NCG060396_Monitoring Report_20220406

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
v
Complete, sign, scan and submit the DMR via the Sinrrnwater NPDFS Permit Dam Monitoring Report (DMR) Uploa� rm within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Rel�'�analy it<_�_.
Certificate of Coverage No. NCG06 0396
Person Collecting Samples: Madison Shoemaker
Facility Name: Amazon.com Services LLC - CLT3
Laboratory Name: Eurofins TestAmerica
Facility County: Cabarrus
Laboratory Cert. No.: 269
Discharge during this period: X❑ Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ® No
If so, which Tier (I, II, or III)?
A copy of this DMR has be n uploaded electronically via htt s: edocs.deq ncRov Forms SW—DMR El Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in
Parameter
Code
Parameter
Outfall 001
Outfall 002
Outfall 003
Outfall004
Outfall
N/A
Receiving Stream Class
C
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
02 04 2022
02 04 2022
02 04 2022
02 04 2022
46529
24-Hour Rainfall in inches
0.28
0.28
0.28
0.28
C0530
TSS in mg/L (1.00 or 50*)
2.7
12
4.8
10
00400
pH in standard units (6.0— 9.0 FW,
8.01
7.71
7.39
7.89
31616
Fecal Coliform per 100 ml of
freshwater (if required) (1000)
N/A
N/A
N/A
N/A
61211
Enterococci per 100 ml of saltwater
(if required) y':-
N/A
N/A
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
<5.0
<5.0
5.4
12
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic
oil on average
NCOIL
Estimated New Motor/Hydraulic Oil
Usage in gal/month
N/A
N/A
N/A
N/A
00552
Non -Polar Oil & Grease in mg/L
N/A
_N/A
N A
N/A
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of All other water classifications have a benchmark of
(Freshwater) (Saltwater)
Notes (optional):
"1 certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personner properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, inm14ingKy
e possibility of fines and imprisonment for knowing violations."
Cib...... I'. Of P. k - '�iolebbatedl Authorized Individual
vvvijayk@amazro_n_.ccom
Email Address
Date
484-252-1748
Phone Number

...,. LINKS
I
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-211023-1
Client Project/Site: Storm Water - Amazon Warehouses CLT3
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
RoxaAtu. 6"rVS
'°6 < U
you,
O�
Authorized for release by:
212312022 7:06: 95 PM
Roxanne Cisneros, Senior Project Manager
[phone]
roxanne.cisneros [e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Defirnon_q n-c--,,-eat ry
Client: ERM-West Job ID: 680-211023-1
Project/Site: Storm Water - Amazon Warehouses CLT3
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
0 Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
MIL Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantltatlon Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 12 2/23/2022

Sarn�©Oc� S�rn�mary
Client: ERM-West Job ID: 680-211023-1
Project/Site: Storm Water - Amazon Warehouses CLT3
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
680-211023-1
CLT3_Sample_Point 01_20220204
Water
02/04/2210:39
02/08/2210:50
680-211023-2
CLT3_Sample_Point 02_20220204
Water
02/04/2210:26
02/08/2210:50
680-211023-3
CLT3_Sample_Point 03_20220204
Water
02/04/2210:19
02/08/2210:50
680-211023-4
CLT3_Sample_Point 04_20220204
Water
02/04/22 09:45
02/08/22 10:50
Page 3 of 12 Eurofins -*M202

Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Job ID: 680-211023-1
Job ID: 680-211023-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-211023-1
Comments
No additional comments.
Receipt
The samples were received on 2/8/2022 10:50 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.20 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Page 4 of 12 Eurofins Savannah
2/23/2022

Client: ERM-West fieM Sample Results
Project/Site: Storm Water -- Amazon Warehouses CLT3
Client Sample ID: CLT3_Sample_Point_01_20220204
Date Collected: 02/04/22 10:39
Date Received: 02/08/22 10:50
General Chemistry
Analyte
Chemical Oxygen Demand
LTotal Suspended Solids
Job ID: 680-211023-1
Lab Sample ID: 680-211023-1
Matrix: Water
Result Qualifier
RL
MDL Unit
Client Sample ID: CLT3_ Sample_Point_02_20220204
Date Collected: 02/04/22 10:26
Date Received: 02/08/22 10:50
General Chemistry
Analyte Result Qualifier RL
Chemical Oxygen Demand <5.0 10
Total Suspended Solids 12 2.5
Client Sample ID: CLT3_Sample_Point 03_20220204
Date Collected: 02/04/22 10:19
Date Received: 02/08/22 10:50
General Chemistry
A It
D Prepared Analyzed
02/17/22 1056
Dil Fac
1
1
Lab Sample ID: 680-211023-2
Matrix: Water
MDL Unit D Prepared Analyzed Dil Fac
5.0 mg/L 02/17/2210:56 1
2.5 mg/L 02/08/22 19:37 1
na y e
Keswt Qualifier
RL
MDL
Unit
Chemical Oxygen Demand
5.4 J
10
5.0
mg/L
Total Suspended Solids
4.8
2.5
2.5
mg/L
Vnent sample ID: CLT3_Sample_Point_04 20220204
Date Collected: 02/04/22 09:46
Date Received: 02/08/22 10:50
General Chemistry
Analyte Result Qualifier RL
Chemical Oxygen Demand 12 10
Total Suspended Solids 1 O 2.5
Lab Sample ID: 680-211023-3
Matrix: Water
D Prepared Analyzed Dil Fac
02/17/22 10:56 1
02/08/22 19:37 1
Lab Sample ID: 680-211023-4
Matrix: Water
MDL Unit D Prepared Analyzed Dil Fac
5.0 mg/L 02/17/2210:56 1
2.5 mg/L 02/08/22 19:37 1
Page 5of12
Eurofins Savannah
2/23/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Method: 5220D-2011 - Chemical Oxygen Demand
F Lab Sample ID: MB 680-707396/3
Matrix: Water
Analysis Batch: 707395
MB MB
Analyte Result Qualifier RL
LChemical Oxygen Demand <5.0
MDL
10
5.0
I
Lab Sample ID: LCS 680-707395/4
Matrix: Water
Analysis Batch: 707395
Spike LCS
LCS
Analyte Added Result
Quail
- Chemical Oxygen Demand 50.0 48.6
Method: SM 2540D - SolidS, Total Suspended (TSS)
Lab S 1 ID
Job ID: 680-211023-1
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
02/17/221056 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
nit D %Rec Limits
g/L 97 90 -110
amp e . MB 680-70617Ulf 9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 706170
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dill Fac
Total Suspended Solids <2.5
2.5 2.5 mg/L
02/08/22 19:37 1
Lab Sample ID: LCS 680-706170/2
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 706170
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Total Suspended Solids
951
828
mg/L 87 80-120
Lab Sample ID: LCSD 680-706170/3
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Analysis Batch: 706170
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Total Suspended Solids
951
842
mg/L 89 80-120 2 25
Eurofins Savannah
Page 6 of 12 2/23/2022

CSC Association Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Job ID: 680-211023-1
General Chemistry
Analysis Batch: 706170
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-211023-1
CLT3_Sample_Point_01_20220204
Total/NA
Water
SM 254 DD
680-211023-2
CLT3_Sample_Point_02_20220204
Total/NA
Water
SM 2540D
680-211023-3
CLT3_ Sample_ Point_03_20220204
Total/NA
Water
SM 2540D
680-211023-4
CLT3_Sample_Point_04_20220204
Total/NA
Water
SM 2540D
MB 680-706170/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-706170/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-706170/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 707395
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-211023-1
CLT3_Sample_Point_01_20220204
Total/NA
Water
522OD-2011
680-211023-2
CLT3_ Sample_ Point_02_20220204
Total/NA
Water
5220D-2011
680-211023-3
CLT3_Sample_Point_03_20220204
Total/NA
Water
5220D-2011
680-211023-4
CLT3_Sample_Point_04_20220204
Total/NA
Water
5220D-2011
MB 680-707395/3
Method Blank
Total/NA
Water
5220D-2011
LCS 680-707395/4
Lab Control Sample
Total/NA
Water
5220D-2011
I� tUrufliiS Savannah
ailiiah
i
Page 7 of 12 2/23/2022

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water -Amazon Warehouses CLT3
Client Sample ID: CLT3_Sample_Point_01_20220204
Date Collected: 02/04/22 10:39
Date Received: 02/08/22 10:50
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 5220D-2011
Instrument ID: SPC7
Total/NA Analysis SM 2540D
Instrument ID: NOEQUIP
Job ID: 680-211023-1
Lab Sample ID: 680-211023-1
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
1
2 mL
2 mL
707395
02/17/22 10:56 ALG TAL SAV
1 1000 mL 1000 mL 706170 02/08/22 19:37 PG TAL SAV
client Sample ID: CLT3_Sample_Point_02_20220204
Date Collected: 02/04/22 10:26
Date Received: 02/08/22 10:50
Batch Batch
Prep Type Type Method
Total/NA Analysis 5220D-2011
Instrument ID: SPC7
Total/NA Analysis SM 2540D
Instrument ID: NOEQUIP
Lab Sample ID: 680-211023-2
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
1
2 mL
2 mL
707395
02/17/22 10:56 ALG TAL SAV
1
1000 mL
1000 mL
706170
02/08/22 19:37 PG TAL SAV
client Sample ID: CLT3_ Sample_Point_03_20220204
Date Collected: 02/04/22 10:19
Date Received: 02/08/22 10:60
Batch Batch
Dil Initial
Prep Type Type Method
Run Factor Amount
Total/NA Analysis 5220D-2011
1 2 mL
Instrument ID: SPC7
T t I/
Lab Sample IU: 680-211023-3
Matrix: Water
Final Batch Prepared
Amount Number or Analyzed Analyst Lab 70 2 mL 7395 02/17/2 110.56 ALG TAL SAV
o a NA Analysis SM 2540D 1 1000 mL 1000 mL 706170 02/08/22 19:37 PG
L Instrument ID: NOEQUIP
Client Sample ID: CLT3_Sample_Point_04_2022-
Date Collected: 02/04/22 09:45 0204
Date Received: 02/08/22 10:50
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 5220D-2011
Instrument ID: SPC7
Total/NA Analysis SM 2540D
Instrument ID: NOEQUIP
TAL SAV
Lab Sample ID: 680-211023-4
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
1
2 mL
2 mL
707395
02/17/22 10:W ALG TAL SAV
1
1000 mL
1000 mL
706170
02/08/22 19:37 PG TAL SAV
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 8 of 12 2/23/2022

Accreditation/Certification Summary
Client: ERM-West Job ID: 680-211023-1
Project/Site: Storm Water - Amazon Warehouses CLT3
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22
Eurofins Savannah
Page 9 of 12 2/23/2022

Client: ERM-West Method Summary
Project/Site: Storm Water - Amazon Warehouses CLT3
Job ID: 680-211023-1
Method
Method Description
Protocol
Laboratory
522OD-2 111
Chemical Oxygen Demand
SM
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
tUroui is SaVai1ilai i
Page 10 of 12 2/23/2022

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Page 11 of 12
2/23/2022

Login Sample Receipt Checklist
Client: ERM-West
Login Number: 211023
List Number: 1
Creator: Hartley, Tyler
Question
Job Number: 680-211023-1
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 12 of 12 2/23/2022