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HomeMy WebLinkAboutWQ0021632_Renewal Application_20220627Non -Discharge Branch Upload/Submittal Form NORTH CAROLINA EnvironmentalQuul1ty Version 2 - Revised June 23, 2020 Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.) * Yes No Permit Number (IR) * WQ0021632 Applicant/Permittee City of Burlington Applicant/Permittee Address PO Box 1358, Burlington NC 27216 Is the owner in BIMS? Yes No Is the facility in BIMS? Yes No Owner Type Municipal Facility Name City of Burlington Class A Residuals Program County Alamance Fee Category Major Fee Amount $0 Is this a complete application?* Yes No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review by the hydrogeologist?* Yes No Regional Office CO Reviewer Admin Reviewer Complete App Date 06/27/2022 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Robert Roth Email Address* rroth@SYNAGRO.com Project Information Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 13364034324 O Modification - Minor O Renewal O GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 O Residual Annual Report O Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type: * Permit Number:* Wastewater Irrigation Other Wastewater Closed -Loop Recycle Single -Family Residence Wastewater Irrigation WQ0021632 Has Current Existing permit number Appl icant/Permittee * City of Burlington Applicant/Permittee Address* PO Box 1358, Burlington NC 27216 Facility Name* City of Burlington Class A Residuals Program Please provide comments/notes on your current submittal below. Renewal with no fee required. High -Rate Infiltration Reclaimed Water Residuals Other At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. * (Application Form, Engineering Plans, Specifications, Calculations, Etc.) City of Burlington DCAR Renewal.pdf 7.39MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless Ole is larger than upload limit. * ✓ By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 6/27/2022 SYNAGRO June 27, 2022, NCDENR-DEQ Division of Water Resources Land Application Permitting and Compliance Unit Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 ATTENTION: Mr. Nathaniel Thornburg REFERENCE: Application No. WQ0021632 Permit Renewal City of Burlington DCAR Alamance County Dear Mr. Thornburg: On behalf of the City of Burlington, Synagro is submitting this application to renew the above referenced residuals land application permit. It should be noted that the following renewal package includes RSC forms and supporting documentation for 2 separate sources (South WWTP and Mackintosh WTP) as opposed to the currently structured Attachment A. It is intended that these 2 sources will be renewed and eligible for land application through the use of this permit. South Burlington WWTP material if land applied will be composted, branded as "COMPOGRO" and sold or given away while the JD Mackintosh material will be land applied by the current land application contractor. Lastly, the most recent analytics for each plant are included with each source. Pathogen and Vector Attraction Reduction for the last application of "COMPOGRO" are included also. This application package should contain all the information necessary to complete the requested renewal of the above referenced permit. However, if you require additional information or have further questions, please contact me at (336) 403-4324 or rroth@synagro.com. Thank you in advance for the timely and efficient review of this renewal application. Sincerely, Robert N. Roth 284 Boger Road, Mocksville, NC 27028 • Phone: (336) 790-1610 DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. • The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification 1 Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 1 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3 D. Program Information (All Application Packages) ® Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. ® How the residuals will be processed/treated (attach process flow diagram). ® How leachate collection will be handled. ® Where the residuals will be stored until processed. ® How the final product will be distributed (packaging, bulk, etc.) ® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ® Name and address of the person who prepared the residual that is sold or given away. ® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ® Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b). ® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). G. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) ® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum- ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. • Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. • Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: City of Burlington Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership [] Privately -Owned Public Utility El Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Shane Fletcher Title: Residuals Management Coordinator Applicant's mailing address: PO Box 1358 City: Burlington State: NC Zip: 27216- Y Telephone number: (336) 570-6138 Email Address: sfletcher@burlingtonnc.gov 2. Consultant's name: N/A License Number (for P.E.): Affiliation- ❑ On Staff ❑ Retained (Firm: ) Consultant's mailing address: City: State: Zip: �- Telephone number: ( ) _- Email Address: 3. Fee submitted: N/A (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0021632 Date of most -recently issued permit: 8/18/2017 Date of most -recently certified Attachment A (if different than the permit): N/A III. FACILITY INFORMATION: 1. Name of residuals processing facility: Source Specific City: State: Zip: Coordinates: Latitude: ° Longitude: _° Datum: Level of accuracy: Method of measurement: County where facility is located: 2. Facility contact (person familiar with residuals preparation): Name: Shane Fletcher Title: Residuals Management Coordinator Mailing address: PO Box 1358 City: Burlington State: NC Zip: 27216- Telephone number: (336) 570-6138 E-mail address: sfletcher@burlingtonnc.gov FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; U No If No, please specify delivery frequency and quantity of residual to be processed: Source Specific 4. Length of residuals storage at facility: Source Specific days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); WTP material is land applied by contractor, WWTP compost material sold/given away in bulk Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added per 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: Source Specific dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: Source Specific dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Source Specific 6. Does the facility have a stormwater management plan? ❑ Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Source Specific V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. RSC 06-16.doc FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) I, , attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my k nowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submi tta 1 packagp may have been developed by otherprofessionals, inclusion of these materials under my signature and seal sign ifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility with out proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15 A NCAC 02T .0105. ❑ Yes 0 No, Explain; I, Shane Fletcher, Residuals Management Coordinator (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for City of Burlington (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technicalreview of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not comp leted and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, anyperson who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as dual -penalties up to $25,000 per violation. Signature: Da te: CP�a 7/2 z Z FORM: DC AR 06-16 Page 3 of 3 SYNAGRO City of Burlington South Burlington Wastewater Treatment Plant Narrative for Class A Residuals This project involves composting and distribution of WWTP residuals from the South Burlington wastewater treatment plant. This material is currently branded as "COMPROGRO". The compost is manufactured from a controlled blend of dewatered biosolids, woody residues, leaves and other compatible organic wastes. The material completes the required process while under a covered shelter and is then moved to the adjacent open air storage pad to await distribution. The material receives no further treatment once moved to the storage pad. The compost is then sold or given away in bulk form. Generally, tractor trailers or dump trucks are loaded with a large loader then these vehicles transport the material to its final destination. An informational label outlining the permit requirements is given to the recipient prior to distribution. SYNAGRO City of Burlington JD Mackintosh Jr WTP Narrative for Class A Residuals This project involves the removal of WTP residuals from the JD Mackintosh Jr water treatment plant. These residuals are produced through the non -biological treatment process. Ultimately the liquid residuals that are developed at the water treatment plant are stored in onsite lagoons. Once field conditions are suitable, the liquid residuals is then hauled to the field via tanker trailers and offloaded to field application equipment. The residuals will then be land applied to agricultural fields at rates well below the agronomic rate due to the low nitrogen content of the material. The residuals receive no further treatment after they are placed in the storage lagoon. Synagro is going to flag the fields to make sure all buffers are followed as outlined in the permit. Synagro is also going to spread all material to further insure that all buffers are followed. SYNAGRO DCAR Marketability Statement JD Mackintosh Jr WTP Residuals will be given to local farmers for crop production. Synagro will land apply material for the local farmers who choose to receive residuals. The spreaders will able to spread the material in an even and consistent manner. The material is going to be land applied on fields that have grass growing on them that are going to either be grazed or cut for hay for animal feed some fields may be in row crop production and rates will be determined by RYE for the crop that is going to be grown for animal consumption. This source has the potential to produce 1300 dry tons annually. SYNAGRO DCAR Marketability Statement South Burlington WWTP Residuals will be given or sold to local farmers for crop production. Recipients will land apply material based on the informational label they receive with the product. The "COMPOGRO" compost is manufactured from a controlled blend of biosolids, woody residues, leaves and other compatible organic wastes. These materials are composted under carefully controlled conditions to assure the highest quality product suitable for topsoil production, flowerbeds, lawn care, shrubbery, golf courses, parks, cemeteries, greenhouses, and nurseries. This source has the potential to produce 2700 dry tons annually. CITY OF BURLINGTON SOUTH BURLINGTON WASTEWATER TREATMENT PLANT 2471 BOYWOOD ROAD, GRAHAM, NC 27253 PO BOX 1358, BURLINGTON, NC 27216-1358 (336) 570-6138 "COMPOGRO" COMPOST INFORMATION SHEET Our "COMPOGRO" compost is manufactured from a controlled blend of biosolids, woody residues, leaves and other compatible organic wastes. These materials are composted under carefully controlled conditions to assure the highest quality product suitable for topsoil production, flowerbeds, lawn care, shrubbery, golf courses, parks, cemeteries, greenhouses, and nurseries. The compost is analyzed routinely and has the following nutrient contents: Available Nutrients per Ton (1 yard of Compogro weighs 812 lbs.) Application Method: N P205 K20 Ca Mg S Fe Mn Zn Cu B Mo Cl Na Broadcast 16.9 6.41 3.49 15.2 2.68 1.31 5.97 0.60 .10 0.03 .02 - - .19 pH 5.5 - 6.5 Soil Incorporation 16.9 6.41 3.49 15.2 2.68 1.31 5.97 0.60 .10 0.03 .02 - - .19 % dry 41.1 Range of values based on the most recent analyses by NCDA&CS for FP # 70 The production of COMPOGRO met all of the temperature requirements for pathogen destruction as required by the EPA and the North Carolina Department of Environment and Natural Resources (NCDENR). The composting process has achieved temperatures of not less than 131 degrees Fahrenheit for three consecutive days, and has been tested for pathogen indicator organisms prior to public distribution. This product has been composted for at least 21 days and cured for more than 21 days to provide additional product quality. The heavy metal content of COMPOGRO is less than or equal to the metals limitations established by EPA and recognized by NCDENR for classification as exceptional quality biosolids. During the composting and curing process, this product met the EPA and NCDENR requirements for vector attraction reduction by achieving an average of 113 degrees Fahrenheit for at least 14 consecutive days. COMPOGRO is suitable for distribution to the public for a variety of agricultural, landscaping, and horticultural uses with the following restrictions: COMPOGRO shall not be applied to land except in accordance with the instructions contained herein. 1. Do not apply if COMPOGRO causes prolonged nuisance conditions 2. Do not ingest or allow others to ingest COMPOGRO. Wash hands after handling. 3. Third parties must be provided with COMPOGRO information sheet. 4. COMPOGRO shall not be applied to any site that is flooded, frozen, or snow covered. 5. COMPOGRO shall not be applied within 25 feet of any surface water. 6. COMPOGRO shall not be applied within 100 feet of any wells or private or public water supply sources. 7. COMPOGRO stored for longer than 14 days must be covered. 8. Adequate precaution must be taken to prevent runoff of COMPOGRO during rainfall events. 9. COMPOGRO should not be applied if it threatens any species listed under section 4 of the Endangered Species Act. 10. COMPOGRO shall not be applied to any area in the 100 Year Flood Elevation unless it is tilled in to the soil. 11. COMPOGRO shall not be applied to an area if there is less than 1-foot separation from the vertical water table. 12. COMPOGRO shall not be applied within 24 hrs following a rainfall event of 0.5 inches or greater. 13. COMPOGRO should be applied at agronomic rates. The end user of this product is expected to use this product as described above. All state and federal regulations are intended for the protection of the public health and the environment. Further educational materials are available upon request. Limited Warranty and Disclaimer: The City of Burlington warrants that the product, COMPOGRO, meets the specifications stated above. Except as stated in the preceding sentence, there are no warranties, express or implied, that extends beyond the representations herein made. Specifically, there are no warranties of merchantability or fitness or suitability thereof for any purpose. If for any reason COMPOGRO fails to meet the specifications, the Buyer's sole remedy shall be limited to the recovery of the purchase price. Under no circumstances shall the City of Burlington be liable for any other damages, including direct, indirect, consequential or special damages. City of Burlington Land Application Permit WQ0021632 Label for Land Application The residuals that are land applied from J.D. Mackintosh JR WTP are produced at: 3400 Harris Rd, Burlington, NC 27215. Mr. Dennis Thomas, JD Mackintosh JR WTP Chief Operator is the preparer of the residuals and responsible for the plant operations. The residuals from J.D. Mackintosh JR WTP will be applied to agricultural fields at agronomic rates based on the RYE rate for the fields and crops to be grown. The WTP residuals will not be applied to frozen, snow covered or flooded fields. The fields will be flagged with the following buffers to help prevent runoff from the applied fields: Setback Description Setback by residual type (feet) Liquid Cake* Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Residuals produced by the City of Burlington will be applied to agricultural fields in bulk and will be applied according this label as well as following all permit conditions as listed in the land application permit WQ0021632. Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters City of Burlington Class A Liquid Residuals Land Application Operations and Maintenance Plan Operational Functions The operational function of this program will involve permit compliant Class A residuals that are land applied to permitted and non -permitted sites by our hired contractor, Synagro. These residuals will be applied at agronomic rates that will be determined by RYE. These residuals will be spread as a liquid at consistent spread patterns by trained Synagro employees. Safety Measures Synagro has a safety program in place in which employees participate in quarterly safety training that is designed to address various safety issues and practices to help prevent accidents. All Synagro employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal injury. The ORC or his designee can suspend operations if there is a condition that warrants such action. The City of Burlington's Water Resources Dept. has an established Safety Program in place that involves yearly training and employee interaction. Equipment Maintenance Schedule Synagro employees will follow the maintenance schedule that is recommended by their fleet manager or site manager. Sampling The City of Burlington will collect all permit required Class A residuals samples and send these out to contract laboratories for analysis. Sampling will be scheduled by the Residuals Management Coordinator (ORC) and collected by the ORC or a designee to conform to event hauling from the specific lagoon where operations are occurring. Effort with be taken to collect representative grab samples directly from the lagoon as operations are occurring. All records generated from sampling will be maintained by the Residuals Management Coordinator and forwarded to Synagro when needed. • Nutrient and Metal samples will be collected based on event volume hauled. One sample will be collected prior to application. The other samples will be collected during the event. • A TCLP will be collected once per year prior to application. • All soil samples from application sites will be collected by Synagro personnel and sent to contract laboratories for analysis. This data will be tracked and shared with the Residuals Management Coordinator for future application purposes. Spill Response Plan See Spill Control Plan, this plan is updated as needed and will always be printed on a nonwhite colored piece of paper. Inspection Plan Inspections of the Land Application fields will be conducted on a weekly basis or as deemed necessary by the ORC or a designee. Prior to an application event the following will be verified by the ORC or designee. • Choose which sites to land apply Class A residuals. • Calculate PAN and check RYE of each field before operations begin to determine application rates. • Check that all manned equipment contains a copy of the Spill Control Plan, NCDWR Permit, and Operations and Maintenance Plan. • Verify that the Application Field Log is correct and that spreader operators are aware of any special circumstances at the site. • Check that all buffering adheres to site application maps or permit required buffers. • Keep a record of all site inspections. The ORC or his designee will report by telephone to the Winston Salem Regional Office as soon as possible but no later than 24 hrs. after or the next working day following the occurrence of the following: • Any occurrence with the land application program which results in the land application of significant amounts of waste which are abnormal in quality or characteristics. • Any failure of the land application program resulting in a release of residuals to receiving waters. • Any time that self- monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of the permit or the parameters on which the system was designed. • Any process unit failure, due to known or unknown reasons that render the facility incapable of adequate residual treatment. • Any spillage or discharge from a vehicle or piping system during transportation of residuals. For any emergency that requires immediate reporting (discharges to surface waters, imminent failure of a storage structure) outside of the normal business hours must be reported to NCDENR at 1-800-662-7956, 1-800-858-0368 or 1-919-733-3300 Persons reporting such occurrences by telephone shall also file a written report in letter form within 5 days following first knowledge of the occurrence. This report must outline the actions taken to remedy the area affected by the discharge and actions taken to avoid future reoccurrence. Persons responsible for inspections of this project are as follows: Shane Fletcher — Residuals Management Coordinator (ORC) or his designee. Last reviewed —1/13/22 BIOSOLIDS SPILL CONTROL PLAN PROJECT: City of Burlington, NC IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Operations Manager shall take immediate charge and initiate clean-up activities. Synagro LLC labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the City of Burlington, the NC Depailnient of Transportation, and other private contractors as necessary. The Operations Manager shall also communicate with the public on the scene, answering questions and advising of the clean-up activities. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation, i.e., local farmers, farm supply centers, nurseries, etc. 4. CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION: As soon as possible after the spill occurs, the Synagro Operations Manager will notify the Synagro Regional office, and they will then be responsible for notifying other key Synagro personnel. The Operations Manager will also be responsible for notifying someone on the calling list from the City of Burlington. After contact has been made with someone from the City, that person will then be responsible for notifying other key city personnel. (See reverse side for contact numbers.) 7. REPORTING: Synagro personnel and/or City of Burlington personnel will notify the Winston-Salem regional office of the NCDENR by telephone immediately, but not more than 24 hours after, or on the next working day following the occurrence. The Operations Manager shall provide a written report within 48 hours of the spill to the Residuals Management Coordinator and the Water Resources Director. The report shall list all relative information and actions taken. Synagro and City of Burlington personnel will file a written report to the Winston-Salem Regional office of the NCDENR within 5 days of the occurrence. A. Synagro Project Manager : Barney James 336-408-8974 mobile C. Residuals Management Coordinator: (City of Burlington) D. Plant Chief Operators: (City of Burlington) E. Water Resources Director (City of Burlington) Assistant Water Resources Director: (City of Burlington) Laboratory Services Manager: (City of Burlington) F. Local Police/Fire Emergency: G. Synagro LLC : Operations Director Operations Manager Technical Services Manager Technical Services Specialist Shane Fletcher 336-675-5927 mobile 336-570-6138 office Rick Asher (South WWTP) 336-350-0387 mobile 336-227-6261 office Darrin Allred (East WWTP) 336-558-8520 mobile 336-578-0515 office Dennis Thomas (Mackintosh WTP) 336-516-5347 mobile 336-584-1393 office Bob Patterson 336-516-2255 mobile 336-227-5743 home 336-222-5130 office Ben Bani 336-264-1474 mobile 336-222-5133 office Sharon Wagoner 336-516-5904 mobile 336-222-5133 office 911 Regional Office 336-790-1610 Todd Larson 336-909-1718 mobile Steve Matchett 704-400-2186 Nate Roth 336-403-4324 mobile Ryan Copeland 336-607-4494 H. NCDENR Winston-Salem Regional Office: NC State Warning Point: (after hours, holidays, weekends) 336-776-9800 800-858-0368 800-662-7956 919-733-3300 (Revised January 7, 2022 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ® For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Maximum Dry Tons Per Year Proposed 1300 2700 Current b 1300 2700 Permit Number N 00 N M 00 O O U z �O t 00 M N O O U z County Alamance Alamance E C0 z U C0 J.D. Mackintosh Jr. WTP South Burlington WWTP Facility Permit Holder City of Burlington NC City of Burlington NC Status Code a P 0) Ct a DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: South Burlington WWTP 2. Facility permit holder is: Federal, State, I Local Government, or Private. Facility permit issued by: I Div. of Water Resources, ▪ Div. of Environmental Health, or 1 Other (explain: _). 3. Facility contact person and title: Richard Asher Complete mailing address: PO Box 1358 City: Burlington State: NC Zip: 27216- Telephone number: (336) 227-6261 E-mail address: rasher@burlingtonnc.gov 4. Facility physical address: 2471 Boywood Rd City: Graham State: NC Zip: 27253-E Coordinates: Latitude: 36' 01' 13" Longitude: 79' 22' 23" Datum: NAD83 Level of accuracy: second Method of measurement: GPS 5. Purpose of the facility: ▪ treatment of municipal wastewater, 1 treatment of 100% domestic wastewater, ▪ treatment of potable water, j treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) ▪ other (explain: _ ). 6. Does the facility have an approved pretreatment program: X Yes No 7. Facility permitted/design flow: 12 MGD and facility average daily flow: 7.58 MGD 8. Average amount of residuals being generated at this facility 2062 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Thickened DAF solids pumped to 1 of 4 digesters Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 digesters with combined storage capacity of 2,357,800 gallons II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: X 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: X Biological Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: E yes X no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: yes X no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: ATT and Date of analysis: 1/18/2022 Passed corrosivity test: X yes 1 no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: X yes no. Flashpoint: °F (> 140°F) Passed reactivity test: X yes Eno. HCN: <0.5 mg/kg (<250) & H2S: <25 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.05 Barium 100.0 <10 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.1 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <0.5 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.1 Lindane 0.4 <0.005 Chlordane 0.03 <0.005 Mercury 0.2 <0.02 Chlorobenzene 100.0 <0.1 Methoxychlor 10.0 <0.1 Chloroform 6.0 <0.1 Methyl Ethyl Ketone 200.0 <2.0 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.5 Pentachlorophenol 100.0 <0.5 o-Cresol 200.0 <0.5 Pyridine 5.0 <0.05 p-Cresol 200.0 <0.5 Selenium 1.0 <0.5 Cresol 200.0 <0.5 Silver 5.0 <1.0 2,4-D 10.0 <1.0 Tetrachloroethylene 0.7 <0.1 1,4-Dichlorobenzene 7.5 <0.05 Toxaphene 0.5 <0.1 1,2-Dichloroethane 0.5 <0.1 Trichloroethylene 0.5 <0.1 1,1-Dichloroethylene 0.7 <0.1 2,4,5-Trichlorophenol 400.0 <0.5 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.5 Endrin 0.02 <0.005 2,4,5-TP (Silvex) 1.0 <1.0 Heptachlor and its Hydroxide 0.008 <0.005 Vinyl Chloride 0.2 <0.2 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: ATT and Date of analysis: 6/1/2022 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <5.0 Cadmium 85 39 <5.0 Copper 4,300 1,500 270 Lead 840 300 <5.0 Mercury 57 17 <0.20 Molybdenum 75 n/a <5.0 Nickel 420 420 <5.0 Selenium 100 100 <5.0 Zinc 7,500 2,800 400 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) n > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 3.27 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: ATT and Date of analysis: 4/29/2022 Parameter Result (mg/kg) Aluminum 3,500 Ammonia -Nitrogen 33,000 Calcium 12,200 Magnesium 8,600 Nitrate -Nitrite Nitrogen 15 pH (Standard Unit) 6.48 Phosphorus 40,000 Potassium 13,000 Sodium 2,000 Total Kjeldahl Nitrogen 45,000 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.61 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This rate is a (check one): X default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN (mg/kg) Five -Year Maximum Adjusted PAN (mg/kg) Surface 19,115 21,116 Injection/Incorporation 35,615 37,616 6. Other Pollutants Determination• S ecify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ▪ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ▪ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): IN Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. El Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. El Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106(b1(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, p heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, ❑ gamma ray irradiation, or pasteurization. b. For Land Application of Class B: ▪ Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or lime stabilization. c. For Surface Disposal: 1171 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. El Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. LI Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ® Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ® Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ® Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. X Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. • Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ® Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 ''A DELORME XMap® 8 :M` AK S�jII `. ALnrBRIGHiT A7,VE';"" _,.INtiGSDVD_ BAor—iTE`S/����1—� HUNTR C �. R0<c..,WELM STQ- i---; Iw'JE-uLLEipire)S� ESAi ST- ,Z,P" --� Graham-,• <<mo N D 1) ,.4Loj O Jonzlrn iron,!, z LJL, u�r %" d y]rn-` ' _148 `-2pT 147 147�� ' (0 BRUCE)TURNEY ST -�'SR� H 1 PU� O. LINA.CIR 9- Q- OIJI P�y OCLC, , ``.p� y 1 '4. 3 �;,./ Op , 2�e 1. car # a r I P AQ P t..1.711.8OODLN U071,.E CR6EK DR McGEE SS :sT cs Rockwood ,S 10 �BioadAcres R'9-O Woodshlre Estates COVIN GTON•RD r 0 SCENIC DR E1.IZABETH 1, ..yP 140 F tV E 0 wr •JOE�R I •� 15011 ��O- 150 J T A I-�o!.I A I 00 y� Mart daIC_Acres { J 'ry �fy• \r1ncO •, f l��cm N!% rn CZ I V' WASTE1WA`7ER,PLAN7 R0, sP , I q 00 Cooper Est'ues ,/ p0 REATKIN LN o Maplc rove Acres, s‘ r, Bo L1R ANNIEI])ANE• 'C'T.. ti� R21 Or B<:UMAN CF B O GG S RANCH RD CHUCK GARNER TR. HERRON• WO)DD �R'�', HOLT LN' m'• 0 z rn • 0 • 0 O� 0 rs, r1` N A j z A r/ II ,GARDEN PEACH_BI D LN mp > D • 3I s U / j, r Iw p. StSPCT . f�,C/% PATRIO ` 5, I•tOUNT HERh10N.;R0CK CRK RD OCK CRK aD r1ouN?at•,_ o�• TRn BR0O —\ Data use subject to license. DeLorme. XMap® 8. www.delorme.com • or e; 1 op/, •, `•P_ , \r 1 QUANDRY TRL i.. 1'1 rin on1 v'o Ohs 5) P 1 is 5) KtMp.�y 0.0 J N Q y2� South Burlington WWTP/Compost Facility, P V ill i- A -t Jr O / \ ,l S `m SwepsonTL r ~/ - ,ERNE57 17 LfJ GROVE LN '• i 1'•: Cy W' T 'm /'y. .ro ";/Melville l I eOIV 4/4,,, O -rt— I > ,00 <N �� CRYSTAL ING GT x P r m 1D LEE Gm • 3 7. Sy LN � /Gnt-mil 1-, Scale 1:50,000 NININE IMMO I■ N 0 1/4 1A 3/4 1" = 4,166.7 ft mi 1 11/4 11/ Data Zoom 12-0 SOUTH BURLINGTON WASTEWATER TREATMENT PLANT QUANTITATIVE JUSTIFICATION FOR RESIDUALS The following is a record of the last 3 years in which class A material was distributed from the above referenced plant: Year Dry Tons Removed 2021 0 2020 244.93 2019 575.84 As shown above the last year material was generated and distributed under this Class A permit was 2020. This was done because of increasing cost and currently available alternate disposal options. However, it is requested that the current combined total of 2700 dry tons per year be kept in place to ensure an additional disposal option is available if needed in the near future. Residuals Sampling Plan South Burlington Wastewater Treatment Plant Class A Distribution Nutrients and Metals Analysis Sampling Point: Compost Pile (Batched) Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Composite Lab: American Testing Technologies Inc Pathogen: Fecal Demonstration/Composting Sampling Point: Compost Pile (Batched) Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Composite Lab: In-house Vector: 14 Day Aerobic Process Sampling Point: Compost Pile (Batched) Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Composite Lab: Temperature/Time verified In-house TCLP Sampling Point: Compost Pile (Batched) Sampling Frequency: Annually Sample Type: Composite Lab: American Testing Technologies, Inc • • • • • ■ • • i Aeration Basin #2 aE • • • N sn • 4D It 023 1-4 d • • • • • • • • O P=1 ciD ( 0 ciD • i pi _____. a L) • • • • U • f c7 0 0 Vehicle Parking IL L a • • • • N i • • i • • i • • • J ORIGINAL- RETURN TO LABORATORY W (S131dWIIVS H m J z c� o U7 { • 0 O 3 173 z . O 0 0 O m 0 z m 0 ni 0 c a 0 m 0 (321f11yN9Is) :A8 03AIMO3a 0 P1 m P1 m P1 m 1 1 EMI 1111111111111111111 III NM IIMENIIMMIIIII VIIMINIIMII MINIM AIIIIIIIMIMIII 0 r; 10. Fn m z a 0 m a m z P1 m m 0 z 0 m m Ink iJ38WfN '0'd 'ON tOVWJNOO COMPOSITE (C) OR GRAB (G) INDICATE AQUEOUS (WATER) SOLID OR SEMISOLID AIR NONAQUEOUS LIQUID (OIL, SOLVENT, ...) IW8f1S SNRNIVIN0 0 1VNV Q3aIflb3a 'ON 10310dd Pz m C co m xm � a Cs m m zn o 0 m 0 u) u) 0 0 0 Co 0 m r m m -- 0 _am 0 v „,„& 0 0 Bu1lsal ueouauUV 0 0 0 0 CD N n 0 X. =�oCD roll• DC� !c tD N CD P. O eS N .� o 3 ra w-u 0 tu S 3 oco o. n co 00get 0 -. wm � N bg 0 0 3 2 _. o i W 0 ngwn j pins 0 0 0) 02/24/2022 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 American Testing Technologies, Inc. Report No.: 010622-22 26 Enclosed are the results of the sample(s) submitted to our laboratory on 01/06/2022.All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on an ``as -received" wet basis unles otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the labo4atory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy(eZamericantestinatechnologies.cosy€ SL- Test performed by an approved subcontract laboratory BRL- Below Reporting limit The results relate only to the items tested. ATT s1811 have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT 's liability with respect to the Test Results exceed the amount paid to ATT by the client therefore. 1350 Home Avenue Akron, Ohio 44310 Tall Free: 877.634.9906 Phone: 330.634.9906 Fax. 330.634.9907 www.ArnericanTestingTechnoiogies.com Page 1 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID if: 010622-22 Date of Analysis: 01/18/2022 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Lints Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenimn <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D Fil rt reviewed by: arat anager 1350 Home Avenue Akron, Ohio 44310 Tali Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingiechnologies.com Page 2 of 31 American Testing Technologies, Inc. City of Burlington, NC Atm: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 01/14/2022 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D ort reviewed by: Laaboora • >> Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericanTestingTechnologies.com Page 3 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.corn Page 4 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received:, 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 808IB Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxyehlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toff Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.corn Page 5 of 31 City of Burlington, NC Atin: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A reviewed by: Laborato 1 a anager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericaniestingTechnologies.com Page 6 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 xng/kg 7.3.4.1 01/17/2022 pH (Lab) 12.75 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 eport reviewed by: Manager 1350 Florae Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologles.com Page 7 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 01/18/2022 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromi»m <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fox: 330.634.9907 www.AmericanTestingTechnologies.com Page 8 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 01/14/2022 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg /i 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 ntg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2:0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 9 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mglL 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C Fin ; ort reviewed by: r- Lab.�'sjt• j :, anger 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 10 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01106/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/11/2022 American Testing Technologies, Inc. Certificate of Analysis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Undone <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 11 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 2,4,5-TP (Silvex) <1.0 mg/L 10.0 8151A mg/L 1.0 8151A 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 12 of 31 City of Burlington NC Attn: Sharon Wagoner 1302 Belmont Street Burlington NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 6.81 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 1350 Home Avenue Akron, Ohio 44310 Tall Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 13 of 31 City of Burlington, NC Attn: Sharon. Wagoner 1302 Belmont Street' Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 01/18/2022 Metals-TCLP (EPA 1311) American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 14 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 01/14/2022 Volatiles-TCLP (EPA 1311) American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D Pik report reviewed by: 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corm Page 15 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 n g/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-CresoI <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4;6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Horne Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax; 330.634.9907 www.Am e ri ca nT est i n gTec h n o l ogi es. co m Page 16 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Receive& 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B Fin•r .art reviewed by: Labs ato 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877_634.9906 Phone: 330.634.9906 Fax; 330.634.9907 www.AmericanTestingTechnologies.com Page 17 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 18 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 6.68 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 1350 Home Avenue Akron. Ohio 44310 ron Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 19 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory 1D #: 010622-25 Date of Analysis: 01/18/2022 Metals-TCLP (EPA 1311) American Testing Technologies, inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium. <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D Fink - . • reviewed by: \Hager 1350 Home Avenue Akron, Ohio 44310 Toll Free; 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericanTestingTechnologies.cam Page 20 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 01/15/2022 American Testing Technologies, inc. • Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichioroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D Fin .a r- rt reviewed by: Labanager 1350 Home Avenue Akron, Oho 44310 Toil Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 21 of 31 American Testing Technologies, Inc. City of Burlington, NC Attu: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexxachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avenue Akron, Ohio 44310 Toil Free_ 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 22 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 nig/L 0.03 8081E Endrin <0.005 mg/L 0.02 8081E Heptachlor <0.005 mg/L 0.008 8081E Heptachlor epoxide <0.005 mg/L 0.008 8081B Linrlane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 23 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/18/2022 Certificate of Analysis Herbicides-TCLP (EPA 1311) Parameter Results Unfits Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A rt reviewed by: Laboraanager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 24 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 7.37 s.u. 9045D 01/07/2022 Flash point >140 of 1010A 01/14/2022 Find r rt reviewed by: Laboxato .ger 1350 Home Avenue Akron, Ohio 44310 Toll Free_ 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 25 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 01/18/2022 American Testing Technologies, Inc. Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium_<0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 rng/L 0.2 7470A Selenium <0.5 nng/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D rt reviewed by: La:. rat. " Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 26 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 01/15/2022 American Testing Technologies, Inc. Certificate of Analvsis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetraehloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 ang/L 0.5 8260D Vinyl chloride <0.2 anglL 0.2 8260D port reviewed by Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fox: 330.634.9907 www.AmericanTestingTechnologies.com Page 27 of 31 American Testing Technologies, fnc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene .<0.05 mg/L 7.5 8270C 2,4-D nitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mglL 0.13 8270C HexaehIorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 . 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol. <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C ort reviewed by: La clzatd \ anager 1350 Home Avenue Akron. Ohio 44310 Toll Free: 877.634.9906 Phone: 330,634.9906 Fax. 330.634.9907 www.AmericanTestingTechnoiogies.com Page 28 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081E Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081E Methoxychlor <0.1 mg/L 10.0 8081R Toxaphene <0.1 mg/L 0.5 8081B port reviewed by: Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 29 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A ort reviewed by: anager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericaraTestingTechnologies.corn Page 30 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 American Testing Technologes, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Snnl Ides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 8.22 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 Fin. e. reviewed by: ger 1350 Home Avenue Akron, Ohio 44310 Tot! Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 31 of 31 LABDRATO,RY U RECEIVED FOR LABA0HATO)r E ' TIME CIISTODYINT CUSTODY (SIGNATURE) I ,SO "YES' . SEAL NO.. -; FECEIVED BY: (SIGNATURE) �d Q m SAMPL) CLIENT ADDMSS (� cI T �X 1 CLIENT NAME Ci°kj everE Mrr '1 CLIENT(SITE) �J - PROJECT MANAdER l�o�n V.i ( Ci ,W/ o m s 2rn m m o m g ATIr ANALYSIS REQUEST AND CHAIN OF CUSTODY. RECORD American Testing Technologies. Inc. a 71 L C SAMPLE IDENTIFICATION m m m m CLIENT EMAIL t' Oli. JtAJGrronte.,r 3"A'�rMat-Ir'�nT1(, CLIENT PHONE P.O. NUMBER PROJECT NO. FM mFMm RECEIVED BY: (SIGNATURE) RELINQUISHED BY:'(sIGNATURE) CLIENT FAX CONTRACT ND. PROJECTLO TION (STATE) j[,. �.. .r,3 COMPOSITE{C) OR GRAB (G) INDICATE 3. m x AQUEOUS (WATER) SOLID OR SEMISOLID AIR American Testing Technologies, Inc. 1350 Home Avenue Akron, OH 44310 Website: www.AmericanTestingrechnoiogies.com Toll Free: 877-634-9906 Phone: (330) 639-9906 Fax: (330) 634-990 7 NONAQUEOUS LIQUID (OIL, SOLVENT, ...) Gil SE.ONLY 1 Co` N MBER OF CONTAINERS SUBMITTED REQUIRED ANALYSIS rn m (`� US, FL rst {{�.. RECEIVED BY (SIGNATURE) RELINQUISHED BY: {SIGNATURE) ('�I� \A 1/45r� d m A Si S NUMBER OF COOLERS SUBMITTED i PER SHIPMENT: !J STANDARD REPORT DELIVERY DATE DUE EXPEDITED REPORT DELIVERY O (SURCHARGE) DATE DUE Q rri G 1 3 4 -n M m M m 06/01/2022 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Report No.: 042822-35 36 American Testing Technologies, Inc. Enclosed are the results of the sample(s) submitted to our laboratory on 04/28/2022. All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on a dry weight basis unless otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the laboratory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy{clamericantestinQtechnologies. com SL- Test performed by an approved subcontract laboratory BRL- Below Reporting linut The results relate only to the items tested. ATT shall have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT 's liability with respect to the Test Results exceed the amount paid to ATT by the client therefore. 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 1 of 3 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 04/28/2022 Date Reported: 06/01/2022 Date Collected: 04/26/2022 Time Collected: 1215 Client ID #: Lagoon #2 Laboratory ID #: 042822-35 American Testing Technologies, Inc. Certificate of Analysis Parameter Result (%) Result (mg/kg) Analysis Date Method . Aluminum, Total 151,100 04/29/2022 6010D Arsenic, Total <5.0 04/29/2022 6010D Cadmium, Total <5.0 04/29/2022 6010D Calcium, Total 1.0 10,200 04/29/2022 6010D Chromium, Total 170 04/29/2022 6010D Copper, Total 40 04/29/2022 6010D Iron, Total 21,000 04/29/2022 6010D Lead, Total <5.0 04/29/2022 6010D Magnesium, Total 0.28 2,800 04/29/2022 6010D Manganese, Total 2,600 04/29/2022 6010D Mercury, Total <0.20 04/29/2022 7471B Molybdenum, Total <5.0 04/29/2022 6010D Phosphorus, Total 0.24 2,400 04/29/2022 6010D Nickel, Total <5.0 04/29/2022 6010D Potassium, Total 0.14 1,400 04/29/2022 6010D Selenium, Total <5.0 04/29/2022 6010D Sodium, Total 0.94 9,400 04/29/2022 6010D Sulfur, Total 1.3 13,000 04/29/2022 6010D Zinc, Total 125 04/29/2022 6010D Total Kjeldahl Nitrogen 1.90 19,000 05/13/2022 SM-4500 Ammonia Nitrogen 0.90 9,000 05/13/2022 SM-4500 Organic Nitrogen 1.00 10,000 05/13/2022 Calculation Nitrate+Nitrite- N 10 05/13/2022 SM-4500C Calcium Carbonate Equivalent 35 350,000 05/20/2022 AOAC 955.01 Total Solids 0.88 8,800 04/30/2022 SM-2540G Total Volatile Solids 20 200,000 04/30/2022 SM-2540G Moisture 99.12 04/30/2022 SM-2540G 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone; 330.634.9906 Fax 330.634.9907 www.AmericanTestingTechnoiogies.com . Page 2 of 3 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 04/28/2022 Date Reported: 06/01/2022 Date Collected: 04/26/2022 Time Collected: 0820 Client ID #: SB Digester 1 'Laboratory ID #: 042822-36 American Testing Technologies, Inc. Certificate of Analysis Parameter Result (%) Result (mgg) Analysis Date Method Alnminum, Total 3,500 04/29/2022 6010D Arsenic, Total <5.0 04/29/2022 6010D Cadmium, Total <5.0 04/29/2022 6010D Calcium, Total 1.2 12,200 04/29/2022 6010D Chromium, Total 40 04/29/2022 6010D Copper, Total 270 04/29/2022 6010D Iron, Total 8,000 04/29/2022 6010D Lead, Total <5.0 04/29/2022 6010D Magnesium, Total 0.86 8,600 04/29/2022 6010D Manganese, Total 600 04/29/2022 6010D Mercury, Total <0.20 04/29/2022 7471B Molybdenum, Total <5.0 04/29/2022 6010D Phosphorus, Total 4.0 40,000 04/29/2022 6010D Nickel, Total <5.0 04/29/2022 6010D Potassium, Total 1.3 13,000 04/29/2022 6010D Selenium, Total <5.0 04/29/2022 6010D Sodium, Total 0.2 2,000 04/29/2022 6010D Sulfur, Total 0.9 9,000 04/29/2022 _ 6010D Zinc, Total 400 04/29/2022 6010D Total Kjeldahl Nitrogen 4.50 45,000 05/13/2022 SM-4500 Ammonia Nitrogen 3.30 33,000 05/13/2022 SM-4500 Organic Nitrogen 1.20 12,000 05/13/2022 Calculation Nitrate+Nitrite- N 15 05/13/2022 , SM-4500C Calcium Carbonate Equivalent 30 300,000 05/20/2022 AOAC 955.01 Total Solids 3.27 32,700 04/30/2022 SM-2540G Total Volatile Solids 55 550,000 04/30/2022 SM-2540G Moisture 96.73 04/30/2022 SM-2540G 1350 Home Avenue Akron, Ohio 44310 Tot! Free: 877.634.9906 Phone: 330.634.9905 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 3 of 3 rYSay,i, ,,.`ICES 336-222-5133 ....., a ,ems :Gl _,-_?., ..,,,,,, .,... , .1.,0 ._., c..., -o-: __, \...---, . +, _._\ ,__, ,---.. PJ_7 b co a South WWTP Digester #2 South WWTP Digester #3 South WWTP Digester #4 East WWTP Digester #1 Mackintosh Lagoon #1 Mackintosh Lagoon #2 Compost ____. 0 .. Cr.; O CITY OF BURLINGTON POST OFFICE BOX 1358 BURLINGTON NC 27216-1358 336-570-6138 CONTACT PERSON — SHANE FLETCHER SOUTH BURLINGTON WASTEWATER TREATMENT PLANT CHAIN OF CUSTODY FOR LAND APPLICATION OF BIOSOLIDS SAMPLE SAMPLE LOCATION: D SQ f te"— SAMPLED BY: SI/l DATE: V/a-4 /7-0 2-2-- PH RESULT Qq DELIVERED TO C.O.B. LAB BY: A-6 i70 'L Z DATE: RECEIVED IN C.O.B. LAB BY: DATE: (L(oi 7,7 SHIPPED FROM C.O.B. LAB BY: dkon\ktynLk2 L-41,(11,f/ PH TIME TIME: OR?� 1 IN 0111 PH ANALYST, T ME: KPz-V\ DATE: RECEIVED IN A & L LAB BY; TIME: (2-'( 3 TIME: j 2,-t r� DATE; TIME; SEND COPY TO SYNAGRO na SYNAGRO SOUTHEAST, INC. 6220-Suite A Hackers Bend Court WINSTON-SALEM, NC 27103 TELEPHONE-1-877-267-2687 FAX - 336-766-8652 SAMPLE I.D.#SB SEND COPY TO SHANE FLETCHER City of Burlington P.O. BOX 1358 BURLINGTON NC 27216-1358 TELEPNONE 336-570-6138 FAX 336-570-6139 DO NOT RUN pH PLEASE RUN: RUN SO4 RUN SL1 & SL2 plus the following - RUN NI14-N, NO3-N, ORGANIC N, Cd, Cr, Ni, Pb, As, Hg, Se, CaCO3 equiv., Volatile Solids, Mo, CI * Will the results of this sample be used for compliance reporting. NCDENR-DWQ WATER QUALITY SECTION NON -DISCHARGE COMPLIANCE ENFORCEMENT SECTION 1617 MAIL SERVICE CENTER RALEIGH NC 27699-1617 YES NO CITY OF BURLINGTON Laboratory Services Report Date: 5/22/2020 Sample ID: Finished Pile 70 ID #: 200504 Initial testing Cetificate of Analyses 60 day repeat Failure Repeat no. FAIL PASS Sample #: A B C C-Dup Sample Date: 0519/20 5/19/2020 5/19/2020 5/19/2020 Sample Time: 0830 0832 0835 0835 pH: 5.6 5.6 5.5 5.5 Solids: 43.0 40.3 47.9 40.4 Fecal Coliform: MPN/dr Y grm) 77 195 501 594 1 �ttif N.t x( a 4i14.1� masl�fi`c-',.uM3iY� (( . >� a.iy1'�.3w.i£s.>� Geometric mean= average of C= 548 MPN/dry grm 258 Certified by: 7{1Jf/7 Glenn cGirt Laboratory Supervisor NC Wastewater Certification #188 NC Water Supply Certification #37612 CITY OF BURLINGTON POST OFFICE BOX 1358 BURLINGTON NC 27216-1358 336-570-6138 CONTACT PERSON - SHANE FLETCHER COMPOST FACILITY CHAIN OF CUSTODY FOR COMPOST FECAL COLIFORM SAMPLE SAMPLE LOCATION: ni:C`21 P ( 0 SAMPLED BY: cc\I-._ C.7) j _ arro�' Q�.7.� DATE:/f /76`20TIME: 3 - /i?i1 DELIVERED BY: s4.0---.-kL.) � DATE: (� �170� TIME: IN LAB BY: G `-' RECEIVED DATE: t y ./1Q "Z6 TIME: SHIPPED BY: DATE: TIME: REMARKS SAMPLE I.D.# 219ciw SAMPLE I.D.# & - OCfO ct SAMPLE I.D.# C - a 00 rag SAMPLE I.D.# * Will the results of this sample be used for compliance reportins. YES NO NCDENR-DWQ WATER QUALITY SECTION NON -DISCHARGE COMPLIANCE ENFORCEMENT UNIT 1617 MAIL SERVICE CENTER RALEIGH NC 27699-1617 COMPOST PILE TEMPERATURE'S ALL TEMPERATURES ARE REPORTED IN FAHRENHEIT 10/18/2019 191003-10 147.5 148 146 146 150 69 191210 SH 10/19/2019 191003-10 156.5 150 158 158 160 69 191210 GH 10/20/2019 191003-10 157 150 158 160 160 69 191210 GH 10/21/2019 191003-10 149 150 150 146 150 69 191210 SH 10/22/2019 191003-10 149 150 150 146 150 69 191210 SH 10/23/2019 191003-10 149 150 150 146 150 69 191210 SH 10/24/2019 191003-10 148.5 146 150 148 150 69 191210 SH 10/25/2019 191003-10 148.5 146 150 148 150 69 191210 SH 10/26/2019 191003-10 148.75 149 148 148 150 69 191210 SH 10/27/2019 191003-10 148 146 148 148 150 69 191210 SH 10/28/2019 191003-10 148 146 150 146 150 69 191210 SH 10/29/2019 191003-10 148 146 150 146 150 69 191210 SH 02/26/20 200225-10 118 115 115 125 117 70 200504 wjs 02/27/20 200225-10 139.25 145 130 150 132 70 200504 wjs 02/28/20 200225-10 144.5 160 136 150 132 70 200504 sh 02/29/20 200225-10 145.5 160 140 150 132 70 200504 jh 03/01/20 200225-10 145.5 160 140 150 132 70 200504 jh 03/02/20 200225-10 145.5 162 144 158 138 70 200504 sh 03/03/20 200225-10 150.5 162 144 158 138 70 200504 sh 03/04/20 200225-10 150.5 162 144 158 138 70 200504 sh 03/05/20 200225-10 153 162 150 158 142 70 200504 sh 03/06/20 200225-10 153 162 150 158 142 70 200504 sh 03/07/20 200225-10 153.5 162 150 160 142 70 200504 gh 03/08/20 200225-10 154 162 150 162 142 70 200504 gh 03/09/20 200225-10 154 162 150 162 142 70 200504 sh 03/10/20 200225-10 154 162 150 162 142 70 200504 sh 03/11/20 200225-10 154 162 150 162 142 70 200504 sh 03/12/20 200225-10 154 162 150 162 142 70 200504 sh 03/13/20 200225-10 155 160 150 160 150 70 200504 sh 03/14/20 200225-10 155 160 150 160 150 70 200504 ac 03/15/20 200225-10 155 160 150 160 150 70 200504 ac 03/16/20 200225-10 155 160 150 160 150 70 200504 sh 03/17/20 200225-10 155 160 150 160 150 70 200504 sh 02/26/20 200225-08 124.5 120 116 140 122 70 200504 wjs 02/27/20 200225-08 129 132 122 140 122 70 200504 wjs 02/28/20 200225-08 132.5 138 132 142 118 70 200504 sh 02/29/20 200225-08 133.25 138 130 145 120 70 200504 jh 03/01/20 200225-08 133.75 140 130 145 120 70 200504 jh 03/02/20 200225-08 134 140 132 142 122 70 200504 sh 03/03/20 200225-08 134 140 132 142 122 70 200504 sh 03/04/20 200225-08 134 140 132 142 122 70 200504 sh 03/05/20 200225-08 137 140 136 142 130 70 200504 sh 03/06/20 200225-08 137 140 136 142 130 70 200504 sh 03/07/20 200225-08 137 140 134 144 130 70 200504 gh 03/08/20 200225-08 137 140 134 144 130 70 200504 gh 03/09/20 200225-08 137 140 134 144 130 70 200504 sh 03/10/20 200225-08 137 140 134 144 130 70 200504 sh 03/11/20 200225-08 137 140 134 144 130 70 200504 sh 03/12/20 200225-08 137 140 134 144 130 70 200504 sh 03/13/20 200225-08 137.5 140 136 144 130 70 200504 sh 03/14/20 200225-08 137.75 140 136 145 130 70 200504 ac 03/15/20 200225-08 138.75 140 140 145 130 70 200504 ac 03/16/20 200225-08 138.75 140 140 145 130 70 200504 sh 03/17/20 200225-08 138.75 140 140 145 130 70 200504 sh 02/26/20 200225-07 120 120 122 118 120 70 200504 wjs 02/27/20 200225-07 131.25 130 130 140 125 70 200504 wjs 02/28/20 200225-07 133 130 136 144 122 70 200504 sh 02/29/20 200225-07 133.75 130 140 145 120 70 200504 jh 03/01/20 200225-07 126.25 130 110 145 120 70 200504 jh DAILY TEMPS.xls Page 556 COMPOST PILE TEMPERATURE'S ALL TEMPERATURES ARE REPORTED IN FAHRENHEIT 03/02/20 200225-07 136.5 134 142 146 124 70 200504 sh 03/03/20 200225-07 136.5 134 142 146 124 70 200504 sh 03/04/20 200225-07 136.5 134 142 146 124 70 200504 sh 03/05/20 200225-07 142 140 150 148 130 70 200504 sh 03/06/20 200225-07 142 140 150 148 130 70 200504 sh 03/07/20 200225-07 143 142 152 148 130 70 200504 gh 03/08/20 200225-07 144 142 152 150 132 70 200504 gh 03/09/20 200225-07 144 142 152 150 132 70 200504 sh 03/10/20 200225-07 144 142 152 150 132 70 200504 sh 03/11/20 200225-07 144 142 152 150 132 70 200504 sh 03/12/20 200225-07 144 142 152 150 132 70 200504 sh 03/13/20 200225-07 143.5 142 154 144 134 70 200504 sh 03/14/20 200225-07 141.5 142 145 145 134 70 200504 ac 03/15/20 200225-07 143.75 142 154 145 134 70 200504 ac 03/16/20 200225-07 143.75 142 154 145 134 70 200504 sh 03/17/20 200225-07 143.75 142 154 145 134 70 200504 sh 02/26/20 200225-06 116.5 117 116 118 115 70 200504 wjs 02/27/20 200225-06 133.25 128 125 140 140 70 200504 wjs 02/28/20 200225-06 135 128 120 142 150 70 200504 sh 02/29/20 200225-06 135 128 120 142 150 70 200504 jh 03/01/20 200225-06 135.5 130 120 142 150 70 200504 jh 03/02/20 200225-06 143 130 130 150 162 70 200504 sh 03/03/20 200225-06 143 130 130 150 162 70 200504 sh 03/04/20 200225-06 143 130 130 150 162 70 200504 sh 03/05/20 200225-06 146 134 138 150 162 70 200504 sh 03/06/20 200225-06 146 134 138 150 162 70 200504 sh 03/07/20 200225-06 146 134 138 150 162 70 200504 gh 03/08/20 200225-06 146.5 134 140 150 162 70 200504 gh 03/09/20 200225-06 146.5 134 140 150 162 70 200504 sh 03/10/20 200225-06 146.5 134 140 150 162 70 200504 sh 03/11/20 200225-06 146.5 134 140 150 162 70 200504 sh 03/12/20 200225-06 146.5 134 140 150 162 70 200504 sh 03/13/20 200225-06 145.5 136 142 142 162 70 200504 sh 03/14/20 200225-06 145.5 136 142 142 162 70 200504 ac 03/15/20 200225-06 145.5 136 142 142 162 70 200504 ac 03/16/20 200225-06 145.5 136 142 142 162 70 200504 sh 03/17/20 200225-06 145.5 136 142 142 162 70 200504 sh 02/26/20 200225-05 115.5 116 117 115 114 70 200504 wjs 02/27/20 200225-05 132.5 130 135 135 130 70 200504 wjs 02/28/20 200225-05 137.5 132 140 138 140 70 200504 sh 02/29/20 200225-05 137.5 132 140 138 140 70 200504 jh 03/01/20 200225-05 137.5 132 140 138 140 70 200504 jh 03/02/20 200225-05 139.5 138 140 140 140 70 200504 sh 03/03/20 200225-05 139.5 138 140 140 140 70 200504 sh 03/04/20 200225-05 139.5 138 140 140 140 70 200504 sh 03/05/20 200225-05 139.5 138 140 140 140 70 200504 sh 03/06/20 200225-05 140.5 140 140 142 140 70 200504 sh 03/07/20 200225-05 141 140 140 144 140 70 200504 gh 03/08/20 200225-05 142 142 140 144 142 70 200504 gh 03/09/20 200225-05 142 142 140 144 142 70 200504 sh 03/10/20 200225-05 142 142 140 144 142 70 200504 sh 03/11/20 200225-05 142 142 140 144 142 70 200504 sh 03/12/20 200225-05 142 142 140 144 142 70 200504 sh 03/13/20 200225-05 138.5 140 140 144 130 70 200504 sh 03/14/20 200225-05 138.5 140 140 144 130 70 200504 ac 03/15/20 200225-05 138.5 140 140 144 130 70 200504 ac 03/16/20 200225-05 138.5 140 140 144 130 70 200504 sh 03/17/20 200225-05 138.5 140 140 144 130 70 200504 sh 02/26/20 200225-04 123.75 142 120 118 115 70 200504 wjs DAILY TEMPS.xls Page 557 COMPOST PILE TEMPERATURE'S ALL TEMPERATURES ARE REPORTED IN FAHRENHEIT 02/27/20 200225-04 141.25 150 145 140 130 70 200504 wjs 02/28/20 200225-04 152 156 158 156 138 70 200504 sh 02/29/20 200225-04 149.25 150 160 155 132 70 200504 jh 03/01/20 200225-04 151.75 155 160 160 132 70 200504 jh 03/02/20 200225-04 156 162 160 158 144 70 200504 sh 03/03/20 200225-04 156 162 160 158 144 70 200504 sh 03/04/20 200225-04 156 162 160 158 144 70 200504 sh 03/05/20 200225-04 157.5 162 162 158 148 70 200504 sh 03/06/20 200225-04 157.5 162 162 158 148 70 200504 sh 03/07/20 200225-04 158.5 164 162 158 150 70 200504 gh 03/08/20 200225-04 159 164 162 160 150 70 200504 gh 03/09/20 200225-04 159 164 162 160 150 70 200504 sh 03/10/20 200225-04 159 164 162 160 150 70 200504 sh 03/11/20 200225-04 159 164 162 160 150 70 200504 sh 03/12/20 200225-04 160 168 162 160 150 70 200504 sh 03/13/20 200225-04 159.5 170 164 156 148 70 200504 sh 03/14/20 200225-04 159.5 170 164 156 148 70 200504 ac 03/15/20 200225-04 159.5 170 164 156 148 70 200504 ac 03/16/20 200225-04 159.5 170 164 156 148 70 200504 sh 03/17/20 200225-04 159.5 170 164 156 148 70 200504 sh 02/26/20 200225-03 120.25 101 141 114 125 70 200504 wjs 02/27/20 200225-03 143 136 158 138 140 70 200504 wjs 02/28/20 200225-03 145 140 160 140 140 70 200504 sh 02/29/20 200225-03 145 140 160 140 140 70 200504 jh 03/01/20 200225-03 145 140 160 140 140 70 200504 jh 03/02/20 200225-03 145 156 162 142 142 70 200504 sh 03/03/20 200225-03 150.5 156 162 142 142 70 200504 sh 03/04/20 200225-03 150.5 156 162 142 142 70 200504 sh 03/05/20 200225-03 153.5 156 162 146 150 70 200504 sh 03/06/20 200225-03 153.5 156 162 146 150 70 200504 sh 03/07/20 200225-03 154 156 164 146 150 70 200504 gh 03/08/20 200225-03 155 156 164 148 152 70 200504 gh 03/09/20 200225-03 155 156 164 148 152 70 200504 sh 03/10/20 200225-03 155 156 164 148 152 70 200504 sh 03/11/20 200225-03 155 156 164 148 152 70 200504 sh 03/12/20 200225-03 155 156 164 148 152 70 200504 sh 03/13/20 200225-03 156.5 152 166 150 158 70 200504 sh 03/14/20 200225-03 156.5 152 166 150 158 70 200504 ac 03/15/20 200225-03 156.5 152 166 150 158 70 200504 ac 03/16/20 200225-03 156.5 152 166 150 158 70 200504 sh 03/17/20 200225-03 156.5 152 166 150 158 70 200504 sh DAILY TEMPS.xls Page 558 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Maximum Dry Tons Per Year Proposed 1300 2700 Current b 1300 2700 Permit Number N 00 N 00 O U z �O r o0 N O U z County Alamance Alamance E C0 z U C0 J.D. Mackintosh Jr. WTP South Burlington WWTP Facility Permit Holder City of Burlington NC City of Burlington NC Status Code a P p 0) GA ees DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: J.D. Mackintosh Jr. WTP 2. Facility permit holder is: ❑ Federal, State, Local Govemment, or [1 Private. Facility permit issued by: 0 Div. of Water Resources, Div. of Environmental Health, or n Other (explain: _). 3. Facility contact person and title: Dennis Thomas, Chief Operator Complete mailing address: 3400 Harris Rd. City: Burington State: NC Zip: 27215- Telephone number: 336-584-1393 E-mail address: 4. Facility physical address: 3400 Harris Rd. City: Burlington State: NC Zip: 27215- Coordinates: Latitude: R6'02' 32" Longitude: 79' 30' 23" Datum: _ Level of accuracy: Seconds Method of measurement: 5. Purpose of the facility: ▪ treatment of municipal wastewater, 1 treatment of 100% domestic wastewater, ▪ treatment of potable water, j treatment of 100% industrial wastewater, ▪ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ® Yes ❑ No 7. Facility permitted/design flow: 18.0 MGD and facility average daily flow: 8_0 MGD 8. Average amount of residuals being generated at this facility est. 350 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Water Treatment Process Type and volume of residuals storage (i.e., outside of residuals treatment units): 2 lagoons est. 4 million gallons each II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ▪ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ▪ Biological Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: El yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: I❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: American Testing and Tech Inc and Date of analysis: 1/18/2022 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >140 °F (> 140°F) Passed reactivity test: ® yes Ono. HCN: <0.5 mg/kg (<250) & H2S: <25 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.05 Barium 100.0 <10 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.1 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <0.5 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.1 Lindane 0.4 <0.005 Chlordane 0.03 <0.005 Mercury 0.2 <0.02 Chlorobenzene 100.0 <0.1 Methoxychlor 10.0 <0.1 Chloroform 6.0 <0.1 Methyl Ethyl Ketone 200.0 <2.0 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.5 Pentachlorophenol 100.0 <0.5 o-Cresol 200.0 <0.5 Pyridine 5.0 <0.05 p-Cresol 200.0 <0.5 Selenium 1.0 <0.5 Cresol 200.0 <0.5 Silver 5.0 <1.0 2,4-D 10.0 <1.0 Tetrachloroethylene 0.7 <0.1 1,4-Dichlorobenzene 7.5 <0.05 Toxaphene 0.5 <0.1 1,2-Dichloroethane 0.5 <0.1 Trichloroethylene 0.5 <0.1 1,1-Dichloroethylene 0.7 <0.1 2,4,5-Trichlorophenol 400.0 <0.5 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.5 Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 <1.0 Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 <0.2 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., basis) for the following metal parameters: Laboratory: American Testing and Tech Inc and Date of analysis: 6/1/2022 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <5.0 Cadmium 85 39 <5.0 Copper 4,300 1,500 40 Lead 840 300 <5.0 Mercury 57 17 <0.2 Molybdenum 75 nia <5.0 Nickel 420 420 <5.0 Selenium 100 100 <5.0 Zinc 7,500 2,800 125 residuals do not on a dry weight b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 ir > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 0.88 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: American Testing and Tech Inc and Date of analysis: 6/1/2022 Parameter Result (mg/kg) Aluminum 151,10 Ammonia -Nitrogen 9,000 Calcium 10,200 Magnesium 2,800 Nitrate -Nitrite Nitrogen 10 pH (Standard Unit) 6.58 Phosphorus 2,400 Potassium 1,400 Sodium 9,400 Total Kjeldahl Nitrogen 19,000 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.99 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): • default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Water Treatment Process e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN (mg/kg) Five -Year Maximum Adjusted PAN (mg/kg) Surface 8,510 10,663 Injection/Incorporation 13,010 15,163 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: Noncl FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: • A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ▪ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): IN Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. El Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. El Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. • Alternative 5 [15A NCAC 02T.1106(b1(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, p heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, ❑ gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. El Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or lime stabilization. c. For Surface Disposal: 111 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. El Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: El Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). El Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). LJ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). LJ Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). LJ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. LJ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. LJ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. LJ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. LJ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. LJ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. 61 Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ▪ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 DELORME Westbrook REAV[S..N XMap® 8 t Tr"— 4—L 1 1 \/ Wedgewood,WesI Cent al Heights �� 111 I 1.,!I _\., fEa\tNG• DOWNI G't4,. 55' N. LL \ /. ` 1 SuhsettAcres TurrentIne•Estatesf 7 �� ASESUR GT 11 Alamanco:Acres� �;.I' z� juntry CibltbCountryClubFrest 9l 6'6- �-l< N/esterwood t \ R��FFS9' l�j o n r 1 slos,Sr / (� 1 m o pREO�'O°�� !J Sn ftiti`00vN k, % (ill 5Q / \O • v.O� n,6i St3f•-AC I.N Ho 3 A z s KENT.WOOD DR `Z,\ ki75Hell m'Place` 0 1i ^z N ,O.o, C� ;1 107�, Y ? ?' a'A.'nRton•Alarn JD Mackintosh Jr. WTPfP, io nl O/ P Sn 1.149. )s P•' ao f. 1 PONDRD ;Alamance `/COUNNC/U.I''' ; CABIN RD RO \PGND R 92 t OS': 77 II -c` �?s J�Gi I y�� 1PSe50. rr- �p��I, 0 10 sy�A 9 GredtibrIer Scale 1:50,000 mi 0 '/a '/z '/a 1 11/4 1% 1" = 4,166.7 ft Data Zoom 12-0 Data use subject to license. ® DeLorme. XMap® 8. www.delorme.com 7N NOIDNI1Ufl Residuals Sampling Plan JD Mackintosh Jr WTP Burlington Distribution Class A Residuals Nutrients and Metals Analysis • Sampling Point: Lagoon • Sampling Frequency: Dry ton dependent • Sample Type: Composite • Lab: American Testing Technologies Inc Pathogen Reduction (not required) Vector Attraction Reduction (not required) TCLP • Sampling Point: Lagoon • Sampling Frequency: Annually • Sample Type: Composite • Lab: American Testing Technologies Inc. JD MACKINTOSH JR WATER TREATMENT PLANT QUANTITATIVE JUSTIFICATION FOR RESIDUALS The following is a record of the last 3 years in which class A material was distributed from the above referenced plant: Year Dry Tons Removed 2021 319.89 2020 330.9 2019 273.52 As shown above the average amount of material being land applied from this plant is roughly 308.1 dry tons each year. It is requested that the currently permitted 1300 dry tons per year be kept in place to allow for future plant cleanouts and maintenance events. ORIGINAL- RETURN TO LABORATORY W (S131dWIIVS H m J z c� o U7 { • 0 O 3 173 z . O 0 0 O m 0 z m 0 ni 0 c a 0 m 0 (321f11yN9Is) :A8 03AIMO3a 0 P1 m P1 m P1 m 1 1 EMI 1111111111111111111 III NM IIMENIIMMIIIII VIIMINIIMII MINIM AIIIIIIIMIMIII 0 r; 10. Fn m z a 0 m a m z P1 m m 0 z 0 m m Ink iJ38WfN '0'd 'ON tOVWJNOO COMPOSITE (C) OR GRAB (G) INDICATE AQUEOUS (WATER) SOLID OR SEMISOLID AIR NONAQUEOUS LIQUID (OIL, SOLVENT, ...) IW8f1S SNRNIVIN0 0 1VNV Q3aIflb3a 'ON 10310dd Pz m C co m xm � a Cs m m zn o 0 m 0 u) u) 0 0 0 Co 0 m r m m -- 0 _am 0 v „,„& 0 0 Bu1lsal ueouauUV 0 0 0 0 CD N n 0 X. =�oCD roll• DC� !c tD N CD P. O eS N .� o 3 ra w-u 0 tu S 3 oco o. n co 00get 0 -. wm � N bg 0 0 3 2 _. o i W 0 ngwn j pins 0 0 0) 02/24/2022 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 American Testing Technologies, Inc. Report No.: 010622-22 26 Enclosed are the results of the sample(s) submitted to our laboratory on 01/06/2022.All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on an ``as -received" wet basis unles otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the labo4atory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy(eZamericantestinatechnologies.cosy€ SL- Test performed by an approved subcontract laboratory BRL- Below Reporting limit The results relate only to the items tested. ATT s1811 have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT 's liability with respect to the Test Results exceed the amount paid to ATT by the client therefore. 1350 Home Avenue Akron, Ohio 44310 Tall Free: 877.634.9906 Phone: 330.634.9906 Fax. 330.634.9907 www.ArnericanTestingTechnoiogies.com Page 1 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID if: 010622-22 Date of Analysis: 01/18/2022 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Lints Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenimn <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D Fil rt reviewed by: arat anager 1350 Home Avenue Akron, Ohio 44310 Tali Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingiechnologies.com Page 2 of 31 American Testing Technologies, Inc. City of Burlington, NC Atm: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 01/14/2022 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D ort reviewed by: Laaboora • >> Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericanTestingTechnologies.com Page 3 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.corn Page 4 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received:, 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 808IB Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxyehlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toff Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.corn Page 5 of 31 City of Burlington, NC Atin: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A reviewed by: Laborato 1 a anager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericaniestingTechnologies.com Page 6 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0817 Client ID #: # 1 Digester Land App Laboratory ID #: 010622-22 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 xng/kg 7.3.4.1 01/17/2022 pH (Lab) 12.75 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 eport reviewed by: Manager 1350 Florae Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologles.com Page 7 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 01/18/2022 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromi»m <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fox: 330.634.9907 www.AmericanTestingTechnologies.com Page 8 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 01/14/2022 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg /i 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 ntg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2:0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 9 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mglL 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C Fin ; ort reviewed by: r- Lab.�'sjt• j :, anger 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 10 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01106/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/11/2022 American Testing Technologies, Inc. Certificate of Analysis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Undone <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 11 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 2,4,5-TP (Silvex) <1.0 mg/L 10.0 8151A mg/L 1.0 8151A 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 12 of 31 City of Burlington NC Attn: Sharon Wagoner 1302 Belmont Street Burlington NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/03/2022 Time Collected: 0834 Client ID #: Rotary Press Laboratory ID #: 010622-23 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 6.81 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 1350 Home Avenue Akron, Ohio 44310 Tall Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 13 of 31 City of Burlington, NC Attn: Sharon. Wagoner 1302 Belmont Street' Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 01/18/2022 Metals-TCLP (EPA 1311) American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 14 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 01/14/2022 Volatiles-TCLP (EPA 1311) American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D Pik report reviewed by: 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corm Page 15 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 n g/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-CresoI <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4;6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Horne Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax; 330.634.9907 www.Am e ri ca nT est i n gTec h n o l ogi es. co m Page 16 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Receive& 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B Fin•r .art reviewed by: Labs ato 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877_634.9906 Phone: 330.634.9906 Fax; 330.634.9907 www.AmericanTestingTechnologies.com Page 17 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 18 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Cake Laboratory ID #: 010622-24 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 6.68 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 1350 Home Avenue Akron. Ohio 44310 ron Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 19 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory 1D #: 010622-25 Date of Analysis: 01/18/2022 Metals-TCLP (EPA 1311) American Testing Technologies, inc. Certificate of Analysis Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium <0.5 mg/L 1.0 6010D Chromium. <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D Fink - . • reviewed by: \Hager 1350 Home Avenue Akron, Ohio 44310 Toll Free; 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.ArnericanTestingTechnologies.cam Page 20 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 01/15/2022 American Testing Technologies, inc. • Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichioroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetrachloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 mg/L 0.5 8260D Vinyl chloride <0.2 mg/L 0.2 8260D Fin .a r- rt reviewed by: Labanager 1350 Home Avenue Akron, Oho 44310 Toil Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 21 of 31 American Testing Technologies, Inc. City of Burlington, NC Attu: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexxachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avenue Akron, Ohio 44310 Toil Free_ 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 22 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 nig/L 0.03 8081E Endrin <0.005 mg/L 0.02 8081E Heptachlor <0.005 mg/L 0.008 8081E Heptachlor epoxide <0.005 mg/L 0.008 8081B Linrlane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 23 of 31 American Testing Technologies, Inc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 Date of Analysis: 02/18/2022 Certificate of Analysis Herbicides-TCLP (EPA 1311) Parameter Results Unfits Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A rt reviewed by: Laboraanager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 24 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0815 Client ID #: SBWWTP Land App Laboratory ID #: 010622-25 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Sulfides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 7.37 s.u. 9045D 01/07/2022 Flash point >140 of 1010A 01/14/2022 Find r rt reviewed by: Laboxato .ger 1350 Home Avenue Akron, Ohio 44310 Toll Free_ 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 25 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 01/18/2022 American Testing Technologies, Inc. Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010D Barium <10 mg/L 100.0 6010D Cadmium_<0.5 mg/L 1.0 6010D Chromium <1.0 mg/L 5.0 6010D Lead <1.0 mg/L 5.0 6010D Mercury <0.02 rng/L 0.2 7470A Selenium <0.5 nng/L 1.0 6010D Silver <1.0 mg/L 5.0 6010D rt reviewed by: La:. rat. " Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 26 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 01/15/2022 American Testing Technologies, Inc. Certificate of Analvsis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260D Carbon tetrachloride <0.1 mg/L 0.5 8260D Chlorobenzene <0.1 mg/L 100 8260D Chloroform <0.1 mg/L 6.0 8260D 1,2-Dichloroethane <0.1 mg/L 0.5 8260D 1,1-Dichloroethene <0.1 mg/L 0.7 8260D Methyl ethyl ketone <2.0 mg/L 200 8260D Tetraehloroethene <0.1 mg/L 0.7 8260D Trichloroethene <0.1 ang/L 0.5 8260D Vinyl chloride <0.2 anglL 0.2 8260D port reviewed by Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fox: 330.634.9907 www.AmericanTestingTechnologies.com Page 27 of 31 American Testing Technologies, fnc. City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/07/2022 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene .<0.05 mg/L 7.5 8270C 2,4-D nitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mglL 0.13 8270C HexaehIorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 . 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol. <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C ort reviewed by: La clzatd \ anager 1350 Home Avenue Akron. Ohio 44310 Toll Free: 877.634.9906 Phone: 330,634.9906 Fax. 330.634.9907 www.AmericanTestingTechnoiogies.com Page 28 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/11/2022 Pesticides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081E Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081E Methoxychlor <0.1 mg/L 10.0 8081R Toxaphene <0.1 mg/L 0.5 8081B port reviewed by: Manager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.corn Page 29 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 Date of Analysis: 02/18/2022 Herbicides-TCLP (EPA 1311) Parameter American Testing Technologies, Inc. Certificate of Analysis Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A ort reviewed by: anager 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericaraTestingTechnologies.corn Page 30 of 31 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 01/06/2022 Date Reported: 02/24/2022 Date Collected: 01/04/2022 Time Collected: 0915 Client ID #: Mackintosh Lagoon # 2 Laboratory ID #: 010622-26 American Testing Technologes, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 01/17/2022 Reactive Snnl Ides <25 mg/kg 7.3.4.1 01/17/2022 pH (Lab) 8.22 s.u. 9045D 01/07/2022 Flash point >140 °F 1010A 01/14/2022 Fin. e. reviewed by: ger 1350 Home Avenue Akron, Ohio 44310 Tot! Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnologies.com Page 31 of 31 LABDRATO,RY U RECEIVED FOR LABA0HATO)r E ' TIME CIISTODYINT CUSTODY (SIGNATURE) I ,SO "YES' . SEAL NO.. -; FECEIVED BY: (SIGNATURE) �d Q m SAMPL) CLIENT ADDMSS (� cI T �X 1 CLIENT NAME Ci°kj everE Mrr '1 CLIENT(SITE) �J - PROJECT MANAdER l�o�n V.i ( Ci ,W/ o m s 2rn m m o m g ATIr ANALYSIS REQUEST AND CHAIN OF CUSTODY. RECORD American Testing Technologies. Inc. a 71 L C SAMPLE IDENTIFICATION m m m m CLIENT EMAIL t' Oli. JtAJGrronte.,r 3"A'�rMat-Ir'�nT1(, CLIENT PHONE P.O. NUMBER PROJECT NO. FM mFMm RECEIVED BY: (SIGNATURE) RELINQUISHED BY:'(sIGNATURE) CLIENT FAX CONTRACT ND. PROJECTLO TION (STATE) j[,. �.. .r,3 COMPOSITE{C) OR GRAB (G) INDICATE 3. m x AQUEOUS (WATER) SOLID OR SEMISOLID AIR American Testing Technologies, Inc. 1350 Home Avenue Akron, OH 44310 Website: www.AmericanTestingrechnoiogies.com Toll Free: 877-634-9906 Phone: (330) 639-9906 Fax: (330) 634-990 7 NONAQUEOUS LIQUID (OIL, SOLVENT, ...) Gil SE.ONLY 1 Co` N MBER OF CONTAINERS SUBMITTED REQUIRED ANALYSIS rn m (`� US, FL rst {{�.. RECEIVED BY (SIGNATURE) RELINQUISHED BY: {SIGNATURE) ('�I� \A 1/45r� d m A Si S NUMBER OF COOLERS SUBMITTED i PER SHIPMENT: !J STANDARD REPORT DELIVERY DATE DUE EXPEDITED REPORT DELIVERY O (SURCHARGE) DATE DUE Q rri G 1 3 4 -n M m M m 06/01/2022 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Report No.: 042822-35 36 American Testing Technologies, Inc. Enclosed are the results of the sample(s) submitted to our laboratory on 04/28/2022. All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on a dry weight basis unless otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the laboratory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy{clamericantestinQtechnologies. com SL- Test performed by an approved subcontract laboratory BRL- Below Reporting linut The results relate only to the items tested. ATT shall have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT 's liability with respect to the Test Results exceed the amount paid to ATT by the client therefore. 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone: 330.634.9906 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 1 of 3 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 04/28/2022 Date Reported: 06/01/2022 Date Collected: 04/26/2022 Time Collected: 1215 Client ID #: Lagoon #2 Laboratory ID #: 042822-35 American Testing Technologies, Inc. Certificate of Analysis Parameter Result (%) Result (mg/kg) Analysis Date Method . Aluminum, Total 151,100 04/29/2022 6010D Arsenic, Total <5.0 04/29/2022 6010D Cadmium, Total <5.0 04/29/2022 6010D Calcium, Total 1.0 10,200 04/29/2022 6010D Chromium, Total 170 04/29/2022 6010D Copper, Total 40 04/29/2022 6010D Iron, Total 21,000 04/29/2022 6010D Lead, Total <5.0 04/29/2022 6010D Magnesium, Total 0.28 2,800 04/29/2022 6010D Manganese, Total 2,600 04/29/2022 6010D Mercury, Total <0.20 04/29/2022 7471B Molybdenum, Total <5.0 04/29/2022 6010D Phosphorus, Total 0.24 2,400 04/29/2022 6010D Nickel, Total <5.0 04/29/2022 6010D Potassium, Total 0.14 1,400 04/29/2022 6010D Selenium, Total <5.0 04/29/2022 6010D Sodium, Total 0.94 9,400 04/29/2022 6010D Sulfur, Total 1.3 13,000 04/29/2022 6010D Zinc, Total 125 04/29/2022 6010D Total Kjeldahl Nitrogen 1.90 19,000 05/13/2022 SM-4500 Ammonia Nitrogen 0.90 9,000 05/13/2022 SM-4500 Organic Nitrogen 1.00 10,000 05/13/2022 Calculation Nitrate+Nitrite- N 10 05/13/2022 SM-4500C Calcium Carbonate Equivalent 35 350,000 05/20/2022 AOAC 955.01 Total Solids 0.88 8,800 04/30/2022 SM-2540G Total Volatile Solids 20 200,000 04/30/2022 SM-2540G Moisture 99.12 04/30/2022 SM-2540G 1350 Home Avenue Akron, Ohio 44310 Toll Free: 877.634.9906 Phone; 330.634.9906 Fax 330.634.9907 www.AmericanTestingTechnoiogies.com . Page 2 of 3 City of Burlington, NC Attn: Sharon Wagoner 1302 Belmont Street Burlington, NC 27215 Date Received: 04/28/2022 Date Reported: 06/01/2022 Date Collected: 04/26/2022 Time Collected: 0820 Client ID #: SB Digester 1 'Laboratory ID #: 042822-36 American Testing Technologies, Inc. Certificate of Analysis Parameter Result (%) Result (mgg) Analysis Date Method Alnminum, Total 3,500 04/29/2022 6010D Arsenic, Total <5.0 04/29/2022 6010D Cadmium, Total <5.0 04/29/2022 6010D Calcium, Total 1.2 12,200 04/29/2022 6010D Chromium, Total 40 04/29/2022 6010D Copper, Total 270 04/29/2022 6010D Iron, Total 8,000 04/29/2022 6010D Lead, Total <5.0 04/29/2022 6010D Magnesium, Total 0.86 8,600 04/29/2022 6010D Manganese, Total 600 04/29/2022 6010D Mercury, Total <0.20 04/29/2022 7471B Molybdenum, Total <5.0 04/29/2022 6010D Phosphorus, Total 4.0 40,000 04/29/2022 6010D Nickel, Total <5.0 04/29/2022 6010D Potassium, Total 1.3 13,000 04/29/2022 6010D Selenium, Total <5.0 04/29/2022 6010D Sodium, Total 0.2 2,000 04/29/2022 6010D Sulfur, Total 0.9 9,000 04/29/2022 _ 6010D Zinc, Total 400 04/29/2022 6010D Total Kjeldahl Nitrogen 4.50 45,000 05/13/2022 SM-4500 Ammonia Nitrogen 3.30 33,000 05/13/2022 SM-4500 Organic Nitrogen 1.20 12,000 05/13/2022 Calculation Nitrate+Nitrite- N 15 05/13/2022 , SM-4500C Calcium Carbonate Equivalent 30 300,000 05/20/2022 AOAC 955.01 Total Solids 3.27 32,700 04/30/2022 SM-2540G Total Volatile Solids 55 550,000 04/30/2022 SM-2540G Moisture 96.73 04/30/2022 SM-2540G 1350 Home Avenue Akron, Ohio 44310 Tot! Free: 877.634.9906 Phone: 330.634.9905 Fax: 330.634.9907 www.AmericanTestingTechnoiogies.com Page 3 of 3