WQ0010583_Additional Information Response_20220405

1
Plummer,Lauren
From:Brent Collins <[e-mail]>
Sent:Tuesday, April 5, 2022 7:06 AM
To:Plummer,Lauren; Lambert, Johnny
Cc:Thornburg, Nathaniel; Snider, Lon; Graznak, Jenny; Caudle, Caitlin; 'Roy Whitaker'
Subject:[External] RE: WQ0010583 - Davie County Class B Residuals Program - Additional Information
Request #2
Attachments:RLAP-06-16.pdf; Davie - Weighted Average Worksheet.pdf; 06.10.21 Cleanout Total.PDF; 03.16.22
Digester Total.PDF
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to 
Report Spam. 

Lauren, 
We have remeasured the basin and are estimating there are approximately 1,371,075 gallons in the basin to clean out. 
We will have to dilute the material to get it out and able to be land applied so we are estimating 2.8 million gallons. This 
is a different material than what is land applied from the digester. There is a lot of mud mixed in with the material, 
making the percent solids higher, but the nitrogen lower. I sent the analysis of this material with the permit renewal but 
was requested to refigure the forms using the digester analysis. The calculations are as follows for the two analyses: 

Cooleemee Digester       ‐              28.88 lbs PAN per dry ton 
Cooleemee Cleanout     ‐              5.02 lbs PAN per dry ton 

Using the calculations for just the digester, on paper it would seem that we are applying a lot more PAN than we are 
actually going to be applying. We would be able to apply more of the mud/mixed material leading to higher dry tons, 
while being able to use the same acreage. I have refigured the forms using a weighted average of the most recent 
analyses of the cleanout material and the digester material. I have included the calculations and the analyses. Please let 
me know if you have any questions. 

‐‐ 
Brent Collins 
Director of Technical Services 
EMA Resources Inc. 

From: Plummer,Lauren <[e-mail]>  
Sent: Friday, April 1, 2022 1:49 PM 
To: Lambert, Johnny <[e-mail]>; [e-mail] 
Cc: Thornburg, Nathaniel <[e-mail]>; Snider, Lon <[e-mail]>; Graznak, Jenny 
<[e-mail]>; Caudle, Caitlin <[e-mail]> 
Subject: WQ0010583 ‐ Davie County Class B Residuals Program ‐ Additional Information Request #2 

Mr. Lambert, 

Division of Water Resources’ Central and Regional Office staff have reviewed the application package and additional 
information response submittal for the above referenced project.  Additional information is required before the review 
may be completed.  Please address the items identified in the attachment no later than the close of business on May 2, 
2022.    

2
Please be aware that failure to provide the requested information within the 30‐day time frame may result in your 
application being returned as incomplete.  If you have any questions or concerns regarding this request, please do not 
hesitate to contact me via email.   

Sincerely, 

Lauren Raup-Plummer, PE
Environmental Engineer III
Non-Discharge Branch
Department of Environmental Quality

919-707-3660 office
[e-mail]

512 N. Salisbury St
1617 Mail Service Center
Raleigh, NC 27699-1617

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

Effective April 6, 2022, the Non‐Discharge Branch is below half‐staff.  As a result, our response and review times will 
be slower than normal.  Thank you in advance for your patience. 

FORM: RLAP 06-16 Page 2 of 5
III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility’s physical address: 175 Hwy 801 South
City: Cooleemee State: NC Zip: 27014-
Coordinates: Latitude: 35○ 48′ 15″ Longitude: 80○ 33′ 40″
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
2. County where residuals land application program is headquartered: Davie
3. List the Operator In Responsible Charge (ORC) and all Back-Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation Name Affiliation Certification Number
ORC Roy Whitaker EMA Resources Inc. 13283
Back-Up ORC Brent Collins EMA Resources Inc. 27651
Additional Back-Up
ORCs
(if applicable)

If an ORC and at least one Back-Up ORC are not currently designated for this residuals land application program, provide the
candidates’ names, affiliations, and an estimated time schedule for each candidate’s completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source-generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 2817 dry tons per year.

PAN Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface Incorporation
or Injection
Surface Incorporation
or Injection
First-Year 7.69 10.23 21656 28812
Five-Year Maximum Adjusted 10.62 13.16 29920 37071
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category Use Acres Comments
Crops Forest or Plantation 0
Row Crops 36.78
Hay/Pasture 142.92

Total: 179.7
Methods Surface 179.7
Incorporation or Injection 0
Total: 179.7

FORM: RLAP 06-16 Page 3 of 5
c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac-yr)
Acres Required Using
First-Year PAN Concentrations

Acres Required Using
Five-Year Maximum Adjusted PAN
Concentrations
Surface Incorporation or
Injection
Surface Incorporation or
Injection
50 433 576 598 741
100 217 288 299 371
150 144 192 200 247
200 108 144 149 185
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.):
7. Specify type of residuals program (See Instruction F): Non-dedicated Dedicated
If Dedicated, specify the following (check all that apply):
Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
Land Application Siite
Certification.doc

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

6/22/2021

EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028

Ref: Analytical Testing
Lab Report Number: 21-162-0021
Client Project Description: Cooleemee/NC

Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 6/11/2021 for the analyses presented in the following report.

The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.

The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.

Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.

The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.

Please do not hesitate to contact me or client services if you have any questions or need additional information.

Sincerely,
Danyale Love
Project Manager
Page 1 of 7
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202240750State ProgramAlabama
02/07/202288-0650State ProgramArkansas
06/30/20212904State ProgramCalifornia
06/30/2021E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202104015State ProgramGeorgia
10/10/2021200078State Program - NELAPIllinois
06/30/202180215State ProgramKentucky
12/31/2021KY90047State ProgramKentucky
12/31/2021LA037State Program - NELAPLouisiana
06/30/202104015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
12/31/2021415State ProgramNorth Carolina
08/31/20219311State ProgramOklahoma
05/31/202268-03195State Program - NELAPPennsylvania
06/30/202184002State ProgramSouth Carolina
06/30/202184002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
10/31/20214313.01A2LA ISO 17025:2017Tennessee
09/30/2021T104704180State Program - NELAPTexas
06/30/202100106State ProgramVirginia
09/14/2021460181State Program - NELAPVirginia
Page 1 of 1 00001/21-162-0021
Page 2 of 7
Report Number:
Sample Summary Table
Client Project Description:
21-162-0021
Cooleemee/NC
Lab No Client Sample ID Matrix Date Collected Date Received
06/10/2021 07:00Solids 95746 Davie County 06/11/2021
Page 3 of 7
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27028
21-162-0021
46245
EMA Resources Inc
755 Yadkinville Rd
Mr. Brent Collins
Mocksville
Danyale Love
Project Manager
Received : 06/11/2021
Cooleemee/NC
Report Date : 06/22/2021
Sample ID :
Lab No :
Sampled:Davie County
95746 Matrix:
6/10/2021 7:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
84.8 %0.010Moisture 1 06/14/21 16:42 SW-DRYWTFMM
2410 mg/Kg - dry 105 658
Ammonia Nitrogen 1 06/17/21 15:00 4500NH3C-2011JPJ
127 mg/Kg - dry 32.6 32.6
Nitrate+Nitrite-N 1 06/15/21 14:50 4500NO3F-2011ZBD
3928 mg/Kg - dry 657.9Organic N 1 06/17/21 15:00 CALCULATION
7.1 s.u.pH 1 06/17/21 16:00 9045DDRS
15.2 %0.010 0.010
Total Solids 1 06/14/21 16:42 2540G-2011FMM
23.1 %0.010 0.010
Total Volatile Solids 1 06/14/21 16:42 2540G-2011FMM
6340 mg/Kg - dry 329Total Kjeldahl Nitrogen 1 06/18/21 13:26 4500NORGD-2011CLP
4390 mg/Kg - dry 18.2 32.9
Phosphorus 1 06/16/21 23:40 6010DTJS
48900 mg/Kg - dry 30.4 32.9
Aluminum 1 06/16/21 23:40 6010DTJS
6.12 mg/Kg - dry 1.58 3.29
Arsenic 1 06/16/21 23:40 6010DTJS
2.24 mg/Kg - dry 0.132 0.658
Cadmium 1 06/16/21 23:40 6010DTJS
4030 mg/Kg - dry 255 329
Calcium 1 06/16/21 23:40 6010DTJS
59.7 mg/Kg - dry 1.55 1.64
Chromium 1 06/16/21 23:40 6010DTJS
103 mg/Kg - dry 2.04 3.29
Copper 1 06/16/21 23:40 6010DTJS
134000 mg/Kg - dry 280 329
Iron 5 06/17/21 18:21 6010DTJS
31.8 mg/Kg - dry 1.18 1.97
Lead 1 06/16/21 23:40 6010DTJS
3050 mg/Kg - dry 17.0 32.9
Magnesium 1 06/16/21 23:40 6010DTJS
796 mg/Kg - dry 2.14 3.29
Manganese 1 06/16/21 23:40 6010DTJS
0.388 mg/Kg - dry 0.0450 0.103
Mercury 1 06/14/21 13:24 7471ADDB
3.44 mg/Kg - dry 0.888 1.64
Molybdenum 1 06/16/21 23:40 6010DTJS
25.9 mg/Kg - dry 0.789 1.64
Nickel 1 06/16/21 23:40 6010DTJS
2140 mg/Kg - dry 40.7 65.8
Potassium 1 06/22/21 02:13 6010DJTR
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 4 of 7
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27028
21-162-0021
46245
EMA Resources Inc
755 Yadkinville Rd
Mr. Brent Collins
Mocksville
Danyale Love
Project Manager
Received : 06/11/2021
Cooleemee/NC
Report Date : 06/22/2021
Sample ID :
Lab No :
Sampled:Davie County
95746 Matrix:
6/10/2021 7:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<2.11 mg/Kg - dry 2.11 3.29
Selenium 1 06/16/21 23:40 6010DTJS
655 mg/Kg - dry 85.5 164
Sodium 1 06/16/21 23:40 6010DTJS
390 mg/Kg - dry 5.33 8.22
Zinc 1 06/16/21 23:40 6010DTJS
3120 mg/Kg - dry 34.1 65.8
Sulfur 1 06/16/21 23:40 6010DTJS
0.73 Ratio 0.01 0.01
Sodium Absorption Ratio 1 06/16/21 23:40 CALCULATION
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Page 5 of 7
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-162-0021
EMA Resources Inc
46245
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:T101
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Makayla Weaver Date & Time:06/11/2021 09:51:20
Special precautions or instructions included?
Comments:
Page 6 of 7
Page 7 of 7

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/28/2022

EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028

Ref: Analytical Testing
Lab Report Number: 22-077-0020
Client Project Description: Cooleemee, NC

Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 3/18/2022 for the analyses presented in the following report.

The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.

The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.

Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.

The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.

Please do not hesitate to contact me or client services if you have any questions or need additional information.

Sincerely,
Connie Cook
Project Manager
Page 1 of 8
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20222904State ProgramCalifornia
06/30/2022E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202204015State ProgramGeorgia
10/10/2022200078State Program - NELAPIllinois
06/30/202280215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202204015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
12/31/2022415State ProgramNorth Carolina
05/31/202268-03195State Program - NELAPPennsylvania
06/30/202284002State ProgramSouth Carolina
06/30/202284002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202200106State ProgramVirginia
09/14/2022460181State Program - NELAPVirginia
Page 1 of 1 00001/22-077-0020
Page 2 of 8
Report Number:
Sample Summary Table
Client Project Description:
22-077-0020
Cooleemee, NC
Lab No Client Sample ID Matrix Date Collected Date Received
03/16/2022 06:30Solids 92406 Cooleemee 03/18/2022
Page 3 of 8

Client: EMA Resources Inc CASE NARRATIVE
Project: Cooleemee, NC
Lab Report Number: 22-077-0020
Date: 3/25/2022

Metals Analysis Method 6010D
Sample 98890 (Mull Bottom)
Analyte: Iron
QC Batch No: L606777/L605969
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.

Sample 98890 (Mull Bottom)
Analyte: Potassium
QC Batch No: L607078/L605969
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.

Solids Total Mercury Analysis - CVAA Method 7471A
Sample 57193 (4 day composite)
Analyte: Mercury
QC Batch No: L606654/L605971
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected

Page 4 of 8
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27028
22-077-0020
46245
EMA Resources Inc
755 Yadkinville Rd
Mr. Brent Collins
Mocksville
Connie Cook
Project Manager
Received : 03/18/2022
Cooleemee, NC
Report Date : 03/28/2022
Sample ID :
Lab No :
Sampled:Cooleemee
92406 Matrix:
3/16/2022 6:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
96.4 %Moisture 1 03/22/22 17:42 SW-DRYWTFMM
3560 mg/Kg - dry 444 2780
Ammonia Nitrogen 1 03/25/22 08:50 4500NH3C-2011JPJ
<136 mg/Kg - dry 136 136
Nitrate+Nitrite-N 1 03/22/22 14:34 4500NO3F-2016ZBD
41720 mg/Kg - dry 5139Organic N 1 03/25/22 08:50 CALCULATION
6.7 s.u.pH 1 03/25/22 14:30 9045DADM
3.57 %0.010 0.010
Total Solids 1 03/22/22 17:42 2540G-2011FMM
63.6 %0.010 0.010
Total Volatile Solids 1 03/22/22 17:42 2540G-2011FMM
45300 mg/Kg - dry 5140Total Kjeldahl Nitrogen 1 03/25/22 16:04 4500NORGD-2011CLP
17300 mg/Kg - dry 76.7 139
Phosphorus 1 03/24/22 01:43 6010DEAL
22600 mg/Kg - dry 128 139
Aluminum 1 03/24/22 01:43 6010DEAL
51.4 mg/Kg - dry 6.67 13.9
Arsenic 1 03/24/22 01:43 6010DEAL
1.61 J
mg/Kg - dry 0.556 2.78
Cadmium 1 03/24/22 01:43 6010DEAL
13000 mg/Kg - dry 1080 1390
Calcium 1 03/25/22 02:08 6010DEAL
37.2 mg/Kg - dry 6.56 6.94
Chromium 1 03/24/22 01:43 6010DEAL
542 mg/Kg - dry 8.61 13.9
Copper 1 03/24/22 01:43 6010DEAL
41700 mg/Kg - dry 237 278
Iron 1 03/24/22 01:43 6010DEAL
47.8 mg/Kg - dry 5.00 8.33
Lead 1 03/24/22 01:43 6010DEAL
2730 mg/Kg - dry 71.7 139
Magnesium 1 03/24/22 01:43 6010DEAL
2380 mg/Kg - dry 9.03 13.9
Manganese 1 03/24/22 01:43 6010DEAL
2.71 mg/Kg - dry 0.185 0.425
Mercury 1 03/23/22 13:11 7471AZMT
6.31 J
mg/Kg - dry 3.75 6.94
Molybdenum 1 03/24/22 01:43 6010DEAL
26.8 mg/Kg - dry 3.33 6.94
Nickel 1 03/24/22 01:43 6010DEAL
2810 mg/Kg - dry 172 278
Potassium 1 03/24/22 01:43 6010DJTR
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 8
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27028
22-077-0020
46245
EMA Resources Inc
755 Yadkinville Rd
Mr. Brent Collins
Mocksville
Connie Cook
Project Manager
Received : 03/18/2022
Cooleemee, NC
Report Date : 03/28/2022
Sample ID :
Lab No :
Sampled:Cooleemee
92406 Matrix:
3/16/2022 6:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<8.89 mg/Kg - dry 8.89 13.9
Selenium 1 03/24/22 01:43 6010DEAL
2500 mg/Kg - dry 361 694
Sodium 1 03/25/22 02:08 6010DEAL
1800 mg/Kg - dry 22.5 34.7
Zinc 1 03/24/22 01:43 6010DEAL
8080 mg/Kg - dry 144 278
Sulfur 1 03/24/22 01:43 6010DEAL
0.98 Ratio 0.01 0.01
Sodium Absorption Ratio 1 03/24/22 01:43 CALCULATION
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 6 of 8
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-077-0020
EMA Resources Inc
46245
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:T102
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Makayla Weaver Date & Time:03/18/2022 09:14:33
Special precautions or instructions included?
Comments:
Page 7 of 8
Page 8 of 8
First YearSURFACEPlant NamePAN/dtWeighted AverageCooleemee28.88 3.23Cleanout5.02 4.460.000.00Total7.69Pounds of Pan Per Year21656INJECTIONPlant NamePAN/dtWeighted AverageCooleemee32.44 3.63Cleanout7.43 6.600.000.00Total10.23Pounds of Pan Per Year288122817 100.00%0.00%0.00%Maximum Dry Tons Per YearPercentage of DTs315 11.18%2502 88.82%28170.00%100.00%Maximum Dry Tons Per Year3152502Percentage of DTs11.18%88.82%0.00%
5 Year AdjustedSURFACEPlant NamePAN/dtWeighted AverageCooleemee43.90 4.91Cleanout6.43 5.710.000.00Total10.62Pounds of Pan Per Year29920INJECTIONPlant NamePAN/dtWeighted AverageCooleemee47.46 5.31Cleanout8.84 7.850.000.00Total13.16Pounds of Pan Per Year370712817 100.00%2502 88.82%0.00%0.00%2817 100.00%Maximum Dry Tons Per YearPercentage of DTs315 11.18%0.00%0.00%Maximum Dry Tons Per YearPercentage of DTs315 11.18%2502 88.82%