NCG200516_Monitoring Report_20220401

IMET Alloys
3000 stitt st I suite 150 1 monroe I nc 28110 1 t. [phone] f. [phone] www.imetalloys.com
Via 2nd Dav FedEx
March 30, 2022
NCDEQ/DEMLR
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: DMR March 2022 — NCG200516
IMET Alloys
3000 Stitt Street
Monroe, North Carolina
H&H Project No. IME.004
Dear Madam/Sir:
IMET Alloys (IMET) is submitting the enclosed hard copy of the semi-annual stormwater Discharge
Monitoring Report (DMR) for the site referenced above in accordance with the industrial stormwater
permit (NCG200516).
The result of the analysis for copper (0.0114 mg/1) was above the permit allowable benchmark
concentration (0.010 mg/1) for Outfall 001. Although the copper concentration slightly exceeds the
benchmark value, the copper concentration does not appear to be attributed to site operations as explained
in the August 20, 2019 Tier II Sampling Status letter by Hart & Hickman and the December 20, 2019
Relief from Monthly Monitoring letter by NCDEQ. IMET Alloys will continue semi-annual outfall
monitoring.
Should you have any questions or need any additional information, please feel free to contact me.
Sincerely,
Mike Oruska
Chief Operations Officer
Enclosure
cc: Mr. Gregory Kanellis, Hart & Hickman (via email)
IMET �111r} -t
�� i. 3000 Stitt St I Suite 150 i monroe 1 nC 28110 1 t. [phone] I f. [phone] www.imetalloys.Com

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG200000
Scrap Metal
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG20 0516
Person Collecting Samples: Derek Haskell (Hart & Hickman, PC)
Facility Name: IMET Alloys
Laboratory Name: Pace Analytical
Facility County: Union
Laboratory Cert. No.: 5342
Discharge during this period: El Yes ❑ No ff no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ❑✓ No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via h_tt_ps://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes []No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in Owdl
Parameter
Code
Parameter
Outfall01
Outfall
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
C
N/A
Date Sample Collected MM/DD/YYYY
03/16/2022
46529
24-Hour Rainfall in inches
0.98
C0530
TSS in mg/L (100 or 50*)
28.7
00340
Chemical Oxygen Demand (120)
47.8
00552
Non -Polar Oil & Grease in mg/L (15)
<4.8
01119
Copper, total recoverable in mg/L
0.010 FW, 0.005 SW
0.0114
01051
Lead, total recoverable (as Pb)in
mg/ L 0.075 FW 0.220 SW
<0.0050
C0034
Zinc, total recoverable in mg/L (0.126
FW, 0.095 SW)
0.0499
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average
NCOIL
Estimated New Motor/Hydraulic Oil
Usage In gal/month
uunans to uutstanomg Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified per onnel properly gather and evaluate the Information submitted. Based on my
inquiry of the person or persons who nage the system, tho rsons directly responsible for gathering the information, the information
submitted is, to the best of my k led and belief, t` e, a r , and complete. I am aware that there are significant penalties for submitting
f Ise inf i cludin th ssibil' y of fines a i iso ent for knowing violations."
Signature o er ttee or D egated Authorize ndividual Date
Email Address [e-mail] Phone Number 704-962-1159

i��
PaceAnalytical '
www.pacelabs.com
race Anaiyucai services, uc
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 23, 2022
Greg Kanellis
Hart & Hickman
3921 Sunset Ridge Rd.
Suite 301
Raleigh, NC 27607
RE: Project: IME-004-2
Pace Project No.: 92594035
Dear Greg Kanellis:
Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
ACCJI<c�,.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
B/ without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

FaceAnalytical
wY w.pacelabsxom
race Anaryncai aervrces, LL :
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: IME-004-2
Pace Project No.: 92594035
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cart. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
VirginiaNELAP Certification M 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification M 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 14

,�aceAnalXical w
www,pacelabs.com
race Nnaryucai —wises, LLc
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: IME-004-2
Pace Project No.: 92594035
Lab ID Sample ID
92594035001 SD-01
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 03/16/22 14:15 03/17/22 07:10
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 14

_ aceAnaocal'
www.pacelabs.com
race Ana yucai bervices, uc
9800 Kincey Ave. Suite 100
H u ntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
IME-004-2
Pace Project No.:
92594035
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92594035001
SD-01
EPA 1664B
CoI
1
PASI-C
EPA 200.7 Rev 4.4 1994
KH
3
PASI-A
SM 254OD-2015
ZMC
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 14

,aeAnalj4ical'
www.pacelabs.com
race Hnaryncai oervmes, LLc
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: IME-004-2
Pace Project No.: 92594035
Sample: SD-01
Lab ID: 92594035001 Collected:
03/16/2214:15
Received: 03/17/2207:10 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 16646
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 4.8
4.8 1
03/21/22 09:38
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
11.4 ug/L 5.0
4.3 1
03/18/22 12:06 03/22/22 05:27 7440-50-8
Lead
NO ug/L 5.0
4.5 1
03/18/22 12:06 03/22/22 05:27 7439-92-1
Zinc
49.9 ug/L 10.0
9.5 1
03/18/22 12:06 03/22/22 05:27 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
Total Suspended Solids
28.7 mg/L 8.3
8.3 1
03/18/22 16:20
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
47.8 mg/L 25.0
12.5 1
03/23/22 01:33 03/23/22 05:02
Date: 03/23/2022 12:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 14

�s
FaceAnalytical
www.pacelabs.com
race wnaryncai bervices, Lw
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: IME-004-2
Pace Project No.: 92594035
QC Batch: 685891 Analysis Method: EPA 16648
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92594035001
METHOD BLANK: 3586612
Associated Lab Samples: 92594035001
Parameter Units
Total Petroleum Hydrocarbons
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
3586613
Units
Total Petroleum Hydrocarbons
mg/L
MATRIX SPIKE SAMPLE:
Parameter
3586614
Units
Total Petroleum Hydrocarbons
mg/L
SAMPLE DUPLICATE: 3586615
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed Qualifiers
ND 5.0 5.0 03/21/22 09:38
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
20 15.1 76 64-132
92594138002 Spike MS MS % Rec
Result Cone. Result % Rec Limits Qualifiers
ND 19.2 14.2 66 64-132
35703177001 Dup Max
Result Result RPD RPD Qualifiers
5.OU ND 30
Results presented on this page are in the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14

V
PceAn*Jcal
/ wwwpacelabs.cam
I
race Anatyucat bervlces, t-u:
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: IME-004-2
Pace Project No.: 92594035
QC Batch: 685691
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.41994
Analysis Description:
200.7 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92594035001
METHOD BLANK: 3585529
Matrix: Water
Associated Lab Samples: 92594035001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Copper
ug/L
NO 6.0
4.3 03/22/22 04:35
Lead
ug/L
NO 5.0
4.5 03/22/22 04:35
Zinc
ug/L
NO 10.0
9.5 03/22/22 04:35
LABORATORY CONTROL SAMPLE:
3585530
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits Qualifiers
Copper
ug/L
500 514
103
85-115
Lead
ug/L
500 495
99
85-115
Zinc
ug/L
500 471
94
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585531 3585532
MS MSD
92592966001
Spike Spike MS
MSD
MS MSD % Rec
Max
Parameter Units
Result
Cone. Cone. Result
Result
% Rec % Rec Limits
RPD
RPD Qual
Copper ug/L
ND
500 500 507
514
101 102 70-130
1
20
Lead ug/L
ND
500 500 479
491
96 98 70-130
2
20
Zinc ug/L
57.2
500 500 528
543
94 97 70-130
3
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585533 3585534
MS MSD
92593915007
Spike Spike MS
MSD
MS MSD % Rec
Max
Parameter Units
Result
Cone. Cone. Result
Result
% Rec % Rec Limits
RPD
RPD Qual
Copper ug/L
NO
500 500 499
515
100 103 70-130
3
20
Lead ug/L
ND
500 500 481
494
96 99 70-130
3
20
Zinc ug/L
0.022
500 500 492
506
94 97 70-130
3
20
mg/L
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

o®
FaceAnalytical
WYmpacelabs.corn
race Anatyncar aervices, t-i-c
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: IME-004-2
Pace Project No.: 92594035
QC Batch: 685827
QC Batch Method: SM 254OD-2015
Associated Lab Samples: 92594035001
METHOD BLANK: 3586317
Associated Lab Samples: 92594035001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 3586318
Parameter Units
Total Suspended Solids mg/L
QUALITY CONTROL DATA
Analysis Method: SM 2540D-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed Qualifiers
ND 2.5 2.5 03/18/2216:16
Spike LCS LCS % Rao
Conc. Result % Rec Limits Qualifiers
250 250 100 90-110
SAMPLE DUPLICATE: 3586494
92593358002 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 6800 6800
SAMPLE DUPLICATE: 3586495
92594174001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 186 160
Max
RPD RPD Qualifiers
0 25
Max
RPD RPD Qualifiers
15 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 14

v®
PaceAnalytical
wmi.pacelabs.com
race Amnyucat Jervlces, u-c
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: IME-004-2
Pace Project No.: 92594035
QC Batch: 686295
Analysis Method:
SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description:
5220D COD
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92594035001
METHOD BLANK: 3588145
Matrix: Water
Associated Lab Samples: 92594035001
Blank Reporting
Parameter Units
Result Limit
MDL Analyzed Qualifiers
Chemical Oxygen Demand mg/L
NO 25.0 12.5 03/23/22 04:57
LABORATORY CONTROL SAMPLE: 3588146
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 796
106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3588147 3588148
MS MSD
92593307001
Spike Spike MS
MSD MS MSD % Rec
Max
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits
RPD RPD Qual
Chemical Oxygen Demand mg/L 276
100 100 295
647 19 371 90-110
75 3 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3588149
3588150
MS MSD
92593307002
Spike Spike MS
MSD MS MSD % Rec
Max
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits
RPD RPD Qual
Chemical Oxygen Demand mg/L 145
100 100 247
259 102 114 90-110
5 3 M1,R1
Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, I.I.C. Page 9 of 14

hceAnalytical
tvvnv.pacelabs.cam
race anajyncai services, LLo
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: IME-004-2
Pace Project No.: 92594035
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcroleln and Acrylonitrile by EPA
Method 8260.
N-Nitrosodlphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, I.I.C.
Page 10 of 14

,ae A nalj4ica
www.pacelabs.com
race Anaryecai services, uc
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
IME-004-2
92594035
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92594035001
SD-01
EPA1664B
685891
92594035001
SD-01
EPA 200.7 Rev 4.4 1994
685691
EPA 200.7 Rev 4.4 1994
685807
92594035001
SD-01
SM 2540D-2015
685827
92594035001
SD-01
SM 5220D-2011
686295
SM 5220D-2011
686578
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2022 12:28 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 14

Document Name: Document Revised: November 15, 2021
=aceAna1jP4tica1C'Sample Conditfon U on Recelpt SCUR Page 1 of 2
Document No.: Issuing Authority:
F•CAR•CS-033•Rev.OB Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvillen Raleigh[] Mechanicsville[] Atlanta❑ Kernersville❑
Client Name:
Wo11 : 92594035
IIp rrProject #:
Courier: Fed Ex ❑UPS USPS ❑Ckent
oPace []Other:_
!!IIIIIIIIIIIIII�'l)❑Commercial
Custody Seal Present? [--]Yes,QNo Seals Intact? ❑I�ld
94035Yes
Date/Initials Person Examining Contenp:% / �Z-
Packing Material: 08ubble Wrap Pubble Bags []None ❑ Other
Biological Tissue Frozen?
Thermometer;
WIRGun ID: 6J'Z: ,"-0J# Qwet []Blue
[]No �'N/A
[]None
Type of ice:
Correction Factor:
Cooler Temp: Add/Subtract (°C)
Temp should be above freezing to VC
Cooler-Temp{orrect CCJ: -__._
❑Samples out of temp criteria. Samples on ice, cooling process
nas bfgan--------
USDA Regulated Sol) ( N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
❑Yes ❑No -
Did samples originate from a foreign source linternationally,
.
Including Hawaii and Puerto Rlron I—lya. r'lu„
Chain
Rush
Correct Containers Used? 10Yes (:)No ❑N/A i 6.
Intact?
urssoweo anal sls: Samples Field Filtered? Oyes ❑No uN/A a,
Sample Labels Match COC?jC'es ONO ❑N/A 9.
Trip Blank Present?
I trip manic Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION Lot ID of split containers:
Person contacted:
Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Field Data Required? ❑Yes []NO
Page 12 of 14

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