WQ0038087_More Information Received_20220315

Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Permit Number (IR) * WQ0038087
Applicant/Permittee Terra Renewal Services, Inc
Email Notifications
....... ........ ......... ...........
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* David C. Coyle
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
479-747-9192
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0038087
Has Current Existing permit number
Applicant/Permittee Address*
P.O. Box 1746 Watkinsville, GA 30677
Facility Name*
Terra Renewal Services Class B Residuals Program
Please provide comments/notes on your current submittal below.
This is the response to the request for additional information sent by Erick Saunders in a letter
dated 2/18/22. If there are any questions or request for additional information, please contact
me at the info below:
David Coyle
479-747-8192
[e-mail]
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
NC WQ0038087 MOD RLAP Terra Renewal AIR
— — — — — 14.01M6
Response _3-14-22. pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617

Signature
Submission Date 3/15/2022

TERRA
renewal
March 14, 2022
Erickson Saunders; Engineer
Division of Water Resources
North Carolina Department of Environmental Quality
512 N. Salisbury Street
Raleigh, NC 27699-1617
RE: RESPONSE TO ADDITIONAL INFORMATION REQUEST
Application No. WQ0038087
Terra Renewal Services Class B Residuals Program
Wilkes Co.
Dear Mr. Saunders,
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
The enclosed documents are provided as response to your letter requesting additional information, dated
February 14, 2022, pertaining to the application to modify RLAP permit number WQ0038087 by the
addition of 174 acres of land, the addition of two residuals sources, the deletion of two residuals sources,
and the modification of the number of dry tons certified for existing residuals sources. Per your request,
the following information is provided (in order listed in letter):
C. Residuals Source Certification (RSC 06-16) Application:
- A revised form RLAP 06-16 reflecting changes in total net acreage (+ 2.0 ac) from the deletion of
the property line setbacks on fields NC-WK-MRF-06 and NC-WK-MRF-12 and the revision of the
Quantitative Justification for Residuals Production Rate calculations based on updated data
presented in form RSC 06-16 for RVI (Tyson) — Harmony and AdvancePierre Foods — Claremont.
- Forms RSC 06-16 for sources RVI (Tyson) — Harmony and AdvancePierre Foods — Claremont.
- Quantitative Justification for Residuals Production Rate calculations including 1 — 5 YR PAN
calculations for the above -mentioned sources and a revised weighted average PAN calculation
for all sources.
- Analyses corresponding to the data entered in form RSC 06-16 for the above -mentioned sources.
D. Land Application Site Certification (LASC 06-16) Form:
- Form LASC 06-16 with revised net acreages for fields NC-WK-MRF-06 and NC-WK-MRF-12
based on removal of the property line buffers due to reciprocating setback waiver forms between
parcels 0100811 and 0100020.
- Revised maps showing these fields with the subject property line boundaries removed.
- An addendum to the Soils and Agronomy Report addressing the soil series contained within the
added land.
F. County Board Notification (CBN 06-16):
- A copy of form CBN 06-16 and corresponding documentation as sent to the Chairman of the
Wilkes County Board of Commissioners.
- A copy of the certified mail receipt showing that the required documents were sent.

- A copy of the email sent to the Chairman containing the same information as sent via USPS and
presented herein.
- A copy of the "green card" for delivery confirmation via USPS can be provided to you upon
receipt.
Please contact me if you have any questions or require further information in order to complete the review
of this application.
Sincerely,
David C. Coyle
Senior Environmental Manager

State of North Carolina
Department of Environmental Quality
DWR Division of Water Resources
Divlsion of Water Resources 15A NCAC 02T 1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Terra Renewal Services, Inc
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal
❑ County
Signature authority's name per 15A NCAC 02T .0106: David C. Cow
Title: Environmental Manager
Applicant's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: 4( 79) 747-8192 Email Address: david.coyleAterrarenewal.com
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip: -
Telephone number: O - Email Address:
3. Agronomist's name: License Number:
Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: )
Agronomist's mailing address:
City: State: Zip: -
Telephone number: (_) - Email Address:
4. Soil Scientist's name: David C. ColeLicense Number: 1315
Affiliation: ❑ N/A ® On Staff ❑ Retained (Firm: )
Soil Scientist's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: [phone] Email Address: david.co rlekterrarenewal.com
5. Fee submitted: $395.00 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00038087
Date of most -recently issued permit: February 4, 2021
Date of most -recently certified Attachment A (if different than the permit): February 4, 2021
Date of most -recently certified Attachment B (if different than the permit): February 4, 2021
FORM: RLAP 06-16 Page 1 of 5

111. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 615 Mathis Farm Rd (Location of Office of LJC Environmental, LLC)
City: Roaring State: NC Zip: 25669-
Coordinates: Latitude: 36' 08' 51" Longitude: 80' 59' 09"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
County where residuals land application program is headquartered: Wilkes
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Luke Mathis
LJC Environmental, LLC
1003524
Back -Up ORC
David Coyle
Terra Renewal Services, Inc
995723
Additional Back -Up
Will Hodges
Denali Water Solutions
997282
ORCs
Ivan Heatwole
Denali Water Solutions
1002031
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test: Andrew Epting; Environmental Specialist; Denali Water Solutions; Estimate Cert. in Summer 2022.
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 5,260 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
45.4
65.6
238,804
345,056
Five -Year Maximum Adjusted
53.2
73.5
279,832
386,610
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
1,704.2
Hay
Pasture
Total:
1,704.2
Methods
Surface
Incorporation or Injection
1,704.2
Total:
1,704.2
FORM: RLAP 06-16 Page 2 of 5

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
4,776
6,901
5,597
7,732
100
2,388
3,451
2,798
3,866
150
1,592
2,300
1,866
2,577
200
1,194
1,725
1,399
1,933
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e. g. not enough storage, not enough land, vector reduction
practices not in place, etc.):
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
ra
--
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
IR
Land Application Siite
Certification.doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VL Applicable to Dedicated Program with fixed irrigationystem only.
M11111U[men lei 011,1u/:11Y[11001IJta01►V0Ioil 1NN[ff.7401110y1060lul
1. The irrigation system is: ❑ Spray ❑ Drip
2. Disposal system is: ❑ existing ❑ proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet
below ground surface. Rules 15A NCAC 02T .0505(12) requires at least one -foot vertical separation between SHWT and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified:
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
Fields within Soil Area
Recommended
Loading Rate
(in/hr)
Recommended
Loading Rate
(in/ r)
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
❑ Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met:
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field /Zone
Design Area
(ft)
Number of
Nozzles
Maximum Application
Rate ( allons/hr)
Design Annual Loading
Rate (gallons/ r)
Total
Spray Irrigation Design Element
Plan Sheet
Number
Specification
Pa a Number
Wetted diameter of nozzles
ft
Wetted area of nozzles
ft2
Nozzle capacity
gpm
Nozzle manufacturer / model
/
Elevation of highest nozzle
ft
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, David C. Coyle Senior Environmental Manager
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Terra Renewal Services, Inc
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
C�E� C. 5��
Date: 3/14/2022
FORM: RLAP 06-16 Page 5 of 5

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
INI�y11111:11 :1d)K4111:il01y[ey.1110[$010
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: ncePierr
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ® Other (explain: Facility discharges to local POTW. Residuals consist of DAF
skimmings from pretreatment).
3. Facility contact person and title: nttionv oci o; hnvironmental Manager
Complete mailing address: 3437 E. Main St
City: Claremo State: �LC Zip:-�
Telephone number: [phone] E-mail address:
4. Facility physical address: 3437 E. Main St
City: � State: a Zip: -�
Coordinates: Latitude: L5° 42' Longitude: 81° 08' 16"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: __ MGD and facility average daily flow: MGD
8. Average amount of residuals being generated at this facility 0 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: T767--generated trom solids removed from D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units):
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
El Biological II Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: We Analytical Services--9M and Date of analysis: 12/3/2021
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: 0 yes L no. Flashpoint EE OF (> 140°F)
Passed reactivity test: Eyes Ino. HCN: 50 mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
0.089
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.040
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/LaudApp&cation: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/3/2021
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg1kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 0.96
Cadmium
85
39
< 0.32
Copper
4,300
1,500
450
Lead
840
300
1.9
Mercury
57
17
< 0.31
Molybdenum
75
n/a
< 2.6
Nickel
420
420
35
Selenium
100
100
< 1.3
Zinc
7,500
2,800
140
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 6.95 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/3/2021
Parameter
Result
(mg1kg)
Aluminum
3400
Ammonia -Nitrogen
170
Calcium
570
Magnesium
< 320
Nitrate -Nitrite Nitrogen
3.8
pH (Standard Unit)
4.3
Phosphorus
800
Potassium
540
Sodium
1700
Total Kjeldahl Nitrogen
11000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 3.71
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or [I actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lam or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mgl'kg)
(mgl'kg)
Surface
4,420
6,750
Injection/Incorporation
4,505
6,835
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/LandApp&cation of'ClassA or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
b
Specify one: 77 composting, heat drying, 77 heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For LandApp&cation of'Class B:
Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal
JSelect One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
JSelect One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
JNot Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] -
38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T.1107(a)(2)] -
40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.1107(a)(3)] -
30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.1107(a)(4)] -
Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.1107(a)(5)] -
14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T.1107(a)(6)] -
Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.1107(a)(7)] -
Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.1107(a)(8)] -
Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.1107(a)(9)] -
Injection.
Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
El
Alternative for Surface Disposal Units Only
- Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Ingredients Ason Foo
2. Facility permit holder is: ❑ Federal, ❑ State, V Local Government, or 0 Private.
Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health,
or ❑ Other (explain:).
3. Facility contact person and title: es; Wastewater Manager
Complete mailing address: 601 Sheffield Rd
City: armon State: Zip:-�
Telephone number: (E) E-M E-mail address:
4. Facility physical address:
City: � State: 0 Zip: 634-
Coordinates: Latitude: 35' 57' 15" Longitude: L° 43' 17"
Datum: � Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0. MGD and facility average daily flow: M MGD
8. Average amount of residuals being generated at this facility = dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: enerate m D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): one 5,000 gallon holding tank
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/3/2021
Passed corrosivity test: yes ❑ no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes ❑ no. Flashpoint EE OF (> 140°F)
Passed reactivity test: Eyes Wo. HCN: < 50 mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
3.3
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
0.83
Selenium
1.0
< 0.20
Cresol
200.0
0.83
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/LaudApp&cation: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/3/2021
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg1kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 6.5
Cadmium
85
39
< 2.2
Copper
4,300
1,500
13
Lead
840
300
< 4.3
Mercury
57
17
< 2.1
Molybdenum
75
n/a
< 17
Nickel
420
420
< 17
Selenium
100
100
< 8.7
Zinc
7,500
2,800
22
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 3.81 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/3/2021
Parameter
Result
(mg1kg)
Aluminum
8100
Ammonia -Nitrogen
12000
Calcium
39000
Magnesium
< 2200
Nitrate -Nitrite Nitrogen
58
pH (Standard Unit)
5.8
Phosphorus
19000
Potassium
3600
Sodium
3700
Total Kjeldahl Nitrogen
59000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.96
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or [I actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lam or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mgl'kg)
(mgl'kg)
Surface
24,860
34,975
Injection/Incorporation
30,860
40,975
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/LandApp&cation of'ClassA or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
b
Specify one: 77 composting, heat drying, 77 heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For LandApp&cation of'Class B:
Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal
JSelect One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
JSelect One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
JNot Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] -
38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T.1107(a)(2)] -
40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.1107(a)(3)] -
30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.1107(a)(4)] -
Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.1107(a)(5)] -
14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T.1107(a)(6)] -
Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.1107(a)(7)] -
Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.1107(a)(8)] -
Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.1107(a)(9)] -
Injection.
Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
El
Alternative for Surface Disposal Units Only
- Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

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Surface Application PAN
Advanceflerre Foods - Claremont
TKN= 11000 mg/kg
NH3= 170 mg/kg
NO3-NO2-N= 4 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 10,830 85 3.80
PAN= 8.84 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 10,830 4,332
PAN= 2.60 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 6,498 1,300
PAN= 1.11 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,198 554
PAN= 0.62 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 4,644 310
PAN= 0.34 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 4.66 Lbs/Pan/DT
Total five-year max. adjusted PAN = 13.50 Lbs/Pan/DT

Incorporation Application PAN
Advanceflerre Foods - Claremont
TKN= 11000 mg/kg
NH3= 170 mg/kg
NO3-NO2-N= 4 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 10,830 170 3.80
PAN= 9.01 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 10,830 4,332
PAN= 2.60 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 6,498 1,300
PAN= 1.11 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,198 554
PAN= 0.62 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 4,644 310
PAN= 0.34 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 4.66 Lbs/Pan/DT
Total five-year max. adjusted PAN = 13.67 Lbs/Pan/DT

Surface Application PAN
RVI - Harmony
TKN= 59000 mg/kg
NH3= 12000 mg/kg
NO3-NO2-N= 58 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 47,000 6,000 58.00
PAN= 49.72 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 47,000 18,800
PAN= 11.28 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 28,200 5,640
PAN= 4.81 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 22,560 2,406
PAN= 2.69 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 20,154 1,344
PAN= 1.46 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 20.24 Lbs/Pan/DT
Total five-year max. adjusted PAN = 69.95 Lbs/Pan/DT

Incorporation Application PAN
RVI - Harmony
TKN= 59000 mg/kg
NH3= 12000 mg/kg
NO3-NO2-N= 58 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 47,000 12,000 58.00
PAN= 61.72 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 47,000 18,800
PAN= 11.28 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 28,200 5,640
PAN= 4.81 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 22,560 2,406
PAN= 2.69 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 20,154 1,344
PAN= 1.46 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 20.24 Lbs/Pan/DT
Total five-year max. adjusted PAN = 81.95 Lbs/Pan/DT

ace
C
Analytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WL01015
Date Completed:01/26/2022
Revision Date: 01/19/2022
I
01/27/2022 9:38 AM
Approved and released by:
Project Manager II: Lucas Odom
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A C C R E D I F E❑
7 EST W: LAMPATOPY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 20

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WL01015
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
This report supersedes all other versions of the same report.
Inorganic Metals
Due to the matrix and low percent solids, these samples had an initial weight that is 3x greater than
standard procedure: WL01015-001, WL01015-002, WL01015-003. The LOQ has been adjusted
accordingly.
Report Revision 01/27/22
Due to client request the % solids result was reanalyzed for sample -003. The sample yielded a lower
result and has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 20

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WL01015
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/Willisboro Solid 11/30/2021 1130 12/01/2021
002 Tyson/Harmond
003 Advanced Foods/Claramont
(3 samples)
Solid 11/30/2021 1230 12/01/2021
Solid 11/30/2021 1430 12/01/2021
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N ) 350.1
10
12/06/2021 1417 DMA
24642
1
(Flashpoint () 1010B
1
12/08/2021 1006 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1645 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
25
12/02/2021 1311 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1043 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1928 NBW
25322
1 351.4
(TKN) 351.2
2
12/08/2021 1554 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
87
%
1
Ammonia - N (gas diffusion)
350.1
12000
2600
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Nitrate -Nitrite - N (soluble)
353.2
58
5.3
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
19000 S
3300
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.3 ° C
9045D
5.8
su
1
TKN
351.2
59000
2600
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12/20/20211333 BWS
26259 12/07/2021 0012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
)ate Received:12/01/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
80 70-130
1,2-Dichloroethane-d4
121 70-130
Toluene-d8
100 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E 1 01/12/2022 2303 CMF
12/10/2021 1730 25236 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.83
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
86 37-129
2-Fluorophenol
79 24-127
Nitrobenzene-d5
101 38-127
Phenol-d5
107 28-128
Terphenyl-d14
101 10-148
2,4,6-Tribromophenol
71 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 12/16/2021 1649 DAL1
12/13/2021 0915 25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
68 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 366013/3665A 8082A 1 12/15/2021 2256 DAL1 12/03/2021 2140 24550
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016
12674-11-2
8082A
ND
440
ug/kg
1
Aroclor 1221
11104-28-2
8082A
ND
440
ug/kg
1
Aroclor 1232
11141-16-5
8082A
ND
440
ug/kg
1
Aroclor 1242
53469-21-9
8082A
ND
440
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
440
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
440
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
440
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
73 41-132
Tetrachloro-m-xylene
71 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 12/16/2021 1928 DAL1 12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
gamma-BHC(Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
81 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 12/08/2021 0815 JAB2 12/08/2021 0331 24447
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 2.1
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 12/10/2021 1249 KSH2
12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A
7470A
1 12/14/2021 1051 JAB2
12/14/2021 0642 25465 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 12/03/2021 1141 KSH2
12/03/2021 0250 24274
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
8100
170
mg/kg
1
Arsenic
7440-38-2 6010D
ND
6.5
mg/kg
1
Cadmium
7440-43-9 6010D
ND
2.2
mg/kg
1
Calcium
7440-70-2 6010D
39000
2200
mg/kg
1
Copper
7440-50-8 6010D
13
4.3
mg/kg
1
Lead
7439-92-1 601OD
ND
4.3
mg/kg
1
Magnesium
7439-95-4 6010D
ND
2200
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
17
mg/kg
1
Nickel
7440-02-0 601OD
ND
17
mg/kg
1
Potassium
7440-09-7 6010D
3600
2200
mg/kg
1
Selenium
7782-49-2 6010D
ND
8.7
mg/kg
1
Sodium
7440-23-5 6010D
3700
2200
mg/kg
1
Zinc
7440-66-6 6010D
56
22
mg/kg
1
Footnote(s): 'Paint Filter: 50ml- collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N ) 350.1
1
12/06/2021 1419 DMA
24642
1
(Flashpoint () 1010B
1
12/08/2021 1040 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1647 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
5
12/02/2021 1156 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1032 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1932 NBW
25322
2 351.4
(TKN) 351.2
5
12/14/2021 1712 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
95
%
1
Ammonia - N (gas diffusion)
350.1
170
41
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Nitrate -Nitrite - N (soluble)
353.2
3.8
0.82
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
800
100
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.3 ° C
9045D
4.3
su
1
TKN
351.2
11000
1000
mg/kg
2
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12/20/20211358 BWS
26259 12/07/2021 0012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
)ate Received:12/01/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
84 70-130
1,2-Dichloroethane-d4
122 70-130
Toluene-d8
101 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E 1 01/10/2022 1915 CMF
12/10/2021 1730 25236 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
90 37-129
2-Fluorophenol
66 24-127
Nitrobenzene-d5
78 38-127
Phenol-d5
87 28-128
Terphenyl-d14
99 10-148
2,4,6-Tribromophenol
131 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 12/16/2021 1712 DAL1
12/13/2021 0915 25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
65 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 366013/3665A 8082A 1 12/15/2021 2309 DAL1 12/03/2021 2140 24550
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016
12674-11-2
8082A
ND
69
ug/kg
1
Aroclor 1221
11104-28-2
8082A
ND
69
ug/kg
1
Aroclor 1232
11141-16-5
8082A
ND
69
ug/kg
1
Aroclor 1242
53469-21-9
8082A
ND
69
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
69
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
69
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
69
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
72 41-132
Tetrachloro-m-xylene
69 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 12/16/2021 1944 DAL1 12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
gamma-BHC(Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
66 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 12/08/2021 0817 JAB2 12/08/2021 0331 24447
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 0.31
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 20

Client: Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 12/10/2021 1300 KSH2
12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A
7470A
1 12/14/2021 1054 JAB2
12/14/2021 0642 25465 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 12/03/2021 1144 KSH2
12/03/2021 0250 24274
2 3050B
601OD
3 12/03/2021 1356 KSH2
12/03/2021 0250 24274
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
3400
26
mg/kg
1
Arsenic
7440-38-2 6010D
ND
0.96
mg/kg
1
Cadmium
7440-43-9 6010D
ND
0.32
mg/kg
1
Calcium
7440-70-2 6010D
570
320
mg/kg
1
Copper
7440-50-8 6010D
450
1.9
mg/kg
2
Lead
7439-92-1 6010D
1.9
0.64
mg/kg
1
Magnesium
7439-95-4 601OD
ND
320
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
2.6
mg/kg
1
Nickel
7440-02-0 6010D
35
2.6
mg/kg
1
Potassium
7440-09-7 6010D
540
320
mg/kg
1
Selenium
7782-49-2 6010D
ND
1.3
mg/kg
1
Sodium
7440-23-5 6010D
1700
320
mg/kg
1
Zinc
7440-66-6 6010D
140
3.2
mg/kg
1
Footnote(s): 'Paint Filter: 72mL collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 20

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 20

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 20

PACE ANALYTICAL SERVICES, LLC
North Carolina Perrtnit Parameters
2, Rcsiduals a:iall be aoalyzoxl to they are - oura� Cpr�yefyatlou
ar_d RTtmvfjy Acr. (RCRA)_ 'Poe amijUp rrwivw V, [pliabibty, r�acii and toxicity
characiriatic lexclxi��g pxocedure TC sl�a 4y apacitied ku
4.tCer,hTnenl. A, aisd the Pcrmijae shall mfflin�xi l.Lww za ukr. :-3x a rtiini M of five years. Any
rxcePtia sT�s fir�»n tlae retluii aittieuts lu diLs vm litkm shall ixe specTicd ii A#tar.Lu=(A.
The TCLP awdygis shall include the Miming piErnmr-tcrs (th(,, in niftpms Per lit"
is it parenthpara};
LU
4
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C}
�'sea.ic (5.0}
] ,�T}itilllorr�attiaene {7.5}
l�ikr4bene {2.0)
Pezimi lm-opbrM]. (100-0)
H nnum (] ODA)
1,2-Dichloroc brw (03)
T# nzgle {i}.5)
1.1-filchlaroe#hyLue (0.71
PyHdinc (5,0)
Selzer-Jm (1,0)
CaEVlriv (1-il)
2,4-Dhdtrota1ivac (0.13)
2,rb [e#sQcfikorida (CS)
Eridriu (0.02)
Sr1v (5-0)
ChlbrdsalC (0,01}
11exa&1urobcnacnc (0,;3)
Tetrae:7loroethyla (0. r)
-r~`liki obanzeita (100.0}
aAorcrfoiin (u_ 0)
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egtaclli (aaud+tshydi xide) ; ToxaplYelae (U 5)
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MCxlj.V 1{]rL1CL7MLUV (3.b1 2,%U-Tri&lvr4?4cal (400A)
meal Mob)
d ($.0) 7,4,6-Trir-}t'nnphcnai (2,0)
v-Cr=Ql MOM)
Lindano (0.4)
2,4,5 ` P (Sslvox) (1-0)
p-Cresol (200-0)
-- Mcrc:uy (0.2)
Vinyl aliln6dde (0.2)
ao1(200.0)
Mr:iaQXWlk14u (10.0)
.2.s4-U. f10,01
h e#h l ttltyl kc,ttmo RO-0,0} --
._..
3_ An mab-sls shill be uvnduutel ar- residuals fbin each fourae gmicrating fkdhly at the tiapxmcy
Epeaifed in Alrachment A, and the I'ermiGtLIZ s13a11 j,a13Ll8i❑ Ole insults fir a-titrmum of live ycar&
The analysis shall inAudt the following pzxarnek+T;
Ablrninum -.
i
Am rionla-Nifmorn
Arsem
Cadrgum
calcium
( pGr
T rlcl
Magmsflm
WQ2036936 Yer6tin 1-D
1tiUmury
patasslum
MiAybdwum
Selr—uum
Nickel
Sodimu
1*x113�taNitrito �ltr�ger
T>i
Port: Total Solids
Ph
c
Fhosplxan,s
Volatile Solids
PCs!$
TERRA RENEWAL SERVICES
479 747-fI92
31r,11 VffMan 140210
Pate 8 of 12
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 20

PACE ANALYTICAL SERVICES, LLC
Samples Receipt CheMist(5R3CI (MEj3aj w15j KeVL3e ,9/29f2020
. ace rr�r+yl,Caf t551-lii•Pkrthoiity_ Pace ENV • WCOL Page 1 ofi
aMPIC receipt C heddiSt (S'R
Client: araKerxnral Onaler lntpcvrM [;yi&,Lte- JI CiY 12rC11f21Y 1 I,cSti : WUJIO15
P
Pane GEjmt UPS Fecif;x Others V, No 1, Were CO80 i . seab PTeW 4311 fte coaltr7
s NU +� NA 2, if ;uEtotiw� scars were rep.ent, were they intact and unbrokcn7Ir1D-- `A C'1torirtr. St-ip ID= -` _ Teml by; r4rt
Wgi:na[ te.ntperdurz upon receipt? f)rrived (Corrected) Lemperaxtrc upon receipt %solid Suap-Cup [1): 3t-2bGl-2�G1
3.7 ++3.7 oe vli f Yiti rKA IKA oC NA fNA v�
Method: E[lamperatum Blank �--V]Againsr I.IotlicA IN Gan ID: III Our. Correc`c)n Far, -or; C `r~
Meal od 4�i 4x*hLut' U1 Wet 1 cr. ❑ 14'e Pa4❑ D r Ica ❑ Norre -
r IIf 1 t f of 4
❑ Yes
❑ Nu
I.Y I ]ri
- Cmpau urI I� awy CO et .,T,;, od G.v C, AwW; rnijCct fvlanager3Nlottlieol(
Pb1 wes ?dtxtifipd b}r� p}lorle f emlil I face-W-fact(cirr lz: nnp),
Yex
No
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d. 15 1[le CClaruncruial CJuriel,'.s packing.0ip a7a0bed Lu this fora,'
zYes
71 Yes
Nu
�. Were proper custody procelimts (rel]nquishaYrcceived) fe€IOP cM
16. Were =ip[-u IDs AstLd on C-in C'f C?
_Yes
Yes
❑M
Na
7. % eJ%e sarn;,le 1D5 :israd w ill 8amp[c conminers?
&Was cu11Vticn date & time 144ud on the COO R_
yes
No
9. Was cullm4iun date & time I -Pled or, all sainpleconklinvrs7
J Ye~;
T'!0 1
10. Did all container Jabal j-0formation (I[}, date, lirae) ftgrcc wit1 Lila COC?
Q Yea
LANOI
I J J , WE't< tuts 0 be perfaimed listed on the C)OC4 -
❑ v's I LjNO
Yes No
Ycs No
El Yed '7No
1 i2- Did a.] samples arrive in Ihe. proper Mitainers fur cwh test aitdlar in goad conditias
(unroroken, lidw on, cri.`.);.
13. Was adequ* sa-1 [a vDlu1neavailubl.0
14- Wtwe JAI samples received wKin Vz the holding time or 48 hours, whEchcvcr caires J M- 0
15, Were zny 9pmplcE containers miFOngkxcess (circle Cnv) salrplc-e lent Iiajt�cl on f_,OC?
❑d NA 16. For VOA and RSK-L75 sialpies, wert�bubblw present "peg-tiiz#r" 4'ra"ar6inm in diam't
is any of the VOA Vlais?
V NA 17. Were all DROlmetali+nuLrient sam pies received at a pi of< 2?
[71NA 18- Wm all cywilde sarrmp'tM reooivcd at a Id > 121u1d suJ17c[r harm ley nxCi'v.d at a pH > 9`
A ..- . War all upp it a NI-kVTK Cyan +pliena i25. l: i j08.3 (-=z 0.5mg i) sarr.'p tFs rce of
20. VYCrC tilicllt rcmarkOracu�`� MS
ts (i.e- requrs(t:d dilutions, 1vtD des ig mtin is, etc...)
�❑ Yes ❑ ri;o �hi turrutly traimcri had Freff he COC into tie gammon[ seWon in LIMS?
Yes ND :-i, Was the UOleltumbcr Iister! tt7t INN: container label? I Fyvb,PUOLriv - —
5ample Preservation (I41ust he cl3mplet i ally s ,ply s} irt+rsarrcxtly preserved or wirtl headspace-)
Sarripia(h) m,' _. were t�eceivcd inmT-crtly presenTedand wcre adjusted a000rJ:rr',
in sample re+caiv[rtgW[1FI K mL Dfc'_rcle nr_o; fi I� O4, HNQ3, I✓]CI, hiu0li u�iur It! 1 t _
T' me of preseryanon If more OM OPreserve V-e is n"&d, p Icasv 11111E in Fit- ccxiiments below.
NA - - -
were reeeimil with bubbles >6 rnm ifS diarrML
tnples(s) NA wcre received with TKC m&+L (I f 4 J 9 is fJ{P ; and tyere
lu5CWkAUcord1ng1y ir, gamllk{ m0eiving wl[it sodium thiouiitsre(Na�S20x1vtitil 811eaJy 1D; A
bwtrnit lxbrls Hllplied by_ JR43Z UBP
Conlint:'aI.5;
0041: 129)Z12Q21
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 20

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TOPOGRAPHIC FIELD MAP
•
1
R
I �
MRF-12
fl
f
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MRF-6
!�
MRF-6
_
OUT
I MRF-3
1�
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WILKES COUNTY, NC /I
FIELDS: MRF-3, MRF-5, MRF-6, MRF-12
PERMITTEE: TERRA RENEWAL SERVICES, INC QUADRANGLE: SCALE:
RONDA
1 inch = 750 feet
REVISED: August 2020 to exclude area containing Mathis-1 Storage facility on edge of Field MRF-6.

SOILS and AGRONOMY REPORT
Addendum
Permit # WQ0038087 — 2021 Modification
Wilkes County
RE: Deletion of property line buffers on fields NC-WK-MRF-06 and NC-WK-MRF-12
The removal of property line buffer setbacks along the boundaries separating parcels 0100811 owned by
Mathis Properties, LLC (containing fields NC-WK-MRF-06 and NC-WK-MRF-12) and parcel 0100020 owned
by Blue Ridge Conservancy (containing field NC-WK-MRF-13 and others) via setback waiver forms would
result in the following:
1) NC-WK-MRF-06: 50 ft wide by 1,300 ft long (1.5 acres) in the same or similar landscape position
and soil catena as the rest of the field.
2) NC-WK-MRF-05: 50 ft wide by 440 ft long (0.5 acres) in the same or similar landscape position
and soil catena as the rest of the field.
Based on the topography and data collected during previous soil evaluations on these sites, there is no
reason to suspect that the soils contained in the added areas would have significantly different
characteristics regarding suitability or limitations; thus, the same yield expectations for the soils listed as
"predominant" in the current Attachment-B of the permit should be applied to the areas for the added
acreage from the removal of the property line buffers in the respective fields.
Soil Scientist:
Cam` L' e 5�e
David Coyle
NCLSS#1315
G�' yip C. Co
V�,t,. 15
.�

North Carolina Department of Environmental Quality
Pat McCrory
Governor
Donald R. van der Vaart
Secretary
Date: -
To: Name of Chairman to the Board of County Commissioners:
Complete mailing address: 110 No�
City: � State: NC Zip: &L77-_M
County where land application sites are located: HIM
From: Applicant's name: s, Inc (on behalf of the Division of Water Resources in accordance with
Session Law 2013-340)
Contact person and title: o le
Complete mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 77-
Telephone number: [phone] E-mail address: david.co. ly e(cr>,terrarenewal.com
Subject: Notification of residual land application site proposal
This is to notify you that the Applicant listed above will be submitting an application to the Division of Water
Resources for the land application of residual solids to site(s) located in your county. During this review, the Division
will ensure that all federal and state regulations are enforced. Attached to this form is information regarding residuals -
generating sources and locations of the proposed land application sites. Please forward this letter and its associated
attachments to the appropriate Department within your County (i.e., Health or Environmental Health Department and
Planning Department) if applicable.
More information of the land application sites included in this application will be available at the following
Division of Water Resources Regional Office:
Name of appropriate regional office: itinston-Salem
Complete mailing address: 450 West Hanes Mill Rd, Suite 300
City: _ nston-Salem State: NC Zip: 27105-
Telephone number: (33 )-=
date of application submission:
Should you desire to comment on this application, please do so no later than 30 calendar days following the
expected application submission date. If you have any questions or comments about this notification, or if you would like
more information, please contact the appropriate regional office at the telephone number provided above. Thank you in
advance for your attention to this matter.
Enclosures: Source Facility Summary
Land Application Site Summary
Maps
Non -Discharge Permitting Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Phone: [phone] \ Internet: http://portal.ncdenr.org/web/wp
An Equal Opportunity \ Aff rmative Action Employer -Made in part with recycled paper FORM: C3N 06-16

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CERTIFIED MAILP RECEIPT
Domestic Mail Only

From: David Coyle
To: kelmoreCalwilkescou ntv. net
Subject: BOC Notification - Permit Mod - WQ0038087
Date: Monday, March 14, 2022 4:18:00 PM
Attachments: imaoe002.ono
NC W00038087 CBN 06-16 BOC Not Wilkes Terra Renewal RLAP 2022 Mod.odf
Chairman Elmore,
Per the requirements of the NCDEQ-DWR, Terra Renewal is providing the attached notification for
modification of the existing land application permit for farm sites in Wilkes County. This permit was
established and has been active since 2016. The proposed modification would add five new farm
sites totaling 172 acres which are managed by ASJ Mathis Farms. A hard copy of this notification and
related documents was sent to you via certified mail on 3/14/22. If you have any questions
regarding the contents or require additional information, please contact me at 479-747-8192 or
david.coyleCo�terrarenewal.com. Thank you for your time and consideration.
Regards,
David Coyle Lss, CCA
Senior Environmental Manager
iry
TERRA
rrnvci
Cell: 479-747-8192
david.coyle(@terrarenewal.com
P.O. Box 1746
Watkinsville, GA 30677
IMPORTANT NOTICE: This e-mail message is intended to be received only by persons entitled to receive the confidential information it may
contain. E-mail messages to clients of Denali Water Solutions or any of its affiliates may contain information that is confidential and
legally privileged. Please do not read, copy, forward, or store this message unless you are an intended recipient of it. If you have received
this message in error, please forward it to the sender and delete it completely from your computer system.