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NC0090123_Application_20220616
veO.STATE a 40, ROY COOPER . Governor - 1 4241 ELIZABETH S.BISER Secretary RICHARD E.ROGERS,JR. NORTH CAROLINA Director Environmental Quality June 16, 2022 Morehead Tryon Land LP Attn: Jason Anderson, VP 150 N Riverside Plz Ste 1800 Chicago, IL 60606 Subject: Permit Application Application No. NC0090123 Queensbridge Collection Mecklenburg County Dear Applicant: The Water Quality Permitting Section acknowledges receipt of your application for a new NPDES WW permit, including supporting documentation and your check number 2946 in the amount of$860.00 as payment of the application fee. These items were received in our offices on June 15, 2022. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. The permit writer will contact you if additional information is required to complete evaluation of your application. Your timely and direct response to any such request will help to expedite the review process. Please note that acceptance of the application does not guarantee a NPDES permit will be issued for the proposed activity. A permit will only be issued following a complete review of the application, concluding the proposed discharge is allowable per applicable statutes and rules. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. Sincerely, Jrtiht._tQ Wren Thedford Administrative Assistant Water Quality Permitting Section cc: M. Neal McElveen-Terracon ec: WQPS Laserfiche File w/application DE North CarolinaRegio DepartmentnalOfce of 610 EnvironmentalEastCenter QA vuenualitye,I Suite Division301 ofMooresville.Water ResouNorces firth Carolina 28115 �"�� 704.663.1699 lierracon June 9, 2022 North Carolina Department of Environmental Quality Division of Water Resources Water Quality Permitting Section — NPDES Archdale Building — 9th Floor 512 North Salisbury Street Raleigh, North Carolina 27604 Attn: Mr. Wren Thetford P: 919-707-3606 Re: Commercial Groundwater Discharge Permit Application Proposed Queensbridge Collective Development 1111 South Tryon Street Charlotte, North Carolina 28202 Terracon Project No. 71227087 Dear Mr. Thetford: On behalf of Morehead Tryon Land LP, Terracon Consultants, Inc. (Terracon) has completed the enclosed NPDES Permit Application and supporting documentation for the above- referenced property. Preparation of this NPDES Individual permit application is associated with proposed dewatering that will be necessary during and after the construction of three high-rise, mixed use towers at the site, which will include a 2- or 3-story below grade parking structure that intersect will intersect the water table. Limited groundwater impacts have been identified at the site, apparently the result of petroleum release(s) from former underground storage tanks located adjacent to the existing Uptown Cabaret building in the northern portion of the site. Morehead Tryon Land LP proposes to pre-treat the groundwater that is dewatered from the sub-grade parking structure and then discharge the effluent to the Charlotte-Mecklenburg County municipal stormwater sewer, with ultimate discharge occurring to Little Sugar Creek, under a new individual NPDES permit. As noted on EPA Forms 3510-2D and 3510-2E, Morehead Tryon Land LP is requesting a waiver for the following effluent characteristics: biochemical oxygen demand, chemical oxygen demand, total organic carbon, ammonia, and oil and grease. These parameters, and the remaining listed in Table A of Form 3510-2D and Section 4.2 of Form 3510-2E (total suspended solids, discharge flow, pH, and temperature), have not been collected. As the discharge in question will be composed solely of groundwater, it is not anticipated that the effluent will contain constituents that would have an impact on biochemical oxygen demand, chemical oxygen demand, total organic carbon, ammonia, or oil and grease. As such, we respectfully request that these parameters be waived from effluent monitoring requirements. Terracon Consultants, Inc. 2701 Westport Road Charlotte. North Carolina 28208 P [704] 509 1777 F [704] 509 1888 terracon.com Geotechnical • Environmental • Construction Materials • Facilities NPDES Permit Application lierracon Queensbridge Collective Charlotte, North Carolina June 9, 2022 Terracon Project No. 71227087 The permit application has been provided to Charlotte-Mecklenburg Stormwater Services (CMSS) for their review. CMSS has indicated that it is willing to accept discharge from the proposed treatment system. A copy of CMSS correspondence is included in Appendix E. Should you have any questions please contact us at your earliest convenience at (704) 594 -8912 or via email at neal.mcelveen(c�terracon.com. Sincerely, Terracon Consultants, Inc. ---71010 William O. Frazier, PG M. Neal McElveen, PE Project Geologist Principal/Environmental Manager Attachments: Exhibits: Exhibit 1: Topographic Map Exhibit 2: Flow Line Diagram Exhibit 3: Groundwater Sample Locations Tables: Table 1: Summary of Groundwater Analytical Results Appendix A: EPA Form 3510-1: General Information EPA Form 3510-2D: New Manufacturing, Commercial, Mining, and Silviculture Operations That Have Not Yet Commenced Discharge of Process Wastewater EPA Form 3510-2E: Manufacturing, Commercial, Mining, and Silviculture Operations Which Discharge Only Non-Process Wastewater Appendix B: Engineering Alternatives Analysis Appendix C: Laboratory Analytical Reports Appendix D: Treatment System Specifications Appendix E: Charlotte-Mecklenburg Correspondence Responsive • Resourceful ■ Reliable 2 („, - — 44144..'.' i , ,NIN. \''' '' '' '' ,--,-"ifilt1 i wail ly. .s-Yrj.,/, -'.•/. 1; irt,\ -:: . . •, ,,, ,,. ,•,:: ....,. 7, 4 iN0Alle,:e-1.'-t__';. ,,,..".;.:k:;:s-:.;-. .-',:,;;••;-,ri-l' 411101,,, ,,.•...7;•:•ty",' ,,i411r-i, ,,. p. . _.‘ 'if C'•., ;'/,, - ,-.,•.:' , .; It aik . 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V \ 1., 0'31'01 -A , ,,,, .4. ,, , ,. - . -, , - .4,-,r,.. ,.....,. .•v., i •*; • 0. , � o \ }, I •` � \\ ... ,, • .. /7., \ .'! 4 , .. . , ,, 4.„ : _ , ,„„, ., ., , _ : '01"/:. /, / /do, -V : . - '' ",-;"•-% ,,,4 ,-//' i't./ N' k V /e� G ! Outfall#1 . •wJ�. s ✓ / :\ y Existing Stormwater Curb Inlet /r t\ c '3..--. w v 35°l3'l1"180°5I'04" s /�rile / .Effluent Flow ( C_ Influent Flow �•. ' /' 4 ° ' I •. / (via flexible pipe) y / irk 49pl. (via flexible pipe) •y . sty , a r "`` / ` A4 •ice / / .. ..�:. ` . V. E t Ir 4 w, ,� p y/ ,. ` t /a. . • 'itt, .J'a / ' ry:•''7 1$ J *1/4 • '.',..*' .;,„,,-,,..- ,----,,,,,. ,„ ;if .4_ - . • ♦ • r:I �1 l, +4 l 1 Site Boundary Ilk . NI ' �\ `a y { O Proposed Location of �f/ • -. • Groundwater Treatment System / \, .. t N ✓ d '��' r i, .,'' ••• Dewatering Flow Direction 3 ♦ a +. �;°�• ;�\ � 0 Example Caisson or Excavation r,% \ , - i" raw Dewatering Location k. • • �4� :' a'ti+. '."`'' s�, sdrAi '.' ..ems c Project Manager: Project No. Flow Line Diagram Exhibit wOF 71227087 +� g Drawn by: Scale: erracu RSB As shown Queensbridge Collective Checked by: MNM File Na 71227087 2 2701 Westport Road 111 East Morehead Street 2 Approved by: MNM Date: May2022 Charlotte,NC Charlotte, North Carolina VAN v% .0 I. ,..; . fkr A, „ , o 4,, ` . '4or 2. "otA • ."` ter k + •, i. • , 1 F r -, .4.\,, 40,0, „or _ ip: ,.1, ii,.• , , ' B-108 11111'. ' Irkri r It\ • 7 q1.7 , it itA,..44),. mr, 5e.e. t ,.. . ' ipt ,r, / , j V. ,,fit B 1 C14 B-107 _—- >, r dir t- • �� • 1 ac •o'- • r , • g • O.J 1033 Sou r , •,_ ,' It 4. _ . ,' B-109 so B-113 PS\ # B-103 r , 7' . ,,,,,,,,,I'i.,N s t i 4.4(1,Ni.4: ,,,,.... 1111\ Nkait, It ' <,. - • 4-1, � . ri I' Y , r ..'4 F t: -; .-- ' 4,. t % A.<6,,,,A l • B-102re t B-112. 7 lb ::; ;k:1. 1r ! _ _ •.,1.1 ‘ B-111 • * p 4 Soil Boring r. N �, ,. Cd l '" 4 0\ �. Soil Boring / r- • •n �-. •'�. j �,. # Monitoring Well G i_' , ' Rdill t Station -so re Jw(� h i _},'° L'itr pis' R_PC: Imaa-naComTom itr filkt Project Manager. Project No. SAMPLE LOCATION MAP Exhibit WOF As shown lierracon Drawn by: Scale: WOF As shown Queensbridge Collective Checked by: FIN Name: 2701 Westport Road MNM 71227087.3 111 East Morehead Street —Approved Date: April2022 Charlotte,NC Charlotte, North Carolina TABLES Table 1 Summary of Groundwater Analytical Results Queensbridge Collective i 111 East Morehead Street Charlotte,Mecklenburg County,North Carolina Terracon Project No.71227087 Residential Residential Sample ID 8-105 B-106 8-108 B-110 B-112 2L Standard GCL VI-GWSL VI-GWSL Volatile Organic Compounds(VOCs)by EPA Method 8260 Acetone <5.1 <5.1 64.9 <5.1 <5.1 6,000 6,000,000 NE NE Benzene <0.34 <0.34 1.6• <0.34 <0.34 1 5,000 1.6 6.9 Bromodichloromethane <0.31 <0.31 <0.31 0.321 <0.31 0.6 NE 0.88 3 2-Butanone(Methyl Ethyl Ketone) <4.0 <4.0 15.6 <4.0 <4.0 4,000 4,000,000 450,000 1,900,000 Chloroform <0.43 1.2 6.1 1.7 0.581 70 70,000 0.81 3.6 Chloromethane <0.54 <0.54 0.731 <0.54 <0.54 3 3,000 52 220 1,2-Dichloroethane <0.32 <0.32 0.421 <0.32 <0.32 0.4 400 2.2 9.8 Ethylbenzene <0.30 <0.30 89 <0.30 <0.30 600 84,500 3.5 15 2-11exanone <0.48 <0.48 2.01 <0.48 <0.48 40 40,000 1,600 6,900 Methyl Isobutyl Ketone <2.7 <2.7 7.0 <2.7 <2.7 100 100,000 110,000 470,000 Naphthalene <0.64 <0.64 28.3" <0.64 <0.64 6 6,000 4.6 20 Toluene <0.48 <0.48 6.1 <0.48 <0.48 600 260,000 3,800 16,000 Kylene(Total) <0.34 <0.34 103 <0.34 <0.34 500 85,500 77 320 Iron by EPA Method 6020 Iron(Total) I 93.6 I 1,t90 I 12,900 I 550 I 67.7 I 300 I NE I NE I NE Notes: All samples collected March 15,2022. Table shows compounds detected above laboratory method detection limits in one or more sample Concentrations given in ug/L. Concentrations exceeding a regulatory standard are shaded in the color correspondening to that regulatory standard. 2L Standard:154 North Carolina Administrative Code(NCAC(021.0202 Groundwater Standards(April 1,2022). GCL:15A NCAC 021.0406 Gross Contaminant Level VIGWSL:Vapor Intrusion Groundwater Screening Level(January 2022). •Concentration also exceeds the Residential VI-GWSL. "Concentration also exceed the Non-Residential VIGWSL. APPENDIX A EPA FORMS EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 Form U.S.Environmental Protection Agency \.EPA Application for NPDES Permit to Discharge Wastewater NPDES GENERAL INFORMATION SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1)) 1.1 Applicants Not Required to Submit Form 1 Is the facility a new or existing publicly owned Is the facility a new or existing treatment works 1.1.1 12 treatment works? 1. . treating domestic sewage? If yes,STOP.Do NOT complete E No If yes,STOP.Do NOT 12 No Form 1.Complete Form 2A. complete Form 1.Complete Form 2S. 1.2 Applicants Required to Submit Form 1 1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing, operation or a concentrated aquatic animal commercial,mining,or silvicultural facility that is a production facility? currently discharging process wastewater? o ❑ Yes 4 Complete Form 1 0 No ❑ Yes 4 Complete Form E No d and Form 2B. 1 and Form 2C. R 1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing, mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that commenced to discharge? discharges only nonprocess wastewater? Yes 4 Complete Form 1 ❑ No E Yes 4 Complete Form ❑ No ce and Form 2D. 1 and Form 2E. 1.2.5 Is the facility a new or existing facility whose discharge is composed entirely of stormwater associated with industrial activity or whose discharge is composed of both stormwater and non-stormwater? ❑ Yes 4 Complete Form 1 ❑� No and Form 2F unless exempted by 40 CFR 122.26(b)(14)(x)or b 15 . SECTION 2.NAIVE.MAILING ADDRESS,AND LOCATION(40 CFR 122.21(f)(2)) 2.1 Facility Name Queensbridge Collective 0 2.2 EPA Identification Number 47. O New Facility J • 2.3 Facility Contact Name(first and last) Title Phone number 11.2 v James Anderson Vice President (312)788-1816 v Email address janderson@riversideid.com • 2.4 Facility Mailing Address Street or P.O.box 150 North Riverside Plaza,Suite 1800 City or town State ZIP code Chicago Illinois 60606 EPA Form 3510-1(revised 3-19) Page 1 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 v 2.5 Facility Location Street,route number,or other specific identifier Q o 1111 South Tryon Street (.) c o County name County code(if known) iMecklenburg City or town State ZIP code z Charlotte North Carolina 28202 SECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3)) 3.1 SIC Code(s) Description(optional) 1522 N d 0 O V Cl) U 3.2 NAICS Code(s) Description(optional) -a fO 237990 U Cl) 531190 SECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4)) 4.1 Name of Operator Morehead Tryon Land LP 4.2 Is the name you listed in Item 4.1 also the owner? D Yes ❑ No 4.3 Operator Status ❑ Public—federal ❑ Public—state CI Other public(specify) ❑✓ Private ❑ Other(specify) 4.4 Phone Number of Operator (312)788-1816 4.5 Operator Address Street or P.O.Box E 150 North Riverside Plaza,Suite 1800 o = City or town State ZIP code o 0 Chicago Illinois 60606 co fl Email address of operator janderson@riversideid.com SECTION 5.INDIAN LAND(40 CFR 122.21(f)(5)) 0 5.1 Is the facility located on Indian Land? c ❑ Yes O No EPA Form 3510-1(revised 3-19) Page 2 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 SECTION 6. EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6)) 6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each) C ❑ NPDES(discharges to surface ❑ RCRA(hazardous wastes) ❑ UIC(underground injection of 0 y water) fluids) w ri ❑ PSD(air emissions) ❑ Nonattainment program(CM) ❑ NESHAPs(CM) •x ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) 0 Other(specify) SECTION 7.MAP(40 CFR 122.21(f)(7)) 7.1 Have you attached a topographic map containing all required information to this application?(See instructions for 0.R specific requirements.) 2 0 Yes ❑ No 0 CAFO—Not Applicable(See requirements in Form 2B.) SECTION 8. NATURE OF BUSINESS(40 CFR 122.21(f)(8)) 8.1 Describe the nature of your business. Morehead Tryon Land LP plans to redevelop the facility property(currently developed with a gentleman's club building,a restaurant,and the associated paved parking areas)with a three mixed-use high-rise towers.The towers will be underlain by a 2-to 3-story tall sub-grade parking feature that will intersect the groundwater table. Groundwater at site has been impacted by petroleum contamination associated with an apparent release(s)from m former underground storage tank systems located adjacent to the gentleman's club building in the northern portion O of the site. As dewatering will be necessary during construction and permanently to prevent infiltration from flooding the sub-grade parking feature,Morehead Tryon Land LP would like authorization to pre-treat dewatered groundwater and discharge it to the stormwater sewer. SECTION 9.COOLING WATER INTAKE STRUCTURES(40 CFR 122.21(f)(9)) 9.1 Does your facility use cooling water? d ❑ Yes El No 4 SKIP to Item 10.1. 9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at a,w 40 CFR 125,Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your NPDES permitting authority to determine what specific information needs to be submitted and when.) Y 0 Not applicable;while the high rise towers may utilize HVAC systems that utilize chilled water,the proposed discharge will consist solely of groundwater. SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10)) 10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that y apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and when.) ❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section ca Section 301(n)) 302(b)(2)) ea ❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a)) Section 301(c)and(g)) El Not applicable EPA Form 3510-1(revised 3-19) Page 3 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d)) 11.1 In Column 1 below, mark the sections of Form 1 that you have completed and are submitting with your application. For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note that not all applicants are required to provide attachments. Column 1 Column 2 ❑✓ Section 1:Activities Requiring an NPDES Permit ❑ w/attachments ❑✓ Section 2:Name, Mailing Address,and Location ❑ w/attachments Ei Section 3:SIC Codes ❑ w/attachments ❑✓ Section 4:Operator Information ❑ w/attachments ❑ Section 5: Indian Land ❑ w/attachments ❑ Section 6: Existing Environmental Permits ❑ w/attachments w/topographic ❑ map ❑ ❑✓ Section 7:Map w/additional attachments co o 0Section 8: Nature of Business ❑ w/attachments ❑ Section 9: Cooling Water Intake Structures ❑ w/attachments ❑ Section 10:Variance Requests ❑ w/attachments ❑✓ Section 11: Checklist and Certification Statement ❑ w/attachments 11.2 Certification Statement t I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name(print or type first and last name) Official title r _- 1 l J cncc o 4 v�� '- 6 rack. J Signature Date signed 6 /I EPA Form 3510-1 (revised 3-19) Page 4 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 U.S.Environmental Protection Agency Form Application for NPDES Permit to Discharge Wastewater 2D NPDES EPA NEW MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURAL OPERATIONS THAT HAVE NOT YET COMMENCED DISCHARGE OF PROCESS WASTEWATER SECTION 1. EXPECTED OUTFALL LOCATION(40 CFR 122.21(k)(1)) 1.1 Provide information on each of the facility's outfalls in the table below. o Outfall Receiving Water Latitude Longitude Number Name U J 1 Little Sugar Creek 35° 13' 2.4” N 80° 50' 42.3" W To 0 SECTION 2. EXPECTED DISCHARGE DATE(40 CFR 122.21(k)(2)) d ° 2.1 Month Day Year d• t • d W o CI 11 1 2022 SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(k)(3)(i)) 3.1 For each outfall identified under Item 1.1,provide average flow and treatment information.Add additional sheets as necessary. **Outfall Number** 1 Operations Contributing to Flow Operation Average Flow Dewatering of sub-grade parking structure and foundation installation 0.0042 mgd mgd mgd R mgd I mgd U) o Treatment Units T. Description (include size,flow rate through each treatment unit, Code from Final Disposal of Solid or Liquid a retention time,etc.) Exhibit 2D-1 Wastes Other Than by Discharge 8K lbs carbon mesh,0.0042 mgd,>7.5-min.retention 2-A Carbon to be disposed off-site EPA Form 3510-2D(Revised 3-19) Page 1 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 3.1 **Outfall Number** Cont. Operations Contributing to Flow Operation Average Flow mgd mgd mgd mgd mgd Treatment Units Description Code from Final Disposal of Solid or Liquid (include size,flow rate through each treatment unit, Exhibit 2D-1 Wastes Other Than by Discharge retention time,etc.) 0 V m E y **Outfall Number** o Operations Contributing to Flow . Operation Average Flow a) d mgd mgd mgd mgd mgd Treatment Units Description Code from Final Disposal of Solid or Liquid (include size,flow rate through each treatment unit, Exhibit 2D-1 Wastes Other Than by Discharge retention time,etc.) EPA Form 3510-2D(Revised 3-19) Page 2 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 SECTION 4. LINE DRAWING(40 CFR 122.21(k)(3)(ii)) 0 4.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water c -3 balance?(See instructions for drawing requirements.See Exhibit 2D-2 at end of instructions for example.) J ` c tEl Yes 0 No SECTION 5.INTERMITTENT OR SEASONAL FLOWS(40 CFR 122.21(k)(3)(iii)) 5.1 Except for stormwater runoff,leaks,or spills,are any expected discharges described in Sections 1 and 3 intermittent or seasonal? ❑ Yes El No 4 SKIP to Section 6. 5.2 Provide information on intermittent or seasonal flows for each applicable outfall.Attach additional pages,if necessary. Outfall Operations Fre uency Rate and Volume Number (list) Average Average Maximum Daily , Maximum Total Duration Days/Week Months/Year Discharge Volume 1 days/week months/year mgd gallons days N c days/week months/year mgd gallons days c days/week months/year mgd gallons days o o FrequencyRate and Volume rn Outfall Operations Average Average Maximum Daily Maximum Total Duration `o Number (list) Days/Week Months/Year Discharge Volume c Edays/week months/year mgd gallons days 1 c days/week months/year mgd gallons days days/week months/year mgd gallons days Outfall Operations Frequency Rate and Volume Number (list) Average Average Maximum Daily Maximum Total Duration Days/Week Months/Year Discharge Volume days/week months/year mgd gallons days mgd gallons days days/week months/year Y9 Y days/week months/year mgd gallons days SECTION 6.PRODUCTION(40 CFR 122.21(k)(4)) 6.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under CWA Section 304 apply to your facility? ❑ Yes ❑✓ No 4 SKIP to Section 7. c 6.2 Provide the following information on applicable ELGs. ELG Category ELG Subcategory Regulatory Citation 0 a EPA Form 3510-2D(Revised 3-19) Page 3 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 6.3 Are the limitations in the applicable ELGs expressed in terms of production(or other measure of operation)? ❑ Yes ❑ No 4 SKIP to Section 7. 6.4 Provide an expected measure of average daily production expressed in terms and units of applicable ELGs. Expected Actual Average Daily Production for First Three Years Outfall Year Operation,Product,or Material Quantity per Day Unit of Measure Number (note basis if applicable) Year 1 Year 2 Year 3 0 c) 0 Year 1 -o 0 a Year 2 Year 3 Year 1 Year 2 Year 3 SECTION 7.EFRUENT CHARACTERISTICS(40 CFR 122.21(k)(5)) See the instructions to determine the parameters and pollutants you are required to monitor and,in turn,the tables you must complete.Note that not all applicants need to complete each table. Table A.Conventional and Non-Conventional Parameters 7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A parameters for any of your outfalls? CI Yes ❑ No 4 SKIP to Item 7.3. 7.2 If yes,indicate the applicable outfalls below.Attach waiver request and other required information to the application. Outfall number 1 Outfall number Outfall number =., 7.3 Have you have provided estimates or actual data for all Table A parameters for each of your outfalls for which a waiver has not been requested and attached the results to this application package? No;a waiver has been requested from my ❑ Yes ❑✓ NPDES permitting authority for all parameters at • all outfalls. 3 Table B.Certain Conventional and Non-Conventional Pollutants w 7.4 Have you checked'Believed Present"for all pollutants listed in Table B that are limited directly or indirectly by an applicable ELG? ❑ Yes ❑✓ No 7.5 Have you checked"Believed Present"or"Believed Absent"for all remaining pollutants listed in Table B? ❑✓ Yes ❑ No 7.6 Have you provided estimated data for those Table B pollutants for which you have indicated are"Believed Present" in your discharge? ❑✓ Yes ❑ No EPA Form 3510-2D(Revised 3-19) Page 4 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 Table C.Toxic Metals,Total Cyanide,and Total Phenols 7.7 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C for all outfalls? ❑✓ Yes El No 7.8 Have you completed Table C by providing estimated data for pollutants you indicated are"Believed Present," including the source of the information,for each applicable outfall? ❑✓ Yes El No Table D.Organic Toxic Pollutants(GC/MS Fractions) 7.9 Do you qualify for a small business exemption under the criteria specified in the Instructions? ❑ Yes 4 Note that you qualify at the top of El No Table D,then SKIP to Item 7.12. a 7.10 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table D for all outfalls? 42.o ❑✓ Yes CI No 4-) 7.11 Have you completed Table D by providing estimated data for pollutants you indicated are"Believed Present," including the source of the information,for each applicable outfall? '.= ❑✓ Yes ❑ No 2,3,7,8-Tetrachlorodibenzo-p-Dioxin(TCDD) 7.12 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the Instructions,or do you know or have reason to believe that TCDD is or may be present in effluent from any of your outfalls? ❑ Yes El No Table E.Certain Hazardous Substances and Asbestos 7.13 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed in Table E for all outfalls? ElYes 0 No 7.14 Have you completed Table E by reporting the reason the pollutants are expected to be present and available quantitative data for pollutants you indicated are"Believed Present"for each applicable outfall? El Yes El No Intake Credits,Tables A through E 7.15 Are you applying for net credits for the presence of any of the pollutants on Tables A through E for any of your outfalls? Yes 4 Consult with your NPDES permitting No authorit . SECTION 8.ENGINEERING REPORT(40 CFR 122.21(k)(6)) 8.1 Do you have any technical evaluations of your wastewater treatment,including engineering reports or pilot plant studies? o CIYes ❑✓ No 4 SKIP to Item 8.3. c 8.2 Have you provided the technical evaluation and all related documents to this application package? ❑ Yes ❑ No cp 8.3 Are you aware of any existing plant(s)that resemble production processes,wastewater constituents,or wastewater treatment at your facility? • Yes ❑ No 4 SKIP to Section 9. EPA Form 3510-2D(Revised 3-19) Page 5 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 8.4 Provide the name and location of the similar plants. 0 Name of Similar Plants Location of Similar Plants d Pending-NPDES application NC0090085-MOD CLT Ve c U d o a) w SECTION 9.OTHER INFORMATION(40 CFR 122.21(k)(7)) 9.1 Have you attached any optional information that you would like considered as part of the application review process (i.e.,material beyond that which you have already noted in the application as being attached)? 2 Yes ❑ No 4 SKIP to Section 10. 0 9.2 List the additional items and briefly note why you have included them. 1.A brief description of estimated effluent concentration calculation methodology is attached following Table C. E 0 2. a7) 0 3. 4. 5. SECTION 10.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d)) 10.1 In Column 1 below,mark the sections of Form 2D that you have completed and are submitting with your application. For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note that not all applicants are required to complete all sections or tables,or provide attachments. Column 1 Column 2 Section 1:Expected Outfall ❑ w/attachments(e.g.,responses for additional outfalls) Location ❑✓ Section 2:Expected ❑ w/attachments Discharge Date ❑✓ Section 3:Average Flows ❑ w/attachments and Treatment ElSection 4:Line Drawing 0 w/line drawing ❑ w/additional attachments Section 5:Intermittent or ❑✓ Seasonal Flows ❑ w/attachments .111 w ❑✓ Section 6:Production ❑ w/attachments ci w/Table A waiver ❑ request or ❑✓ Table A ,1 approval Section 7:Effluent CI Table B El Table C CD ❑✓ Characteristics El Table Table D Table E ❑ w/other attachments Section 8:Engineering ❑ w/technical evaluations and related attachments Report r❑ Section 9:Other Information El w/optional information Q Section 10:Checklist and ❑ w/attachments Certification Statement EPA Form 3510-2D(Revised 3-19) Page 6 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective New No.2040-0004 10.2 Certification Statement d I certify under penalty of law that this document and all attachments were prepared under my direction or supervision y in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons .4.7. ICSdirectly responsible for gathering the information, the information submitted is, to the best of my knowledge and VS CU belief,true, accurate,and complete. I am aware that there are significant penalties for submitting false information, -� including the possibility of fine and imprisonment for knowing violations. o c� Name(print or type first and last name) Official title ca Avril....1 S,,ccv ,-,,, m.— A Signature Date signed e4—'s —rrTh—e- A LA-f{"=•-;--zooS,1• ocriri co 6/4/da EPA Form 3510-2D(Revised 3-19) Page 7 a This page intentionally left blank. EPA IdeNifcation Number ' Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE A.CONVENTIONAL AND NON CONVENTIONAL PARAMETER ESTIMATES(40 CFR 122.21(k)(5)(i))1 Effluent Data Intake Water Waiver Units Maximum Daily Average Daily Believed Present? Pollutant Requested Source of Information (if applicable) Discharge Discharge (use codes in instructions) only one response per (required) (if available) parameter) ❑ Check here if you have applied to your NPDES authority for a waiver for all of the pollutants listed on this table for the noted outfall. 1 Biochemical oxygen 0 Concentration No data Groundwater data does not include ❑ Yes ❑ No demand(BOD5) Mass No data Groundwater data does not include 2 Chemical oxygen demand ❑ Concentration No data Groundwater data does not include 0 Yes ❑ No (COD) Mass No data Groundwater data does not include 3 Total organic carbon 0 Concentration No data Groundwater data does not include 0 Yes ❑ No (TOC) Mass No data Groundwater data does not include 4 Total suspended solids 0 Concentration No data Groundwater data does not include ❑ Yes ElNo (TSS) Mass No data Groundwater data does not include Concentration No data Groundwater data does not include 5. Ammonia(as N) 0 0 Yes r❑ No Mass No data Groundwater data does not include 6. Flow ❑ Rate No data Groundwater data does not include ElYes ❑ No Temperature(winter) ❑ °C °C No data Groundwater data does not include 7. r❑ Yes El No Temperature(summer) ❑ °C °C No data Groundwater data does not include pH(minimum) ❑ Standard units S.U. No data Groundwater data does not include 8. ' - El Yes ❑ No pH(maximum) 0 Standard units S.u. No data Groundwater data does not include 'Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2D(Revised 3-19) Page 1 This page intentionally left blank. EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE B.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(k)(5)(ii))r Presence or Absence Estimated Data for Pollutants Expected to be Present or Limited by an ELG (check one) (Provide both concentration and mass estimates for each pollutant.) Pollutant Effluent Intake Water Believed Believed Maximum Daily Average Daily Source of Information Believed Present? Present Absent Units Discharge Discharge (check only one (required) (it available) (use codes in instructions) response per item) ❑ Check(✓)here if you believe all pollutants listed to be absent from the discharge.You need not complete Table B for the noted outfall unless you have quantitative data available. Bromide Concentration 1. (24959-67-9) El El ElElYes 0No Chlorine,total Concentration 2. residual El El El Yes 0No Mass Concentration 3. Color ❑ ❑ 0 Yes ✓❑ No Mass Concentration 4. Fecal coliform ❑ ❑ 0 Yes 0 No Mass Fluoride Concentration 0 0 Yes 0No 5' (16984 48-8) Mass Concentration 6. Nitrate-nitrite ❑ ❑ 0 Yes ✓❑ No Mass Nitrogen,total Concentration 7' organic(as N) El ❑ Mass ❑ Yes ❑ No Concentration 8. Oil and grease 0 0 0 Yes ❑r No Mass 9 Phosphorus(as P), ❑ El Concentration ❑ Yes ❑✓ No total(7723-14-0) Mass 10. Sulfate(as SO4) ❑ 0 Concentration 0 Yes ❑ No (14808-79-8) Mass Concentration 11. Sulfide(as S) ❑ ❑ ❑ Yes El No Mass EPA Form 3510-2D(Revised 3-19) Page 3 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE B.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(k)(5)(ii))t Presence or Absence Estimated Data for Pollutants Expected to be Present or Limited by an ELG (check one) (Provide both concentration and mass estimates for each pollutant.) Pollutant Effluent Intake Water Believed Believed Maximum Daily Average Daily Source of Information Believed Present? Present Absent Units Discharge Discharge (check only one response(if available) (use codes in instructions) per item)Sulfite(as SO3) Concentration I 12. (14265 45-3) El Mass El Yes ❑� No Concentration 13. Surfactants ❑ 0 0 Yes El No Mass Aluminum,total Concentration 14. (7429-90-5) El El Mass 0 Yes 0 No 15. Barium,total El ❑ Concentration El Yes 0 No (7440-39-3) Mass Boron,total Concentration 16. (7440 42-8) 0 ElMass 0 Yes 0 No Cobalt,total Concentration 17. (7440-48-0) El Mass 0 Yes 0 No Iron,total Concentration ug/L 3.013 Average concentration 18. (7439-89-6) El Mass lb/day 0.0001046 See Tables 1 and Attachment 0 Yes 0 No _ __ Magnesium,total Concentration 19. (7439-95 4) El Mass 0 Yes 0 No 20 Molybdenum,total El 0 Concentration 0 Yes 0 No (7439-98-7) Mass Manganese,total Concentration 21. (7439-96-5) El ❑ Mass 0 Yes 0 No Tin,total Concentration 22. (7440-31-5) 0 El — 0 Yes 0 No Mass EPA Form 3510-2D(Revised 3-19) Page4 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE B.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(k)(5)(ii))1 Presence or Absence Estimated Data for Pollutants Expected to be Present or Limited by an ELG (check one) (Provide both concentration and mass estimates for each pollutant.) Pollutant Effluent Intake Water Believed Believed Maximum Daily Average Daily Source of Information Believed Present? Present Absent Units Discharge Discharge (use codes in instructions) (check only one (required) (if available) response per item) Titanium,total Concentration ❑ Yes ❑r No 23. (7440-32-6) ❑ El 24. Radioactivity Concentration 24.1 Alpha,total ❑ ❑ 0 Yes ❑r No Mass Concentration 24.2 Beta,total ❑ ❑ Mass El Yes ElNo Concentration 24.3. Radium,total ❑ ❑ Mass El Yes El No Concentration 24.4 Radium 226,total ❑ ❑ Mass ❑ Yes ElNo 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510.2D(Revised 3-19) Pape 5 This page intentionally left blank. EPA Identification Number Facility Name 0utfall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE C.TOXIC METALS,TOTAL CYANIDE,AND TOTAL PHENOLS(40 CFR 122.21(k)(5)(iii)(A))1 Presence or Absence Estimated Data for Pollutants Expected to be Present in Discharge (check one) (Provide both concentration and mass estimates for each pollutant.) 1 Effluent Intake Water Pollutant Maximum Avera e (CAS Number,it available) Believed Believed g Believed Present? Present Absent Units Daily Daily Source of Information (Check only one Discharge Discharge (Use codes in Instructions.) response per pollutant) (required) (if available) ❑ Check(✓)here if you believe all pollutants listed to be absent from the discharge.You need not complete Table C for the noted outfall unless you have quantitative data available. 1. Antimony,Total0 El Concentration(7440-36-0) Mass ❑ Yes ❑ No 2. Arsenic,TotalEl El Concentration(7440-38-2) Mass ❑ Yes ❑ No 3. Beryllium,Total Concentration (7440-41-7) Mass ❑ Yes ❑✓ No 4. Cadmium,TotalD El Concentration ✓ (7440-43-9) Mass 0 Yes No 5. Chromium,TotalEl 0 Concentration CI No (7440-47-3) Mass 0 Yes 6. Copper,TotalEl El Concentration(7440-50-8) Mass • ❑ Yes ❑ No 7. Lead,Total0 El Concentration (7439-92-1) Mass CI Yes ❑✓ No 8. Mercury,TotalEl El Concentration(7439-97-6) Mass 0 Yes ❑ No 9. Nickel,TotalEl El Concentration 0(7440-02-0) Mass . Yes No 10. Selenium,TotalEl El Concentration ✓ (7782-49-2) Mass El Yes No 11. Silver,TotalEl El Concentration No (7440-22-4) Mass ❑ Yes 12. Thallium,Total Concentration (7440-28 0) ❑ Mass El Yes ❑✓ No 13. Zinc,Total0 El Concentration • (7440-66-6) Mass 0 Yes ❑✓ No 14. Cyanide,Total12 El Concentration ✓ (57-12-5) Mass 0 Yes No 15. Phenols,Total0 0 Concentration El Yes 0 No • Mass 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See Instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2D(Revised 3-19) Page 7 This page intentionally left blank. EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))1 Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) ❑ Check here if all pollutants listed in Table D are expected to be absent from your facility's discharge. ❑ Check here if the facility believes it is exempt from Table D reporting requirements because it is a qualified small business.See the instructions for exemption criteria and for a list of materials you must attach to the application. Note:If you check either of the above boxes,you do not need to complete Table D for the noted outfall unless you have quantitative data available. 1.Organic Toxic Pollutants(GCIMS Fraction—Volatile Compounds) 1.1 Acrolein Concentration (107-02-8) 0 0 I 0 Yes 0 No Mass 1.2 Acrylonitrile Concentration (107-13-1) 0 0 Mass 0 Yes 0 No 1.3 Benzene Concentration ug/L <0.0016 See Tables 1 and (71 43-2) 0 Mass Ib/d <0.00000005: Attachment to Frm 2D Yes 0 No 1.4 Bromoform Concentration (75-25-2) ❑ ❑ Mass ElYes 0 No 1.5 Carbon tetrachloride Concentration (56-23-5) 0 0 Mass 0 Yes 0 No 1.6 Chlorobenzene Concentration (108-90-7) 0 0 Mass El Yes 0 No 1.7 Chlorodibromomethane Concentration (124-48-1) 0 0 Mass 0 Yes 0 No 1.8 Chloroethane Concentration (75-00-3) ❑ 0 Mass ❑ Yes 0 No 1.9 2-chloroethylvinyl ether Concentration (110-75-8) ❑ El Mass 0 Yes 0 No 1.10 Chloroform(67-66-3) ❑ El See ug/L <0.0061 See Tables 1 and CI Yes 0 No Mass Ib/d <0.00000021. Attachment to Frm 2D 1.11 Dichlorobromomethane Concentration (75-27-4) 0 ❑ Mass 0 Yes 0 No EPA Form 3510-20(Revised 3-19) Page 9 ' 1 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))t Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 1.12 1,1-dichloroethane Concentration (75-34-3) 0 r❑ 0 Yes 0 No Mass 1.13 1,2-dichloroethane Concentration ug/L <0.00042 See Tables 1 and (107-06-2) 0 0 Attach.to Frm 2D 0 Yes ❑ No Mass Ib/d <0.00000001• 1.14 1,1-dichloroethylene Concentration (75-35-4) 0 0 Mass 0 Yes 0 No 1.15 1,2-dichloropropane Concentration (78-87-5) ❑ 0 Mass -' 0 Yes 0 No 1.16 1,3-dichloropropylene Concentration (542-75-6) 0 0 Mass 0 Yes 0 No 1.17 Ethylbenzene Concentration ug/L <0.089 See Tables 1 and (100-41 4) 0 0 Mass Ib/d <0.0000031 Attach.to Frm 2D Yes El No 1.18 Methyl bromide Concentration (74-83-9) 0 0 Mass 0 Yes 0 No 1.19 Methyl chloride Concentration ug/L <0.00073 See Tables 1 and (74 87-3) 0 0 Mass Ib/d <0.00000002 Attach.to Frm 2D El Yes 0 No 1.20 Methylene chloride Concentration (75-09-2) ❑ El Mass 0 Yes 0 No 1.21 1,1,2,2-tetrachloroethane 0 ❑ Concentration 0 Yes ❑ No (79-34-5) Mass 1.22 Tetrachloroethylene Concentration (127-18-4) ❑ 0 Mass ❑ Yes 0 No 1.23 Toluene Concentration ug/L <0.0061 See Tables 1 and CI (108-88-3) 0 Mass Ib/d <0.00000021 Attach.to Frm 2D Yes El No 1.24 1,2-trans-dichloroethylene 0 CI Concentration ❑ Yes CI No (156-60-5) Mass EPA Form 3510.2D(Revised 3.19) Page 10 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No,2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))l Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Maximum Average Source of Believed Present? Present ' Absent Units Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 1.25 1,1,1-trichloroethane Concentration (71-55-6) 0 0 Mass 0 Yes 0 No 1.26 1,1,2-trichloroethane Concentration (79-00-5) 0 0 Mass 0 Yes 0 No 1.27 Trichloroethylene Concentration (79-01-6) 0 0 0 Yes 0 No Mass 1.28 Vinyl chloride Concentration (75-01-4) ❑ E Mass 0 Yes 0No 2.Organic Toxic Pollutants(GC/MS Fraction—Acid Compounds) 2.1 2-chlorophenol ❑ Concentration ❑ Yes 0 No (95-57-8) Mass 2.2 2,4-dichlorophenol Concentration (120-83.2) 0 0 Mass 0 Yes IDNo 2.3 2,4-dimethylphenol Concentration (105-67-9) ❑ a Mass ❑ Yes 0No 2.4 4,6-dinitro-o-cresol Concentration (534-52-1) ❑ 0 Mass 0 Yes 0 No 2.5 2,4-dinitrophenol 0 ❑ Concentration ❑ Yes ❑ No (51-28-5) Mass 2.6 2-nitrophenol 0 Concentration ❑ Yes ❑" No (88-75 5) Mass 2.7 4-nitrophenol ❑ Concentration ❑ Yes CI No (100-02-7) Mass 2.8 p-chloro-m-cresol Concentration (59-50-7) ❑ ❑ Mass 0 Yes 0 No 2.9 Pentachlorophenol Concentration ' (87-86-5) ❑ aMass ❑ Yes ElNo EPA Form 3510-2D(Revised 3-19) Page 11 EPA Identification Number Facility Name 0utfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas ChromatographylMass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))1 Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 2.10 Phenol Concentration (108-95-2) ❑ 0 Mass ❑ Yes ❑r No 2.11 2,4,6-trichlorophenol 0 El Concentration ❑ Yes 0 No (88-05-2) Mass 3.Organic Toxic Pollutants(GC/MS Fraction—Base/Neutral Compounds) 3.1 Acenaphthene Concentration (83-32-9) 0 E Mass ❑ Yes 0No 3.2 Acenaphthylene 0 Concentration ❑ Yes ❑ No (208-96-8) Mass 3.3 Anthracene ❑ ❑ Concentration ❑ Yes No (120-12-7) Mass 3.4 Benzidine ❑ El Concentration ❑ Yes ❑ No (92-87-5) Mass 3.5 Benzo(a)anthracene Concentration (56-55-3) 0 0 Mass 0 Yes El No 3.6 Benzo(a)pyrene ❑ El Concentration El Yes El No (50 32 8) Mass 3.7 3,4-benzofluoranthene Concentration (205-99-2) El ❑ Mass ❑ Yes 0 No 3.8 Benzo(ghi)perylene ❑ ❑ Concentration ❑ Yes ElNo (191-24-2) Mass 3.9 Benzo(k)fluoranthene Concentration (207-08-9) 0 ❑ 0 Yes 0 No Mass 3.10 Bis(2-chioroethoxy)methane - ❑ ❑ Concentration ❑ Yes El No (111-91-1) Mass 3.11 Bis(2-chloroethyl)ether - Concentration (111-44-4) ❑ 0 Mass ❑ Yes ❑r No EPA Form 3510-2D(Revised 3-19) Page 12 1 EPA Identification Number Facility Name Outfall Number Form Approved 03/05119 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GCIMS Fractions)(40 CFR 122.21(k)(5)(iii)(B))r Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 3.12 Bis(2-chloroisopropyl)ether Concentration(102-80-1) El El Mass 0 Yes 0 No 3.13 Bis(2-ethylhexyl)phthalate 0 ❑ Concentration ❑ yes No (117-81-7) Mass ✓ 3.14 4-bromophenyl phenyl ether Concentration (101-55-3) ❑ 0 Mass El Yes Yes El 3.15 Butyl benzyl phthalate Concentration (85-68-7) 0 ❑ Mass 0 Yes El No 3.16 2-chloronaphthalene Concentration (91-58-7) ❑ 0 Mass 0 Yes 0No 3.17 4-chlorophenyl phenyl ether Concentration (7005-72-3) 0 0 Mass 0 Yes 0 No 3.18 Chrysene Concentration (218-01-9) 0 0 Mass 0 Yes 0 No 3.19 Dibenzo(a,h)anthracene Concentration (53-70-3) 0 Mass 0 Yes 0 No 3.20 1,2-dichlorobenzene Concentration (95-50-1) El 0 Mass 0 Yes 0No 3.21 1,3-dichlorobenzene Concentration (541-73-1) ❑ 0 Mass 0 Yes 0 No 3.22 1,4-dichlorobenzene Concentration (106-46-7) 0 0 Mass ElYes 0 No 3.23 3,3-dichlorobenzidine Concentration (91-94-1) ❑ 0 Mass ❑ Yes 0No 3.24 Diethyl phthalate Concentration (84-66-2) ❑ ❑ Mass 0 Yes 0 No 3.25 Dimethyl phthalate ❑ 0 Concentration ❑ Yes 0 No (131-11-3) Mass EPA Form 3510.2D(Revised 3-19) Page 13 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))1 Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 3.26 Di-n-butyl phthalate Concentration (84-74-2) ❑ 0 Mass CIYes 0 No 3.27 2,4-dinitrotoluene Concentration (121-14-2) ❑ 0 Mass El Yes 0 No 3.28 2,6-dinitrotoluene Concentration (606-20-2) 0 0 Mass CI Yes 0 No 3.29 Di-n-octyl phthalate 0 0 Concentration CI Yes ❑ No (117-84-0) Mass 3.30 1,2-diphenylhydrazine Concentration (as azobenzene)(122-66-7) ❑ 0 Mass CIYes 0 No 3.31 Fluoranthene 0 Concentration ❑ Yes (206-44-0) Mass ✓ No 3.32 Fluorene 0 ❑ Concentration ❑ Yes 0 No (86 73-7) Mass 3.33 Hexachlorobenzene Concentration (118-74-1) CI ❑ Mass ❑ Yes 0 No 3.34 Hexachlorobutadiene Concentration (87-68-3) 0 ❑ Mass 0 Yes 0 No 3.35 Hexachlorocyclopentadiene Concentration (77-47-4) 0 0 Mass 0 Yes 0 No 3.36 Hexachloroethane ❑ 0 Concentration CI Yes ❑ No (67-72-1) Mass ✓ 3.37. Indeno(1,2,3-cd)pyrene Concentration (193-39-5) 0 0 Mass 0 Yes 0 No 3.38 Isophorone Concentration (78-59-1) 0 ❑ Mass 0 Yes 0 No 3.39 Naphthalene Concentration ug/I <0.0283 (91-20-3) 0 ❑ Seet Tablesand ❑✓ Yes 0 No Mass Ib/d <0.00000099 Attach.to Frm 2D EPA Form 3510.2D(Revised 3-19) Page 14 EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLED.ORGANIC TOXIC POLLUTANTS(Gas ChromatographylMass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))1 Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 3.40 Nitrobenzene Concentration (98-95-3) 0 0 Mass 0 Yes 0 No 3.41 N-nitrosodimethylamine Concentration(62-75-9) CI CI Mass 0 Yes 13 No 3.42 N-nitrosodi-n-propylamine Concentration (621-64-7) ❑ ❑ Mass ElYes 0 No 3.43 N-nitrosodiphenylamine Concentration (86-30-6) ❑ a Mass ❑ Yes CI No 3.44 Phenanthrene Concentration (85-01-8) ❑ ❑ Mass El Yes ElNo 3.45 Pyrene Concentration (129-00-0) ❑ ❑ Mass ElYes 0 No 3.46 1,2,4-trichlorobenzene 0 Concentration ❑ Yes No (120-82-1) Mass 4.Organic Toxic Pollutants(GCIMS Fraction—Pesticides) 4.1. Aldrin Concentration (309-00-2) 0 0 Mass 0 Yes 0 No 4.2 a-BHC Concentration 0 No (319-84-0) El El ElElYes 4.3 )3-BHC Concentration (319-85-7) 0 CI Mass - ❑ Yes 0 No 4.4 y-BHC Concentration (58-89-9) 0 0 Mass - ❑ Yes 0 No 4.5 6-BHC Concentration (319-86-8) 0 Mass 0 Yes 0 No 4.6 Chlordane Concentration (57-74-9) 0 CI Mass ❑ Yes 0 No EPA Form 3510-2D(Revised 3-19) Page 15 I EPA Identification Number Facility Name Outfall Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.204D-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))r Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 4.7 4,4'-DDT Concentration (50-29-3) 0 IDMass 0 Yes 0 No 4.8 4,4'-DDE Concentration (72-55-9) ❑ 0 Mass El Yes 0No 4.9 4,4'-DDD Concentration (72-54-8) ❑ ❑ Mass 0 Yes CI No 4.10 Dieldrin Concentration (60-57-1) 0 ❑ Mass ❑ Yes El No 4.11 a-endosulfan Concentration (115-29-7) ❑ El 0 Yes 0 No Mass 4.12 f-endosulfan Concentration (115-29-7) 0 0 Mass 0 Yes CI No 4.13 Endosulfan sulfate Concentration (1031-07-8) 0 ❑✓ 0 Yes ❑r No Mass 4.14 Endrin Concentration (72-20-8) 0 ❑ Mass ❑ Yes 0 No 4.15 Endrin aldehyde Concentration (7421-93-4) ❑ ❑r ❑ Yes CI No Mass EPA Form 3510-20(Revised 3-19) Page 16 it EPA Identification Number Facility Name Outran Number Form Approved 03/05/19 New Facility Queensbridge Collective 1 OMB No.2040-0004 TABLE D.ORGANIC TOXIC POLLUTANTS(Gas Chromatography/Mass Spectrometry or GC/MS Fractions)(40 CFR 122.21(k)(5)(iii)(B))1 Presence or Absence Estimated Data for Pollutants Expected to Be Present in Discharge (check one) (provide both concentration and mass estimates for each pollutant) Pollutant Effluent Intake Water (CAS Number,if available) Believed Believed Units Maximum Average Source of Believed Present? Present Absent Daily Daily Information (check only one response per Discharge Discharge (use codes in instructions) pollutant) 4.16 Heptachlor Concentration (76-44-8) ❑ 0 Mass IDYes 0 No 4.17 Heptachlor epoxide Concentration (1024-57-3) 0 0 Mass 0 Yes 0 No 4.18 PCB-1242 0 ❑ Concentration ❑ Yes ❑ No (53469-21-9) Mass 4.19 PCB-1254 Concentration (11097-69-1) 0 ❑ Mass 0 Yes 0 No 4.20 PCB-1221 Concentration (11104-28-2) ❑ ❑ Mass ❑ Yes 0 No 4.21 PCB-1232 Concentration (11141-16-5) 0 E Mass 0 Yes 0 No 4.22 PCB-1248 Concentration (12672-29-6) 0 0 Mass 0 Yes 0 No 4.23 PCB-1260 Concentration (11096-82-5) 0 0 Mass 0 Yes 0 No 4.24 PCB-1016 0 Concentration ❑ Yes ❑ No (12674-11-2) Mass 4.25 Toxaphene Concentration (8001-35-2) 0 ❑� Mass 0 Yes 0 No 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2D(Revised 3-19) Page 17 r This page intentionally left blank. EPA Identlication Numbe, Facility Name Outfall Number Form Approved 03/05(19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE E.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(k)(5)(v))1 Presence or Absence Pollutant check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data Believed Believed (spedty units) Present Absent ❑ Check(/)here if you believe all pollutants listed to be absent from the discharge.You need not complete Table E for the noted outfall unless you have quantitative data available. 1. Asbestos 0 ❑r 2. Acetaldehyde ❑ r❑ 3. Allyl alcohol 0 r❑ 4. Allyl chloride ❑ ❑✓ 5. Amyl acetate ❑ ❑✓ 6. Aniline 0 ❑✓ 7. Benzonitrile 0 ❑✓ 8. Benzyl chloride 0 ✓❑ 9. Butyl acetate 0 ❑r 10. Butylamine ❑ El 11. Captan 0 ❑r 12. Carbaryl ❑ El 13. Carbofuran 0 ❑.. 14. Carbon disulfide ❑ ❑r 15. Chlorpyrifos 0 ❑✓ 16. Coumaphos ❑ ❑r 17. Cresol ❑ ❑✓ 18. Crotonaldehyde 0 ❑r EPA Form 3510.2D(Revised 3-19) Page 19 EPA Identification Number Facility Name 0ut(all Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE E.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(10(5)(v)), Presence or Absence Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data Believed Believed (specify units) Present Absent 19. Cyclohexane ❑ ✓❑ 20. 2,4-D(2,4-dichlorophenoxyacetic acid) ❑ El 21. Diazinon 0 El 22. Dicamba 0 ❑✓ 23. Dichlobenil ❑ ❑✓ 24. Dichlone 0 ❑✓ 25. 2,2-dichloropropionic acid 0 ✓❑ 26. Dichlorvos 0 ❑r 27. Diethyl amine 0 ❑r 28. Dimethyl amine ❑ ✓❑ 29. Dintrobenzene ❑ ❑✓ 30. Diquat 0 ❑✓ 31. Disulfoton ❑ ❑✓ 32. Diuron ❑ ❑r 33. Epichlorohydrin ❑ ❑✓ 34. Ethion ❑ ❑r 35. Ethylene diamine ❑ ❑✓ 36. Ethylene dibromide ❑ ❑r 37. Formaldehyde ❑ 0 EPA Form 3510-2D(Revised 3-19) Page 20 EPA Identification Number Facility Name Oudall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE E.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(k)(5)(v))1 Presence or Absence Pollutant (check one) Available Quantitative Data Believed Believed Reason Pollutant Believed Present in Discharge (specify units) Present Absent 38. Furfural 0 CI 39. Guthion ❑ ❑ 40. Isoprene 0 ❑✓ 41. Isopropanolamine 0 ❑✓ 42. Kelthane 0 ❑✓ 43. Kepone 0 0 44. Malathion 0 ✓❑ 45. Mercaptodimethur 0 ✓❑ 46. Methoxychlor 0 ❑✓ 47. Methyl mercaptan 0 ❑r 48. Methyl methacrylate 0 ❑r 49. Methyl parathion ❑ ❑ 50. Mevinphos ❑ ❑r 51. Mexacarbate 0 ❑✓ 52. Monoethyl amine 0 ❑✓ 53. Monomethyl amine 0 ❑✓ ' 54. Naled 0 ❑r 55. Naphthenic acid 0 ✓❑ 56. Nitrotoluene 0 ❑r EPA Form 3510-2D(Revised 3-19) Page 21 EPA Identification Number Facility Name 0utfall Number Form Approved 03/05/19 New Facility Queensbridge Collective OMB No.2040-0004 TABLE E.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(k)(5)(v))1 Presence or Absence Pollutant check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data Believed Believed (specify units) Present Absent 57. Parathion ❑ ✓❑ 58. Phenolsulfonate 0 ✓❑ 59. Phosgene 0 ❑✓ 60. Propargite ❑ ❑✓ 61. Propylene oxide ❑ El 62. Pyrethrins ❑ ❑✓ 63. Quinoline ❑ ❑✓ 64. Resorcinol ❑ ❑✓ 65. Strontium ❑ ❑✓ 66. Strychnine ❑ 0 67. Styrene 0 0 2,4 5-T(2,4,5-trichlorophenoxyacetic ✓ 68. Elacid) ❑ 69. TDE(tetrachlorodiphenyl ethane) ❑ ✓❑ 2,4,5-TP[2-(2,4,5-trichlorophenoxy) 70. propanoic acid] ❑ ❑ 71. Trichlorofon ❑ El 72. Triethanolamine ❑ ✓❑ 73. Triethylamine 0 El 74. Trimethylamine ❑ ❑✓ 75. Uranium ❑ II EPA Form 3510-2D(Revised 3.19) Page 22 EPA Identification Number Facility Name Outlall Number Form Approved 010519 New Facility Queensbridge Collective OMB No.2040-0004 TABLE E.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(k)(5)(v))1 Presence or Absence Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data Believed Believed (spedfy units) Present Absent 76. Vanadium 0 ❑✓ 77. Vinyl acetate 0 2 • 78. Xylene ❑✓ ❑ Petroleum impacts <0.103 ug/L;<0.0000036Ib/d 79. Xylenol ❑ ❑ 80. Zirconium 0 I Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2D(Revised 3-19) Page 23 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 U.S.Environmental Protection Agency FORM n Application for NPDES Permit to Discharge Wastewater 2E NPDES ������ MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURAL FACILITIES WHICH DISCHARGE ONLY NONPROCESS WASTEWATER SECTION 1.OUTFALL LOCATION(40 CFR 122.21(h)(1)) 1.1 Provide information on each of the facility's outfalls in the table below. c Outfall Receiving Water Name Latitude Longitude — Number 0 1 Little Sugar Creek 35° 13' 2.4" N 80° 50' 42.3" W 0 SECTION 2.DISCHARGE DATE(40 CFR 122.21(h)(2)) 2.1 Are you a new or existing discharger?(Check only one response.) s ❑r New discharger ElExisting discharger 4 SKIP to Section 3. 2.2 Specify your anticipated discharge date:11/01/2022 SECTION 3.WASTE TYPES(40 CFR 122.21(h)(3)) 3.1 What types of wastes are currently being discharged if you are an existing discharger or will be discharged if you are a new discharger?(Check all that apply.) ❑ Sanitary wastes E Other nonprocess wastewater(describe/explain ❑ Restaurant or cafeteria waste directly below) a ❑ Non-contact cooling water Groundwater from construction dewatering I— 3.2 Does the facility use cooling water additives? 0 � Yes ❑✓ No 4 SKIP to Section 4. 3.3 List the cooling water additives used and describe their comaosition. Cooling Water Additives Composition of Additives (list) (if available to you) SECTION 4.EFFLUENT CHARACTERISTICS(40 CFR 122.21(h)(4)) 4.1 Have you completed monitoring for all parameters in the table below at each of your outfalls and attached the results to this application package? El Yes 0 No;a waiver has been requested from my NPDES permitting authority (attach waiver request and additional information)4 SKIP to Section 5. 4.2 Provide data as requested in the table below.1(See instructions for specifics.) Number of Maximum Daily Average Daily Source Parameter or Pollutant Analyses Discharge Discharge (use codes (if actual data (specify units) (specify units) per reported) Mass Conc. Mass Conc. instructions) Biochemical oxygen demand(BOD5) See cover letter Total suspended solids(TSS) Oil and grease Ammonia(as N) Discharge flow pH(report as range) Temperature(winter) Temperature(summer) Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2E(revised 3-19) Page 1 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 4.3 Is fecal coliform believed present,or is sanitary waste discharged(or will it be discharged)? ❑ Yes ❑ No+SKIP to Item 4.5. 4.4 Provide data as requested in the table below."(See instructions for specifics.) Number of Maximum Daily Average Daily Source Parameter or Pollutant Analyses Discharge Discharge (Use codes (if actual data (specify units) (specify units) per reported) Mass Conc. Mass Conc. Instructions.) Fecal coliform d E.soli • = Enterococci 0 4.5 Is chlorine used(or will it be used)? ❑ Yes ElNo 4 SKIP to Item 4.7. 4.6 Provide data as requested in the table below.' (See instructions for specifics.) Number of Maximum Daily Average Daily Source to Parameter or Pollutant Analyses Discharge Discharge (use codes (if actual data (specify units) (speci units) per w reported) Mass Conc. Mass Conc. instructions) _ Total Residual Chlorine 4.7 Is non-contact cooling water discharged(or will it be discharged)? ❑ Yes El No 4 SKIP to Section 5. 4.8 Provide data as requested in the table below.' (See instructions for specifics.) Number of Maximum Daily Average Daily Source Parameter or Pollutant Analyses Discharge Discharge (use codes (if actual data (specify units) (specify units) per reported) Mass Conc. Mass Conc. instructions) Chemical oxygen demand(COD) Total organic carbon(TOC) SECTION 5.FLOW(40 CFR 122.21(h)(5)) 5.1 Except for stormwater water runoff,leaks,or spills,are any of the discharges you described in Sections 1 and 3 of this application intermittent or seasonal? ElYes 4 Complete this section. ❑ No 4 SKIP to Section 6. c 5.2 Briefly describe the frequency and duration of flow. uL The discharge will result from the temporary dewatering of caisson boreholes and excavation for subgrade foundation construction. The subgrade foundation is designed to intersect the reported groundwater surface elevation with approximately 153,900 square feet of floor area 2 feet below static water table level.Terracon is assuming a maximum flow rate for temporary construction dewatering at 112 gallons per minute(GPM).Flow is anticipated to be significantly below this rate because only small areas associated with construction progress would require dewatering. SECTION 6.TREATMENT SYSTEM(40 CFR 122.21(h)(6)) 6.1 Briefly describe any treatment system(s)used(or to be used). fR = FracTank collection with flow to Carbon Filter with Bag Filter System with mnimum flow of 50 gpm I Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2E(revised 3-19) Page 2 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 New Facility New Facility Queensbridge Collective OMB No.2040-0004 SECTION 7.OTHER INFORMATION(40 CFR 122.21(h)(7)) 7.1 Use the space below to expand upon any of the above items. Use this space to provide any information you believe the reviewer should consider in establishing permit limitations.Attach additional sheets as needed. C 0 E See Attached Engineering Alternatives Analysis 0 c N 0 SECTION 8.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d)) 8.1 In Column 1 below,mark the sections of Form 2E that you have completed and are submitting with your application. For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note that not all applicants are required to provide attachments. Column 1 Column 2 ❑✓ Section 1:Outfall Location ❑ w/attachments(e.g.,responses for additional outfalls) 2 Section 2: Discharge Date ❑ w/attachments ❑✓ Section 3:Waste Types ❑ w/attachments CI Section 4: Effluent Characteristics ❑ w/attachments 0 Section 5: Flow ❑ w/attachments c c 2 Section 6:Treatment System w/attachments w ❑ Section 7: Other Information ❑ w/attachments ❑✓ Section 8:Checklist and Certification Statement ❑ w/attachments - 8.2 Certification Statement 7) I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in CD accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name(print or type first and last name) Official titleit �^14 Vero G. SCE cc. H�,�'f{r�i Z� J c r 5 y Signature Date signed EPA Form 3510-2E(revised 3-19) Page 3 APPENDIX B ENGINEERING ALTERNATIVE ANALYSIS lierracon Memorandum TO: TERRACON PROJECT FILE 71227087 AND ATTACHMENT FOR NPDES PERMIT APPLICATION FROM: Neal McElveen; Will Frazier DATE: June 2, 2022 RE: Engineering Alternatives Analysis — Morehead Tryon Land LP NPDES Permit, 111 East Morehead Street, Charlotte, Mecklenburg County, North Carolina Description of Proposed Project Terracon was retained by Morehead Tryon Land LP to prepare an Engineering Alternatives Analysis (EAA) for the site located at 111 East Morehead Street in Charlotte, North Carolina. The site consists of six (6) contiguous tax parcels (Parcel Nos. 123-012-02, 123-012-03, 123- 012-05, 123-012-06, 123-012-07 and 123-0140-01.) totaling approximately 2.74 acres. The northernmost parcel is developed with an 11,298 sq. ft. nightclub/lounge building which operates as The Uptown Cabaret. The south-westernmost parcel is developed with a 2,964 sq. ft. restaurant building which operates as Midnight Diner. The remainder of the site includes paved parking lots and access drives. The site location and layout are shown on Exhibits 1 and 2 of the permit application. Morehead Tryon Land LP plans to redevelop the site with three mixed-use high-rise towers which will overlay an approximate 2- to 3-story sub-grade parking structure. Limited groundwater impacts have been identified at the site (see Table 1 and Exhibit 2), apparently the result of petroleum release(s) from former underground storage tanks located adjacent to the existing Uptown Cabaret building in the northern portion of the site. Morehead Tryon Land LP proposes to pre-treat the groundwater that is dewatered during construction activities and then discharge the effluent to the Charlotte-Mecklenburg County municipal stormwater sewer, with ultimate discharge occurring to Little Sugar Creek, under a new individual NPDES permit. Preparation of this EAA has been completed in conjunction with a NPDES application for the proposed discharge of pre-treated groundwater associated with Morehead Tryon Land LP's proposed construction. A description of the proposed project follows. Projections for flow, evaluation of technical and financial feasibility, and Local Government Review are provided in later sections. Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum Contact Information for Applicant, Facility, and EAA Preparer Applicant Morehead Tryon Land LP Attn: James Anderson 150 North Riverside Plaza, Suite 1800 Chicago, Illinois 60606 Phone: 317-788-1800 Email:janderson@riversideid.com Facility Queensbridge Collective 111 East Morehead Street Charlotte, Mecklenburg County, North Carolina 28202 Same as applicant EAA Preparer Terracon Consultants, Inc. Attn: M. Neal McElveen, P.E. 2701 Westport Road Charlotte, NC 28208 Phone:704-594-8912 Fax:704-509-1888 Email: neal.mcelveen@terracon.com STEP 1. Determination of Discharge Permit Eligibility Terracon has reviewed the potential restrictions identified in the EAA guidance document and does not believe that the identified restrictions will pose an impediment to an NPDES discharge from this location, as discussed below. The discharge will be to Little Sugar Creek and will occur after the groundwater has been treated. 1) Zero Flow Stream Restrictions According to the United States Geological Survey (USGS), Little Sugar Creek, the receiving stream for the proposed discharge, is not a zero-flow stream. As such, Little Sugar Creek is not subject to zero-flow stream restrictions. A copy of USGS correspondence providing flow estimates is included as an attachment to this memo. Please note while the correspondence is in response to a prior inquiry associated with a different project/proposed discharge (Radius Overlook Dilworth; 615 East Morehead Street), the Queensbridge Collective project (111 East Morehead Street) is located Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum approximately 1,700 feet northwest of the Radius Overlook Dilworth project and is also located within the Upper Little Sugar Creek watershed. As such, the proposed discharge will also enter Little Sugar Creek at a similar location and the USGS-provided flow characteristics provided in December 2021 are applicable for the Queensbridge Collective project. 2) Receiving Stream Classification According to NCDEQ DWR's online surface water classifications map, the receiving stream for the proposed discharge, Little Sugar Creek, is a Class C water. Class C waters are not subject to discharge restrictions and/or stricter treatment standards such as those that may be required for certain stream classifications(e.g. ORW, WS, SA, NSW, and HQ). 2) Basinwide Water Quality Plan According to the most recent Catawba River Basinwide Water Quality Plan (2010), Little Sugar Creek is listed as impaired for copper, mercury, and turbidity standards as well as biological integrity of fish and benthic communities (page 3.12 of the Plan). The Basinwide Plan includes total maximum daily load (TMDL) restrictions (see Item # 3 below for more information regarding TMDLs) to limit wastewater discharge within the Catawba River Basin. The Basinwide Plan indicates that Little Sugar Creek is subject to TMDLs for turbidity and fecal coliform bacteria (FCB; page 3.13 of the Plan). It should be noted that the Basinwide Plan also indicates that during the TMDL study window (1997 to 2004), Little Sugar Creek turbidity did not exceed the applicable turbidity standard and that the TMDL in question only covers Long Creek(page 1.43 of the Plan). 3) Impaired Waters and TMDLs According to a Final Report issued by NCDEQ in 2005 establishing TMDLs for turbidity within the Catawba River Basin, the TMDL for turbidity is only applicable to the portion of Little Sugar Creek between North Carolina Highway 51 and the North Carolina-South Carolina state line, which begins approximately 8 miles south of the site. As such, the proposed discharge to Little Sugar Creek is not limited by an established TMDL. According to a Final Report issued by NCDEQ in 2002 establishing TMDLs for FCB in four watersheds within Mecklenburg County, the entirety of Little Sugar Creek from its source to the state line is subject to the FCB TMDL. The proposed discharge is not a potential source of FCB, as it originates as dewatered groundwater generated during installation of deep foundations at a construction site. As such, the proposed discharge will not result in FCB impact to Little Sugar Creek or result in exceedance of the established TMDL. A TMDL was also established for dissolved oxygen (DO) in Little Sugar Creek in 1996. The proposed discharge is not expected to significantly affect the DO within Little Sugar Creek, as it is composed of groundwater from dewatered foundation installation activities in an urban area and it is not expected to be loaded with nutrients such as phosphorus and nitrate that would reduce DO. Further, the effluent will be treated on-site via carbon filtration prior to discharge. This carbon Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum filtration will remove volatile organic compounds that could be utilized by microbes within Little Sugar Creek as a food source, the metabolisms of which would also consume oxygen and lower DO. As such, the DO TMDL should not limit the proposed discharge. 4) Presence of Endangered Species According to the USFWS Information for Planning and Consultation (iPAC) online system, the following listed endangered species are potentially present in the general region of the site and down-stream portions (within approximately 3 miles of the proposed discharge point) of Little Sugar Creek: Michaux's Sumac (flowering plant), Schweinitz's Sunflower (flowering plant), Smooth Coneflower (flowering plant), Northern Long-eared Bat (mammal), Monarch Butterfly (insect), and Carolina Heelsplitter (clam). In addition, a number of migratory birds are listed in the iPAC information. As the Carolina Heelsplitter is the only aquatic species potentially present in Little Sugar Creek, there would be no expected impact to the other species listed above. According to the most recent Catawba River Basinwide Water Quality Plan (2010), the only stream in the Catawba River basin that supports populations of the Carolina Heelspliter is Waxhaw Creek(page 3.16 of the Plan), which enters the Catawba River some 30 miles south of the point of proposed discharge to Little Sugar Creek. As such, there would be no expected impact to the Carolina Heelsplitter from the proposed discharge. A summary of the iPAC endangered species information is included as an attachment to this letter. STEP 2 . Determination of Discharge Permit Eligibility A. Summary of Process Information and Flow Estimates The discharge will result from the temporary dewatering of caisson boreholes and excavation for subgrade foundation construction. The boreholes will range in diameter from 2.5 feet to 6 feet and will be advanced via auger rotary and rock core methods. A temporary casing will be driven ahead of the drill tooling to limit infiltration of the groundwater into the borehole. Once a borehole has reached the appropriate depth, it is anticipated that the borehole will remain open for a maximum of approximately one day prior to the installation of the concrete caisson via tremie pipe. Based on Terracon's geotechnical experience in the Charlotte area, groundwater is typically encountered within boreholes that are allowed to remain open overnight at the approximate expected depth of the water table based on the lithological conditions observed in the cuttings (e.g. saturated soil conditions). As such, Terracon conservatively assumes that groundwater will rise to the depth of the water table within the boreholes prior to caisson installation. Caissons are planned to be installed one at a time, with construction crews finishing one before moving to the next. The subgrade foundation is designed to intersect the reported groundwater surface elevation with approximately 153,900 square feet of floor area 2 feet below static water table level. Based on the caisson drilling schedule and dewatering to 2 feet below Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum groundwater surface elevation for the subgrade foundation construction, Terracon is assuming a maximum flow rate for temporary construction dewatering at 112 gallons per minute (GPM). Groundwater will be directed into a frac tank which discharges into a treatment train consisting of bag filtration (to remove sediment) and a steel vessel containing 8,000 pounds of reactivated carbon, as detailed in the NPDES permit application. The technical specifications of the treatment system are provided in Appendix D of the permit application. Please note that while the proposed pre-treatment is not considered a groundwater remediation treatment for the purposes of reducing petroleum concentrations of impacted groundwater within the subsurface at the site, for the purposes of this EAA and the NPDES Permit Application, it is referred to as a groundwater remediation system below. Terracon anticipates that the maximum discharge during working days will be approximately 112 GPM. Per the carbon filter manufacturer, the system should be operated at above 50 GPM to minimize channeling within the carbon vessel. As such, the system will be operated to maintain an average flow rate between 50 and 112 GPM. Flow rates will be intermittent, not continuous, based on construction phasing and groundwater infiltration. B. Low Flow Data for Receiving Stream Low flow information for the receiving water(s) was obtained from the US Geological Society (USGS)and the NCDEQ in Raleigh, North Carolina. Correspondence from the agencies is provided in Attachment A. Generally, the discharge from the system will be directed to a designated outfall through underground piping. From the point of discharge, underground piping discharges to a topographic depression in which stormwater ultimately flows into Little Sugar Creek. The USGS provided the following low-flow statistics based on a period of analysis of 1995 through 2011 climatic years: Frequency Discharge 7Q10 1.5 cubic feet per second (cfs) 30Q2 4.0 cfs W 7Q 10 2.3 cfs 7Q2 2.5 cfs Based on the USGS-provided information, Little Sugar Creek is not considered a zero-flow stream and is therefore not subject to zero-flow stream restrictions as set forth in 15A NCAC 2B.0206(d)(2). Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum STEP 2. Reasonable Projections for Flow As discussed in the EAA Guidance Document, non—municipal flow projections for groundwater remediation projects are based on engineering design considerations and/or production projections rather than population projections. As discussed in Step 1C above, the anticipated maximum flow associated with the temporary construction dewatering activities will be approximately 112 GPM. As there currently is no firm projection for the phases of construction, the flow rate is based on the calculation of hydraulic conductivity and infiltration into the maximum floor area anticipated to be below the groundwater elevation during construction activities — 2 feet saturated at 153,900 square feet. Flow rates will be intermittent, not continuous, based on construction phasing and groundwater infiltration. STEP 3. Evaluate Technologically Feasible Alternatives As discussed in the EAA Guidance Document, discharges from groundwater remediation systems are required to evaluate whether wastewater treatment plant (WWTP) connection, land application, infiltration galleries, in-situ groundwater remediation wells, or closed-loop groundwater remediation wells. As these alternatives have not been deemed technologically feasible, as discussed below, Terracon has also considered closed-wastewater reuse, discharge to surface waters, and combinations of the above as possible alternatives. A. Connection to an Existing WWTP The Charlotte-Mecklenburg Utilities (CMU) has discontinued accepting groundwater discharges. Specifically, the City of Charlotte Sewer Use Ordinance prohibits the discharge of groundwater in Section 23-79 (14) without permission from the CMU-System Protection (SP). Based on conversations with representatives of SP, CMU will not accept discharge of the dewatered groundwater, making this treatment alternative infeasible. B. Land Application The facility is located at 111 East Morehead Street in Charlotte, North Carolina. This location is just outside Uptown Charlotte in an urban area consisting predominantly of commercial development. Ground cover in the area is predominantly already developed hardscape. Land application of the discharge would interfere with construction. Based on the design and land constraints and the available land, land application is not feasible at this time. Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum C. Infiltration Galleries As discussed above, there is not space on the site to install an infiltration gallery. As such, infiltration galleries are not a technologically feasible alternative. D. In-Site or Closed-Loop Groundwater Remediation Wells As the proposed discharge is temporary, and it would be difficult to protect/maintain wells on an active construction site, permanent re-injection well infrastructure is unnecessary and not technically feasible. E. Wastewater Reuse The site will consist of an active construction site during the dewatering activities. As such, there are no site processes available in which the dewatered groundwater could be reused. Therefore, wastewater reuse is not technically feasible. F. Off-site Disposal of Discharge via Vacuum Truck The off-site disposal of temporarily containerized dewatered groundwater via vacuum truck ("batch and haul") is a technologically feasible alternative for disposal. However, as discussed in Step 5 below, it is not an economically feasible alternative compared to NPDES surface water discharge. G. Direct Discharge to Surface Waters Surface water discharge has been determined to be a technically feasible alternative for disposal of the dewatered groundwater based on the presence of Charlotte-Mecklenburg stormwater infrastructure at/adjacent to the site and its ultimate discharge to surface water. The discharge from the outlet of the treatment system will be directed into a stormwater intake located in an existing stormwater detention basin located at the southeast boundary of the property along Morehead Square Drive. Treated flow from dewatering activities ultimately discharges into Little Sugar Creek. Refer to Exhibit 1 for the approximate and location of the facility in relation to the Little Sugar Creek. Exhibit 2 shows the location of designated Outfall #1. Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum STEP 5. Evaluate Economically Feasible Alternatives "Batch and haul" and surface water discharge have been determined to be the only technically feasible alternatives for disposal of dewatered groundwater. As the proposed discharge is temporary and will only occur during an approximate 4-month period during 2022/2023, a 20- year present value cost analysis (PVCA) has not been completed. However, Terracon has completed a comparison of the overall projected costs of the two identified technologically feasible alternatives. Below is a table comparing costs for the disposal of the dewatered groundwater via "batch and haul" versus surface water discharge under a NPDES Individual Permit. The costs are estimates and are limited to those elements specific to the discharge, e.g. operational requirements, treatment costs, monitoring costs and maintenance. As the disposal facility will require characterization sampling of groundwater exported from the site via "batch and haul," and periodic sampling of pre-treated groundwater discharge is anticipated under the NPDES permit requirements, it has been assumed that the difference in sampling costs (labor and laboratory analysis) is negligible. In addition, as dewatered groundwater will be containerized within a rented frac tank in either scenario, its cost has not been included in the table below. Description Present Value (2022 only) "Batch and Haul" NPDES Discharge Vacuum Truck Services $100,000 NA (assumes 100 mobilizations of a 5,000-gallon tanker; assumes 8- hour round trips at $125/hour) Disposal ($0.35/gallon)-Based $175,000 NA on intermittent dewatering - Assume 500,000 gallons Bag Filter Rental (4 months)* NA $2,400 Carbon Filter Rental (4 months)* NA $26,461 Hoses and connections NA $1,800 TOTAL COST $275,000 $30,661 *Includes mobilization/demobilization fees Based on the above cost analysis, the opportunity cost to pursue a "batch and haul" alternative to NPDES-permitted discharge under an individual permit is $244,339. As such, the NPDES permit is by far the most economically feasible option for disposal of the dewatered groundwater at the site. Charlotte,NC Environmental • Facilities • Geotechnical • Materials lierracon Memorandum ATTACHMENTS Charlotte,NC Environmental • Facilities • Geotechnical • Materials Frazier, William 0 From: Weaver,John C <jcweaver@usgs.gov> Sent: Wednesday, December 1, 2021 12:20 PM To: Frazier, William 0 Cc: Hill, David A; adugna.kebede@ncdenr.gov; Montebello, Michael J; Dowden, Doug; Albertin, Klaus P; Weaver, John C Subject: USGS response to DWR USGS Low Flows request# 2022-163 (dated 2021/11/23)for Little Sugar Creek Mecklenburg County...RE: [EXTERNAL) Low-flow request approval Mr. Frazier, In response to your inquiry about the low-flow characteristics for a location immediately upstream from USGS Sta. 02146409 Little Sugar Creek at Medical Center Drive at Charlotte (station id 02146409, NWIS drainage area 11.8 sqmi) in downtown Charlotte in Mecklenburg County,the following information is provided: A check of the low-flow files here at the USGS South Atlantic Water Science Center(Raleigh office) indicates the point of interest is located immediately upstream from a USGS continuous-record streamgage on Little Sugar Creek, as identified by the lat/long coordinates(35.20361, -80.83694) provided via email dated 11/23/2021 from the DWR USGS Low Flow portal following your request submission. A basin delineation completed usingthe online USGS StreamStats application for North Carolina p PP (https://streamstats.usgs.gov/ss/) indicates the drainage area for the point of interest (StreamStats adjusted coordinates 35.20360, -80.83711 NAD83) is 12 sqmi. published bythe USGS are provided in the following streams in Mecklenburg County, low-flow characteristics g reports: (1)The first is a statewide report completed in the early 1990's. It is USGS Water-Supply Paper 2403, "Low-flow characteristics of streams in North Carolina" (Giese and Mason, 1993). An online version of the report is available at https://pubs.usgs.gov/wsp/2403/report.pdf. The report provides the low-flow characteristics (based on data through 1988)via regional relations and at-site values for sites with drainage basins between 1 and 400 sqmi and not considered or known to be affected by regulation and/or diversions. (2) The second is a statewide report published in March 2015. It is USGS Scientific Investigations Report 2015-5001, "Low-flow characteristics and flow-duration statistics for selected USGS continuous-record streamgaging stations in North Carolina through 2012" (Weaver, 2015). The report is available online at https://pubs.usgs.gov/sir/2015/5001/. The report provides updated low-flow characteristics and flow-duration statistics for 266 active(as of 2012 water year) and discontinued streamgages across the state where a minimum of 10 climatic years discharge records were available for flow analyses. Low-flow characteristics estimated for point of interest: Inspection of the most recent USGS statewide low-flow report (#2 above-referenced report) indicates the low-flow characteristics for this streamgage were published. In table 3 on page 26 of this report,the following low-flow statistics are provided: Period of analysis: 1995-2011 climatic years 1 Annual 7Q10 discharge= 1.5 cfs Annual 30Q2 discharge=4.0 cfs Annual winter 7Q10(W7Q10) discharge= 2.3 cfs Annual 7Q2 discharge = 2.5 cfs Annual average discharge = 19.2 cfs (period of analysis 1995-2012 water years,table 5 on page 83) Please note: (1) The estimated flows are provided in units of cubic feet per second per square mile drainage area (cfsm). (2) The climatic year is the standard period used for low-flow analyses at USGS continuous-record streamgages. The climatic year is from April 1 through March 31, designated by the year in which the period begins. For example,the 2011 climatic year is from April 1, 2011, through March 31, 2012. Again, please understand the information provided in this message is based on a preliminary assessment and considered provisional, subject to revision pending collection of future data and further analyses. These provisional streamflow statistics are provided via the DWR USGS Low Flows cooperative agreement between USGS and the N.C. Department of Environmental Quality, Division of Water Resources. Hope this information is helpful. Thank you. Curtis Weaver J. Curtis Weaver, Hydrologist, PE Email:icweaver(r usgs.gov USGS South Atlantic Water Science Center Online:https://www.usgs.gov/centers/sa-water North Carolina -South Carolina -Georgia 3916 Sunset Ridge Road Raleigh, NC 27607 Phone: (919) 571-4043 // Fax: (919)571-4041 From: Albertin, Klaus P<klaus.albertin@ncdenr.gov> Sent:Tuesday, November 23, 2021 3:20 PM To:will.frazier@terracon.com Cc:Albertin, Klaus P<klaus.albertin@ncdenr.gov>; Hill, David A<david.hill@ncdenr.gov>; adugna.kebede@ncdenr.gov; Weaver,John C<jcweaver@usgs.gov>; Montebello, Michael J <Michael.Montebello@ncdenr.gov>; Dowden, Doug <doug.dowden@ncdenr.gov> Subject: [EXTERNAL] Low-flow request approval [-This email has been received from outside of DOI-Use caution before clicking on links,opening attachments,or responding. 2 Your request has been approved and will be forwarded to USGS. A response from USGS usually takes 7 - 10 business days. Request Flow Statistic Approval Request ID: 163 Requestor:Will Frazier Requestor e-mail: will.frazier@terracon.com Requestor Phone: 3364090772 Local Government: Public Water Supply: Consultant:Terracon Consultants, Inc. Contact: Will Frazier Reason: Permit River/Stream: Little Sugar Creek Drainage Area (sq. mi.): 11.8 Latitude: 35.20361 Longitude: -80.83694 Other Information:We are applying for an individual NPDES permit to discharge pre-treated (via carbon filtration) petroleum-impacted groundwater generated from temporary dewatering during the construction of a high-rise tower building located at 615 East Morehead Street in Charlotte, NC(35.216565, -80.846559). Statististics: ["7Q10","30021 Approved by:Albertin, Klaus P 3 it APPENDIX C ANALYTICAL REPORT TERRACON 2022 SAMPLING Pace Analytical Services,LLC aceAnalytical a 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 WWMAlcNIbs.coe (704)875-9092 March 23, 2022 Will Frazier Terracon 2701 Westport Rd Charlotte, NC 28208 RE: Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Dear Will Frazier: Enclosed are the analytical results for sample(s)received by the laboratory on March 16,2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: •Pace Analytical Services-Asheville •Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyler Forney tyler.forney@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Robert Brookshire,Terracon ; j • REPORT OF LABORATORY ANALYSIS hialk This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 31 Pace Analytical Services,LLC ^Ql_1'^''® 9800 Kincey Ave. Suite 100 a tiG yt ca Huntersville,NC 28078 www.pacNaba.con (704)875-9092 CERTIFICATIONS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 31 aceAnalytical® Pace Analytical Services,LLC 9800 KinceyAve. Suite 100 Huntersville,NC 28078 rrrn►.peNN»can (704)875-9092 SAMPLE SUMMARY Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Lab ID Sample ID Matrix Date Collected Date Received 92593649001 B-105 Water 03/15/22 14:20 03/16/22 11:10 92593649002 B-106 Water 03/15/22 11:15 03/16/22 11:10 92593649003 B-108 Water 03/15/22 13:20 03/16/22 11:10 92593649004 B-110 Water 03/15/22 12:40 03/16/22 11:10 92593649005 B-112 Water 03/15/22 11:00 03/16/22 11:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 31 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 wrw.wultibs con (704)875-9092 SAMPLE ANALYTE COUNT Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92593649001 B-105 EPA 6020B CRW 1 PASI-A EPA 8260D NSCQ 63 PASI-C 92593649002 B-106 EPA 6020E CRW 1 PASI-A EPA 8260D SAS 63 PASI-C 92593649003 B-108 EPA 6020B CRW 1 PASI-A EPA 8260D NSCQ 63 PASI-C 92593649004 B-110 EPA 6020B CRW 1 PASI-A EPA 8260D NSCQ 63 PASI-C 92593649005 B-112 EPA 6020E CRW 1 PASI-A EPA 8260D NSCQ 63 PASI-C PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 4 of 31 1 Pace Analytical Services,LLC aceAnalytical to 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacNsbs.cas (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-105 Lab ID: 92593649001 Collected: 03/15/22 14:20 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method:EPA 6020B Preparation Method:EPA 3010A Pace Analytical Services-Asheville Iron 93.6 ug/L 50.0 20.9 1 03/17/22 13:45 03/18/22 13:12 7439-89-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 25.0 5.1 1 03/19/22 00:50 67-64-1 Benzene ND ug/L 1.0 0.34 1 03/19/22 00:50 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 03/19/22 00:50 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 03/19/22 00:50 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 03/19/22 00:50 75-27-4 Bromoform ND ug/L 1.0 0.34 1 03/19/22 00:50 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 03/19/22 00:50 74-83-9 2-Butanone(MEK) ND ug/L 5.0 4.0 1 03/19/22 00:50 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 03/19/22 00:50 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 03/19/22 00:50 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 03/19/22 00:50 75-00-3 Chloroform ND ug/L 1.0 0.43 1 03/19/22 00:50 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 03/19/22 00:50 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 03/19/22 00:50 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 03/19/22 00:50 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 03/19/22 00:50 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 03/19/22 00:50 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 0.27 1 03/19/22 00:50 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 03/19/22 00:50 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 03/19/22 00:50 95-50-1 I 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 03/19/22 00:50 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 03/19/22 00:50 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 03/19/22 00:50 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 03/19/22 00:50 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 03/19/22 00:50 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 03/19/22 00:50 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 03/19/22 00:50 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 03/19/22 00:50 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 03/19/22 00:50 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 03/19/22 00:50 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 03/19/22 00:50 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 03/19/22 00:50 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/19/22 00:50 10061-01-5 Vans-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/19/22 00:50 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.31 1 03/19/22 00:50 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 03/19/22 00:50 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 03/19/22 00:50 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 03/19/22 00:50 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.41 1 03/19/22 00:50 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 03/19/22 00:50 75-09-2 L1,v1 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 2.7 1 03/19/22 00:50 108-10-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 31 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www•pacelabs.can (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-105 Lab ID: 92593649001 Collected: 03/15/22 14:20 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 03/19/22 00:50 1634-04-4 Naphthalene ND ug/L 1.0 0.64 1 03/19/22 00:50 91-20-3 Styrene ND ug/L 1.0 0.29 1 03/19/22 00:50 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 03/19/22 00:50 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 03/19/22 00:50 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 03/19/22 00:50 127-18-4 Toluene ND ug/L 1.0 0.48 1 03/19/22 00:50 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 03/19/22 00:50 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 03/19/22 00:50 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 03/19/22 00:50 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 03/19/22 00:50 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 03/19/22 00:50 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 03/19/22 00:50 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 03/19/22 00:50 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 03/19/22 00:50 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 03/19/22 00:50 75-01-4 Xylene(Total) ND ug/L 1.0 0.34 1 03/19/22 00:50 1330-20-7 m&p-Xylene ND ug/L 2.0 0.71 1 03/19/22 00:50 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 03/19/22 00:50 95-47-6 Surrogates 4-Bromofluorobenzene(S) 97 % 70-130 1 03/19/22 00:50 460-00-4 1,2-Dichloroethane-d4(S) 106 % 70-130 1 03/19/22 00:50 17060-07-0 Toluene-d8(S) 101 % 70-130 1 03/19/22 00:50 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 31 I Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnal is ' Huntersville,NC 28078 www.pac .con (704)875-9092 I ANALYTICAL RESULTS 1 Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-106 Lab ID: 92593649002 Collected: 03/15/22 11:15 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method:EPA 6020E Preparation Method:EPA 3010A Pace Analytical Services-Asheville Iron 1890 ug/L 50.0 20.9 1 03/17/22 13:45 03/18/22 13:30 7439-89-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 25.0 5.1 1 03/22/22 15:10 67-64-1 Benzene ND ug/L 1.0 0.34 1 03/22/22 15:10 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 03/22/22 15:10 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 03/22/22 15:10 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 03/22/22 15:10 75-27-4 Bromoform ND ug/L 1.0 0.34 1 03/22/22 15:10 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 03/22/22 15:10 74-83-9 2-Butanone(MEK) ND ug/L 5.0 4.0 1 03/22/22 15:10 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 03/22/22 15:10 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 03/22/22 15:10 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 03/22/22 15:10 75-00-3 Chloroform 1.2 ug/L 1.0 0.43 1 03/22/22 15:10 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 03/22/22 15:10 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 03/22/22 15:10 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 03/22/22 15:10 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 03/22/22 15:10 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 03/22/22 15:10 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 0.27 1 03/22/22 15:10 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 03/22/22 15:10 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 03/22/22 15:10 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 03/22/22 15:10 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 03/22/22 15:10 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 03/22/22 15:10 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 03/22/22 15:10 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 03/22/22 15:10 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 03/22/22 15:10 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 03/22/22 15:10 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 03/22/22 15:10 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 03/22/22 15:10 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 03/22/22 15:10 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 03/22/22 15:10 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 03/22/22 15:10 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/22/22 15:10 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/22/22 15:10 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.31 1 03/22/22 15:10 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 03/22/22 15:10 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 03/22/22 15:10 87-68-3 IK 2-Hexanone ND ug/L 5.0 0.48 1 03/22/22 15:10 591-78-6 p-lsopropyltoluene ND ug/L 1.0 0.41 1 03/22/22 15:10 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 03/22/22 15:10 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 2.7 1 03/22/22 15:10 108-10-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 31 Pace Analytical Services,LLC e 9800 Kince Ave. Suite 100 aceAnalytical Y Huntersville,NC 28078 www.wcaabs.wa (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-106 Lab ID: 92593649002 Collected: 03/15/22 11:15 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 03/22/22 15:10 1634-04-4 Naphthalene ND ug/L 1.0 0.64 1 03/22/22 15:10 91-20-3 IK Styrene ND ug/L 1.0 0.29 1 03/22/22 15:10 100-42-5 1 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 03/22/22 15:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 03/22/22 15:10 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 03/22/22 15:10 127-18-4 Toluene ND ug/L 1.0 0.48 1 03/22/22 15:10 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 03/22/22 15:10 87-61-6 IK 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 03/22/22 15:10 120-82-1 IK 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 03/22/22 15:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 03/22/22 15:10 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 03/22/22 15:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 03/22/22 15:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 03/22/22 15:10 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 03/22/22 15:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 03/22/22 15:10 75-01-4 Xylene(Total) ND ug/L 1.0 0.34 1 03/22/22 15:10 1330-20-7 m&p-Xylene ND ug/L 2.0 0.71 1 03/22/22 15:10 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 03/22/22 15:10 95-47-6 Surrogates 4-Bromofluorobenzene(S) 105 % 70-130 1 03/22/22 15:10 460-00-4 1,2-Dichloroethane-d4(S) 106 % 70-130 1 03/22/22 15:10 17060-07-0 Toluene-d8(S) 102 % 70-130 1 03/22/22 15:10 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 31 Pace Analytical Services,LLC ceAnalytica,• 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacNabs.cae (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-108 Lab ID: 92593649003 Collected: 03/15/22 13:20 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method:EPA 6020B Preparation Method:EPA 3010A Pace Analytical Services-Asheville Iron 12900 ug/L 500 209 10 03/17/22 13:45 03/18/22 15:16 7439-89-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone 64.9 ug/L 25.0 5.1 1 03/19/22 00:14 67-64-1 Benzene 1.6 ug/L 1.0 0.34 1 03/19/22 00:14 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 03/19/22 00:14 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 03/19/22 00:14 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 03/19/22 00:14 75-27-4 Bromoform ND ug/L 1.0 0.34 1 03/19/22 00:14 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 03/19/22 00:14 74-83-9 2-Butanone(MEK) 15.6 ug/L 5.0 4.0 1 03/19/22 00:14 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 03/19/22 00:14 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 03/19/22 00:14 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 03/19/22 00:14 75-00-3 Chloroform 6.1 ug/L 1.0 0.43 1 03/19/22 00:14 67-66-3 1 Chloromethane 0.73J ug/L 1.0 0.54 1 03/19/22 00:14 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 03/19/22 00:14 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 03/19/22 00:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 03/19/22 00:14 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 03/19/22 00:14 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 0.27 1 03/19/22 00:14 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 03/19/22 00:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 03/19/22 00:14 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 03/19/22 00:14 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 03/19/22 00:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 03/19/22 00:14 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 03/19/22 00:14 75-34-3 1,2-Dichloroethane 0.42J ug/L 1.0 0.32 1 03/19/22 00:14 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 03/19/22 00:14 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 03/19/22 00:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 03/19/22 00:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 03/19/22 00:14 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 03/19/22 00:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 03/19/22 00:14 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 03/19/22 00:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/19/22 00:14 10061-01-5 Vans-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/19/22 00:14 10061-02-6 1 Diisopropyl ether ND ug/L 1.0 0.31 1 03/19/22 00:14 108-20-3 Ethylbenzene 89.0 ug/L 1.0 0.30 1 03/19/22 00:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 03/19/22 00:14 87-68-3 2-Hexanone 2.0J ug/L 5.0 0.48 1 03/19/22 00:14 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.41 1 03/19/22 00:14 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 03/19/22 00:14 75-09-2 L1,v1 4-Methyl-2-pentanone(MIBK) 7.0 ug/L 5.0 2.7 1 03/19/22 00:14 108-10-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 31 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pnUbs.can (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-108 Lab ID: 92593649003 Collected: 03/15/22 13:20 Received: 03/16/22 11:10 Matrix: Water Report 1 Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 03/19/22 00:14 1634-04-4 Naphthalene 28.3 ug/L 1.0 0.64 1 03/19/22 00:14 91-20-3 Styrene ND ug/L 1.0 0.29 1 03/19/22 00:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 03/19/22 00:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 03/19/22 00:14 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 03/19/22 00:14 127-18-4 Toluene 6.1 ug/L 1.0 0.48 1 03/19/22 00:14 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 03/19/22 00:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 03/19/22 00:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 03/19/22 00:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 03/19/22 00:14 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 03/19/22 00:14 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 03/19/22 00:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 03/19/22 00:14 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 03/19/22 00:14 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 03/19/22 00:14 75-01-4 Xylene(Total) 103 ug/L 1.0 0.34 1 03/19/22 00:14 1330-20-7 m&p-Xylene 96.6 ug/L 2.0 0.71 1 03/19/22 00:14 179601-23-1 o-Xylene 6.2 ug/L 1.0 0.34 1 03/19/22 00:14 95-47-6 Surrogates 4-Bromofluorobenzene(S) 98 % 70-130 1 03/19/22 00:14 460-00-4 1,2-Dichloroethane-d4(S) 109 % 70-130 1 03/19/22 00:14 17060-07-0 Toluene-d8(S) 101 % 70-130 1 03/19/22 00:14 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 31 Pace Analytical Services,LLC I a, 9800 Kincey Ave. Suite 100 (, 9 Huntersville,NC 28078 www.wcelabs.cae (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-110 Lab ID: 92593649004 Collected: 03/15/22 12:40 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua! 6020 MET ICPMS Analytical Method:EPA 6020E Preparation Method:EPA 3010A Pace Analytical Services-Asheville Iron 550 ug/L 50.0 20.9 1 03/17/22 13:45 03/18/22 13:45 7439-89-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 25.0 5.1 1 03/18/22 23:56 67-64-1 Benzene ND ug/L 1.0 0.34 1 03/18/22 23:56 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 03/18/22 23:56 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 03/18/22 23:56 74-97-5 Bromodichloromethane 0.32J ug/L 1.0 0.31 1 03/18/22 23:56 75-27-4 Bromoform ND ug/L 1.0 0.34 1 03/18/22 23:56 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 03/18/22 23:56 74-83-9 2-Butanone(MEK) ND ug/L 5.0 4.0 1 03/18/22 23:56 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 03/18/22 23:56 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 03/18/22 23:56 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 03/18/22 23:56 75-00-3 Chloroform 1.7 ug/L 1.0 0.43 1 03/18/22 23:56 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 03/18/22 23:56 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 03/18/22 23:56 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 03/18/22 23:56 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 03/18/22 23:56 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 03/18/22 23:56 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 0.27 1 03/18/22 23:56 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 03/18/22 23:56 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 03/18/22 23:56 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 03/18/22 23:56 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 03/18/22 23:56 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 03/18/22 23:56 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 03/18/22 23:56 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 03/18/22 23:56 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 03/18/22 23:56 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 03/18/22 23:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 03/18/22 23:56 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 03/18/22 23:56 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 03/18/22 23:56 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 03/18/22 23:56 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 03/18/22 23:56 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/18/22 23:56 10061-01-5 Vans-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/18/22 23:56 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.31 1 03/18/22 23:56 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 03/18/22 23:56 100-41-4 1 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 03/18/22 23:56 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 03/18/22 23:56 591-78-6 p-lsopropyltoluene ND ug/L 1.0 0.41 1 03/18/22 23:56 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 03/18/22 23:56 75-09-2 L1,v1 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 2.7 1 03/18/22 23:56 108-10-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 31 I Pace Analytical Services,LLC �n� � a 9800 Kincey Ave. Suite 100 ceAnaViV/+aI Huntersville,NC 28078 winv.pecelabs.coe (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-110 Lab ID: 92593649004 Collected: 03/15/22 12:40 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 03/18/22 23:56 1634-04-4 Naphthalene ND ug/L 1.0 0.64 1 03/18/22 23:56 91-20-3 Styrene ND ug/L 1.0 0.29 1 03/18/22 23:56 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 03/18/22 23:56 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 03/18/22 23:56 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 03/18/22 23:56 127-18-4 Toluene ND ug/L 1.0 0.48 1 03/18/22 23:56 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 03/18/22 23:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 03/18/22 23:56 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 03/18/22 23:56 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 03/18/22 23:56 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 03/18/22 23:56 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 03/18/22 23:56 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 03/18/22 23:56 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 03/18/22 23:56 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 03/18/22 23:56 75-01-4 Xylene(Total) ND ug/L 1.0 0.34 1 03/18/22 23:56 1330-20-7 m&p-Xylene ND ug/L 2.0 0.71 1 03/18/22 23:56 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 03/18/22 23:56 95-47-6 Surrogates 4-Bromofluorobenzene(S) 94 % 70-130 1 03/18/22 23:56 460-00-4 1,2-Dichloroethane-d4(S) 105 % 70-130 1 03/18/22 23:56 17060-07-0 Toluene-d8(S) 99 % 70-130 1 03/18/22 23:56 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 31 Pace Services,LLC aceAnalytical® 9800 Ki Analytical Services, Suite 100 Huntersville,NC 28078 wwn pudabs con (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-112 Lab ID: 92593649005 Collected: 03/15/22 11:00 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua! 6020 MET ICPMS Analytical Method:EPA 6020B Preparation Method:EPA 3010A Pace Analytical Services-Asheville Iron 67.7 ug/L 50.0 20.9 1 03/17/22 13:45 03/18/22 13:48 7439-89-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 25.0 5.1 1 03/18/22 23:38 67-64-1 Benzene ND ug/L 1.0 0.34 1 03/18/22 23:38 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 03/18/22 23:38 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 03/18/22 23:38 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 03/18/22 23:38 75-27-4 Bromoform ND ug/L 1.0 0.34 1 03/18/22 23:38 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 03/18/22 23:38 74-83-9 2-Butanone(MEK) ND ug/L 5.0 4.0 1 03/18/22 23:38 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 03/18/22 23:38 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 03/18/22 23:38 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 03/18/22 23:38 75-00-3 Chloroform 0.58J ug/L 1.0 0.43 1 03/18/22 23:38 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 03/18/22 23:38 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 03/18/22 23:38 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 03/18/22 23:38 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 03/18/22 23:38 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 03/18/22 23:38 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 0.27 1 03/18/22 23:38 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 03/18/22 23:38 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 03/18/22 23:38 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 03/18/22 23:38 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 03/18/22 23:38 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 03/18/22 23:38 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 03/18/22 23:38 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 03/18/22 23:38 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 03/18/22 23:38 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 03/18/22 23:38 156-59-2 Vans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 03/18/22 23:38 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 03/18/22 23:38 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 03/18/22 23:38 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 03/18/22 23:38 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 03/18/22 23:38 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/18/22 23:38 10061-01-5 Vans-1,3-Dichloropropene ND ug/L 1.0 0.36 1 03/18/22 23:38 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.31 1 03/18/22 23:38 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 03/18/22 23:38 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 03/18/22 23:38 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 03/18/22 23:38 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.41 1 03/18/22 23:38 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 03/18/22 23:38 75-09-2 L1,v1 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 2.7 1 03/18/22 23:38 108-10-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 31 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacUlabs.com (704)875-9092 ANALYTICAL RESULTS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Sample: B-112 Lab ID: 92593649005 Collected: 03/15/22 11:00 Received: 03/16/22 11:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 03/18/22 23:38 1634-04-4 Naphthalene ND ug/L 1.0 0.64 1 03/18/22 23:38 91-20-3 Styrene ND ug/L 1.0 0.29 1 03/18/22 23:38 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 03/18/22 23:38 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 03/18/22 23:38 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 03/18/22 23:38 127-18-4 Toluene ND ug/L 1.0 0.48 1 03/18/22 23:38 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 03/18/22 23:38 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 03/18/22 23:38 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 03/18/22 23:38 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 03/18/22 23:38 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 03/18/22 23:38 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 03/18/22 23:38 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 03/18/22 23:38 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 03/18/22 23:38 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 03/18/22 23:38 75-01-4 Xylene(Total) ND ug/L 1.0 0.34 1 03/18/22 23:38 1330-20-7 m&p-Xylene ND ug/L 2.0 0.71 1 03/18/22 23:38 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 03/18/22 23:38 95-47-6 Surrogates 4-Bromofluorobenzene(S) 98 % 70-130 1 03/18/22 23:38 460-00-4 1,2-Dichloroethane-d4(S) 103 % 70-130 1 03/18/22 23:38 17060-07-0 Toluene-d8(S) 99 % 70-130 1 03/18/22 23:38 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 31 Pace Analytical Services,LLC • 9800 KinceyAve. Suite 100 aceAnalytical Huntersville,NC 28078 traw.pcelak.cae (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 QC Batch: 685432 Analysis Method: EPA 6020B IDescription: QC Batch Method: EPA 3010A Analysis 6020 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92593649001,92593649002,92593649003,92593649004,92593649005 METHOD BLANK: 3583998 Matrix: Water Associated Lab Samples: 92593649001,92593649002,92593649003,92593649004,92593649005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Iron ug/L ND 50.0 20.9 03/18/22 13:04 LABORATORY CONTROL SAMPLE: 3583999 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Iron ug/L 1250 1280 103 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3584000 3584001 MS MSD 92593649001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Iron ug/L 93.6 1250 1250 1380 1320 103 98 75-125 4 20 Results presented on this page are In the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 31 Pace Analytical Services,LLC aceAnalytical m 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 QC Batch: 685904 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92593649001,92593649003,92593649004,92593649005 METHOD BLANK: 3586658 Matrix: Water Associated Lab Samples: 92593649001,92593649003,92593649004,92593649005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 03/18/22 21:41 1,1,1-Trichloroethane ug/L ND 1.0 0.33 03/18/22 21:41 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 03/18/22 21:41 1,1,2-Trichloroethane ug/L ND 1.0 0.32 03/18/22 21:41 1,1-Dichloroethane ug/L ND 1.0 0.37 03/18/22 21:41 1,1-Dichloroethene ug/L ND 1.0 0.35 03/18/22 21:41 1,1-Dichloropropene ug/L ND 1.0 0.43 03/18/22 21:41 1,2,3-Trichlorobenzene ug/L ND 1.0 0.81 03/18/22 21:41 1,2,3-Tiichloropropane ug/L ND 1.0 0.26 03/18/22 21:41 1,2,4-Trichlorobenzene ug/L ND 1.0 0.64 03/18/22 21:41 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 03/18/22 21:41 1,2-Dibromoethane(EDB) ug/L ND 1.0 0.27 03/18/22 21:41 1,2-Dichlorobenzene ug/L ND 1.0 0.34 03/18/22 21:41 1,2-Dichloroethane ug/L ND 1.0 0.32 03/18/22 21:41 1,2-Dichloropropane ug/L ND 1.0 0.36 03/18/22 21:41 1,3-Dichlorobenzene ug/L ND 1.0 0.34 03/18/22 21:41 1,3-Dichloropropane ug/L ND 1.0 0.28 03/18/22 21:41 1,4-Dichlorobenzene ug/L ND 1.0 0.33 03/18/22 21:41 2,2-Dichloropropane ug/L ND 1.0 0.39 03/18/22 21:41 2-Butanone(MEK) ug/L ND 5.0 4.0 03/18/22 21:41 2-Chlorotoluene ug/L ND 1.0 0.32 03/18/22 21:41 2-Hexanone ug/L ND 5.0 0.48 03/18/22 21:41 4-Chlorotoluene ug/L ND 1.0 0.32 03/18/22 21:41 4-Methyl-2-pentanone(MIBK) ug/L ND 5.0 2.7 03/18/22 21:41 Acetone ug/L ND 25.0 5.1 03/18/22 21:41 Benzene ug/L ND 1.0 0.34 03/18/22 21:41 Bromobenzene ug/L ND 1.0 0.29 03/18/22 21:41 Bromochloromethane ug/L ND 1.0 0.47 03/18/22 21:41 Bromodichloromethane ug/L ND 1.0 0.31 03/18/22 21:41 Bromoform ug/L ND 1.0 0.34 03/18/22 21:41 Bromomethane ug/L ND 2.0 1.7 03/18/22 21:41 Carbon tetrachloride ug/L ND 1.0 0.33 03/18/22 21:41 Chlorobenzene ug/L ND 1.0 0.28 03/18/22 21:41 Chloroethane ug/L ND 1.0 0.65 03/18/22 21:41 Chloroform ug/L ND 1.0 0.43 03/18/22 21:41 Chloromethane ug/L ND 1.0 0.54 03/18/22 21:41 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 03/18/22 21:41 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 03/18/22 21:41 Dibromochloromethane ug/L ND 1.0 0.36 03/18/22 21:41 Dibromomethane ug/L ND 1.0 0.39 03/18/22 21:41 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 31 l aceAnalytical a Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacstalts.com (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 METHOD BLANK: 3586658 Matrix: Water Associated Lab Samples: 92593649001,92593649003,92593649004,92593649005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.35 03/18/22 21:41 Diisopropyl ether ug/L ND 1.0 0.31 03/18/22 21:41 Ethylbenzene ug/L ND 1.0 0.30 03/18/22 21:41 Hexachloro-1,3-butadiene ug/L ND 2.0 1.5 03/18/22 21:41 m&p-Xylene ug/L ND 2.0 0.71 03/18/22 21:41 Methyl-tert-butyl ether ug/L ND 1.0 0.42 03/18/22 21:41 Methylene Chloride ug/L ND 5.0 2.0 03/18/22 21:41 v1 Naphthalene ug/L ND 1.0 0.64 03/18/22 21:41 o-Xylene ug/L ND 1.0 0.34 03/18/22 21:41 p-Isopropyltoluene ug/L ND 1.0 0.41 03/18/22 21:41 Styrene ug/L ND 1.0 0.29 03/18/22 21:41 Tetrachloroethene ug/L ND 1.0 0.29 03/18/22 21:41 Toluene ug/L ND 1.0 0.48 03/18/22 21:41 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 03/18/22 21:41 trans-1,3-Dichloropropene ug/L ND 1.0 0.36 03/18/22 21:41 Trichloroethene ug/L ND 1.0 0.38 03/18/22 21:41 Trichlorofluoromethane ug/L ND 1.0 0.30 03/18/22 21:41 Vinyl acetate ug/L ND 2.0 1.3 03/18/22 21:41 Vinyl chloride ug/L ND 1.0 0.39 03/18/22 21:41 Xylene(Total) ug/L ND 1.0 0.34 03/18/22 21:41 1,2-Dichloroethane-d4(S) % 103 70-130 03/18/22 21:41 4-Bromofluorobenzene(S) % 101 70-130 03/18/22 21:41 Toluene-d8(S) % 114 70-130 03/18/22 21:41 LABORATORY CONTROL SAMPLE: 3586659 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.1 102 70-130 1,1,1-Trichloroethane ug/L 50 50.2 100 70-130 1,1,2,2-Tetrachloroethane ug/L 50 52.0 104 70-130 1,1,2-Trichloroethane ug/L 50 53.8 108 70-130 1,1-Dichloroethane ug/L 50 49.9 100 70-130 1,1-Dichloroethene ug/L 50 50.6 101 70-132 1,1-Dichloropropene ug/L 50 51.8 104 70-131 1,2,3-Trichlorobenzene ug/L 50 53.3 107 70-134 1,2,3-Trichloropropane ug/L 50 49.7 99 70-130 1,2,4-Trichlorobenzene ug/L 50 53.0 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.8 100 70-132 1,2-Dibromoethane(EDB) ug/L 50 51.6 103 70-130 1,2-Dichlorobenzene ug/L 50 51.8 104 70-130 1,2-Dichloroethane ug/L 50 53.6 107 70-130 1,2-Dichloropropane ug/L 50 52.6 105 70-130 1 1,3-Dichlorobenzene ug/L 50 52.3 105 70-130 1,3-Dichloropropane ug/L 50 52.0 104 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 31 aceAnalytica! Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 LABORATORY CONTROL SAMPLE: 3586659 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 51.5 103 70-130 2,2-Dichloropropane ug/L 50 54.8 110 70-130 2-Butanone(MEK) ug/L 100 104 104 70-133 2-Chlorotoluene ug/L 50 52.3 105 70-130 2-Hexanone ug/L 100 97.2 97 70-130 4-Chlorotoluene ug/L 50 50.0 100 70-130 4-Methyl-2-pentanone(MIBK) ug/L 100 105 105 70-130 Acetone ug/L 100 105 105 70-144 1 Benzene ug/L 50 51.6 103 70-130 Bromobenzene ug/L 50 52.7 105 70-130 Bromochloromethane ug/L 50 50.4 101 70-130 Bromodichloromethane ug/L 50 53.9 108 70-130 Bromoform ug/L 50 51.3 103 70-131 Bromomethane ug/L 50 47.6 95 30-177 Carbon tetrachloride ug/L 50 53.4 107 70-130 Chlorobenzene ug/L 50 51.9 104 70-130 Chloroethane ug/L 50 47.3 95 46-131 Chloroform ug/L 50 51.2 102 70-130 Chloromethane ug/L 50 47.0 94 49-130 cis-1,2-Dichloroethene ug/L 50 52.2 104 70-130 cis-1,3-Dichloropropene ug/L 50 54.3 109 70-130 Dibromochloromethane ug/L 50 49.3 99 70-130 Dibromomethane ug/L 50 49.5 99 70-130 Dichlorodifluoromethane ug/L 50 52.3 105 52-134 Diisopropyl ether ug/L 50 49.3 99 70-131 Ethylbenzene ug/L 50 51.5 103 70-130 Hexachloro-1,3-butadiene ug/L 50 56.2 112 70-131 m&p-Xylene ug/L 100 104 104 70-130 Methyl-tert-butyl ether ug/L 50 48.8 98 70-130 Methylene Chloride ug/L 50 83.5 167 68-130 L1,v1 Naphthalene ug/L 50 53.3 107 70-133 o-Xylene ug/L 50 51.1 102 70-130 p-lsopropyltoluene ug/L 50 52.7 105 70-130 Styrene ug/L 50 52.3 105 70-130 Tetrachloroethene ug/L 50 50.9 102 70-130 Toluene ug/L 50 51.5 103 70-130 trans-1,2-Dichloroethene ug/L 50 51.6 103 70-130 trans-1,3-Dichloropropene ug/L 50 53.9 108 70-130 Trichloroethene ug/L 50 49.6 99 70-130 Trichlorofluoromethane ug/L 50 49.0 98 61-130 Vinyl acetate ug/L 100 107 107 70-140 Vinyl chloride ug/L 50 50.5 101 59-142 Xylene(Total) ug/L 150 155 103 70-130 1,2-Dichloroethane-d4(S) % 105 70-130 4-Bromofluorobenzene(S) % 99 70-130 Toluene-d8(S) % 103 70-130 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 31 1 Pace Analytical rvi Services,LLC 9800® tnnv.pacelabs.C� Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3586660 3586661 MS MSD 92594272005 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 23.0 22.1 115 110 70-135 4 30 1,1,1-Trichloroethane ug/L ND 20 20 23.3 22.7 116 114 70-148 2 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 22.8 22.7 114 114 70-131 0 30 1,1,2-Trichloroethane ug/L ND 20 20 22.1 21.6 111 108 70-136 2 30 1,1-Dichloroethane ug/L ND 20 20 22.8 22.5 114 112 70-147 1 30 1,1-Dichloroethene ug/L ND 20 20 22.8 22.2 114 111 70-158 3 30 1,1-Dichloropropene ug/L ND 20 20 24.0 23.0 120 115 70-149 4 30 1,2,3-Trichlorobenzene ug/L ND 20 20 22.3 20.3 111 102 68-140 9 30 1 2 3-Trichloro ro ane ug/L ND p p g 20 20 22.3 21.7 112 108 67-137 3 30 1,2,4-Trichlorobenzene ug/L ND 20 20 21.8 20.4 109 102 70-139 6 30 1,2-Dibromo-3- ug/L ND 20 20 20.7 19.5 104 98 69-136 6 30 chloropropane 1,2-Dibromoethane(EDB) ug/L ND 20 20 21.7 22.5 108 113 70-137 4 30 1,2-Dichlorobenzene ug/L ND 20 20 22.3 21.2 112 106 70-133 5 30 1,2-Dichloroethane ug/L ND 20 20 22.7 21.5 114 107 67-138 6 30 1,2-Dichloropropane ug/L ND 20 20 22.8 22.4 114 112 70-138 2 30 1,3-Dichlorobenzene ug/L ND 20 20 23.0 22.3 115 111 70-133 3 30 1,3-Dichloropropane ug/L ND 20 20 22.0 22.9 110 115 70-136 4 30 1,4-Dichlorobenzene ug/L ND 20 20 22.6 21.9 113 110 70-133 3 30 2,2-Dichloropropane ug/L ND 20 20 25.1 24.6 126 123 52-155 2 30 v2 2-Butanone(MEK) ug/L ND 40 40 43.5 42.1 109 105 61-147 3 30 2-Chlorotoluene ug/L ND 20 20 23.6 22.4 118 112 70-141 5 30 2-Hexanone ug/L ND 40 40 39.7 42.6 99 106 67-139 7 30 4-Chlorotoluene ug/L ND 20 20 22.8 21.7 114 108 70-135 5 30 4-Meth l-2- entanone Y P ug/L N D 40 g 40 41.9 40.2 105 101 67- 136 4 30 (MIBK) Acetone ug/L ND 40 40 44.6 41.2 111 103 55-159 8 30 Benzene ug/L ND 20 20 22.4 21.5 112 108 67-150 4 30 Bromobenzene ug/L ND 20 20 23.6 22.5 118 113 70-134 5 30 Bromochloromethane ug/L ND 20 20 22.2 21.9 111 109 70-146 2 30 Bromodichloromethane ug/L ND 20 20 22.4 21.8 112 109 70-138 3 30 Bromoform ug/L ND 20 20 21.7 21.7 109 109 57-138 0 30 Bromomethane ug/L ND 20 20 22.0 21.8 110 109 10-200 1 30 Carbon tetrachloride ug/L ND 20 20 23.6 23.0 118 115 70-147 2 30 Chlorobenzene ug/L ND 20 20 23.2 22.4 116 112 70-137 4 30 Chloroethane ug/L ND 20 20 23.7 23.7 118 119 51-166 0 30 Chloroform ug/L ND 20 20 23.3 22.8 117 114 70-144 2 30 Chloromethane ug/L ND 20 20 17.5 17.3 88 86 24-161 2 30 cis-1,2-Dichloroethene ug/L ND 20 20 23.8 23.0 119 115 67-148 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 22.1 21.4 111 107 70-142 3 30 Dibromochloromethane ug/L ND 20 20 21.7 21.0 109 105 68-138 3 30 Dibromomethane ug/L ND 20 20 21.6 21.0 108 105 70-134 3 30 Dichlorodifluoromethane ug/L ND 20 20 12.5 12.5 63 63 43-155 0 30 Diisopropyl ether ug/L ND 20 20 21.5 20.8 108 104 65-146 4 30 Ethylbenzene ug/L ND 20 20 23.7 23.2 119 116 68-143 2 30 Hexachloro-1,3-butadiene ug/L ND 20 20 23.9 22.5 120 113 62-151 6 30 Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 31 aceAnalyfical® Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 rr�rrr pt Nabstan (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 MATRIX SPIK E E&MATRIX SPIKE DUPLICATE: 3586660 3586661 MS MSD 92594272005 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 40 40 48.5 47.6 121 119 53-157 2 30 Methyl-tert-butyl ether ug/L ND 20 20 20.6 20.3 102 100 59-156 2 30 Methylene Chloride ug/L ND 20 20 23.0 22.6 115 113 64-148 1 30 Naphthalene ug/L ND 20 20 20.9 20.0 105 100 57-150 4 30 o-Xylene ug/L ND 20 20 23.3 22.5 116 113 68-143 3 30 p-Isopropyltoluene ug/L ND 20 20 23.5 22.4 118 112 70-141 5 30 Styrene ug/L ND 20 20 23.4 23.8 117 119 70-136 2 30 Tetrachloroethene ug/L ND 20 20 23.8 23.2 119 116 70-139 3 30 Toluene ug/L ND 20 20 22.4 21.8 112 109 47-157 3 30 trans-1,2-Dichloroethene ug/L ND 20 20 23.3 23.2 117 116 70-149 1 30 trans-1,3-Dichloropropene ug/L ND 20 20 22.0 21.0 110 105 70-138 4 30 Trichloroethene ug/L ND 20 20 22.3 22.0 112 110 70-149 1 30 Trichlorofluoromethane ug/L ND 20 20 21.9 21.5 110 108 61-154 2 30 Vinyl acetate ug/L ND 40 40 44.1 42.7 110 107 48-156 3 30 Vinyl chloride ug/L ND 20 20 19.4 19.2 97 96 55-172 1 30 Xylene(Total) ug/L ND 60 60 71.7 70.1 120 117 66-145 2 30 1,2-Dichloroethane-d4(S) % 105 107 70-130 4-Bromofluorobenzene(S) % 102 106 70-130 Toluene-d8(S) % 99 98 70-130 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 31 Pace Analytical Services,LLC 8 /t„,„ ,�'a 9800 Kincey Ave. Suite 100 CeAna�,jlc Huntersville,NC 28078 wwwpacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 QC Batch: 686235 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92593649002 METHOD BLANK: 3588044 Matrix: Water Associated Lab Samples: 92593649002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 03/22/22 13:05 1,1,1-Trichloroethane ug/L ND 1.0 0.33 03/22/22 13:05 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 03/22/22 13:05 1,1,2-Trichloroethane ug/L ND 1.0 0.32 03/22/22 13:05 1,1-Dichloroethane ug/L ND 1.0 0.37 03/22/22 13:05 1,1-Dichloroethene ug/L ND 1.0 0.35 03/22/22 13:05 1,1-Dichloropropene ug/L ND 1.0 0.43 03/22/22 13:05 1,2,3-Trichlorobenzene ug/L ND 1.0 0.81 03/22/22 13:05 IK 1,2,3-Trichloropropane ug/L ND 1.0 0.26 03/22/22 13:05 1,2,4-Trichlorobenzene ug/L ND 1.0 0.64 03/22/22 13:05 IK 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 03/22/22 13:05 1,2-Dibromoethane(EDB) ug/L ND 1.0 0.27 03/22/22 13:05 1,2-Dichlorobenzene ug/L ND 1.0 0.34 03/22/22 13:05 1,2-Dichloroethane ug/L ND 1.0 0.32 03/22/22 13:05 I 1,2-Dichloropropane ug/L ND 1.0 0.36 03/22/22 13:05 1,3-Dichlorobenzene ug/L ND 1.0 0.34 03/22/22 13:05 1,3-Dichloropropane ug/L ND 1.0 0.28 03/22/22 13:05 1,4-Dichlorobenzene ug/L ND 1.0 0.33 03/22/22 13:05 2,2-Dichloropropane ug/L ND 1.0 0.39 03/22/22 13:05 2-Butanone(MEK) ug/L ND 5.0 4.0 03/22/22 13:05 2-Chlorotoluene ug/L ND 1.0 0.32 03/22/22 13:05 2-Hexanone ug/L ND 5.0 0.48 03/22/22 13:05 4-Chlorotoluene ug/L ND 1.0 0.32 03/22/22 13:05 4-Methyl-2-pentanone(MIBK) ug/L ND 5.0 2.7 03/22/22 13:05 Acetone ug/L ND 25.0 5.1 03/22/22 13:05 Benzene ug/L ND 1.0 0.34 03/22/22 13:05 Bromobenzene ug/L ND 1.0 0.29 03/22/22 13:05 Bromochloromethane ug/L ND 1.0 0.47 03/22/22 13:05 I Bromodichloromethane ug/L ND 1.0 0.31 03/22/22 13:05 Bromoform ug/L ND 1.0 0.34 03/22/22 13:05 Bromomethane ug/L ND 2.0 1.7 03/22/22 13:05 Carbon tetrachloride ug/L ND 1.0 0.33 03/22/22 13:05 Chlorobenzene ug/L ND 1.0 0.28 03/22/22 13:05 Chloroethane ug/L ND 1.0 0.65 03/22/22 13:05 Chloroform ug/L ND 1.0 0.43 03/22/22 13:05 Chloromethane ug/L ND 1.0 0.54 03/22/22 13:05 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 03/22/22 13:05 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 03/22/22 13:05 Dibromochloromethane ug/L ND 1.0 0.36 03/22/22 13:05 Dibromomethane ug/L ND 1.0 0.39 03/22/22 13:05 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 31 Pace Analytical Services,LLC 9800 Kincey tical S aceAnalytical'31' e. Suite 100 Huntersville,NC 28078 wwn.acNNn ct>til (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 METHOD BLANK: 3588044 Matrix: Water Associated Lab Samples: 92593649002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.35 03/22/22 13:05 Diisopropyl ether ug/L ND 1.0 0.31 03/22/22 13:05 Ethylbenzene ug/L ND 1.0 0.30 03/22/22 13:05 Hexachloro-1,3-butadiene ug/L ND 2.0 1.5 03/22/22 13:05 IK m&p-Xylene ug/L ND 2.0 0.71 03/22/22 13:05 Methyl-tert-butyl ether ug/L ND 1.0 0.42 03/22/22 13:05 Methylene Chloride ug/L ND 5.0 2.0 03/22/22 13:05 Naphthalene ug/L ND 1.0 0.64 03/22/22 13:05 IK o-Xylene ug/L ND 1.0 0.34 03/22/22 13:05 p-lsopropyltoluene ug/L ND 1.0 0.41 03/22/22 13:05 Styrene ug/L ND 1.0 0.29 03/22/22 13:05 Tetrachloroethene ug/L ND 1.0 0.29 03/22/22 13:05 Toluene ug/L ND 1.0 0.48 03/22/22 13:05 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 03/22/22 13:05 trans-1,3-Dichloropropene ug/L ND 1.0 0.36 03/22/22 13:05 Trichloroethene ug/L ND 1.0 0.38 03/22/22 13:05 Trichlorofluoromethane ug/L ND 1.0 0.30 03/22/22 13:05 Vinyl acetate ug/L ND 2.0 1.3 03/22/22 13:05 Vinyl chloride ug/L ND 1.0 0.39 03/22/22 13:05 Xylene(Total) ug/L ND 1.0 0.34 03/22/22 13:05 1,2-Dichloroethane-d4(S) % 102 70-130 03/22/22 13:05 4-Bromofluorobenzene(S) % 104 70-130 03/22/22 13:05 Toluene-d8(S) % 103 70-130 03/22/22 13:05 LABORATORY CONTROL SAMPLE: 3588045 Spike LCS LCS °A°Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 47.8 96 70-130 1,1,1-Trichloroethane ug/L 50 54.9 110 70-130 1,1,2,2-Tetrachloroethane ug/L 50 47.5 95 70-130 1,1,2-Trichloroethane ug/L 50 51.0 102 70-130 1,1-Dichloroethane ug/L 50 50.3 101 70-130 I 1,1-Dichloroethene ug/L 50 51.5 103 70-132 1,1-Dichloropropene ug/L 50 54.8 110 70-131 1,2,3-Trichlorobenzene ug/L 50 46.6 93 70-134 IK 1,2,3-Trichloropropane ug/L 50 47.4 95 70-130 1,2,4-Trichlorobenzene ug/L 50 47.0 94 70-130 IK 1,2-Dibromo-3-chloropropane ug/L 50 46.2 92 70-132 1,2-Dibromoethane(EDB) ug/L 50 49.3 99 70-130 1,2-Dichlorobenzene ug/L 50 45.6 91 70-130 1 1,2-Dichloroethane ug/L 50 53.2 106 70-130 1,2-Dichloropropane ug/L 50 50.5 101 70-130 1,3-Dichlorobenzene ug/L 50 46.9 94 70-130 1,3-Dichloropropane ug/L 50 48.5 97 70-130 Results presented on this page are In the units indicated by the"units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 22 of 31 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 witw.pscslabs.ctas (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 LABORATORY CONTROL SAMPLE: 3588045 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 45.8 92 70-130 2,2-Dichloropropane ug/L 50 53.4 107 70-130 2-Butanone(MEK) ug/L 100 105 105 70-133 2-Chlorotoluene ug/L 50 46.7 93 70-130 2-Hexanone ug/L 100 91.3 91 70-130 4-Chlorotoluene ug/L 50 44.9 90 70-130 4-Methyl-2-pentanone(MIBK) ug/L 100 99.9 100 70-130 Acetone ug/L 100 99.7 100 70-144 Benzene ug/L 50 48.2 96 70-130 Bromobenzene ug/L 50 46.1 92 70-130 Bromochloromethane ug/L 50 50.8 102 70-130 Bromodichloromethane ug/L 50 49.8 100 70-130 Bromoform ug/L 50 46.0 92 70-131 Bromomethane ug/L 50 44.2 88 30-177 Carbon tetrachloride ug/L 50 53.1 106 70-130 Chlorobenzene ug/L 50 46.4 93 70-130 Chloroethane ug/L 50 59.9 120 46-131 Chloroform ug/L 50 51.0 102 70-130 Chloromethane ug/L 50 38.3 77 49-130 cis-1,2-Dichloroethene ug/L 50 52.5 105 70-130 cis-1,3-Dichloropropene ug/L 50 50.7 101 70-130 Dibromochloromethane ug/L 50 46.2 92 70-130 Dibromomethane ug/L 50 47.9 96 70-130 Dichlorodifluoromethane ug/L 50 46.7 93 52-134 Diisopropyl ether ug/L 50 51.8 104 70-131 Ethylbenzene ug/L 50 47.6 95 70-130 Hexachloro-1,3-butadiene ug/L 50 48.3 97 70-131 IK m&p-Xylene ug/L 100 94.2 94 70-130 Methyl-tert-butyl ether ug/L 50 57.1 114 70-130 Methylene Chloride ug/L 50 45.0 90 68-130 Naphthalene ug/L 50 47.0 94 70-133 IK o-Xylene ug/L 50 45.3 91 70-130 p-lsopropyltoluene ug/L 50 47.3 95 70-130 Styrene ug/L 50 46.0 92 70-130 Tetrachloroethene ug/L 50 44.1 88 70-130 Toluene ug/L 50 47.1 94 70-130 trans-1,2-Dichloroethene ug/L 50 51.5 103 70-130 trans-1,3-Dichloropropene ug/L 50 50.1 100 70-130 Trichloroethene ug/L 50 48.9 98 70-130 Trichlorofluoromethane ug/L 50 54.0 108 61-130 Vinyl acetate ug/L 100 108 108 70-140 Vinyl chloride ug/L 50 47.1 94 59-142 Xylene(Total) ug/L 150 139 93 70-130 1,2-Dichloroethane-d4(S) % 113 70-130 4-Bromofluorobenzene(S) °A) 101 70-130 Toluene-d8(S) % 99 70-130 Results presented on this page are In the units Indicated by the"units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 31 aceAnalytical® Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 mrrrr.yuelatbs con (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 MATRIX SPIKE SAMPLE: 3588047 92593935030 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 20.7 103 70-135 1,1,1-Trichloroethane ug/L ND 20 24.0 120 70-148 1,1,2,2-Tetrachloroethane ug/L ND 20 21.0 105 70-131 1,1,2-Trichloroethane ug/L ND 20 22.1 110 70-136 1,1-Dichloroethane ug/L ND 20 22.0 110 70-147 1,1-Dichloroethene ug/L ND 20 21.2 106 70-158 1,1-Dichloropropene ug/L ND 20 22.6 113 70-149 1,2,3-Trichlorobenzene ug/L ND 20 21.8 109 68-140 1K 1,2,3-Trichloropropane ug/L ND 20 20.6 103 67-137 1,2,4-Trichlorobenzene ug/L ND 20 22.1 110 70-139 1K 1,2-Dibromo-3-chloropropane ug/L ND 20 19.5 97 69-136 1,2-Dibromoethane(EDB) ug/L ND 20 21.9 110 70-137 1,2-Dichlorobenzene ug/L ND 20 20.4 102 70-133 1,2-Dichloroethane ug/L ND 20 23.7 119 67-138 1,2-Dichloropropane ug/L ND 20 22.1 111 70-138 1,3-Dichlorobenzene ug/L ND 20 20.8 104 70-133 1,3-Dichloropropane ug/L ND 20 20.9 104 70-136 1,4-Dichlorobenzene ug/L ND 20 20.6 103 70-133 2,2-Dichloropropane ug/L ND 20 23.8 119 52-155 2-Butanone(MEK) ug/L ND 40 41.7 104 61-147 2-Chlorotoluene ug/L ND 20 21.0 105 70-141 2-Hexanone ug/L ND 40 40.8 102 67-139 ' 4-Chlorotoluene ug/L ND 20 20.6 103 70-135 4-Methyl-2-pentanone(MIBK) ug/L ND 40 43.2 108 67-136 Acetone ug/L ND 40 43.1 108 55-159 Benzene ug/L ND 20 20.7 103 67-150 Bromobenzene ug/L ND 20 21.3 107 70-134 Bromochloromethane ug/L ND 20 21.9 110 70-146 Bromodichloromethane ug/L ND 20 22.2 111 70-138 Bromoform ug/L ND 20 20.5 103 57-138 Bromomethane ug/L ND 20 21.1 106 10-200 Carbon tetrachloride ug/L ND 20 23.7 118 70-147 Chlorobenzene ug/L ND 20 20.8 104 70-137 1 Chloroethane ug/L ND 20 20.6 103 51-166 v1 Chloroform ug/L ND 20 22.6 113 70-144 Chloromethane ug/L ND 20 11.6 58 24-161 cis-1,2-Dichloroethene ug/L ND 20 23.3 116 67-148 cis-1,3-Dichloropropene ug/L ND 20 21.3 106 70-142 Dibromochloromethane ug/L ND 20 19.0 95 68-138 Dibromomethane ug/L ND 20 21.0 105 70-134 Dichlorodifluoromethane ug/L ND 20 5.5 28 43-155 M1 Diisopropyl ether ug/L ND 20 21.9 110 65-146 Ethylbenzene ug/L ND 20 21.5 108 68-143 Hexachloro-1,3-butadiene ug/L ND 20 24.0 120 62-151 IK m&p-Xylene ug/L ND 40 43.3 108 53-157 Methyl-tert-butyl ether ug/L ND 20 22.4 112 59-156 Methylene Chloride ug/L ND 20 20.2 101 64-148 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 24 of 31 Pace Analytical Services,LLC aceAnalytical a 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.coe (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 MATRIX SPIKE SAMPLE: 3588047 92593935030 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Naphthalene ug/L ND 20 21.0 105 57-150 1K o-Xylene ug/L ND 20 21.0 105 68-143 p-lsopropyltoluene ug/L ND 20 21.9 110 70-141 Styrene ug/L ND 20 20.3 101 70-136 Tetrachloroethene ug/L ND 20 19.6 98 70-139 Toluene ug/L ND 20 21.6 108 47-157 trans-1,2-Dichloroethene ug/L ND 20 22.4 112 70-149 trans-1,3-Dichloropropene ug/L ND 20 21.9 110 70-138 Trichloroethene ug/L ND 20 22.0 107 70-149 Trichlorofluoromethane ug/L ND 20 21.3 106 61-154 Vinyl acetate ug/L ND 40 42.6 106 48-156 Vinyl chloride ug/L ND 20 13.7 69 55-172 Xylene(Total) ug/L ND 60 64.3 107 66-145 1,2-Dichloroethane-d4(S) % 107 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 102 70-130 SAMPLE DUPLICATE: 3588046 92593935023 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichlorobenzene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane(EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone(MEK) ug/L ND ND 30 2-Chlorotoluene ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Chlorotoluene ug/L ND ND 30 4-Methyl-2-pentanone(MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 31 aceAnalytical® Pace Analytical Services,LLC winspacelabs 9800 KinceyAve. Suite 100 Huntersville,NC 28078 �� (704)875-9092 QUALITY CONTROL DATA Project: TRYON&MOREHEAD DEVELOPMENT 1 Pace Project No.: 92593649 SAMPLE DUPLICATE: 3588046 92593935023 Dup Max Parameter Units Result Result RPD RPD Qualifiers Benzene ug/L ND ND 30 I Bromobenzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 v1 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 1 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Diisopropyl ether ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 m&p-Xylene ug/L ND ND 30 Methyl-tert-butyl ether ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 o-Xylene ug/L ND ND 30 P P PY ug/L ro (toluene u /L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans-1,3-Dichloropropene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 Xylene(Total) ug/L ND ND 30 1,2-Dichloroethane-d4(S) % 106 101 4-Bromofluorobenzene(S) % 105 100 Toluene-d8(S) % 104 102 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 26 of 31 Pace Analytical Services,LLC Q�►�� tic 9800 Kincey Ave. Suite 100 CGI na is l Huntersville,NC 28078 tnnr pcNebs can (704)875-9092 QUALIFIERS Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s)did not meet method acceptance criteria;this result should be considered an estimated value. L1 Analyte recovery in the laboratory control sample(LCS)was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. v1 The continuing calibration verification was above the method acceptance limit.Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit.The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 31 Pace Analytical Services,LLC (iff-ce Atom 9800 Kincey Ave. Suite 100 liliHl I ti Huntersville,NC 28078 www.pacelabs,com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: TRYON&MOREHEAD DEVELOPMENT Pace Project No.: 92593649 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92593649001 B-105 EPA 3010A 685432 EPA 6020B 685567 92593649002 B-106 EPA 3010A 685432 EPA 6020B 685567 92593649003 B-108 EPA 3010A 685432 EPA 6020B 685567 92593649004 B-110 EPA 3010A 685432 EPA 6020B 685567 92593649005 8-112 EPA 3010A 685432 EPA 6020B 685567 92593649001 B-105 EPA 8260D 685904 92593649002 B-106 EPA 8260D 686235 92593649003 8-108 EPA 8260D 685904 92593649004 8-110 EPA 8260D 685904 92593649005 8-112 EPA 8260D 685904 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/23/2022 03:08 PM without the written consent of Pace Analytical Services,LLC. Page 28 of 31 (11 Document Name: Document Revised:November 15,2021 aceAna! lCa�� Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR C5 033 Rev.08 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood n Huntersville RI Raleigh Mechanicsville❑ Atlanta❑ Kernersvllle❑ Sample Condition Client Name: W0# • 92593649 Upon Receipt �f' lei) 611(Aptife A c Project ■ Courier: ❑Fed Ex ['UPS DUSPS ['Client 111111 I 1111 I I II 11111 III 0 Commercial DOthe Pace Other: 92593649 Custody Seal Present? Dyes %No Seals Intact? Des FINo Date/Initials Person Examining Contents:3 112 Packing Material: (Bubble Wrap Rfaubble Bags ❑None 0 Other Biological Tissue Frozen? Thermometer: /� Wet Delue ❑None � Eves ❑No jai/A gl IR Gun ID: Q Trc64 Type of Ice: • Correction Factor: Cooler Temp: l• Add/Subtract(°Cj v 4 v Temp should be above freezing to 6•C ❑Samples out of temp criteria.Samples on ice,cooling process Cooler Temp-Correctedj'C). r has ks USDA Regulated Soli('4 N/A,water sample) Did samples originate in a quarantine zone.within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally, Des No Including Hawaii and Puerto Rico)?Des QNo .CommenteJolscrepancy: Chain of Custody Present? ®Yes Olio ❑N/A 1. Samples Arrived within Hold Time? erns Onto ❑N/A 2. Short Hold Time Analysis(c72 hr.)? Ores giro ❑N/A 3. _Rush Turn Around Time Requested? ( Yes ONE, ON/A 4. Sufficient Volume? eves ❑No ON/A S. Correct Containers Used? j$)Yes ❑No QN/A 6. -Pace Containers Used? 4Yes ❑No ❑N/A Containers Intact? EYes ❑No UN/A 7. Dissolved analysis:Samples Field Filtered? MYes ❑No ON/A 8. Sample Labels Match COC? ArYes Otto ❑N/A 9. -Indudes Date/Time/ID/Analysis Matrix: W Headspace in VOA Vials(>5.6mm)? DYes No ON/A _ Trip Blank Present?. Over � 10. No LIN/A . 11. Trip Blank Custody Seals Present? DYes Otto 'j[EN/A 1 COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes ❑No Lot ID of split containers: CUENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: - Date: Page 29 of 31 Document Name: Document Revised;November 15,2021 Sample Condition Upon Receipt(SOUR) Page 2 of 2 (2eAnatytical- Document No.: Issuing Authority: F-CAR-CS-033-Rev.08 Pace Carolinas.Quality Office i *Check mark top half of box if pH and/or dechlorination is Project f WO# 9259 verified and within the acceptance range for preservation 92593649 _ samples. PH: ATF Due Date: 03/23/22 Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015(water)DOC,LLHg CLIENT: 92-Terrae NC **Bottom half of box is to list number of bottles ..▪ Z Z V. _ Om E Z z F. a 2-3 �' a ... T. N °a A 7 Z v z ? 1✓ a a It °� z m 2 Z g E. I. Ti. Z T, N z • S < p Z N u ar N C m .�, v a Z z . Y i1 z z °' — azi iN q 1 u 'a A c e c c. "i z z 0 c t `" Q E. rA, : 3 v�i j ro � Z e o c V .. 4 j = 2 N z .2 S T. iv x z J ri 4 c ran .'L .L . a g ° ' iq oar < a (<< ! g E E 2 J J J A.-- J __,'2` G is < Q Al J9 T 3 a vi Q o o E E E t 4 cE� E E E E E a E E E N ry +� .i J v I°I m h N g N .y g m $ 8 a m i i \m 3 a a i • a o > L tit, > 8i 9" m W i. \'''' .. . \ . \ \...3 . . . 2 \ II 3 \ 1 J \ 3 ' \. \ 3 ti \—\ - 7 N 8 \ 9 \ ' i \ -10 11 \ ,\ ' \ \ ' . \ 12 \ pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot a adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(I.e. Out of hold,incorrect preservative,out of temp,Incorrect containers, Page 30 of 31 is n I( g'g g)� � ns :. ,I cp +r O 0 a w �Iv .+ ITEM# d m 3 a X I 1 ii Niiy'. "� CA60 a•�r a g. n 2 a l -�—_ gz � ti -ia !trig _. Q d O o z g ji'hdk N d Do Fi7 C.f) :° " c� f o g n 6 D a = �{ y CD. '• I. n r ,2 8 a . • `vN i Sya-° m & ff m 3 1f ° is dilip� $?g2.2-g24f a 1 Ilk if � g 3 . v v A o �°) in))yOV1 � � a � C. a Atic O a s \ 70 I i 4�----- MATRIX CODE (see valid codes to left) r .1_ SAMPLE TYPE (G--GRAB C-COMP) g T 5 g. \a o 0 N" i. ,,t rn _ _ _ , R O "' k U [Jt O m or nr1. a a kh''iEii m 8 rn 9 (15 _ '414, S_.._ \ y b = Z h t gab C1 N m " n rp r' t4 "'y'rii , ., SAMPLE TEMP ATCOLLEC11oN oe 0 ,� � - A OF CONTAINERS a o 3 A - $.. _ W PEA Unpreserved y _ m �� f /As H2SO4 )Q .Z 3 n m r-01 '"-1 L g:U1 t! 03 .. r g D INIig I IR • m a� li Methanol 3 w _ I Other• Q ¢ g ➢ to 'i` '4 -0000-e;'3kat, Y1$ ;i! g < a70 9 1 k k ) S..: >4 6260. +y' m = y yj " -�' �'G Sf, a 6020 Fe o `n ,, C 3 Cm T. a) K.3iid 0' a N ;ii�' r 3 N , O ftg4. UI . „,,,,.., . . _ , . 0) Io- Cl j-ji Residual Choine(YIN) ;t h' �\ z w N k a ',II', , �;.+ N a 1 Page 31 of 31 APPENDIX D TREATMENT SYSTEM SPECIFICATIONS ... --t . -i t i ', .1't .:,.-..-..';',.— r. - ;,,T4T,L, i. ,-,-. i la ° $11[B. 4 17 1 1 ! 6 ) _ _ _1_ _ PPi w,� _ _I - _ir :. r :: - -4—) ii IN a C -li _ _ 3 rIr_f- ! I_____ r 3 0 ELEVATION PLAN kiATERI-LE OF CONSTRUCTIONPP 8-1E, PEN Jc'ry ()UADPLEi: IGG BAG FILTERS - 504L STMIIILESS STEEL E:+G FILTER SLID PIPE - SCH SO PVC BALL VAL"ES - PVC_ TRUE-UNION BALL PP'''M0 "'E' SKID - SA-36 WELDED STEEL (PAII`1TED) pro.:-;;g_�,uSur.� -,x corporation PRESSURE GAGE - 0-60 PSIG ri, -! .p.{;:g=;°';j,+: HARDWARE - ASTP1 A307 Gr B (PLATED) DP"e e S AN S. ELE\'ATI 'I i �E �._ A.! ,EF--1001 1-0 JHTE rilliiiiii.Mak I t 0 ill 0 i •, , T 1 III 9 W/ C A.,I C T l 4,II,,, III - I L 1 (� j 45. ` NI I: I I I 0 IIII i I 5 I o O o 1 I 1 J /B 8'24/10 1 I1EIF, I JB 1/20/04 I-I_ L -- 7 ,I 1 -- PR GATE VESSEL STA\ DARDS VESSEL MATERIALS SA 516 70 LIQUID DRAIN ASSEMBLY : CARBON STEEL BALL>. IGG LINING : EPDXY VOLUME OF VESSEL . 400 FT' J N' EXTERIOR PAINT . EPDXY BASE /URETHANE TOP STANDARD/MAX rARRO8! FII I . 8.000 LBS /10,'1^ I PA o?;L,cs"�e^ '" corporation HEAD THICKNESS 5/16" CODE F&D SHIP WT. OPE' 14,500 LBS sPR.— iis""eg` RAWN BY JB SHELL THICKNESS : 5/16" 516 - 70 MAX. OP _ . 50 P 10 BY eL INTERNALS : PVC MAY IT 7'' 1401 eY BI. 1 ADSORBENT OUTLET ASSEMBLY . 14" X 18"MANWAY J,I I LI'u, 111FFIGG TIGG 5DR 0830 Reactivated Liquid Phase Coal Based Activated Carbon www.TIGG.com DESCRIPTION TIGG 5DR 0830 granular activated carbon made from selected grades of bituminous coal, which has been thermally reactivated. Depending upon the application, this activated carbon can provide performance similar to virgin activated carbon at a reduced cost. TYPICAL PROPERTIES TIGG 5DR 0830 U.S Sieve, 90 wt% min 8 x 30* Iodine Number, mg/g 750 Apparent Density, (dense packing) g/cc 0.45 - 0.55 lbs/ft3 28 - 34 Moisture -wt% max (as packed) 2 Abrasion No. - min 70 1 *Size 840 is also available TYPICAL APPLICATIONS This activated carbon can be used to remove: • BTEX and other organic compounds from ground water. • Organic compounds from wastewater and potable water. • Trace organics from process streams such as alcohols, glycerine, MEA, acids, etc Standard packaging of the activated carbon is in 50 pound bags or 1000 pound supersacks. Wet drained activated carbon adsorbs oxygen from the air. Therefore, when workers need to enter a vessel containing wet activated carbon, they should follow confined space/low oxygen level procedures. Activated carbon dust does not present an explosion hazard. 800-925-0011 I TIGG, LLC Purifying Air & Water www.TlGG.com 1 Willow Avenue www.TlGGtanks.com Oakdale, PA 15071 APPENDIX E CHARLOTTE MECKLEBURG CORRESPONDENCE / / / Charlotte-Mecklenburg / / 1 STORM WATER StormWater.CharMeck.org j Services M June 6,2022 NC Department of Environmental Quality Mooresville Regional Office Division of Water Resources-Water Quality Permitting Unit 610 East Center Avenue Suite 301 Mooresville,NC 28115 Subject: NPDES Permit Application-request to discharge into the City of Charlotte municipal stormwater system at 1111 South Tryon Street in Charlotte,NC Division of Water Resources: Regarding Terracon's request on behalf of Morehead Tryon Land LP in their NPDES permit application to discharge treated water from a remediation system at the above-referenced location into Charlotte's stormwater system,Charlotte Mecklenburg Storm Water Services(CMSWS) approves the discharge. CMSWS would like to make the permittee and NC DEQ aware of the following considerations and information: • CMSWS reserves the right to access,inspect,sample,and review documentation regarding the groundwater treatment system at any time. • In the event of an illicit discharge,bypass,or exceedance of permit discharge limits, Morehead Tryon Land LP Or its consultant shall immediately notify CMSWS and immediately implement corrective actions. • CMSWS reserves the right to rescind approval to discharge to the City of Charlotte's MS4 for due cause including gross improper operation of the system,and established trend of discharge limit exceedances,failure to provide notification of illicit discharges,system bypasses,and similar reasons. • CMSWS does not guarantee adequate capacity is available to permitted dischargers to keep any property or street free of water or harm as a result of this discharge. It is recommended that if discharge flows are anticipated to be high,the discharger should avoid discharging during wet weather. • CMSWS takes no responsibility for backflows from the public drainage system into the permitted discharger's system. If you have any questions or concerns,please contact Andrew DeCristofaro at(704) 517-8771. • ©� C2 45 Sunk Avenue MIX 600 East Qh street C:hopOtiP, NC 7870P, CnaAotte.NC 282(Y2 char$ottenc.gov Division of Water Resources June 6,2022 Page 2 Sincerely, Andrew DeCristofaro Water Quality Program Specialist cc: William Frazier,Terracon Consultants Robert Brookshire,Terracon Consultants