Loading...
HomeMy WebLinkAboutWQ0001684_2021 Residual Annual Report_20220228 Non-Discharge Branch Upload/Submittal Form �. NORTH CAROLINA EnWrvnmenfol Quoity Version 2-Revised June 23,2020 Initial Review Reviewer EADS\ndthornburg Is this submittal an application?(Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number(IR)* WQ0001684 Applicant/Permittee City of Asheboro Email Notifications Does this need review by the hydrogeologist?* Yes • No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Brent Collins Email Address* Phone Number* brent.collins@emaresourcesinc.com 336-399-3646 Project Information Application/Document Type* New(Fee Required) Modification-Minor Modification-Major(Fee Required) Renewal Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1, Required) NDAR-2 Annual Report Residual Annual Report Additional Information Change of Ownership Other We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High-Rate Infiltration Other Wastewater Reclaimed Water Closed-Loop Recycle Residuals Single-Family Residence Wastewater Other Irrigation Permit Number:* WQ0001684 Has Current Existing permit number Applicant/Permittee Address* PO Box 1106,Asheboro,NC 27204 Facility Name* City of Asheboro Class B Residuals Program Please provide comments/notes on your current submittal below. At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form,Engineering Plans,Specifications,Calculations,Etc.) 2021 Asheboro Annual Report-WQ0001684.pdf 10.42MB Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre-review until the fee(if required)has been received by the Non- Discharge Branch.Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order(as specified by the application). Mail payment to: NCDEQ—Division of Water Resources Attn:Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Signature ate- -ad Submission Date 2/28/2022 --Resources, Inc. February 28, 2022 DENR/Water Quality Section Non-Discharge Compliance Unit 1617 Mail Service Center Raleigh,NC 27699-1617 Re: 2021 Annual Report-Asheboro Treatment and Land Application of Residuals Permit No. WQ0001684 Dear Sir or Madam: Enclosed is the 2021 Annual Report for the above referenced land application permit. During 2021 EMA Resources, Inc. land applied 1032.05 dry tons of wastewater residuals to 216 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Brent Collins Director of Technical Services brent.collins@emaresourcesinc.com Phone 336.751.1441 —Fax 336.751.1442 755 Yadkinville Rd—Mocksville,NC 27028 EMA ---Resources, Inc. City of Asheboro 2021 Annual Report Residuals Land Application Permit No. WQ0001684 Prepared By: EMA Resources, Inc. Phone 336.751.1441 — Fax 336.751.1442 755 Yadkinville Rd— Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001684 County: Randolph Year: 2021 Facility Name (as shown on permit): City of Asheboro Land Application Operator: EMA Resources Inc. Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the residuals were handled. Part A- Residuals Application Summary: Total number of application fields in the permit: 39 Total number of fields utilized for land application during the year: 9 Total amount of dry tons applied during the year for all application sites: 1032.05 Total number of acres utilizes for land application during the year: 216 Part B -Annual Compiance Statement: Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below)issued by the Division of Water Quality. n Yes 0 No If no please,provide a written description why the facility was not compliant,the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3)copies of laboratory results are attached. 4) Annual TCLP analysis (if required)was performed and three (3)copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a)or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with(applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C- Certification: "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true, accurate, and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Michael R. Wiseman-Plant Manager � L�!�%�Z '^� Jan 26,2022 Permittee Name and Title (type or print) Signature of Permittee Date zygte 1/26/2022 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B WQ Permit Number: WQ0001684 Laboratory: 1) Waypoint Analytical Facility Name: City of Asheboro 2) Residual Source WQ#or 3) NPDES#: NC0026123 4 ) WWTP Name: Asheboro WWTP 5) Residual Analysis Data Conc. Sample or Composite Date Parameter Limit (mg/kg) (mg/kg)a 1/13/21 4/1/21 7/7/21 10/5/21 Percent Solids(%) NA 20.4 20.2 22.7 20.7 Arsenic 75 6.32 7.82 4.67 5.99 Cadmium 85 0.564 0.609 0.758 0.662 Copper 4,300 395 271 305 280 Chromium NA 83.8 64.4 67.8 65.7 Lead 840 28.5 18.8 27.4 18.9 Mercury 57 0.405 0.423 0.559 0.363 Molybdenum 75 36.6 22.6 24.5 19.3 Nickel 420 37 26.7 22.3 17.1 Selenium 100 7.84 4.01 2.56 3.19 Zinc 7,500 931 649 731 696 Total Phosphorus NA 30700 22200 24000 23.500 TKN NA 18400 30500 36500 44300 Ammonia-Nitrogen NA 7790 9900 7360 4090 Nitrate and Nitrite NA 39.5 22.6 87.2 841 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �� - Jan 26,2022 Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001684 Laboratory: 1) Waypoint Analytical Facility Name: City of Asheboro 2) Residual Source NC0026123 3) NPDES #or WQ#: 4) WWTP Name: Asheboro WWTP 5) Residual Analysis Data Sample or Composite Date Parameter (mg/kg) 1/13/21 4/1/21 7/7/21 10/5/21 Aluminum 64200 52500 54200 55100 Calcium 18400 14500 16200 13600 Magnesium 3550 3040 3000 2600 pH 7.6 7.6 7.4 6.5 Potassium 2500 1980 1760 1570 Sodium 1180 1100 1110 1240 PAN 6057 9093 9595 10928 SAR 0.94 0.97 1 1.16 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � � — Jan 26,2022 Signature of Preparer* Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 119.43 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Carl Sardi Owner: Carl Sardi Predominant Soil Series: EnB Acres Used: 23.2 Acres Permitted: 23.2 Site#: GU015 Field#: 1 Residual Analysis Data (Heavy (Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 3 3 L L S L 6 L L 10 11 12 Com 4/1/21 posite Date % Solids 20.2 Arsenic 7.82 Cadmium 0.609 Copper 271 Chromiumr 64.4 Lead 18.8 Mercury 0.423 Molyb- 22 6 denum Nickel 26.7 Selenium 4.01 Zinc 649 Total Phos- 22200 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 5.15 Arsenic 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 2.790 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.790 Chromium 0.663 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.663 Lead 0.194 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.194 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb 0.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.233 denum Nickel 0.275 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.275 Selenium 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Zinc 6.682 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.682 Total Phos- 228.571 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 228.571 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 1 Acres Utilized: 23.2 Land Owner: Carl Sardi Annual Dry Tons Applied: 119.43 Site#: GU015 Acres Permitted: 23.2 Operator: Carl Sardi Predominant Soil Series: EnB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 194 Crop 2 Name: Crop 2 Max.PAN: Volume applied Volume Residual Sources Soil Precip. . o 4 Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 n '� w w TKN o and Receiving Residual ,rt vc (lbs/acre) Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. a w. * w * �. Nitrite Application Waste,etc) Moist) * o Cu.Yds Gallons (Dry Tons/Ac) inches o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4/20 702 20.2 5.148 Asheboro WWTP D <.5" S 0.5 0.2 30500 9900 22.6 93.610 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 702 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 93.610 0.000 Lime Applied Annual lbs/acre 0.081 0.006 2.790 0.663 0.194 0.004 0.233 0.275 0.041 6.682 228.571 Date lbs/ac Prior Years Cumulative lbs/ac 0.405 0.099 16.061 10.497 1.396 0.041 1.68 1.996 0.324 45.033 Current Cumulative lbs/ac 0.486 0.105 18.851 11.160 1.590 0.045 1.913 2.271 0.365 51.715 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 194 "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." d4Z *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 77.22 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Rocking F.Farm Owner: Rocking F.Farm Predominant Soil Series: EnB Acres Used: 7.3 Acres Permitted: 7.3 Site#: GU016 Field#: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 1 2 3 L4 I r 5 L6 I r 7 L8 L9 10 11 12 Com- Piedmont 4/1/21 Water posite 1/21/21 Date %Solids 20.2 24.5 Arsenic 7.82 14.6 Cadmium 0.609 15.8 Copper 271 74.3 Chromium 64.4 3.37 Lead 18.8 12.5 Mercury 0.423 0.0416 Molyb- 22 6 25.2 denum Nickel 26.7 9.1 Selenium 4.01 10.3 Zinc 649 12.6 Total Phos- 22200 1480 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 J 3J 4 J 6 7 L 8 ` 91 1II 11] 12 DT/Ac./ App. CA Event 7.27 3.31 Arsenic 0.114 0.097 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210 Cadmium 0.009 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.113 Copper 3.941 0.491 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.432 Chromium 0.937 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.959 Lead 0.273 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.356 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.329 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.495 denum Nickel 0.388 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.448 Selenium 0.058 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.126 Zinc 9.438 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.521 Total Phos- 322.832 9.789 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 332.621 phorus "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 3 Acres Utilized: 7.3 Land Owner: Rocking F.Farm Annual Dry Tons Applied: 77.22 Site#: GU016 Acres Permitted: 7.3 Operator: Rocking F.Farm Predominant Soil Series: EnB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 194 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. o Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 it-1 7� F, r, • TKN o and Receiving Residual Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. °Q�. w. E' * N. cm p,. Nitrite (lbs/acre) Application Waste,etc) Moist) * ' o' F Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4/21 312 20.2 7.271 Asheboro WWTP D <.5" S 0.5 0.2 30500 9900 22.6 132.222 NA Fescue 6/16 117 24.5 3.307 Piedmont Water Dry <.5" S 0.5 0.4 6040 976 17.6 16.741 16.741 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 429 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 148.963 16.741 Lime Applied Annual lbs/acre 0.210 0.113 4.432 0.959 0.356 0.006 0.495 0.448 0.126 9.521 332.621 Date lbs/ac Prior Years Cumulative lbs/ac 0.248 0.063 11.746 6.072 0.887 0.028 1.145 1.2 0.196 29.255 11/19 2000 Current Cumulative lbs/ac 0.458 0.176 16.178 7.031 1.243 0.034 1.640 1.648 0.322 38.776 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 194 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 86.24 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Rocking F.Farm Owner: Rocking F.Farm Predominant Soil Series: EnB Acres Used: 15.2 Acres Permitted: 15.2 Site#: GU016 Field#: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 21 3 4' 5 10 11 12 Com- 4/1/21 posite Date %Solids 20.2 Arsenic 7.82 Cadmium 0.609 Copper 271 Chromium 64.4 Lead 18.8 Mercury 0.423 Molyb- 22 6 denum Nickel 26.7 Selenium 4.01 Zinc 649 Total Phos- 22200 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3J 4 J 6 7 ` 91 1II 11] 12 DT/Ac./ App. Event 5.67 Arsenic 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 3.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.075 Chromium 0.731 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.731 Lead 0.213 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.213 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.256 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.256 denum Nickel 0.303 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.303 Selenium 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 Zinc 7.365 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.365 Total Phos- 251.926 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 251.926 phorus "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 4 Acres Utilized: 15.2 Land Owner: Rocking F.Farm Annual Dry Tons Applied: 86.24 Site#: GU016 Acres Permitted: 15.2 Operator: Rocking F.Farm Predominant Soil Series: EnB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Pasture Crop 1 Max.PAN: 145 Crop 2 Name: Crop 2 Max.PAN: Volume applied Volume Residual Sources Soil Precip. . o 4 Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 n '� w w TKN o and Receiving Residual ,rt vc (lbs/acre) Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. a w. * w * �. Nitrite Application Waste,etc) Moist) * o Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4/21 195 20.2 2.182 Asheboro WWTP D <.5" S 0.5 0.2 30500 9900 22.6 39.688 NA Fescue 4/22 312 20.2 3.492 Asheboro WWTP D <.5" S 0.5 0.2 30500 9900 22.6 63.501 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 507 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 103.189 0.000 Lime Applied Annual lbs/acre 0.089 0.007 3.075 0.731 0.213 0.005 0.256 0.303 0.046 7.365 251.926 Date lbs/ac Prior Years Cumulative lbs/ac 0.362 0.101 16.49 10.372 1.336 0.038 1.584 1.776 0.301 41.562 11/19 2000 Current Cumulative lbs/ac 0.451 0.108 19.565 11.103 1.549 0.043 1.840 2.079 0.347 48.927 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 145 "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." d4Z *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 135.03 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Levon Hopkins Owner: Levon Hopkins Predominant Soil Series: BtC2 Acres Used: 24.7 Acres Permitted: 24.7 Site#: RD034 Field#: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 1 2 3 ' 4' r 5 • I r 7 t L10 . 11 12 Com 1/13/21 posite Date % Solids 20.4 Arsenic 6.32 Cadmium 0.564 Copper 395 Chromiuir 83.8 Lead 28.5 Mercury 0.405 Molyb- 36.6 denum Nickel 37 Selenium 7.84 Zinc 931 Total Phos- 30700 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total L L3 Li LS L6 t 9 10 11 12 y DT/Ac./ App. Event 5.47 Arsenic 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.069 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 4.319 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.319 Chromium 0.916 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.916 Lead 0.312 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.312 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb 0.400 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.400 denum Nickel 0.405 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.405 Selenium 0.086 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.086 Zinc 10.180 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.180 Total Phos- 335.674 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 335.674 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 1 Acres Utilized: 24.7 Land Owner: Levon Hopkins Annual Dry Tons Applied: 135.03 Site#: RD034 Acres Permitted: 24.7 Operator: Levon Hopkins Predominant Soil Series: BtC2 Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 143 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. a o 4 a i Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 co ', 7� w r, TKN o and Receiving Residual Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. °Qi". w V' co; N. cm p,. Nitrite (lbs/acre) Application Q * Waste,etc) Moist) * ' o' F Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3/9 117 20.4 0.814 Asheboro WWTP D <.5" S 0.5 0.2 18400 7790 39.5 9.858 NA Fescue 3/10 312 20.4 2.170 Asheboro WWTP D <.5" S 0.5 0.2 18400 7790 39.5 26.287 NA Fescue 3/11 357 20.4 2.483 Asheboro WWTP D <.5" S 0.5 0.2 18400 7790 39.5 30.078 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 786 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 66.223 0.000 Lime Applied Annual lbs/acre 0.069 0.006 4.319 0.916 0.312 0.004 0.400 0.405 0.086 10.180 335.674 Date lbs/ac Prior Years Cumulative lbs/ac 0.116 0.013 4.052 1.374 0.318 0.011 0.491 0.469 0.065 12.65 Current Cumulative lbs/ac 0.185 0.019 8.371 2.290 0.630 0.015 0.891 0.874 0.151 22.830 Permitted C.P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 143 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 163.10 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Kimball Markham Owner: Markham Properties Predominant Soil Series: BaB Acres Used: 15.1 Acres Permitted: 15.1 Site#: RD042 Field#: 1 Residual Analysis Data (Heavy (Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 3 3 L L S L 6 L L 10 11 12 Com 1/13/21 7/7/21 posite Date % Solids 20.4 22.7 Arsenic 6.32 4.67 Cadmium 0.564 0.758 Copper 395 305 Chromiumr 83.8 67.8 Lead 28.5 27.4 Mercury 0.405 0.559 Molyb- 36.6 24.5 denum Nickel 37 22.3 Selenium 7.84 2.56 Zinc 931 731 Total Phos- 30700 24000 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 5.94 4.86 Arsenic 0.075 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 Cadmium 0.007 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 4.692 2.966 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.658 Chromium 0.995 0.659 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.655 Lead 0.339 0.266 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.605 Mercury 0.005 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Molyb 0.435 0.238 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.673 denum Nickel 0.439 0.217 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.656 Selenium 0.093 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Zinc 11.058 7.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 18.167 Total Phos- 364.655 233.376 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 598.031 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 1 Acres Utilized: 15.1 Land Owner: Markham Properties Annual Dry Tons Applied: 163.10 Site#: RD042 Acres Permitted: 15.1 Operator: Kimball Markham Predominant Soil Series: BaB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 171 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. a o 4 a i Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 co ', 7� w r, TKN o and Receiving Residual Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. °Qi". w V' co; N. cm p,. Nitrite (lbs/acre) Application Q * Waste,etc) Moist) * ' o' F Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3/8 522 20.4 5.939 Asheboro WWTP D <.5" S 0.5 0.2 18400 7790 39.5 71.941 NA Fescue 8/4 24 22.7 0.304 Asheboro WWTP D <.5" S 0.5 0.2 36500 7360 87.2 5.831 NA Fescue 8/5 360 22.7 4.558 Asheboro WWTP D <.5" S 0.5 0.2 36500 7360 87.2 87.466 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 906 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 165.238 0.000 Lime Applied Annual lbs/acre 0.120 0.014 7.658 1.655 0.605 0.010 0.673 0.656 0.118 18.167 598.031 Date lbs/ac Prior Years Cumulative lbs/ac 0.179 0.039 7.448 3.095 0.588 0.017 0.856 0.739 0.152 21.63 11/19 2000 Current Cumulative lbs/ac 0.299 0.053 15.106 4.750 1.193 0.027 1.529 1.395 0.270 39.797 Permitted C.P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 171 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 67.73 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Kimball Markham Owner: Tony Jackson Predominant Soil Series: BaB Acres Used: 8.6 Acres Permitted: 8.6 Site#: RD042 Field#: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 1 2 3 L L L 6 L L 10 11 12 Com 1/13/21 7/7/21 posite Date % Solids 20.4 22.7 Arsenic 6.32 4.67 Cadmium 0.564 0.758 Copper 395 305 Chromiumr 83.8 67.8 Lead 28.5 27.4 Mercury 0.405 0.559 Molyb- 36.6 24.5 denum Nickel 37 22.3 Selenium 7.84 2.56 Zinc 931 731 Total Phos- 30700 24000 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 4.68 3.20 Arsenic 0.059 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Cadmium 0.005 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 3.693 1.953 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.646 Chromium 0.784 0.434 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.218 Lead 0.266 0.175 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.442 Mercury 0.004 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Molyb 0.342 0.157 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.499 denum Nickel 0.346 0.143 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.489 Selenium 0.073 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090 Zinc 8.705 4.680 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 13.385 Total Phos- 287.045 153.648 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 440.693 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 2 Acres Utilized: 8.6 Land Owner: Tony Jackson Annual Dry Tons Applied: 67.73 Site#: RD042 Acres Permitted: 8.6 Operator: Kimball Markham Predominant Soil Series: BaB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Pasture Crop 1 Max.PAN: 128 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. o Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 it-1 7� w r, • TKN o and Receiving Residual Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. °Q�. w. E' * N. cm p,. Nitrite (lbs/acre) Application Waste,etc) Moist) * ' o' F Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3/9 234 20.4 4.675 Asheboro WWTP D <.5" S 0.5 0.2 18400 7790 39.5 56.624 NA Fescue 8/4 144 22.7 3.201 Asheboro WWTP D <.5" S 0.5 0.2 36500 7360 87.2 61.429 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 378 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 118.053 0.000 Lime Applied Annual lbs/acre 0.089 0.010 5.646 1.218 0.442 0.007 0.499 0.489 0.090 13.385 440.693 Date lbs/ac Prior Years Cumulative lbs/ac 0.095 0.027 4.5 1.887 0.344 0.009 0.477 0.401 0.093 11.946 11/19 2000 Current Cumulative lbs/ac 0.184 0.037 10.146 3.105 0.786 0.016 0.976 0.890 0.183 25.331 Permitted C.P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 128 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 50.47 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Kimball Markham Owner: Markham Properties Predominant Soil Series: BaB Acres Used: 7.1 Acres Permitted: 7.1 Site#: RD042 Field#: 3 Residual Analysis Data (Heavy (Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 3 3 L L S L 6 L L 10 11 12 Com 7/7/21 posite Date % Solids 22.7 Arsenic 4.67 Cadmium 0.758 Copper 305 Chromiumr 67.8 Lead 27.4 Mercury 0.559 Molyb- 24.5 denum Nickel 22.3 Selenium 2.56 Zinc 731 Total Phos- 24000 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 7.11 Arsenic 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 4.336 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.336 Chromium 0.964 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.964 Lead 0.390 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.390 Mercury 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Molyb 0.348 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.348 denum Nickel 0.317 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.317 Selenium 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Zinc 10.392 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.392 Total Phos- 341.184 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 341.184 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 3 Acres Utilized: 7.1 Land Owner: Markham Properties Annual Dry Tons Applied: 50.47 Site#: RD042 Acres Permitted: 7.1 Operator: Kimball Markham Predominant Soil Series: BaB Cation Exchange Capacity(non 503): 0 Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 171 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. o Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 it-1 7� w 7, • TKN o and Receiving Residual Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. RE- w. E' * N. cm p,. Nitrite (lbs/acre) Application Waste,etc) Moist) * o' * w. Cu.Yds Gallons (Dry Tons/Ac) inches o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 8/4 264 22.7 7.108 Asheboro WWTP D <.5" S 0.5 0.2 36500 7360 87.2 136.413 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 264 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 136.413 0.000 Lime Applied Annual lbs/acre 0.066 0.011 4.336 0.964 0.390 0.008 0.348 0.317 0.036 10.392 341.184 Date lbs/ac Prior Years Cumulative lbs/ac 0.082 0.027 3.848 1.725 0.303 0.008 0.402 0.355 0.084 10.544 11/19 2000 Current Cumulative lbs/ac 0.148 0.038 8.184 2.689 0.693 0.016 0.750 0.672 0.120 20.936 Permitted C.P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 171 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 197.19 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Earl York Owner: Earl York Predominant Soil Series: BtB2 Acres Used: 43.5 Acres Permitted: 43.5 Site#: RD101 Field#: 2 Residual Analysis Data (Heavy (Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 3 3 L L S L 6 L L 10 11 12 Com 10/5/21 posite Date % Solids 20.7 Arsenic 5.99 Cadmium 0.662 Copper 280 Chromiumr 65.7 Lead 18.9 Mercury 0.363 Molyb- denum 19.3 Nickel 17.1 Selenium 3.19 Zinc 696 Total Phos- 23500 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 4.53 Arsenic 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 2.538 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.538 Chromium 0.596 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.596 Lead 0.171 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.171 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb 0.175 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.175 denum Nickel 0.155 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.155 Selenium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 6.310 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.310 Total Phos- 213.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 213.051 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 2 Acres Utilized: 43.5 Land Owner: Earl York Annual Dry Tons Applied: 197.19 Site#: RD 101 Acres Permitted: 43.5 Operator: Earl York Predominant Soil Series: BtB2 Cation Exchange Capacity(non 503): 0 Crop 1 Name: Wheat Crop 1 Max.PAN: 100 Crop 2 Name: Crop 2 Max.PAN: O Volume applied Volume Residual Sources Soil Precip. a o 4 a i Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 co ', 7� w 7, TKN o and Receiving Residual Liquid Solids Acre Pert.,Animal (Dry,Wet, Hrs. °Qi". w V' co; N. cm p,. Nitrite (lbs/acre) Application Q * Waste,etc) Moist) * ' o' F Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 10/14 351 20.7 1.407 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 30.744 NA Wheat 10/15 273 20.7 1.094 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 23.912 NA Wheat 10/18 390 20.7 1.563 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 34.160 NA Wheat 10/19 117 20.7 0.469 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 10.248 NA Wheat 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 1131 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 99.064 0.000 Lime Applied Annual lbs/acre 0.054 0.006 2.538 0.596 0.171 0.003 0.175 0.155 0.029 6.310 213.051 Date lbs/ac Prior Years Cumulative lbs/ac o 0 0 0 0 0 0 0 0 0 11/19 2000 Current Cumulative lbs/ac 0.054 0.006 2.538 0.596 0.171 0.003 0.175 0.155 0.029 6.310 Permitted C.P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 100 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied(Annual): 159.78 Permit#: WQ0001684 Cation Exchange Capacity(non 503 only): Operator: Earl York Owner: Earl York Predominant Soil Series: BtC2 Acres Used: 71.3 Acres Permitted: 71.3 Site#: RD101 Field#: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 1 2 3 L L L 6 L L 10 11 12 Com 10/5/21 posite Date % Solids 20.7 Arsenic 5.99 Cadmium 0.662 Copper 280 Chromiumr 65.7 Lead 18.9 Mercury 0.363 Molyb- denum 19.3 Nickel 17.1 Selenium 3.19 Zinc 696 Total Phos- 23500 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 10 11 12 y DT/Ac./ App. Event 2.24 Arsenic 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 1.255 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.255 Chromium 0.294 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.294 Lead 0.085 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.085 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 denum Nickel 0.077 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.077 Selenium 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Zinc 3.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.119 Total Phos- 105.327 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 105.327 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". 1/26/2022 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Asheboro WWTP WQ Permit#: WQ0001684 Field#: 3 Acres Utilized: 71.3 Land Owner: Earl York Annual Dry Tons Applied: 159.78 Site#: RD 101 Acres Permitted: 71.3 Operator: Earl York Predominant Soil Series: BtC2 Cation Exchange Capacity(non 503): 0 Crop 1 Name: Wheat Crop 1 Max.PAN: 84 Crop 2 Name: Crop 2 Max.PAN: Volume applied Volume Residual Sources Soil Precip. . o 4 Nitrate PAN Applied Name of Crop Type (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 n '� w w TKN o and Receiving Residual ,rt vc (lbs/acre) Liquid Solids Acre Fert.,Animal (Dry,Wet, Hrs. a w. * w * �. Nitrite Application Waste,etc) Moist) * o Cu.Yds Gallons (Dry Tons/Ac) inches � o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 10/19 195 20.7 0.477 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 10.420 NA Wheat 10/20 351 20.7 0.858 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 18.757 NA Wheat 10/21 390 20.7 0.954 Asheboro WWTP D <.5" S 0.5 0.2 44300 4090 841 20.841 NA Wheat 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 936 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 50.018 0.000 Lime Applied Annual lbs/acre 0.027 0.003 1.255 0.294 0.085 0.002 0.087 0.077 0.014 3.119 105.327 Date lbs/ac Prior Years Cumulative lbs/ac 0.024 0.003 1.242 0.471 0.082 0.002 0.121 0.095 0.021 3.325 11/19 2000 Current Cumulative lbs/ac 0.051 0.006 2.497 0.765 0.167 0.004 0.208 0.172 0.035 6.444 Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 84 "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." d4Z *Application Method: S-Surface,IN-Injection,INC-Incorporation 1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0 Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) w° Wapoi nt 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 1/21/2021 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 21-014-0058 Client Project Description: Asheboro Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 1/14/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, LCLkc: 0_.)---,--Q--- Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. rrI fR Page 1 of 9 �D • Waypoint^ 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/21-014-0058 Page 2 of 9 \( tanIoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-014-0058 Client Project Description: Asheboro Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 85980 Asheboro WWTP Solids 01/13/2021 09:00 01/14/2021 Page 3 of 9 YY� Waypoi nt.M 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: EMA Resources Inc CASE NARRATIVE Project: Asheboro Lab Report Number: 21-014-0058 Date: 1/21/2021 Metals Analysis Method 6010D Sample 85980 (Asheboro VWVfP) QC Batch No: L532173/L531666 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required. Analyte: Aluminum QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Manganese QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L532264/L531666 Page 4 of 9 Waypoi nt 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°fax 901.213.2440 ANALYTICAL www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Sulfur QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: L532264/L531666 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 v Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro Mr. Brent Collins Report Date : 01/21/2021 755 Yadkinville Rd Information : Asheboro, NC Received :01/14/2021 Mocksville , NC 27028 Report Number :21-014-0058 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 85980 Matrix: Solids Sample ID :Asheboro WWTP Sampled: 1/13/2021 9:00 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Moisture 79.6 % 0.010 0.010 1 01/19/21 16:31 FMM SW-DRYWT Ammonia Nitrogen 7790 mg/Kg-dry 123 123 1 01/21/21 15:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 39.5 mg/Kg-dry 22.9 22.9 1 01/19/21 14:32 ZBD 4500NO3F-2011 Organic N 10640 mg/Kg-dry 245.1 1 01/21/21 15:00 CALCULATION pH 7.6 s.u. 1 01/21/21 15:32 CxC 9045D Total Solids 20.4 % 0.010 0.010 1 01/19/21 16:31 FMM 2540G-2011 Total Volatile Solids 55.4 % 0.010 0.010 1 01/19/21 16:31 FMM 2540G-2011 Total Kjeldahl Nitrogen 18400 mg/Kg-dry 245 1 01/21/21 15:20 CLP 4500NORGD-2011 Phosphorus 30700 mg/Kg-dry 67.6 123 5 01/20/21 18:26 JADS 6010D Aluminum 64200 mg/Kg-dry 113 123 5 01/20/21 18:26 JADS 6010D Arsenic 6.323 mg/Kg-dry 5.88 12.3 5 01/20/21 18:26 JADS 6010D Cadmium 0.5643 mg/Kg-dry 0.490 2.45 5 01/20/21 18:26 JADS 6010D Calcium 18400 mg/Kg-dry 951 1230 5 01/20/21 18:26 JADS 6010D Chromium 83.8 mg/Kg-dry 5.78 6.13 5 01/20/21 18:26 JADS 6010D Copper 395 mg/Kg-dry 7.60 12.3 5 01/20/21 18:26 JADS 6010D Iron 31400 mg/Kg-dry 209 245 5 01/20/21 18:26 JADS 6010D Lead 28.5 mg/Kg-dry 4.41 7.35 5 01/20/21 18:26 JADS 6010D Magnesium 3550 mg/Kg-dry 63.2 123 5 01/20/21 18:26 JADS 6010D Manganese 7450 mg/Kg-dry 7.99 12.3 5 01/20/21 18:26 JADS 6010D Mercury 0.405 mg/Kg-dry 0.0170 0.0770 1 01/21/21 11:26 DDB 7471A Molybdenum 36.6 mg/Kg-dry 3.31 6.13 5 01/20/21 18:26 JADS 6010D Nickel 37.0 mg/Kg-dry 2.94 6.13 5 01/20/21 18:26 JADS 6010D Potassium 2500 mg/Kg-dry 151 245 5 01/20/21 18:26 JADS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 6 of 9 w \Alaypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro Mr. Brent Collins Report Date : 01/21/2021 755 Yadkinville Rd Information : Asheboro, NC Received :01/14/2021 Mocksville , NC 27028 Report Number :21-014-0058 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 85980 Matrix: Solids Sample ID :Asheboro WWTP Sampled: 1/13/2021 9:00 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Selenium <7.84 mg/Kg-dry 7.84 12.3 5 01/20/21 18:26 DADS 6010D Sodium 1180 mg/Kg-dry 319 613 5 01/20/21 18:26 DADS 6010D Zinc 931 mg/Kg-dry 19.9 30.6 5 01/20/21 18:26 DADS 6010D Sulfur 10400 mg/Kg-dry 127 245 5 01/20/21 18:26 DADS 6010D Sodium Absorption Ratio 0.93 Ratio 0.01 0.01 5 01/20/21 18:26 CALCULATION Qualifiers/ DF Dilution Factor J Estimated value Definitions Page 7 of 9 s YV WaypOi nt,. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytica l.com Shipment Receipt Form Customer Number:46245 Customer Name: EMA Resources Inc Report Number: 21-014-0058 Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: I#102 Shipping container/cooler uncompromised? ® Yes O No Number of coolers/boxes received Custody seals intact on shipping container/cooler? O Yes O No ® Not Present Custody seals intact on sample bottles? 0 Yes O No ® Not Present Chain of Custody(COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes O No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. ® Yes O No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No ® N/A Water- VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No ® N/A Soil VOA method 5035—compliance criteria met O Yes 0 No ® N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: KristinaA. McAdams Date &Time: 01/14/2021 13:35:54 Page 8 of 9 j.r 4 U �L F i= F + o N I] 2 m - 1 �, o a n a C] yr N o r� y 9Z Cl? ., roEr a v r a a= v CIJ = CD O d S m a p_ u Q wa y cc g Oa, a a n'7 , 2 i� m p0 ❑ In✓ g C u L W V S Z 2 2 S S y ¢ 0 �j . 3 3 y VS C7 L x { 6 p 2 ii 2 CD ro dP C] a 'uf m V fl W w l7 x ce Ct rd .t xi mil! 1_Il k .e.: -o ,:b ''` 0 --,, I (12) U`+ of . 1 �•+ er o Ecm E n a E w --• .r. g `� E v Hd _ r Cu -'� �J ~ ❑ n m tel a � ,��, E sp{IoS fool v a H ° L I, twi u o N 3iueloie;ea}�N 1 I h in S E'V v V - --. r......gfaa Z a r ° z E e!U€awwd/N)l 2 4r tin 0 I w -.-r 2 �, a 1iJ E 4-, C O m e C �� •�- ,l x C zaU �° m v!' Di- ZA � o a asadwa�)Jo qe.1{9} —__w a am Q i Az, z thayl o;Jam))(limn, -r},i i N - r . cy c t `1 co saaulauoo,pa JagwnN ._. m a n� Tv • ce S a (0 v C ,_ E� • �+ g a m ro {I} o u V g C Z Q a a aci C . 6 {� N 5 E a) E. 9 _ 3 ❑ D. c s m N. O E v, k 0 V 6 .3 . 0 (NI 0 ` L o m `�r a .. m M h a 13 i��� • Q 2 m r w A. i U �p II) CI) ) .2 o w p a V2jZ !" ` Q N w »la) .Ea F LI A x (1 Page 9 of 9 1/13/2021 mg/kg mg/L Equiv Weight Milli Equiv Sodium 1180 240.72 23 10.46609 Calcium 18400 3753.6 20 187.68 Magnesium 3550 724.2 12 60.35 Percent Solids 20.4 Na+ SAR = /2(Ca2+ + Mg2+) SAR 0.94 V w° Wapoi nt 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 4/9/2021 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 21-092-0142 Client Project Description: Asheboro Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 4/2/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, c Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. rrI fR Page 1 of 7 �D • Waypoint^ 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/21-092-0142 Page 2 of 7 \( tanIoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-092-0142 Client Project Description: Asheboro Lab No Client Sample ID Matrix Date Collected Date Received 87859 Asheboro Solids 04/01/2021 10:00 04/02/2021 Page 3 of 7 v Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro Mr. Brent Collins Report Date : 04/09/2021 755 Yadkinville Rd Information : Received :04/02/2021 Mocksville , NC 27028 Report Number :21-092-0142 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 87859 Matrix: Solids Sample ID :Asheboro Sampled: 4/1/2021 10:00 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Moisture 79.8 % 0.010 1 04/07/21 16:43 FMM SW-DRYWT Ammonia Nitrogen 9900 mg/Kg-dry 79.2 495 1 04/09/21 15:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <22.6 mg/Kg-dry 22.6 22.6 1 04/06/21 15:37 ZBD 4500NO3F-2011 Organic N 20590 mg/Kg-dry 1228 2475 1 04/07/21 14:57 CALCULATION pH 7.6 s.u. 1 04/06/21 15:20 ADM 9045D Total Solids 20.2 % 0.010 0.010 1 04/07/21 16:43 FMM 2540G-2011 Total Volatile Solids 53.3 % 0.010 0.010 1 04/07/21 16:43 FMM 2540G-2011 Total Kjeldahl Nitrogen 30500 mg/Kg-dry 2480 10 04/07/21 14:57 CLP 4500NORGD-2011 Phosphorus 22200 mg/Kg-dry 13.7 24.8 1 04/08/21 02:20 TJS 6010D Aluminum 52500 mg/Kg-dry 229 248 10 04/08/21 17:48 JADS 6010D Arsenic 7.82 mg/Kg-dry 1.19 2.48 1 04/08/21 02:20 TJS 6010D Cadmium 0.609 mg/Kg-dry 0.0990 0.495 1 04/08/21 17:43 JADS 6010D Calcium 14500 mg/Kg-dry 192 248 1 04/08/21 02:20 TJS 6010D Chromium 64.4 mg/Kg-dry 1.17 1.24 1 04/08/21 02:20 TJS 6010D Copper 271 mg/Kg-dry 1.53 2.48 1 04/08/21 02:20 TJS 6010D Iron 26300 mg/Kg-dry 42.2 49.5 1 04/08/21 02:20 TJS 6010D Lead 18.8 mg/Kg-dry 0.891 1.49 1 04/08/21 17:43 JADS 6010D Magnesium 3040 mg/Kg-dry 12.8 24.8 1 04/08/21 02:20 TJS 6010D Manganese 7130 mg/Kg-dry 16.1 24.8 10 04/08/21 17:48 JADS 6010D Mercury 0.423 mg/Kg-dry 0.0341 0.0782 1 04/06/21 11:58 DDB 7471A Molybdenum 22.6 mg/Kg-dry 0.668 1.24 1 04/08/21 17:43 JADS 6010D Nickel 26.7 mg/Kg-dry 0.594 1.24 1 04/08/21 02:20 TJS 6010D Potassium 1980 mg/Kg-dry 30.6 49.5 1 04/08/21 17:43 JADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 w \Alaypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro Mr. Brent Collins Report Date : 04/09/2021 755 Yadkinville Rd Information : Received :04/02/2021 Mocksville , NC 27028 Report Number :21-092-0142 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 87859 Matrix: Solids Sample ID :Asheboro Sampled: 4/1/2021 10:00 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Selenium 4.01 mg/Kg-dry 1.58 2.48 1 04/08/21 02:20 TJS 6010D Sodium 1100 mg/Kg-dry 64.4 124 1 04/08/21 17:43 JADS 6010D Zinc 649 mg/Kg-dry 4.01 6.19 1 04/08/21 17:43 JADS 6010D Sulfur 8760 mg/Kg-dry 25.6 49.5 1 04/08/21 17:43 JADS 6010D Sodium Absorption Ratio 0.97 Ratio 0.01 0.01 1 04/08/21 02:20 CALCULATION Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 5 of 7 s YV WaypOi nt,. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytica l.com Shipment Receipt Form Customer Number:46245 Customer Name: EMA Resources Inc Report Number: 21-092-0142 Shipping Method ® Fed Ex O US Postal O Lab 0 Other : O UPS 0 Client 0 Courier Thermometer ID: IT102 Shipping container/cooler uncompromised? ® Yes O No Number of coolers/boxes received Custody seals intact on shipping container/cooler? O Yes 0 No ® Not Present Custody seals intact on sample bottles? 0 Yes O No ® Not Present Chain of Custody(COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes O No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. ® Yes O No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No ® N/A Water- VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No ® N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No ® N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: Makayla Weaver Date &Time: 04/02/2021 14:59:35 Page 6 of 7 JO C. 0_ N U o tli E E E (jam, : :� H P.i NN ...6 ( ^ d 0 O�� vi m u o y w LB VZJ V V N y ti N V Z = p` cuN wacr= z1 a.� pE C7 _C 4 N2 r° vp d u T m ¢p �p` U CI1 N�� iM } ffM -VS Ch �T 4 L+ 4 x S 2 2 N 7 M 1" it i LL MCI 4. ;'a 3 a2. __ CD L2 3 C a yr a m LJ R iY V S .. p .� te a VI Oul OMEI II a ir ,..... LS aCI' C 13 ri 0 j C y -6 ti 00 .1 , i eh di .Ei E 2ct u� � j , ps12 SA1 E g i 'Egli g g Hd ��� �D a TS k %r a C n 8 epos !2}ol 77 N [III .N alU6JC/ e4!N i v Ilhililill ill iuowwbIN)l ! ;Ii ; y app _d o tOfl 109) $4��aW l Iii`` 1111111 4 m = _ `� L�7 le7 m Q ! 1 a a;rsadwo17]ro qet{�1 uPhill � £ 1�``n c c co sraulewo7{o iagwnw .-, MEM (-3-l'Pg111114''5 g ul Et`44- CC c 1 dr C. r...9 6 C 8 . , c ,„ a C_4.. ,..., a 0) o u I. O Q 75 ii 0 _ C W O_ 7 L.a a) u Ct ►r+ r SEllj V co a` a. CO j Q z E 9 0 ` .0 oa `bL9 a o U V It T cx , .5 Z o. r= E y . .T. i- a o _ e� O Et n1 E. 4 J , U La r-2 a Page 7 of 7 4/1/2021 mg/kg mg/L Equiv Weight Milli Equiv Sodium 1100 222.2 23 9.66087 Calcium 14500 2929 20 146.45 Magnesium 3040 614.08 12 51.17333 Percent Solids 20.2 Na+ SAR = /2(Ca2+ + Mg2+) SAR 0.97 V w° Wapoi nt 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 7/22/2021 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 21-189-0097 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 7/8/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, c Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. rrI fR Page 1 of 7 �D • Waypoint^ 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/21-189-0097 Page 2 of 7 \( tanIoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-189-0097 Client Project Description: Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 91317 Asheboro Solids 07/07/2021 06:30 07/08/2021 Page 3 of 7 v Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 07/22/2021 755 Yadkinville Rd Information : Received :07/08/2021 Mocksville , NC 27028 Report Number :21-189-0097 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 91317 Matrix: Solids Sample ID :Asheboro Sampled: 7/7/2021 6:30 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Moisture 77.3 % 0.010 1 07/13/21 16:53 FMM SW-DRYWT Ammonia Nitrogen 7360 mg/Kg-dry 70.5 441 1 07/15/21 15:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 87.2 mg/Kg-dry 20.7 20.7 1 07/21/21 15:40 ZBD 4500NO3F-2011 Organic N 29120 mg/Kg-dry 70.48 440.5 1 07/15/21 11:00 CALCULATION pH 7.4 s.u. 1 07/14/21 14:00 DRS 9045D Total Solids 22.7 % 0.010 0.010 1 07/13/21 16:53 FMM 2540G-2011 Total Volatile Solids 52.1 % 0.010 0.010 1 07/13/21 16:53 FMM 2540G-2011 Total Kjeldahl Nitrogen 36500 mg/Kg-dry 44.1 1100 1 07/15/21 11:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 24000 mg/Kg-dry 12.2 22.0 1 07/13/21 20:57 TJS 6010D Aluminum 54200 mg/Kg-dry 102 110 5 07/14/21 19:47 JTR 6010D Arsenic 4.67 mg/Kg-dry 1.06 2.20 1 07/13/21 20:57 TJS 6010D Cadmium 0.758 mg/Kg-dry 0.0881 0.441 1 07/13/21 20:57 TJS 6010D Calcium 16200 mg/Kg-dry 170 220 1 07/13/21 20:57 TJS 6010D Chromium 67.8 mg/Kg-dry 1.04 1.10 1 07/13/21 20:57 TJS 6010D Copper 305 mg/Kg-dry 1.37 2.20 1 07/13/21 20:57 TJS 6010D Iron 21000 mg/Kg-dry 37.5 44.1 1 07/13/21 20:57 TJS 6010D Lead 27.4 mg/Kg-dry 0.792 1.32 1 07/13/21 20:57 TJS 6010D Magnesium 3000 mg/Kg-dry 11.4 22.0 1 07/13/21 20:57 TJS 6010D Manganese 4850 mg/Kg-dry 7.18 11.0 5 07/14/21 19:47 JTR 6010D Mercury 0.559 mg/Kg-dry 0.0286 0.0656 1 07/12/21 13:58 TJS 7471A Molybdenum 24.5 mg/Kg-dry 0.594 1.10 1 07/13/21 20:57 TJS 6010D Nickel 22.3 mg/Kg-dry 0.528 1.10 1 07/13/21 20:57 TJS 6010D Potassium 1760 mg/Kg-dry 27.2 44.1 1 07/19/21 23:16 JADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 w \Alaypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 07/22/2021 755 Yadkinville Rd Information : Received :07/08/2021 Mocksville , NC 27028 Report Number :21-189-0097 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 91317 Matrix: Solids Sample ID :Asheboro Sampled: 7/7/2021 6:30 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Selenium 2.56 mg/Kg-dry 1.41 2.20 1 07/13/21 20:57 TJS 6010D Sodium 1110 mg/Kg-dry 57.3 110 1 07/13/21 20:57 TJS 6010D Zinc 731 mg/Kg-dry 3.57 5.51 1 07/13/21 20:57 TJS 6010D Sulfur 9160 mg/Kg-dry 22.8 44.1 1 07/13/21 20:57 TJS 6010D Sodium Absorption Ratio 1.00 Ratio 0.01 0.01 1 07/13/21 20:57 CALCULATION Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 5 of 7 s YV WaypOi nt,. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytica l.com Shipment Receipt Form Customer Number:46245 Customer Name: EMA Resources Inc Report Number: 21-189-0097 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other : 0 UPS 0 Client 0 Courier Thermometer ID: IT102 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No 0 N/A Water- VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Makayla Weaver Date &Time: 07/08/2021 16:21:09 Page 6 of 7 - - a N c-a (S. Y f.+ a I. vim" a : () Z g oA �? u 0 a : U U) It 4 h4iIiiNi.. ❑ ro3 . 1IT1'xQ cs w - a2D 20 33 z ; sii Q rnN __ 0. Q " Q 6 N p— w --- � � O 4 g �in L. O u� 40 I _ i i L I - •f 7 xi a 4 — a 16 Y NM a Q A >T . o0 - f �w ♦ - yi S �� n C V L J fl- SAn \ .. C az OV N d r — � U • VI P F y4 O u —LY — 7z ea i w. ❑ G . d �`ff 8 �{ A w u (n 4 A n o 8 5P!IoS Ie1ol 1 a N m y o N 3!ue5JO/a1ea�1N °C N in .c E b `1 r —' I `� 1 Cs-4 g'o d g m e!UOWWVIN)U. m a AlV y • (001Q9) SIe3aW af a i z } 1.3 u L3 c a I� trt 0 _u + ,,tom- 1 L+q m Q ! I f 'a` p` aNsodIuo �o qaft91 V 1 ? \J k •i n _ v 'Mx olaa 1 xu4eyy -F a [�,� " 1 c 7 7 ii CO sr au1eluo3;o AagwnN £ l"'ttt - at cr ea v 2 CY) N € - - i °,. o 1-+ � - _ o 3 = c 0 m 07 m = i° „ V N m g d _ 4 I a. C Z C rya d W Ate] d Q _ & E a ✓ m a a Cr) O 9 L. Y E 0 ...8,, i S1 8 a , via.1 .1 NdN Cu fix 11 ~ Ox a- c a 2 a E f C g Uo .. Z ¢ tJI as N N r tuO .T. ii r c2-2 Vp a } a, �_, V 2 Q t zm � ad 'o ° 1� rCVVVl • �r-+ lsa t• M a. w Page 7 of 7 7/7/2021 mg/kg mg/L Equiv Weight Milli Equiv Sodium 1110 251.97 23 10.95522 Calcium 16200 3677.4 20 183.87 Magnesium 3000 681 12 56.75 Percent Solids 22.7 Na+ SAR = /2(Ca2+ + Mg2+) SAR 1.00 V w° Wapoi nt 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 10/14/2021 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 21-279-0046 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 10/6/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, c Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. rrI fR Page 1 of 8 �D • Waypoint^ 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2022 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001/21-279-0046 Page 2 of 8 \( tanIoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-279-0046 Client Project Description: Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 97123 Asheboro Solids 10/05/2021 11:15 10/06/2021 Page 3 of 8 YY� Waypoi nt.M 2790 Whitten Road, Memphis,TN 38133 Main 901.213.2400°fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: EMA Resources Inc CASE NARRATIVE Project: Asheboro, NC Lab Report Number: 21-279-0046 Date: 10/14/2021 Metals Analysis Method 6010D Analyte: Aluminum QC Batch No: L578167/L577809 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L578167/L577809 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 v Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 10/14/2021 755 Yadkinville Rd Information : Received : 10/06/2021 Mocksville , NC 27028 Report Number :21-279-0046 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 97123 Matrix: Solids Sample ID :Asheboro Sampled: 10/5/2021 11:15 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Moisture 79.3 % 0.010 0.010 1 10/12/21 16:25 FMM SW-DRYWT Ammonia Nitrogen 4090 mg/Kg-dry 77.3 483 1 10/13/21 13:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 841 mg/Kg-dry 24.2 24.2 1 10/11/21 14:30 ZBD 4500NO3F-2011 Organic N 40260 mg/Kg-dry 77.29 483.1 1 10/13/21 09:00 DH CALCULATION pH 6.5 s.u. 1 10/13/21 14:30 DRS 9045D Total Solids 20.7 % 0.010 0.010 1 10/12/21 16:25 FMM 2540G-2011 Total Volatile Solids 56.0 % 0.010 0.010 1 10/12/21 16:25 FMM 2540G-2011 Total Kjeldahl Nitrogen 44300 mg/Kg-dry 48.3 1210 1 10/13/21 09:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 23500 mg/Kg-dry 13.3 24.2 1 10/08/21 20:04 JTR 6010D Aluminum 55100 mg/Kg-dry 112 121 5 10/08/21 20:09 JTR 6010D Arsenic 5.99 mg/Kg-dry 1.16 2.42 1 10/08/21 20:04 JTR 6010D Cadmium 0.662 mg/Kg-dry 0.0966 0.483 1 10/08/21 20:04 JTR 6010D Calcium 13600 mg/Kg-dry 187 242 1 10/07/21 22:07 JTR 6010D Chromium 65.7 mg/Kg-dry 1.14 1.21 1 10/07/21 22:07 JTR 6010D Copper 280 mg/Kg-dry 1.50 2.42 1 10/07/21 22:07 JTR 6010D Iron 17200 mg/Kg-dry 41.2 48.3 1 10/08/21 20:04 JTR 6010D Lead 18.9 mg/Kg-dry 0.869 1.45 1 10/07/21 22:07 JTR 6010D Magnesium 2600 mg/Kg-dry 12.5 24.2 1 10/08/21 20:04 JTR 6010D Manganese 4230 mg/Kg-dry 7.87 12.1 5 10/08/21 20:09 JTR 6010D Mercury 0.363 mg/Kg-dry 0.0307 0.0705 1 10/12/21 14:21 JW2 7471A Molybdenum 19.3 mg/Kg-dry 0.652 1.21 1 10/07/21 22:07 JTR 6010D Nickel 17.1 mg/Kg-dry 0.579 1.21 1 10/07/21 22:07 JTR 6010D Potassium 1570 mg/Kg-dry 29.9 48.3 1 10/07/21 22:07 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 5 of 8 w \Alaypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 10/14/2021 755 Yadkinville Rd Information : Received : 10/06/2021 Mocksville , NC 27028 Report Number :21-279-0046 REPORT OF ANALYSIS Danyale Love Project Manager Lab No : 97123 Matrix: Solids Sample ID :Asheboro Sampled: 10/5/2021 11:15 Test Results Units MDL MQL DF Date/Time By Analytical Analyzed Method Selenium 3.19 mg/Kg-dry 1.55 2.42 1 10/07/21 22:07 JTR 6010D Sodium 1240 mg/Kg-dry 62.8 121 1 10/07/21 22:07 JTR 6010D Zinc 696 mg/Kg-dry 3.91 6.04 1 10/07/21 22:07 JTR 6010D Sulfur 9610 mg/Kg-dry 25.0 48.3 1 10/07/21 22:07 JTR 6010D Sodium Absorption Ratio 1.16 Ratio 0.01 0.01 1 10/07/21 22:07 CALCULATION Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 6 of 8 s YV WaypOi nt,. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytica l.com Shipment Receipt Form Customer Number:46245 Customer Name: EMA Resources Inc Report Number: 21-279-0046 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other : 0 UPS 0 Client 0 Courier Thermometer ID: I#136 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No 0 N/A Water- VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Kristina A. McAdams Date &Time: 10/06/2021 09:48:07 Page 7 of 8 CL Nnv 4i YNI -a"'' l, LJ- a E d IV t 3 0 p M a g P P VYJ '0eU 4-5 0 U 5. a a a 0 I o°n O D ? -o cr.) U _ r. C V. CC"' `6sO ¢ +Z.x s a w E U 0 O fO 3 C =G Y V - C I,!CL± Co. V ❑ 0 I w a m� ° g 8 o ° ry � 8 ¢ a Z. UU22Z2XXU Q a L 2 30 a On QEDUa W 4. S7z » C L NV.a cc re a fl N I N -$ I a a a MIR ii'j5 fa w �� L ,_,, - N — C1I V of I N oU. a _ = � O a .0 a o y 0 — N 15 E D.. �. � E _ 3�� E ( w m , ar m .-E x v a 5111 a) 1 � EE_ ,� _E E_ ❑ W Q N • d d S r F W r � �0 3 Hd _ I —- , � Y N7- 6. d i d ❑ z r� m p a A 1 a u O - C C E splIO I3Lol g a N J ..I' a. D N 3!Ue6JO/aaei1!N e ❑ 70 o - �rt il 2 W E eiuowwd/N)�1 a Q 1 ;. y N W .7 W E ... Q o N cc m C I pi ,: 1- IF c I — {�41�9� 51e]aW > > > N Y g 0 r% ; 4 z C Ca cc us a d • -. a I N V 71 ' am a;�sadwv{�}av qe���] �] a a¢ a o •o .0 (Aax al JapH)xpleoj t -o cr Cr Cr c e c c E _ . saau+ewo);o JagwnN y L w y ' ❑ U r U 1 a C m u. e6 02 L I U C b CS,] o U 0 g a 1 67 ° v ui N t ❑ y a m c d V r d o o N c .o ra E e8 a L a o 2 a ad c LT., a` it C ) = a p 3 ui o; Cl j E Z' ro 0 i ni v a 0::, '~a T " C lz ° ••�Y 0 m N a E /�� v �i }cy- .. �Z a i•ti-1 « zg £ = d m ❑ x . v if' .d a ali v 2 Nyl a m a W N a a Page 8 of 8 10/5/2021 mg/kg mg/L Equiv Weight Milli Equiv Sodium 1240 256.68 23 11.16 Calcium 13600 2815.2 20 140.76 Magnesium 2600 538.2 12 44.85 Percent Solids 20.7 Na+ SAR = /2(Ca2+ + Mg2+) SAR 1.16 V NaclCAnalytical® A \ A L Y T I C A L REPORT 1 National Center for Testing&Innovation January 2 5, 2 0 21 Cp 2 Tc 3 SS EMA Resources 4 Sample Delivery Group: L13O6181 Cn Samples Received: 01/14/2021 5Sr Project Number: 6 Description: Sludge ASHEBORO Qc 7 GI Report To: Mr. Brent Collins 755 Yadkinville Road rAll Mocksville, NC 27028 II 9 Sc Entire Report Reviewed By: ,, dV- Justin Carr Project Manager Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be Aim X. reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ft ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided, and as the samples are received. —1111 IIII Illie p. 4 djill. dr ) e°°. Mb. IMMEni , 110011111 11.7111211.111Mar. ish. ) 11114(1: . 11111- ' j .., i )1 *i I a Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 1 of 20 TABLE OF CONTENTS ONE LAB.NATIONWIDE. * Cp: Cover Page 1 1 Cp Tc: Table of Contents 2 Ss:Sample Summary 3 'Tc Cn:Case Narrative 4 3 Sr:Sample Results 5 Ss ASHEBORO WWTP L1306181-01 5 4 Cn Qc: Quality Control Summary 7 Wet Chemistry by Method 9012 B 7 5Sr Wet Chemistry by Method 9034-9030B 8 6 Wet Chemistry by Method 9045D 9 Qc Wet Chemistry by Method D93/1010A 10 GI Mercury by Method 7470A 11 Metals(ICP) by Method 6010D 12 8AI Volatile Organic Compounds(GC/MS) by Method 8260D 13 9 Chlorinated Acid Herbicides(GC) by Method 8151A 14 Sc Pesticides(GC) by Method 8081B 15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 16 GI: Glossary of Terms 18 Al:Accreditations&Locations 19 Sc:Sample Chain of Custody 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 2 of 20 SAMPLE SUMMARY ONE LAB.NATIONWIDE. * Collected by Collected date/time Received date/time ASHEBORO WWTP L1306181-01 Waste Landon Whitaker 01/13/21 09:30 01/14/21 09:00 1Cp Method Batch Dilution Preparation Analysis Analyst Location date/time date/time 2 - Tc Preparation by Method 1311 WG1608546 1 01/20/2110:37 01/20/2110:37 IDW Mt.Juliet,TN Preparation by Method 1311 WG1608795 1 01/20/2115:01 01/20/2115:01 IDW Mt.Juliet,TN Wet Chemistry by Method 9012 B WG1608874 1 01/20/21 21:32 01/21/2115:51 JER Mt.Juliet,TN Ss Wet Chemistry by Method 9034-9030B WG1608678 1 01/20/21 21:00 01/20/21 21:00 LDT Mt.Juliet,TN Wet Chemistry by Method 9045D WG1607108 1 01/19/2116:48 01/20/21 00:57 WOS Mt.Juliet,TN 4 Cn Wet Chemistry by Method D93/1010A WG1608937 1 01/21/21 03:59 01/21/21 03:59 CAT Mt.Juliet,TN Mercury by Method 7470A WG1609335 1 01/21/2111:52 01/21/2115:16 BMF Mt.Juliet,TN 6 Metals(ICP)by Method 6010D WG1609356 1 01/21/2112:18 01/21/2114:26 CCE Mt.Juliet,TN Sr Volatile Organic Compounds(GC/MS)by Method 8260D WG1609535 1 01/21/2118:08 01/21/2118:08 JLB Mt.Juliet,TN Chlorinated Acid Herbicides(GC)by Method 8151A WG1609799 1 01/22/21 01:29 01/22/2115:33 SSH Mt.Juliet,TN 6 Qc Pesticides(GC)by Method 8081B WG1609775 1 01/23/21 07:04 01/23/2115:13 TAB Mt.Juliet,TN Semi Volatile Organic Compounds (GC/MS)by Method 8270E WG1610414 1 01/23/2111:25 01/24/2110:39 AO Mt.Juliet,TN 7 GI 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 3 of 20 CASE NARRATIVE ONE LAB.NATIONWIDE. * Cp All sample aliquots were received at the correct temperature, in the proper containers,with the appropriate preservatives, and within method specified holding times, unless qualified or notated within 2 the report. Where applicable, all MDL(LOD) and RDL(LOQ)values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form 3 or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been 4 knowingly withheld that would affect the quality of the data. Cn Sr 56 QC 7 GI Justin Carr 8A1 Project Manager 9 Sc Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 4 of 20 ASHEBORO WWTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. * Collected date/time: 01/13/21 09:30 L1306181 Preparation by Method 1311 Result Qualifier Prep Batch Cp Analyte date/time 2 TCLP Extraction - 1/20/202110:37:17 AM WG1608546 Tc TCLP ZHE Extraction - 1/20/2021 3:01:01 PM WG1608795 Fluid 1 1/20/202110:37:17 AM WG1608546 3 SS Initial pH 7.70 1/20/202110:37:17 AM WG1608546 Final pH 5.13 1/20/202110:37:17 AM WG1608546 4 Cn Wet Chemistry by Method 9012 B Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date/time Reactive Cyanide 0.604 0.250 1 01/21/202115:51 WG1608874 6 Qc Wet Chemistry by Method 9034-9030B 7 GI Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date/time 8 Reactive Sulfide ND 25.0 1 01/20/202121:00 WG1608678 Al Wet Chemistry by Method 9045D 9Sc Result Qualifier Dilution Analysis Batch Analyte su date/time Corrosivity by pH 8.14 T8 1 01/20/2021 00:57 WG1607108 Sample Narrative: L1306181-01 WG1607108:8.14 at 20.1C Wet Chemistry by Method D93/1010A Result Qualifier Dilution Analysis Batch Analyte Deg.F date/time Ignitability DNI at170 1 01/21/2021 03:59 WG1608937 Mercury by Method 7470A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Mercury ND 0.0100 0.20 1 01/21/202115:16 WG1609335 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Arsenic ND 0.100 5 1 01/21/202114:26 WG1609356 Barium 0.150 0.100 100 1 01/21/202114:26 WG1609356 Cadmium ND 0.100 1 1 01/21/202114:26 WG1609356 Chromium ND 0.100 5 1 01/21/202114:26 WG1609356 Lead ND 0.100 5 1 01/21/202114:26 WG1609356 Selenium ND 0.100 1 1 01/21/202114:26 WG1609356 Silver ND 0.100 5 1 01/21/202114:26 WG1609356 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Benzene ND 0.0500 0.50 1 01/21/202118:08 WG1609535 Carbon tetrachloride ND 0.0500 0.50 1 01/21/202118:08 WG1609535 Chlorobenzene ND 0.0500 100 1 01/21/202118:08 WG1609535 Chloroform ND 0.250 6 1 01/21/202118:08 WG1609535 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 5 of 20 ASHEBORO WWTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. * Collected date/time: 01/13/21 09:30 L1306181 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND 0.0500 0.50 1 01/21/202118:08 WG1609535 z Tc 1,1-Dichloroethene ND 0.0500 0.70 1 01/21/202118:08 WG1609535 2-Butanone(MEK) ND C3 0.500 200 1 01/21/202118:08 WG1609535 3 Tetrachloroethene ND 0.0500 0.70 1 01/21/202118:08 WG1609535 SS Trichloroethene ND 0.0500 0.50 1 01/21/202118:08 WG1609535 Vinyl chloride ND 0.0500 0.20 1 01/21/202118:08 WG1609535 4 Cn (S)Toluene-d8 98.5 80.0-120 01/21/202118:08 WG1609535 (S)4-Bromofluorobenzene 90.7 77.0-126 01/21/202118:08 WG1609535 (S)1,2-Dichloroethane-d4 95.9 70.0-130 01/21/202118:08 WG1609535 Chlorinated Acid Herbicides (GC) by Method 8151A 60c Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 7 - GI 2,4,5-TP(Silvex) ND 0.00200 1 1 01/22/202115:33 WG1609799 2,4-D ND 0.00200 10 1 01/22/202115:33 WG1609799 8 (S)2,4-Dichlorophenyl Acetic Acid 88.6 14.0-158 01/22/202115:33 WG1609799 Al Pesticides (GC) by Method 8081B 9Sc Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Chlordane ND 0.00500 0.03 1 01/23/202115:13 WG1609775 Endrin ND 0.00500 0.02 1 01/23/202115:13 WG1609775 Heptachlor ND 0.00500 0.0080 1 01/23/202115:13 WG1609775 Lindane ND 0.00500 0.40 1 01/23/202115:13 WG1609775 Methoxychlor ND 0.00500 10 1 01/23/202115:13 WG1609775 Toxaphene ND 0.0100 0.50 1 01/23/202115:13 WG1609775 (S)Decachlorobiphenyl 33.3 10.0-128 01/23/202115:13 WG1609775 (S)Tetrachloro-m-xylene 59.9 10.0-127 01/23/202115:13 WG1609775 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,4-Dichlorobenzene ND 0.100 7.50 1 01/24/202110:39 WG1610414 2,4-Dinitrotoluene ND 0.100 0.13 1 01/24/202110:39 WG1610414 Hexachlorobenzene ND 0.100 0.13 1 01/24/202110:39 WG1610414 Hexachloro-1,3-butadiene ND 0.100 0.50 1 01/24/202110:39 WG1610414 Hexachloroethane ND 0.100 3 1 01/24/202110:39 WG1610414 Nitrobenzene ND 0.100 2 1 01/24/202110:39 WG1610414 Pyridine ND 0.100 5 1 01/24/202110:39 WG1610414 3&4-Methyl Phenol ND 0.100 400 1 01/24/202110:39 WG1610414 2-Methylphenol ND 0.100 200 1 01/24/202110:39 WG1610414 Pentachlorophenol ND 0.100 100 1 01/24/202110:39 WG1610414 2,4,5-Trichlorophenol ND 0.100 400 1 01/24/202110:39 WG1610414 2,4,6-Trichlorophenol ND 0.100 2 1 01/24/202110:39 WG1610414 (S)2-Fluorophenol 51.5 10.0-120 01/24/202110.39 WG1610414 (S)Phenol-d5 31.2 10.0-120 01/24/202110.39 WG1610414 (S)Nitrobenzene-d5 79.4 10.0-127 01/24/202110.39 WG1610414 (S)2-Fluorobiphenyl 82.0 10.0-130 01/24/202110.39 WG1610414 (S)2,4,6-Tribromophenol 91.5 10.0-155 01/24/202110.39 WG1610414 (S)p-Terphenyl-d14 89.0 10.0-128 01/24/202110.39 WG1610414 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 6 of 20 WG1608874 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Wet Chemistry by Method 9012 B L1306181-01 Method Blank (MB) 1 Cp R3615005-1 01/21/2115:05 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/kg mg/kg mg/kg Tc Reactive Cyanide U 0.0390 0.250 3 Ss Laboratory Control Sample (LCS) 4 (LCS)R3615005-2 01/21/2115:06 Cn Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier s Analyte mg/kg mg/kg % % Sr Reactive Cyanide 2.50 2.23 89.3 85.0-115 6 Qc L1306180-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 7 (OS)L1306180-01 01/21/2115:45•(MS)R3615005-7 01/21/2115:48•(MSD)R3615005-8 01/21/2115:50 GI Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg % % % % % 8Al Reactive Cyanide 1.67 0.266 0.994 0.953 43.7 41.3 1 75.0-125 J6 J6 4.17 20 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 7 of 20 WG1608678 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Wet Chemistry by Method 9034-9030B L1306181-01 Method Blank (MB) 1 Cp R3614572-1 01/20/21 21:00 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/kg mg/kg mg/kg Tc Reactive Sulfide U 7.63 25.0 3 Ss L1305552-02 Original Sample (OS) • Duplicate (DUP) 4 (OS)L1305552-02 01/20/21 21:00•(DUP)R3614572-3 01/20/21 21:00 Cn Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD 5 Limits Sr Analyte mg/kg mg/kg Reactive Sulfide ND ND 1 0.000 20 6 Qc L1307070-01 Original Sample (OS) • Duplicate (DUP) 7GI (OS)L1307070-01 01/20/21 21:00•(DUP)R3614572-6 01/20/21 21:00 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD 8 Limits Al Analyte mg/kg mg/kg Reactive Sulfide ND ND 1 0.000 20 9 Sc Laboratory Control Sample (LCS) (LCS)R3614572-2 01/20/21 21:00 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/kg mg/kg Reactive Sulfide 100 92.2 92.2 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 8 of 20 WG1607108 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .41111 Wet Chemistry by Method 9045D L1306181-01 Laboratory Control Sample (LCS) 1 Cp R3614171-1 01/20/21 00:57 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2 Analyte su su % % Tc Corrosivity by pH 10.0 10.1 101 99.0-101 3 SS Sample Narrative: LCS:10.07 at18.9C 4 Cn 5 Sr 6 QC 7 GI 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 9 of 20 WG1608937 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .41111 Wet Chemistry by Method D93/1010A L1306181-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 1 Cp R3614633-1 01/21/21 03:59•(LCSD)R3614633-2 01/21/21 03:59 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 2 Analyte Deg.F Deg.F Deg.F % % % % % Tc Ignitability 126 127 129 101 102 95.6-104 1.57 10 3 SS 4 Cn 5 Sr 6 Qc 7 GI 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 10 of 20 WG1609335 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Mercury by Method 7470A L1306181-01 Method Blank (MB) 1 Cp R3614996-1 01/21/2114:52 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Mercury U 0.00330 0.0100 3 Ss Laboratory Control Sample (LCS) 4 (LCS)R3614996-2 01/21/2114:54 Cn Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/I mg/I % % Sr Mercury 0.0300 0.0296 98.8 80.0-120 6 QC 7 GI 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 11 of 20 WG1609356 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Metals (ICP) by Method 6010D L1306181-01 Method Blank (MB) 1 Cp R3614934-1 01/21/2113:48 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Arsenic U 0.0333 0.100 Barium U 0.0333 0.100 3 SS Cadmium U 0.0333 0.100 Chromium U 0.0333 0.100 4 Lead U 0.0333 0.100 Cn Selenium U 0.0333 0.100 Silver U 0.0333 0.100 5 Sr 6 Laboratory Control Sample (LCS) Qc (LCS)R3614934-2 01/21/21 13:50 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier GI Analyte mg/I mg/I Arsenic 10.0 9.60 96.0 80.0-120 8Al Barium 10.0 9.75 97.5 80.0-120 Cadmium 10.0 9.56 95.6 80.0-120 9 Chromium 10.0 9.75 97.5 80.0-120 SC Lead 10.0 9.83 98.3 80.0-120 Selenium 10.0 9.72 97.2 80.0-120 Silver 2.00 1.73 86.5 80.0-120 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 12 of 20 WG1609535 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Volatile Organic Compounds (GC/MS) by Method 8260D L1306181-01 Method Blank (MB) 1 Cp R3615091-3 01/21/2116:20 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Benzene U 0.0167 0.0500 Carbon tetrachloride U 0.0167 0.0500 3 SS Chlorobenzene U 0.0167 0.0500 Chloroform U 0.0833 0.250 4 1,2-Dichloroethane U 0.0167 0.0500 Cn 1,1-Dichloroethene U 0.0167 0.0500 2-Butanone(MEK) U 0.167 0.500 5Sr Tetrachloroethene U 0.0167 0.0500 Trichloroethene U 0.0167 0.0500 6 Vinyl chloride U 0.0167 0.0500 Qc (S)Toluene-d8 99.2 80.0-120 (S)4-Bromofluorobenzene 89.8 770-126 7 GI (S)1,2-Dichloroethane-d4 96.1 70.0-130 8 Al Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 9 (LCS)R3615091-1 01/21/21 09:32•(LCSD)R3615091-2 01/21/2115:58 SC Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I Benzene 0.250 0.249 0.229 99.6 91.6 70.0-123 8.37 20 Carbon tetrachloride 0.250 0.246 0.240 98.4 96.0 68.0-126 2.47 20 Chlorobenzene 0.250 0.250 0.232 100 92.8 80.0-121 7.47 20 Chloroform 0.250 0.269 0.255 108 102 73.0-120 5.34 20 1,2-Dichloroethane 0.250 0.258 0.245 103 98.0 70.0-128 5.17 20 1,1-Dichloroethene 0.250 0.278 0.259 111 104 71.0-124 7.08 20 2-Butanone(MEK) 1.25 0.865 0.847 69.2 67.8 44.0-160 2.10 20 Tetrachloroethene 0.250 0.271 0.255 108 102 72.0-132 6.08 20 Trichloroethene 0.250 0.235 0.214 94.0 85.6 78.0-124 9.35 20 Vinyl chloride 0.250 0.269 0.250 108 100 67.0-131 7.32 20 (S)Toluene-d8 96.4 97.7 80.0-120 (S)4-Bromofluorobenzene 91.2 93.6 77.0-126 (S)1,2-Dichloroethane-d4 97.2 98.6 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 13 of 20 WG1609799 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Chlorinated Acid Herbicides (GC) by Method 8151A L1306181-01 Method Blank (MB) 1 Cp R3615526-1 01/22/2113:23 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc 2,4-D U 0.000667 0.00200 2,4,5-TP(Silvex) U 0.000667 0.00200 3SS (S)2,4-Dichlorophenyl Acetic 924 14.0-158 Acid 4 Cn Laboratory Control Sample (LCS) 5 Sr (LCS)R3615526-2 01/22/2113:37 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 6 Analyte mg/I mg/I % % QC 2,4-D 0.0500 0.0462 92.4 50.0-120 2,4,5-TP(Silvex) 0.0500 0.0548 110 50.0-125 7GI (S)2,4-Dichiorophenyl Acetic 97.2 14.0-158 Acid 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 14 of 20 WG1609775 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Pesticides (GC) by Method 8081B L1306181-01 Method Blank (MB) 1 Cp R3615893-1 01/23/2113:13 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Gamma BHC U 0.00167 0.00500 Endrin U 0.00167 0.00500 3 SS Heptachlor U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 4 Chlordane U 0.00167 0.00500 Cn Toxaphene U 0.00333 0.0100 (S)Decachlorobiphenyl 72.0 10.0-128 5 Sr (S)Tetrachloro-m-xylene 76.0 10.0-127 6 Qc Laboratory Control Sample (LCS) 7 (LCS)R3615893-2 01/23/2113:27 GI Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/I mg/I % % 8AI Gamma BHC 0.0100 0.00847 84.7 55.0-129 Endrin 0.0100 0.00868 86.8 57.0-134 9 Heptachlor 0.0100 0.00812 81.2 27.0-132 SC Methoxychlor 0.0100 0.0125 125 54.0-155 P (S)Decachlorobiphenyl 56.0 10.0-128 (S)Tetrachloro-m-xylene 70.0 10.0-127 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) •(MS)R3615893-3 01/23/21 14:07•(MSD)R3615893-4 01/23/2114:20 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I Gamma BHC 0.0100 0.00853 0.00907 85.3 90.7 1 14.0-141 6.14 40 Endrin 0.0100 0.00873 0.00945 87.3 94.5 1 10.0-160 7.92 39 Heptachlor 0.0100 0.00824 0.00877 82.4 87.7 1 16.0-136 6.23 40 Methoxychlor 0.0100 0.0136 0.0143 136 143 1 10.0-160 P P 5.02 34 (S)Decachlorobiphenyl 55.5 63.4 10.0-128 (S)Tetrachloro-m-xylene 71.3 76.4 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 15 of 20 WG1610414 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. * Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1306181-01 Method Blank (MB) 1 Cp R3615744-2 01/24/21 06:21 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc 1,4-Dichlorobenzene U 0.0333 0.100 2,4-Dinitrotoluene U 0.0333 0.100 3 SS Hexachlorobenzene U 0.0333 0.100 Hexachloro-1,3-butadiene U 0.0333 0.100 4 Hexachloroethane U 0.0333 0.100 Cn Nitrobenzene U 0.0333 0.100 Pyridine U 0.0333 0.100 6 Sr 2-Methylphenol U 0.0333 0.100 3&4-Methyl Phenol U 0.0333 0.100 6 Pentachlorophenol U 0.0333 0.100 QC 2,4,5-Trichlorophenol U 0.0333 0.100 2,4,6-Trichlorophenol U 0.0333 0.100 7Gl (S)Nitrobenzene-d5 76.9 10.0-127 (S)2-Fluorobiphenyl 79.9 10.0-130 8 (S)p-Terphenyl-d14 91.4 10.0-128 Al (S)Phenol-d5 29.6 10.0-120 (S)2-Fluorophenol 49.0 10.0-120 9 SC (S)2,4,6-Tribromophenol 92.0 10.0-155 Laboratory Control Sample (LCS) (LCS)R3615744-1 01/24/21 05:59 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/I mg/I 1,4-Dichlorobenzene 0.500 0.393 78.6 18.0-120 2,4-Dinitrotoluene 0.500 0.454 90.8 49.0-124 Hexachlorobenzene 0.500 0.478 95.6 44.0-120 Hexachloro-1,3-butadiene 0.500 0.451 90.2 19.0-120 Hexachloroethane 0.500 0.400 80.0 15.0-120 Nitrobenzene 0.500 0.380 76.0 27.0-120 Pyridine 0.500 0.130 26.0 10.0-120 2-Methylphenol 0.500 0.375 75.0 28.0-120 3&4-Methyl Phenol 0.500 0.383 76.6 31.0-120 Pentachlorophenol 0.500 0.391 78.2 23.0-120 2,4,5-Trichlorophenol 0.500 0.454 90.8 44.0-120 2,4,6-Trichlorophenol 0.500 0.435 87.0 42.0-120 (S)Nitrobenzene-d5 79.2 10.0-127 (S)2-Fluorobiphenyl 81.9 10.0-130 (S)p-Terphenyl-d14 86.7 10.0-128 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 16 of 20 WG1610414 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. 41111 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1306181-01 Laboratory Control Sample (LCS) 1 Cp R3615744-1 01/24/21 05:59 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2 Analyte mg/I mg/I % % Tc (S)Phenol-d5 30.9 10.0-120 (S)2-Fluorophenol 50.5 10.0-120 3 SS (S)2,4,6-Tribromophenol 102 10.0-155 4 Cn 5 Sr 6 QC 7 GI 8 Al 9 SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 17 of 20 GLOSSARY OF TERMS ONE LAB.NATIONWIDE. * Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp intended as a comprehensive explanation,and if you have additional questions please contact your project representative. 2 Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, Tc Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received. 3 Abbreviations and Definitions Ss MDL Method Detection Limit. 4 ND Not detected at the Reporting Limit(or MDL where applicable). Cn RDL Reported Detection Limit. Rec. Recovery. 5 RPD Relative Percent Difference. Sr SDG Sample Delivery Group. 6 Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and Qc (S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit(or MDL where applicable). 7 GI Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes reported. 8 If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the Al Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the result reported has already been corrected for this factor. 9 These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control sample.The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL" Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL (Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty Confidence level of 2 sigma. (Radiochemistry) A brief discussion about the included sample results,including a discussion of any non-conformances to protocol Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not being performed on your samples typically,but on laboratory generated material. This is the document created in the field when your samples were initially collected.This is used to verify the time and Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples.These results are provided Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and i tmes of preparation and/or analysis. Qualifier Description C3 The reported concentration is an estimate.The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptable. J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low. P RPD between the primary and confirmatory analysis exceeded 40%. T8 Sample(s)received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 18 of 20 ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. 411 Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network 1 laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing Cp turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. *Not all certifications held by the laboratory are applicable to the results reported in the attached report. *Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2 Tc Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN, 37122 3 Alabama 40660 Nebraska N E-OS-15-05 SS Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 4 Arkansas 88-0469 New Jersey—NELAP TN002 Cn California 2932 New Mexico' TN00003 Colorado TN00003 New York 11742 5 Connecticut PH-0197 _ North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 3 41 6 Georgia' 923 North Dakota R-140 QC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 7 Indiana C-TN-01 Oregon TN200002 GI Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky'6 KY90010 South Carolina 84004002 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'4 2006 9 Louisiana LA018 Texas T104704245-20-18 SC Maine TN00003 Texas 5 LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 _ Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA—ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Pace Analytical National 1313 Point Mallard Parkway SE Suite B Decatur, AL, 35601 Alabama 40160 ANSI National Accreditation Board L2239 — Pace Analytical National 660 Bercut Dr. Ste. C Sacramento, CA, 95811 California _ 2961 Oregon CA300002 Minnesota 006-999-465 Washington C926 North Dakota R-214 Pace Analytical National 6000 South Eastern Avenue Ste 9A Las Vegas, NV, 89119 Nevada NV009412021-1 Pace Analytical National 1606 E. Brazos Street Suite D Victoria, TX, 77901 Texas T104704328-20-18 'Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1306181 01/25/2116:25 19 of 20 I— Billing Information: _ Analysis/Container/Pr servat:ve Chain of Custody Page of EMA Resources Mr. Brent Collins Pres 755 Yadkinville Road Chk aeAnaIi1'755 Yadkinville Road Mocksville, NC 27028 cenn far recR,a nnn arron Mocksville, NC 27028 Report to: Email To:Brent.collins@emaresourcesinc.cam 12065 Lebanon Rd EN74.13 Mount Whet,TN 37122 . F Mr.Brent Collins Phone:615-758-SRSR Phone:800 767 5859 'Project City/State Please Circl Far:615-75R-SRS3 ❑� + IV:11. Description: Sludge 1 1/J1 C � 0 R(� Collected: Asa PT MT CT� '� / Client Project# Lab P ojf 'ect# SDG P ( 1 506, Ili Phone:336-751-1441 Fax: 336-751-1442 v, Ta 1141 Collected by(print): Site/Facility ID# P.O.# IS A1l,bon/ I•'+ /409r, O Acctnum:tMARES Z Template:T11413 Coil cte�,hy�ignacur Rush? (Lab MUST Be Notified) Quote# y G�6/ Same Day _Five Day p 417 J Prelogm:P748424 Next Day _5 Day(Rad Only) Date Results Needed l Z r-i PM:807-Justin Carr I mediatelyIce / Two Day _10 Day[Rad Only) No. �- = ‘) V/ PB:1!� I Packed on N Y _Three Day of J `. - a Shipped Via:FedEX Standard Sample ID Comp/Grab Matrix• Depth Date Time Fntrs J t..1 U Remarks I Sample a(lab only) /9sliabgo [n KI r �- ss /J3# 9, 301 0 z x x i 6 1 { - a I . _ - - _ _. *Matrix: Remarks: Sample Receipt Chec ist S5-Soil AIR-Air F-Filter pH Temp COC Seal Present/Intact: it_tIP Y _N COC Signed/Accurate: 14 N GW-Groundwater B-Bioassay Flow Other Bottles arrive intact: /f N WW-WasteWater Correct bottles used: /Y _%: DW-Drinking Water Sufficient volume sent: _ZY ,N Samples ret ed via: If Applicable , 7 OT Other _ _ XX Tracking# /,S` 7 VO' UPS edEx Courier Z- / r 7 VOA Zero Headspace: —Y _N Preservation Correct/Checked: Y N /7 Relin - he by:( at e Date: Time: Received by:(Signature) Trip Blank Received: Yes/to) RAG screen <0.5 mR/hr: �[ �N �yu/ 0 HCL!MeoH wished by:(Signature) Date: f Time: Received by:(Signature) T_/ °C Bottles Received: If preservation required by Login:Date/Time Z Relinquished by:(Signature) Date: Time Received for lab ;(Sig tur Date:l �if Time: Hold: Conditio ' f / f / gyp O NCF / OK ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQ0001684 WWTP Name: Asheboro WWTP NPDES Number: NC0026123 Monitoring Period: From 1/1/221 To 3/31/2021 Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed(Class A only)indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen DensityNumber of Parameter gExcee- in Frequency Sample Analytical Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 955 3731 64738 col/g 0 Quarterly C 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(thy coliform) weight) Vector Attraction Reduction (15A NCAC 02T.1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) r❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman -Plant Manager Brent Collins; Director of Technical Services Preparer Name eand Title!� (type) or print) Land Applier Name and /Title e((if applicable)(type or print) "tt .-(t Jan 26,2022 1/26/2022 Signature of Preparer* Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503(White House Manual)Appendix D Revised 5-28-14 Fay 1 Date Moisture and Dry Solids Average Dish# 1 0 3 Li c ,• J Wt Dish+Wet Solids, g - g , 911 Li .;1Ug Ro )Go J .g5:9-7 93.3ZR Wt Dish, g r7f. ❑q 5 • '7g f1/0 78.O3j L '7SP.,:27y1 - 75).9 31g WtWetSolids, g 1 . SS'IS(0 , , q .09 _ . t'd9tc I©• _ , I. 5 t1(, 14. 3sit, Wt Dish+Dry Solids, g rJ , 3 3 i.i a , ri q, ii 14y9 7.1,, a �Q "]Q,,.5q$1c . 1 q,3� n Wt Dish, g '�7g. 09 79.1510 . 7sr•03 72: :7y1 , -7 .�i.39 Wt Dry Solids, g O.a38ZF 0.7151 0.2 r . 0. 32u5-' 0.1-Lk{N %Dry Solids 3.05R._ 3.0 C970 3.0, 3.01Q I 5 .O°I,` , 3 .07 Volatile Solids Wt Dish+Dry Solids, g 91, ?y')ttz, 9 CI, s)l lq ri , WAG, 1$, 5q n `7 q , 5(136 Wt Dish+lgn Solids, g rill, ac 99, 265.4.ip 1ci .,1 i-K0 le&,L V?3 rlc( a 13l. Wt Ign Solids, g 0.13 Q.b 5L}3 0.1 i-t 0.t W 3 02q 1 % Vol solid 5�0� 55.14 Z. 5t.e. --4 G S,L2_7 '3' Tl Z 5S , Analyst Checked by ' Day 20 Date 1 Moisture and Dry Solids Average g Dish# r - Z. 3 4 wt Dish+Wet Solids,g 349 2.s-0 F_ 4 3 o 5 ql-e 9 z-Z 88.33(q q 0. 39(07. o9 Wt Dish, g 70- 3I --7 I i 3Q3 .i$•035( 18.2739 -7S•Q34v Wt Wet Solids,9 1 .$Sic), 10. 3031 1 1 .71541 I O n o'))1 . . I L H 1& Wt Dish+Dry Solids, g �g.4 500 1' This,9 t r$.3 gat, ig 57y , r7 8713 WtDish, g -1t•Og31 -11. 13633 "18.05S 18 .273E ''7WO 5117 �x:Wt Dry Solids,g 0.1)Slv9 , Q.1 R Y' 0.35L-I.S , O. Ll 0 3ti a �. %Dry Solids '3.(71 i 3.0 11, 2 (461% Q. Z .41.cli 3 .00 Volatile Solids Wt Dish+Dry Solids, g if AA co --lg.ilLtad r12,3c1Q ,, •571-1 i� ig.'i2 Wt Dish+lgn Solids,g '7 a cy( .P7 7ff 97 g,,q 7/Z '7 '.'b i 7q•oq 0/49 Wt lgn Solids, g 0. 11i_p0 all l Q. 1 54 0•l(OCOa 0 .1Sli % Vol Solids 514.6A 1 ' 5•'-6 'Z 5 5.1 2, JS•'S Z, 5� • 1 Z `75. t Analys i Checked by 20 Day VSR ,''19. Day 4 Date �17•2/ 1 Moisture and Dry Solids Average Dish# I ea, 3IMIMS Wt Dish+ Wet Solids, g el 1.-1,511 ,ci 01515 .it.--5-icf" Egig251 $-7 7 3-7- Wt Dish, g TheI1 _ -71l '!3437 '75• a . o MEMO `15 .93B Wt Wet Solids, g 1-.3 ,10f010t II . in 13 i `�..� '�r�.. $ ,1 qq O Wt Dish+Dry Solids,g /46 , yqicl 1 q f /4 ebiti M f.r• IMITSM 1 q . 1 q13 Wt Dish, g if3.C09 1°1 '11 . 1357 l i'C73 7D MN= -1 3. `i3Fil Wt Dry Solids, g D,kD70 0.3 011 i r a 9 1 p . 1 O, R5` (o %Dry Solids Q,4S% !'), on 'al,• • ' , Q ,' .1, _ a ,q> bb a ,ii u , Volatile Solids Wt Dish+Dry Solids, g 9% ,4 riq ,i1 fo{ 7t ,3cn, 'I%1&O$7c1 I a a )q7 3 Wt Dish+lgn Solids, g l'S, rl rig .3009 . VgrJ1D it 1llQta Z� Wt lgn Solids, g U . IDS. 0. 1cn5 Q• l.�'S'. ,2-. off- O. I Cr/3 ,. f% Vol Solids r 3. (0 3.1 Quo S�,.q Z. . : . : 5 S Analyst L4L) Checked by 40 Day VSR VSR= VS0,igi„ai-VSf„al .'ZZ i` �✓3 ,C9 d (VSoriginai � S VSoriginal-(VSoriginai X VSfinal) 1l4 ' • City of Asheboro January 2021 1 Digester Pilot Plant Temperature Log (Record once per shift) 1st..shift..._ 2nd shift ,�. '�3rd shift':.: Date Time 1 Temp. Initials Time Temp. Initials Time Temp. Initials 1 (P o© . 3_0.- .3_M_ n-i /S3 0 1 311 Chow'"w'... 0.5`C-- j 31.3 *S fe — 11' 2 0-)0 13i,2 Omm /S3o 11,2_ _s3riin 2%00 31.a, 31✓c, 3 07/0 31.E y— 15o5 131.a -. g30o 51,2 5wc 4 045S A DA& IScpo 1 Sx.1 P3`'" . ,/ -se- 5 °705 _31, Z Znifh ISeo -1'2' - Z+A"l .2VA' 7r. g- - " 6 070s I.2 En)n� plot) f31,Z _ omen g3o0 31 ,i Svc 7 (5)os 31, 3 13ri ivi-- (56o ,310 GSM itvk �c.3 Do 5(<S - 5we 8 big.° M.5 TAG IS05 13i3). 7 -r}& / 9,S j 31.3 6ff 9 _ Pmo! -1 •$ 1714, __.. 15110— t.P,S _ - —MG 2 a -u t 0(G1 S fe 10 6)Is 31,2 13vr--i 1560 .31.3 Sm a CA) j Yo- c - _ 11_ 07(0 _i31. G 8)1.101. 1500 131,(e C3r.►rh ,Z3D'O ` 1 A 5 wic 12 o7c.z i 31.1. Ti16. I,(s7 13i.i., T1 C a3°° ! 31, 7 5 'c 13 A705,_ 51. TisG 1500 a 3 w `3 1 - ce 14 o717 , <.5 TN- 1SCsa 3\.7 TW-G 07.3rc> J 31 . ; S.6 15 0109 11.5 6u.i,„ 1So0 ! 31, 5 13r+vv) 2-3 3‘. ce SIC 16 Dloa 31,(P gfton i5©© 1-M,(0 Ban hi 30b 31,(s Swe. 17 . 0/0❑ L• -- 'r4G k5 o 13\ le J'aG a 3Oo 3 .7 SwC 18 D90 I3t,`7 -5W ' 1500 13i.‘, T51.0,G 734-0 1I. SC('' 19 f5706 104 aid 19051 Ilt,5" ..i'-J , 3ru 31• G '" 20 O.?b 1 311r erctJ 1 15' ,31,b c. _ I6‘3p 3),&I e51 21 0`100 31, b oc 1403_ lJ i 5 `Tcc,/ -- 100 21, C CSi 22 T700 31, 5- --5*wc oO0 ! 31, 5 -3w G 1 °MyS 31, 6 c,5S 23 07013 31 .5 . 5c 1500 ; 31, 5 SAC, p36o j I .. -S;if t 24 &p5i 31,(0 `laIV j Sb a 3, ti S' -r C i,� . 2309 1 3) r 843 25 tbs ' 14 . 1.„ Ki4 31, 6 rk,ij 3__ o 3\. 5 _13M� 26 9700 31. 5 -5�c_ V500 131,6 -SwC 00 31.`] cS f 27 0700 31.5 5wc I' 99 1 31. 5 3 tfv L ;x1t,c, 1I. sfe 28 0700 31 7s,- 5i ' / COO ' 3 ,0 15(.,./c ,1VA. 3 ; ` 'N'it, 29 _..trio '", sc,5 121 )5-14 3�,5.' 6 a31P Sz 5 30 ( 341S •IC.0 kiliiS 1 3 ) - <- li 2,360 13115 GrAN 31 0790 ; 3�. ' 'vC /5O3 SZ 5 5 ►v'(-- 1-)66 I -3Z=S 1 13N["1 City of Asheboro February 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift '2nd 3rd: shift Date Time Temp. initials „ Time Temp. Initials Time Temp. Initials 1 0700 3A.S -5,A-C, 1500 ; 3 g.1.1 e23.40 3,2 ce, 2 62/3 3(2. 1;--(A) Nob 3Q.•LI Te-t-i) '3)< 3 ic57.p 34.,q f‘bb Qq "V__)14) 136° 13z°9 6" 4 0,0 2,a rre4 Our '1,1,( vu 7.5ot ervil 5 °7°° 3 Q 16/ 150.0 za.o 3 WC Q3-3,s I32II 6 0709 S2,3 -S4,6 )4-ov , -31v C d_300 3d, g sce 7 6101 33,‘ -Th( (,vf )-50 -sfc 8 0703 37 ( kt) jLi36" ere-k) 1130 31 ecç 9 07oLi -3215 biti141 150o 13 za lalyto -7100 s CO. 10 6/15 M. 5 8m sl }Soo 32,5 f3,0-yyn 23'0 ; ' S'Ict 11 Op) - 32,S Bryirfri o12,S Bayki et$LAD ; -sire 12 E3-20a s-•-•.0- 1 Lr Is/3D 207ia Li >2• 13 065-Z) • ss-o l'SZ 6 ______MAO 14 6705 32. &PI 1506 13M)vi Mor) %a. MC& 15 0719 4S7, _1311/1/1 1506 32, 4 (3/10) Z;OP 1 .5Z,7 N 16 72713t, S„1,1d spx ;A03 11.p ‘b le= 17 4_3 3a0,21r214q -L, ILLAL 10,12.o i 3,Es 7.8.6 is Diocd fQ IA\ I/13 it 12, Ictx t rtsk-9- T/442 19 0116 S2, Brio,/ /Say -52• ffvlyvl kcvic LS2.0 20 OWO 371,-0 ervii )56G 81 S o rytrii 2100 3 i,1 21 Q)cC 41%7 ‘-k-,1^.) 121E, -14_LIJ 22 657 301 tA,1 IS-15/ i- a o 12_0 Icloq . 31.\ TAG 23 oi$ a . 9 wv-i 1500 32.0 (irb)r-i I 900 311 24 0-110 311/ 6111A /1012 13?4,6$ 6/17/A_ '251'3 14-6- 25 7jCL eprr 1505 13z3 Stun 230 # gafi 26 27 28 1 29 30 31 1 CITY OF ASHEBORO 'N Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503(White House Manual)Appendix D Revised 5-28-14 iy Date2 Z( Moisture and Dry Solids Average ..Dish# \ I 3 _ 5- Wt Dish+Wet Solids,g CI 0..30 Z'Z g I.5?o 3 ( .02 o q D-(0 570 $7. Wt Dish, g 15.•013 - (Lfo0 -76-c1,302 78 2 i37 15-g3r:T'- wt Wet Solids,g 12.2.0 (2.'231_, 1 O.7886. 12.3 `g (O. 5 73 Wt Dish+Dry Solids, g ~76.T ZJ_�l. '7 l• Lf g©9 •7 S-3Jo , 7 5•&71 a •7q. 2 32 s' Wt Dish,g -1$.013�a ` or. I qv v 7g-038. .7g- TJ . -^70,q3q Wt Dry Solids,g I 0 �j3(L/ 0.3 4_00 . O.2925 O• J 573 O.2Q 3( %Dry Solids 2.7 % ( G 2.74 2.-7(% 2;72%i , 2.•;12°4 2. 72`'6 Volatile Solids Wt Dish+Dry Solids, g 7SS 47i p -71 L/ 00 .. .�j 3C)'7 75. (o f l(J '7 ci.2 34S Wt Dish+Ign Solids,g 7S. L/H7 , `7q. 2ew:4-7F3.i741- , -713•``2$q ~741•O Wt Ign Solids,g _0. 1777 F O.1137 0 (5 Z O.s432FQ J (0. 1570 %Vol Solids 53.(D°4 •0°ail 63.-°5, 6Lf O 5. ( _ ,706 Analyst Checked by Day 20 Pate z•'Z5-2 Moisture and Dry Solids Average Dish# Wt Dish+Wet Solids,g g5.555 . 6-c .5-1 Ot l cgCi.$Df 5 al 2 5 30 115..10(LID Wt Dish, g . 1 8 • 09'w -Ft. (3q 1 --i g•O3'7O ,1''.'27 27 "7 9 3 7~) Wt Wet Solids,g i 0.`-ko 3 7 9.571.3 1 1 .7 Z (a5 I ` .300.7) d1.627fe 3 Wt Dish+Dry Solids, g 78.371 -( i. 3 g 625 -7 .3 .41 0 --1 Pj-Coto 0 I' 7 .. (1 Wt Dish,g -15, 2O 1ci• (39 1 7�-0370 --iiS•27Z7 -715,01, -/-7 Wt Dry Solids,g , 0.V ` 5 0,214111 (0.31 Zoo_ O.3 87r''it , ®.25 3 %DrySolids 2,(p`7°, _ 2.Ce 6(4 ZZeigDI Z-71 2•CQ S �2 627% Volatile Solids Wt Dish+DrySolids, g .^15.3'7IS `7(u 3 ' --if •3 4G '$•Co %.., 1 1.9 •19 440, Wt Dish+lgn Solids, g "]$.2?2 0,.--1R.25'L 1 18. 1e:8,2e/ Qua -1T tO' sBQ Wt lgn Solids, g 0, (`--9 8 0.1'32 0. 1(Q(4.7 ifl v + 10, 13(a D S 3 -b % Vol Solids 53,sl ' 3, 53:3°6 %:tea'"�1_ S ., I,°' °i Analyst li_� Checked by - A--753. 7 20 Day VSR fr] Day 40 ate3•/7 2j Moisture and Dry Solids Average Dish# I _. 5 Wt Dish+Wet Solids,g 13.a, i -,1-1 , •cj. ' ,q . . Ch 5 , 0� 8 Wt Dish, g '� . 1~1 a 1 IQ . < , i I 11`b .q3 79 Wt Wet Solids, g 5. I e=bl,e% ffalgairi WIMP' w'� o • 0%9 Wt Dish+Dry Solids, g P-145,a 31.'D_g in . t , •�win" -I MI.f 9 .10 33 Wt Dish, g 91). i.la • _EMAMA Minn 1 .q`9 Wt Dry Solids, g 0. 4�a4 0. a, . . V • 0. f ,r5►-1 %Dry Solids off,tplq, es % a . ', Metal a,-1 ti' . a . I Vlo oa:II°l%T Volatile Solids _ Wt Dish+Dry Solids, g rn , WAD ,mat 7' , . 0 ot 7 .141454 7q . J O3 , Wt Dish+Ign Solids, g 'r'195 , 'so '1 9,aoc I_ ?, 1 :_ Pr,. 35 5 'A , 01717 Wt lgn Solids, g 0. 07L13 , 010110 b.DtV i U, 0°146 C).0%163 % Vol Solids 53,3°b 5 .3% 5a. D% 5a,o4% 5'a. °z 5D,5% Analyst Checked by ira--040 Day VSR 4,7 D VSR= VSomg,,,a,-VSar„i VSoriginal-(VSoriginal X VSfinal) City of Asheboro February 2021 Digester Pilot Plant Temperature Log (Record once per shift) _ 1st shift 2nd shift 3rd :shift' , Date Time Temp. Initials Time Temp. Initials Time ' Temp. Initials 0701() SS -5"'C' 1500 3 R,14 A340 3 02•ce 2 62/3 3(2.1 Ti-w) 1'11;lb rr ) 3 ei7 o a , ,34„q tt JQ ,q 1EA4J aso 3 1,(il Swim 4 0'70, aa rre-tut tr 5f.f' 14. 61) 7zocil 97o-0 3 2. c 5 15_00 a wc Q3/,s i?304/17 _ 6 0709 5i2, .S‘ve 6"O'D , -311/ c -se 7 6,0 .3 %g- J I -%ft 8 07® Z 3.:1, 7 rk.s.j 4116- f3P:7 rre_tj J3oi 31 6C'f 07 Nvtri 150.40 3 2. am in ' 9° CO. 10 1:3/15 s 81,1 Ai oci 132,5 bovyyli 34,0 ; .c fe 11 C)7/6 S2,5 all/1'7 LoMiS 601/77 ,X$ •'.; .6 -se 12 D00. izs-,a 14/37) 207,s- 13 0610 3Qjc, jj I CO 6 1r<J,I.1 ictA0 Iaz.z_ 14 005 L3Z. /31,041 t5c5o /900 I -sa. no& 15 070 ISZ,(, 13111Fi 506, _132, 15Z17 tiO 16 7:2761:, 12.1j it 13p xttAD ro,p .,0 17 0'2O I .!'lala '12 ki o 1LJ .n2-0 1_319-5 is PicSd 0 fc tq3 XQIb kekke Tr* 19 0)16 S2, 0 - Bn.tfi So 132'e" 1%.))4-1 kRoc) jhs2.c.) •T•jara_ 20 0700 j3L0 erio-i 1566 1, 31 %cif o mr-) 00 31'1 21 Q.)5 4 ‘cit• ILLJ 121,b 22 6 657 tAl IS-1( 0 iorz_tit) ‘ckoLl ! 31.. TAG _23 0715 31 . 13Pirvl 1500 1-37,0 61-1)1 I 900 24 olio 31 lc? 13tvirki IS?,c) 6/174_. ,gsta 25 0316 .51i? Iginrrl 1505 3Z,1 Shrn 23 " 3( fafi 26 tab% 11.0 fz_ ii.161/ 3 4cJ 27 06 O3i -- c..(„r ii? 2. 7e,14 IctkO 28 O7' sa• iire— 0 65 .3Q' .0EIC 000 A.C) 29 2_300 1Z-11 g 7 30 31 City of Asheboro March 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift `2nd shift ` 'Ord : Date Time Temp. Initials Time Temp. Initials Time I Temp. Initials 700 g2.a T 6 1500 3 _T► 233n 4 71Z f' 2 C ' L C 1'c"NI . tgGv 31a p''3 ' Jai 3 6 6.6 _3),a t --ALB 2 30O 32 5'c- 4 ob ?a,v 12,Li 3a, Tc.I.) gwo i 32D -3 `✓C 5 (,Zs 3,.ck r L5i , -11.15 -036 a 30 o 32,9 "3 w c 6 v703 3a..z , 7136 ILI1l7 ( A.1 7'14r`n Z.?;'0 32, /50 7- OM 313 c_ I4f3r 313 ric 2'30(— 3Z /V 8 ab(( �3.13 (Ai tq9 31,3 30O ► 3 . ,O 5wc . ' 9 ,1-_ �y �53a 17 g30o 32,3 '-swc _ 10 0,7ts 33,y TN. I`{5b 33.0 Tx, „?..z 1 i `�3it 'Sie 11 ocy _ •5_ THg+ 14 p -- 33,5 __ , Zan° )2)-) -- d04.. 12 _ ©�a5" Lie LJ (11o9 3.15" j• 2300 f i5.5 ,'fg _ 13 _ ��J w iz..1 I-aa � 33,y_ . .lc-1_+4 .?S0 V 3 3, 41 n 14 c�1o5 �a3 �{ T1 1'LSo : .i1 `1!'14(� OL3a0 133.4 51-c 15 GZvo. 33.3 ._T'f6_ S 6 33.LI T144 Z 3 03- 133. 3 16 bb'Q 133,E I436 ;33,3 `�C 0/-303 133 .5 -34 old '3, I _ `re', J LLb2I 3,Q '-1!f 0300 333 5wC 18 _c�7 �4i Si 3 Ili a9 ►t.3 I �G gsoQ SS3,( .34,c 19 070,0 33k —. 1146 1`130 133_Z 774f, a300 333..1 20 0 7c,3 ?3 t irk= LI S.S /5 eg 55) — 21 - 10E3 3,� 1rAJ i��� 12,E z300 33.3 fai 22 ‘7611 , 8Pi[✓] 506 32' 3 6 :. 30`O 2g,3 sw 23 70 �s - /14� 03©U j 30,3 �t✓c 24 25 26 27 28 I ; 29 30 31 - CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503(White House Manual)Appendix D Revised 5-28-14 Day 1 Date '5 .�../ Moisture and Dry Solids Average Dish# j '7 ti 5 Wt Dish+Wet Solids, g 4'2, 925i q, I, ewoO7 ei27-7001 el -2= 1Zz( , i5-6164o7 Wt Dish, g S. Uri13 `7(.t3d1 75 . 0:36G176.27I 'j ,`7S.9_3-1'� Wt Wet Solids, g I 4.53408 1 2_.9,?LY? t Lk13 ( 1 13. 'jt 7 (7-©�q 5: Wt Dish+Dry Solids, g `7 S• 1'5 2, 1(-16 711 S3 i`-, -7S:7 41 741.L f Lf L-f WtDish,g `75• 0RJ3 -7q -6399 '7.Q.055p,, 1g,2' i4 .-78. 3�72 Wt Dry Solids,g 0,501 9 -n,Lk3 18 0•` Q , Zt 3_ 0. --77-- 3,3Vie %Dry Solids 3.3 S' 3,37 0 _3.3 • ©Z 3,4-6% 3.z(©a 'yi2 Volatile Solids Wt Dish+Dry Solids, g -7f3 :-5--q5a �Q-5`7I7 ' i1S.531 LI -7S-7411 1 -rq-4-f841` -, Wt Dish+ign Solids,g 78.33143 9.3 L o •-7`6.ZYTS -zq7.5006_ -7 .7.0 L, Wt Ign Solids, g _ 0.2589' , 0.2 Z27 0.2539 O,Z-t orj a.Z ,1 % Vol Solids 5_1.£A 1 d 5 oca 5( 2 4 5 2. d, da 5143 t Analyst Checked by 3 sp (. [' Day 20 Da a 3•2_ -2 Moisture and Dry Solids Average Dish# 3 q 5 Wt Dish+ Wet Solids, g MIPM qb .1 ' . 00753 .~ra 69 $6.11. 40 SS'. agy5- Wt Dish, g NORM • a 134 IS • O 367 ii' l .a-Ja- IS. 937% Wt Wet Solids, g '..5aa ro . Ca ' . (o q .55n (0.351n7 ►,11 Wt Dish+Dry Solids, g I b9`] • ' v76. S 1 to n c , 1J 3 Wt Dish, g •.©" - MAMA ,78-•UJA7 7 . ;7D1) 7 .937E ,Wt DrySolids,g • , a• . Maim 0. V?MS' 0 . a/431 0. 1a . %Dry Solids . 41:,' . . o} 3. , to-,76 3,1 V9, 3 . D`b Volatile Solids Wt Dish+Dry.Solids, g tl .5031 l q.323a /1 .92)2 Sl tea c7. 1353 Wt Dish+Ign Solids, g s"1$.,�I(Q(...0(...01 q.a 9(13 . 1.503 73 � .z 97�( -r79•Q3al7 Wt Ign Solids, g . ow vDDS D, O 1 0 . � 0 . 1.v 1b, , 0. O(&, % Vol Solids LA,Gld� �,%, 4 ,3°b Lt$ :No r ii Li� 01 Analyst Checked by_ 20 Day VSR Day 4 Da e 4.i4-24 v Moisture and Dry Solids __ Average Dish# 1 g,. 3 `- .. Wt Dish+Wet Solids, g 4 , " 33O .1)3.'1'J aS %3.3D I q_^4b3. (031)0 55,5 q95 L Wt Dish, g `)%t . a��3 99 . 1`.1.aa. ri% .a313 9% . 1tD_ ' s , g3c21t, Wt Wet Solids,g. `-4 r‘Q 4 1 �. 10313 5.a o2k 6- .31 `i•. t D6 Wt Dish+Dry Solids, g rAs. al 3 7 • ,chtto leg \cvL.ci .146. `I Spa.,ric b`b�5 " WtDish, g f • i)an3 qa. vita , ' i V3 3 rf•• aJw , c % Wt Dry Solids, g 0, PS Ex) b .1 1 p•,' b . % o(t,1 0. 141., 0. Ili p - %Dry Solids 3 r ate, 3,`¶°2.. a IA% 3.43% 3.QD523•av6 Volatile Solids Wt Dish+Dry Solids, g ', to 7 $. 1e: I g, yb , `-/q 't1S95 . Wt Dish+Ign Solids, g 7 r. 1 0 ELMER -743. I (71 7g •3&47 1 c. n 5--7 Wt Ign Solids, g l► i i ni D, 0111_I (• O3S 0 L O7 _ % Vol Solids \ MilaffillEMOVI .`ra• ro 5 O /in _401 a° t % AAnalyst Checked by 40 Day VSR 4z3, Lib el VSR= VS„.,g,,-VSfuvi VSoriginal-(VSoriginal X VSfinal) City of Asheboro March 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time 1 Temp. Initials Time Temp. Initials 1 700 L.Z.0 Toc. 1500 3.1.0 TA-Co 2311) 73 2 0(0'1- o ieicv .3;:) ,A11_ 3 ,1.3.4& :12LJ i . L vd ° J 32:0Z 4 6/° $-- ait-) i24 :30. 1 g300 3,7-0 5 07 NS k-ck rti6 L5_/0 , Z1. nu, g goo I 3 2,0 6 0701 12.:z 7A6 -rA6 7 _0-70,0 as3 rrc—t4) 313 20() '3Z/2. 8 bb(5' 313 -re. 1414/2 32,3 IL(Ai 3c)c ,oSwc g300 32,3 io 33,1 -7746, Jila, I 33 q yz LA) ,4 3, 1 1 '33.5 "1-1—`V—G _TAO Z7 0 72,9 ( 12 °66-a 33S (1' iAJ (1109 3 (6- IJ 70 13 006.-3 7ov 3 3, 3-,,c 14 0/05 -MG 5 0 1 331 171-6, e)300 133.11 15 crs= 4.313_ -rii_s? ias 711-(._ 2 5" 33. /99 16 olDSV' 133,a 1244 143 17 o7b -Bd. 1 ,J jjQ C300 l333c 19 oLf i3Q A ia ttj 140.9 33J 7<44 gsoo 33,( 19 0,70,0 Z5A._ 14 3 13 TAG a3©0 33.1 z-tdc. 20 - -CL7c'5 33k -046 s s %.s .-Z3c, 33.) Ag..fi 21 10S- ,T3 T-A) tqtm `3Q..s7 lai„) f-300 L33,) .1. 22 (-1_ bin, 506 132,3 IS t`iv-i .:23a0 ! 291 ')0 3 .5 tOJC 23 7 cpc., 52. 24 7o5 2.. TM(• 145'5 !-52.3 Mc, ,23c0 i Sg.3 get 25 0 1/ 315 114::) IS 00 H-32.3ii2340 Z __ 26 /vs S 2 7:4(9 ra6 Z-3 13245 27 100 _ Zi 15;41tA i600 3i, 8' srvriSIO 13-5, 1 28 liot, 33'6 _41 13,3g rfc_W g 500 29 7c)sl .12 _ . 1i3t, %)Oa a AO. 30 700 3 f 31 13ca "11 19 (10% I 0 1 3110 al%101 °D° 3'9"(1 Stl" City of Asheboro April 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials 1 - 7cc 32` 13n'ir� f 32- fM1'1 - 2 i30 32 .ss . /3i i )5, 32.K iceim g 300 330 -0-G/C 3 70ue—__. 33' _s_ _ _ 13 Itcap 3.3 ._Tn G __ 2 Q 9 _ 3J ,.6a5 'o0 33 Z m 4 ,'3s-3 ,� /sma ,3 Z3 o TO *5 5 1. 33.1. 13ai i /5-e Z3 6v4 a 304 33,3 -5 6 705 33• TA& Ns o 33.3 T'A-G 114 1 3?,3 C.S S 7 703 33.3 Tom-- - 143 5 .33.Y. - - �3� 5 8 7 tZ 33.3 TAB 4 5 v 6 33.3 7,96 7,429 33-) 9 125' '33.3 I3 �. /sow 33,3 � i t i 23 2 33.? e 10 o0 313, '1 13p, 33.4 ? -2 3°D 33. Cf I Vik, PISS__ N T -- 3..?O 23,4 Css 12 700 33.3 TM I't5 33.3 TAG Z300 133 . 13 t,761 23 rc --�43 _ 3A` _ ga L,� o j 33.3 esc. ! 193a 33. css 14 �c5c, 3 3• Z $ram Nt LSe� �2� �M.r-► � , 15 73 a 13?- a A,tit j53 ;3z q ,w, 19 36 3). Gs� 16 0700 33. I riavJ 00 ,33•a C5f 17 18 _ 19 I — - -- -- 20 21H -- - _ I 23 25 26 _ I f 27 — I 28 ti 29 30 31 Th City of Ar"_boro Department of rester Quality Fecal Coliform in Sludge �;-; Sample Collection Ci) Sample# i2� ' n a) .1 5_) CO (1) Date -3/• 2I 3. 2• 2-1 S- q• z 5 • 9. 2I 3. 10• 2-f 3 ' 10 • z-f 3 •II,Z1 Time, 0 1 1,44 II2-!r I.431 _ 0616i( 1333 , 11SfS Location ancpvera,bul Vrit4tiakizA bidyauavci b1(45 ---_____�y ") :Analyst .-, 6MI, EM1_ RMt- FJML. 1if'tl_ gM Ir %Solids Dish Number ' S 4 5 Ip• -1 Wt Dish&WtS lg- 0e 7 10-717F 11 - El2_L. Lo 15. 1S le , 9 13 is, psis 10. tt>z4 butDI1 .56,37 0m7(iLi 0, 1119 0 .(;)13t 0-ITS 0.% of 0.971Z WtWetsoHds r l55b57) 1 .01234 10. ri5417 19, 18So g. "750S 14. 08z9 el . 19Oy Hilt Dish& Dry-S 5775-15 3.2 2 S f, 3.,1a s 4. '.3s547 , j -1 0(3 ,3 -1 C)10 9 2-`'l S Wt Dish Z.C31037 0. Twq- 0 .9`11 a a .9 1 i, 0. cil 7S 0.1IQ`d°J . 0 . 9-1(-1 Wt.Dry-Scilicis 3.157 . e.Z5'l2 2.104-1-110 33iti I --13g$ _ 07-86 _ 1 _ Cil i5 96 Dry Solids 2D.& th 22.'7 d� 2J..2`7 2 3-g .7. 1 i 9. 21_S 9, 2,1-g la Analyst ?fil-i,=, .'1',M[ r'�i- 4L_ E mt._ $M L $nil. 8 M� Fecal Coliform Date In 3 I ti 3•9.-7-4 3Ff. za 31*. z.4 ' .3 - f o• sl 3- 10/?-1 3. 1i -1-f , rl-u Time in 1 33 15y3 135[F 12:12 1217_ 1301 1307 Analyst in $Aqc_ 6'ML- 6ML L. 1114 t._ 8mt.- 8M _ 6n1 L ml sample #colonies *colonies Sicolonies it colonies #colonies #colonies #colonies 04001 i 6 _] 0 00 -7 0 7 0.0003 4 0 I 0 7 0 0 0 aon7. i 3 b I; 0 0 0 3 okoa --yi 0 J 447 -j6 I 2.. .A 0 -s 0 es Fecal Caiifc raa/R` .111_37637 4.i 1 b 0 I � S. it 9 5 Sk 2128 y <11 051 < i 10101 17:az, gram Dry Siudge , jf ,I0'7 ��1c R,,rt., ►R�-c Zb --R.I6 210 -kick Zb Buie V6 `► III DateOut 3-1e 3- ►0 • 2-f 3- I0. 2- 5 - 1H-2-1 3-11.2ii - i2-z( 1- iL• Li Time Out i111 12V1 12-11 1140 1146 1111 • nil Analyst.00. 8l l L S W1_ 5 Al Sni L.- 6fV1 L- "13m_ SPA L Coliform Colonies/gram=Coliform colonies counted X 100 ml X%Dry Solids -----., Geometric Mean + ( 3 i ) 3 5 i o-24., �j 13O C , m r Cite of ca jeboro % Dry Solids for Sludge Hauling Date 3/1/2-1 , 3 /1/Zt 3/i°'/Z/ 3 /0/2-r Analyst Initials a-4k' /3n-r[J 1 ML Dish Number a5 0 Source P % (1-A kt �i-C-5sCakpj )2ntS'S Caks2, Presc cdace, Wt. Dish &Wt. Soiid (g) j 3 £ 431 -75 7. � L1 BD 13_ '2)f0 3 111. Wt. Dish (g) aR • QQ LF7 -78 .812319 _ ��?_� 7 •g1 Wt. Wet Solid (g) ct . 1 55-7 1e{ , 11-1-19 1 5_ Lluoi j Wt. Dish & Dry Solid (g) cb b. ni41411 ISD-QZ 3 �l g 4 Zl 41. ell 1"-`, Dish (g) -i9. 0412(o T1S-gJS4 WL Dry Solids (g) rJ Z. I 2, 1 '11 S 3, lq 0 % Dry Solids al .Q sD 23,2.7. 19_ 9 % t0. 10`Z Weight(Ib/ft3) Ibt q cl 1 s S2- i IL( S-t7161 Operators Initials CIS GP- _ CPS C'S JANUARY 20211 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS • Dig ,Influent Dig Effluent % # DATE D-GALS D % S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tem,%vol Re'D#1 tern D#2 Tern % Solids %Vol Inf % Solids %Vol CO2 Dig 1 22700_ 0.0609 11529.47 0.02234 115472.5 30.5 125 116 135 6.09 71.6 42 2 2 17200 0.0542 7774.882 0.01218 97708 41.3 125 115 135 5.42 69.1 44 2 3 18300 0.0654 9981.479 0.00584 75501 40.0 125 116 134 6.54 63.4 45 2 4 15300 0.0625 7975.125. 48710 11903 8120 0.0196 1327 62178 48.7 126 37.7' 116 135 6.25 67.6 3 56.5 46 2 5 25500 0.065 13823.55 47966 11601 9920 0.023 1903_ 94155 28.0 126 36.6 117 135 6.5 66.2 3.01 55.4 44 2 6 23300 0.0536 10415.66 44699 11407 8760 0.02055 1501 106590 30.1 126 25.8 117 135' 5.36 66.1 3.08 55.6 42 2' 7 13800 0.0603' 6940.048 25557 6437 9500 0.02565' 2032 129685 49.1 126 40.1 117 135 6.03' 68.1 3.11 56.1 42 2 8 30400 0.0607 15389.64' 8620 0.03416 2456 62178 24.5 126 116 135 6.07 68.4 46 2 9 17500 0.0483 7049.385 0.03572 106590 40.1 124 116 133 4.83 71.2 45 2 10 14600 0.0517 6295.199 0.03636 106590 48.0 126 115 136 5.17 72.6 40 2 11 30100 0.0479 12024.53' 36352' 8277 9660 0.03872 3119 74613' 24.4 126 51.8 115 136' 4.79) 71.2 2.95' 54.4 42 2 12 28100 0.0506 11858.31 ' 47311' 11679 9160 0.04297 3283 75501 26.1 125 51.1E 117 134 5.06 71 W 2.99 54.5 44 2 13 24200 0.0518 10454.69 9300 0.04777 3705 97708 29.3 125 117 134 5.18' 72.6 44 2 14 14100' 0.0631 7420.181 58675 14240 9060 0.05105 3857 66619 52.6 123 55.6 112 134 6.31 73.4 3.04 55.7 44 2 15 25700 0.0537 11509.95 47291 11556 8720 0.05084 3697 106590 27.3 121 60.8 103 138 5.37 75.4 3.04 54.6 42 2 16 13000 0.0554 6006.468 0.05409 124355 52.6 121 103 140 5.54 71.7 42 2 17 15400 0.053 6807.108 0.05239 111031 45.2 123 103 143 5.3 70' 46 2 18 28900 0.0485 11689.76 0.04913 93266 24.7 123 103 143 4.85 69.8 40 2 19 24600 0.0476 9765.806 46703 10750 8140 0.05265 3574 62178 30.3 123 49.1 103 142 4.76 70.6 2.83 55 44 2 20 33300 0.0443 12303.08 47893 11064 8560 0.05309 3790 84384 21.7 123 51.1 103 143 4.43 70.6 2.72 54 40 2 21 21600 0.0427 7692.149 48285 11598 7480 0.05043 3146 106590 32.5 123 49.1 103 144 4.27 70.6 2.78 55 42 2 22 31600 0.0678 17868.28 36340 7759' 8140 0.04808 3264 115473 21.9' 128 47.6 113 143' 6.78 70.4 2.7 55.5 42 2 23 17000 0.0506 7174.068 0.03755 119914 40.5 134 127 142 5.06 73 47 2 24 16100 0.0509 6834.547 0.03969 106590 43.61 133 125 142 5.09 71.1 42 2 25 29200 0.0454 11056.17 36235 8220 8100 0.04219 2850' 106590 24.0 133 48.5 124 142 4.54_ 70.2 2.72 54.8 42 2 26 20500 0.0536 9163.992 47616 9610 7120 0.01961 1164 88825 35.1 132 48.1 124 140 5.36 69.5 2.61 54.2 44 2 27 32400 0.0534 14429.53 48009 10010 9540 0.03375 2685 115473' 21.4 133 41.6 124 142 5.34 68.1 2.68 55.5 44 2 28 29300 0.0562 13733.14 12707 2671 7160 0.021 1254 124355 23.3 123 45.4 110 136 5.62 69.8, 2.71 55.8 42 2 29 32400 0.0508 13726.97 35372 7346 9080 0.03638 2755 106590 21.6 120 44.7 104 136 5.08 69.2 2.66 55.4 40 2 30 26300 0.047 10309.07 0.03684 88825 27.3 121 104 137 4.7 67.1 42 2 31 24100 0.0617 12401.33 0.00875 75501 30.4 122 104 140 6.17 68 44 2 TOT 716500 1.6786 321404 715721' 166128 164140 1.102 51365 3007615 1036.159 3891 784.7 3501 4282 168 2168 49 938 1335 62 AVG 23112.9 0.054 10368 42101.2 9772.2 8639 0.036, 2703 97020 33.42448 125.5 46.1588 113 138. 5 69.9, 3 55.2 43. 2 tS FEBRUARI 2021 1 1 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D% S D- LBS PR GAL PR LBS RAS Nit Gal 'Nit Lbs Gal Room Det Time Avg Tern % vol Re D#1 tern D#2 Tern % Solids %Vol Inf % Solids %Vol CO2 _Dig 1 28900 0.0506 12195.92 47773 9363 9440 0.03372 2655 53295 26.1 122 39 104 140 5.06 65.9 2.56 54.1 42 2 2 22000 0.0505 9265.74 49466 9860 9920 0.03918. 3241 71060 33.5 123 43.9 104 141 5.05 68.9 2.62 55.4 0 2 3 368001 0.0511 15683.2 50196 10424 9240 0.03885 2994 88825 19.5 123 44.9 104 141 5.11 68.4 2.59 54.4 40 2 4 334001 0.0516 14373.49 61150 12903 6380 0.04101 2182 97708 21.3 122 45.2 104_ 140 5.16 67.3 2.64 53 42 2 5 30700 0.0488 12494.65 49706 10654 9260 0.03968 3064 115473 22.6 122 37.4 104 140 4.88 66.5 2.73 55.41 40 2 6 21600 1 0.0578 10412.32 0.03792 133238 31.2 121 102 140 5.78 67.8 44 2 7 333001 0.0526 14608.18 0.00123[ 106590 21.1 122 102 142 5.26 66.7 40 2 8 441001 0.0501 18426.48 36504 8403 9640� 0.03816 3068 67507 16.8 122 42.6 103 140 5.01 68.2 2.88 55.2 40 2 9 29600 0.0506 12491.32 51964 11571 9920 0.04089 3383 71060 24.9 122 40.4 104' 139 5.06 67.3 2.94 55.1 42 2 10 26700 0.0501 11156.17 50508 11879 9440 0.04514 3554 79943 27.3 123 _ 48.4 105 140 5.01 69.9 2.89 54.5 42 2 11 34400 0.0571 . 16381.76 55156 13110 9320 0.03415 2654 88825 20.9 123 51.3. 105 141 5.71 70 2.98 53.2 42 2 12 39200 0.0491 16052.16 53488 13740 8960 0.04261 3184 115473 17.7 122 45.3 106 137 4.91 67.7 3.2 53.4 38 2 13 26400 0.0427 9401.515 0.02192 115473 26.2 122 107 137 4.27 68.4 38 2 14 23400 0.0607 11845.97 0.00003 97708 30.3 123 107_ 139 6.07 66.2 _ 42 2 15 29100 0.0528 12814.24 44148 11230 9160 0.00007 5 79943 25.0 124 44.7 107 141 5.28 67.8 3.11 53.8 44 2 16 24600 0.0577 11837.96 42098 10603 9680 0.00039 31 79943 29.61 124 38 107 141 5.77 64.6 7 3.1 53.3 44 2 17 34400 0.052 14918.59 41066 10788 10940 0.05289 4826 106590 20.4' 124 43.7 107 140 5.2 65.7 3.16 52 42 2 18 25500 0.0453 9633.951 44430 11857 10040 0.02351 1969 97708 27.8 123 41.9 106 140 4.53 68.2 3.25 53 42 2 19 29700 0.0678 16793.92 42050 10977 9900 0.00002 2 115473 23.3 123 42.8 106 141 6.78 71.5 3.12 55.1 42 2 20 10700 0.0649 5791.546 0.04431 128796 63.5 124 106 143 6.49 74.1 44 2 21 13800 0.0479 5512.907 0.05266 106590 50.8 127 108 145 4.79 69.3 42 2 22 28700 0.0518 12398.74 44204 11281 10860 0.03331 3017 97708 24.7 125 51.1 106 143 5.18 70.3 3.19 52.1 40 2 23 22800 0.0443 8423.734 51884 13328 11280 0.06646 6252 115473 30.4 124 51.9 106 142 4.43 72 3.27 51.8 42 2 24 29800 0.0466 11581.59 31860 8078 10700 0.06473 5776 133238 22.6 125 53.2 106 144 4.66 74 3.16 52.2 44 2 25 35600 0.0507 15053.03 38472 9497 9900 0.06667 5505 133238 18.9 124 50.2 106 142 5.07 71.9 3.12 52.1 42 2 26 30700 0.0476 12187.41 20938 5256 10380 0.04246 3676 124355 22.3 123 54.5' 106' 141 4.76 73.4 3.17: 52.2 40 2 27 14900 0.0526 6536.392 0.01161 106590 47.1' 124 106 143 5.26 69.5 42' 2 28 16100 0.048 6445.152 0.03975 97708 44.1 125 106 145 4.8 68 43 2 TOT 776900 1.4534 334718 907061 214801 194360 0.953 61039 2825523 789.8781 3449 910.4 2950 3947 145 1930T 60 1071 1125 56 AVG T 27746.431 0.052 11954 45353.1 107401 9718 0.034 3052 100912 28.20993 123.2 45.52 105 141 5 68.9 3 53.6 40 2 r MARCH 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D % S D- LBS PR GAL 1 PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern D#2 Tern %Solids %Vol Inf % Solids %Vol -CO2 Dig 1 41600 0.0487 16896.17 40194 10291 10440 0.05033 4382 83495.5 17.4 124 42 105 144 4.87 70.4 3.22 53.4 48 2 2 22200 0.0451 8350.175 50424 13205 12160 0.06909 7007 88825 32.4 124 63.5 106 142 4.51 74.8 3.19 52 40 2 3 31800 0.0465 12332.36 50138 12795 9940 0.06437 5336 111031 21.9 124 53.2 105 142 4.65 74.6 3.15 52.9 40 2 4 40900 0.0257 8766.424 40520 10949 10440 0.0648 5642 124355 16.7 123 49.2 106 141 2.57 73.3 3.31 51.5 40 2 __ 5 21900 0.0682 12456.46 48194 13264 10320 0.04358 3751 106590 32.0 122 41.2 106 138 6.82 80.7 3.18 64.8 38 2 6 19300 0.0543 8740.237 I 0.03952 142120 34.5 123 106 140 5.43 73.3 42 2 7 24200 0.0416 8396.045 0.04466 120802 28.4 122 106 139 4.16 69.1 ' 40 2 8 38600 0.0462 14872.89 30134 8017 10220' 0.0586 4995 106590 18.2 127 36.8 117 136 4.62 67.9 3.32 52.9 42 2 9 36900 0.0442 13602.37 39052 10911 12920 0.08838 9523 97708 19.2 127 55.4 118 136 4.42 74.8 4.62 68.1 38 10 35300 0.0494: 14543.46 40020 11582 10600 0.08611 7612 128796 19.2 124 75.2 116 132 4.941 75.8 3.56 53.1 39 2 11 54700 0.0442 20163.95 40092' 11302 10380 0.08615 7458 97708 13.0 127 55.2 115 139 4.42 74.2 3.48 52.4 39 2 12 36200 0.0565 17057.8 50338 13938 9880 0.06964 5737 88825 19.9 122 52.9 116 128 5.65 74.1 3.59 53.8 42 2 13 16600. 0.0627 8680.439 0.04252 103037 42.5 122 115 130 6.27 72.2 40 2 14 30000 0.0552 13811.04 41224 11414 0.03541 93266 23.8 122 48.7 114 130 5.52 71.2 3.53 53.2 38' 2 15 36200 0.051 15397.31 29984 8402 8560 0.04149 2962 115473 19.1 123 52.7 114 132 5.1 72.2 3.47 53.2 40 2 16 30900 0.0426 10978.28 50228 14033 8840 0.04333 3195 88825 23.3 122 52.11 114 129 4.26 74.7 3.5 54.2 40 2 17 25900 0.0477 10303.49 40178 11091 9080 0.03937 2981 115473 26.7 123 56 115 130 4.77 74.7 3.44 53.3 38 2 18 36500 0.0476 14489.92 40152 10816 9860 0.03266 2686 122579 f 18.8 124 50.5 115 133 4.76 73.7 3.35 54.21 38 2 19 28600 0.0738 17603.07 40178 10656- 8980 0.02767 2072 124355 23.9 124 50.5 114 135 7.38 72 3.16 54.8 40 2 20 17500 0.0541 7895.895 0.0414 133238 38.5 127 114 139 5.41 76' 38 2 21 27000 0.053 11934.54 0.03933 111920 25.8 128 114 142 5.3 66.6 38 2 22 40700 0.0608 20637.83 31138 7973 10000 0.04944 4123 79943 17.9 128 114 142 6.08 70.7 3.32 54.8 36 2 23 36600 0.05 15262.2 52249 13596 9740 0.06685 5430 84384 19.8 127 49.7 114 140 5 71.4 3.2 54.7 36 2 24 28300 0.0487 11494.27 51426 13725 8300 0.06453 4467_ 102149 24.9 128 50.2 114 142 4.87 72.9 3.27 55.2 37 2 25 39200 0.0515 16836.79 51342 12974 8160 0.05414 3684 115473' 17.7 128 50.8' 114 143 5.15 73.8_ 3.11 54.9 38 2 26 13500 0.0496 5584.464 8360 0.00004 3 124355 50.6 128 114 142 4.96 70.9 38 2 27 13600 0.0602 6828.125 0.03782 106590 51.6 129 114 145 6.021 70.3 46 2 28 25800 0.0502 10801.63 42098 _ 10673 0.01452 88825 27.9 129 65.4 114_ 143 5.02 71.5 3.03 54.5 40 2 29 32100 0.0502 13439.241 41211 10174 10720 0.03771 3371 115473 21.6 128 39.3 114 143 5.02 69.9 3.09 55.2 38 2 30 36200 0.0481 14521.77 22330 5494 10300 0.06087 5229 110143 19.3 128 114 142 4.81 69 3.11 54.1 38 2 31 34300 0.0471 13473.52 34221 8391 8120 0.04132 2798 94155 20.8 128 48 114 142 4.71 71.3 3.12 55 34' 2 TOT 953100 1.5747 396152 997065 265665 226320 1.536 104446 3326496 787.1799 3885 1138.5 3491 4280 157 2248 80 1316 1219 62 AVG 30745.16 0.051 12779 41544.4. 11069 9840 0.050 4541 107306 25.3929 125.3 51.75 113 138 5 72.5 3 54.8 39 2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQ0001684 WWTP Name: Asheboro WWTP NPDES Number: NC0026123 Monitoring Period: From 4/1/2021 To 6/30/2021 Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed(Class A only)indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen DensityNumber of Parameter gExcee- in Frequency Sample Analytical Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 950 1356 7400 col/g 0 Quarterly C 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(thy coliform) weight) Vector Attraction Reduction (15A NCAC 02T.1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman -Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name andTitle (if applicable)(type or print) Jan 26,2022 1/26/2022 Signature of Preparer* Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503(White House Manual)Appendix D Revised 5-28-14 Day 1 Date if.1.2-1 Moisture and Dry Solids Average 2 IDish# g . -- Wt Dish+Wet Solids,g a a472- q- 0/ -87Z. /n ,Z WtDish, g 78,0 2- -7'7 (y , 7�•D, -ati,- --Tbi Wt Wet Solids, g 1-77 a, 1- Z.1:] p 16.1. 2m- (Q J g/ 1 �� Wt Dish+Dry Solids,g �� F 042- .3124 7 Wt Dish,g 7S-Ogz0 ,��, ( 4-O f '70. O 7 7F5.�731- .7 i3S Wt Dry Solids, g 0.5 OS D , 0. 42.47 , 0 . '-t83 0 0.53 a$ 0_yS 43 %Dry Solids 3. ud 7 3.2,o I 3. 18 % 3,2Q ?- 3.Z.a g, ^3 /'1tp7 Volatile Solids. Wt Dish+Dry Solids,g I g.5'fl-0 -11.S(o51 ` ?g.Si 51 "17-$042_ ---141.89 zg WtDish+lgnSolids, g 1g. 31g5 lei 3',11 59. 25ta1 -1g. SIll 19 I44.3 Wt Ign Solids, g . 0. 2-!g S 0. 233 Li , 0 . 2L,310 0. 2`t 1S _ 0.2425 % Vol Solids SS- 1 9 5 5. 0 2 59-i.1,9. 51 °J 5-9.1 % .1 5 L4 .7 1.7 Analyst j `�($MI-- Checked b� Day 2 i Date q-Z(•21 Moisture and Dry Solids Average Dish# I a 4 - 5 Wt Dish+ Wet Solids, g q a q e,5 g s 5-'tstp, o ci a.7 33 Sq.o -/i ,g6v-67577_ Wt Dish, g - 7R.0cm-) 1q Woe? •&53 -TS.Z �Di ..7g.93J� , Wt Wet Solids, g l , A �`�.1 1 d51 . 1 b. 1 5.5 15 . v?b Wt Dish+Dry Solids, g '-r`p , R 4q , 6l r � , I s, torm +j q WtDish, g --Mr, -- 761•140j '7 '.03g3 7S•-70 -7c:13 ;t, 1,Wt Dry Solids,g 0,k pr 3o5 r). �R133 ,"5'i l ID.a5,. � �` %Dry Solids � �,, net 3 , 1,02 . - .1'A°� .1 D% 3 , 19b`rl, 3. i 5 6, Volatile Solids Wt Dish+Dry Solids,g . Dci 9q , 1 r1% •4 o fl . �0 1gL11 4S Wt Dish+ign Solids, g rJ s'_ g' q. 2 59.i 7 2 Y4 W.11.5 - iq.0561(.0' Wt Ign Solids, g Q• off)4 c1 0. 1(A . .°1 0.Q)32 ©•m 19 t4 Q.1`'3 L4 % Vol Solids 'JO.5 4 5 a. 1 5 3.5 2. 5, . 1 z ` rg 7, 5,26) Analys Checked by �Q 20 Day VSR 57 7 3 q.sg `i Day 4 Date Moisture and Dry Solids Aver e Dish# 1 2 , 3 4 S ? t Wt Dish+ Wet Solids, g g-T. $`1(,$ g1 . S go 79 . 0403 , gg- F011 $[. 358$ Wt Dish, g "?$• 012-S 11 . 14 71-f -22 - 037g •-18- 2141 71$$.1435 Wt Wet Solids,g - 1 .17 43 , 10, 4 324 _ ( 1 , 00 CT _ 10 ,S2V2 . 10 . `-t 1 S3 _ Wt Dish+Dry Solids, g 1 g.sot oz. "1'1. 4tp33 -4_ S lo2-1 1 _59 Q`1 19 . 2.59(0 Wt Dish, g 7 g. OhZS 11, 14244 _ 7 g .0 2 $ , _7q _ Z.-149 •9 43S Wt Dry Solids,g 0.2P11-1 0 .314 ai 0,32'11 1) , S2-540 .. 0.3151 %Dry Solids 3 .04-'/_ -343 3.07.../. S. aq i _ 2).fl$./- ,-02 y , 3 0364 Volatile Solids Wt Dish+Dry Solids,g 1 g. 31 aZ 19. 1-1-1,- _, 17. 165n -K -Soli 9 -19. LC$lo Wt Dish+ign Solids, g 1? - Z•.5 l 7 . 291r 1 12• Ilip J 18- t fl "19. 0 r11 g5 Wt Ign Solids, g - 0. 6S I 0,i1.ri2. 0. i 12.10 0.1'101.. 0.1kAii • % Vol Solids 3 2 . 1/. S3.i I. 52,37. S2-S I. SZ-1'/. ��L. 0- Analyst Toil- Checked by 40 Day VSR - VSR= VSn.,g,nal-VSfinai 5-GDcUeo VP 1/2/21 Vsoriginal-(Vsoriginal X final City of Asheboro April 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials 1 7ccc 32• ' 13r" fro 32• r f4r'I gat sa,1a 2 1-)3 a /3'i frk )53e I 32.r 6TruLA p 3oa j 3?3 0 �wc 3 —lszsz_ 33' —_.15m '33-3 _. - G zia 9 1��•� 4 "" /5-0d 10pi al Z9 a 0 13.3 5 _ - 3.2 6riw1 Tee - Z3, _. 300 ; 33.3 -3 6 ?Os 33.3 -rn PIS° 33.3 TftG 1°I 5' 3?.3 c S S 7 703 33.3 11L6 —. 33—q _—.- '[14C2 2,9e 33.3 _fie 8 71z 33.3 TH.& 45ca6 -53.3 17g, 7399 33 3 9 7z ' 3.3 - 13r,.►. 1sco... 3,3 /ri M 239q 33''z _ - 10 ?oo _ 34 e1 13t., /S 33 mr-7 ,2 300 33. (5,5 11 ? y 133 - - - O?330 . 33,4 6-SS 12 70r) 33.3 TAB I45'. 33.3 TAG 7,0 , Z4.6e 601-0 33.3 e 14 -Tho 33. Z gm h r 564, i,) 8 ►1-. 19 30 33. 3 cs,s 15 73 -- 33, 6 -13',k ./.3 36 32 ' _. mow. lei 30 -_ c_51 16 0700 33. 1 potty.) 'Sot 32.c TR( 2 OD 33.0) ASS 17 ,_a .3z55 -ram a-cxo ; - -- IA& Z3 0 9 i 3 2. 18 cc?k 3� u} 1�1�f ?-4 LJ 2,3 0 9 p ,9 19 ()VG 3119 ts,,„m ISIS' 32, 13 )3Da 3.'?, uf 20 670 5 33.c) A.TC /660 42.,9 Air :2 3i 3).01 c,1 21 07►5 52. A3G 1560 33.� 1,300 2,9 li!' 22 0 7/ . 3 a c 670 33.3 Z3 9° �33-.� 6-1 23 (t13h S3.1 GN -1S36 `vl �1hm U29 3343 24 310(1 33,3 51y1 M _ /5-0,6 333 ?3c O 33, CSS _ 25 cy-,„ \r m f3 60 3,3 h^" .2300--I 3 3, 3> Li; 26 0 2 % , 33 J. 7- r co 31. 3 TAG 23� J 3 G ( 27- 02, _ 33.3 7710 _ 19 55 33 q ?'AG _:" 33 t ' 28 `-1(�a %,„, 1� zS:9 New, .43+0 s.3:=1 s< , �3,`{ -- � - )` vo )3,3 6 7 !29 °boa 33, h f3� 5-60� — — 30 a 7io 33. / /4-3t_ /SG 5 33. L ,4T .BoD Y3.3 s 31 _ City of Asheboro May 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials — 1 (11/6 33 i 5 i(� _� '_'Y _.. A3 j_P-k f& 2 GG5t, 33.E TA[, ti5o0 3'S.Y T/46 31x -S� 4 07So 35.`1 gOlti ic0,0 37J.ur .n'1f''1 33. cfs 5 33.y -- 15S9u 3.s 7744., 0,3r7+) 33,� cfr -- 6 070o 33.3 Tint 1g'oo 33 3 TAG d`d 3 7 0 l 1 333 (3132r1 IJ 60 32 , iam 11,.66I 8 aim 33, . �M I�o� 4 33,E w, 3 -1'.I,5/ CST 10 0 7Q 33' ,.14/51' 53,4 G .2300 1-33.s G jf 11 0763 33.3 ASc- 15e s __- 13.Q !/-� s �'S 4 S Zt 12 D-)Eb 33'3 I$.w n1 /5-66 33,T 5,1 _ 24`b 31.2- 146 13 (-113 0 33�t 3-�1 i s3o 133 .2 t3m1,1 -7 0 31..2 cif 14 616 t 3. jeX- I Si5 33.a �', -?3c�(� 37,� cfj 15 6706 -_ 33,. Sc_- 15/0 3'3`-2 "M.- le did 3 133'.. . ,ate 1515 33, a. ;`� 3. -5 17 15—, ,1 1 ( lid � -(,� - 3. a -�, 18 oI 2 I�3i � ._ OM ;33,a. `�G 2399 33 2- , 19 D?/5 33,A ,c _J5cf 133. , Z399 33.2_, /- 20 0 74-5' ?3.a Azt, 1561 33,..1 2300 21 _. .aVaq I°' fa . I4o _ t 2561 ! 33.1 13fv► �, _. 22 07 n 0 33� .L (4 a 33, 1 1Z itJ Z-39 3.1 Z 23 C7� -0„ IAA/ tutze 1I ._ fICJ Z 90 ! 33.2 6 24 olef 33'.2_ Art 1 0 3 d113t. 230.0 33,Z 25 d A. Ash - - - Z 60 F✓�,Z .5(Mi__ 26 - 27 28 29 _ _ 30 31 I Qitp of clightboro (.). % Dry Solids for Sludge Hauling Date . - I 2-2j _ /l ZOIL( '4 c l Z/ 4a/u Analyst Initials •IN- . 7r;od "Wl. 'Y►IV Dish Number S' 0 6:61 9z164( S Source _ Wt. Dish.&Wt. Solid (g) I 0 I. el- - g,4^1 t14b D(9 l. 0ci Zi Wt. Dish (g) 78 (3S ,93mA Di 7 (54't Wt. Wet Solid (g) 049. tl(70 6 ._ t 3erli , -!i, q to q _ q' S�O Wt. Dish & Dry Sol - d (g) J. 00/4a Iq , 95(.05 -7 •-717 I -7 3. 24 (. Dish (g) _-75•515 Ifl dbma. 7� .1 O1 �� (- 1331) V t. Dry Solids (g) 11•-7 q 5 . 10;3 0.1 D Co Li Z.,'6 1 y- % Dry Solids oZ/-d-Z, c 1 r ° _ zo,Leblo Weight(Ib/ft3) 6316-h4ILIALAA-- 3-Co 1 4 c Operators Initials C/S CAS CI-S ell' '6" -°Le141) '614 t,,t-ANAAJ *_.- - - w City of lF _boro Department of Water Quality Fecal Coliform in Sludge Sample Collection Sample# �� 2 i 3_) 4O '5) � c'J Date L-{ •12-.21 ^4 - to- ?-1 . 14' 2-8 - 2-4 . 4.21•14 Li,2..1•1-1 4- 21 14•Z2-- 4 Time _ i S-7 _ 1143 S R I7 12H-3 cm 11'-(a Location turd Uri rim,c1 b ld5 ani bidq cIu.r-01 inI d� , eoveid wci ol civ hi c#qq Analyst. B M F M L 6M L t2.4oL. 6M L_ AM(, J %Solids Dish Number _ 0 -Z 3 Lf 5 (e / 1Nt Dish&WtS _ !in 1414I4 (1 34113 II. Z-107 10- i1`l3 , 12. 2"1--1.7 I0- 120c6 14. soo wt Dish -1q. B ISM 0.17 tog 0- 1-14-1 o.9-aq I. 112- 1 1 n i3 4 r . 0 5 a wt Wet Solids 22-_ Ivo09 10 . 4.22.1 ID . 2c1 1,e, , 1 . ,q o r I 1 . I L al. 01 2'4 i 3• l Szu vet Dish&Drys ig . (DO zf0 _ 3- 318-7 3, 8Sso , 3.©7o9 as (z( - .2.5-71 4 osq S Wt Dish '1 8.213E 0. 9 7 (o`i 6-1-11+ 1 0 .118yf r, 1121 1. ( n S Si- , I o l 6 Wt Dry Solids 4.-190S , 2.3423 2.. 1103 Z.0.12s ',ici2._ 2- 114 7 2. 931g %Dry Solids 2-1-Z'/ 22-5 r 00.51. -Zs-.1 I- 21. s r 23_g 7_ 2_1..3•. Analyst BPI(-- $mc.._ 131141_, 8 Mtn 611/ t- $M U E Fecal Coliform Date In E 9- 22.24 L4.2-Z• zi iI•22-21 Li-22 2l (-1 LZ: 24 '-f•ZZ Time In I ZS3 .13 j S 13 h 13 as 1,. 5.1 _ 1582. 15j 3 Analyst In gML 'pit_ 43m t✓ _ (`3ML 13 c. 13n11, PAL- _ ml sample #colonies #colonies #colonies #colonies #colonies #colonies #colonies o.oaot 0 0 0 0 0 3 0.0003 0 0 0 0 0 0 0 0.001 0 _ a 0 0 Z 0 0 0,003 0 0 0 a 5 0 0 2 Rule used for calculation 1 3 3 3 3 _ L 3 _ 3 A _ Fecal Coliform) < I,0�e C , 1/DI p < ((roc) < ga 0 -14 60 2- < qSO < I 0 2-et gram Dry Sludge A 4,- * ' -* Date Out 23- 24 4-• 23.7 t 1+23. 24 `•t•23- 1-4-23•?-'1 `-23-ZI H-z .21 Time Out , 125 2- 12.53 I25 4 i zss- 13 i 5 - 15 it" 13 1l Analyst out ;;>>.,t_ 13m4- _ 13niL ►3rhL. 136 13M tSML Coliform Colonies/gram=Coliform colonies counted X 100 il"fi _s hQ.wz.. besyn ml X%Dry Solids POUn494 to 2- SI f5S l L#0 ('�fc �� Geometric Mean �' du/ml City of Sobeboro Dry Solids for Sludge Hauling Date 7-ZG, 2 '� 1 S° .1 Analyst Initials - pj L 8rte%. Dish Number YQ g0 ( 6b C.t�vto-�``� Source r J s 1ca/Prt cc ckte.... Pre ss Wt. Dish &Wet Solid (g) dldl. 3(p€3,1; g9, gS Z-I 10(f.(12 1 Wt. Dish (g) 7'I5 .,C5 1 'Zo �� q 122 S. 1211 Wt. Wet Solid (g) 26 - SSip9 I I . 0311 1 S. 1987 Wt. Dish &Dry Solid (g) t 3- 32-74 51,2(p SS $g 1-9 2-- Wt. Dish (g) .�J -1 S.. 2(?y 7S". 12(9 Wt. Dry Solid (g) Li .5) Sy- 2 . 4 SIS -S to g3 % Dry Solid 23g-2-4? 22.. 2. 22 .Li" Weight (Ib/ft3) 5o ( 6 Operator Initials JFE J City of C aboro Department of Water Quality Fecal Coliform in Sludge Sample Collection Sample# Z., 3 "( S Date -7.2. •L, ?•tt•z-r S .4F.-2-r 8"•9-•2.-/ z .S 2-, 8"-S'=z--i g-S--ram Time . 0752. 12-3 0 1418 0 560 11 CIS 1411 Location rou-e--g4 bI ug --------7 Analyst - J M. gib L _ B rn L.- giro L. lIm L _ Mu__ gnu. %Solids Dish Number I Z. 3 4- S ko --7 Wt Dish&WtS 7 .9 lob' S -1-790(o g.Z_‘-130 3S62.- .Q !n 10.01p I? 16.51tn`-t WtDish 1. 101'-F I. 104Lo 140'74 I.litrt$ gto I.1S19 MITI WtWetSolids (o. 3te11 , L-(p3tp0 . 1RSb 10.2.399. -l .g(plb g.9299 1.g9-2S WtDish& DryS 2. .+4•99S Z.SS3Te 2.. .1,F202- 2.Io630 Z-1204 3-locnO 3.14712 Wt Dish l •10-th 1-lb 4(e I .1 01 L# 1,114,7 1 .I z-gtv I- 13 i9 0- ci9 8R WtDrySolids • I-3924 I .434-Z I SI2. I )-F r Z. 1 .11(0ik Z •SLvSI 2-4/03 % Dry Solids 2-I.9'/_ Zl .i.,-! 21 •Z'! _ 23,fit% ZZ_S'/. 2•7-7/ ZS.z..."/- Analyst BrnL- EMI- 13rhlr Rm1- grnc. gi1. Fa1'Y1L • Fecal Coliform Date In 7 •4-zr F. 4.. Z, f - LP,7,1 g •S- zi $•S•?-r f - S- 2 1 i•S Time In IZS9 1309 _ & (32,0 13'-Fio _ 13SS /`ias (440 Analyst In grit_ ^ i . 18rn� 13mL t tiiL grni, 8mL ml sample #colonies #colonies #colonies #colonies #colonies #colonies #colonies 0.0001 0 - 0 0 0 - 0 0 0 0.0003 0 (J 0 2 ) 3 O • Z. 0.001 0 IS }Go O >tvO 2 0 7 0.003 0 > S' No 0 • O '-((U (C1 _ 0 $ Rule used for calculation 3 _ 2. (1) 3 1 I 3 p Z Fecal Coliform/ 30 geo'� "0,'`�u 53 3 - -- Fecal Dry Sludge e. < I�O�$ � . < Ij412 2.3 7 b ����G.ci, G1RZ 142-34 Date Out $- S. . S. g , _ I! 2/ r S 7� , 8- (n - z.4 `L - (v-71 7- {v • 14 f $- (a- 7---t Time Out l'i_Z-f ^ IZZS 1224p 1330 1332.- /33 (33 y- Analyst out gmL 1 C- b/hL- _ 15A014.. 1?iric., bmu p niu a) x-10o)/ ,Dt703 k 2(.69 =‘ OY> Coliform Colonies/gram=Coliform colonies counted X 100 0 5K/obl oDOo3 x z ,� - ®(l404/ ml X%Dry Solids RXLt,�D o03 X 22,E = 5--.333 Geometric Mean .2.--- /72Y cfu/g e4 4ef4L) cx46 a-/.h)- ., U ",_) 'I U APRIL 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D% S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re'D#1 tern D#2 Tern %Solids -%Vol Inf %Solids %Vol CO2 Dig 1 34400 0.0543 15578.45 30814 8095 8620 0.06171 4436 94154.5 20.7 128 39.8 115 142 5.43 68.4 3.14 54.2 38 2 2 8100 0.0399 2695.405 0.06729 93266 88.2 129 115 143 3.99 39 2 3 44100 0.0548 20155.11 40846 _ 10526 F 0.0645 88825 16.3 129 115 143 5.48 36 2 4 35900 0.0422 12634.93 30591 7858 0.06009_ 79943 20.3 129 34.1 115 142 4.22 72.5 3.2 54.8 36 2 5 45700 0.0411 15664.77 63142 14834 7800 0.06092 3963 88825 15.7 128 48.1 115 141 4.11 71.3 3.31 52.9 36 2 6 24500 0.047 9603.51 21221 5858 8300 0.06779 4693 93266 29.2 128 47.6 115 141 4.7 71.9 3.31 53.6 38 2 7 24300 0.0425 8613.135 29985 8002 9160 0.06516 4978 115473 28.5 129 81.6 114 143 4.25 70 3.32 53.3 37 2 8 41200 0.0526 18073.78" 43356 8672 8560 0.04462' 3185 106590 17.0 129 49.9 114 143 5.26- 72.3 3.36 53.2 38 2 9 25100 0.0517 10822.57 9978 2688 7800 0.03878 2523 97708' 28.3 129 47.7 114 144 5.17 71.8 3.41 53.9 38 2 10 36800 0.0475 14578.32 21268 5623' 0.03922 ° 79943 19.8 129 44.4 115 144 4.75 70.6 3.3 53 38' 2 11 40200 0.037 12404.92 27993 7798' 0.03726 66619' 18.4 130 45.5 115 144 3.7 71 3.28 54.1 37 2 12 37800 0.0534 16834.46 48636 12808 7400 0.03929 2425 62178 19.7 129 49.9 115 143 5.34 72.5 3.26 53.8 38 2 13 27000 0.0525 11821.95' 40053 10489 8000 0.03369 2248 62178 27.6 129 52.6 115 143 5.25 72.9 3.3 53.5 38 2 14 28200 0.0563 13241.08 40559 10418 8140 0.02008 1363 71060 26.1 130 38.3 115 145 5.63 65.2 3.25 53.6 38 2 15 20700 30374 7980 8160 0.01881 1280 88825 34.7 130 115 145 3.16 52.3 38 2 16 36500 0.083 25266.03 31235 8623 8760 0.02681 1959 97708 19.5 125 60.9 115 134 8.3 77.1 2.91 50 37 2 17 43200 0.0592 21329.05 31037 8335 0.01889 79943 16.8' 125 52.7 115 136 5.92 65.9 2.66 49 38 2 18 20300 0.0522 8837.564 0.01905 71060 36.3 129 115 142 5.22 66.8 36 2 19 43100 0.0447 16067.59 30478 8439 9400 0.01961 1537 62178 17.3 129 48.9 115 144 4.47 66.3 3.25 53.7 38 2 20 45700 0.0506 19285.58 79429 ' 20801 9420 0.02249 1767 53295 16.5 128 50.1 115 142 5.06 66 3.29 53.8 38 2 21 23600 0.052 10234.85 154573 36890 9320 0.01788 1390 159885 27.5 128 50 115 142 5.2 65.5 3.18 52.9 38 2 22 34300. 0.0558 15962.26 160800 41322' 10780 0.01827 1643 302005 14.7 128 47.9 114 142 5.58 68 3.12 53.7 37 2 23 26600 0.0611 13554.67 87100' 31961 9220 0.01869 1437 399713 15.3 142 36.9 142 6.11 66.4 4.72 55.5 38 2 24 28100 0.0517 12116.1 0.02232 399713 14.5 143 143 5.17 67 38 2 25 27400 0.0576 13162.52 0.01854 373065' 15.9' 145 145 5.76 65.8 37 2 26 31400 0.0848 i 22207.08 9180 0.01944 1488 373065 13.8 144 144 8.48 62.6_ 39 2 27 22700 0.0613 11605.19 50689 31199 9520 0.01242 986 319770 21.5 139 58.5 136 142 6.13 70 7.54 49.2 38 2 28 22700 0.0625 11832.38 61882 26189 9180 0.02601 1991 399713 18.0 139 51.2 134 144 6.25 67.5 5.35 50.4 36 2" 29 32800 0.0507 13869.09 98796 26614 8780 0.03907 2861 355300 13.8' 131 126 136 5.07 68.4 37 2 30 30500 0.0535 13608.8 41613 24953 9600 0.04413 3533 404154 13.2 123 63.9 123 5.35 67.1 2.01 42.4 37' 2 TOT 942900 1.5535 411661 1306448 386974 185100 1.063 51686 5139415 685.3826 3931 1100.5 3042 4123 155 1861 81 1207 1125 60 AVG 31430. 0.054 14195 52257.9 15479 8814 0.035' 2461 171314 22.84609 131.0 50.0227 117 142 5 68.9, 41 52.5 38 2 MAY 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D- GALS D% S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern D#2 Ter_% Solids_%Vol Inf % Solids %Vol CO2 Dig 1 28700 0.0492 11776.41 0.04065 390830 14.5 121 121 4.92 67 37 1 2 31100 0.0508 13176.2 0.04569 373065 14.0 120 120 5.08 68 38 1 3 23600 0.0518 10195.48 15264 6263 8740 0.03948 2878 359741 19.0 118 63.4 119 117 5.18 68.5 6.09 44.3' 38 2 4 33500 0.0553 15450.27 6900 0.03309 1904 314441 14.7 121 118 125 5.53 66.3 38 2 5 28600 0.059 14072.92 7840 0.01999 1307 270916 18.8 127 117 138 5.9 64.6 41 2 6 31700 0.0653 17263.88 7700 0.01801 1157 248710 17.6 129 117 142 6.53 64.9 _ 38 2 7 33300 0.0538 14941.44 8240 0.01657 1139 239828 17.1 _ 125 118 133 5.38 64.5 _ 37 2 8 26600 0.0507 11247.49 0.02563 186533 23.4 126 120 132 5.07 68.9 38 2 9 25100 0.0457 9566.564 0.0237 159885 25.8 127 123 131 4.57 71.6 39' 2 10 26900 0.0541 12137.12 8320 0.02201 1527 133238 25.1 132 130 135 5.41 73.6 37 2 11 21700 0.0565 10225.26 31137 9868 7540 0.02008 1263 1 106590 32.3' 135 0 134 135 5.65 71.1 4.05 48.9 39 2 12 23000 0.0554 10626.83 29587 8908 8640 0.02282 1644 111031 30.3 132 57.5 133 131 5.54 72.5 3.57 52.3 39 2 13 21100 0.0546 9608.18' 21200 6100 8840 0.0189 1393 111031 33.0 129 50.8 127 130 5.46 68.9 3.54 53.1 39 2 14 13600 0.0551 6249.662 48755 13866 7780 0.02086 1354 111031 51.2 133 51.7 130 135 5.51 70 3.46 53 38 2 15 16300 0.0625 8496.375 0.02672 142120 40.8 134 131 136 6.25 70 39 2 16 14900 0.0579 7195.001 0.02227 124355 45.9 134 130 138 5.79 70.3 39 2 17 16800 0.058 8126.496 10320 0.02404 2069 106590 41.7 134 128_ 140 5.8 72 39 2 18 18000 0.058 8706.961 20645 5493 8780 0.02092 1532 106590 39.0 133 56.5 126 140 5.8 72.2 3.35 53.1 40 2 19 17400 0.0549 7966.868 12097 3128 9880 0.02177 1794 97708 40.8 134 49.5. 128 141 5.49 69.5 3.31 53.5 39 2 T 20 16500 0.051 7018.11 22211 5872 10140 0.02295 1941 106590 42.5 134 48.8 128 139 5.1 69.3 3.29 53.6 39 2 21 16200 0.0547 7390.408 8520 0.02102 1494 88825 44.4 133 127 139 5.47 70.9 39 2 22 14200_ 0.0618 7318.85 22096 5602 0.02762 88825 50.6 135 59.7 126 143 6.18 72.2 2.91 51.2 40 2 23 16500 0.0679 9343.719 26026 6685 0.02105 106590 42.5 135 62.9 126 144 6.79 75.9 3.22 53.8 40_ 2 24 13400 0.0607 6783.589 7180 0.02095 1255 84384 54.0 136 127 145 6.07 72.2 35 2 25 15700 0.0664 8694.283 21676 5532 10080 0.02023 1701 93266 45.5 137 58.5 128 145 6.64 7.36 3.17 53.6 39 2 26 16000 0.0477 6365.088 22627 5775 9240 0.03505 2701E 97708 44.4 136 128 145 4.77 72.7 40 2 27 16600 0.0545 7545.198 9260 0.0404 3120 88825 43.3 137 _ 129 144 5.45 73 40 23 28 16600 0.0546 7559.042 10440 0.03978 3464 53295 45.5 137 129 145 5.46 71.7 35 2 -29 16800 0.0635 8897.112 22964 5707 0.04003 66619 44.1 137 51.3 128 146 6.35 70.8, 3.11 54.1 36 2 30 17600 0.05781 8484.115 23482 5738 0.03952 71060 41.9 136 52.3 127 144 5.78 70.9 3.08' 53.7 35 2 31 17600 0.0591 18674.934 22117 5589 0.04017 79943 41.4 135 44.4 127 144' 35 2 TOT - 645600 1.7483 301104 361884 100125 174380 0.852 36635 4720161 1085.056' 4071 707.3 3899 4001' 169 2041 46 678 1185 60 AVG 20825.81 0.056, 9713 24125.6 6675 8719 0.027 1832 152263 35.00182' 131.3 50.52143 126 138 6 68.0 4 52.2 38 2 JUNE 2021 I SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D% S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern D#2 Tern % Solids %Vol Inf% Solids %Vol CO2 Dig 1 209001 0.0504 8785.022 7000 0.04167 2433 58624.5 35.8 136 127 145 5.04 70.1 36 2 2 19300 0.0568 9142.642 24252 5845 6840 0.04219 2407 57736 38.9 135 54.7 126 144 5.68 71.8 3.18 53.6 40 2- 3 16600 0.0514 7116.022 22791 5797 8300 0.0237 1641 71060 44.4 135_ 49 127 143 5.14 71.1 3.07 55.6 39 2 4 17000 0.0727 10307.41 23952 6073 9340 0.03827 2981 65731 43.7 136 127 144 7.27 66.1 39 2 5 16600 0.0656 9081.926 43022 10595 0.03666 65731 44.7 136 35 127 144 6.56 65.2 3.16 54.9 35 2 6 16800 0.0613 8588.866 23423 6134 0.03958 97708 42.3 136 37 127 145 6.13_ 65.8 3.15 54.8 35 2 7 16900 0.0577 8132.584 11904 2959 8320 0.04338 3010 88825 42.5 136 32.2 127 145 5.771 64.9 3.13 54.6 35 2 8' 15900 0.0538 7134.203 2464E 6064 9100 0.04204 3191 106590 44.1 136 35.7 127 145' 5- .38 67.4 3.16 54.6 39 2 9 15500 0.0648 8376.69E 7800 0.04013 2611 76390 47.2 135 126 1441 6- .48 68.7 39 2 10 13800 0.056 6445.152 52677 13531 8740 0.0394 28721 66619 53.7 136 38.3 126 146 5.6 66.2, 3.13 54.7 39 2 11 14700 0.0842 10322.75 35044 8680 8640 0.02268 1634 151003 44.7 136 47.9 127 145 8.42 69.2 3.08 53.9 35 2 12 16200 0.0632 8538.826 0.04335 115473 42.7 136 127 145. 6- .32 61.7 38 2 13 16800 0.069 9667.728 0.04291 88825 42.8 136 126 146 6.9 61.6 38 2 14 15300 0.0591 7541.278 10060 0.03748 3145 84384 47.3 136 127 145 5.91 61.8 39 2 15 20500 0.0549 9386.253 30811 7786 6380 0.03715 1977_ 62178 36.4 137 28 126 147 5.49 61.9 3.12 5.3.9 39 2 16, 26500 0.0534 11801.93 11200 0.0425, 3970 75501 27.E 135 126 144 5.34 65.2 35 2 17' 26600 0.0445 9872.058 22321 5827 8600 0.04524 3245 71060 27.7 136 39.2 127 145 4.45 66.1 3.17' 54.3 36 2 18 19500 0.0526 8554.338 43550 11259 7580 0.04936 3120 62178 38.2 136 46.8 126 146 5.26 68.4 3.17 53.5 40 2 19 23100 0.0601 11578.51 30695 7885 0.04966 53295 32.7 136 39.3 127 145 6.01 65.7 3.2 53.7 40 2 20 29800 0.0537 13346.17 41213 10724 0.04973 71060 24.7 136 35 127 145 5.37 65.9 3.24 55.7 39 2 21 30100 0.0458 11497.36 9660 0.05557 4477 71060 24.5 134 127 142 4.58 68 36 2 22 22800 0.0524 9963.965 10400 0.03971 3444 48854 33.3 134 127 142 5.24 67.8 36 2 23 18800 0.0538 8435.41 41045 11159 8320 0.04913 3409 26648 41.6 135 44.1 127 142 5.38 68 3.28 54.2- 36 2 24 18900 0.0621 9788.575 31183 8140 6160 0.04058 2085 44413 40.4 135 43.8 127 142 6.21, 67.9 3.27 54.3 38 2 25 19800 0.0567 9362.984 9820 0.04819 3947 62178 37.7 135 1271 144 5.67 65.3' 35 2 26 22000 0.0537 9852.876 25572 6675 0.04643 97708 32.3 137 39.4 127 147 5.37 66.6 3.25 54.7 38 2 27 18800 0.0431 6757.735 23894 6516 0.04506 62178 39.7 136 42.8 127 145 4.31 66.6 3.3 54.4 36 2 28 17400 0.0579 8402.216 23598 6475 1340_ 0.03725 416 71060 42.3 135 47.4 127 143 5.79 68.9 3.26 53.9 39 2 29 19500 0.0688 11188.94 3186E 8337 7880 0.0376 2471 58625 38.4 136 45.1 127 145 6.88 68.2 3.31 54.1 39 2 30 26000 0.0554 12012.94 9891 2871 6180 0.04305 2219_ 71060_ 28.3 137 46.5 127 146^ 5.54 68.4 3.35 53.6 36 2 TOT 592400 1.7349 280983 617350 159332 177660 1.250 60703 2203748-1160.534 4070 827.2 3805 4335 173 2001 64 1087 1124 60 AVG 19746.67 0.058 9366 29397.E 7587.3 8075 0.042 2759 73458 38.68446 135.7 41.36 127 145 6 66.7 3' 54.4 37 2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQ0001684 WWTP Name: Asheboro WWTP NPDES Number: NC0026123 Monitoring Period: From 7/1/2021 To 9/30/2021 Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed(Class A only)indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen DensityNumber of Parameter gExcee- in Frequency Sample Analytical Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 792 9728 350140 col/g 0 Quarterly C 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(thy coliform) weight) Vector Attraction Reduction (15A NCAC 02T.1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman -Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name andTitle (if applicable)(type or print) Jan 26,2022 1/26/2022 Signature of Preparer* Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) QCitp of abeboro % Dry Solids for Sludge Hauling Date -7-Z(0 •2( • y •Zf 2-1 Analyst Initials 01( 8Ant, Dish Number YQ Sd ( 60 Source r T�75s �co/P SS G Pre sS C�- Wt. Dish&Wet Solid (g) 9C!. 3(p - S1. gs 10Q,(I--? Wt. Dish (g) S •,C5. I ZO ^1 , 4 122 cS- 1211 Wt. Wet Solid (g) 26 , SSC.9 I I , 031i IS-- -1977 Wt. Dish &Dry Solid (g) 3- 32:14 81 2tp 3S gg• 1 102- Wt. Dish (g) •‘6 1 20 -i a. �(?Z 7S. 1219 Wt. Dry Solid (g) `I .S1 S`f 2 . y sis S 6283 % Dry Solid 2*21..-0 . 2 22 .(o-/, • Weight (Ib/ft3) S0 to b Operator Initials J FE 1 FE caty..c, arte.,46 City of( _boro Department of Water Quality Fecal Coliform in Sludge Sample Collection Sample# fl Z. 3 f 5 L _7 Date -7.24f.z, g-t-}.e.-f g-4-1-•2-1 E'-{+•z-i 3-. S 2-, E'-S=z-f g•s-z-, Time 0752 I2-3o , Il-fl 3700 Il4S Pill Location _cb,A. .,-ei bl Le, _ �_ Analyst j l _ 13111i- 0 III L f3n1 L iSnic_ BAAL rRih1✓ • %Solids Dish Number I 2_ S a+ S la -7 WtDish&WtS 7 •'-Ila5 "1-•7ctOlo 4 .Z.Lf30 1•3SI,2- q -01719 10,0417 KS.$milla`t WtDish f. Ip14 I, I0 '+l0 , I.10'icf 1.111.J _ I . I2glo 1-I3I9 0.619F11 Wt Wet Solids (o• lpll , lo-(t3(p0 I , ) 51a (0.z,i9Lt '] .q(o`10 Z•329 3 1.21-7s WtDish& DryS 2- .499S Z-S3 2 .1p2AZ 2.1oa30 ZZII2.t54 3.1fe170 3-Lt712, Wt Dish . I •10 7y- I-l o 4to , I .101LF I -lit.Sr' I . 1 ZAlo I- 1311 O. 619 S`I~ •WtDrySolids I.3 Zl 1 .434Z _ I -Si 2 1-LfYIaZ I71q(oS z -Slrs) Z-Lf10g %Dry Solids 2-l.9i'/_ 2-1 .L•i zl -Z% 23.e7. 22--_S-4 2-7•7/_ 2c1_2/ Analyst Siva- 8ML 'BmL Rvm. 'BAIL smu smu Fecal Coliform Date In 7 -4-24 P• 4-- Z, 8' - 4• z-I g•S- z $.S• z-r ' S- 5- 2-r 1•5-zi .. Time In IZ.59 /369 132.0 13`flo 13SS 1'f OS I 440 Analyst In B&lL ttVhL 1gfl1L 131\eiL En/IL. 131'V►L 8ThL ml sample #colonies #colonies #colonies #colonies #colonies #colonies #colonies o.000i 0 0 0 0 0 0 0 0.0003 0 C 0 43003 0 z 0.001S }lad 0 7 Lv0 2 _ O S 0.003 0 > S' (aO 0 c ,(oa 3i� p Rule used for calculation 3 Z. (7 3 • I I o 3 z Fecal Coliform/ < p 3 8 3,03(o e/ 0 I u 53,333 gram Dry Sludge < f/012 z,3, e -4p I..Ev . C-7RZ i (cf23 Q. Date Out � 1�bt21 ���r � J S- S- z. _ i'' S' za g•S_ z. 8- (n - u 9 - t -z4 c' • ta - I-I $• (v- Time Out 11r211- (2 2S I22to I334) f 332- 15'S (33 y- Analyst out $mom elo C. Iti M L.- 1S/vr i. , POI L., 131Yi c.. A m u • Q '.Z.. xaoo� 6Ynvo3 x 2(•62 _ Coliform Colonies/gram=Coliform colonies counted X 100 s /o oioO3 23 - ®� mlX%Dry Solids D . ex oD t o 03 X 22 = 53 3 Geometric Mean (-4-r =`Lt 1 72 Y cfu/g C '4"ef4L) ' C, fr/.hl-2 , CITY OF ASHEBORO } Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part S03(White House Manual)Appendix D Revised 5-28-14 IDay 1 Date-7•a• zr Moisture and Dry Solids Avera : Dish# I Z 3 4 3 Wt Dish+Wet Solids, g gg- 02;32 rk0 .7500 94.-4 ' I _ SfF . 42tQ0 �I�-I. 41a31 Wt Dish, g ,- g..4ii2 -in- 144� -12. 040-7 "78• 39' 12• 9g0d Wt Wet Solids, g 1_ g314 I1 .1 054 , Ito-3I-10 , _ l0• IS2Z _ IS.S2_31 Wt Dish+Dry Solids, g -7 g, 9243 -1,9 .5370 7 9. s 7g Z. _ i 9. 1010 4 7`i. -S1.4 ; , WtDish,g 78 .011V 11-144to 19- 0407 _ 18. Znig 12.9400 Wt Dry Solids, g 0.3 29s O. S g-1`t 0.S31s 0.3 3 EA, _ Q.S 1 L94 %Dry Solids 5.3 i '/. g.31 -i 3.2c1 .4. 5.31 •!' 3.33 % _ S 31 V. Volatile Solids Wt Dish+Dry Solids, g ")Q. 4-i2_03 -19 .532.0 , -)g•71VZ 15. (010� n9_ 41„q,„ l Wt Dish+Ign Solids,g -7 g 24 p. '�,CF _1�I. 32 up 'Y g . 2��l0 1 S. `t 31{ "1 1.1 S 03 Wt Ign Solids, g n. 11s'7 0• 91-1 - 0.Z.V co 0. ►113 0.2'1 t.1 %Vol Solids S3_Sr. 5''MY.. S3.1% S3. 3•r. 53 .5'! 53_i:/••s. Analyst 8M1- Checked by.�Q Day/0 Date 7.1. -•2-1 Moisture and Dry Solids Average Dish# I '` 2.. 3 `I S Wt Dish+Wet Solids, g ill. SO Zs ?LA.34.183 g -1. S313 LtS , ie1sa 2t._ 114g Wt Dish, g 12 . ()e) `_11. I Lf 38 `)2. 0 3qz 75(.27111 ,72. 00-12_ WtWetSolids, g • lQ . 4 016 1.1_0HZ (, .99g1 7.4v1 • 7. g5110 Wt Dish+Dry Solids, g erg, soles r -1q 3193 , 1g. Z'-'- 0 1 q. 5Z30 erg. i911 Wt Dish, g $. 0 9 2S _"19_i 4 38 19 .059 2 '12-t)39 1 g . `1`I 3 z Wt Dry Solids, g • o.2091 G LDS 0..2-0 efq 0,21411 , 0,ZS41 %Dry Solids 5.Z(o Y. _ ?i_ 21 . . 5 2�i 1- 42.3(i i 17_1-'-1-4 -i -2'7 X Volatile Solids ,9 r -1 9 Wt Dish+Dry.Solids, g 1 g.3 o n0 19.37' 3 , g- 2-410 '1 S1 .5 2.30 y i WtDish+IgnSolids, g 78, 1903 -7`1. 2547 _ _- . 1373 7g. 3892_? °I. 0(..01S .• Wt Ign Solids, g 0. 11 13 0.12..c}(o [I, Ill-1 (3 . I33$ _ 0.I3l,9 %Vol Solids 53 Z.% 5 a-1'/.. 53.2'/ _ 53.')'/ 6.3.107. S3.3/ Analyst stilt, Checked by - 20 Day VSR tales-i, 1.21c ` ay 40 Date '.11. 2-1 Moisture and Dry Solids v rage Dish# -1 a ,_ 4 c- $'rrr,lzl Wt Dish+Wet Solids, g ; ,. ��, Chin . Si 13 sin.a li 955 , (name, ct 5.5�� 1 f Wt Dish, g Mani i IV Q •l a� 11% , 03�0 TriS i alai it,g3g1 • , Wt Wet Solids, g Wirlign I, 4 a.9,c •ti.,]9l o9a_ , 7,314s1 , 1, (let, Wt Dish+Dry Solids, g f M aP 119 6311,11 Din IS,3.C116 'T% .c04,A ICIa 6a5- ii Wt Dish, g i, . D' . "Zq , log a$ 11%, f 3`M0 i4. .z,-tai ,1'1 • " f), atia��`�• Wt Dry Solids, g d 1 'A' 0 a3-il, 0, a,SSbt O.a3t5 � %Dry Solids • ' , 3' ZY'Z, 3. VA, 5 '1% _ 3 . 2),1'1#4 Volatile Solids Wt Dish+Dry Solids, g SWIM --ic1 ,.bikci Q --deb,ads iiS.5 3 '1.9,, ',sac- Wt Dish+lgn Solids, g MIMI 14, aSC1,i t19 ,X.L04,7 17 ,3ca IC/, ID Iq_ Wt Ign Solids, g © . 0`.P" 0.1.a jq (3. talS b . ti TC 0_.1. t i, i : '% Vol Solids . 5F�.`�% �.t,'-�ifio 514,90 _ SD rri� 5t],ciuta. Analyst i _ Checked by _ / ! 40 Day VSR �� - = t�o-�n VSR= VSorig,,,ai-VSry a► VSonginal-(VSoriginal X VSfinal) City of Asheboro July 2021 Digester Pilot Plant Temperature Log (Record once per shift) ... .... ... . .... 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials 1 o-1s _ 39.7 PG- _ �5�0 3 I a Z3c__-�-`� epq 2 o-rso 3u-3 - --� 2 34 .e T 15 Va 3ti•2 'TAO 3 070.5 31.v __Tian _1`I5d— -Zy•cz__._ TAG _. 2' 9 3W _10 4 070D 3�[.Z apt Ss :3 TrG 23v Yi.Z 5_ 0103— 3f 3 - i56 5 3l'3 ATC, 23 09 39•tI 6 070`� 3Y i�a 5 3�f3 . Z 300 ••3 erlin 7 _ _ 0705 _3_�3 -- - Liao__- - -3 _r _— 2 :56 8 O?c)p 34.A 7#W, 150.3 34.3 TiKa 2.399 1311.3 ►54/ 9 o 7.V .341 3 _ig0.5 34, .3 ./ 23Q0 31. 3 _ 10 0 7/0 3ki:q Are, 1515 34. 3 2 30© 34. L1 l3r v f 11 s lo3 3Y• 1465 3�' L , t �-I-3 1 • - 1v 12 C,76Z ){,3 0'60 34.3 o 23 99 i 3 I-2 13 p 7 35%) _ram — 1t-60 Jy Z ( +'] ' is I 31, C5f 14 SIX 3�I,'1 2'd7 3/. Cf J G _ }-fir-�r+-� � � j --- 15 -1--� ' 6ss �C�'zt?c� .��:� __TOG _��0'6 �� o� avti,w� �..,�.�t� 1� 16 .,.p Ir 3 3q Y 1l46 t CO a 39, C n ,3e90 31.4 C s f 17 1_9_55_ ems - -1 Z349 3 � 3 18 _ 15 v o 341-3 TA, 23Q9 Yt 3 ( 19 o7cx. 3UJ 3 C 5 !503 3 - 2330 3 �,3 -e/ -- 20 1-21t) Ai 3 6 SS 107 3'Y, y A3C, 2.31 S 39. 3 rbM�! 21 0-7 i 3Y,3 C-S,I L ... y - 23O3 3 11,1. 22 07ex, 31,3 C-SS" ►'° I ey; G �30 ‘ tit all- _ 23 0°7c 3q, c-S.S /6/6 I 2 � -3`t 13rAr/- 24 act 5 i rz THG r 'D N,a CS'S 43os -c _Tfic 25 ozod IN6 13.0o 311,a _ as , :�y. 1_ -TMs 26 01o0 13y11 16r9,, /507 a At- - 2-3" -ct 3 t'PL) 27 61 - „L(-1 611, , lsl/ 3Y t3 c'0 _3L(3 ►wR+a 28 6)0(1 ,ti rf"tV\ 15is 1r,3 c- 000 3Li_Z puto 29 CPI,' ' �•3itiL Gr lY\ /5./0 YY.3 / LSO ' 3LisZ r'I w 30 61 '3(-\, r-, l5/2 3'43 oc) 31 r97oo 3LL ,Z '- I ZO 134IS A30O 34,2 CS.. City of Asheboro August 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd h' shift J Date Time Temp. Initials Time Temp. Initials Time Temp. Initials __ 700 35.2 - _Css Z _ 16/1A4 2 � L 3 CS 2 (a 4 1' 3(I, t �c, l 5o% 344 �iS� 3`� 3 i"irzu.. ._ 3 101 3411 )5e4, 34. Arm--- 2300 3% 4 ?o 4 Li,0 fre, rSao 3y,a Pr• Z30c ;t1,a 1"12,,.) 5_ 203 i333 era - 1565" 33.5 — - Z3oo 5y, r F1 6 , 7bC 33,7 ��1,ti l s-0s 33? >x— 2: 0(1 awl 8 07cso '3(1 o (nl NI 15 0 5 33 s teizt .3--) .91 Om j1'1 9__.07©O 33.3-- _.75: ,, 15 leg ' 'O 8' -t 23 3 3. Yik�,J 1 o b 2O a .-3 3;' i L1 :31 erc_t° .300 . 1,P CIS 11 c Sal 3?a' cc, _ l3�s 3� �� . � l5 cv o _ � Jai_� .�'�-G 12 G707 341.. 7146 15C90 3y.' ~TA6 7-366 -Y1,0 (,ai►1 13 oL11 _3 t_l -144 1. db -3 ,1 _2_a _ -z o -.34''7I J3Mr1 `�L`7 14 b g (rcpt.) j q lJ q. o� f G J ��� i `� / 15 0/01itb_ 4 .j Ls IL,27 341,v— ."14_ ( Q3015 3Y� 2 Orr 16 0705 34. 1 ,�tC - "li ?Gb 13'1 D Cif 17 a 7/0 g4.O '�� -e dam-18 19 -- - 1 �- - -- 20 21 22 23 - I 24 25 26 27 28 29 30 31 SEPTEMBa 20211 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig influent Dig Effluent % # _ DATE D- GALS D %S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern ,D#2 Tern % Solids %Vol Inf % Solids %Vol CO2 Dig 1 21200 0.0497 8787.358 34160 8775 10360 0.0226 1953 88825 33.9 135 57.4 129 142 4.97 74.6 3.15 55.5 37 2 2 20000 0.0521 8690.28 7400 0.02659 1641 67507 37.0 137 129 145' 5.21 72.6 37 2 3 19500 0.0482 7838.766 30144 7844 7120 0.03883 2306 51519 38.8 137 49.1 128 146 4.82 72.1 3.2 56.8 37 2 4 14600 0.0451 5491.556 40183 10255 0.04055 60401 51.2 137 57 128 146 4.51 75.3 3.17 57.2 39 2 5 16000 0.0485 6471.84 31619 7890 0.03842 94155 44.6 137 58.4 128 146 4.85 74.9 3.31 55.4 39 2 6 18100 0.0439 6626.881 0.03931 97708 39.2 137 _ 128_ 147 4.39 75.8 40 2 7 16600 0.0413 5717.737 8640 0.03918 2823 79943 43.8 137 127 147 4.13 75 39 2 8 15600 0.0456 5932.742 30175 7600 9260 0.04059 3135 692841 47.3 137 53.8 127 147 4.56 74 3.18 56.8 38 2 9 17800 0.0516 7660.123 20153 5110 7860 0.04011 2629 79943 40.9 137 52.8 127 147 5.16 73.2 3.14 56.3 38 2 10 16600 0.0421' 5828.492 22134 5519 4280 0.03442 1229 97708 42.8 137 53.1 127 147 4.21 73.7 3.13 56.8 38 2 11 17300 0.0458 6608.116 0.02135 79943 42.1 137 126 147 4.58 73.6 38 2 12 19200 0.0459 7349.875 0.02473 62178 38.8 137 126 147 4.59 75 39~2 13 27300 0.0499 11361.33 40269_ 10277 7120_ 0.02818 1673 44413 28.0 137 54 127 147 4.99 74.8 3.19 57.7 39 2 14 25900 0.0476 10281.89 45526 11490 6440 0.02485 1335 72837 28.4 137 55.5_ 128 147 4.76 75.1 3.16 57.3 41 2 15 16700 0.0494 6880.333 5860 0.02298 1123 84384 43.3 137 128 146 4.94 75.2 37 2 16 15100 0.0478 6019.645 5480 0.02134. 975 58625 49.6 137 127 147 4.78 75.6 36 2 17 14800 0.0471 5813.647 35959 8787 8240 0.02622 1802 51519 51.1 137 50.8 127 147 4.71 73.8 3.14 58.1 36 2 18 17300 0.0423 6103.129 44610 10941 0.0231 95931 41.2 137 50.4 128 147 4.23 73.9 3.1 58.4 37 2 19 18800 0.0469 7353.545 24056 5918 0.01982. 88825 38.2 138 46.8 128 147 4.69 72.6 3.15 58.5 36 2 20 20600 0.0454 7799.902 7340 0.02005. 1227 97708 34.5 137 127 146 4.54 72.4 39 2 21 19400 0.0503 8138.339 5340 0.01602 713 83496 _ 37.3 136 126 146 5.03 72.2 _ 38 2 22 19400 0.044 7119.024 48112 11797 9700 0.02154 1743 53295 38.9 136 41.1 127 146 4.4 70.1 3.1 58 35 2 23 11100 0.0585 5415.579 48053 11742 10180 0.01415 1201 87049 64.9 138 29.7 128 147 5.85 67 3.1 58.8 38 f 2 24 15000 0.0522 6530.22 9380 0.01863 1457_110143 46.5 137 127 146 5.22 64.5 38 2 25 16700 0.0485 6754.983 0.02249 95931 42.6 136 126 146 4.85 64.5 38 2 26 17600 0.0468 6869.491 0.02243 88825 40.9 136 124 147 4.68 66.2 37 2 27 17600 0.0536 7867.622 9060 0.02348 1774, 63954 42.3 137 126 148 5.36 65.1 34 2 28 19600 0.0652 10657.85 48367 11598 10060 0.02082 1747, 78166 37.2 138 34.9 128 148 6.52 68.5 3.13 58.6 39 2 29 20600 0.0471 8091.968 22150 5523 6820 0.02626 1494 94155 34.6 137 31.5 127 146 4.71 67.2 3.13 58.4 34 2 30 18000 0.0478 7175.736 10400 0.03818 3312 71060 40.9 136 125 147 4.78 69.2 35 2 TOT 544000 1.4502 219238 565670 141066 166340 0.817 37292 2349421 1241.015 4105_ 776.3 3816 4393 145 2158 50 919 1126 60 AVG 18133.33 0.048 7308 35354.4 8816.61 7921 0.027 1776 78314 41.36717 136.8 48.51875 127 146 5 71.9 3 57.4 38 2 JULY 2021 - SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D % S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re -D#1 tem D#2 Tern % Solids %Vol Inf % Solids %Vol CO2 Dig 1 25200 0.0554 11643.31 24483 6657 7200 0.03949 2371 71060 29.2 137 46.6 127 147 5.54 68.6 3.29 53.8 39 2 2 23400 0.0377 7357.381 22811 6449 4920 0.02887 1185 71060 31.5 135 47.1 127 142 3.77 69.6 3.06 54.8 37 2 3 23100' 0.0535 10306.99 31395 8353 0.01925 35530 33.4 136 46.1 128 143_ 5.35 68.4 3.34 53.8 37 2- 4 22600 0.0534 10065.05' 40470 10784 0.02187 62178 33.0 136 43.4 128 144 5.34 67.3 3.35 53.8 39 2 5 18500 0.0554 8547.666 20031 5396 0.02009 79943 39.3 137 f 44.1 128 145 5.54 68.1 3.32 54.4 38 2 6 17900 0.0506 7553.872 22386 5974 2360 0.02638 519 88825 40.2 138 47.8 128 147 5.06 69.6 3.36 54.4 38 2 7 15800 0.051 6720.372 23727 6906 5100 0.01177 501 88825 45.5 138 129 147 5.1 71 40 2 8 14000 0.0484 5651.184 10130 2720. 4180 88825 51.4 137 52.2 129 145 4.84 71.2 3.35 54.1 38 2 9 15300 0.0655 8357.931 5820 71060 48.2 137 128 145 6.55 66.4T 37 2 10 12900 0.0616 6627.298 21855 5796 79943 56.4 137 46.7 128 146 6.16 68.8 3.22 54 38 2 11 14800 0.0618 7628.0981 220811 : 5948 79943 49.2 138 49.6 128 147 6.18 70.1 2.36 54.1 38 2 12 12500 0.0583 6077.775 20811 5380 5200 71060 58.9 138 55.9 128 147_ 5.83 72.9 3.33 54.3 40 2 13 11100 0.0603 5582.212 32117 8735 5320 79943 65.6 138 58.4 128 147 6.03 73.9 3.36 54.1 40 2 14 13100 0.0523 5713.984 20217 5379 8120 _ 88825 54.9 138 52.9 128 148 5.23 71.6 3.32 54.3 39 2 15 13500 0.0502 5652.018 3920 _ 97708 52.6 138 128 148 5.02 71.6 39 2 16 14600' 0.0481 5856.848 4120 88825 49.2 138 128 148 4.81 70.9 38 2 17 12700 0.0541 5730.164 20480 5346 94155 56.2 138 54.9 128 148 5.41 68.5 2.96 49.5 37 2 18 16100 0.0571 7667.045 99484 44.0 138 128 148 5.71 73.5 38 2 19 13200 0.0532 5856.682 21017 5556 9120 84384 54.8 137 57.2 127 147 5.32 68.2 3.23 54.3 39 2 20 12300 0.0596 6113.887 21959 5805, 9120 93266 58.1 137 31.2 127 147 5.96 63.3 3.18 54.2 39 2 21 12000 0.0595 5954.76 9580 79943 60.7 137 127 148 5.95_ 64 39 2 22 14200 0.0601 7117.523 4620 62178 52.5 138' 127 148 6.01 65 35 2 231 13600 0.0594 6737.386 4240 48.854 55.8 137 126 149 5.94 70.2 39 2 24 15000 0.0586 7330.86 39083 51.3 137 126 149 5.86 70.5 37 2 25 14400 0.0608 7301.837 30476 7574 408601 53.3 137 54.8 125 149 6.08 71.8 3.09 53.5 39 2 26 16400 0.056 7659.456, 21344 5483 7680 35530 47.1 138 55.3 126_ 150 5.6 72.4 3.13 54 38 2 27 11700 0.0582 5679.04 22350 5927 8520 53295 64.5 138 62.2 126 150 5.82 75.8 3.15 54.2 40 2 28 14600 0.0539 6563.08 22023 5767 9640 0.02183. 1755 53295 51.7 139 57.2 127 150 5.39 73.5 3.14 54.3 40 2 29' 13500 0.0515 5798.385 19750 4941 8580 0.01782 1275 56848 55.6 139 58.7 127 150 5.15 73.8 3.14 53.7 38 2 30 11800 0.0537 5284.724 20456 ' 5374 4940 0.02806 1156 65731 62.9 138 63.2 126 149 5.37 75.6 3.09_ 53.2 39 2 31 16500 0.0533 7334.613 30655' 7261 0.02166 71060 44.7 138 58.5 127 149 37 2 TOT 476300 1.7125 217471, 543024 143514 132300 0.257 8762 2221513 1551.573 4259 1144 3949 4569 166 2106 67 1131 1189 62 AVG 15364.52 0.055 7015 23609.7 6239.72 6300 0.023 1252 71662 50.05075 137.4 52 127 147 6 70.2 3 53.8 38 2 U AUGUST 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D%S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tem D#2 Tern %Solids %Vol Inf %Solids %Vol 'CO2 Dig 1 15800 0.0487 6417.296 22917 5696 0.01969 84383.75 45.8 137 56.2 127 147 4.87 73.2 3.17 54.4 38 2 2 18300 0.0555 8470.521 19629 5189 4440 0.02902 1075 88825 39.3 136 47.7 127 145 5.55 68.9 3.18 53.7' 36 2 3 16400 0.055 7522.68 10114 2632 8880' 0.02226 1649 92378 43.6 136 52.4 127 145 5.5 71.4 3.15 54.3 35 2 4 15100 0.0523 6586.348 35990 8885 8320 0.02201 1527 88825 47.6 136 55.8 127 145 5.23 72.5 3.17 53.8 35 2 5 15100 0.0503 6334.48 30297 7707 6420 0.02 1071 104814 46.6 136 55.8 126 145 5.03 72.9 3.15 54.2 38 2 6 13400 0.0805 8996.358 10331 2680 7280 0.01999 1214 124355 51.0 135 56.8 126 145 8.05 48.2 3.1 54.1 38 2 7 10200 0.0529 4500.097 0.01886 119914 67.4 135 126 144 5.29 73.2 35 2 8 15400 0.0564 7243.79 0.02054 97708 46.1 135 125 145 5.64 67 37 2' 9 15900 0.0542 7187.245 5840 0.02014 981 79943 45.8 134 124 145 5.42 69 36 2 10 17000 0.0523 7415.094 8700 0.01886 1368 62178 43.9 135 124 145 5.23 66.6 36 2 11 20900 0.0503 8767.592 75690 19250 6120 0.02266 1157 53295 36.1, 135 45.1 125 145 5.03 67.8 3.02 53.6 38 2 12 21700 0.0528 9555.638 20491 5640 6480 0.01765 954 102149 32.5 135 41.6 125 145 5.28 68.1 3.09 55.5 38 2 13 14900 0.0493 6126.314 23955, 5954 6260 0.03364 1756 115473 46.5 136 48.4 125 146 4.93 69.8 3.07 54.4 36 2 14 19200 0.054 8646.912 0.04136 103037 36.7 135 125 146 5.4 69.3 _ _ 36 2 15 28600 0.0439 10471.2 0.04077 76390 25.6 135 126 145 4.39 70.2 36 2 16 31000 0.0467 12073.82' 40442 10254 6800 0.0388 2200 47966 24.5 135 50.3 126 145 4.67 71.5 3.17 55.5 36 2 17_ 21800 0.0458 8326.99 46324 11434 6360 0.04107 2178 88825 33.0 136 53.7 127 146 4.58 73 3.22 55.6 36 2 18 19800 0.0554 9148.313 7480 0.03163 1973 79943 36.8 135 126 145 5.54 70.9 39 2 19 16600 0.062 8583.528 7560 0.0357 2251 58625 45.1 135 127 144 6.2 67.4 39 2 20 25200 0.0462 9709.762 32246 8041 9840 0.03824 3138 39971 30.5 136 41.6 127 145 4.62 68.5 3.16 55.9 39 2 21_ 27900 0.0401 9330.709 48167 11971 0.0403 44413 27.4 136 40.7 127 145 4.01 68.5 3.24 56.3 36T 2 22 17900 0.0534 7971.872 43373 11539 0.03633 _ 62178 41.7 136_ 49.8 127 145 5.34 72.3 3.19 56.7 37` 2 23 16700 0.0518 7214.6I 7580 0.03889 2459_ 79943 43.6 136 128 145 5.18 67.5 39 2 24 16700 0.0497 6922.117 6160 0.03785 1945 63954 44.5 137 127 147 4.97 6.86 39 2 25 20100 0.0533 8934.892 41920 10418 7520 0.03903 2448 49742 37.7 137 46.6 128 147 5.33 70.2 3.14 55.7 39 2 26 13600 0.0497 5637.173 44079 11102 7240 0.01594 962 97708 52.2 138 43.6 128 147 4.97 69.6 3.18 56.3' 39 2 27 17900 0.0554' 8270.444 7480 0.02193 1368 97708 39.7 138 129 147 5.54 71.2 38 2 28 16100 0.0434 5827.492 0.0206 79943 45.2 138 129 148 4.34 69.4 39 2 29 17800 0.0522 7749.194 0.01849 62178 41.9 _ 139 129 149 5.22 69.8 39 2 30 26500 0.0528 11669.33 22468 6015 9280 0.01655 1281 42636 28.9 136 45.6 129 142 5.28 70.6 3.15 56.6 37V 2 31 20000 0.0525 8757 31451 7977 8800 0.02387 1752 67507 37.0 134 51 129 139 5.25 72.6 3.2 56.5 37 2 TOT 583500 1.6188 250369 599884' 152381 160840 0.863 36706 2456900 1264.069' 4215 882.7 3927 4503 162 2088 57 993 1156 62 AVG _ 18822.58 0.052 8076 33326.9 8465.6 7311 0.028 1668 79255 40.77643 136.0 49.03889 127 145 5 67.4 31 55.2 37 2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQ0001684 WWTP Name: Asheboro WWTP NPDES Number: NC0026123 Monitoring Period: From 10/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed(Class A only)indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen DensityNumber of Parameter gExcee- in Frequency Sample Analytical Sludge Minimum Geo. Mean Maximum Units dences of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1028 7625 1973684 col/g 0 Quarterly C 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(thy coliform) weight) Vector Attraction Reduction (15A NCAC 02T.1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) r❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman -Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name andTitle (if applicable)(type or print) Jan 26,2022 1/26/2022 Signature of Preparer* Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) City of A, '1oro Department of Water Quality Fecal Coliform in Sludge r-. to q.z . 101t- z1 ,10. 15.0 10.1�• l! Jo. 11--zl to. 2:.a-.1 Ire. l.2r Tine : :. `LIo 131, g:00 10 z.Q qi 25 5',' 5 - � Location ( ✓ 7u.r.•1 L Co v.),u; d ,CLN tou.�.1 d v bct..'ld o v ►4o( f�v fr c6, Un%v�)9c4-c 1 d l ,4i st:', 1(4- e—f, kyr `�44-- ,ter Dish Number I 3 P 5 C 1 t'Dio&Wts:::. /0• og>g 3 /R. 2717 //- ,ov 1a• 10 4i IQ•0198"3 11- 00g7 q1t q33 ur_ Dish /• i i ci 1. 1 i -3 g- , d eqci-)() 1. 12 72 , i . 103 3 i 611 3 - ) , I27 vyt Wret Solids.,. ‘3.i.11.9011 11 , 1519 1 o - M 2 30 9, L/71(s ?.q to q t ?c.f - 3°S� rt '4 ;s:: . . v� 350 .- . Ll 3. �9 sZ .3. d17q O8 , 3, J7g Jv fJ� WtDish- - ///.- / 1 l 3 0 - 6? 7c2 1. 1 I . 103_3 w►tp�;s�Tts � - 10 � 15s ,�. `3r7 3q � ( • 1 j�� Z�17 7 SD , . 090 i , 50 a. r1 � �. sal s :%Dry sooltds ,20. . .20. 7 , .7��Imo' , . 06 , . ] , , 1 (, 30 . Fetal to • Date in t 0• I L-1. 21 10 , l U.-21 10.1w.2.1 1 e .7 2f 1 O. l c(• 2,t 1Q 20. 1 10 at T a 1 q`a7 I3: 3% :'40 11 : 09 (0B3 1005 1I aysUn 'JD c�03--- Pit color ies` _-ices":;::: :'';' Yco dflTe : ml'sariFr le #colonies ;��,h�-• . � . 0 - -..#�: t�es �. � #colonies *colonies 0-Uo01 C' 0 `. 0 _ O 0 Ca 0 0.0003: n P O 0 0 0 7 to a 0 o0i. C - 0 i S 0 U o:0a p _ 0 7 coo gra ri[ y: fudge 1 Z, 109�` l 0474,,106,14 2..t, cras. �5 1 5 Li.9�� < 150 F� ' ! 5'!C) >1 t? l t ate:0M.D to. 15. 2-110: 15 -21 I o o .7 I cf• i 1.0.2.(0 ), o?I a- , t 51 : ro)`e _ :.45 1 © 3' 1©o--- ' 1.O 3 0 S�,1 ,And sti'out `. DIr � 71,E-4r _ �� i Coliform Colonies/gram=Coliform colonies counted X 100 4 mI X%Dry Solids rats? 2 _4 4 a Geometric Mean W9 S5 alp of alcbeboro Dry Solids for Sludge Hauling ,Date • J4- Z-I 0 . I5.'/I 1a •) $ 47/ 10-1q.21 fO 2o.?-1 Analyst Initials --Bur - f- Dish Number 1612 , (ZZ v5g S vvV; 1 op �J1au- theyt.A., Source _ 51uGi' 51�� 5/t SLL. S/ko[r, Wt. Dish &Wet Solid (g) /I. /5113 qo2 (Oto 91. ,9O, 90. viii5e /03. F9 Wt. Dish (g) 71. 0930 7(e V61(. 7g. qy0' 10. 3 o ys.11 i I Wt. Wet Solid (g) _ 6- 0013 I,. 9 732 1 200 1 y. 142 73?Y Wt. Dish & Dry Solid (g) eK 0 . 0 333- '79. EeW U. 6 739 ?q. 49 759 181- %$( Wt. Dish (g) 18r-t19 `l 61- 5xer 1 S.g y07 '7&. 3.)Lo 5'5 !)j l Wt. Dry Solid (g) 11(402. 3133-M, . . 0332! 0,15) . 3 -8 6' 3 ib Dry Solid 094• t Z P•V ! o , 20 OZ 020,5Z c2O- (9 .54 ea Weight(Ib/ft3) 51er ihS 13v )h5 5v /b 601 1,5 509s' Operator Initials .j4) /6/1 ) ntgrA) rfr-rnl alto xz� .. 1P' • Cttp of Abe olro % Dry Solids for Sludge Hauling Date f O.l ). 1 Analyst Initials Dish Number Hnta Source SJiid- er Wt. Dish &Wet Solid (g) 1•/v(,1 Wt. Dish (g) 'dp. S1/6 Wt. Wet Solid (g) 1 t15--q Wt. Dish &Dry Solid (g) GQ. 33/5 Wt. Dish (g) -7(P• g'/f'3 Wt. Dry Solid (g) . q j 2 % Dry Solid g0. 0e, Weight (Ib/ft3) 5 /65 Operator Initials ^ meid CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503(White House Manual)Appendix D Revised 5-28-14 [bay 1 Date- j I) 1•,21 Moisture and d Dry Solids Average Dish# j rQ r 'JWt Dish+Wet Solids, g S'4•Sq�j_ �Io•3'�_ �] ItoR. ,,,W, 7I•Of2Wt Dish _I ��, g . /W. D ao . 70. S7_ 735. 9'7 , 17 .94077 Wt Wet Solids, g .t•I S 15 9.4 e) 70l 5. . q. S-qqq jv/. ay 1 . ` ` Wt Dish+Dry Solids, g •g2i -d 170 )qj Tr-454 r7F.S7 •3 i U WtDish, g ,`7 .o o(, .1(,.3057. 7 $'. U3$S_ 78'. 27 7�3'•9w i Wt Dry Solids, g 10.19(.e C( O. 30 3i Q•'-I 15' ❑•CO 0. %Dry Solids ' 3 3•b57 _ 3.03 3.o37�, 3. 0 Z r;. d14Z -'1.)7.dq Volatile Solids Wt Dish+Dry Solids, g isfr.2 7&.(0,2441 '.f -j3 1 .57 y _ 7 .713.31 m Wt Dish+Ign Solids, g lg./f7 1.7(P•LI _% r7 I I r7�.` Wt Ign Solids, �7 � � �� •'7�' �y 5 g g Q. ► 1 � 0.1755 0. 7i-i1:2 0. 175W Q. 2JL 3 %Vol Solid 'j�. 1 Z 51. Z 52.0 Z 5g4 Z 50-.0 Z .' 1 Analyst Checked by Day 20 Date j W. 11. 1 ) Moisture and Dry Solids Average lurr� Dish# �� . q 5 g �p - • 3 . Wt Dish+Wet Solids, g , Oo7.5'I7O _eq. S5S'Q . 2563 %L%• 0715- • 1t/ ' Wt Dish,g v7'. 13;3 r7g. 093 . 7g. U377 . i7< 2-719 7 3.939 . Wt Wet Solids, g I l. £J 7 10.12c7 10..l0(.e 7 79'' -7. SD8 Wt Dish+Dry Solids,g '7/. y ffa 9 •• 1 •125(e, Fv. 3536 I-n.5 6 , 72. 1011 Wt Dish, g 71 13 k5 . 7? .• 7R 0317 7k 2711 7g-:y • Dry Solids,g .-Du�r(0 0 3i(03 10.3ai 3 ❑. ��qt, 0. aai ry Solids 3 .1:2)a _ Q.95 3. 15 _ 3, 0 h'3 3. 0`2i Volatile Solids Wt Dish+Dry.Solids,g 1 i.`lg-)ci 9 Li, I gLo 1g 35 3o. i r.5215 '7q. I a( 1 Wt Dish+lgn Solids, g 7(.2S5o g,qq•Ltz5 7 S.17.q() 72.3 7 6 -7 G• -3 Wt Ign Solids, g ❑•1 i 7 C1 . Q.I 11 ('). 15f tt 0.1 d2 d_ (' % Vol Solids _ 57.' 4 4-z �7. 99(o.O 5 7� 5'7 3 Z . 7.( Analyst , Checked by 120 Day VSR1 ,� _ Day 40 Date 11. 1 0-„I1 oisture and Dry Solids Average Dish# I •. g iWt Dish+Wet Solids, g !Y•a�'1 . p5. . __$ �'v. t 9/.2 se O%& ( 'O I Wt Dish, g t: 4 .. - 7,•/A. 3 � '1i b375 - riS• g7 r '. 9.39�] Wt Wet Solids,g I1l liJ `T. 5 7 q.72"1- V/691-2;Wt Dish+Dry Solids,g ;, 0 j 7[a.. � ' 2 4, t7f 559 ,2 Wt Dish, g ,0 -� �7 - Wt Dry Solids, g fl '7j a %Dry Solids _ , . ,2 . O 7 _ Volatile Solids _ Wt Dish+Dry Solids, g ,L -Q a . � 1 p - 7t. SSO , 79 2773 Wt Dish +Ign Solids, g -7 5 :,9dG 2 °?(o.q 9to `7 ./4I 31 '7 .3 q I. 7 4.ow 1 ir Wt!gn Solids, g t 7 0. 155C) - 0. 11455 O.1 Cv.3046,55 _ • y%Vol Solids 5 to. 5 t'7, 7 Z 5'7. 9 z _ S'7. qT Z 5 rl. (o ? . S 7,Cp 1/AnalystChecked by 40 Day VSR �, VSR= VS,,dgIn,1-VSfi.,,i VSoriginal- (VSoriginal X VSfinal) City of Asheboro October 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. ; Initials Time Temp. Initials Time Temp. Initials 1 _ 07/0 33.6 / - .._ 15o6 t a•it\ 23co _ .T.i c}s"2 0705 Si, LS_ 14 45 3 , fr.:SZ - 33. I ,s , 3 0703 33.a / 14455— 33.3 ,ram Asa., xSa 4 Ob(7 33r.'i 1L//Ca 33, r i l P.3306 3i�i St 5 C!65-6 3'3 r er =) 1 L, r G azio� 13)..?, J.f 6 d 33.6 !95S W. 3t.+c) ?3. crY 7 07/d 33E /45G �33,5 jtrc. j �3-te 1� 8 0)57 33,5' 11 )9 4, 6 any 31 G �; 9- 6tfb 33, 7 1 `Z � ! 30o 3) ( Csf 1 o a '33, 1 `i G.� )(Jac 3 %7 `�1,f 30D 2 �2 Gss 11 _ .7o� 3„7 -z /5/s- 113.4 / - 30.2 32. (1 C5S — 12 074 f3: 5 yea s3,/ /4C i S 1C2 1S1 13 665-49 33,6 ` I _I Y3,O 3'.�, _ b 3(,0 14 0i A ' r33,6d -cc l zi lb 3,to Jf IAi a 300 33 : 65-r 15 6 7/5 - 33. I-PS. Z.31 O 3 3. {o (h�+J 16 O7'D 33.S- — _ r 17 6745 Y. � fr=s-c--- 1 53 33.E Xrc - a 3 DC- -3 18 870 I. 3316r .�3°( f 19 0 700 3 )14 j2rw/ � `� Q 33 N G; ' 2300 33.3 <55 20 6.765 33. del''( 33.G . eiSoo 33,Li 65 21 D7// ff 3.2.7 F' /550 I — 2,8 .23 v J 37 5 5K 22 D70 L 3 '— t Ito 1.1; -- ,2.3 uJ ,3 a.g Iry v ?3 65 t4L N21 33 it ILIA/ -2,3,0 31, 24 p LI- 9 ,D 1430 Soo 33,1-6 QY 25 O 775 33,0 /510/ 13. I rc-,a C9 1 - 26 67/O s � I /� 53•v . 27 E105q 13)3 . iy4 ) ff � erg -Alb- I ) 3 �s► — 28 6 VO S,q TC.- , eq 3e ' 3t2 -eC., 4* '3 (-1S 29 0 7/61 Via, 9 �:rC� iits5 336 - _ 3300 -Ill Cif 30 O767 z•9 ,AC- J5'?5 J r tAc 2.300 3 3, t -3-4+7_ 31 67/5 •? Arc. /575 _V ono Q City of Asheboro November 2021 Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time I Temp. Initials Time Temp. Initials Time Temp. Initials 1 :039 '-fatAl Ltipo „Ito rad 2.3_04, 2 b697 3L' iiJ iLU 0 "‘ill 2aoU 3.S. cl_SY 3 es-7/ 52, 1 _,E4z. sza,9 AT., )AV 3çi, 4 o To 8 3d. 8 1i:cr._ r 55 3Q, s Arc. f9- 5 b1: ZoR9 (j jq2 c 6 8700 -33lb 1 /36 33,o -rck -?30s- 7 rii,‘L, 3PS 1(4Ltil 141)S3t2iLZ_3 00 3z..9 8 6760 3,o Asc_ 14130 133, I AsC... .3(:) E 9 0700 Si-(i At W‘ t..15 33.1 ICC 2_ 443 ? 10 0-700 3 /fakAi °Z3,0 1-iLd nao r 32- ob5V 33,t (14) lq (7 33 le-ted -?360 33' 1 r.IE 12 0--7"0 33.3 Ar.— q30 33‘ ,4 OC IG 13 ,e)7/6 33.a Arc /5'36 33. AC N=)4(2_ 37-2 a 14 0 7/5 13,45 AJ /5ic5 3?.0 2_ 5 (96 3 tq- 15 cf? 33 ER le-1.4 )10'6 33 laLij oc?6 16 0-20 0 33, 144. a3 Gt. 33 e.E 17 18 19 20 21 22 23 24 25 26 27 — • 28 29 30 31 _} 5-R , ) City of i " boro IA- Department of Water Quality 11- 2 -2_1 40 I l -12 21 Fecal Coliform in Sludge Sample Collection Sample S (Jo Date _ 11.?-21 11-.9.--21 I I .11 , 21 I l.10. 2_1 II . 11 . 2-1 II . 11 _21 14 ._.p. I Time _ '1: 30 i o : ZS 1&; 2 5 T.' L'• 10:Z0 10:2.6 I ID:S Location CO/ 6u.:-101 rnv 3 1ecI C4.1%/ 'B r k CAS 10u:;Id Cziv T31ei - cfw F)(R51 CA%.1 Rw id Analyst -11 r11 -11,45- t ux- %:Solids Dish Number ( r? 3 4- 5 Wt Dish&Wt s i O.Q •' I:o. s a4's�s q, �i _ I I. )2 59 ha. en 3c, 13 3 i 1 . 2q 7 . WtDish 0 ,c1914 . 1 .0 'dB 1 . 1 )Q1i t, Or(4l11 /. ! 117t9 j.- 113'- , 1. 08Goq WtWetSolids _ q.cot ice) c1,45(00 2. 3 )O. nn5(OS ? .9)(v5 7 /1. 1 (a(v 10. v7933 Wt Dish& Dry S ' 0,1150S a .�(1) 5' . a ,NS 70 3.0(pp�S , 3. O -003 3,5455 �f, 3, 1.,F WtDISK 0ga"14 _ 1 . 01GD I .13D/i 1 1. O I/ jF 10I I+ 1r //3 / 1... orrIpLf Wt Dry Solids . 1 .15 dA Lc 7 vs _ I .q 51, , _ /.q 7 5 I • i 2j� , d. 43 a/ . 357 to %`Dry Solids 11 . 3 Z , i67, 510 , ,g . 1 719. 7 / 0/. Li Z c)0. Q Z _ .7/ .q Analyst `)L.i?r _ "Dl TD 1 17- '1 ,�~ r Fecal Conform Date In 11rS- o1 iIA ' ! 11 .9, 1 f? . it 2i 17. 11. E a 11. v,21 1l 1(7, 1 Time In J 1.'I 11:0'7 )t;07 1 t:,J7 ! 13 /1113 _ /1 : a _ Analyst In 3i,t 71 li ]2i -al Jr ml sample #colonies # lonies #colonies s #cnies #colonies #'colonies #colonies 0.0001 0.0003 n - ,,��rr o _ 0 V 0 0V / 0 J) 0.001 -! 0 (.9 0 c 0 / 0,003 cQ (9 (r9 0 5 0 3 - Rule used for calculation j6, S 9 .2) 21, 21,. - Fecai Coliform/ gram Dry Sludge h. 1/7/0 L /68 /50ff L /692 C yz-i9 P L )(Pt 27 2)/51 'Date Out /].q.71 , /I- /0.2/ ll. ro•2/ 1/. //.2/ H. I2-2/ /1 -' Z•71 //. /?.2/ Time Out 1107 1/;Z7 /1 : 27 //:/3 1 1.7 2 j is z7 0i73f7 Analyst out s f j 5 . � 2)t,[i� 1l"G gloliform Colonies ram=Colifor m lonies counted)400 �-- ml X%Dry Solids Geometric Mean G e2 /l-�50 cfu/g C City of A )oro In. 574-&-v-- Department of Water Quality Fecal Coliform in Sludge Date. . :_ //. 29• �/ 11. )9,2( /1 .v _ //. 3b Z/ 12• l•z-/ 12 •(-2I j2-(p2.t Titae ::,-:.. /'-1 ZU /tew 1635 ia33 /(5, l/575' r751) ;kcs i.e.:: Co•✓bi id ki_ Go✓b.u./IdigktCw b 'ld!r.AA- avlor.iJ) w- 60r61 6- . 611i:61 .11 ! eb _ i:,- ) eFA . Dish Number f .2- - - 69 _ tDish&wts, 10. 3 c2 77 Jo. -s- F. (i(iiS' . / o2 `?'- clo ' iZ-Z7o I2`n2 -`j' ::, :. . . I. ioo2 _ /. oq 19 , J. o7 [, q4 5 /, /f•: . f 1 (7 . 1 lam/ 4,4.Wet.5PJids,:. 9. �(a ` co1.5 s 9 l I .7 _ 2r, 7 O _ 1. 155.• _ i t on C'1'�? Dire&0.0,.. . Q.611 g saLii4- -)�(P`f" �. 22/ ;7. i5 3259 , 3,1438-5 ati t:Disli ------ %. / • /oO S 1009161 1 . 1019 1 O 99I S [. i l 3 1' / 1 (77 /- (ZzI )41.0fi l s:...-- . I, 1 g. i51 1 . 4IR% 0 • i ' 1. 70/e 9 /Li/ c `�.r5,(4 ,:%:Dry s_olyds. c� gg. « ,110 17 1 c7• lg. �z k 9 5?1-9 _ Analyst ,- A.1— - � Date In jO. Z• ZI //• 2q_21 I1 . .30. 21 it. 3C•2J /Z•t.z.( tZ•(•2,1 12-.67.�1 tithe i; . 1517 _ 1577 11 1.-2- I, 1 Z Z `2S 12 1 (5 2. Aitt is stio Rif sample #colonies #`colonies..' ,..:,,,,i: . % c:..,: � .tte . !ri(q�ri�:�s> cf. :����� '� ial�ea #colonies LJ#:colonies _ 'Si 0.0003: _ 2 3-7� 7. 60 DO IFe.q:C lifbrrol { a ,rAr e grai l Urysi..0 g'e 2 3l ci 4 I O 33 (0 61 X? L. 1�0 a (0# , 13CI 7 3,J 5,aoo 'a-MR 1100 11• 3(') •FA l Z111. la. a•g1 i .a 1 flme Oet: .` I 50 i'-3' I i . 114.3 11 i 1 t 1 1 11 Coliform Colonie 11.ram=Colifarti colonies counted X 100 ml X%Dry Solids Geometric Mean a `5 DECEMBEE 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig Influent Dig Effluent % # DATE D-GALS D % S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tem D#2 Tern %Solids %Vol Ini%Solids %Vol CO2 Dig 1 15400 0.0551 7076.824 40692 9536 8960 0.00003 2 155443.8 42.4 131 46.1 117 144 5.51 72.9 3.01 59.2 36 2 2 14000 0.0544 6351.744 12500 0.0075 782 142120 47.6 130 117 143 5.44 74.6 41 2 3 11200 0.0547 5109.418 41443 10023 6840 0.00865 493 124355 61.0 130 116 145 5.47 75.2 39 2 4 15300 0.0525 6699.105 0.00953 159885 42.4 131 51.8 116 146 5.25 75.2 2.94 59.4 35 2 5 14700 0.054 6620.292 0.01074 142120 45.3 130 115 146 5.4 74.8 39 2 6 14700 0.05 6129.9 44216 10325 10260 0.01387 1187 164326 43.8 131 48.9 117 146 5 74.5 3 59.9 35' 2 7 16200 0.0494 6674.335 11260 0.01626 1527 159885 40.0 131 117 145 4.94 76.2 35 2 8 15200 0.0489 6198.955 12260 0.02013 2058 133238 44.4 131 117 145 4.89 76.1 40 2 9 11900 0.0564 5597.474 _ 11800 0.02407 2369 124355 57.4 132 118 145 5.64 77.4 40' 2 101 18900 0.0543 8559.092 20373 4944 12340 0.01858 1912 133238 35.7 132 47.6 118 145 5.43 74.5 3.01 60.5 40 2 11 15400 0.0521 6691.516 0.01886 115473 45.0 131 117 145 5.21 74.8 34 2 12 15800 0.0537 7076.156 0.01955 97708 44.9 131 118 145 5.37 73.2 39 2 13 17600 0.0488 7163.059 12660 0.03171 3348 79943 41.4 130 116' 145 4.88 73.3 39 2 14 11600 0.0464- 4488.922 50217 11266 10540 0.01725 1516 115473 59.7 131 49.2 118 145 4.64 73.6 2.88 58.6 34 2 15 13100 0.0546 5965.268 39978 94021 12960 0.01972 2131 142120 50.8 132 46.2 118 145 5.46 73.1 2.97 59.4 33 2 16 10400 0.0546 4735.786 9380 0.02295 1795 133238 64.9 131 118 145 5.46 75 38 2 17 12400 0.0488 5046.701 20134 4702 7100 0.02182 1292 115473 55.8 132 116 147 4.88 74.9- 38 2 18 12700 0.0563 5963.183 0.02698 127908 53.5 132 55.4 118 147 5.63 76.4 2.84 59.1 39 2 19 15700 0.0505 6612.369 20624 4954 0.01863 133238 43.0 131 55 116 147 5.05 76.4 2.89 59.3 40 2 20 14500 0.0551 6663.243 40361 9492 12700 0.02015 2134 155444 45.0 132 50.7 119 145 5.51 74.4 2.84 58.9 39 2 21 15300 0.062 7911.324 40711 9914 10320 0.02158 1857 137679 43.8 131 118 143 6.2 78.6 35 2 22 15300 0.0456 5818.651 11000 0.01989 1825 124355 44.7 131 119 143j 4.56 75.5 34 2 23 13800 0.0472 5432.342 20661 5100 0.02071 151003 47.6 131 51.7 118 145 4.72 75.4 3.25 59.7 38 2 24 14500 0.054 6530.22 0.01821 159885 44.7 1311 59.3 118 144 5.4 75.8 2.87 59.3 33 2 25 1 14200 0.0526 6229.313 0.02112 142120 46.9 131 118 144 5.26 75 38 2 26 12100 0.0506 5106.248 0.0191 128796 56.1 131 117 145 5.06 73.8 - 37 2 27 12300 0.0549 5631.752 0.02511 120802 55.9 132 45.6 118 146 5.49 74.1 ' 2.94 60.9 38 2 28 13700 0.0528 6032.822-, 31170 7643 10320 0.01969 1695 127908 49.6 131 52.5 117 146 5.28 74.8 2.86 58.5 38 2 29 15400 0.0578 7423.601 20942 4960 14160 0.01665 1966 120802 44.6 132 117 146 5.78 67.2 38 2 30 13400 0.0507 5666.029 9980 0.01812 1508 127908 50.7 131 117 146 5.07 75.8 39 2 31 15300 0.0512 6533.222 0.02542 111920 45.5 132 I 116 147 38' 2 TOT 442000 1.63 193739 431522 102263 207340 0.573 31399 4108156 1493.914 4070 660 3638 4502 158 2243 38 773 1159 62 AVG , 14258.06 0.053 6250 33194 7866.4, 10913 0.018 1653 132521 48.19076 131.3 50.7692 117 145 5 74.8, 3 59.4 37 2 c U OCTOBEF 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS F Dig Influent Dig Effluent % # DATE D-GALS D % S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern D#2 Tern % Solids %Vol Inf%Solids %Vol CO2 Dig 1 20200 0.0466 7850.609 35035 8590 8880 0.04266 3159 60401 37.0 137 43.3 127 147' 4.66 71.4 3.02' 58.6 35 2 2 19200 0.0532 8518.81 60548 1 14392 0.03946 72837 38.3 137 43.6 127 147 5.32 71.1 3.03 58.1 38 2 3 19500 0.0472 7676.136 0.04082 106590 36.0 136 126 145 4.72 71.3 36 2' 4 22600 0.0515 9706.926 8960 0.03633 2715 97708 31.4 136' 126 146 5.15 74 36 2 5 22200 0.0462 8553.838 11979 2937 7720 0.04235 2727 74613 33.0 135 48.9' 126 145 4.62 73.4 3.07 58.5 38 2 6 25800 0.0444 9553.637 43704 10424 8220 0.039 2674, 62178 28.9 136 46.6 126 145 4.44 72.6 3.08 58.6 36 2' 7 25100 0.0461 9650.297 44582 10820 8560 0.03844 2744 79943_ 29.0 136 44.7 127 145 4.61 71.9 3.11 58.6 36 2 8 22200 0.0441 8165.027 31532 7837 1 8180 0.03068 2093 97708 32.0 135 47.7 126 144 4.41 72.7 3.08 58.2; 38 2 9 24100 0.0496 9969.302 0.01254 97708 29.5 135 126 144 4.96 70 36 2 10 24500 0.0445 9092.685 0.01917 76390 29.9 134 125 143 4.45 67 38 2 11 24200 0.052 10495.06 41478 9893 8320 0.02243 1556 44413 31.5 135 33.4 126 143 5.2 68.1 3.1 58.7 39 2 12 20000 0.0477 7956.36 51454 12917 8500 0.02397 1699 71060 36.8 _ 135 45.6 126 143 4.77 72.4 3.14 58.8 37 2 13 17200 0.0477 6842.47 53361 13262 8480 0.02678 1894 106590 40.8 136 47.7 128 144 4.77 73.5 3.16 59.2 39 2 14 17600 0.0473 6942.883 _ 9140 0.02596 1979 140344 37.9 136 127 145 4.73 74- 39 2 15 16600 0.058 8029.752 7500 0.01486 929' 119026 41.5 136 126 145 5.8 76.2 37 2 16 15000 0.0522 6530.22 0.03678 97708 47.3 135 125 145 5.22 75.4 39 2 17 15400 0.0506 6498.862 _ 0.0223 88825 46.7 135 123 146 5.06 74.4 39 2 18 16100 0.0483 6485.434 44098 11328 9300 0.02088 1619 65731 46.1 134 51.6 123 145 4.83' 74.6 3.1 58.7 37 2 19 14500 0.0485 5865.105 8860 0.02293 1694' 97708 49.0 135 124 145 4.85 75.7 39 2 20 17400 0.0488 7081.6611 71066 17484 10060 0.02205 1850 85272 41.5 135 54.5 124 146 4.88 75.3 3.1 54.5 38 2 21 16100 0.0578 7761.037 40493 10030 9300 0.01956 1517 142120 41.3 135 56.5 124 146 5.78 76.7 3.13 58.9 39 2 22 17300 0.0542 7820.084 10500 0.02408 2109 168768 36.9 135 124 146 5.42 74.6 39 2 23 19300 0.0507_8160.773 0.02088 142120 34.5 134 122 146 5.07 76.3 - 37 2 24 19000 0.0482 7637.772 0.02057 124355 36.0 133 121 145 4.82 76.7 39 2 25 18600 0.0468 7259.803 21179 5140 8520 0.0197 1400 103037 37.9 134 58 123 145' 4.68 77.7 3.16 59.4 37 2 26 19900 0.0543 9011.954 55904 13568 8580 0.01661 1189 108367 35.1 134 56.1 124 145 5.43 76.2 3.11 58.4 40 2 27 20000 0.0545 9090.6 7700 0.02353 1511 142120 33.3 134 123 144 5.45 75 39 2 28 19000 0.0474 7511.004 _ 8080 0.02298 1549 124355 36.0 133 121 144. 4.74 76.1. 38 2 29 18800 0.0514 8059.109 10120 0.01892 1597 97708 37.8 133 122 145 5.14 75.1 37 2 30 17500 0.0483 7049.385 60948 14283 0.02031 83496 41.4 134 42.2 123 145 4.83 71 3.05 59.8 38 2 31 17500 0.0482 7034.79 43554 10352 0.01789 124355 39.1 133 43.7 123 144 4.82, 71.8 3.04 58.9 38 2 TOT 602400 1.5363 247861 710915 173258 183480 0.805 40204 3103546 1153.386 4178 764.1 3866 4491 154 2282 49 936 1171 62 AVG 19432.26 0.050 7996, 44432.2 10829 8737 0.026, 1914 100114 37.20601 134.8 47.7563 125 145 5 73.6, 3 58.5 38 2 NOVEMBE, 2021 SLUDGE REPORT FOR DIG, PRESS, NIT WASTING AND DET TIME FOR 503 REGS Dig _Influent Dig Effluent % # DATE D-GALS D% S D- LBS PR GAL PR LBS RAS Nit Gal Nit Lbs Gal Room Det Time Avg Tern %vol Re D#1 tern D#2 Tern % Solids %Vol Inf % Solids %Vol CO2 Dig 1 18700 0.046 7174.068 8680_ 0.02429 1758 151002.5 35.1 134 122 145 4.6 73.7 39 2 2 15800 0.0473 6232.816 7540 0.02308 1451 133238 42.7 133 120 145 4.73 73 37 2 3 14900 0.0482 5989.621 59231 14326 9540 0.0264 2100 120802 46.1 133 44.8 121 145 4.82 72.1 3.01 58.8 39 2 4 15500 0.0489 6321.303 24141 5758 10200 0.02013 1712 163438 41.6 135 46.3 124 146 4.89 73 3.06 59.2 39 2 5 18300 0.0469 7157.972 8320 0.0263 1825 168768 34.9 134 122 145 4.69 74.2 39 2 6 17500 0.0474 6918.03 0.02019 163438 36.8 132 121 144 4.74 76.1 39 2 7 17600 0.0447 6561.245 0.02304 127908 38.6 132 119 144 4.47 74.8' 38 2 8 20000 0.0484 8073.12 59308 13899 8340 0.01929 1342 115473 34.6 133 52 121 145 4.84 75.3 3.03 59.4 34 2 9 17000 0.0498 7060.644 46836 11093 8300 0.02413 1670 154556 38.4 133 49.7 122 144 4.98 74.9 3.06 60 39 2 10 14700 0.0506. 6203.459 _ 10160 0.02304 1952 186533 42.3 134 123 145 5.06 75.8 38 2 11 16300. 0.0554 7531.187 8380 0.03029 2117 168768 39.2 133 _ 121 146 5.54 76.6 _ 38 2 12 17800 0.0512 7600.742 8740 0.00514 _ 375 151003 36.9 132 120 145 5.12 76.4 _ 38 2 13 18200 0.0509 7726.009 0.00004 133238 37.1 132 120 145 5.09 74.6 38 2 14 13900 0.0544 6306.374 0.00002 119914 49.5 132 120 145 5.44 75 39 2 15 18200 0.0501 7604.579 9760 0.00004 3 99484 38.9 132 118 145 5.01 76 40 2 16 14100 0.0601 7067.399 42289 9840 10420 0.00003 3 124355 48.5 133 51.7 120 145 6.01 75.5 3.01 59.8 37 2 17 15700 0.0584 7646.779 41001_ 10122 11780 0.00003 3 151003 41.8 133 50.3 121 145 5.84 75.1 3.04 59.9_ 39 2 18 13800 0.0536 6168.931 11000 0.00003 3 133238 48.9 133 122 145 5.36 74.5 37 2 19 10800 0.0393 3539.83 44252 10260 11740 0.00004 4 124355 63.3 133 119 146 3.93 74.8 37 2 20 14400 0.0536 6437.146 21638 5233 0.00104 159885_ 45.0 132 _ 53.2 119 145 5.36 75.8 2.88 59.4 39 2 21 13900 0.0536 6213.634 22569 5082 0.00005 177650 45.3 132 50.1 120 143 5.36 74.5 2.94 59.3 39 2 22 16100 0.0536 7197.086 11520 0.00003 31 177650 39.1 131 _ 50.3 121 142 5.36 74.8 3 59.6 38- 2 23 17100 0.0566 8071.952 10320 0.00003 3 159885 37.9 130 _ 119 140 5.66 73.7 36 2 24 14000 0.0515. 6013.14 6220 0.00002 1 _ 115473 49.5_ 129_ 117 140 5.15 73.6 _ 38 2 25 16600 0.0536 7420.598 0.00003 124355 41.2 130 119 141 5.36 76.6 36 2 26 15300 0.0513 6545.983 38338 9272 0.00002 71060 48.2 130 53.2 118 142 5.13 76.1 2.98 59.7 36 2 27 17000 0.0498. 7060.644 0.00003 146561 38.9 130 117 142 4.98 74.3 37 2 28 12700 0.0522 5528.92 0.00003 115473 54.5 130 117 143 5.22 75.4 37 2 29 11300. 0.0494 4655.555 7180 0.00002 1 97708 62.8 130_ 117 143 4.94 76 _ 40 2 30 16600 0.0524- 7254.466 39872 7815 11620 0.00004 4 133238 40.6 130 48.5 116 144 5.24 74.2 2.93 59.7 39 2 TOT 473800 1.5292 201283 439475 102700 189760 0.267 16331 4169446 1298.313 3958 550.1 3596 4320 153 2246 33 655 1139 60 AVG 15793.33 0.051' 6709 39952.3 9336.39 9488' 0.009, 817 138982 43.27711 131.9 50.00909 120 144 5 74.9 3 59.5 38 2 NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL004982 k5i I14'4+;4 Client: Carl Sardi Advisor: Brent Collins . 9;a Predictive 6741 Monnett Rd EMA Resources Inc °± f Climax, NC 27233 755 Yadkinville Rd t �- Soi I Report Mehlich-3 Extraction Mocksville, NC 27028 ‹.#'%- .`/ Sampled County : Guilford v,t'r+_ Links to Helpful Information Client ID: 419418 Advisor ID: 405413 Sampled: Received: 09/21/2021 Completed: 09/29/2021 Farm: GUIS Sample ID: 00001 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 100 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.46 1.09 10.1 86 1.4 6.0 364 22 72 13 63 384 247 766 766 454 0.1 1 North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. A.: Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Trumk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL004984 k5i I14'4+;4 Client: Steve Fields Advisor: Brent Collins . 9;a Predictive 6741 Monnett Rd. EMA Resources Inc °± f Climax, NC 27233 755 Yadkinville Rd t . Soi I Report Mehlich-3 Extraction Mocksville, NC 27028 ‹#'%- .`/ Sampled County : Guilford v,t'r+_ Links to Helpful Information Client ID: 419419 Advisor ID: 405413 Sampled: Received: 09/21/2021 Completed: 09/29/2021 Farm: GU16 Sample ID: 00003 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.5 120-200 0 80 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.51 1.08 10.7 84 1.8 5.8 345 27 68 14 72 275 182 826 826 486 0.1 1 Sample ID: 00004 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.6 120-200 0 90 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.56 1.07 10.6 82 1.9 5.7 343 23 68 13 59 280 185 805 805 449 0.1 1 North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. A.: Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Trumk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL004983 k5i I14'4+;4 Client: Walter(Standish W) Hopkins Advisor: Brent Collins . 9;a Predictive 9543 NC Hwy 49 S EMA Resources Inc °± f Denton, NC 27239 755 Yadkinville Rd t . Soi I Report Mehlich-3 Extraction Mocksville, NC 27028 ‹#'%- .`/ Sampled County : Randolph v,t'r+_ Links to Helpful Information Client ID: 330393 Advisor ID: 405413 Sampled: Received: 09/21/2021 Completed: 09/29/2021 Farm: RD34 Sample ID: 00001 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.56 1.01 10.2 84 1.6 6.0 306 88 68 12 56 363 235 419 419 564 0.1 1 North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. A.: Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Totbari Truk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL004981 k5i I14'4+;4 Client: Kimball Markham Advisor: Brent Collins . 9;a Predictive 4794 Valley Farm Rd EMA Resources Inc °± f Denton, NC 27239 755 Yadkinville Rd t . Soi I Report Mehlich-3 Extraction Mocksville, NC 27028 ‹#'%- .`/ Sampled County : Randolph v,t'r+_ Links to Helpful Information Client ID: 460568 Advisor ID: 405413 Sampled: Received: 09/21/2021 Completed: 09/29/2021 Farm: RD42 Sample ID: 00001 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.36 0.99 9.2 82 1.6 5.9 249 70 66 13 51 335 218 356 356 461 0.1 1 Sample ID: 00002 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.41 0.93 9.1 82 1.6 5.9 245 72 67 11 49 300 197 313 313 475 0.1 1 North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. A.: Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Trumk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL004981 Kimball Markham Page 2 of 3 Sample ID: 00003 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.3 120-200 0 20 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.56 0.91 10.3 83 1.8 5.9 274 68 68 12 54 384 247 426 426 510 0.0 NCDA&CS Agronomic Division Phone: (919)733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL011173 k5i I14'4+;4 Client: Earl York Advisor: Brent Collins . 9;a Predictive 3119 Ramseur Julian Rd EMA Resources Inc °± f Liberty, NC 27298 755 Yadkinville Rd t . Soi I Report Mehlich-3 Extraction Mocksville, NC 27028 ‹#'%- .`/ Sampled County : Randolph v,t'r+_ Links to Helpful Information Client ID: 452781 Advisor ID: 405413 Sampled: Received: 10/25/2021 Completed: 11/08/2021 Farm: RD101 Sample ID: 00002 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 0.0 80-100 0 50 0 0 0 0 0 0 Note: 3 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.27 1.01 7.2 86 1.0 6.2 63 46 66 17 27 914 556 324 324 144 0.0 Sample ID: 00003 Recommendations: Lime Nutrients(lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 0.0 80-100 0 50 0 20 0 0 0 0 Note: 3 2- 0.0 Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N 0.27 1.06 8.6 88 1.0 6.3 69 46 59 26 25 516 315 320 320 155 0.1 1 North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. A.: Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Toibacco Truk fund Coininlbskm Asheboro Signature Pages Final Audit Report 2022-01-26 Created: 2022-01-26 By: Brent Collins(brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAAysG5TQUgCT-pogk0w28phygi5ppPYFpa "Asheboro Signature Pages" History e Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2022-01-26-5:51:17 PM GMT-IP address:24.88.129.34 Py Document emailed to Michael R. Wiseman (mwiseman@ci.asheboro.nc.us) for signature 2022-01-26-5:58:00 PM GMT Email viewed by Michael R. Wiseman (mwiseman@ci.asheboro.nc.us) 2022-01-26-5:58:49 PM GMT-IP address:71.2.234.82 Document e-signed by Michael R. Wiseman (mwiseman@ci.asheboro.nc.us) Signature Date:2022-01-26-6:06:11 PM GMT-Time Source:server-IP address:71.2.234.82 Agreement completed. 2022-01-26-6:06:11 PM GMT Eal Adobe Sign