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Home My WebLink AboutNCG060396_Monitoring Report_20211006NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCGO60000 Food and Kindred Click here for Instructions Complete, sign, scan and submit the DMR via the s_ 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the 0 oadQ�?m within Certificate of Coverage No. N0306 0396 Person Collecting Samples: Parker Cliatt Facility Name: Amazon.com Services LLC - CLT3 Laboratory Name: Eurofins TestAmerica Facility County: Cabanus Laboratory Cert. No.:269 Discharge during this period: + Yes r7l No (if no, skip to signature and date) Has your facility implemented mandatoryTier response actions this sample period for any benchmark exceedances? El Yes No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR QYes [:]No Date Uploaded: 0 02_ Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter code parameter Outfall 001 Outfall 002 Outfall 003 Outfall 004 Outfall N/A Receiving Stream Class C C C C N/A Date Sample CollectedMM/DD/YYYY 9/8/2021 9/8/2021 9/8/2021 9/8/2021 46529 24-Hour Rainfall in inches 0.5 0.5 0.5 0.5 C0530 TSS in mg/L (100 or 50*) <2.5 <2.5 7.6 <2.5 pH in standard units (6.0— 9.0 FW, 00400 6.8 — 8.5 S" 9.0 7.28 7.25 6.86 00556 Oil & Grease in mg/L(30) N/A N/A N/A INIA Fecal Coliform per 100 ml of 31616 freshwater (if required (1000 N/A WA N/A NIA Enterococci per 100 ml of saltwater 61211 (if required) (500 NIA N/A N/A N/A Chemical Oxygen Demand in mg/L 00340 (120) 5.9 12 14 8.5 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A NIA NIA 00552 1 Non -Polar Oil & Grease in mg/L (15) 1 N/A I N/A I N/A I N/A * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L All other water classifications have a benchmark of 100 mg/L FW (Freshwater) SW (saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my Yowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the nosskbility of fines and imprisonment for knowing violations." Signature of Permittee or vvviiayk@amazon.com Email Address Individual 101 Date (484) 252-1748 Phone Number urofins C T.... :.... t_tivilvinn1etit, 1cau116 MII ICI iCQ o d ANALYTiCAI REPORT px m Eurofins TestAmerica, Savannah Z? < G 5102 LaRoche Avenue i Q Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-204517-1 Laboratory SDG: 6500 Davidson Highway, Concord, NC 28027 Client Project/Site: Storm Water - Amazon Warehouses CLT3 For: ERM-Southeast, Inc. The Towers at Wildwood Plaza 3200 Windy Hill Road Suite 150OW Atlanta, Georgia 30339 Attn: Dena Haverland RoxahtU_ (A"rvs Authorized for release by: 912812021 4:49:10 PM Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@E _irofinset.r_.om The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Eleclronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1❑ Client: ERM-Southeast, Inc. Laboratory Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 N Table of Contents Cover Page .............................................. 1 Table of Contents ......................................... 2 Case Narrative ........................................... 3 Sample Summary ......................................... 4 Method Summary......................................... 5 Definitions ............................................... 6 Client Sample Results ...................................... 7 QC Sample Results ........................................ 11 Chronicle................................................ 13 Chain of Custody .......................................... 14 Certification Summary ...................................... 15 Eurofins TestAmedca Savannah Page 2 of 15 9/�8/2021 Case Narrative Client: ERM-Southeast, Inc. Project/Site: Storm Water - Amazon Warehouses CLT3 Job ID, 680-204517-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-204517-1 Comments No additional comments. Job ID: 680-204517-1 SDG: 6500 Davidson Highway, Concord, NC 28027 Receipt The samples were received on 9/16/2021 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, propedy preserved and on ice. The temperature of the cooler at receipt was 3.50 C. General Chemistry Method SM 254OD: The following samples were received with less than 2 days remaining on the holding time or less than one shift (8 hours) remaining on a test with a holding time of 48 hours or less. As such, the laboratory had insufficient time remaining to perform the analysis within holding time: CLT3_Sample_Point_01_20210908 (680-204517-1), CLT3_Sample_Point 02 20210908 (680-204517-2), CLT3_Sample_Point 03_20210908 (680-204517-3) and CLT3 Sample_Point 04 20210908 (680-204517-4). No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 3 of 15 9/28/2021 Sample Summary Client: ERM-Southeast, Inc. Job ID: 680-204517-1 ProjectlSite: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Lab Sample ID Client Sample ID Matrix Collected Received 680-204517-1 CLT3_Sample_Point 01 20210908 Water 09/08/21 10:08 09/16/21 10:30 680-204517-2 CLT3 Sample Point 02 20210908 Water 09/08/21 10:20 09/16/21 10:30 680-204517-3 CLT3 Sample Point 03 20210908 Water 09/08/21 09:55 09/16/21 10:30 680-2045174 CLT3 Sample_Point 04 20210908 Water 09/08/21 09:43 09/16/21 10:30 Page 4 of 15 Eurofins TestAmerica, SDI MM1 Method Summary Client: ERM-Southeast, Inc. Project/Site: Storm Water - Amazon Warehouses CLT3 Method Method Description 5220D-2011 Chemical Oxygen Demand SM 2540D Solids, Total Suspended (TSS) Protocol References: SM = "Standard Methods For The Examination Of Water And Wastewater' Job ID: 680-204517-1 SDG: 6500 Davidson Highway, Concord, NC 28027 Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 SM SM Laboratory TAL SAV TAL SAV Eurofins TestAmerica, Savannah Page 5 of 15 9/28/2021 Definitions/Glossary Client: ERM-Southeast, Inc. Project/Site: Stone Water - Amazon Warehouses CLT3 Qualifiers General Chemistry Qualifier Qualifier Description Job ID: 680-204517-1 SDG: 6500 Davidson Highway, Concord, NC 28027 H Sample was prepped or analyzed beyond the specified holding time H3 Sample was received and analyzed past holding time. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary -- Abbreviation These commonly used abbreviations may or may not be present in this report n Listed underthe "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) oil Fac Dilution Factor DL Detection Limit(DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated NO Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative/Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 6 of 15 9/28/2021 Client Sample Results Client: ERM-Southeast, Inc. Project/Site: Storm Water - Amazon Warehouses CLT3 Client Sample ID: CLT3_ Sam ple_Point_01_20210908 Date Collected: 09/08121 10:08 Date Received:09116/21 10:30 Job ID: 660-204517-1 SDG: 6500 Davidson Highway, Concord, NC 28027 Lab Sam le ID: 680-20464M Matrix: Water General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Chemical Oxygen Demand 5.9 J 10 5.0 mg/L 09/27/21 12:45 1 Total Suspended Solids <2.5 H H3 2.5 2.5 mg/L 09/18/21 10:35 1 Eurofins TestAmerica, Savannah Page 7 of 15 9/28/2021 Client Sample Results Client: ERM-Southeast, Inc. Job ID: 680-204517-1 Project/Site: Stone Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Client Sample ID: ulm sample_Point_02_20210908 Lab Sample ID: 680-204517-2 Date Collected: 09/08/21 10:20 Matrix: Water Date Received: 09/16/21 10:30 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Chemical Oxygen Demand 12 10 5.0 mg/L 09/27/21 12:45 1 Total Suspended Solids <2.5 H H3 2.5 2.5 mg/L 09/17/21 13:25 1 A Eurof ns TestAmerica, Savannah Page 8 of 15 9/28/2021 Client Sample Results Client: ERM-Southeast, Inc. Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Client Sample ID: CLT3_Sample_Point 03_20210908 Lab Sample ID: 680-204517-3 Date Collected: 09/08/21 09:65 Matrix: Water Date Received: 09/16/21 10:30 F General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fee Chemical Oxygen Demand 14 10 5.6 mg/L 09/27/21 12:45 1 Total Suspended Solids 7.6 H H3 5.0 5.0 mg/L 09/17/21 13:25 1 Eurofins TestAmerica, Savannah Page 9 of 15 9/28/2021 Client Sample Results Client: ERM-Southeast, Inc. Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Client Sample ID: CLT3 Sample_Point 04_20210908 Lab Sample ID: 680-204517-4 Date Collected: 09/08/21 09:43 Matrix: Water Date Received: 09/16/21 10:30 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Chemical Oxygen Demand 8.5 J 10 5.0 mg/L 09/27/21 12:45 1 Total Suspended Solids <2.5 H H3 2.5 2.5 mg/L 09/18/21 10:35 1 Eurofins TestAmerica, Savannah Page 10 of 15 9/28/2021 QC Sample Results Client: ERMSoutheast, Inc. Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Method: 5220D-2011 - Chemical Oxygen Demand Lab Sample ID: MB 680-68678713 Matrix: Water Analysis Batch: 686787 Client Sample ID: Method Blank Prep Type: Total/NA Me Me Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 09/27/21 12:45 1 Lab Sample ID: LCS 680-68678714 Matrix: Water Analysis Batch: 686787 Anew Chemical Oxygen Demand Lab Sample ID: 680-204517-1 MS Matrix: Water Analysis Batch: 686787 Sample Sample Analyte Result Qualifier Chemical Oxygen Demand 5.9 J Lab Sample ID: 680-204517-1 MSD Matrix: Water Analysis Batch: 686787 Sample Sample Analyte Result Qualifier Chemical Oxygen Demand 5.9 J Lab Sample ID: 680-204517-4 MS Matrix: Water Analysis Batch: 686787 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 50.9 mg/L 102 90 -110 Client Sample ID: CLT3_Sample_ Point _01_20210908 Prep Type: Total/NA Spike MS MS %Rec. Added Result Qualifier Unit 0 %Rec Limits 50.0 55.0 mg/L 98 90 -110 Client Sample ID: CLT3_Sample_Point_01_20210908 Prep Type: Total/NA Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 50.0 52.8 mg/L 94 90 -110 4 30 Client Sample ID: CLT3_Sample_Point _04_20210908 Prep Type: Total/NA Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 8.5 J 50.0 55.3 mg/L 94 90- 110 Lab Sample ID: 680-204517-4 MSD Client Sample ID: CLT3_Sample_Point_04 20210908 Matrix: Water Prep Type: Total/NA Analysis Batch: 686787 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Chemical Oxygen Demand 8.5 J 50.0 56.9 mg/L 97 90- 110 3 30 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 680-685364/1 Matrix: Water Analysis Batch: 685364 Me Me Analyte Result Qualifier RL MDL Unit D Total Suspended Solids <2.5 2.5 2.5 mg/L Client Sample ID: Method Blank Prep Type: Total/NA Prepared Analyzed oil Fac 09/17/21 13:25 1 Eurofins TestAmerica, Savannah Page 11 of 15 9/28/2021 QC Sample Results Client: ERMSoutheast, Inc. Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Method: SM 2540D - Solids, Total Suspended (TSS) (Continued) Lab Sample ID: LCS 680-68536412 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 685364 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 1050 mg/L 111 80-120 Lab Sample ID: LCSD 680-685364/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 685364 Spike LCSD LCSD %Rec. RPD r Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit i_ Total Suspended Solids 951 894 nr lL 94 80-120 16 25 Lab Sample ID: MB 680-685470/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 685470 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac Total Suspended Solids <2.5 2.5 2.5 mg/L 09/18/21 10:35 1 Lab Sample ID: LCS 680-685470/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 685470 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 870 mg/L 91 80.120 Lab Sample ID: LCSD 680-685470/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 685470 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 798 mg/L 84 80 -120 9 25 Eurofins TestAmerica, Savannah Page 12 of 15 9/28/2021 Lab Chronicle Client: ERM-Southeast, Inc. Job ID: 680-204517-1 Project/Site: Storm Water - Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Client Sample ID: CLT3_Sample_Point 01_20210908 Lab Sample ID: 680-204517-1 Date Collected: 09/08/21 10:08 Matrix: Water Date Received: 09/16/21 10:30 Batch Batch oil Initial Final Batch Prep Type Type Method Run Factor Amount Amount Number TotaVNA Analysis 52205-2011 1 2 mL 2 mL 686787 Instrument ID: SPC7 TotaVNA Analysis SM 2540D 1 1000 mL 1000 mL 685470 Instrument ID: NOEQUIP Prepared or Analyzed Analyst Lab 09/2721 12:45 ALG TAL SAV 0911821 10:35 ALG TAL SAV Client Sample ID: CLT3_ Sam ple_Point_02_20210908 Lab Sample ID: 680-204517-2 Date Collected: 09/08/21 10:20 Matrix: Water Date Received: 09116/21 10:30 Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaVNA Analysis 52200-2011 1 2 mL 2 mL 686787 092721 12:45 ALG TAL SAV Instrument ID: 8PC7 I TotaVNA Analysis SM 2540D 1 1000 mL 1000 mL 685364 0911721 13:25 ALG TAL SAV Instrument ID: NOEQUIP Client Sample ID: CLT3_ Sample_Point _03_20210908 Date Collected: 09108/21 09:55 Date Received: 09/16/21 10:30 Lab Sample ID: 680-204517-3 Matrix: Water Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaVNA Analysis 5220D-2611 1 2 mL 2 mL 686787 0927/21 12:46 ALG TAL SAV Instrument ID: SPC7 TctaVNA Analysis SM 2540D 1 500 mL Instrument ID: NOEQUIP Client Sample ID: CLT3_Sample_Point 04_20210908 Date Collected: 09/08/21 09:43 Date Received: 09116/21 10:30 1000 mL 685364 09/1721 13:25 ALG TAL SAV Lab Sample ID: 680-204517-4-4 Matrix: Water Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaVNA Analysis 52205-2011 1 2 mL 2 mL 686787 092721 12:45 ALG TAL SAV Instrument ID: SPC7 TotaVNA Analysis SM 2540D 1 1000 mL 1000 mL 685470 09/1821 10:35 ALG TAL SAV Instrument ID: NOEQUIP Laboratory References: TAL SAV = Eurofins TestAmenca, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 13 of 15 9/28/2021 ❑c .- 610ZJ91/10 .¢A 1' ON e s0Z V awvuwb..+O M ne I.NN+I+duwt.+IpoJ ON IeaS FD01sn0 IJeWI s1eeS Fp01sn0 Auedw+J --.i.P Ad p+,.a�od bepupJ au:,an+p b wn�a:�wa Auedwop y 05(1) 1 '1� rGiwy+lep ..,. 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Y •..-••...+ (qet :9 awiy oleo a( weS zo 0 o 6 " •-` •duNaaol aldweS Aj qa 0 ; O a e1AleW aldWeS y3 S < 09ZOZOOZ ( 1 sas.ngwem wzewy - /aleM uu01S ,Ap+dn.Auw t ro3 1 i S¢vd M v103 + a it a +wWN aweN lwbAd won w.a!@0 ape. 6rwp Yy]w A NNMInn' f O 0 .1" n e +oM INw3 WISanOaN .ap.p aseVvnd (I81)9e00'Z{S'E00 .O$LN $ wrv.wv O COT$AN'tl IlOew'! ap.1 audy ON ¢ aaA V Ip+1 1 .Unld.1 p19Z6 'vo COSL+N'O TOSN¢N 3 SPE)"N d DW �ww 0 aT ne15 d~v O Innvw J aUIN1 Aq e N WJ[N a Ouc," n 1JN.a '.I+I+pl pn++pa+tl let 00C aiL pnS pa.iS weld OZ61 :aapop uoPwnud :M)udaetl nap+p0 asaip patsanbaa slsRleuy . wr IsaM'wa3 _ —abed ulsNa !„¢a„dJ )0 won lesw)Wn3@suey ua apeM &b0 3s+d -unNne1i "' ,.ryuOwJw+vJ 9901E-y1ZSy-ovz a uwnel 'sdeA3_44 1 aOgeW)O)ul )UapU ON J 31 rvd qel wdwe9 S910'ZSE (Zt6) -el SM.PSE (Zt6) au04d ' 00v1E V0 '4euueAe ap+., p�oaab �(po;sn�;o uley� S SUI)01n��- �t_? °gy= t ��anuany aVJOyeI ZOIS yeuueneg'eouawytSal su!;om3 N N Cb N 2L La cu a d m ( Accreditation/Certification Summary Client: ERMSoutheast, Inc. Job ID: 680-204517-1 Project/Site: Stone Water -Amazon Warehouses CLT3 SDG: 6500 Davidson Highway, Concord, NC 28027 Laboratory: Eurofins TestAmerica, Savannah The accreditations/certifcations listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (NNV/SW) State 269 12-31-21 Eurofins TestAmerica, Savannah Page 15 of 15 9/28/2021