phone: [phone] Fax: [phone]
O 900 Lakeside Drive, Mobile, AL 36693 Phone: [phone] Fax: [phone]
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD p 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Phone: [phone] Fax: [phone]
ED 100 Alpha Drive, Suite 110, Destrehan, LA 70047 Phone: [phone] Fax: [phone]
PROJECT REFERENCE
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DATE
TIME
RELINQUISHED BY: (SIGNATURE)
DATE
TIME
RECEIVED BY: (SIGNATURE)
i AT TIME
RECEIVED BY: (SIGNATURE)
DATE
TIME
RECEIVED BY: (SIGNATURE)
DATE
TIME
LABORATORY USE ONLY .
RECEIVED;.FORLABORATORYBY:(SIGNATURE)
DAT
TIME
CUSTODY INTACT
CUSTODY SEAL Na
SL,LOGNO
LABORATORY REMARKS:•
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0

.
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 1
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Suspended Solids (160.2)
Suspended Solids, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Biochemical Oxygen Demand (5-Day) (405.1)
Biochemical Oxygen Demand (5 Day), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Settleable Matter (Imhoff), ml/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
10
03.16.99
JH
03.17.99
0930
0316A
1.0
<2.0
03.16.99
JE
03.16.99
1510
0316A
1.0
<0.20
03.16.99
PB
03.16.99
1400
0316A
1.0
Cc 4613-
von
ors - YoDI6A-i
ie. G. 1.6frciete - yooz,A1
y.,1: 'He - yopee,,„i
,170.

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 2
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
pH (150.1)
pH, units
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Oil & Grease (Hexane Extractable Material) (1664)
Oil & Grease (Hexane Extractable Material), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Total Recoverable Phenolics (420.2)
Phenolics, Total Recoverable, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
6.5
03.16.99
JE
03.16.99
1140
0316A
1.0
<5.0
03.18.99
LG
03.19.99
0700
0318A
1.0
<0.050
03.19.99
AW
03.19.99
1100
0319A
1.0

I r
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 3
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Chemical Oxygen Demand (410.2)
Chemical Oxygen Demand, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Ammonia-N (350.1)
Ammonia-N, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cyanide (335.4)
Cyanide, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<20
03.17.99
JH
03.18.99
0950
0317A
1.0
0.14
03.18.99
DM
03.18.99
0802
0318C
1.0
<0.0050
03.22.99
LR
03.22.99
1329
0322S
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO:
Received:
Reported:
S9-11667
16 MAR 99
24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 4
DATE/
TIME SAMPLED
11667-1
N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Arsenic (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Barium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Silver (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.16.99
CK
03.19.99
1649
0316H
1.0
0.040
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.010
03.16.99
CK
03.19.99
1649
0316H
1.0

t
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 5
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Aluminum (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Beryllium (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cadmium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
0.97
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.0040
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.0050
03.16.99
CK
03.19.99
1649
0316H
1.0

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 6
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Chromium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Copper (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.020
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.040
03.16.99
CK
03.19.99
1649
0316H
1.0

BL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client P0. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 7
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Selenium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Zinc (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Mercury (245.1)
Mercury, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.16.99
CK
03.19.99
1649
0316H
1.0
0.21
03.16.99
CK
03.19.99
1649
0316H
1.0
<0.00020
03.16.99
BJB
03.16.99
2159
0316R
1.0

-SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 8
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Lead (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Lead (Dissolved) (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
0.30
03.16.99
CK
03.19.99
1649
0316H
1.0
0.057
03.16.99
CK
03.19.99
1645
0316H
1.0

-SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 9
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Volatiles in TCLP Extract (8260)
Benzene (TCLP), mg/1
Carbon tetrachloride (TCLP), mg/1
Chlorobenzene (TCLP), mg/1
Chloroform (TCLP) , mg/1
1,2-Dichloroethane (TCLP), mg/1
1,1-Dichloroethylene (TCLP), mg/1
Methyl ethyl ketone (TCLP), mg/1
Tetrachloroethylene (TCLP), mg/1
Trichloroethylene (TCLP), mg/1
Vinyl chloride (TCLP), mg/1
Surrogate - Toluene-d8
Surrogate - 4-Bromofluorobenzene
Surrogate - Dibromofluoromethane
TCLP (1311) Sec. 7.3 Extraction Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.020
<0.020
<0.020
<0.020
<0.020
<0.020
<0.10
<0.020
<0.020
<0.040
100 I
95 1
105 1
03.17.99
ES
03.23.99
0732
2L0322
1.0

'SLSAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 10
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
Semivolatiles in TCLP Extract (8270)
Cresol (ortho) (TCLP), mg/1
Cresol m & p (TCLP) , mg/1
Cresol o,m,p (TCLP), mg/1
1,4-Dichlorobenzene (TCLP), mg/1
2,4-Dinitrotoluene (TCLP), mg/1
Hexachlorobenzene (TCLP), mg/1
Hexachlorobutadiene (TCLP), mg/1
Hexachloroethane (TCLP), mg/1
Nitrobenzene (TCLP), mg/1
Pentachlorophenol (TCLP), mg/1
2,4,5-Trichlorophenol (TCLP), mg/1
2,4,6-Trichlorophenol (TCLP), mg/1
Pyridine (TCLP), mg/1
Surrogate-2FP
Surrogate-PHL
Surrogate-NBZ
Surrogate-2FBP
Surrogate-TBP
Surrogate-TPH
TCLP (1311) Sec. 7.2 Extraction Date
Extraction Date (Extract)
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.25
<0.050
<0.050
<0.25
80 %
82 1
88 1
88 1
90 1
96 1
03.15.99
03.16.99
03.16.99
KH
03.18.99
1518
0316A
1.0

S L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 11
DATE/
TIME SAMPLED
11667-1 N-SUMP-1
03-15-99/1520
PARAMETER
11667-1
PCB's (8082)
Aroclor-1016, ug/1
Aroclor-1221,.ug/1
Aroclor-1232, ug/1
Aroclor-1242, ug/1
Aroclor-1248, ug/1
Aroclor-1254, ug/1
Aroclor-1260, ug/1
Surrogate - TCX
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
50 Is
03.16.99
TG
03.18.99
2032
0316N
1.0

taLSAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 12
DATE/
SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11667-2 TCLP Method Blank
PARAMETER
11667-2
Volatiles in TCLP Extract (8260)
Benzene (TCLP) , mg/1
Carbon tetrachloride (TCLP), mg/1
Chlorobenzene (TCLP), mg/1
Chloroform (TCLP) , mg/1
1,2-Dichloroethane (TCLP), mg/1
1,1-Dichloroethylene (TCLP), mg/1
Methyl ethyl ketone (TCLP), mg/1
Tetrachloroethylene (TCLP), mg/1
Trichloroethylene (TCLP), mg/1
Vinyl chloride (TCLP), mg/1
Surrogate - Toluene-d8
Surrogate - 4-Bromofluorobenzene
Surrogate - Dibromofluoromethane
TCLP (1311) Sec. 7.3 Extraction Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.020
<0.020
<0.020
<0.020
<0.020
<0.020
<0.10
<0.020
<0.020
<0.040
100 %
90 %
110 Is
03.17.99
ES
03.23.99
1709
1L0323
1.0

BL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 13
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11667-2 TCLP Method Blank
PARAMETER 11667-2
Semivolatiles in TCLP Extract (8270)
Cresol (ortho) (TCLP), mg/1 <0.050
Cresol m & p (TCLP), mg/1 <0.050
Cresol o,m,p (TCLP), mg/1 <0.050
1,4-Dichlorobenzene (TCLP), mg/1 <0.050
2,4-Dinitrotoluene (TCLP), mg/1 <0.050
Hexachlorobenzene (TCLP), mg/1 <0.050
Hexachlorobutadiene (TCLP), mg/1 <0.050
Hexachloroethane (TCLP), mg/1 <0.050
Nitrobenzene (TCLP), mg/1 <0.050
Pentachlorophenol (TCLP), mg/1 <0.25
2,4,5-Trichlorophenol (TCLP), mg/1 <0.050
2,4,6-Trichlorophenol (TCLP), mg/1 <0.050
Pyridine (TCLP), mg/1 <0.25
Surrogate-2FP 72 $
Surrogate-PHL 74 $
Surrogate-NBZ 72
Surrogate-2FBP 80 %
Surrogate-TBP 82 %
Surrogate-TPH 80 %
TCLP (1311) Sec. 7.2 Extraction Date 03.15.99
Extraction Date (Extract) 03.16.99
Prep Date 03.16.99
Analyst KH
Analysis Date 03.18.99
Analysis Time 1819
Batch ID 0316A
Dilution Factor 1.0

BL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 14
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11667-2 TCLP Method Blank
PARAMETER
11667-2

.SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 15
DATE/
LIQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER 11667-3
11667-4 11667-5 11667-6
Suspended Solids (160.2)
Suspended Solids, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Biochemical Oxygen Demand (5-Day) (405.1)
Biochemical Oxygen Demand (5 Day), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Settleable Matter (Imhoff), ml/1
Analyst
<5.0
03.16.99
JH
03.17.99
0930
0316A
1.0
<2.0
03.16.99
JE
03.16.99
1510
0316A
1.0
PB
104 %
03.16.99
JH
03.17.99
0930
0316A
1.0
88 %
03.16.99
JE
03.16.99
1510
0316A
1.0
PB
5.0
JH JH
2.0
03.16.99
JE
03.16.99
1510
0316A
1.0
PB
2.0
03.16.99
JE
03.16.99
1510
0316A
1.0
0.20
PB

.eLSAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 16
DATE/
TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3 11667-4
11667-5 11667-6
pH (150.1)
pH, units
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution Factor
Oil & Grease (Hexane Extractable Material)
Oil & Grease (Hexane Extractable
Material), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Date
Time
03.16.99
JE
03.16.99
1140
0316A
1.0
(1664)
c5.0
03.18.99
LG
03.19.99
0700
0318A
1.0
115 %
03.16.99
JE
03.16.99
1140
0316A
1.0
91
03.18.99
LG
03.19.99
0700
0318A
1.0
JE JE
04.0,00
0.55 5.0
LG
40.
40
LG

.SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 17
DATE/
IQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Total Recoverable Phenolics (420.2)
Phenolics, Total Recoverable, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Chemical Oxygen Demand (410.2)
Chemical Oxygen Demand, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.050
03.19.99
AW
03.19.99
1100
0319A
1.0
<20
03.17.99
JH
03.18.99
0950
0317A
1.0
99
03.19.99
AW
03.19.99
1100
0319A
1.0
85 %
03.17.99
JH
03.18.99
0950
0317A
1.0
0.0090
AW
0.050
AW
9.6 20
JH JH

.SLSAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR
LOG NO:
Received:
Reported:
Client PO. No.:
S9-11667
16 MAR 99
24 MAR 99
BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 18
DATE/
LIQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Ammonia-N (350.1)
Ammonia-N,
Prep Date
Analyst
Analysis
Analysis
Batch ID
Dilution
mg/1
Date
Time
Factor
Cyanide (335.4)
Cyanide, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.030
03.18.99
DM
03.18.99
0801
0318C
1.0
<0.0050
03.22.99
LR
03.22.99
1329
0322S
1.0
99 %
03.18.99
DM
03.18.99
0800
0318C
1.0
101 %
03.22.99
LR
03.22.99
1329
0322S
1.0
0.015 0.030
03.18.99 03.18.99
DM DM
03.18.99 03.18.99
0318C 0318C
1.0 1.0
0.0013 0.0050
LR LR

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 19
DATE/
•
SAMPLE DESCRIPTION , QC REPORT FOR L
IQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard ' Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Arsenic (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Barium (200.7) ,
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Silver (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
mg/1
<0.010
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.010
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.010
03.16.99
CK
03.19.99
1633
0316H
1.0
103 W
03.16.99
CK
03.19.99
1637
0316H
1.0
105 %
03.16.99
CK
03.19.99
1637
0316H
1.0
105 %
03.16.99
CK
03.19.99
1637
0316H
1.0
0.0032 0.010
RR RR
0.0012 0.010
RR RR
0.0019 0.010
RR RR

S
LSAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 20
DATE/
IQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Aluminum (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Beryllium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Cadmium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.20
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.0040
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.0050
03.16.99
CK
03.19.99
1633
0316H
1.0
103 %
03.16.99
CK
03.19.99
1637
0316H
1.0
105
03.16.99
CK
03.19.99
1637
0316H
1.0
108 %
03.16.99
CK
03.19.99
1637
0316H
1.0
0.027 0.20
RR RR
0.00054
RR
0.0040
RR
0.00071 0.0050
RP. RR
MD MI OD

T q
SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR LIQUID
LOG NO:
Received:
Reported:
Client PO. No.:
S9-11667
16 MAR 99
24 MAR 99
BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 21
DATE/
SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Chromium (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Copper (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Nickel (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.020
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.040
03.16.99
CK
03.19.99
1633
0316H
1.0
107 %
03.16.99
CK
03.19.99
1637
0316H
1.0
105
03.16.99
CK
03.19.99
1637
0316H
1.0
107 $
03.16.99
CK
03.19.99
1637
0316H
1.0
0.0017 0.010
RR RR
0.00090 0.020
RR RR
0.0047
RR
0.040
RR

-SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 22
DATE/
IQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard 1 Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Selenium (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Zinc (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Mercury (245.1)
Mercury, mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.010
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.020
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.00020
03.16.99
BJB
03.16.99
2114
0316R
1.0
105 1
03.16.99
CK
03.19.99
1637
0316H
1.0
104 1
03.16.99
CK
03.19.99
1637
0316H
1.0
96 1
03.16.99
BJB
03.16.99
2117
0316R
1.0
0.0042 0.010
RR RR
0.0059 0.020
RR RR
OP
0.000072
BOB
NO MP
0.00020
BJB

SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
SAMPLE DESCRIPTION , QC REPORT FOR L
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 23
DATE/
IQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (MDL)
Practical Quantitation Limit (PQL)
PARAMETER
11667-3
11667-4 11667-5 11667-6
Lead (200.7), mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
Lead (Dissolved) (200.7) , mg/1
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<0.0050
03.16.99
CK
03.19.99
1633
0316H
1.0
<0.0050
03.16.99
CK
03.19.99
1641
0316H
1.0
105 %
03.16.99
CK
03.19.99
1637
0316H
1.0
105
03.16.99
CK
03.19.99
1637
0316H
1.0
0.0015 0.0050
RR RR
0,0.40
0.0015 0.0050
RR RR
OD OD

�SL
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Larry McCaskill
Aluminum Company of America
P.O. Box 576
Badin, NC 28009
CC: Jamey Jones, Law Engineering
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR
LOG NO: S9-11667
Received: 16 MAR 99
Reported: 24 MAR 99
Client PO. No.: BA149626BA
Project: ALCOA-YADKIN
Sampled By: Client
Code: 143090324
Page 24
DATE/
LIQUID SAMPLES TIME SAMPLED
11667-3
11667-4
11667-5
11667-6
Method Blank
Lab Control Standard % Recovery
Method Detection Limit (Mn.)
Practical Quantitation Limit (PQL)
PARAMETER 11667-3
11667-4 11667-5 11667-6
PCB's (8082)
Aroclor-1016, ug/1
Aroclor-1221, ug/1
Aroclor-1232, ug/1
Aroclor-1242, ug/1
Aroclor-1248, ug/1
Aroclor-1254, ug/1
Aroclor-1260, ug/1
Surrogate - TCX
Prep Date
Analyst
Analysis Date
Analysis Time
Batch ID
Dilution Factor
<1.0 92 %
<2.0 •--
<1.0
<1.0
<1.0
<1.0
<1.0 104 %
50 % 50
03.16.99 03.16.99
TG TG
03.18.99 03.18.99
1757 1859
0316N 0316N
1.0 1.0
0.095
0.35
0.19
0.16
0.17
0.063
0.059
TG
1.0
2.0
1.0
1.0
1.0
1.0
1.0
TG
Methods: EPA SW-846, Update III.
Methods: EPA 40 CFR Part 136
(3111
J%t/i&
Steven J. ite, Project Manager
Final Page Of Report

Serial Number 097013
1...SAVANNAH LABORATORIES 0 5102 LaRoche Avenue, Savannah, GA 31404 Phone: [phone] Fax: [phone]
0 2846 Industrial Plaza Drive, Tallahassee, FL 32301 Phone: [phone] Fax: [phone]
& ENVIRONMENTAL SERVICES, INC. 0 414 SW 12th Avenue, Deerfield Beach, FL 33442 Phone: [phone] Fax: [phone]
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD 0 900 Lakeside Drive, Mobile, AL 36693 Phone: [phone] Fax: [phone]
O 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Phone: [phone] Fax: [phone]
0 100 Alpha Drive, Suite 110, Destrehan, LA 70047 Phone: [phone] Fax: [phone]
REFERENCE
PROJECT NO.
P.O. NUMBER '
PROJECT
ALCc'/- r4-pkj�
MATRIX
TYPE
REQUIRED ANALYSES
PAGE
of
PROJECT LOC.
SAMPLER(s) NAME
PHONE/ ) 3S7_ Q tx..,
.,
(State)N C' .
i- Y
FAX (74,1t) 35? /6 -z i l.
O STANDARD
CLIENT NAME
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CLIENT PROJECT MANAGER � q�d' �� ¢ O I/� REPORT
C O a 4. v q !� ❑ DELIVERY
L. �-R� Y M— �1 L.�. � of h z � " v v
CLIENT ADDRESS (CITY, STATE, ZIP) �l ` V• ,�+ XV -- kv Q„ EXPEDITED REPORT
O �1 h DELIVERY(squvcQhar e)
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/`7f' I� n[ .. , Date ue:. ,rL /_
SAMPLE
a s �► 'a°' } 3 .�
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DATE
TIME
NO.
SAMPLE IDENTIFICATION
�02
NUMBER OF CONTAINERS SIOBMITTED
REMARKS
3-)5-99
15,2e7
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$4,4454) A�Vb1//JC)
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RELINUISH'-' :Y: (SIGNATUR
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DATE
TIME
INQUISHED BY: (SI �.A�/'-
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DATE
3-if.79
TIME
/s
RELINQUISHED BY: (SIGNATURE)
DATE
TIME
Aa 9 l0_'
�
—
/
RE ED B . SIGNAT
)
i, •
DATE
TIME
RECEIVED BY: (SI I ATURE)
DATE
TIME
RECEIVED BY: (SIGNATURE)
DATE
TIME
• LABORATORY USE ONLY
ROZEIVED FORIAl3ORAT.ORY BY7GN.TURE);;
•c,
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TIME
(�
CUSTODY INTACT
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LABORATORY'REMMARKS: .

Yadkin, Inc.
Post Office Box 576
Badin, North Carolina 28009-0576
March 01, 1999
North Carolina Department of
Environment, and Natural Resources
Division of Water Quality
Post Office Box 29535
Raleigh, North Carolina 27626-0535
Attn: Mr. Charles H. Weaver, Jr.
Re: NPDES Permit Applications — Yadkin, Inc.
Falls Powerhouse — NC0076775
Narrows Powerhouse — NC0081957
Tuckertown Powerhouse —NC0081949
High Rock Powerhouse —NC0081931
Gentlemen:
Enclosed are permit applications for the four Yadkin, Inc. hydro -generation plants.
gamin Inc
•
r1
We request consideration of a best management practice (BMP) provision for all permitted outfalls.
Since our discharges consist primarily of non -contact cooling water and the volume of water used to cool
the turbines relative to the total discharge volume is so small, we question the necessity of boiler plate
language in the current permits related to instream temperature rise. Also, since we are not adding
anything to the cooling water which would alter the pH, we question the necessity of boiler plate
language in the current permits related to pH.
You will note that we have added an additional outfall at the Narrows Powerhouse (004). We are
currently in the process of sampling the discharge and will be forwarding the data to you as an
amendment to this application.
Also, .please note that High Rock Powerhouse is actually located in Davidson County; however, during
previous permit renewals, for consistency sake, permitting oversight has been provided from one regional
office. Yadkin requests that this approach to permitting oversight be continued from one regional office.
We do not produce sludge in our process; therefore, a sludge management plan is not included in the
submittal.
Please call me at [phone] should you have questions or comments concerning
this submittal.
Sincer
'Julian Polk, P.E. •
Vice President

NPDES PERMIT APPLICATION - SHORT FORM C
To be filed only by persons engaged in manufacturing and mining
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
P. O. Box 29535, Raleigh, NC 27626-0535
North Carolina NPDES Permit Number
(if known)
1. Applicant and facility producing discharge
A. Name NARROWS POWERHOUSE
NC00 81957
B. Mailing address of applicant: CIO YADKIN, INC.
1. Street address P.O. BOX 576
2. City BADIN 3. County STANLY
4. State NC 5. Zip Code 28009
C. Location of facility:
1. Street NCSR 1704
2. City BADIN 3. County STANLY
4. State NC 5. Zip Code 28009
D. Telephone Number ( 704 ) 422-5637
E. Fax Number (704 ) 422-5776
F. e-mail address [e-mail]
2. Standard Industrial Classification (SIC) code(s): 4911
3. Number of employees: 20
4. Principal product(s) produced:
ELECTRICITY
Principal raw material(s) consumed:
5. Principal process(es): HYDROELECTRIC GENERATION
6. Amount of principal product produced or raw material consumed
(List specific amounts consumed and/or units of production
u;
Product Produced or
Raw Material Consumed
(AVERAGE)
Product Produced or
Raw Material Consumed
(PEAK)
per Day
1403 MEGAWATT HOURS
112 MEGAWATT HOURS
per Month
per Year
7. (a) Check here if discharge occurs all year X, or
(b) Circle the month(s) in which discharge occurs: January February March April
May June July August September October November December
(c) Days per week discharge .occurs: SEVEN
NOTE: If the facility has separate discharge points (outfalls) or multiple industrial processes, include a
schematic diagram of wastewater flow at the facility.
Page 1 of 2
Version 9-97

NPDES PERMIT APPLICATION - SHORT FORM C
To be filed only by persons engaged in manufacturing and mining
8. Types of wastewater discharged to surface waters only (check as applicable).
Discharge per operating day
Flow
(GALLONS PER OPERATING DAY)
Volume treated before discharging
(PERCENT)
Sanitary - daily average
Cooling water, etc. - daily average
1,903,280
0
Process water - daily average
Maximum per operating day for
total discharge (all types)
1,903,280
0
9. If any of the types of wastewater identified in item 8 (either treated or untreated) are discharged to places
other than surface waters, record the amount(s) discharged below:
A. Municipal sewer system gpd
B. Underground well gpd
C. Septic tank gpd
D. Evaporation lagoon or pond gpd
E. Other, specify gpd
10. Number of separate discharge points: 7 (SEVEN)
11. Name of receiving water(s): YADKIN RIVER
12. Does your discharge contain or is it possible for your discharge to contain one or more of the following
substances added as a result of your operations, activities, or processes? Circle all that apply:
aluminum ammonia beryllium cadmium chromium chlorine (residual)
copper cyanide lead mercury nickel
phenols selenium zinc None of the above
I certify that I am familiar with the information contained in the application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
B. JULIAN POLK VICE PRESIDENT
Printed name of Person Signing Title
Ap
plicant
pplicant
re of
01/14/99
Date
North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false statement
representation, or certification in any application, record, report, plan, or other document files or required to be maintained
under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies,
tampers with, or knowly renders inaccurate any recording or monitoring device or method required to be operated or
maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be
guilty of a misdemeanor punishable by a fine not to exceed $10,000, or by imprisonment not to exceed six months, or by
both.
(18 U.S.C. Section 1001 provides a punishment by a fine of not more than $10,000 or imprisonment not more than 5 years, or
both, for a similar offense.)
Page 2 of 2 Version 9-97

NARROWS POWERHOUSE
NPDES PERMIT NO. NC 0004308
Narrows
Unit One
Scroll Case
Yadkin River
Narrows
Unit Two
Scroll Case
Narrows
Unit Three
Scroll Case
Narrows
Unit Four
Scroll Case
Unit One
Units 1,2,3 & 4
Unit Two
Units 1,2,3,& 4
Generator
Thrust Bearing
Generator
Turbine Wheelpits,
Cooling Water
Cooling Water
Cooling Water
and floor drains
432,000 Gal/Day
172,400 Gal/Day
432,000 GaVDay
2,880 Gal/Day
V
Unit Three
Generator
Cooling Water
432,000 Gal/Day
Inspection
Sump
All Units Draft
Tube Leakage
Powerhouse
Sump
II
Penstock leakage
Rainwater
♦
Unit Four
Generator
Cooling Water
432,000 Gal/Day
Outfall # 001
Outfall # 002
Outfall # 006
Outfall # 003
Outfall # 004
Outfall # 005
Outfall # 007
Into Yadkin
Into Yadkin
Into Yadkin
Into Yadkin
Into Yadkin
Into Yadkin
Into Yadkin
River
River
River
River
River
River
River
Unit One Generator
Discharge/24 Hrs.
1,379,894,400 gals.
Unit Two Generator
Discharge/24 Hrs.
1,357,257,600 gals.
Unit Three Generator
Discharge/24 Hrs.
1,583,452,800 gals.
Unit Four Generator
Discharge/24 Hrs.
1,357,257,600 gals.