NCS000329_2022 DMR_20220505

May 5, 2022 P.o_ sox 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Division of Energy Mineral and Land Resources Phone: [phone]
Fax: [phone]
Attn: Central Files Email: mi&[e-mail]
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files: Tier 2 Monthly Monitoring- April 2022
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
0 Outfall 402 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
If you have any questions or need additional information, please contact me at 704-289-4511
x3800. Thank you.
Sincerely,
/?X9 - — �
Michael McManus
EHS Coordinator

AT I
Specialty Materials
ATI (Allvac) — Bakers Campus (BNO)
Stormwater Monitoring Report Form
Sample Date: I;"Pr
Z 6Wt G
Sample Time:
Sample Location:
Stormwater Discharge Outfall # 01 (Commingled)
Drainage Area= 2,915,470 sq. ft. = 69 Acres
Impervious= 34%
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
40 CFR Part 136
Results of Sample Analysis:
Parameter
Results (mg/1)
Benchmark Values (mg/1)
TSS
100
BO D
30
COD
u cr;
120
Cadmium
a. ti C
te
0.003
Chromium
0.905
Total Calcium
915
Total Copper
0.01
Total Nickel
0.335
Total Zinc
0.126
pH
(std units)
6-9
Temperature
Deg. Celsius
Total Residual Chlorine
017
Oil and Grease
15
Storm Date; Storm Duration: (Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q (Total) = Q (Pervious Area) + Q (Impervious Area)
Rev. 01
Date of Rev.: 1/22/2020

AI
Specialty Materials
ATI (Allvac) — Bakers Campus (BN4)
Stormwater Monitoring Report Form
Q (Tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + (.9 x inches rain/12 inches/ft. x 69 x .34)
Q (Total, cfs) = 1.15180 x (Inches of rain) + 1.7595 x (Inches of rain)
cfs
Rev. 01
Date of Rev.: 1/22/2020

%-*0- AT I
Ar
Specialty Materials
ATI (Allvac) -- Bakers Campus (BNO)
5tormwater Monitoring Report Form
Sample Date:
Sample Time:
12 2 Z
Sample Location:
Stormwater Discharge Outfall # 02 (Non -
Commingled)
Drainage Area= 212,952 sq. ft. = 4.9 Acres
Impervious= 12%
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
40 CFR Part 136
Results of Sample Analysis:
Parameter
Results (mg/1)
Benchmark Values (mg/1)
TSS
100
BOD
e C/4,
30
COD
�y
Al�4r` 9 � 1
120
Cadmium
0.003
Chromium
0.905
Total Calcium
915
Total Copper
0.01
Total Nickel
0.335
Total Zinc
0.126
pH
(std units)
6-9
Temperature
Deg. Celsius
Storm Date: Storm Duration; (Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q (Total) = Q (Pervious Area) + Q (Impervious Area)
Q (Tot., cfs) = (.4 x inches rain/12 inches/ft. x 4.9 acres x .88) + (.9 x inches rain/12 inches/ft. x 4.9 x .12)
Rev. 01
Date of Rev.: 1/22/2020

I
Specialty Materials
ATI (Allvac) --- Bakers Campus (BNO)
Stormwater Monitoring Report Form
Q (Total, cfs) = 0.1437 x (Inches of rain) + 0.0441 x (Inches of rainy
cfs
Rev. 01
Date of Rev.: 1/22/2020

WAI I
Specialty Materials
AT] (Allvac) — Bakers Campus (BNO)
Stormwater Monitoring Report Form
Sample Date:,
Sample Time:
r
Sample Location:
Stormwater Discharge Outfall # 03 (Non -
Commingled)
Drainage Area= 336,580 sq. ft. = 7.8 Acres
Impervious= 15%
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
40 CFR Part 136
Results of Sample Analysis:
Parameter
Results (mg/1)
Benchmark Values (mg/1)
TSS
100
BOD
30
COD
120
Cadmium
0.003
Chromium
0.905
Total Calcium
/k4l
915
Total Copper
0.01
Total Nickel
0.335
Total Zinc
0.126
pH
(std units)
6-9
Temperature
Deg. Celsius
Storm Date: Storm Duration: (Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q (Total) = Q (Pervious Area) + Q (Impervious Area)
Q (Tot., ifs) = (.4 x inches rain/12 inches/ft. x 7.8 acres x .85) + (.9 x inches rain/12 inches/ft. x 7.8 x .15)
Rev. 01
Date of Rev.: 1/22/2020

-41
-94,-ATI
Specialty Matedais
AT (Allvac) — Bakers Campus (BNO)
Stormwater Monitoring Report Form
Q (Total, cfs) = 0.2210 x (inches of rain) f 0.0878 x (Inches of rain)
= cfs
Rev. 01
Date of Rev.: 1/22/2020

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aceAnalytical
{ www.pacelsbs.com
April 28, 2022
Mr. Larry Allen
Allvac
RE: Project: Non Contact Cooling Water
Pace Project No.: 92599482
Dear Mr. Allen:
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Muntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 15, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIINEtAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: David Ethridge
Mr. Tommy Long, Allvac
Mike McManus, ATI Specialty Metals
Rick Moore, ATt Specialty Materials
James Moser
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

1�9aneAnalyticalo
www.paceiabs.com
f
Project: Non Contact Coaling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
V rginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
www.picalabs.com
r
SAMPLE ANALYTE COUNT
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
A nalytes
Reported
Laboratory
92599482001
NON -CONTACT #1
EPA 1664B
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482002
NON-CONTACT#2
EPA1664B
ICO
1
PASI-C
SM 4500-Cl G-2011
MDW
1
PASI-A
92599482003
NON -CONTACT #3
EPA 1664E
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482004
NON -CONTACT #4
EPA 1664B
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482005
NON -CONTACT #5
EPA 1664B
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482006
NON -CONTACT #6
EPA 1664B
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482007
NON -CONTACT #7
EPA 1664B
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92599482008
NON -CONTACT #8
EPA 1664E
ICO
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
PASI-A= Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

aceAnalytical
www.pactiabs.com
t
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Sample: NON-CONTACT#1 Lab ID: 92599482001 Collected: 04/14/22 09:50 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mglL 4.9 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
Chlorine, Total Residual 0.064 mglL 0.024 1 04/27122 20:26 7782-50-5 H3
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

aceAnalyfical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Sample: NON -CONTACT #2 Lab ID: 92599482002 Collected: 04/14/22 10:12 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mglL 4.9 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
Chlorine, Total Residual ND mglL 0.024 1 04/27/22 20:22 7782-50-5 H3
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

aceAnalyi#ical
j www.pecolabs.com
I
ANALYTICAL RESULTS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Sample: NON -CONTACT #3 Labit): 92599482003 Collected: 04114/22 10:30 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mglL 4.8 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services -Asheville
Chlorine, Total Residual 0.025 mglL 0,024 1 04/27/22 20:18 7782-50-5 H3
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 6 of 20

aceAnalytical
www pacelabs.com
ANALYTICAL RESULTS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON -CONTACT #4 Lad ID: 92599482004 Collected: 04/14/22 10:50 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mg1L 4.9 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
Chlorine, Total Residual 0,042 mglL 0.024 1 04/27/22 20:13 7782-50-5 H3
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

aceAnalytical
www.pacalalss.com
I
ANALYTICAL RESULTS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON -CONTACT #5 Lab ID: 92599482005 Collected: 04/14/22 11:08 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 166413
Pace Analytical Services - Charlotte
Oil and Grease ND mg/L 4.8 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services -Asheville
Chlorine, Total Residual 0.11 mg/L 0.024 1 04/27/22 20:09 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2022 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 20

lacreAnalytical
f www.pacelaha.cam
f
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
[phone]
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Sample: NON -CONTACT #6 Lab ID: 92599482006 Collected: 04/14/22 11:30 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease ND mg1L 4.9 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
Chlorine, Total Residual 0.13 mg1L 0.024 1 04/27/22 19:55 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2022 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 20

aceAnafytica!®
www.picel:bs-tam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Sample: NON -CONTACT #7 Labit), 92599482007 Collected: 04/14/22 11:52 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 04/28/2022 09:36 AM
Analytical Method: EPA 166413
Pace Analytical Services - Charlotte
ND mg/L 4.9 1 04/21/22 05:30
Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
0.15 mg1L 0.024 1 04/2712219:51 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 20

aceAnalj4kal
www.pacolabs.ccm
ANALYTICAL RESULTS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON -CONTACT #8 Lab ID: 92599482008 Collected: 04/14/22 12:15 Received: 04/15/22 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Quaff
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mg1L 4.8 1 04/21/22 05:30
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Pace Analytical Services -Asheville
Chlorine, Total Residual 2.4 mglL 0,24 10 04/27/22 19:46 7782-50-5 H3
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

aceAnaiytical"
www.pacelabs.com
QUALITY CONTROL DATA
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 692994 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92599482001, 92599482002, 92599482003, 92599482004, 92599482005, 92599482006, 92599482007,
92599482008
METHOD BLANK: 3620396 Matrix: Water
Associated Lab Samples: 92599482001, 92599482002, 92599482003, 92599482004, 92599482005, 92599482006, 92599482007,
92599482008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 04/21/22 05:30
LABORATORY CONTROL SAMPLE:
3620397
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 32.2
80
78-114
MATRIX SPIKE SAMPLE:
3620398
92599726002 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
29.7
74
78-114 M1
SAMPLE DUPLICATE: 3620399
92599613001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Oil and Grease
mg/L
ND 1.4J
Results presented on this page are in the units Indicated 4y the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2022 09:36 AM without the written consent of Pace Analytical Services, L.I.C. Page 12 of 20

aceAnalytical
www.pacelabs.eam
f
f
QUALITY CONTROL DATA
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 694562 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CLG Chlorine, Total Residual
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92599482001, 92599482002, 92599482003, 92599482004, 92599482005, 92599482006, 92599482007,
92599482008
METHOD BLANK: 3628012 Matrix: Water
Associated Lab Samples: 92599482001, 92599482002, 92599482003, 92599482004, 92599482005, 92599482006, 92599482007,
92599482008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg1L ND 0.024 04/27/22 18:40
SAMPLE DUPLICATE: 3628013
92598262001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L ND ND H1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2022 09:36 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

aceAnalytical
www.parelabs.cam
I
QUALIFIERS
Project: Non Contact Cooling Water
Pace Project No.: 92599482
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2022 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

aceAnalytical
( www.pacllabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Non Contact Cooling Water
Pace Project No.: 92599482
Lab ID Sample ID QC Batch Method QC Batch
92599482001
NON -CONTACT #1
EPA 1664B
692994
92599482002
NON-CONTACT42
EPA 1664E
692994
92599482003
NON-CONTACT#3
EPA 1664E
692994
92599482004
NON-CONTACT#4
EPA166413
692994
92599482005
NON-CONTACT#5
EPA1664B
692994
92599482006
NON -CONTACT #6
EPA 1664B
692994
92599482007
NON -CONTACT #7
EPA 1664E
692994
92599482008
NON -CONTACT #8
EPA 1664B
692994
92599482001
NON -CONTACT #1
SM 4500-CI G-2011
694562
92599482002
NON -CONTACT #2
SM 4500-CI G-2011
694562
92599482003
NON -CONTACT #3
SM 4500-CI G-2011
694562
92599482004
NON -CONTACT #4
SM 4500-CI G-2011
694562
92599482005
NON -CONTACT #5
SM 4500-Cl G-2011
694562
92599482006
NON-CONTACT#6
SM 4500-Cl G-2011
694562
92599482007
NON-CONTACT#7
SM 4500-CI G-2011
694562
92599482008
NON -CONTACT #8
SM 4500-Cl G-2011
694562
Date: 04/28/2022 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
Page 15 of 20

Document Name:
Document Revlsed: [November 15, 2021
aceArtalrCal n
Upon Rece€ t (SCUR)
Page1 of2
Document No.:
[!:ptleo"dition
Issuing Authority:
AR-CS-033-Rev.08
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville[] Atlanta[] Kernersvilie❑
Custody Seal Present? ❑Yes ❑No
Seals Intact? Des ❑Nil
Project q
92588482 _
Date/lnitiats Person Ekamining Contents;)! `i q i
f"
Packing Material: []Bubble Wrap (,]bubble Bags []None ❑ Other Biological Tissue Frozen?
Thermometer; _ ❑Yes ❑No ❑N/A
❑'IR Gun in: - .I Jt i ❑++`uet ❑slue []None Type of Ice:
• k.1 z r Correction Factor.
Conley Temp:' `' Add/Subtract f °Cj > Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler-Temp•Corrected-('C): Burt
USDA Regulated Soil (❑r N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a foreign source {internationally,
nYPS F INn - enrh,d7na Wawali and P—rtn RI-12 F"IV— MN.
Comments/Discrepancy:
Chain of Custody Present?
Yeses
ONO
N A
1.
Sam €es Arrived within Hold Time?
, les
[]No
N/A
2.
Short Hold Time Analysis (e72 hr.)?
ElYes
Q Np
N/A
3.
Rush Turn Around Time Requested?
Yes_ON'
N/A
4,
Sufficient Volume?
- Ve,
QNo
N/A
5.
Correct Containers Used?
-Pace Containers Used?
oic's
, Vs
ONO
0No
(]N/A
N/A
6.
Containers Intact?
Eaf,,
QN.
N/A
7.
Dissolved analysis: Samples Feld Rltered?
Elyes
Quo
EINA
S.
Sample Labels Match COC?
-Includes Date/Time/Ip/Analysis Matr►u:
I]Yes
❑No
[]NIA
9.
Headspace In VOA vials (>S•Smm)?
Yes
QNo
CN/A
10.
Trip thank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
[]No
QNO
❑NJA
WfA
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted: -
Project Manager SCURF Review:
Project Manager SRF Review:
Date/iime:
Lot ID of split containers
Date:
Date:
Field Data Required? ❑Yes []NO
Page 16 of 20

Document Name:
Qocument Revised: November 15, 2021
n
Analytical'
Sample Condition Upon Receipt (SCURj
Page 2 of 2
Document No.:
Issuing Authority:
f-CAR•CS•033•Rev.08
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechlorination is Project Al
verified and Within the acceptance range for preservation
samples. PH: MNB Due Date: 04/29/22_......_._.._._._
Exceptions: VOA, CO I orm, OC, 01 an rease, i f {water} 0t1C; ECFfg - CLIENT: 92—A1 i vac NC
"Bottom half of box Is to list number of bottles
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pH Adjustment tog for Preserved Samples
Sample to
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot a
Note: Whenever there is a discrepancy affecting North Catalina compliance samples, a copy of this form will be sent to the North Carolina 6EHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containars.
Page 17 of 20

(NON CONTACT)
IBahers North
Chailt pf Custody Record
Project Nuniber/Narne: Note Contact Cooling Water
JPrqject
Location: AT[ -Sill - Bakers
Sampler's Signature:
•
Date:
?
°
Requested Test
Parameters
Non -Contact fl
- y-
.'O,
G
G
HCI
Y
.1
Oil & Grease
( �
Nor[ -Contact #2
1p:
G
G
HCI
Y
Oil & Grease
Non -Contact #3
p :3
G
G
HCI
Y
Oil & Grease
Non -Contact #4
p :D
G
G
HCI
Y
��
Oil &Grease
('
Non -Contact #5
:p
G
G
HCI
Y
��.�'
Oil &Grease
Ole
Non -Contact #6
0,,
G
G
HCI
Y
, p
Oil & Grease
Nan -Contact #7
: ,�
G
G
HCI
Y
/, p
Oil & Grease
G
Non -Contact #8
.`
G
G
HCI
Y
ww, 3
Oil & Grease
Meter Calibrated:
1 N
Therntometer Calibrated:&-/ N
Sampling and Field analysis completed by:
�
n
Relinquished by:
Received by:<;>"-f
Date:
Time: /' S- f',
Date: -5iz
Time: Q
Relinquished by: ��. �% free.
Received by: j �
<<w i-j
Date:
Time: //4/.5
Date: `'t,! r y / ^
Time: t t -/
3.0
Stormwater Monitoring -Non Contact Cooling Water Chain of Custody (Oil & Grease) Rev. 03 6/2/2020 j �
3C
y�
Page 18 of 20

(NON CONTACT)
linhe s North
Chain of Custody Record
Project Nuniber/Natne: Non Contact Cool in T Water
Project 3.ocatiEnt:
A 11-S,�R Bakers
Samptet's Signature:
, ;
' '
Date: Z0
a�
a
0
C
s U
>U
,w
.�.
Requested Test
N
® Or O
Parameters
:B
U
Non -Contact #1
per„
G
G
HCI
Y
V
Oil & Grease
Ly
Non -Contact #2
G
G
HCI
Y
, j
Oil & Grease
Non -Contact #3
G
G
HCI
Y
,�;a
Oil & Grease;'
Non -Contact #4
:,ate
G
G
HCl
Y
, y
Oil & Grease
Qe
Non -Contact #5
:0
G
G
HCI
Y
Oil & Grease
Non -Contact #6
Ip god,
G
G
HCl
Y
, p
OiI & Grease
� -
Non -Contact #7
,.
G
G
HCl
Y
, p
Oil & Grease
? .7
Non -Contact 48
HCI
Y
aK.S
Oil. & Grease
Meter Calibrated: f it
IThermometer Calibrated: 6 I is
Sampling and Field analysis completedZI
Relinquished by: - f'- `�,�'-
Received by:c"7,��
Dante: "7 '% Time:
Date:
Time: (j r
Relinquished by: C F'f �i�'�c
Received
by:
Date: c 5 �z Time:
1
Date: ` t „- ;- ,
Time:
5tormwater Monitoring -Nan Contact Cooling Water Chain of Custody foil & Grease) Rev. 03 b/2/ZUZU
Page 19 of 20

Bakers Nor(h
Project Number/Name; Non Contact Cooling Water
Project Location: ATI SM - Bakers North
Sampler's Siggaturc: a / Date:
C�
;ma
Requested Test Parameters
Fi iC
�
�
+d
w6
�
a
•� t:
U
Non -Contact #1
- -
g-��
G
P
None
Y
Residual Chlorine
Non -Contact #2
G
P
None
Y
Residual Chlorine
Non Contact #3
: p
G
P
None
Y
Residual Chlorine
Non -Contact #4
p.
G
P
None
Y
„�
, ,"
Residual Chlorine cp, "
Non-Contacl #5
j1 0G
P
None
Y
„
Residual Chlorine &J�
Non -Contact #6
/PS,,
G
P
None
Y
, Q
Residual Chlorine .�
Non -Contact #7
: y
G
P
None
Y
,p
Residual Chlorine
Non -Contact #8
4—G
P
None
Y
Residual Chlorine C23
Meter Calibrated: / N Thermometer Calibrated: j}% I N
Sampling and Field analysis completed by:
Relinquished by:
Received y- C"?[ c
Date: r`./ ;'a -Time: /.'J ,`'".'�' fl
Date: Time: i
Relinquished by- (;?z,�vl ��c-
Received by:
Date: 5 t Time: (�
Date: Time:
EHS-SW-Stormwater Monitoring -Nero Contact Cooling Water Chain of Custody (Residual Chlorine) -Rev 004
Page 20 of 20