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HomeMy WebLinkAboutWQ0004972_Monitoring - 01-2022_20220303Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * January Report Information WQ0004972 Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* Forest Lakes —Jan 22.pdf 1.68MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Gerald, Wanda 3/3/2022 This will be filled in automatically Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Accepted Date: 4/11 /2022 Page 1- of 2 NON-DISCIIARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: WQ0004972 MONTH: January YEAR: 2022 FACILITY'NAME: Foi-est Lakes 1'reset-ve ELS COUNTY: Davic Flow MonAoring Poiw: Effluent: Lyj lnflueW; u Parameter Morfto6ng PoInt EflluenL LIV Influent: (SW): SW Code/Name: Was There Effluent Flow for lhis Morlh Generate At'rhf', Facility: Yes: u No: u Op,, at,r 50050 001WO O(K"' 10 130610 00530 316;6 OM615 00625 COOD 00600 MX20 70300 00940 D A T L Arrivall Time 2460 Operate; Tme on Meng CR,C on Sac? rgidy Rim (Flowinto, Tmattrertl m nrvw oil R'Ouhl hk"- HOD 20 t NH SS Fecal C Afo- {Cco -I", M-O� I 'T ph'� jr",',I Km,],Mfl Nmog- Nut NuM, Naah " a n t r 7V 1'nad IN"ol'.1 "7'A4N hlmidc HR YIN CAID ;"'d I --=- ing L MO L %Iu I iffl, MG 11 M tlfill NOAL w h 440 L %V.l I Mt; L. Hil� MO 1. "'M' NIG 1, Wffl%........ MG I %k 2 3 4 0804 1455 0.25 11,25 Y B 8,000 81000 6.4 6.3 <111.01 <11.01 5 1505 0,25 B 8j11m 6.2 "AL01 6 1415 0.50 11 &0011 6,11 '(1.0 1 7 111211 0.25 V 8,041111 6.2 8 8,11410 to 1455 0125 13 &IIIJI) 63 1 <Ofil tl 1,345 0,25 13 sm),l) 6.1 <OAll 1 12 1545 11.25 13 8,10(1) 6.0 <0M I 13 1016 W50 1, 3,000 5.9 <11,91 W 0811 0.25 8'41w1 5.9 'COA)l t 1-1 - 8,000 1 16 1 If 8,000 17 Is 19 0804 14411 1.115 41.25 0?5 US 1' B B 81000 8,000 8,000 519 6.0 6.2 �'0'01 •A).411 0.01 20 41745 0.50 Y 8,000 fi.t -'u.11 I 21 0915 0 2 -1; B 8,01)1) 6A <111.01 2: MOO 23 8,000 24 1420 0.2,5 It 81000 63 "'0.01 25 WOO 0.25 it 8,()1)1) 6.2 "0.01 26 Hq15 0.25 11 sjml) 63 <11.01 27 0716 1 0.50 y &000 63 ""0.01 9.4 2&9 8A 2420 15 1 34.4 <0.040 34.4 <0,04(f 2, 104() 0.25 11 8 ,000 6A "0.01 Z9 0 1 8,000 .33 31 1310 1 0.215 f3 8'm1) 6.30 <401 A'Crjy,v E4j111f) I= <jI.j)j 9.4 28.1) S.N 24211 34.4 <0.040 .44.4 <0.040 Datik, Nlakinitun 8MOO !tA <11.01 S.N 2420 3.5 14.4 75.575 -777- -.7 777M 7 Daily m Minimu1000 8 5111 <0.0 9.4 28.9 U 1 34.4 <0.040 34.4 <0.11400 M011011.1 t 11mits (S) Composite'; / Grab ((;) How I'victer Inopenabie flows' Estimated Glcimllri(T Grade: If Phone: 336-996»2841 Check Box if ORCHas Changed: ORC Certification Number. 987931/20771 Cei-fified Laboratories (1). Pace Analytical ScHyces (2). Pei-SO11(s) Collecling Samples: clelln pl-ice Mail ORIGINAL and'Fkko COPIES Itp: XFFN': Non -Discharge Compliance Unit x $ 1) FN R (SIGN VFU R E' fah 0 11 E IM () R IN R ES P 0 N S 113 1, E C I LA R G E) 1) i i s i 4) ji of "' a t o r Q i j ; t I i I) fly this %ignaturv, I certify that this report is accurate Hit(] 1617 Malt Ser-vice Center COMI)ICIC W the best of my knoiNledv. RALEAGM, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant ,4N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Flow Estimated Flow meter inoperable "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 -Conductivity01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facilit,�s permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 _ of _..2____ NON-1)[SCH�kR(.1i'Al"PLICA'rION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUINIBER: WQ004972 INIONTIJ: January YEAR: 2022 FACILITYNANIE: Forest Lakes Preserve ELS. COUNTY: Da%,ie Formulas: Daily Loading (incines) = [VoluTne Applies (galions) x 0.1336 (cubic foeLgWon) x 12 (Inch"Anot)] f jAroa Sprayed (acres) x 43,560 (squat e feeLlacro) or (Volume Appred (gallons) ( (Area Sprayed (acres) x 27,152 (gaflons/acre-ancin), Max-inum Hourly Loading linchrs) Daily Loading (inches))'Finne irrigated (minutos) 160 (niinwps)hoturtj Monthly Loading (linchos), mSurn of Daily Loading (inchas) 12 Month Floating Joi (inOiosl = Suni of this month"s i Loading (inches) and previous 11 month's Monttnly Loadings (inches) Avi;irage Weekly Loading (inches) = [%knitbly Loading (inchesinnon(h) / Nurnoer of dav,r in the month (day0i I] x 7 (days//­eek I '%N catticar Codi C-clear. K-par dv clocid, , Cl-clouirb, R-rwir, SI-dret Spray Irrigation Operator in WSPOVISHAC Charge (ORC); Gicall Price - - Phone: 336996-2841 ORC Certification Number: 987931120771 Cheek Box if ORCHas Changed: Mail ORIGINAI, and'hvo COPIES to: A'Ft N: Non-Discluirge Compliance Unit X . . ..... Zs, 1) EN R (SIGNA'fURE 01, OPERA'll IN RESPONSIBIX CHARGE) Division of Water Quvr1i1% By this signutilivol I evill-tili that tins report is accurate and 1617 Mail Service Centel, coroplew to the best of il kno"10ge. NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). r, 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal MCDuffie (Authorized Agent) (Permittee-Please print or type) 2N. Riverside Plaza, Suite 800 Chicago. I1 60606I 160606 (Permittee Address) Field Services Director (Pace Services Director (Pace AnalZical Services) (Position or Title) 3/31/2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). Analytical WWW'Pacirlabs'COM February 09, 2022 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lake Pace Project No.: 92584837 Dear Tracy Overclurf: Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Enclosed are the analyfical results for sample(s) received by the laboratory on January 27, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville Pace Analytical Services - Eden If you have any questions concerning tNs report, please feel free to contact me. Sincerely, Stephanie Knott stepl)anie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 16 IweAnalytical wrw.pacelabu m Project: Forest Lake Pace Project No.: 92584837 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NO 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NO 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Yrginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 1�5aaqceAnalytical WMIS ISI)Leam SAMPLE ANALYTE COUNT Project: Forest Lake Pace Project No.: 92584837 Pace Analytical Services, LLG 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92584837001 Effluent SM 254OD-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 AMI 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 521OB-2016 AED 1 PASI-E Colilert-18 LRB 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 KDF1 1 PASI-A PASI-A = Pace Analytical Services -Asheville PAS I-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 act. Analj cal" www.paeetabs.com ANALYTICAL RESULTS Project: Forest Lake Pace Project No.: 92584837 Pace Analytical Services, LLC 1377 South Park Drive Kemersvipe, NC 27284 (704)977.0981 Sample: Effluent Lab ID: 92584837001 Collected: 01127/22 11:03 Received: 01/27/22 14:15 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 8.8 mg/L 6.3 1 01/28/22 17:27 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia 28.9 mg/L 0.50 5 02101/2212:55 7664.41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.040 1 01/27/22 19:01 14797-55-8 5210E SOD, 5 day EON Analytical Method: SM 521 OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden SOD, 5 day 9.4 mg/L 2.0 1 01/27/22 18:00 02101/22 15:49 Colilerl:48 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 01/27/22 17:33 01/28/22 12:07 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 34.4 mg/L 0.52 1 0210712212:00 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 34A mg/L 2.5 5 02/02/22 13:25 02/03/22 04:41 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 363.2 Rev 2.01993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 02103/2210:58 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 3.5 mg/L 0.050 1 02/08/22 23:29 02/09/22 15:10 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16 aceAnalytical www.pacelaba.eam QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 Pace Analytical Services, LLC 1377 South Park Drive Kernersvilie. NC 27284 (704)977-0981 QC Batch: 674743 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92584837001 METHOD BLANK: 3531713 Matrix: Water Associated Lab Samples: 92584837001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01/28/22 17:23 LABORATORY CONTROL SAMPLE: 3531714 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 3531715 92584846001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 91.6 91.0 1 SAMPLE DUPLICATE: 3531716 92584848001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 748 660 12 Resuns presented on this page are In the units indicated by the 'Unite column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, L.L.C. Page 5 of 16 IeAnalyticai� tmaw.pacelabseom QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 QC Batch: 674912 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92584837001 METHOD BLANK: 3532600 Associated Lab Samples: 92584837001 Parameter Units Nitrogen, Ammonia mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 02/01/2211:29 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3532601 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.4 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3532602 3532603 MS MSD 92584816001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.6 5.5 109 109 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3532604 3532605 MS MSD 92584822002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.6 5.6 111 111 90-110 0 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, I.I.C. Page 6 of 16 acmnalytical www.pacelabuom QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 QC Batch: 674409 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92584837001 METHOD BLANK: 3530199 Associated Lab Samples: 92584837001 Parameter Units Nitrogen, Nitrate mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 01127/2218:58 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3530200 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530201 3530202 MS MSD 92584837001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 100 99 90-110 1 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 16 acmnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 QC Batch: 674357 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92584837001 METHOD BLANK: 3529651 Matrix: Water Associated Lab Samples: 92584837001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 02/01/22 14:20 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3529652 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 176 89 84.6-115 SAMPLE DUPLICATE. 3529654 92584726002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 156 158 2 R6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fug, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, L-C. Page 8 of 16 aceAnalXical www.pacolabs.com Project: Forest Lake Pace Project No.: 92584837 QC Batch: 674413 QC Batch Method: Colilert-18 Associated Lab Samples: 92584837001 SAMPLE DUPLICATE: 3530208 Parameter Units Fecal Coliforms MPN/100mL QUALITY CONTROL DATA Analysis Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden 92584797004 Dup Result Result RPD Qualifiers ND ND Pace Ana"cal Services, LLC 1377 South Park Drive Kerners ille, NC 27284 (704)977-0981 Results presented an this page are In the units indicated by the 'units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 16 aceAnaiytical www:pacelatis.eom t Project: Forest Lake Pace Project No.: 92SU837 QC Batch: 675517 QC Batch Method: EPA 351.2 Rev 2.0 1993 Associated Lab Samples: 92584837001 METHOD BLANK: 3535321 Associated Lab Samples: 92584837001 Parameter Units Nitrogen, Kjeldahl, Total mg/L QUALITY CONTROL DATA Analysis Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 02/03/22 03:35 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3535322 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.9 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3535323 3535324 MS MSD 92584807005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 651 10 10 578 632 -733 -189 90-110 9 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3535325 3535326 MS MSD 92584815001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 10.7 10 10 19.6 19.2 89 85 90-110 2 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in hull, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 aceAldj cal www,pacelobteom QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 QC Batch: 675717 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92584837001 METHOD BLANK: 3536607 Matrix: Water Associated Lab Samples: 92584837001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 02/03/22 10:31 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3536608 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3536609 3536610 MS MSD 92585573001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.22 2.5 2.5 2.7 2.7 101 99 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3536611 3536612 MS MSD 92585574001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L NO 2.5 2.5 2.4 2.4 95 95 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/0912022 05:16 PM without the written consent of Pace Analytical Services, I.L.C. Page 11 of 16 ID acmnalytical tvwtv.pacelabs.wM QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92584837 QC Batch: 676630 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92584837001 METHOD BLANK: 3641547 Matrix: Water Associated Lab Samples: 92584837001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg1L ND 0.050 0210912214:59 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3541548 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mgiL 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3541549 3541550 MS MSD 92584054003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP0 Qual Phosphorus mgiL 0.17 2.5 2.5 2.7 2.7 102 101 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3541551 3541552 MS MSD 92584711001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mgiL 4.5 2.5 2.5 7.2 4.9 109 17 90-110 38 M1,R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 1�5aa'uceeAnalytical www.pacelab.cam Project: Forest Lake Pace Project No.: 92584837 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyze in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as 'Total' may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/09/2022 05:16 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16 aceAnalj6cal www.pacelaba.ecm 1 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 Project: Forest Lake Pace Project No.: 92584837 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92584837001 Effluent SM 254OD-2015 674743 92584837001 Effluent EPA 350.1 Rev 2.0 1993 674912 92584837001 Effluent EPA 353.2 Rev 2.0 1993 674409 92584837001 Effluent SM 52106-2016 674357 SM 521OB-2016 674591 92584837001 Effluent Colilert-18 674413 Colilert-18 674415 92584837001 Effluent TKN+NO3+NO2 676437 Calculation 92684837001 Effluent EPA 351.2 Rev 2.0 1993 675517 EPA 351.2 Rev 2.0 1993 675697 92584837001 Effluent EPA 353.2 Rev 2.0 1993 675717 92584837001 Effluent EPA 365.1 Rev 2.0 1993 676630 EPA 365.1 Rev 2.0 1993 676995 Date: 02109/2022 05:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 16 CHAIN -OF -CUSTODY Analytical Request Document _... aceAnalytica(' Chain -of -Custody is il LEGAL DOCUMENT- Complete all relevent fields fnBusEraNLY-f : Wo# * 925g4837 W 1! ALL Container Preser. . , 92584837 . u, , 2 �8 . Company: Forest Lakes Billing Information: Address: Report To: Email To: •• Preservative Types: (1) nitric add, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (4) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other Copy To: Site Collection Info/Address: Analyses Lab,ProfileiUne: Customer Project Name/Number: State: County/City: Time Zone Collected: / ( IPT[ JMT( )CT [ ]ET {— d Ep Z ;v Fes— a: O 12 Z 0 Z Z = o Lab Sample Roo 1pt Chackl ut r Custody seals Prosenc/Intact Y N 10 Custody Signatures Present V N NA collector Signature Preoont N NA Bottles intact, N NA Correct .Bottles N NA Sufficient Volume . N NA Samples Received on Ice l Yoh - Haddopaco Acceptable y N USDA Regulated Soils �t, N Samples in Holding Time (YJ KNA Residual Chlorin P Y C" Cl Strips: " Sample pH ojtja Y J NA pH Stripe41 Sulfide Prevent Y N Lead Acetate Strips t LAB USE ONLY: Lab Sample # / Comments: Phone: Email: Site/Facility ID #: Compliance Monitoring? [ V/Yes [ ] No Collect y (print): j. Purchase Order #: Quote q: DW PWS ID #: DW Location Code: Co eMed B (signat re): Turnaround Date Required: Immediately Pace on Ice: [ ]Yes [ ]NO Sample Disposal: I ) Dispose as appropriate ( ] Return I J Archive: ( J Hold: Rush: ( ] Same Day [ ] Next Day ( 12 Day ( 13 Day [ 14 Day [ 15 Day (Expedite charges Apply) Field Filtered (if applicable): [ ] Yes [ ] No Analysis: ' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (51.), Oil IOL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix Comp / Grab Collected (or Composite Start) Composite End Res Cl # of Ctns Date Time Date Time Effluent VVW G t Z9 / 8 Customer Remarks / Special Conditions / Possible Hazards: Type of ice Used: Wet Blue Dry Notre SHORT HOLDS PRESENT (02 hours): Y NIA Lab Sample Temperature Info: Temp Blank R Y N NA ThermfD#: Cooler 1 Temh Upon Receipt: C Cooler 1 Therm Corr. Factor: oC Cooler 1 Corrected Temp: oC Comments: Packing Material Used: Lab Tracking 11: dt hem sample(s) screened (aSOD cpm): Y N NA Et Samples received via: FEDEX UPS Client Courier Pace Course Relinquished byJCom ny:ISignature) l e/Ti e: 7 ZZ Ric d by/Co any: (Sig ature) DateJTime: 1 1 MTJL NLY Table#• AcMnum: Re wishedby/Company- Si Aster �q g _ Date/Time: Receiv by/ ompany: {5 gnature) Date/T1me: Template, P Ptelogim PM: pB: Trip Blank Received: Y N NA HCL McOH TSP Other Rei214uished by/Company: (Signature) 0)Nan Date/Time: Received by/Company: (Signature) Date/Time: Conformance(s): YES / NO Page: of: -3 a 0 ti ro 0 M 2 a 0 m � a n CL O C w d r+ a ru � m 3 M. �. o o 3 Gq a O e 'r N .D C LA As m 3 a y N ro � c � (D w D °c a a. rfS 9 CL N Z a S ro s ar rr 0 CD Matrix N n tZi OC -4H N t+ Iteml! zzBP411-125 mL Plastic Unpreserved (N/A) (CI-) BP3U-250 mL Plastic Unpreserved (N/A) BP211-500 ml. Plastic Unpreserved (N/A) SP1U-1 liter Plastic Unpreserved (N/A) BP45.125 mL Plastic 112SO4 (pit < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 21 BP4Z-12S mL Plastic ZN Acetate & NaOH (>9) BP40-125 mL Plastic NoOl i (pH > 12) (CI-) WGM-Wide-mouthed Glass jar Unpreserved AGiU-1 liter Amber Unpreserved (N/A) (Cl-) AG1H-1 liter Amber HCI (pH < 2) AG3U-250 ml. Amber Unpreserved (N/A) (Cl-) AG1S-1 liter Amber Ii25O4 (piI < 2) AG35-250 mt. Amber H2504 (pH < 2) AG3A(DG3A)-250 ml.Amber NH4CI (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) VG9T-40 mt. VOA Na25203 (N/A) VG91.11-40 mL VOA Unpreserved (N/A) DG9P-40 mL VOA 143PO4 (N/A) VOAK (3 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mi. Sterile Plastic (N/A — lab) SP2T-250 mL Sterile Plastic (N/A — lab) ZT -- zzz BP3A-250 mL Plastic (NH2)2SO4 (9.3.9.7) -Z AGOU-100 ml. Amher Unpreserved vials (N/A) VSGU-20 ml. Scintillation vials (N/A) OG9U-40 ml Amber Unpreserved vials (N/Al s LA fi x � w 3 O O o 0 N 0 0] O p 3 X O .r - N O M R C � ro N 1 O 0 Cr C. rD � w D+ ro 0 a n 2 w Cb ea t.V) 0 0 rrDD O -n fD m � r� at a o w z 0 c on O 0 O w 3 n 3 O w w n C. ^O* fl 0 DZi A O T 3 r 3 m T t' c Doi � n n N .�. :3 Do DU 0. N D 10 .. .0 ~ a 0 d o to 2 � ro- O .. ro �+ N rJ N V O rD n R U