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Home My WebLink AboutWQ0036561_Residual Annual Report 2021_20220228Initial Review Reviewer EADS\ndthornburg Is this submittal an application? (Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number (IR) * WQ0036561 ApplicantlPermittee City of Danville Email Notifications Does this need review by the hydrogeologist?* Yes No Regional Office CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 336-399-3646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Perm it Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number: * WQ0036561 Has Current Existing permit number Applicant/Permittee Address* 279 Park Avenue, Danville, VA 24541 Facility Name* City of Danville Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2021 Danville Annual Report - WO0036561.pdf 16.62MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/28/2022 MA --Resources, Inc. February 28, 2022 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2021 Annual Report — City of Danville, VA Treatment and Land Application of Residuals Permit No. WQ0036561 Dear Sir or Madam: Enclosed is one copy of the 2021 Annual Report for the above referenced land application permit During 2021 EMA Resources, Inc. land applied 489.35 dry tons of wastewater residuals to 226.05 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Brent Collins Director of Technical Services brent.collins@emaresourcesinc.com Phone 336.751.1441 — Fax 336.751.1442 755 Yadkinville Rd — Mocksville, NC 27028 ---Resources, Inc. City of Danville 2021 Annual Report Residuals Land Application Permit No. WQ0036561 Prepared By: EMA Resources, Inc. Phone 336.751.1441 — Fax 336.751.1442 755 Yadkinville Rd — Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0036561 County: Facility Name (as shown on permit): Land Application Operator: Pittsylvania County, VA Year: 2021 City of Danville, Northside WWTP EMA Resources Inc. Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 33 Total number of fields utilized for land application during the year: 8 Total amount of dry tons applied during the year for all application sites: 489.35 Total number of acres utilizes for land application during the year: 226.05 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. In Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Alan Johnson - Division Director of -Water & Wastewater Treatment Permittee Name and Title (type or print) GG`qgo`ry,nd 6�4y/grnEST) Feb 9, 2022 Ethatd 77h1zr5 vi Richard Alan Johnson (Feb 11, 2022 09:23 EST) Feb 11, 2022 Signature of Permittee Date 2/6/2022 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) Pages from Signed Final Audit Report 2022-02-11 Created: 2022-02-11 By: Brent Collins (brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAAbe1 pfEOTHMJMIdfOVF2OcMD40hc039KK "Pages from Signed" History Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2022-02-11 - 2:10:06 PM GMT- IP address: 206.85.202.26 Document emailed to Richard Alan Johnson (johnsra@danvilleva.gov) for signature 2022-02-11 - 2:10:42 PM GMT Email viewed by Richard Alan Johnson (johnsra@danvilleva.gov) 2022-02-11 - 2:21:25 PM GMT- IP address: 216.146.48.10 Document e-signed by Richard Alan Johnson (johnsra@danvilleva.gov) Signature Date: 2022-02-11 - 2:23:36 PM GMT - Time Source: server- IP address: 216.146.48.10 Agreement completed. 2022-02-11 - 2:23:36 PM GMT Ea Adobe Sign ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data WQ0036561 City of Danville VA0060593 Northside WWTP Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Conc. Limit (mg/kg)a Sample or Composite Date 4/13/21 4/27/21 5/10/21 5/24/21 Average Percent Solids (%) NA 4.25 3.8 3.49 4.59 4.03 Arsenic 75 37 13.2 14.3 10.9 18.85 Cadmium 85 11.6 2.63 2.86 2.17 4.82 Copper 4,300 440 382 284 424 382.50 Chromium NA 55.1 41.3 32.3 42.8 42.88 Lead 840 70.9 42.4 31.7 49.8 48.70 Mercury 57 3.58 0.876 0.917 0.307 1.42 Molybdenum 75 29.1 10.1 7.14 10.3 14.16 Nickel 420 61.9 53.9 39.4 60.2 53.85 Selenium 100 58.1 13.2 14.3 10.9 24.13 Zinc 7,500 2170 2080 1630 2390 2067.5 Total Phosphorus NA 22200 18200 14400 20600 18850 TKN NA 38100 54200 68600 45000 51475 Ammonia -Nitrogen NA 9020 11300 11000 9740 10265 Nitrate and Nitrite NA 153 713 294 107 316.75 a For surface disposal facilities the ceiling concentration limits listed in this fo u are not applicable. Reference the individual peunit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 6t Pohl Xii d Feb 9, 2022 Gregory A. Rj and (Feb 9, 022 13:55 EST) Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name: Residual Source NPDES # or WQ#: WWTP Name: WQ0036561 Laboratory: 1) Waypoint Analytical City of Danville VA0060593 Northside WWTP Residual Analysis Data 2) 3) 4) 5) Parameter (mg/kg) Sample or Composite Date 4/13/21 4/27/21 5/10/21 5/24/21 Average Aluminum 32600 28200 24700 30900 29100 Calcium 14600 12500 10000 13700 12700 Magnesium 3770 3080 2570 3410 3207.5 pH 7.4 7.1 7.3 7 7.2 Potassium 3210 3160 3140 3090 3150 Sodium 8600 8610 9630 7500 8585 PAN 13387 19233 23074 15555 17812 SAR 3.37 3.48 4.14 3.17 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Gregory / ,4 ify/�W i' Signature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Feb 9, 2022 Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): 89.57 Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series: RnB Acres Used: 65 Acres Permitted: 65 Site #: CS09 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 14 15 16 17 18 19 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L L 3 Li L L 6 t L L 10 11 12 Totals: 1.38 Arsenic 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 1.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.054 Chromium 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Lead 0.134 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.134 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb denum 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 Nickel 0.148 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.148 Selenium 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Zinc 5.698 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.698 Total Phos- phorus 51.951 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 51.951 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 3 Land Owner: Glenn Hodges Annual Dry Tons Applied: 89.57 Operator: Glenn Hodges Crop 1 Name: Fescue -Pasture Predominant Soil Series: RnB Site #: CS09 Crop 1 Max. PAN: 125 Crop 2 Name: Acres Utilized: 65 Acres Permitted: 65 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper PP Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/11 234000 4.03 0.605 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 21.552 NA Fescue 8/12 156000 4.03 0.403 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 14.368 NA Fescue 8/13 143000 4.03 0.370 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 13.171 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 533000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 49.091 0.000 Lime Applied Annual lbs/acre 0.052 0.013 1.054 0.118 0.134 0.004 0.039 0.148 0.067 5.698 51.951 Date lbs/ac Prior Years Cumulative lbs/ac 0.166 0.045 8.152 1.307 1.077 0.024 0.244 1.356 0.128 41.397 Current Cumulative lbs/ac 0.218 0.058 9.206 1.425 1.211 0.028 0.283 1.504 0.195 47.095 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 125 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 21.84 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Marc Thomas Owner: Marc Thomas Predominant Soil Series: CfB Acres Used: 9.8 Acres Permitted: 9.8 Site #: CS10 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 1 4 1 5 1 6 1 7 1 8 1 9 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L 3 Li L L 6 t L L 10 11 12 Totals: 2.23 Arsenic 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 1.705 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.705 Chromium 0.191 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.191 Lead 0.217 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.217 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb denum 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Nickel 0.240 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.240 Selenium 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Zinc 9.217 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.217 Total Phos- phorus 84.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 84.033 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 1 Land Owner: Marc Thomas Annual Dry Tons Applied: 21.84 Operator: Marc Thomas Crop 1 Name: Fescue -Hay Predominant Soil Series: CfB Site #: CS10 Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: 9.8 Acres Permitted: 9.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper pp Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/20 65000 4.03 1.115 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 39.708 NA Fescue 8/21 65000 4.03 1.115 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 39.708 39.708 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 130000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 79.416 39.708 Lime Applied Annual lbs/acre 0.084 0.021 1.705 0.191 0.217 0.006 0.063 0.240 0.108 9.217 84.033 Date lbs/ac Prior Years Cumulative lbs/ac 0.347 0.095 17.974 3.811 2.412 0.048 0.521 2.535 0.238 59.183 Current Cumulative lbs/ac 0.431 0.116 19.679 4.002 2.629 0.054 0.584 2.775 0.346 68.400 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): 83.01 Marc Thomas Owner: Marc Thomas Predominant Soil Series: Clifford 38.5 Acres Permitted: 38.5 Site #: CS10 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 14 15 16 17 18 19 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L 3 Li L L 6 t L L 10 11 12 Totals: 2.16 Arsenic 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 1.649 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.649 Chromium 0.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.185 Lead 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb denum 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.061 Nickel 0.232 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.232 Selenium 0.104 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Zinc 8.915 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.915 Total Phos- phorus 81.281 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 81.281 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 5 Land Owner: Marc Thomas Annual Dry Tons Applied: 83.01 Operator: Marc Thomas Crop 1 Name: Fescue -Pasture Predominant Soil Series: Clifford Site #: CS10 Crop 1 Max. PAN: 162 Crop 2 Name: Acres Utilized: 38.5 Acres Permitted: 38.5 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper pp Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/21 91000 4.03 0.397 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 14.150 NA Fescue 8/23 169000 4.03 0.738 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 26.279 NA Fescue 8/24 234000 4.03 1.021 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 36.387 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 494000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 76.817 0.000 Lime Applied Annual lbs/acre 0.081 0.021 1.649 0.185 0.210 0.006 0.061 0.232 0.104 8.915 81.281 Date lbs/ac Prior Years Cumulative lbs/ac 0.328 0.095 18.867 3.829 2.516 0.049 0.495 2.655 0.25 60.808 Current Cumulative lbs/ac 0.409 0.116 20.516 4.014 2.726 0.055 0.556 2.887 0.354 69.723 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 159.48 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: ToB Acres Used: 51 Acres Permitted: 61.4 Site #: CS14 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 1 4 1 5 1 6 1 7 1 8 1 9 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L 3 Li L L 6 t L L 10 11 12 Totals: 3.13 Arsenic 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Cadmium 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030 Copper 2.392 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.392 Chromium 0.268 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.268 Lead 0.305 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb denum 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Nickel 0.337 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.337 Selenium 0.151 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.151 Zinc 12.930 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.930 Total Phos- phorus 117.888 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 117.888 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 1 Land Owner: David Sartin Operator: David Sartin Crop 1 Name: Bermuda -Pasture Annual Dry Tons Applied: 159.48 Predominant Soil Series: ToB Site #: CS14 Crop 1 Max. PAN: 162 Crop 2 Name: Acres Utilized: 51 Acres Permitted: 61.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper PP Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/3 162500 4.03 0.535 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 19.075 NA Fescue 8/4 84500 4.03 0.278 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 9.919 NA Fescue 8/5 97500 4.03 0.321 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 11.445 NA Fescue 8/6 188500 4.03 0.621 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 22.127 NA Fescue 8/9 195000 4.03 0.643 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 22.890 NA Fescue 8/10 221000 4.03 0.728 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 25.943 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 949000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 111.400 0.000 Lime Applied Annual lbs/acre 0.118 0.030 2.392 0.268 0.305 0.009 0.089 0.337 0.151 12.930 117.888 Date lbs/ac Prior Years Cumulative lbs/ac 0.312 0.066 13.408 2.332 1.997 0.039 0.376 2.079 0.173 52.412 Current Cumulative lbs/ac 0.430 0.096 15.800 2.600 2.302 0.048 0.465 2.416 0.324 65.342 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville Total Dry Tons Applied (Annual): WQ0036561 Cation Exchange Capacity (non 503 only): 39.33 David Sartin Owner: David Sartin Predominant Soil Series: Toast 18.25 Acres Permitted: 24.3 Site #: CS14 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 1 4 1 5 1 6 1 7 1 8 1 9 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L 3 Li L L 6 t L L 10 11 12 Totals: 2.16 Arsenic 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 1.649 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.649 Chromium 0.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.185 Lead 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb denum 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.061 Nickel 0.232 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.232 Selenium 0.104 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Zinc 8.911 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.911 Total Phos- phorus 81.244 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 81.244 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Danville WQ Permit #: WQ0036561 Field #: 2 Land Owner: David Sartin Operator: David Sartin Crop 1 Name: Fescue -Pasture Annual Dry Tons Applied: 39.33 Predominant Soil Series: Toast Site #: CS14 Crop 1 Max. PAN: 96 Crop 2 Name: Acres Utilized: 18.25 Acres Permitted: 24.3 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper pp Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/3 91000 4.03 0.838 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 29.852 NA Fescue 8/4 84500 4.03 0.778 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 27.719 NA Fescue 8/5 58500 4.03 0.539 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 19.190 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 234000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 76.761 0.000 Lime Applied Annual lbs/acre 0.081 0.021 1.649 0.185 0.210 0.006 0.061 0.232 0.104 8.911 81.244 Date lbs/ac Prior Years Cumulative lbs/ac 0.164 0.035 5.875 1.006 0.778 0.019 0.182 0.895 0.065 26.315 Current Cumulative lbs/ac 0.245 0.056 7.524 1.191 0.988 0.025 0.243 1.127 0.169 35.226 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 96 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Danville WQ0036561 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): 18.57 David Sartin Owner: David Sartin Predominant Soil Series: CmB 5 Acres Permitted: 5 Site #: CS14 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 14 15 16 17 18 19 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L L 3 Li L L 6 t L L 10 11 12 Totals: 3.71 Arsenic 0.140 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.140 Cadmium 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Copper 2.841 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.841 Chromium 0.319 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.319 Lead 0.362 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.362 Mercury 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Molyb denum 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.105 Nickel 0.400 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.400 Selenium 0.179 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.179 Zinc 15.357 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.357 Total Phos- phorus 140.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 140.018 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0036561 Field #: 3 Site #: CS14 City of Danville David Sartin David Sartin Crop 1 Name: Fescue -Hay Annual Dry Tons Applied: 18.57 Predominant Soil Series: CmB Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 5 5 0 Date or Month Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper PP Acre (Dry Tons/Ac) Residual (NPDES Pert , Waste, Sources #, WQ#, Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* 110pUZMIVIOA Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application etc) Crop 1 Crop 2 Crop 1 Crop 2 8/2 110500 4.03 3.714 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 132.307 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 110500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 132.307 0.000 Lime Applied Annual lbs/acre 0.140 0.036 2.841 0.319 0.362 0.011 0.105 0.400 0.179 15.357 140.018 Date lbs/ac Prior Years Cumulative lbs/ac 0.044 0.016 2.766 0.372 0.364 0.007 0.083 0.45 0.031 14.279 Current Cumulative lbs/ac 0.184 0.052 5.607 0.691 0.726 0.018 0.188 0.850 0.210 29.636 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Danville WQ0036561 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): 29.50 Operator: James Poindexter Owner: James Poindexter Predominant Soil Series: HaB Acres Used: 17 Acres Permitted: 17 Site #: PS02 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 1 4 1 5 1 6 1 7 1 8 1 9 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L 3 Li L L 6 t L L 10 11 12 Totals: 1.74 Arsenic 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Cadmium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Copper 1.327 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.327 Chromium 0.149 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.149 Lead 0.169 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.169 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb denum 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Nickel 0.187 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.187 Selenium 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Zinc 7.174 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.174 Total Phos- phorus 65.410 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 65.410 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) Facility Name: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0036561 Field #: 2 City of Danville Land Owner: James Poindexter Operator: James Poindexter Crop 1 Name: Fescue -Hay Annual Dry Tons Applied: 29.50 Predominant Soil Series: HaB Site #: PS02 Crop 1 Max. PAN: 158 Crop 2 Name: Acres Utilized: 17 Acres Permitted: 17 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: Date or Month Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper PP Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#, Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* 110pUZMIVIOA Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application etc) Crop 1 Crop 2 Crop 1 Crop 2 8/25 175500 4.03 1.735 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 61.804 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 175500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 61.804 0.000 Lime Applied Annual lbs/acre 0.065 0.017 1.327 0.149 0.169 0.005 0.049 0.187 0.084 7.174 65.410 Date lbs/ac Prior Years Cumulative lbs/ac 0.049 0.015 3.001 0.483 0.344 0.007 0.106 0.487 0.034 14.495 Current Cumulative lbs/ac 0.114 0.032 4.328 0.632 0.513 0.012 0.155 0.674 0.118 21.669 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 158 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Danville WQ0036561 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): 48.05 Operator: James Poindexter Owner: James Poindexter Predominant Soil Series: FaB3 Acres Used: 21.5 Acres Permitted: 21.5 Site #: PS02 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Avg. 2 1 3 14 15 16 17 18 19 110 111 112 % Solids 4.03 Arsenic 18.85 Cadmium 4.82 Copper 382.5 Chromiumr 42.88 Lead 48.7 Mercury 1.42 Molyb- denum 14.16 Nickel 53.85 Selenium 24.13 Zinc 2067.5 Total Phos- phorus 18850 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event L L L 3 Li L L 6 t L L 10 11 12 Totals: 2.24 Arsenic 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Cadmium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Copper 1.710 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.710 Chromium 0.192 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.192 Lead 0.218 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.218 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb denum 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Nickel 0.241 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.241 Selenium 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Zinc 9.242 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.242 Total Phos- phorus 84.260 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 84.260 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2/6/2022 Date DENR FORM MFLSF (12/2006) Facility Name: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0036561 Field #: 3 City of Danville Land Owner: James Poindexter Operator: James Poindexter Crop 1 Name: Fescue -Pasture Annual Dry Tons Applied: 48.05 Predominant Soil Series: FaB3 Site #: PS02 Crop 1 Max. PAN: 145 Crop 2 Name: Acres Utilized: 21.5 Acres Permitted: 21.5 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: Date or Month Volume (enter one) Liquid 9 Cu. Yds applied Solids/ Gallons % Solids Volume Appliedper pp Acre (Dry Tons/Ac) Residual (NPDES Fert , Waste, Sources #, WQ#,7j Animal Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Application Method* o w w . N' 1,?-,' Mineralizatio n Rate* * * TKN mg/kg Ammonia Y rn Nitrogen E Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP etc) Crop 1 Crop 2 Crop 1 Crop 2 8/26 188500 4.03 1.473 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 52.488 NA Fescue 8/27 97500 4.03 0.762 Northside WWTP Dry <.5" S 0.5 0.3 51475 10265 316.75 27.149 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 286000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 79.637 0.000 Lime Applied Annual lbs/acre 0.084 0.022 1.710 0.192 0.218 0.006 0.063 0.241 0.108 9.242 84.260 Date lbs/ac Prior Years Cumulative lbs/ac 0.649 0.18 108.999 5.734 4.093 0.077 0.746 3.314 0.254 98.652 Current Cumulative lbs/ac 0.733 0.202 110.709 5.926 4.311 0.083 0.809 3.555 0.362 107.894 Permitted C. P. L. R. * * * * 36 34 1338 267 15 374 89 2498 Permit PAN Limit 1 st/2nd Crop 145 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/6/2022 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Waypoint ANALYTICAL 5/5/2021 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 21-106-0004 Project Description: VPDES Permit#VA0060593 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.tom Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/16/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, frl c &foc r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypoint, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Sample Summary Table Report Number: 21-106-0004 Client Project Description: VPDES Permit#VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SM-2320 B WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 6010D WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SM-4500-NH3C WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SM-4500-NH3C-TKN WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 4500NO3F-2011 WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SM-2540G WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SW-7.3.3 WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SW-7.3.4 WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 SW-7471B WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 9045D WP MTN 75910 LTS A -BASIN 21-1250 Solids 04/13/2021 07:50 04/16/2021 ASTM D93-80 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0004 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit#VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/10/2021 Received : 04/16/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75910 Matrix: Solids Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 4.25 % 0.010 1 04/19/21 16:15 FMM SM-2540G Total Kjeldahl Nitrogen 38100 mg/Kg - dry 5810 1 04/23/21 11:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 22200 mg/Kg - dry 116 1 04/28/21 18:12 JTR 6010D Potassium 3210 mg/Kg - dry 233 1 05/04/21 19:48 JADS 6010D Sulfur 13000 mg/Kg - dry 233 1 04/28/21 18:12 JTR 6010D Calcium 14600 mg/Kg - dry 1160 1 04/28/21 18:12 JTR 6010D Magnesium 3770 mg/Kg - dry 116 1 04/28/21 18:12 JTR 6010D Sodium 8600 mg/Kg - dry 581 1 04/28/21 18:12 JTR 6010D Iron 34700 mg/Kg - dry 233 1 04/28/21 18:12 JTR 6010D Manganese 1040 mg/Kg - dry 11.6 1 04/28/21 18:12 JTR 6010D Copper 440 mg/Kg - dry 11.6 1 04/28/21 18:12 JTR 6010D Zinc 2170 mg/Kg - dry 29.1 1 04/28/21 18:12 JTR 6010D Organic N 29100 mg/Kg - dry 5810 1 04/23/21 11:00 DH CALCULATION Nitrate+Nitrite-N 153 mg/Kg - dry 113 1 04/21/21 14:54 ZBD 4500NO3F-2011 Nickel 61.9 mg/Kg - dry 5.81 1 04/28/21 18:12 JTR 6010D Mercury 3.58 mg/Kg - dry 0.347 1 04/26/21 13:52 DDB SW-7471B Selenium <58.1 mg/Kg - dry 58.1 5 04/29/21 18:24 JTR 6010D pH 7.4 s.u. 1 04/28/21 16:03 CxC 9045D Total Volatile Solids 48.1 % 0.010 1 04/19/21 16:15 FMM SM-2540G Qualifiers/ Definitions * Outside QC Limit B Analyte detected in blank C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 8 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0004 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit#VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/10/2021 Received : 04/16/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75910 Matrix: Solids Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Flashpoint >96 degrees C 1 04/28/21 00:30 CJR ASTM D93-80 Sulfide (Reactivity) <581 mg/Kg - dry 581 1 04/22/21 12:25 FMM SW-7.3.4 Alkalinity (as CaCO3) 38400 mg/Kg - dry 2330 1 04/19/21 16:00 CXB SM-2320 B Ammonia Nitrogen 9020 mg/Kg - dry 2330 1 04/28/21 16:00 JPJ SM-4500-NH3C Cyanide (Reactivity) <2.91 mg/Kg - dry 2.91 1 04/22/21 12:25 FMM SW-7.3.3 Aluminum 32600 mg/Kg - dry 116 1 04/28/21 18:12 JTR 6010D Arsenic 37.0 mg/Kg - dry 11.6 1 04/28/21 18:12 JTR 6010D Cadmium <11.6 mg/Kg - dry 11.6 5 04/29/21 18:24 JTR 6010D Chromium 55.1 mg/Kg - dry 5.81 1 04/28/21 18:12 JTR 6010D Lead 70.9 mg/Kg - dry 6.98 1 04/28/21 18:12 JTR 6010D Molybdenum <29.1 mg/Kg - dry 29.1 5 04/29/21 18:24 JTR 6010D Analytical Method: SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Batch Moisture 95.7 010 0.010 1 04/19/21 16:15 FMM L548033 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 4 of 8 Waypol nt.M ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalyt-ical.com Client: Inframark Project: VPDES Permit#VA0060593 Lab Report Number: 21-106-0004 Date: 5/5/2021 CASE NARRATIVE Metals Analysis Method 6010D Sample 76040 Analyte: Aluminum QC Batch No: L550919 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L551020 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 8 Waypoint.. ANALYTICAL Customer Number: 79434 Customer Name: Inframark Report Number: 21-106-0004 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytica I.com Shipment Receipt Form Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? () Yes Custody seals intact on sample bottles? 0 Yes O No O No ® Not Present ® Not Present Chain of Custody (COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes 0 No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes O No Water - Sample containers properly preserved Water - VOA vials free of headspace O Yes O Yes O No O No ® N/A ® N/A Trip Blanks received with VOAs 0 Yes O No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes O No ® N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: ® No Signature: Brandi Watson Date & Time: Page 6 of 8 04/16/2021 12:26:20 Client Name/Address Inframark - Danville W VTP 229 Northside Dr Danville, VA 24540 Cl,ent Project Manager/Contact Robert Clifton - Lab Mgr Kim Wickemeyer - Sr. Lab Tech. Billing Information Inframark 229 Northside Dr. Danville. VA 24540 For Laboratory Use Qniy Project Description VPDES Permit #: VA0060593[i511 Project/Site location (City/State} Danville, VA Wastewater Treatment Plant RUSH - Additiona. char e+ Sr Detection ter, ri. Ik Date sulis Ne _ de:: Sf2Ct21 Method of Shipment I 1 F t'd Ea I1 Courie j�j l -J- 1 lit ne r ❑>✓ 1 UPS Dust's Client Drop OH Matrix Key WW - Wastewater OW -Groundwater OW - Drinking Water S - Soil /Solid 0 - Oil P - product M Misc Project Number Waypolnt Acct. 79434 Project Manager Phone It 434-799-5137 Project Manager Email robert.clifton@inframark.com Purchase 119377 Order Number Site/Facility ID a VPDES #: VA0060593 ` � ■V,��,►�•�L �y/ i : ■ ■aypoin Number of Containers Y u - _ _ � _ d Cool c irK Na75203 (Mitre Only) ® Cool c= 6C C H25Uspiic2 ED Wane pH, e E NabHpHaLi# f Ht O3 pH,2 Ha 014.2 H H3PO4 pi1e2 r Coal c,..bC NAM° I ,... .. ° _ E' u /// ( [ -.., l7 .- _ _ _ I. �.. •:. • ui. 9 jrrtti ie2t nrr Required An-ay,is i/ Preservative Comments/Notes LTS A -Basin 21-1250A 1 s C 1✓ _ 0.5 L plastic: preservative = B ~• • , r LTS A -Basin 21-12 50 B 1 S c 1/ 1 L aril her glass, preservative = B LTS A -Basin 21-1250C 1 S c ✓ say- • 1 L amber glass. preservative = By -- - - I l a• r p -/-r ,r r)., INN IIINIIIIIPIIIIIIIIIIIIfIII1INIIIIIIIII WA Cornp©s / k- Intramark 047942 s° 21 1225:24 a 1 0 70 C2 - Q 750 on VPDES FrermOVA0060593 au- p Let -..-rim For Laboratory Use Only Sampled by (Name - Print) Client Remarks/Comments All Analyses must be performed by a certified lab', ice Custody Seals Lab Comments Robert Clifton Robert L I l l L 1 ON Reii ed b (SIG Ill Date Time y/r/3/0 0y30 Received by: (SIGNATURE) Date Time Blank ,,,,,,...o''ery1 Temp Q° Relinquisher% by: (SIGN ATUR Date Time Received y: ( TURE) 1Rel+nquished Date Time by: (SIGNATURE) Date Time Rece (SIGN. t1RE) { CL).1 a Ti r DP .50 Required Biosolids Tests for Inframark Danville, VA WWTP (Waypoint VA Account 79434) Sample: LTS A Basin 21 - I a,o PO: 1 \C' T1 J%TS ,,%%TVS / pH %Alkalinity -"TKN ✓Ammonia -Nitrogen I Nitrate + Nitrite as Nitrogen 'Organic Nitrogen (calculation) /Phosphorus Potassium Sulfur /Calcium -"Magnesium /Sodium / Iron Aluminum /Manganese //Copper inc pyrnmenettova:4 VPDE5 Permit#VAppGp5g3 i2:25:24 Lab# E 75909-1 Cust: 79434 Inframark Col: 04/ 13/ 2021 07:50 Rec: 04 / 16 / 2021 00:00 21-106-0004 Preservation: 1-IN03,pH < 2 LTS A -BASIN 21-1250 ✓Cadmium Lab# E 75910-1 L75 A -BASIN 21-1250 Cust: 79434 Inframark Chromium Co!: 04Q 3/2021 07:50 Rec: 04/16/2021 o0zo0 Preservation: 6 degrees C Nickel ./Lead /Arsenic a 1# E 75910- Cust: 79434 Z Li5 A -BASIN 2I 1.2s0 �/(Nercury Inframark Col: 04/13/2021 07:50 Rec: 04/16/2021 00:00 21-106-0004 ^4eie ni um PreSerVdtlori: ✓ino€ybdenum Page 8 of 8 Sodium Calcium Magnesium Percent Solids 4/13/2021 mg/kg mg/L Equiv Weight Milli Equiv 8600 365.5 23 15.8913 14600 620.5 20 31.025 3770 160.225 12 13.35208 4.25 SAR= SAR 3.37 Na+ /2 (Ca2+ + Mg2+) Waypoint ANALYTICAL 5/11/2021 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.tom Ref: Analytical Testing Report Number: 21-123-0007 Project Description: Wastewater Treat Plant Danville VA Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/3/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, frl c &foc r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 10 Waypoint, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical, com Sample Summary Table Report Number: 21-123-0007 Client Project Description: Wastewater Treat Plant Danville VA Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 SM-2540G WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 SW-7471B WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 SM-4500-NH3C-TKN WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 4500NO3F-2011 WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 6010D WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 SM-4500-NH3C WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 9045D WP MTN 76145 LTS A BASIN 21-1280 Solids 04/27/2021 07:40 05/03/2021 SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 10 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-123-0007 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Wastewater Treat Plant Danville VA Information : REPORT OF ANALYSIS Report Date : 05/11/2021 Received : 05/03/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76145 Matrix: Solids Sample ID : LTS A BASIN 21-1280 Sampled: 4/27/2021 7:40 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 3.80 % 0.010 1 05/04/21 16:30 FMM SM-2540G Total Kjeldahl Nitrogen 54200 mg/Kg - dry 6580 1 05/10/21 09:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 18200 mg/Kg - dry 132 1 05/06/21 20:29 TJS 6010D Potassium 3160 mg/Kg - dry 263 1 05/06/21 20:29 TJS 6010D Sulfur 11600 mg/Kg - dry 263 1 05/06/21 20:29 TJS 6010D Calcium 12500 mg/Kg - dry 1320 1 05/06/21 20:29 TJS 6010D Magnesium 3080 mg/Kg - dry 132 1 05/06/21 20:29 TJS 6010D Sodium 8610 mg/Kg - dry 658 1 05/06/21 20:29 TJS 6010D Iron 28900 mg/Kg - dry 263 1 05/06/21 20:29 TJS 6010D Manganese 921 mg/Kg - dry 13.2 1 05/06/21 20:29 TJS 6010D Copper 382 mg/Kg - dry 13.2 1 05/06/21 20:29 TJS 6010D Zinc 2080 mg/Kg - dry 32.9 1 05/06/21 20:29 TJS 6010D Organic N 42900 mg/Kg - dry 6580 1 05/10/21 09:00 CALCULATION Nitrate+Nitrite-N 713 mg/Kg - dry 126 1 05/05/21 13:34 ZBD 4500NO3F-2011 Nickel 53.9 mg/Kg - dry 6.58 1 05/06/21 20:29 TJS 6010D Mercury 0.876 mg/Kg - dry 0.363 1 05/06/21 13:30 DDB SW-7471B Selenium <13.2 mg/Kg - dry 13.2 1 05/06/21 20:29 TJS 6010D pH 7.1 s.u. 1 05/08/21 15:30 CxC 9045D Total Volatile Solids 50.6 % 0.010 1 05/04/21 16:30 FMM SM-2540G Qualifiers/ Definitions * Outside QC Limit B Analyte detected in blank C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 10 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-123-0007 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Wastewater Treat Plant Danville VA Information : REPORT OF ANALYSIS Report Date : 05/11/2021 Received : 05/03/2021 awi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76145 Matrix: Solids Sample ID : LTS A BASIN 21-1280 Sampled: 4/27/2021 7:40 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 19300 mg/Kg - dry 2630 1 05/10/21 09:00 JAE SM-2320 B Ammonia Nitrogen 11300 mg/Kg - dry 2630 1 05/10/21 09:00 JPJ SM-4500-NH3C Aluminum 28200 mg/Kg - dry 132 1 05/06/21 20:29 TJS 6010D Arsenic <13.2 mg/Kg - dry 13.2 1 05/06/21 20:29 TJS 6010D Cadmium <2.63 mg/Kg - dry 2.63 1 05/06/21 20:29 TJS 6010D Chromium 41.3 mg/Kg - dry 6.58 1 05/06/21 20:29 TJS 6010D Lead 42.4 mg/Kg - dry 7.89 1 05/06/21 20:29 TJS 6010D Molybdenum 10.1 mg/Kg - dry 6.58 1 05/06/21 20:29 TJS 6010D Analytical Method: SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Batch Moisture 96.2 010 0.010 1 05/04/21 16:30 FMM L551007 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 4 of 10 Waypol nt.M ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalyt-ical.com Client: Inframark Project: Wastewater Treat Plant Danville VA Lab Report Number: 21-123-0007 Date: 5/10/2021 CASE NARRATIVE Metals Analysis Method 6010D Sample 76145 (LTS A BASIN 21-1280) Analyte: Aluminum QC Batch No: L551658/L551346 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 10 Waypoint.. ANALYTICAL Customer Number: 79434 Customer Name: Inframark Report Number: 21-123-0007 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytica I.com Shipment Receipt Form Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? () Yes Custody seals intact on sample bottles? 0 Yes O No O No ® Not Present ® Not Present Chain of Custody (COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes 0 No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes O No Water - Sample containers properly preserved Water - VOA vials free of headspace O Yes O Yes O No O No ® N/A ® N/A Trip Blanks received with VOAs 0 Yes O No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes O No ® N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: ® No Signature: Brandi Watson Date & Time: Page 6 of 10 05/03/2021 14:47:31 Client Name/Address Inframark - Danville WWTP 229 Northside Dr. Danville, VA 24540 Client Project Manager/Contact Robert Clifton - Lab Mgr. Kim Wickemeyer - Sr. Lab Tech. Billing Information Inframark 229 Northside Dr. Danville,, VA 24540 ill l Inframark Waslewwater 13 1Ir11i Treat I0III Plant Danville +1lI 1Ill VA II ! III II IIII H 1 Illl055-03_2021 794 23-7 14 4508 Project Description VPDES Permit #: VA0060593 Project/Site Location {City/State} Danville, VA Wastewater Treatment Plant — 05/15/2021 RUSH - Additional charges apply Special Detection Limitls} Date Results Needed �M--etIhod or Nr..yiv.s... l l red Ex ❑ Courier other ✓ "~ — UPS FIUSPS Client prop aft WW - Wastewater GW -Groundwater DIN - Drinking Water 5 - Soil /Solid Cl - ail Q . Product M -Misr ~Project Number Waypoint Acct. 79434 Project Manager Phone it 434-799-5137 Project Manager Email rotlert.ciifton©inframark.com Purchase 1 Order 20003 Number Site/racility ID* VPDES #: VA0060593 • W' " n - M■Q+ ANALYTICAL 2790 Whitten Road Memphis. TN 38133 N OI) 213 2400 Unless noted, all containers per Table II of 48CFR Part 136. Number of Containers Y cl i s m OG)rab or (C]ornposite a, �', N i % w 4 A Cool [ IOC Na25I03(Micro Onlyl d 6 Coc= 6C H25t34 pH@ U None Required r Na014 p14}10 HNO3 pHe2 C HCL pHc2 H H3 04 pHe2 Cool c= 6C NA2c703 Required Analysis / Preservative s Comments/Notes Date times Sample Identification _ 04f27'' ni4D LTS A -Basin 21-1280 1 S 0 1,/ 0.5 L plastic; preservative = B 1:1;-- HT Lab# E 76145-1 LTS A BASIN 21-1280— Cust: Cal: 04/27/2021 79434 Inframark 07:40 Rec: 05/03/2021 00:00 21-123-0007 Preservation: < = 6 degrees C For laboratory Use Only Sampled by {Name - Print} Robert Clifton Client Remarks/Comments All Analyses must be performed by a certified lab ice y l custody Seals Lab Comments ^o O4l� © DrJ --07 Pell quished by: (SI NAT € l Date Time Received by: i5IGNATURE) Date Time BIanli(oler Temp , Relinquished by: *NATURE) Date Time Received by: (SIGNATURE} Date Time `((�ITO C3 -C'd 9 - Relinquished by: {SIGNATURE} Date Time Received by: {SIGNATURE} Date Time Page 7 of 10 Required Biosolids Tests for Inframark Danville, VA 1NWTP (Waypoint VA Account 79434) Sample: LTS A Basin 21 - 0 pp; ) Dsoo. ./% TS %TVS pH Alkalinity ,rKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen Organic Nitrogen (calculation) Phosphorus -*Potassium -"Sulfur Xalcium "Magnesium -"Sodium ,,/(ron _Aluminum 6/Manganese `Copper -"Zinc Cadmium Chromium '-'fickel ►/Lead ./Arsenic ✓Mercury Selenium Molybdenum iNaz eiss ors Page 8 of 10 1NFRAMARK Vendor Waypoint Analytical Inc Phone. 901-327-2750 Contact Contact Email Bill To: 229 Northside Drive Danville Virginia 24540 United States Purchase Order PC : 120003 Date: 4/23/2021 Buyer Name: Anjelina Munoz Buyer Email: anielina.munozftinframark com End User Email; kimberiy.wickerneyeraa inframark.corn End User Phone: 434-799-5137 Payment Terms: Net 30 Ship To; 229 Northside Drive Danville Virginia 24540 United States Attn: Kimberly Wickemeyer Line Item ID Protect Qty Units Expected Detavery Date Rate SIR00012 DANVILLE t Ea 6/15/2021 $249 90 $249 90 Description: *g.. 503 E Heavy Metals Line !tern Project Qty Units Expected Delnisry Date Rate Amount ID 2 SIR00012 DANVILLE 1 Ea 6/15/2021 $21.0O $21 00 Description: Ammonia Nitrogen by distiilaiton Line Item JD Prclect Oty Units Expected Delivery Date Rate 3 SIR00012 DANVILLE 1 Ea 6/15/2021 $21 00 Description: Nlitrate+Nitrite as N • Page 9 of 10 INFRAMARK Vendor Waypoint Analytical Inc Phone: 901-327-2750 Contact. Contact Email Purchase Order PO#: 120003 Date: 4123/2021 Buyer Name: Anjelina Munoz Buyer Email: anjellna munoz@inframark cam End User Email: It berlywickArmgr a inframerk-com End User Phone: 434-799-5137 Payment Terms: Net 30 Total $422.10 All packing lists and proofs of delivery must be sent to receiving@inframark.com within 48 hours of delivery Please reference the PC number above on ail documentation. Inframark, LLC General Conditions of Purchase. a copy of which is available at https tiwww inframark corn/contact-us/doing-business- with-us/ . and any specific conditions or other terms not included in these General Conditions of Purchase that are mutually agreed upon in writing (herein after "Specific Conditions") shalt govern this Purchase Order in the event of a conflict between any Specific Conditions noted in the Purchase Order and the General Conditions of Purchase. the Specific Conditions shall control All terms and conditions included in any Supplier documentation are specifically rejected by Purchaser and shall be of no effect on this Purchase Order Please reference this Purchase Order number on all shipping and billing documents related to this order. VendorAcceptance Date • • • 3 of 3 Page 10 of 10 Sodium Calcium Magnesium Percent Solids 4/27/2021 mg/kg mg/L Equiv Weight Milli Equiv 8610 327.18 23 14.22522 12500 475 20 23.75 3080 117.04 12 9.753333 3.8 SAR= SAR 3.48 Na+ /2 (Ca2+ + Mg2+) Waypoint ANALYTICAL 5/18/2021 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.tom Ref: Analytical Testing Report Number: 21-131-0008 Project Description: Wastewater Treatment Plant -Danville VA VPDES PERMIT #VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/11/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, c 4lj I( Grow/ Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 11 Waypoint, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical, com Sample Summary Table Report Number: 21-131-0008 Client Project Description: Wastewater Treatment Plant -Danville VA VPDES PERMIT #VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 SM-2540G WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 SW-7471B WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 SM-4500-NH3C-TKN WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 4500NO3F-2011 WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 6010D WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 SM-4500-NH3C WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 9045D WP MTN 76292 LTS A -Basin 21-1322 Solids 05/10/2021 08:30 05/11/2021 SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 11 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-131-0008 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Wastewater Treatment Plant -Danville VA Information : VPDES PERMIT #VA0060593 REPORT OF ANALYSIS Report Date : 05/18/2021 Received : 05/11/2021 owi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76292 Matrix: Solids Sample ID : LTS A -Basin 21-1322 Sampled: 5/10/2021 8:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 3.49 % 0.010 1 05/13/21 16:07 FMM SM-2540G Total Kjeldahl Nitrogen 68600 mg/Kg - dry 7140 1 05/17/21 13:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 14400 mg/Kg - dry 143 1 05/13/21 00:31 JTR 6010D Potassium 3140 mg/Kg - dry 286 1 05/13/21 00:31 JTR 6010D Sulfur 8540 mg/Kg - dry 286 1 05/13/21 00:31 JTR 6010D Calcium 10000 mg/Kg - dry 1430 1 05/13/21 00:31 JTR 6010D Magnesium 2570 mg/Kg - dry 143 1 05/13/21 00:31 JTR 6010D Sodium 9630 mg/Kg - dry 714 1 05/13/21 00:31 JTR 6010D Iron 21000 mg/Kg - dry 286 1 05/13/21 00:31 JTR 6010D Manganese 720 mg/Kg - dry 14.3 1 05/13/21 00:31 JTR 6010D Copper 284 mg/Kg - dry 14.3 1 05/13/21 00:31 JTR 6010D Zinc 1630 mg/Kg - dry 35.7 1 05/13/21 00:31 JTR 6010D Organic N 57600 mg/Kg - dry 7143 1 05/17/21 13:00 CALCULATION Nitrate+Nitrite-N 294 mg/Kg - dry 139 1 05/17/21 14:46 ZBD 4500NO3F-2011 Nickel 39.4 mg/Kg - dry 7.14 1 05/13/21 00:31 JTR 6010D Mercury 0.917 mg/Kg - dry 0.437 1 05/13/21 11:21 DDB SW-7471B Selenium <14.3 mg/Kg - dry 14.3 1 05/13/21 00:31 JTR 6010D pH 7.3 s.u. 1 05/17/21 15:30 KEW 9045D Total Volatile Solids 51.3 % 0.010 1 05/13/21 16:07 FMM SM-2540G Qualifiers/ Definitions * Outside QC Limit B Analyte detected in blank C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 11 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-131-0008 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Wastewater Treatment Plant -Danville VA Information : VPDES PERMIT #VA0060593 REPORT OF ANALYSIS Report Date : 05/18/2021 Received : 05/11/2021 owi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76292 Matrix: Solids Sample ID : LTS A -Basin 21-1322 Sampled: 5/10/2021 8:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 44300 mg/Kg - dry 2860 1 05/12/21 09:30 JAE SM-2320 B Ammonia Nitrogen 11000 mg/Kg - dry 2860 1 05/17/21 15:00 JPJ SM-4500-NH3C Aluminum 24700 mg/Kg - dry 143 1 05/13/21 00:31 JTR 6010D Arsenic <14.3 mg/Kg - dry 14.3 1 05/13/21 00:31 JTR 6010D Cadmium <2.86 mg/Kg - dry 2.86 1 05/13/21 00:31 JTR 6010D Chromium 32.3 mg/Kg - dry 7.14 1 05/13/21 00:31 JTR 6010D Lead 31.7 mg/Kg - dry 8.57 1 05/13/21 00:31 JTR 6010D Molybdenum <7.14 mg/Kg - dry 7.14 1 05/13/21 00:31 JTR 6010D Analytical Method: SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Batch Moisture 96.5 010 0.010 1 05/13/21 16:07 FMM L552919 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 4 of 11 Waypol nt.. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalyt-ical.com Client: Inframark Project: Wastewater Treatment Plant -Danville VA Lab Report Number: 21-131-0008 Date: 5/18/2021 CASE NARRATIVE Metals Analysis Method 6010D Sample 76292 (LTS A -Basin 21-1322) Analyte: Selenium QC Batch No: L552756/L552397 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 11 Waypoint.. ANALYTICAL Customer Number: 79434 Customer Name: Inframark Report Number: 21-131-0008 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytica I.com Shipment Receipt Form Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? () Yes Custody seals intact on sample bottles? 0 Yes O No O No ® Not Present ® Not Present Chain of Custody (COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes 0 No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes O No Water - Sample containers properly preserved Water - VOA vials free of headspace O Yes O Yes O No O No ® N/A ® N/A Trip Blanks received with VOAs 0 Yes O No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes O No ® N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: ® No Signature: Brandi Watson Date & Time: Page 6 of 11 05/11 /2021 14:40:52 1 • a Z n ry C L .-Project Number Waypoint Acct. 79434 Project Description VPDES Permit #- VA0060593 Client Name/Address Inframark - Danville ONVIT1 229 Northside Dr. Danville, VA 24540 , Lab# E 76292-1 LTS A -Basin 21-1322 Cust: 79434 Inframark Col: 05/ 10/ 2021 08:30 Rec: 05/ 11/ 2021 00:00 21-131-0008 Preservation: < = 5 degrees C 1 11 loz I LTS A -Basin 21-r o- 1 • , a 3 n rr g - n ❑ c.) 47 a n o 3 3 • 2 7. g d o c J6 D 7 ' n m a - w a Unless Hated, aH containers per Table II of 40 CFR Part 136. Project Manager Phone 1F 434-799-5137 Protect/Site location (City/State) Danville, VA Wastewater Treatment Plant Client Project Manager/Contact Robert Clifton - Lab Mgr. Kim Wickemeyer - Sr Lab Tech. [Relinquished by. (SIGNATURE) wished hr.( IGN RE Relinquished by. ISIGNATUR Sampled by (Name - Print' Robert Clifton Number of Containers Matri>< {Refer to Key} I C.) G}rab or /C}omposite Project Manager Email robert.clifton@inframark.com RUSH - Additional charges apply Special Detection Limit's) Date Results Needed 05/30/2021 Billing Information Inframark 229 Northside Dr. Danville. VA 2454C II 1 f lc 1 see attached itsi at !esls I * a 7 m v 3 o • o A w 3 A �v o ; eel L 3 n Client Remarks/Comments All Analyses must be performed by a certified lab J 4 / Purchase Order Number 120725 .1 I m A 1 Al • R ive by SIGNATURE) F A m a Cr z a 8 a A m n a Cr z > "c m II1111111111111111111111114111I1111111I1 111011111111 o1B-20213 ramark 14:03:12 astewaler Trealmen€ PlanI-Danville VA I •npOlf 0W-Drinking Water 5-Soil/Solid D-oif P - Product M - Mlsc I r - i t 0.5 L plastic; preservative - B I n 0 3 3 m 2 a g :° ..__. A Cod c IOC N125203 {Micro Only! g Coat <= 6C 1425.04 pHc2 ❑ None Required NaOH pHr10 HNO3 pHc2 G HCt pHc2 • H31.04 pHc2 Coal c.• 6C NA25203 Site/Facility ID Ir VPDES #: VA0060593 rr v n -I — 5 -- n tti ❑ y n -I 3 n 0 m n -I 3 e Page 7 of 11 t TT 3o 8 abE'd Required Biosolids Tests for inf-a-nark Danville, VA WWTP (Waypoint VA Account 79434) Sample: LTSABasin21- 132- - Po: .+07tA5 ,,f/+S %TVS Alkalinity IKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen Organic Nitrogen (calculation) ✓ Phosphorus N/Potassium _ulfur ./Calcium ✓Magnesium N./Sodium Aron ✓Aluminum Manganese './Copper \ /Zinc Cadmium A7- g r- o — Chromium Nickel Lead Arsenic Mercury Selenium Molybdenum c TT 30 6 a5Pd ( INFRAMARK Vendor Waypomt Analytical Inc. Phone:901-327-2750 Contact Contact Email Bill To. 229 Northside Drive Danville Virginia 24540 United States c 0 Purchase Order P©##: Date: End User Email: End User Phone: Payment Terms: Ship To: 229 Northside Drive Danville Virginia 24540 United States 120725 5+7/2021 kimberly wickemeverea inframark.com 434-799-5137 Net 30 Attn: Kimberly Wickemeyer Line item ID Project Qty Units Expected Delivery Dale Rate Amount SIR00012 DANVILLE 1 6/ 15(2021 5249 90 5249.90 Description: 503 E Heavy Metals Line Item ID Project Qty Units Expected Delivery Date Rate Amount SIR00012 DANVILLE 1 Ea 6/15/2021 $21,00 $21.00 Description: Ammonia Nitrogen by distillation Line (tern ID Qty Units Expected Delivery Date Rate Amount 3 51R00012 DANVILLE 1 Ea 6/15/2021 $2100 $21.00 Description: Nttrate+Nrtnte as N 1 af3 TT 3o 0T abed ANFRAMARK Vendor Waypoint Analytical Inc. Phone: 901-327.2750 Contact: Contact Email: Line Item fD Prr4ect 4 SIR00012 DANVILLE Description: pH Purchase Order PO#: 120725 Date: 51712021 End User Email: kimberly.wickemeyer{ inframark.com End User Phone: 434-799-5137 Payment Terms: Net 30 Units Expected Delivery Date Rate Amount Ea 6/15/2021 $1 S 75 $15.75 Line Item ID Project Qty Units Expected Delivery Date Rate mount SIR00012 DANV}LLE Ea 6/15/2021 $79 80 379.80 Description: SL2 Biosofios Test Package Line Item ID Protect Qty Unlb Expected Delivery Date Rate Amount 6 SIR00012 DANVILLE- Ea 1_ 1 $16 80 $16 80 Description: Total Alkalinity Line Item ID Project Qty Units Expected Delivery Date Rate Amount 7 SIR00012 DANVILLE 1 Ea 6/15/2021 517.85 $17 85 Description: Total Volatile Solids (TVS as %) 2 of 3 TT 30 TT abed }INFRAMARK Vendor Waypoint Analytical Inc. Phone-901-327-2750 Contact. Contact Email: Purchase Order PO#: 120725 Date: 517l2021 End User Email: kimberly,w ek.erleyer@inframark.cor't1 End User Phone: 434-799-5137 Payment Terms: Net 30 Total S422.10 All packing lists and proofs of delivery must be sent to receivingjmframark cam within 48 hours of delivery Please reference the PO number above on all documentation Inframark, LLC General Conditions of Purchase, a copy of which is aval:able at https //www inframark com/contact-us/doing-business- with-usil and any specific conditions or other terms not included in these General Conditions of Purchase that are mutually agreed upon in writing (herein after "'Specific Conditions') shall govern this Purchase Order In the event of a conflict between any Specific Conditions noted in the Purchase Order and the General Conditions of Purchase, the Specific Conditions shall control. All terms and conditions included in any Supplier documentation are specifically releced by Purchaser and shall be of no effect on this Purchase Order Please reference this Purchase Order number on all shipping and billing documents related to this order Vendor Acceptance. Date. 3 of 3 Sodium Calcium Magnesium Percent Solids 5/10/2021 mg/kg mg/L Equiv Weight Milli Equiv 9630 336.087 23 14.61248 10000 349 20 17.45 2570 89.693 12 7.474417 3.49 SAR= SAR 4.14 Na+ /2 (Ca2+ + Mg2+) Waypoint ANALYTICAL 6/3/2021 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 21-145-0022 Project Description: Danville WWTP VPDES Permit#VA0060593 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.tom Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/25/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, c 4lj I( Grow/ Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 10 Waypoint, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical, com Sample Summary Table Report Number: 21-145-0022 Client Project Description: Danville WWTP VPDES Permit#VA0060593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 SM-2540G WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 SW-7471B WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 SM-4500-NH3C-TKN WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 4500NO3F-2011 WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 6010D WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 SM-4500-NH3C WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 9045D WP MTN 76503 LTS A -Basin 21-1363 Solids 05/24/2021 08:05 05/25/2021 SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 10 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-145-0022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Danville WWTP Information : VPDES Permit#VA0060593 REPORT OF ANALYSIS Report Date : 06/03/2021 Received : 05/25/2021 owi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76503 Matrix: Solids Sample ID : LTS A -Basin 21-1363 Sampled: 5/24/2021 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 95.4 % 0.010 1 05/26/21 16:05 FMM SM-2540G Potassium 3090 mg/Kg - dry 217 1 05/28/21 20:52 JTR 6010D Sulfur 12100 mg/Kg - dry 217 1 05/28/21 20:52 JTR 6010D Calcium 13700 mg/Kg - dry 1090 1 05/28/21 20:52 JTR 6010D Magnesium 3410 mg/Kg - dry 109 1 05/28/21 20:52 JTR 6010D Sodium 7500 mg/Kg - dry 543 1 05/28/21 20:52 JTR 6010D Iron 32800 mg/Kg - dry 217 1 05/28/21 20:52 JTR 6010D Aluminum 30900 mg/Kg - dry 109 1 05/28/21 20:52 JTR 6010D Manganese 1090 mg/Kg - dry 10.9 1 05/28/21 20:52 JTR 6010D Copper 424 mg/Kg - dry 10.9 1 05/28/21 20:52 JTR 6010D Zinc 2390 mg/Kg - dry 27.2 1 05/28/21 20:52 JTR 6010D Cadmium <2.17 mg/Kg - dry 2.17 1 05/28/21 20:52 JTR 6010D Chromium 42.8 mg/Kg - dry 5.43 1 06/01/21 19:56 JTR 6010D Nickel 60.2 mg/Kg - dry 5.43 1 05/28/21 20:52 JTR 6010D Lead 49.8 mg/Kg - dry 6.52 1 05/28/21 20:52 JTR 6010D Arsenic <10.9 mg/Kg - dry 10.9 1 05/28/21 20:52 JTR 6010D Mercury <0.307 mg/Kg - dry 0.307 1 05/28/21 12:33 DDB SW-7471B Selenium <10.9 mg/Kg - dry 10.9 1 05/28/21 20:52 JTR 6010D Molybdenum 10.3 mg/Kg - dry 5.43 1 05/28/21 20:52 JTR 6010D Qualifiers/ Definitions * Outside QC Limit B Analyte detected in blank C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 10 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-145-0022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project Danville WWTP Information : VPDES Permit#VA0060593 REPORT OF ANALYSIS Report Date : 06/03/2021 Received : 05/25/2021 owi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 76503 Matrix: Solids Sample ID : LTS A -Basin 21-1363 Sampled: 5/24/2021 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 7480 mg/Kg - dry 2170 1 06/01/21 09:10 JAE SM-2320 B Ammonia Nitrogen 9740 mg/Kg - dry 2170 1 06/02/21 15:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <107 mg/Kg - dry 107 1 05/26/21 14:06 ZBD 4500NO3F-2011 Organic N 35260 mg/Kg - dry 5435 1 06/02/21 10:00 CALCULATION pH 7.0 s.u. 1 06/01/21 15:30 ADM 9045D Total Solids 4.59 % 0.010 1 05/26/21 16:05 FMM SM-2540G Total Volatile Solids 50.7 % 0.010 1 05/26/21 16:05 FMM SM-2540G Total Kjeldahl Nitrogen 45000 mg/Kg - dry 5430 1 06/02/21 10:00 JPJ ;M-4500-NH3C-TKI` Phosphorus 20600 mg/Kg - dry 109 1 05/28/21 20:52 JTR 6010D Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit L Limit Exceeded Page 4 of 10 Waypoint.. ANALYTICAL Customer Number: 79434 Customer Name: Inframark Report Number: 21-145-0022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytica I.com Shipment Receipt Form Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? () Yes Custody seals intact on sample bottles? 0 Yes O No O No ® Not Present ® Not Present Chain of Custody (COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes 0 No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes O No Water - Sample containers properly preserved Water - VOA vials free of headspace O Yes O Yes O No O No ® N/A ® N/A Trip Blanks received with VOAs 0 Yes O No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes O No ® N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: ® No Signature: Brandi Watson Date & Time: Page 5 of 10 05/25/2021 15:34:24 Client Name/Address lnframark - Danville VW'WTP 229 Northside Dr. Danville, VA 24540 Client Project Manager/Contact Robert Clifton - Lab Mgr. Kim Wickemeyer - Sr. Lab Tech. Billing Information inframark 229 Northside Dr. Danville, VA 24540 i r,f ,�,��}�� rarn� l k ��11�VI�11��1 TP ``ii hh44 4ll 1 y y `��}��111111 ., Z1 14�OO2` os4 5-2D21 i22aas Protect Description VPDES Permit #: VA0060593 Project/site Location {City/State} Danville, VA Wastewater Treatment Plant III,Special 'J 06/11 RUSH — Additional charges apply Detection Umit(s) Pate Results Needed /2021 Danville YVW N. [ t_-_I Other *r „rr — winking Water 5 — Soil /Solid 0 —ail P- Product M - Mlsc Project Number Waypoint Acct. 79434 Project. Manager Phone N 434-799-5137 Project Manager Email robert.ciifton@inframark.com Purchase Order Number / .. / i 4- Site/Facility ID a VPDES #: VA0060593 Waypoint•0 ANALYTICAL 2790 wh:tun Road Memphis. TN 343133 ,!dr.11+i._4,10 ` Unless noted, a"I containers per Table II of 4OCfRpart 136. Number of Containers Matrix (Refer to Keyl E `c s A t7 15 A Cool < 10C Ha252Q3 Mao Only' 8 Cool <= 6C . C H2504 pH<7 U None Required E NaOH pH>IO F HH03 pHc2 G HCL pH`a H H3PO4 pHe2 I Cool <. 6C HA25201 C�al�• •*�.• ,s+nole Identification Required An lysis / Preservative Comments/Notes 16,1 05 LTS A -Basin 21-1510 1 s rC le,- ~0.5 L plastic; preservative = B - Al s1 - -- i +1 VI t 1 41, � ' A -Basin 211363 - c - r 1. r . v Lab# E 76503-1 Cust: 79.434 Inframark Rec:05/25/202100:0D l 5 21/c.... Col: fl5/24/ 202108:fl5 23 1 45-0422 Preservation: t= b degrees C ► _ ' 1 1 11 �i C?fiC..i 1 y _ For Laboratory Use Only AS Sampled by !Name — Print) ' Client Remarks/Comments All Analyses must be performed by a certified lab ice Custody Seals lab Comments Robert Clifton 'r N �* SrIA++ J Re - quished try: 51 NAT EI +YLt- Date,Time,,., I� I""t i4 0c i Received by: !SIGNATURE) Date Time Blank ooi Temp 0. Relinquished by: (SI ATUREJ Date Time Received by: !SIGNATURE) Date Time Relinquished by: (SIGNATURE) Date Time fl7e4lh:k ISIG UR } ate Time Required Biosolids Tests for lnframark Danville, VA WWTP (Waypoint VA Account 79434) Sample: LTS A Basin 21- Pp: li 'eTS� 76T'd5-� py Wi1-y TEAL gen --N itrite as Nitrogen — ,gniitNitrogen (calculation) --Pfterrypkus llur1liurli Page 7 of 10 tOENFRAMARK Vendor Waypaint Analyt+cal Inc Phone: 901-327-2750 Contact: Contact Email. Bill To: 229 Northside Drive Danville Virginia 24540 United States Purchase Order PO#: 121142 Date: 5/1812021 End User Email: kimberlywickemeyer@inframark.cam End User Phone: 434-799-5137 Payment Terms: Net 30 Ship To: 229 Northside Drive Danville Virginia 24540 United States Attn: Kimberly Wfckemeyer Line ID Project Units Expected Derivery Data Rate 1 SIR00012 DANVILLE 1 6115/2021 $249.90 $249 90 Description: 503 E heavy Metals Lbie item ID Project Qty Units E per ed De►thery Gabe Rate 2 SIR00012 DANVILLE 1 a 6/15/2021 $21 00 $21.00 Description: Ammonia Nitrogen by distillaitan Line hem ID Praiect Oty Expected Delivery Date Rate Amount SIR00012 DANVILLE 1 Ea 6/15/2021 $21.00 $21 00 Description: Nitrate+Nitrite as N of 3 Page 8 of 10 dINFRAMA'RK Vendor Waypomi Analytical Inc Phone.901-327-2750 Coniacl Conlac' Email Purchase Order PO#: 121142 Date: 5118/2021 End User Email: kimberly.wicken1eyer[tinframark.COm End User Phone: 434-799-5137 Payment Terms; Net 30 4 SIROLIO'2 DANVILLE 1 Ea 6/1512021 $15.75 $15.75 Description: pH Line Neat ID Project Oty Units Expelled Delivery Dale Rate Amount 5 SIR00012 DANVILLE Ea 6/15/2021 $79 80 $79 80 Description: SL2 Biosolids Test Package Description: Total Alkalinity Description: Total Volatile Solids (TVS as %) 2 of 3 Page 9 of 10 *INFRAMARK Vendor Waypoint Analytical Inc Phone.901-327-2750 Contact' Contact Email. Purchase Order PO#: 121142 Date: 5/18/2021 End User Email: kirnberlywickemeyer@inframark.corn End User Phone: 434-799-5137 Payment Terms: Net 30 Total S422.10 All packing fists and proofs of delivery must be sent to receiving@inframark.com within 48 hours of delivery Please reference the PO number above on all documentation Inframark, LLC General Conditions of Purchase, a copy of which is available at https //www rnframark corn/contact-us/doing-business- with-us/ . and any specific conditions or other terms not included in these General Conditions of Purchase that are mutually agreed upon in writing (herein after "Specific Conditions ) shall govern this Purchase Order In the event of a conflict between any Specific Conditions noted in the Purchase Order and the General Conditions of Purchase. the Specific Conditions shall control All terms and conditions included in any Supplier documentation are specifically rejected by Purchaser and shall be of no effect on this Purchase Order Please reference this Purchase Order number on all shipping and billing documents related to this order Vendor Acceptance; Date 3 of 3 Page 10 of 10 Sodium Calcium Magnesium Percent Solids 5/24/2021 mg/kg mg/L Equiv Weight Milli Equiv 7500 344.25 23 14.96739 13700 628.83 20 31.4415 3410 156.519 12 13.04325 4.59 SAR= SAR 3.17 Na+ /2 (Ca2+ + Mg2+) Waypoint ANALYTICAL 5/4/2021 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 21-106-0094 Project Description: VPDES Permit # VA0060593 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.tom Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/4/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, frl c &foc r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 Waypoint, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical, com Sample Summary Table Report Number: 21-106-0094 Client Project Description: VPDES Permit # VA0060593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 75909 LTS A -BASIN 21-1250 TCLP TCLP TCLP TCLP TCLP TCLP TCLP TCLP 04/13/2021 07:50 05/04/2021 SW-1311 (ZHE) WP MTN 04/13/2021 07:50 05/04/2021 6010D WP MTN 04/13/2021 07:50 05/04/2021 7470A WP MTN 04/13/2021 07:50 05/04/2021 8081A WP MTN 04/13/2021 07:50 05/04/2021 8151A WP MTN 04/13/2021 07:50 05/04/2021 8260B WP MTN 04/13/2021 07:50 05/04/2021 8270C WP MTN 04/13/2021 07:50 05/04/2021 SW-1311 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 9 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0094 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit # VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/04/2021 Received : 05/04/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75909 Matrix: TCLP Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 04/21/21 14:00 JAN SW-1311 TCLP Metals Extraction Leachate 1 04/21/21 14:00 JAN SW-1311 TCLP Pesticide Extraction Leachate 1 04/21/21 14:00 JAN SW-1311 TCLP SVOC Extraction Leachate 1 04/21/21 14:00 JAN SW-1311 TCLP VOC ZHE Extraction Filtrate 1 04/22/21 14:00 PHE SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L549252 04/27/21 08:16 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/28/21 11:46 TJS L549770 TCLP Barium <0.250 mg/L 0.250 1 04/28/21 11:46 TJS L549770 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/28/21 11:46 TJS L549770 TCLP Chromium <0.100 mg/L 0.100 1 04/28/21 11:46 TJS L549770 TCLP Lead <0.100 mg/L 0.100 1 04/28/21 11:46 TJS L549770 TCLP Selenium <0.500 mg/L 0.500 1 04/28/21 11:46 TJS L549770 TCLP Silver <0.0500 mg/L 0.0500 1 04/28/21 11:46 TJS L549770 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 3 of 9 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0094 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit # VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/04/2021 Received : 05/04/2021 owi•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75909 Matrix: TCLP Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Analytical Method: 7470A Prep Batch(es): L548912 04/23/21 08:00 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/23/21 11:42 DDB L549040 Analytical Method: 8081A Prep Batch(es): L549577 04/27/21 11:40 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.005000 mg/L 0.005000 10 04/28/21 01:30 NFP L549798 TCLP gamma-BHC <0.005000 mg/L 0.005000 10 04/28/21 01:30 NFP L549798 TCLP Methoxychlor <0.005000 mg/L 0.005000 10 04/28/21 01:30 NFP L549798 TCLP Toxaphene <0.03750 mg/L 0.03750 10 04/28/21 01:30 NFP L549798 TCLP Chlordane <0.02500 mg/L 0.02500 10 04/28/21 01:30 NFP L549798 TCLP Heptachlor Epoxide <0.005000 mg/L 0.005000 10 04/28/21 01:30 NFP L549798 TCLP Heptachlor <0.005000 mg/L 0.005000 10 04/28/21 01:30 NFP L549798 Analytical Method: 8151A Prep Batch(es): L548845 04/22/21 15:15 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D TCLP 2,4,5-TP (Silvex) <0.1000 <0.0100 mg/L mg/L 0.1000 1 04/26/21 16:03 NFP L549553 0.0100 1 04/26/21 16:03 NFP L549553 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 4 of 9 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0094 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit # VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/04/2021 Received : 05/04/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75909 Matrix: TCLP Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Analytical Method: 8260B Prep Batch(es): L549173 04/23/21 22:40 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Carbon Tetrachloride <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Chlorobenzene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Chloroform <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP 1,4-Dichlorobenzene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP 1,2-Dichloroethane <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP 1,1-Dichloroethene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Methyl Ethyl Ketone (MEK) <0.200 mg/L 0.200 1 04/24/21 07:30 ASH L549240 TCLP Tetrachloroethene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Trichloroethene <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 TCLP Vinyl Chloride <0.0100 mg/L 0.0100 1 04/24/21 07:30 ASH L549240 Analytical Method: 8270C Prep Batch(es): L549519 04/27/21 09:40 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP 3&4 Methylphenol <0.125 mg/L 0.125 1 04/27/21 18:22 BGV L549796 TCLP 2,4-Dinitrotoluene <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP Hexachlorobenzene <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP Hexachlorobutadiene <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP Hexachloroethane <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 5 of 9 Waypoint, ANALYTICAL 79434 Inframark A/P Northside WWTP 229 Northside Drive Danville , VA 24540 Report Number : 21-106-0094 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointa nalytical. com Project VPDES Permit # VA0060593 Information : REPORT OF ANALYSIS Report Date : 05/04/2021 Received : 05/04/2021 oiui•e row Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 75909 Matrix: TCLP Sample ID : LTS A -BASIN 21-1250 Sampled: 4/13/2021 7:50 Analytical Method: 8270C Prep Batch(es): L549519 04/27/21 09:40 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Nitrobenzene <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP Pentachlorophenol <0.125 mg/L 0.125 1 04/27/21 18:22 BGV L549796 TCLP Pyridine <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP 2,4,5-Trichlorophenol <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 TCLP 2,4,6-Trichlorophenol <0.0620 mg/L 0.0620 1 04/27/21 18:22 BGV L549796 Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 6 of 9 Waypol nt.M ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalyt-ical.com Client: Inframark Project: VPDES Permit # VA0060593 Lab Report Number: 21-106-0094 Date: 5/4/2021 CASE NARRATIVE Separatory Funnel Extraction 8081 Method 3510C Sample 75909 (LTS A -BASIN 21-1250) QC Batch No: L549577/L549577 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction Method 3510C QC Batch No: L549519/L549519 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Extraction for SW-8151 Phenoxy Herbicides Method 8151A QC Batch No: L548845/L548845 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Page 7 of 9 Waypoint.. ANALYTICAL Customer Number: 79434 Customer Name: Inframark Report Number: 21-106-0094 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytica I.com Shipment Receipt Form Shipping Method O Fed Ex O US Postal O Lab O Other : ® UPS 0 Client O Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? () Yes Custody seals intact on sample bottles? 0 Yes O No O No ® Not Present ® Not Present Chain of Custody (COC) present? ® Yes 0 No COC agrees with sample label(s)? ® Yes 0 No COC properly completed ® Yes O No Samples in proper containers? ® Yes O No Sample containers intact? ® Yes O No Sufficient sample volume for indicated test(s)? ® Yes O No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? ® Yes O No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes O No Water - Sample containers properly preserved Water - VOA vials free of headspace O Yes O Yes O No O No ® N/A ® N/A Trip Blanks received with VOAs 0 Yes O No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes O No ® N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: ® No Signature: Samantha Clarke Date & Time: Page 8 of 9 05/04/2021 15:43:27 Gienr NameIAddress Inirarnark Danville +f'MTP 229 Northside Dr Danville, VA 24540 y client Project Mang[[/CUmatt Robe['. Cltflon Lab Mgr KIrn WlLkerneyer - Sr Lab Tech ruling tnrc,r, vumor, lnrrarnark. 229 Northside L1' Danville, VA 2454C For Laboratory Use Only Projrci Drssnption VPDES Permit # VA0060593 ProjeCt/>'te Location {City/Sralel Danville, VA Wastewater Treatment Plant il 05/ RIJSIt - Md t a.. ,... spree LrPt I. • 1]�e II, •-.•rc, r., ,. 15/2021 Wined El ®� of Shipment I, •I t r,r, ,. r .,... D. , i I . - , U..,,. f“4 Mat rra, Ary v,,,'. [Td. .. •. I , Praiett Number Waypoint Acct 79434 Noma' Manager Phone R 434-799-5137 Protect Manager (mail roberi cliftongintrantark.wou1 Purchase 11 Order Nr:mber 9377 SetIJF.tcpier y ID r VPDES #: VA0060593 0a 4 !GP aCor {Clurnuosric luol, IOC NAISZOI{Ma ea Orr PyI R Caul a' SC +rrsoc to I. 2 N.rne It ern.re ed ai;.l P1a.i ..ra0i eN.: be %an:. I vaypOift C _ Y k c. i E i i I _ z } keauPree a nl. e. , . .,r.•: irm mentsiNotet LTS A -Basin 21-1250A 1 6 _ �' Ilii� r AN • r► _ i t — ` , ;i ` L Plastic- preservative LTS A -Basin 21-1250B 1 S t---_�--^V��-.. -1 .. , ,?r;Itier gtass v,r-,servative = P .. LTS A -Basin 21-1250C 1 S . - �/ _ i i arleter glass- preservative = l; y- — .— w :44 fy�rI p -rh m, — I'�III II III nY If UI1 uIrI I I'II iI I U 2,-,oe oc>sa u 05-G4 2021 / w _ , a ` p j�7f' .] Ng1F Iri rarnark 15:42'33 VPDES Permcl # VA0060593 ` , --- _ .. -- . \ +}/ 0 ry f`� d '00 " J on !� ri A � rn L ice-' in. tabor,Amy Use Only S.cmpted by !Name-ParcI Client II mar kc/Cammrnt5 All Analyses must be performed by a certified lab co 1uttocty Sir Ait rr. tabCom+nt% Robert Clifton Oki Y ::) Real MII+y )SIG TIJR' �i► i Datee Tinto tf /7' 0/3D. Received by{SIGNATURE) Date time Shank lynxl.l�+' T Rrl,nyulchwl by. {SIGNAIUR - Dale time Received y. 1 4URk) Date time b y Rri+^yu+shed by 'SIGNATUAi Date Same Rlfe (SIGN URI) s [�a F[it 2 1 DO . sO Page 9 of 9 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: City of Danville Northside WWTP WQ Permit Number: WQ0036561 NPDES Number: VA0060593 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) • Alt B (Alk Treatment) ■ Alt. C (Prior Testing) ■ A1t.D (No Prior Test) 0 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray • Ganuna Ray • Pasteurization • Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ I Ei If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization • Air Drying • Composting • Aerobic Digestion • Anaerobic Digestion • If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 200 275 500 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ■ Alt. 2 (40-day bench) • Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) • Alt. 5 (14-Day Aerobic) ■ Alt. 6 (Alk. Stabilization II 7 (Drying -Stable) ■ Alt. 8 (Drying - Unstable) MI Alt. 9 (Injection) • Alt. 10 (Incorporation) ■ No vector attraction reduction alternatives were performed • CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Gregory Ryland - Regional Manager Preparer Name and Title (type or print) GAY A 0V Al (FebRy and /VG/MG(Grego13:55 T) Signature of Preparer* Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) Feb 9, 2022 2/6/2022 Date Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) (eAnaIYticaI vw.p�tlehsen www.pacelabs.cam April 22, 2021 Mr. Robert Clifton INFRAMARK 229 NORTHSIDE DR Danville, VA 24540 RE: Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Dear Mr. Clifton: Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - WestVirginia • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Stacy Heasley stacy.heasley@pacelabs.com 800-999-0105 Project Manager Enclosures cc: Ms. Kimberly Wickemeyer, INFRAMARK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 (eAnaIYtica/ e www.pacelabs.com CERTIFICATIONS Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Pace Analytical Services Beaver 225 Industrial Park Drive, Beaver, WV 25813 Virginia VELAP 460148 West Virginia DEP 060 West Virginia DHHR 00412CM North Carolina DEQ 466 Kentucky Wastewater Certification KY90039 Pennsylvania DEP 68-00839 Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 (eAnaIYtica/ e www.pacelabs.com SAMPLE SUMMARY Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Matrix Date Collected Date Received 7367252001 CATWALK Al #6 Solid 04/13/21 07:50 04/13/21 12:06 7367252002 CATWALK A2 #1 Solid 04/13/21 07:15 04/13/21 12:06 7367252003 CATWALK A3 #5 Solid 04/13/21 07:45 04/13/21 12:06 7367252004 CATWALK A4 #2 Solid 04/13/21 07:25 04/13/21 12:06 7367252005 CATWALK A5 #4 Solid 04/13/21 07:40 04/13/21 12:06 7367252006 CATWALK A6 #3 Solid 04/13/21 07:30 04/13/21 12:06 7367252007 CATWALK A2 #7 Solid 04/13/21 07:20 04/13/21 12:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 (eAnaIYtica/ e www.paeelabs.enm SAMPLE ANALYTE COUNT Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Method Analytes Analysts Reported Laboratory 7367252001 CATWALK Al #6 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252002 CATWALK A2 #1 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252003 CATWALK A3 #5 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252004 CATWALK A4 #2 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252005 CATWALK A5 #4 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252006 CATWALK A6 #3 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7367252007 CATWALK A2 #7 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV PASI-BVWV = Pace Analytical Services - WestVirginia PASI-LX = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK Al #6 Lab ID: 7367252001 Collected: 04/13/21 07:50 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <222 CFU/g 223 0.223 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.5 % 0.10 1 04/15/21 09:40 Sample: CATWALK A2 #1 Lab ID: 7367252002 Collected: 04/13/21 07:15 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <500 CFU/g 500 0.5 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 98.0 % 0.10 1 04/15/21 09:40 Sample: CATWALK A3 #5 Lab ID: 7367252003 Collected: 04/13/21 07:45 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <200 CFU/g 200 0.2 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.0 % 0.10 1 04/15/21 09:40 Sample: CATWALK A4 #2 Lab ID: 7367252004 Collected: 04/13/21 07:25 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <244 CFU/g 244 0.244 04/13/21 16:20 04/14/21 16:45 REPORT OF LABORATORY ANALYSIS Date: 04/22/2021 02:42 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 10 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK A4 #2 Lab ID: 7367252004 Collected: 04/13/21 07:25 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.9 % 0.10 1 04/15/21 09:40 Sample: CATWALK A5 #4 Lab ID: 7367252005 Collected: 04/13/21 07:40 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <244 CFU/g 244 0.244 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.1 % 0.10 1 04/15/21 09:40 Sample: CATWALK A6 #3 Lab ID: 7367252006 Collected: 04/13/21 07:30 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <244 CFU/g 244 0.244 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.9 % 0.10 1 04/15/21 09:40 Sample: CATWALK A2 #7 Lab ID: 7367252007 Collected: 04/13/21 07:20 Received: 04/13/21 12:06 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <370 CFU/g 371 0.371 04/13/21 16:20 04/14/21 16:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.3 % 0.10 1 04/15/21 09:40 REPORT OF LABORATORY ANALYSIS Date: 04/22/2021 02:42 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 (eAnaIYtica/ e www.pacelabs.com QUALIFIERS Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS Date: 04/22/2021 02:42 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 10 (eAnaIYtica/ e www.paeelabs.enm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK-DANVILLE Pace Project No.: 7367252 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 7367252001 CATWALK Al #6 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252002 CATWALK A2 #1 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252003 CATWALK A3 #5 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252004 CATWALK A4 #2 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252005 CATWALK A5 #4 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252006 CATWALK A6 #3 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252007 CATWALK A2 #7 SM 9222D - 2006 65503 SM 9222D - 2006 65504 7367252001 CATWALK Al #6 SM 2540G-11 65279 7367252002 CATWALK A2 #1 SM 2540G-11 65279 7367252003 CATWALK A3 #5 SM 2540G-11 65279 7367252004 CATWALK A4 #2 SM 2540G-11 65279 7367252005 CATWALK A5 #4 SM 2540G-11 65279 7367252006 CATWALK A6 #3 SM 2540G-11 65279 7367252007 CATWALK A2 #7 SM 2540G-11 65279 REPORT OF LABORATORY ANALYSIS Date: 04/22/2021 02:42 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 ace Analytical' CHAIN -OF -CUSTODY Analytical Request Uocumen Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields Company: Inframark-Danville Address: 229 Northside Dr., Danville, VA 24540 Billing Information: Inframark-Danville WWTP 229 Northside Drive Danville, VA 24540 Report To: Robert.Clifton@Inframark.com Email To: Stephanie.Mosko@Inframark.com Copy To: Kimberly.Wickemeyer@Inframark.com Customer Project Name/Number: Inframark-Danville (client #: 92-618203) Phone: 434-799-5137 Email: kimberly.wickemeyer@inframark.com Collected By (print): Robert Clifton Coll cted By(signature) Sample Disposal!' [✓] Dispose as appropriate [ J Return [ ) Archive: [ ] Hold: * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Site Collection Info/Address: Danville VA WWTP 229 Northside, Dr., Danville, VA 24540 State: County/City: Time Zone Collected: VA /Danville Site/Facility ID #: Danville, VA WWTP permit VA0060593 Purchase Order #: 119372 Quote #: 00091909 Rush: [ ] Same Day [ 1 Next Day [ ]2Day [ J3Day [ ]4Day [ ]5Day (Expedite Charges Apply) Customer Sample ID Matrix * a a •• awa atWa -AS—# Catwalk A4 #2 atwalk atwa Comp / Grab Grab Grab Grab Grab Grab Grab Grab Collected (or Composite Start) 04/13/21 7.1. 04/13/21 0740 04/13/21 Di 04/13/21 7.10 [ ]PT[ ]MT[ ]CT VET Compliance Monitoring? [$YYes [ ]No DW PWS ID #: DW Location Code: Immelate y Pac ed on Ice: [iIJ'Yes [ ] No Field Filtered (if applicable): [ ] Yes V] No Analysis: # of Ctns WO#:7367252 IIII III IIIIIIIIIIIIIIIIII ** Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acei. (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other Analyses Customer Remarks / Special Conditions / Possible Hazards: `Biosolids for Fecal Coliform Bottles: 150 mL Sterile for microbiology Typ of Ice Used eWet Blue Dry None Packing tvtat , al Used ned (<500 cpm): Y N NA Relinquished by/Company: (Signature) Relinquished y/Company: (Signature) Date/Time: y /3-L/ Date/Time, Receive Com.- y: Signature) led by/Company: (Signature) iHORE HOLDS PRESLNT (<72 hvu+�`: mp(es receivedvia UPS Date/Time: `if 13/Q Date/Time: Courier Pace Courier f JL LA3 USE ONLY `able 4: .Acctnum Template • °re(ogin: Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: b Sample Temperetu e Info: Temp Blank feceived: Y N NA Therm iDtf: <-XTYI't a'-t Cooler 1 Ternp Upon Receipt: I 11D oC Cooler 1 Therm Corr. factory—O.% oC Cooler 1 Corrected Temp: Or ' oC Comments: ip Blank Received: Y N NA HCL McOH TSP Other Non Conformances) !Page: r� i. / NO of: 1 LIMS73 Lab Sample Condition Upon Receipt (West Virginia) 7367252 .. PaceAnarytical Client Name: ckAA PM: SDH Due Date: 04/23/21 "4 CLIENT: INFRAMARK Courier: ❑ Fed Ex ['UPS ❑ USPS alOdnt ❑ Commercial ❑ Pace ❑ Oth, Tracking #: Custody Seal on Cooler/Box/Containers Present: ❑ yes Iolo Thermometer Used Cooler Temperature Comments: Seals Intact: ❑ yes ❑ no Type of Ice: Blue None Observed Temp 4* e C Correction Factor7011 C Final Temp: 0 ,% C pH paper Lot# Date and Initia *oo�f erson exa/nlnin 6J contents: r tl_/•,� Y Yes No N/A Chain of Custody Present: 1 Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COC: 4. Sample Labels match COC: _ 5. -Includes date/time/ID Matrix: '� Samples Arrived within Hold Time: V 6. Short Hold Time Analysis (<72hr remaining): 7. Rush Turn Around Time Requested: L/ 8. Sufficient Volume: 9. Correct Containers Used: 10. -Pace Containers Used: Containers Intact: 11. Orthophosphate field filtered: t .412. Hex Cr Aqueous sample field filtered: v13. -pH adjusted within 24 hours? (If yes, indicate acid lot #) Filtered volume received for Dissolved tests: V14. All containers have been checked for preservation: ( ,1'5. exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: Initial whe1...........-- Datenime samesrre%/];)�1 f�'completed provided to lab (�11 G(J �4 Tests not preserved: Headspace in VOA Vials: '..—,..-16. Trip Blank Present: L. 17. .^ Trip Blank Custody Seals Present: `--� Initial when +completed: Date:I 43/96a Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. SCUR_WV - rP 41:9of 10 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: 7/23/2021 Date Sample Rcvd: 6/14/2021 Vector Attraction Reduction / Aerobically Digested Sludge [30 Day Test) Meritech Work Order # 06142101 Sample: Danville Composite 6/14/21 Total Solids Volatile Solids % Volatile Solids Week 1 0.830 0.430 0.524 Week 2 0.840 0.500 0.598 Week 3 0.790 0.500 0.635 Week 4 0.890 0.470 0.526 Week 5 0.810 0.440 0.542 Van Kleek Reduction (%): -7.15 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass knanth dJctnrgnko Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Analyst: t1:11 Date: (1/4-1 Recorded By: 2i PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 P-6' 1st Clean IN 550°C lst Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample 114 104°C 2nd Sample OUT 104°C B - A x 100 = % TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C _ SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (6g) Ist Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS OL0ILIa1 - 01 Dctr-A 14.45-t g,1 al.(t 3 Q1•I.o643 0 a1.-fl •s at•1igs o 0,19 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for l hour) D 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS al•-.1t7k '1•1l"71 U 0 •112 SA,11PL g USED DISH # IstTARE WT. (g) 2nd TARE Wt (g) Tare %VT Diff (6g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1C.023r- 3.4 a3.3914Z 23 ,3942 0 a3. SZ(Z R3. 5712_ o 0, XLI (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS t 3.95c.,g of?), y (,,,S O o, it 9) SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (6g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 14•G $[ S. 3 3t'i.1$L S 3LI. (VAS 0 . Lilt L1t Sy . 444L-i b 0 1,1 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) D 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 34•3S0 3y,3Sty Q O.lri SAMP g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (6g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 11-i.979 I.i 41.74l4 (H.-4?4 e. _ 4(.K7SZ L11.K75Z o 0,S5 WB512 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for I hour) lst Ignition Wt (g) 2nd Ignition Wt (g) Ignite WI Diff (finall-initial) % VOL SOLIDS Li1 _goia (-I1.0ol2- 0 o,1/4-it Analyst: N N e f) sd PERCENT TOTAL SOLIDS PER ENT VOLATILE SOLIDS SM2540I1 ",�� Date: 6,r'2 / ? 1 11- Recorded By: /21 7L. SAMPLE SAMPLE 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample 1N 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C g USED 1< C41 2 g USED g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) 3G3'SI A Tare WT Di (AO ijc67 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) . 416-63 77 DISH # 2nd TARE Wt (g) B - A x 100 = % TOTAL SOLIDS C B -Dx 100=%VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C Tare WT Diff Os} 1st Dry Wt (g) 2nd Dry Wt (g) D Dry Wt Diff (final -initial) 0 % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3g.li2qi ?E• ugic G7 0 -54 1st Dry Wt (g) u4.6 3 7 c 4‘.7‘“C (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 14 38,502 Tare WT Diff (pg) 30.0 c 3i-6326 2nd Dry Wt (g) D Dry Wt Diff (final -initial) % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS ill PI61 K 14.('a K c in i 2nd TARE Wt (g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) Dry Wt Diff (final -initial) 3F, c3Zb D 41) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3'•c 36•c,56o e (7.0 SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt Tare WT Diff (g) (flg) 0,g LJl-J33 111. 3•3 1st Dry Wt (g) 2nd Dry Wt (g) tt'2711g' Dry Wt Diff (final -initial) % TOT SOLIDS a, ,LI WB512 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) D 1st Ignition Wt (g) �1. 11� 1 Ignite Wt Diff 2nd Ignition Wt (g) (final -initial) G' % VOL SOLIDS Analyst: 8 F Date: Loi3°12I Recorded By: Vve, ncSdc,,,pu11,tt"3 SAMPLE Oeo1L)21-v! SANV PLE SAM SA WB512 PLE 10PLE PERCT T TOTAL SOLIDS / PERCENT VOLATILE SOLIDS // SM 2540 B-2011 1st Clean IN 550°C lst Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C g USED lyIAD g USED -1-014 14)141S tp. opI g USED 111..850 g USED I .7'17.5 DISH # DISH # T DISH # 9z DISH # 1.I C A 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (AO .0002 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 59 . 6p'-F5 io 2nd TARE Wt (g) 59.co` 5u Tare WT Diff (oe) 0 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 46- 3t...01r4 3 2nd TARE Wt (g) Tare WT Diff (AO (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) L11. "i -189 2nd TARE Wt (g) 1.ri489 Tare WT Diff (Ag) Y' (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) B - A x 100 = % TOTAL SOLIDS C B -D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C 1st Dry Wt (g) Li _R5 32 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS D 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1st Dry Wt (g) )1r 2nd Dry Wt (g) �_71"54t. Dry Wt Diff (final -initial) c % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1st Dry Wt (g) 3-2123 2nd Dry Wt (g) '3; 21 2 D Dry Wt Diff (final -initial) % TOT SOLIDS 7 -7 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS .36.1LIILI `k12,0L; e i.LO 1st Dry Wt (g) 01 gee' 2nd Dry Wt (g) Dry Wt Diff (final -initial) 0 % TOT SOLIDS Q 4 %0 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS / 01 7. 141-717-5 • G Ci,47 Analyst: {SCr Date: 71712 I Recorded By: PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample 1N 104°C 2nd Sample OUT 104°C B - A x 100 = % TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (4g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 0(f%11re: 1----01 Kinn C . t332 I'53c),, 0 as, .' fly av . g.33t4 0 r) (n[6 (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS . I lr 5 & r,, r I (tP)5 0 Via. Li la^ SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (6g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS _ is,a?"x {4 16g - D.oa-r 2 xot 0 3 .339 a 30, ...3a(75 oo Lc S- a, (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3a . (0(-I' 2)Q . gL 3 0 _ r) ILkt-I SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (4g) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS ' I> Clabi o- 1 ,Q)0. 627 . a),k1 0 5.8RaP w. "'n n o .1f (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) VOL SOLIDS TThy o Q O t�� S jMjLE " g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff gig) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS JJ j 4 .77 WB512 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) D 1st Ignition Wt (g) 2nd Ignition Wt (g)}} Ignite Wt Diff (final -initial) % VOL SOLIDS i5. CnCri . , q CI(37 0 ()IL to Analyst: Nt) Date:�t Recorded By: MIL PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B} 011 hpirid 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C SAMPLE g USED DISH # C 1st TARE WT. (g) :74_0 L1I.25i SAMPLE g USED DISH # 1st TAI (I 1)-1N Mc' 2-Z 37,u' S� WB512 MPLE g USED 11.1.` 2nd TARE Wt (g) A Tare WT Diff (ac) C3 13� I B - A x 100 = % TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C 1st Dry Wt (g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) E WT, 2nd TARE Wt (g) 6.3 37- 114163 Tare WT Diff (❑g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff' (ng) i 2 ,► 3ivg "3q. 36S e (initial ignition 550°C for 1 hour) (repeat iginition 550°C far I hour) lst TARE WT. (g) IL( 372318 2nd TARE Wt (g) 37.230 g Tare WT Diff 00 0 37 35 VI lst Ignition Wt (g) 1.)[,2)Zo- 1st DryWt(g) 3 /3c 8 2nd Dry Wt (g) uy egg D 2nd Ignition Wt (g) 2nd Dry Wt (g) 3'7• (icy Dry Wt Diff (final -initial) Ignite Wt Diff (final -initial) Dry Wt Diff (final -initial) % TOT SOLIDS % VOL SOLIDS % TOT SOLIDS 0 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) %VOL SOLIDS 'c.lJZ 1.- 5 0 -50 L 37-52Jg-77-/- . 0 lst Dry Wt (g) '3611 1/6 % TOT SOLIDS 2nd Dry Wt (g) Dry Wt Diff (final -initial) 1st Ignition Wt (g) 31.90a 1st Dry Wt (g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 2nd Ignition Wt (g) 341- 9 clo 2nd Dry Wt (g) Ignite Wt Diff (final -initiai) t'v Dry Wt Diff (final-initiai) 0 VOL SOLIDS Vo TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 371gT5 37., 2 g 75 C 0,.43 5-9.2016 Chain of Custody Record (COC) NPDES#: Client: EMA Resources inc. Phone:336-753.-1�}�F1 MERITECH l INC. Address: 755 Yadkinville Rd Fax: 336-751-1442 ENVIRONMENTAL LABORATORIES Mocksville NC 27028 Email: brent.collins@emaresourcesinc.com 642 Tamco Rd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: ' Email: info@meritechlabs.com Attention:_ Brent Collins Turn Around Time* *RUSH How would you like your report sent? work needs prior approval. w echlabs.com www.meritechlabs.com Std IOda s) 3 s 2a_42Hrs .meri4} Circle all that apply: 1��referred) , Fax, Mail Sampling Dates & Times Person Taking Sample (Sign/Print): f� /� f0,1l Lab Use Only Sample Location and/or ID # Start End On Ice? pH OK? Date Time Date Time crab? Cont. Test(s) Required Yes / No Cl OK? 1.,chrvv it c 6,//v /0:35" ".. C ! 3' 13(2', ,3«c4 0 7 Temperature Upon Receipt: Method of *** Dechiorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Shipment: Comments: fj c..�/'!fw /lei /2/e,r4 ,T,7,o+/ cd e-,/..��, sic. Compositor # L❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes II ---- No ❑ Report results in: mg/L ❑ mg/kg L ug/L ❑ ❑ Hand Delivery Relinquished by: deff.Date:/,V Time: //.oso., Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: ReceiV a J /li qte: i i ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: City of Danville Northside WWTP WQ Permit Number: WQ0036561 NPDES Number: VA0060593 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) • Alt B (Alk Treatment) ■ Alt. C (Prior Testing) ■ A1t.D (No Prior Test) 0 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray • Ganuna Ray • Pasteurization • Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ I Ei If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization • Air Drying • Composting • Aerobic Digestion • Anaerobic Digestion • If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number of Excee- deuces Frequency of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 217 296 435 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ■ Alt. 2 (40-day bench) • Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) • Alt. 5 (14-Day Aerobic) ■ Alt. 6 (Alk. Stabilization II 7 (Drying -Stable) ■ Alt. 8 (Drying - Unstable) MI Alt. 9 (Injection) • Alt. 10 (Incorporation) ■ No vector attraction reduction alternatives were performed • CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Gregory Ryland - Regional Manager Preparer Name and Title (type or print) Gregor6,� 0V /ai. /VG/MG(T) Feb 9, 2022 Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) 2/6/2022 Date DENR FORM PVRF 02T (12/2006) (eAnaIYticaI vw.p�tlehsen www.pacelabs.cam May 07, 2021 Mr. Robert Clifton INFRAMARK 229 NORTHSIDE DR Danville, VA 24540 RE: Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Dear Mr. Clifton: Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - WestVirginia • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Stacy Heasley stacy.heasley@pacelabs.com 800-999-0105 Project Manager Enclosures cc: Ms. Kimberly Wickemeyer, INFRAMARK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 11 (eAnaIYtica/ e www.pacelabs.com CERTIFICATIONS Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Pace Analytical Services Beaver 225 Industrial Park Drive, Beaver, WV 25813 Virginia VELAP 460148 West Virginia DEP 060 West Virginia DHHR 00412CM North Carolina DEQ 466 Kentucky Wastewater Certification KY90039 Pennsylvania DEP 68-00839 Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 11 (eAnaIYtica/ e www.pacelabs.com SAMPLE SUMMARY Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Matrix Date Collected Date Received 7368940001 CATWALK Al #7 Solid 04/27/21 07:40 04/27/21 11:51 7368940002 CATWALK A2 #1 Solid 04/27/21 07:05 04/27/21 11:51 7368940003 CATWALK A3 #6 Solid 04/27/21 07:35 04/27/21 11:51 7368940004 CATWALK A4 #3 Solid 04/27/21 07:15 04/27/21 11:51 7368940005 CATWALK A5 #5 Solid 04/27/21 07:30 04/27/21 11:51 7368940006 CATWALK A6 #4 Solid 04/27/21 07:20 04/27/21 11:51 7368940007 CATWALK A2 #2 Solid 04/27/21 07:10 04/27/21 11:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 11 (eAnaIYtica/ e www.paeelabs.enm SAMPLE ANALYTE COUNT Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Method Analytes Analysts Reported Laboratory 7368940001 CATWALK Al #7 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940002 CATWALK A2 #1 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940003 CATWALK A3 #6 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940004 CATWALK A4 #3 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940005 CATWALK A5 #5 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940006 CATWALK A6 #4 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7368940007 CATWALK A2 #2 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV PASI-BVWV = Pace Analytical Services - WestVirginia PASI-LX = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 11 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK Al #7 Lab ID: 7368940001 Collected: 04/27/21 07:40 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <238 CFU/g 239 0.239 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.8 % 0.10 1 04/29/21 09:23 Sample: CATWALK A2 #1 Lab ID: 7368940002 Collected: 04/27/21 07:05 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <435 CFU/g 435 0.435 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.7 % 0.10 1 04/29/21 09:24 Sample: CATWALK A3 #6 Lab ID: 7368940003 Collected: 04/27/21 07:35 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <222 CFU/g 223 0.223 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.5 % 0.10 1 04/29/21 09:24 Sample: CATWALK A4 #3 Lab ID: 7368940004 Collected: 04/27/21 07:15 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <385 CFU/g 385 0.385 04/27/21 17:45 04/28/21 16:15 REPORT OF LABORATORY ANALYSIS Date: 05/07/2021 04:28 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 11 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK A4 #3 Lab ID: 7368940004 Collected: 04/27/21 07:15 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.4 % 0.10 1 04/29/21 09:25 Sample: CATWALK A5 #5 Lab ID: 7368940005 Collected: 04/27/21 07:30 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <217 CFU/g 218 0.218 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.4 % 0.10 1 04/29/21 09:26 Sample: CATWALK A6 #4 Lab ID: 7368940006 Collected: 04/27/21 07:20 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <250 CFU/g 250 0.25 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 96.0 % 0.10 1 04/29/21 09:27 Sample: CATWALK A2 #2 Lab ID: 7368940007 Collected: 04/27/21 07:10 Received: 04/27/21 11:51 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <417 CFU/g 417 0.417 04/27/21 17:45 04/28/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.6 % 0.10 1 04/29/21 09:27 REPORT OF LABORATORY ANALYSIS Date: 05/07/2021 04:28 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 11 (eAnaIYtica/ e www.pacelabs.com QUALIFIERS Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS Date: 05/07/2021 04:28 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 11 (eAnaIYtica/ e www.paeelabs.enm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK - DANVILLE Pace Project No.: 7368940 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 7368940001 CATWALK Al #7 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940002 CATWALK A2 #1 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940003 CATWALK A3 #6 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940004 CATWALK A4 #3 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940005 CATWALK A5 #5 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940006 CATWALK A6 #4 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940007 CATWALK A2 #2 SM 9222D - 2006 66861 SM 9222D - 2006 66862 7368940001 CATWALK Al #7 SM 2540G-11 66831 7368940002 CATWALK A2 #1 SM 2540G-11 66831 7368940003 CATWALK A3 #6 SM 2540G-11 66831 7368940004 CATWALK A4 #3 SM 2540G-11 66831 7368940005 CATWALK A5 #5 SM 2540G-11 66831 7368940006 CATWALK A6 #4 SM 2540G-11 66831 7368940007 CATWALK A2 #2 SM 2540G-11 66831 REPORT OF LABORATORY ANALYSIS Date: 05/07/2021 04:28 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 11 CHAIN -OF -CUSTODY Analytical Request Document LAB USE ONLY- Affix Workorder/Login Label Here or List Pace Workorder Number or MTIL Log -in Number Here ace Analytical Chain-of-CustodylsaLEGAL DOCUMENT- Completeallreleventffelds . Company: Inframark-Danville Billing Information: Inframark-Danville WWTP WO# �/�� • 3 8 r Address: Dr., Danville, VA 24540 2 229 Northside Contz 111 1 III II l 1111111 229 Northside Danville, VA 24540 2 2 11111 Rep°Pero:Rebert.Clifton@Inframark.com EmailT°: Stephanie.Mosko@Inframark.com "`FreservativeType (6) methanol, (7) sodi:.. 736894(d )zinc acetate, um sulfate, Copy To: Site Collection Info/Address: (C) ammonium hydroxide, (D) TSA, (U) Unpreserved, (0) Other Kimberly.Wickemeyer@Inframark.com Danville VA WWTP 229 Norlhside, Dr., Danville, VA 24540 Analyses Lab Profile/Line: Customer Project Name/Number: Inframark-Danville (client#: 92-618203) State: County/City: Time Zone Collected: VA /Danville [ ]PT( ]MT( ]CT VET Ammonia (NH3-N) Nitrate+Nitrite (NO3-N + NO2-N) Total Phosphorus BOD TSS Oil & Grease Fecal Coliform Lab Sample Receipt Checklist: Custody Seals Present/Intact Y W Phone:434.799-5137 Email: zentm iy.wickemeyer@lnframark.com Site/Facility ID #: Danville, VA WWTP permit VA0060593 Compliance Monitoring? [ 1Yes [ ] No Custody signatures Present 0 N DA Collector Signature Prevent Ky NIA Bottles Intact ION NA Collected By (print): Clifton Purchase Order #: 120019 Quote It: 00091909 DW PWS ID #: ❑W Location Code: Correct Bottles NA. d Sufficient volume . NA Samples Received on Ice N NA Col e i na r l��C. Turnaround Date Required: � �� 512OG� Immediately Packed on Ice: . / [nYes [ ] No VOA' - Reads ace Acceptable V t. NA t p - Sang Regulated Soils N i'rri Samples in Holding Time \ NP. Sample Disposal: 161 Dispose as appropriate [ l Return Rush: 1 ] Same Day [ ] Next Day Field Filtered (if applicable): [ ] Yes [i/] No Residual Chlorine Present _ N NA Cl Strips: ] I Archive: [ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day Sample pH Acceptable Y N t1A Analysis: pH Strips: t IHold. (Expedite Charges Apply) Sulfide Present i hr NA * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Lead Acetate Strips: Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), other (OTJ _ LAB USE ONLY Customer Sample ID Matrix * Comp/ Grab Collected (or Composite Start) Composite End Res CI #of Ctns Z p Ca ❑ Q Lab Sample # / Comments: Date Time Date Time [— Li] 0 Catwalk Al #7 SL Grab 04/27/21 co"%ilD - - - - - - •° - No 1 Catwalk A2 #1 SL* Grab 04/27/21 CVRS - - -- - - -- No 1 Catwalk A3 #6 SL* Grab 04/27/21 07_33 - - - - - - - - NO 1 CatwalkalA4 #3 SL* Grab 04/27/21 07L5 - - - - - - - - No 1 Catwalk A5 #5 SL* Grab 04/27/21 0730 - - - - - - - - No 1 X catwalk A6 #4 SL* Grab 04/27/21 07A..0 - - - - - - - - No 1 X Catwalk A2 #2 SL* Grab 04/27/21 07/0 - - -- - - -- No 1 Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: Blue Dry None SHORT HOLDS PRESENT (<72 hours): ON N/A Lab Sample Temperature Info: ......1.....) Packing Material Used: Lab Tracking #: Temp Blank Received: Y N f A Therm IN: LX f r'Z4 `Diosolids for Fecal Caliform Cooler 1 Temp Upon Receipt: 3 , g oC Bottles: 150 mL Sterile for microbic ogy Samples received vla: Cooler 1 Therm Corr. Factor:'d'r7 oC plastic Radchem sample(s) screened (<500 cpm): Y N NA FEDEX UPS Courier Pace Courier Cooler 1 Corrected Temp: 3 • oC Relinquished by/Company: (Signature) Date/Time: f } y/� Received by/Company: (Signature) Date/Time: MTJL LAB USE ONLY Comments: // �..A �Y %/ ut a Table 4: l�r/�rn'f �•7((2.4 LraG`'�" i ts1 IISf Acctnum: Relinquished b ompa y: (Signature) Date/Time: f l "(—GO—H �� Received by/Company: (Signature) ^-1 J Date/Time: t/-2.a-2/ r G Template: Preiogin: Trip Blank Received: Y N NA p HCL Me0H TSP Other Re quished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM: Non Conformance{s): Page: Page 9 of 11 -----/-.-? _, r, /��' 28 -2lr f 7 PB- YES / NO of: 1 slLr LIMS73 Lab Sample Condition Upon Receipt (West Vi .. PaceAnalytical Client Name: Courier: ❑ Fed Ex ❑ UPS ❑ USPS Client ❑ Commercial ❑ Pace Tracking #: Custody Seal on Cooler/Box/Containers Present: ❑ yes no Thermometer Used t.k1 h _q Type of Ice: Cooler Temperature Observed Temp 3 • 3t Comments: y WO# : 7368940 PM: SOH Due Date: 05/07/21 CLIENT: INFRAMARK Blue Seals intact: ❑ yes ❑ no None C Correction Factor: — Q• 7 o C Final Temp: ) r "C pH paper Lot# Date and Initials of person examining contents: Yes No NIA Chain of Custody Present: 7 1. Chain of Custody Filled Out: ! 2. Chain of Custody Relinquished: / 3. Sampler Name & Signature on COC: 4. Sample Labels match COC: -Includes dateltime/ID Matrix: .i 5. SL Samples Arrived within Hold Time: / 6. Short Hold Time Analysis (<72hr remaining): ,7/ 7. Rush Turn Around Time Requested: / 8. Sufficient Volume: % 9. Correct Containers Used: -Pace Containers Used: 7' 10. Containers Intact: 7' 11. Orthophosphate field filtered: .7 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) 13. Filtered volume received for Dissolved tests: f 14. All containers have been checked far preservation: exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix All containers meet method preservation requirements: 15. f / initial when completed Dateltime sampl1` I / L1 provided to lab ! `27 dr/ Tests not preserved: Headspace in VOA Vials: % 16. Trip Blank Present: Trip Blank Custody Seals Present: % 17. Initial when feo -IDate: 1-1completed: (~ 2-,/ Client Notification) Resolution: Person Contacted: Comments/ Resolution: Date/Time: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. `PM review is documented electronically in LIMS, when the Proect Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. 0 0 SCUR VdV-rev.082219 w CD m 0 INERAMARK Vendor Pace Analytical Services, LLC Phone: 504-469-0333 Contact: Contact EmaII: Bill To: 229 Northside Drive Danville Virginia 24540 United States Purchase Order PO#: Date: Buyer Name: Buyer Email: End User Email: End User Phone: Payment Terms: Ship To: 229 Northside Drive Danville Virginia 24540 United States 120019 4/23/2021 Anjelina Munoz anjelina.munoz(&inframark.com kimberly.wickemeyeq@inframark.com 434-799-5137 Net 30 Attn: Kimberly Wickemeyer 1 SIR00012 DANVILLE 7 Ea 6/15/2021 $42.00 $294.00 Description: Fecal Coliform, Biosolids Line ID 2 SIR00012 Project DANVILLE Qty 1 nits Ea Expected Delivery Date Rate 6/15/2021 $5.00 Amount $5.00 Description: Environmental Impact Fee Total $299.00 1 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 .45/ Contact: Brent Collins Report Date: 8/3/2021 Client EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 6/22/2021 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 06222142 Sample: Danville Composite 6/22/21 Total Solids Volatile Solids % Volatile Solids Week 1 0.860 0.430 0.506 Week 2 0.890 0.510 0.569 Week 3 1.29 0.710 0.554 Week 4 1.05 0.550 0.527 Week 5 0.790 0.420 0.529 Van Kleek Reduction (%): -9.80 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 rt LJ1'1�1 1vittL WJi,,LY, JL 1� SM 2540 B-2011 Analyst: Ay p Date: 6 CL9. Recorded By: SAMPLE 0a2z2/-Lz SAMPLE WB512 SAMPLE SAMPLE G rdi lst Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C g USED g USED g USED 314 g USED DISH # u•2 DISH # DISH # S•0_ DISH # C A 1st TARE WT. (g) 1-1131? 2nd TARE Wt (g) 211•1-J.1LI Tare WT Diff (Ag) (initial ignition 550°C far 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2t4°1 2nd TARE Wt (g) Tare WT Diff (Ag) C' (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) lst TARE WT. (g) 1Z-51431 2nd TARE Wt (g) 9.2-11.31 Tare WT Diff (Ag) 0 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) lst TARE WT. (g) 2r.“2T 2nd TARE Wt (g) B - A x 100 = % TOTAL SOLIDS C B - D x 100 w % VOLATILE SOLIDS C 1st Sample IN 550°C lst Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C 1st Dry Wt (g) u 3 O 2nd Dry Wt (g) 21/:• 30 Dry Wt Diff (final -initial) q % TOT SOLIDS �• g3 latIgnition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS VI. if tlo 21-1071l G 0,213 Tare WT Diff (Ae) C (initial ignition 550°C far 1 hour) (repeat iginition 550°C for 1 hour) 1st Dry Wt (g) 2nd Dry Wt (g) 21. -F3 r 3 D Dry Wt Dlff (final -initial) 0 % TOT SOLIDS tat Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 21-G-FO 71-((,S)24 c, 0-1,1Li 1st Dry Wt (g) 22- 610 2nd Dry Wt (g) 6169 Dry Wt Diff (final -initial) TOT SOLIDS i.'-1 7 1st Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS Ignition ((]] 27-Goo 6 n 22,60(/6(.,'(Y413. 1st Dry Wt (g) 2nd Dry Wt (g) 21: L1(4 5 Dry Wt Diff (final -initial) c % TOT SOLIDS T 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 7).. 2go g 1 - 72 g 0 t? d, q SM 2540 B-2011 Analyst:�7 Date: 7 1 Recorded By: 1st Clean IN 550°C 2nd Clean IN 550°C B - A x 100 = % TOTAL SOLIDS C 1st Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS 2nd Clean OUT 550°C C 1st Sample IN 550°C 1st Sample OUT 550°C C 2nd Sample IN 550°C 2nd Sample OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C A 1st TARE WT. 2nd TARE Wt Tare WT Diff Dry Wt Diff SAMPLE g USED DISH # (g) (g) (Ag) 1st Dry Wt (g) 2nd Dry Wt (g) (final -initial) % TOT SOLIDS OC 2221-H Z l .ig2; 3-Z uo- fq-1G 0o.17- _ 0 tio.3C g5 1.10,30g5 G , (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) D 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -Initial) % VOL SOLIDS Gi9_23 15 ito.2315 0 0 ,5O SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (AM 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS I);.l)/7 0,0 110.274Z CIc_27g2„ c. 110. aq3 5 a0.1i!n 5 0 I .,91 (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1Io-3g- 7-0 'U0 '3S70 0 ' 0:10 SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Agi 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1'' 2i ?4 Tie 111.2060 141a-i gc, c uf,3g61-1 r) �31 0 _ :.1 CM (initial ignition 550°C for 1 hour) (repeat iginition 550°C for I hour) 0 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS til` 3©96 t(1, 615 0 0, 6a. .' SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt MT (final-lnitial) % TOT SOLIDS 1 -// 191 till' '53c 1111 5%30 o Zie-I,,Dg32 ale'. 6e3 2_ i o Q,q(n WB5 12 (initial ignition 550°C for 1 hour) (repent iginition 550°C for 1 hour) 1) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS IN. 60 Cal a u. 606q 0 r i Analyst: Nih SM 254013-2011 B - A x 100 = % TOTAL SOLIDS Date: '1{ L _ Recorded By: Foil oii 3 1st Clean IN 550°C 2nd Clean IN 550°C 1st Clean OUT 550°C 2nd Clean OUT 550°C lst Sample IN 104°C 8 1st Sample OUT 104°C q 2nd Sample IN 104°C (0 2nd Sample OUT 104°CJ I C B -D x 100=%VOLATILE SOLIDS C lst Sample IN 550°C lst Sample OUT 550°C `c , 2nd Sample IN 550°C 3 2nd Sample OUT 550°C SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (t,g) _ 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 0C2221-U2 )'6.WWoo g.) 21.6610 21-6G3o a 0t.8378 ,Q4;°g37g 0 I (5 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) Ignitionn Wt (g) Ignite Wt Diff (final -initial) % VOL/SOLIDS r7 Gi. U r�2nd 2/ V3[. 0 �S /G1 SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (81) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS )5, q2 6.2 21.3q92 21.31 ?2_ a c 1. Gov( P. (C.00,s I © ) ,'3(a (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (Gnat -initial) % VOL SOLIDS SAMPLE g USED DISH # Ist TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) _ lot Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (Final -initial) % 'I'01SOLIDS I _l°lo 3,) 211.oq 1 24-0171 0 ail,3077 ,‘I 307`7 0 1,3 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) D lst Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOi, SOLIDS 2U1i I� •( 7,1l.f1 15 . a 0.76 SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS '15 t344 a° 21-el Z 21.252e 0 Q(. Lis (0 at, t.,13;(0 o 1, ( ) WB512 (Initial ignition 550°C for 1 hour) (repeat iginition S50°C for 1 hour) D 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 2r_3) �5 C 2 SM 254013-2011 Analyst: _ • )3 /A/) ) Its B - A x 100 = % TOTAL SOLIDS Date: -fir f; C Recorded By: 77'1 I i � lst Clean MI 550°C 1st Clean OUT 550°C B - D x 100 = %VOLATILE SOLIDS 2nd Clean IN 550°C 2nd Clean OUT 550°C C 1\ 1st Sample IN 104°C 1st Sample OUT 104°C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample 1N 550°C 2nd Sample OUT 550°C C A g SAMPLE g USED DISH# 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff • (tls) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS G22l t1 L I)-]`/rnO /1- ?g.Mol -3V . faa 0 3V, 55 ?4 Vt) 0 _. JIL i 5' (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS S MPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (As) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS fti•g1gd. i-G 3q-o�3'3 31-06 3 e 3c1.216,i- 3"1.72-47- o 1;1 (initial ignition 551E°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignitinn Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS SAMPLE, g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Agi 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1 .W470.2-0 LI1.13 o LI/1,, e 0 la- 2gPi WI. 2SilI 6, 1,03 (initial ignition 550°C for 1 hour) (repeat iginition 550°C far 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite WI Diff (final -initial) % VOL SOLIDS 2-11. 2 ur n 2 ft� i SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS l/ ILI-923 q- 36t:3° c 31-MC' C 3-1-'u311 3q< q3tt _ WB512 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite WI Diff (final -initial) % VOL SOLIDS 3�-zIC2� �E2 o i t,; .i, Analyst: Pin PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS 5M 2540 B-2011/ r Date: Ii t tut 5 Recorded By: j 4 I 1 ) SAMPLE o(22'2.I_'U2 Ist Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (AO lko tdl5 116 3g-1 0 02 3 . got/ o (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) B - A x 100 = %TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C 1st Dry Wt (g) •3S. l 2nd Dry Wt (g) 32A1 46 3S•lI 'i Dry WtDiff (final -initial) % TOT SOLIDS 1st Ignition Wt (g) 2n�d Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS { SA LE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (dg) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) °f° TOT SOLIDS [0.70R U-ci `3V6 3 37- g‘--,3 c 3 Tq771 3 7.4771 c (,. f( 5A� ''SAMPLE WB512 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT, (g) 2nd TARE Wt (g) 2-? 37--ZI'Sc! Tare WT Diff (AO (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) L(C)-1O3 bra-7163 (Initial ignition 550°C for 1 hour) (repeat ignnition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3741 g'3 317:11 S'; c 0- u C 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 37:5514 37-552C c r,t1l2, 1st Dry Wt (g) 2nd Dry Wt (g) D Dry Wt Diff (Iinnl-initial) % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite WtDiff (final -initial) % VOL SOLIDS -Io,Yzl 07- go-gi4 g7 c "i,`:U11;i 5-9-201G Chain of Custody Record (COC) Client: Address: Resources Inc. 755 755 Yadkinville Rd Mocksville NC 27028 NPDES#: i ' + ME ENVIRONMENTAL 642 Talmo Reidsville NC Email: www.meritechaabs.com R I T E Rd. 27320 info@meritechlabs.com C LABORATORIES Phone: Fax: H INC. 1 336-342-4748 336-342-1522 Phone: Fax: 336-751-1441 336-751-1442 brent.coilins@emaresourcesinc.com Email: Project: P.O.#: Attention:_ Brent Collins Turn Around Time* *RUSH work needs prior approval, How would you like your report sent? Circle allthatapply: 1 11 preferred] , Fax, Mall Sld(lodays) 3-5 Days 111 If—�I 1_4-4gHrs sample Location and/or ID # Sampling Dates &Times p Person Taking Sample (Sign/Print): tad ',7S Lab Use Only Start End comp? Grab? #of Cont. Test(s) Required es Ice? Yes / No pH OK? CIO e Date Time Date Time �, ,�4nv:Ite- £/Z2 /0:14„., e I 3o bnr 4,04 4:7,-$ Fsv,, L , Temperature Upon Receipt: AVj� ✓ ! Method of Shipment: *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: ,,7fr.rre se.;W G',r/e,.4,44.s ,sileeA k►/ /era /f Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg EI ug/L ❑ ❑ Hand Delivery Relinquished by: Date: Time: au_ /0,-5,36.4. Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rect gd by Lab: 1, `.22 ( Date: Time: I n 0 cvli ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: City of Danville Northside WWTP WQ Permit Number: WQ0036561 NPDES Number: VA0060593 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) • Alt B (Alk Treatment) ■ Alt. C (Prior Testing) ■ A1t.D (No Prior Test) 0 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray • Ganuna Ray • Pasteurization • Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ I Ei If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization • Air Drying • Composting • Aerobic Digestion • Anaerobic Digestion • If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 244 363 625 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ■ Alt. 2 (40-day bench) • Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) • Alt. 5 (14-Day Aerobic) ■ Alt. 6 (Alk. Stabilization II 7 (Drying -Stable) ■ Alt. 8 (Drying - Unstable) MI Alt. 9 (Injection) • Alt. 10 (Incorporation) ■ No vector attraction reduction alternatives were performed • CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Gregory Ryland - Regional Manager Preparer Name and Title (type or print) GAY A 0V Al (FebRy and /VG/MG(Grego13:55 T) Signature of Preparer* Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) Feb 9, 2022 2/6/2022 Date Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) (eAnaIYticaI vw.p�tlehsen www.pacelabs.cam May 17, 2021 Mr. Robert Clifton INFRAMARK 229 NORTHSIDE DR Danville, VA 24540 RE: Project: DANVILLE (CLIENT#92-618203) Pace Project No.: 7370679 Dear Mr. Clifton: Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Enclosed are the analytical results for sample(s) received by the laboratory on May 10, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - WestVirginia • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Stacy Heasley stacy.heasley@pacelabs.com 800-999-0105 Project Manager Enclosures cc: Ms. Kimberly Wickemeyer, INFRAMARK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 (eAnaIYtica/ e www.pacelabs.com CERTIFICATIONS Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Pace Analytical Services Beaver 225 Industrial Park Drive, Beaver, WV 25813 Virginia VELAP 460148 West Virginia DEP 060 West Virginia DHHR 00412CM North Carolina DEQ 466 Kentucky Wastewater Certification KY90039 Pennsylvania DEP 68-00839 Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 (eAnaIYtica/ e www.pacelabs.com SAMPLE SUMMARY Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Matrix Date Collected Date Received 7370679001 CATWALK Al #7 Solid 05/10/21 08:30 05/10/21 13:17 7370679002 CATWALK A2 #1 Solid 05/10/21 07:55 05/10/21 13:17 7370679003 CATWALK A3 #6 Solid 05/10/21 08:25 05/10/21 13:17 7370679004 CATWALK A4 #3 Solid 05/10/21 08:05 05/10/21 13:17 7370679005 CATWALK A5 #5 Solid 05/10/21 08:20 05/10/21 13:17 7370679006 CATWALK A6 #4 Solid 05/10/21 08:10 05/10/21 13:17 7370679007 CATWALK A2 #2 Solid 05/10/21 08:00 05/10/21 13:17 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 (eAnaIYtica/ e www.paeelabs.enm SAMPLE ANALYTE COUNT Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Method Analytes Analysts Reported Laboratory 7370679001 CATWALK Al #7 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679002 CATWALK A2 #1 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679003 CATWALK A3 #6 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679004 CATWALK A4 #3 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679005 CATWALK A5 #5 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679006 CATWALK A6 #4 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7370679007 CATWALK A2 #2 SM 9222D - 2006 MJV 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV PASI-BVWV = Pace Analytical Services - WestVirginia PASI-LX = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK Al #7 Lab ID: 7370679001 Collected: 05/10/21 08:30 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <256 CFU/g 257 0.257 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 96.1 % 0.10 1 05/12/21 08:54 Sample: CATWALK A2 #1 Lab ID: 7370679002 Collected: 05/10/21 07:55 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <476 CFU/g 477 0.477 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.9 % 0.10 1 05/12/21 08:55 Sample: CATWALK A3 #6 Lab ID: 7370679003 Collected: 05/10/21 08:25 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <244 CFU/g 244 0.244 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.9 % 0.10 1 05/12/21 08:57 Sample: CATWALK A4 #3 Lab ID: 7370679004 Collected: 05/10/21 08:05 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <625 CFU/g 625 0.625 05/10/21 17:25 05/11/21 15:45 REPORT OF LABORATORY ANALYSIS Date: 05/17/2021 03:30 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 12 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK A4 #3 Lab ID: 7370679004 Collected: 05/10/21 08:05 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 98.4 % 0.10 1 05/12/21 08:57 Sample: CATWALK A5 #5 Lab ID: 7370679005 Collected: 05/10/21 08:20 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <250 CFU/g 250 0.25 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 96.0 % 0.10 1 05/12/21 08:58 Sample: CATWALK A6 #4 Lab ID: 7370679006 Collected: 05/10/21 08:10 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <286 CFU/g 286 0.286 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 96.5 % 0.10 1 05/12/21 08:59 Sample: CATWALK A2 #2 Lab ID: 7370679007 Collected: 05/10/21 08:00 Received: 05/10/21 13:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <625 CFU/g 625 0.625 05/10/21 17:25 05/11/21 15:45 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 98.4 % 0.10 1 05/12/21 09:00 REPORT OF LABORATORY ANALYSIS Date: 05/17/2021 03:30 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 12 (eAnaIYtica/ e www.pacelabs.com QUALIFIERS Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS Date: 05/17/2021 03:30 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 12 (eAnaIYtica/ e www.paeelabs.enm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: DANVILLE (CLIENT #92-618203) Pace Project No.: 7370679 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 7370679001 CATWALK Al #7 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679002 CATWALK A2 #1 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679003 CATWALK A3 #6 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679004 CATWALK A4 #3 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679005 CATWALK A5 #5 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679006 CATWALK A6 #4 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679007 CATWALK A2 #2 SM 9222D - 2006 68579 SM 9222D - 2006 68581 7370679001 CATWALK Al #7 SM 2540G-11 68331 7370679002 CATWALK A2 #1 SM 2540G-11 68331 7370679003 CATWALK A3 #6 SM 2540G-11 68331 7370679004 CATWALK A4 #3 SM 2540G-11 68331 7370679005 CATWALK A5 #5 SM 2540G-11 68331 7370679006 CATWALK A6 #4 SM 2540G-11 68331 7370679007 CATWALK A2 #2 SM 2540G-11 68331 REPORT OF LABORATORY ANALYSIS Date: 05/17/2021 03:30 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 12 CHAIN -OF -CUSTODY Analytical Request Document Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields Company: Inframark-Danville Address: 229 Northside Dr., Danville, VA 24540 Billing Information: Inframark-Danville WWTP 229 Northside Drive Danville, VA 24540 LAB USE ONLY- Affix Workorder/Login Label Here or Llst Pace Workortler Number or Container Report To: Robert.Clifton@Infrarnark.com Copy To: Kimberly.Wickemeyer@Inframark.com 2 1 2 1 2 i 2 WO#:7370679 I 1 IIII II IIIIIIIIIIIIIII Email To: Stephanie.Mosko©Inframark.com •* Preservative Types: (1) nu,, " , , „_, _...c acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, Site Collection Info/Address: (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other Danville VA WWTP 229 Northside, Dr., Danville, VA 24540 Customer Pro)ect Name/Number: Inframark-Danville (client #: 92-618203) State: County/City: Time Zone Collected: VA /Danville [ ]PT[ IMT[ ]CT ryfET Analyses ab Profile/Line: Phone: 434-799-5137 Email: klmberly.wickemeyerginrramark.com Site/Facility ID #: Danville, VA WWTP permit VA0060593 Compliance Monitoring? [ iJYes [ ] No Collected By (print): Robert Clifton Purchase Order #: 120625 Quote #: 00091909 Co cted By /igna Sample Disposal: (11 Dispose as appropriate ( J Return ] I Archive: I 1 Hold: Turnaround Date Required: 05/24/2021 Rush: [ ] Same Day [ ] Next Day [ ]2Day [ ]3Day [ ]4Day [ ]5Day (Expedite Charges Apply) DW PWS ID #: OW Location Code: Immediately Packed on Ice: [IYes [ ] No Field Filtered (if applicable): [ ]Yes V No Analysis: Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (W W), Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix * Catwalk Al #7 SL* Catwalk A2 #f sL* Comp / Collected (or Grab Composite Start) Composite End Date Grab 05/10/21 Grab 05/10/21 Time Date 041,3t ---- ip7 -- Res CI Time - _-- No -- No # of Ctns 1 Ammonia (NH3-N) Nitrate+Nitrite cn 2 Total Phosph 0 W E O O LL Lab sample Receipt Checllist: Custody Seals Present/intact Y N NA Custody Signatures Pres,ant Y N NA Collector Signature Present Y N NA Bottles Intact i N NA Correct Bottles Y N NA Sufficient Volume Y N NA Samples Received on tce Y N NA VOA - Headspace Acrepteo.le Y N NA USDA Regulated Soils Y N NA Samples in Holding, Time 't N NA Residual Chlorine Presort Y N NA Cl Strips: Sample pH Acceptable - Y N NA pH Strips; Sulfide Present Y N NA Load Acetate Strips: LAM USE ONLY: Lab Sample 4 / Comment.,: Catwalk A3 #6 sL Catwalk A4 #3 sLy Catwalk A5 #5 sL* Catwalk A6 #4 sL* Catwalk A2 #2 sLk Grab G5/10/21 Grab 05/10/21 Grab 05/10/21 Grab 05/10/21 Grab 05/10/2 0101-6 0-30 No N No No No 1 X Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: et' Blue Dry None SHORT HOLDS PRESENT (<72 hours): N NIA Packing Material Used: `Biosolids for Fecal Coliform Bottles: 150 mL Sterile plastic for microbiology Radchem sample(s) screened (<500 corn); Lab Tracking #: N NA Samples received via: FEDEX UPS ie Courier Pace Courier Relinquished by/Company: (Signature) 7/40ed#,°1,10RX Relinquished 5 /Company: (Signature) Relinquished by/ m : (Signature) Date/Time: Date/Time: 4. t'°_e.) Date/Time: 5/lZ//r7.56. Received by/Company: (Signature) Received by/Company: (Signature) —27 Received by/Company: (Signature) Date/Time: l6. L Date/Time: 5./l-zr Date/Time: 3t �+ MTJL LAB USE ONLY Table #: Acctnum: Template: Prelogin: PM: P8: Lab Sample Temperature Info: Temp Blank Received: Y N NA Therm ID#:/ Cooler 1 Temp Upon Receipt: oC Cooler 1 Therm Corr. Factor: 0,-7 oC Cooler 1 Corrected Temp: ©, oC Comments: Trip Blank Received: Y N NA HCL McOH TSP Other Non Conformance(s): YES / NO Page: y oT IL of: LIMS73 Lab Sample Condition Upon Receipt (West Virginiz Wofl : 7370679 E. a;;BAnatyt. Client Name: N 0 PM: SDH Due Date: 05/20/218, h�iGr*- c `41.4-1.1 CLIENT: INFRAMARK Courier: ❑ Fed Ex ❑ UPS ❑ USPS /1 Client ❑ Commercial ❑ Pace ❑ Other: Tracking #: Custody Seal on Cooler/Box/Containers Present: ❑ yes o Thermometer Used /xI;,M 2-4 Cooler Temperature Observed Temp Comments: (- Q Seals intact: ❑ yes ❑ no Type of Ice: Wet Blue None C Correction Factor — 0- % °C Final Temple pH paper Lot# Date and Initials of person examining contents: Yes No NIA Chain of Custody Present: V. 1. Chain of Custody Filled Out: ' 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COC: % 4, Sample Labels match COC: -Includes dateltimelld Matrix: /" 5. SL Samples Arrived within Hold Time: 6. Short Hold Time Analysis (<72hr remaining): 7. Rush Turn Around Time Requested: t 8. Sufficient Volume: -/ 9. Correct Containers Used: -Pace Containers Used: 10. f Containers Intact: V 11. Orthophosphate field filtered: / 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) / 13. Filtered volume received for Dissolved tests: 14. All containers have been checked for preservation: exceptions: VOA, coliform, O&G. LLMercury, Non -aqueous matrix All containers meet method preservation requirements: f 15. / / Init al when completed J Date/time samples provided to 3ab S / ci-2-4? /3/ 7 Tests not preserved: Headspace in VOA Vials: % 16. Trip Blank Present: Trip Blank Custody Seals Present: % 17. Initial when completed: Date: J'//-Z/ Client Notification) Resolution: Person Contacted: Comments/ Resolution: Dateffime: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in MIS. The status may be reviewed in the Status section of the Workorder Edit Screen. SCUR WV- rev.082219 N FRAMARK Vendor Pace Analytical Services, LLC Phone:504-469-0333 Contact: Contact Email: Bill To: 229 Northside Drive Danville Virginia 24540 United States Purchase Order PO#: Date: End User Email: End User Phone: Payment Terms: Ship To: 229 Northside Drive Danville Virginia 24540 United States 120625 5/6/2021 kmberly.wickemeyerainframark.com 434-799-5137 Net 30 Attn: Kimberly Wickemeyer Expected Delivery. 1 SIR00012 DANVILLE 7 Ea 6/15/2021 $42.00 $294.00 Description: Fecal Conform, Biosolids Line ID Project Units Expected Delivery Date 2 SIR00012 DANVILLE 1 Ea 6/15/2021 $5,00 $5.00 Description: Environmental Impact Fee Total $299.00 1 of2 6LNFRA ARK Vendor Pace Analytical Services, LLC Phone: 504-469-0333 Contact: Contact Email: Purchase Order PO#: Date: 120625 5/6/2021 End User Email: kimberly.wickemeyer@inframark.com End User Phone: 434-799-5137 Payment Terms: Net 30 All packing lists and proofs of delivery must be sent to receiving@inframark.com within 48 hours of delivery. Please reference the PO number above on all documentation. Inframark, LLC General Conditions of Purchase, a copy of which is available at https://www.inframark.com/contact-us/doing-business- with-us/ , and any specific conditions or other terms not included in these General Conditions of Purchase that are mutually agreed upon in writing (herein after "Specific Conditions") shall govern this Purchase Order. In the event of a conflict between any Specific Conditions noted in the Purchase Order and the General Conditions of Purchase, the Specific Conditions shall control. At terms and conditions included in any Supplier documentation are specifically rejected by Purchaser and shall be of no effect on this Purchase Order. Please reference this Purchase Order number on all shipping and billing documents related to this order. Vendor Acceptance: Date: 2 of 2 alk Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: 9/15/2021 Date Sample Revd: 8/6/2021 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 08062102 Sample: Danville Composite 8/6/21 Total Solids Volatile Solids % Volatile Solids Week 1 1.16 0.550 0.470 Week 2 1.15 0.550 0.482 Week 3 0.980 0.470 0.485 Week 4 0.890 0.420 0.468 Week 5 0.940 0.420 0.445 Van Kleek Reduction (%): 9.62 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 Analyst: /VD ur_PAL 1 rri'�tJ Date: S, j Recorded By: 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample 1N 104°C 2nd Sample OUT 104°C B _ A x 100 = % TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE g USEDD DISH # 1st TARE WT. (g) 2nd TARE Wt (g)/f Tare WT Diff 1st Dry Wt� (g) Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS _ !�11 ((']]�� ////,�,, r/'� l!i/t1/lV tr tr©1 -( I s`/ ��j( ) If 1.211'O - ,yry L` V � /((A) Y J(� - ,J 1. u3 I �2,%nd1Dry .1 -"1). ,a(`-,..' (initial ignition 550°C for I hour) (repeat Iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignitiion Wt (g) Ignite W t Diff (final -initial) % VOL SOLIDS 3q ?/,al1 3q,3511 Q 0,5,5- SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (tag) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS I5:0g56 1- g tiF-023 a 247--0Z3( 0 1I7-1ct o OF-116.0 c I- , ( (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition WI (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS u 1111Z 117'1)07 a 01/!' SA LE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Agl Ist Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS �'-18� MZN' �f3n��g213 •��I�2 v �13-�� did 01' (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS , 6 u3�.(5 °9 cl3, ' a9 0,t SAMPLE g USED DISH # Ist TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ctg) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS YI k5noACig ‘'? 31i^(D O r 39.6°71 0 31.7F' 2 `I 31 78'11 o 1417 ;. , ': WB516 71 (initial ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 39. 0 9 3':6195 o .,,N Analyst: NI) Date; C(f 2 Recorded By: PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 pi.((1 Z 1st Clean IN 550°C 1st Clean DUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C B - A x 100 = % TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C A 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (!Is) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLID a F06 1,- on iu./ T 505 110-036g /lo.?3a1 0 1114,2107 ell. 09a 7. o SAMPLE g USED Ia. d354 DISH 27 (Initial ignition 550°C for 1 hour) (repeat Iginition 550°C for 1 hour) Ist TARE WT. (g) 2nd TARE Wt (g) 3e, g;1 Tare WT Dlff (fig) C; (initial Ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL S ID //0.CW 3'7 V G• q g 31 0 0\.j. ist Dry Wt (g) • 3(-13o5 2nd Dry Wt (g) -3`1 I3a Dry Wt Diff (final -initial) 0 % TOT SOLID 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLID 3',ot429 39.oZ1Z c ;0.5 SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WTDiff (As) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLID 15A i 3I 3 3. 1 a3 9'Z3 / 1-1,. `123i-/ 0 uu. O 9 ? u u!-o925 a (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) Ist Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLID tat OIIq Obi-orrq 6 WB516 SAMPLE g USED '5.27/# DISH it .15 1st TARE WT. (g) -113I1-1 2nd TARE Wt (g) / t It f)-I Tare WT Diff (AO) c (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st DryWt(g) UM- 'G fir; 2nd Dry Wt (g) D Dry Wt Diff (final -initial) C % TOT SOLID 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite WI Diff (final -initial) % VOL SOLID ■a — ow ow low owl Elm ......,ot 1st TARE WT. 2nd TAIL SAMPLE g USED DISH if (g) (g) c. OC21,-02- )54)r15 2'6 3'?.V5aA 3j.E5 LE g USED DISH M Analyst: ,v() Date: F Z�'� r Recorded By: i eel�3 PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 s lst Clean IN 550°C 2nd Clean IN 550°C 1st Clean OUT 550°C 2nd Clean OUT 550°C lst Sample IN 104°C lst Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C C A B Wt Tare WT Diff (ag) 1st Dry Wt (g) u c .3. 2o (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) SAN 2nd TARE Wt (g) Tare WT Diff (As) 2nd Dry Wt (g) 31. 7.020 B - A x 100 = % TOTAL SOLIDS C 13 - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C Dry Wt Diff (final -initial) TOT SOLIDS lst Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Dili (final -initial) % VOL SOLIDS 3,-.6297 3q,6297 _ e 0,14 1st Dry Wt (g) •00" Q c) 3 0, 15 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (ag) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) Si.MPLE g USED DISH tt 1st TARE WT. (g) 2nd V I5,15JJ 4,3 q 3 ..`12 2 3 L/ WB516 TARE Wt (g) Tare WT Diff (as) LtLI -01 15 (initial ignition 550°C for 1 hour) (repeat Iginition 550°C for 1 hour) 1st Ignition Wt (g) 3.Uo 1st Dry Wt (g) 2nd DryWt(g) D Dry Wt Diff (final -initial) Ignite Wt Diff 2nd Ignition Wt (g) (final -Initial) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS % VOL SOLIDS tad-° ' % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3'1,0 3 G 34?. O 3 gc 6 c Ist Dry Wt (g) 2nd Dry Wt (g) Dry WI Diff (final -initial) % TOT SOLIDS V G q Is( Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VO SO\ S /I14-WO 3 41Li•o00 °3 C 0- ' 1 Analyst: AID Date: 91 3 Recorded By: PERCENT TOTAL SOLIDS / PERC�T.+ NT VOLATILE SOLIDS SM 2S4O -011 it_ Li rr(tatr, 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C f B - A x 100 = % TOTAL SOLIDS C B -Dx 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE o`6G61/ C)? g USED DISH # 1st TARE WT. (g) 2.Li U1.13P5 2nd TARE Wt (g) t1.13 -) Tare WT Diff (og) 0 1st Dry Wt (g) L1L2614e 2nd Dry Wt (g) Dry Wt Diff (final -Initial) 0 % TOT SOLIDS (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS IV-2o 65 /4/-2o 6 ca 0-3q . SAMPLE g USED - /7 DISH tt /vIo I\ 1st TARE WT. (g) U Z • L79-q6 2nd TARE Wt (g) Tare WT Diff (Ag) 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS r5-10 61 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT, (g) 2nd TAME Wt (g) Tare WT Diff (As) (initial ignition 550°C for 1 hour) (repeat Iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 142- 6 30 LI2-- 613c 0 ' t 1st Dry Wt (g) 2nd Dry Wt (g) • Dry Wt Diff (final-Initiai) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) yy % VOL S a I1� . Li3,qd60 43 `7`?6d c, okl,o 1 N. SAMPLE g USED DISH # 1st TARE WT. (g) 2 37. L/(2r 2nd TARE Wt (g) Tare WT Diff (asi 377. //c156 0 1st Dry Wt (g) u 16 2nd Dry Wt (g) 3?.511�G Dry Wt Diff (final-lnitl I) TOT SOLIDS WB516 (initial ignition 550°C for 1 Hour) (repeal iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 37.V7614 371 u. C adia Analyst: ND Date: 91 I Q Recorded By: PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS wec 5 SM 2540 B-2011 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT I04°C 2nd Sample IN 104°C 2nd Sample OUT 104°C B - A x 100 = %° TOTAL SOLIDS c B - D x 100 = % VOLATILE SOLIDS C I st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C II SAMPLE g USED 1 — 1st TARE WT. DISH # (g)++11 2nd TARE Wt (g) 153 $9 3?.)('L15 Tare WT Diff (de) 0 Ist Dry Wt (g) 2nd Dry Wt (g) 3:''SU3. Dry Wt Diff (final -initial) G % TOT SOLIDS 0,02 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) ist Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS .AMPLE g USED DISH 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (bg} 1st Dry Wt (g) -urZ3 2nd Dry Wt (g) LI.L 23: .. Dry Wt Diff (final -initial) % TOT SOLIDS (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 0' 30 6r 1-11. 3 g 5 67 alli, SAMPLE g USED DISH # 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (oei 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff ((root -initial) % TOT SOLIDS SAMPLE WB516 g USED DISH # 15.2852 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) 3 Tare WT Diff (AO (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SODS UU'065 U�.d.0 00.I6 Ist Dry Wt (g) 6,0 2nd Dry Wt (g) 6611 Dry Wt Diff (final -initial) 0 TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 3_> II 3 I c 0a 5.9.ZD1fi Chain of Custody Record (COC) NPDES#: Client: Resources Inc. Phone: 336-751-1441 ME R fTE C H l INC. Address:755 Yadkinville Rd Fax: 336-751-1442 ENVIRONMENTAL LABORATORIES _755 Mocksvllle NC 27028 Email: brent.collins@Zemaresourcesinc.com 642 Tamco Rd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritechlabs.com Attention:_ Brent Collins Turn Around Time* *RUSH How would you like your report sent? work needs prior approval. WWW.f71eCl#echlabS.com Ereferred), 5td soda s) 3-5 Days 24-48►Irs Circle all that appl j Fax, Mail Sampling Dates & Times Person Taking Sample (Sign/Print}: /OwU fa `As Lab Use Only Sample Location and/or ID # Start End comp? #of On Ice? pH OK? Date Time Date Time Grab? Cont. Test s Required Yes / No CI OK? 'o n.11 It t C42 7 50,„,,, e / 3c, 1 a y �,�.7c Li Q.s he v, n.,-1 0 Temperature Upon Receipt: Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Shipment: Comments: rt'j,, aF ?/tacr.e trim Lya/c•�l,f.,w.q s"-1•r,s-r''1 t..../ l J Compositor # p ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes P' No ❑ Report results in: mg/L ❑ mg/kg ffr ug/L ❑ n Hand Delivery Relinquished by: Date: Time: �f(p ;i?'�a o-,,� Received by: Date: Time: Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Re " ed ab:. c f f _ 3e� C s ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: City of Danville Northside WWTP WQ Permit Number: WQ0036561 NPDES Number: VA0060593 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) • Alt B (Alk Treatment) ■ Alt. C (Prior Testing) ■ A1t.D (No Prior Test) 0 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray • Ganuna Ray • Pasteurization • Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ Ei If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization • Air Drying • Composting • Aerobic Digestion • Anaerobic Digestion • If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number of Excee- deuces Frequency of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1754 4192 94000 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ■ Alt. 2 (40-day bench) ■ Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) • Alt. 5 (14-Day Aerobic) ■ Alt. 6 (Alk. Stabilization II 7 (Drying -Stable) ■ Alt. 8 (Drying - Unstable) MI Alt. 9 (Injection) • Alt. 10 (Incorporation) ■ No vector attraction reduction alternatives were performed • CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Gregory Ryland - Regional Manager Preparer Name and Title (type or print) GAY A 0V Al (FebRy and /VG/MG(Grego13:55 T) Signature of Preparer* Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) Feb 9, 2022 2/6/2022 Date Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) (eAnaIYticaI vw.p�tlehsen www.pacelabs.cam June 04, 2021 Mr. Robert Clifton INFRAMARK 229 NORTHSIDE DR Danville, VA 24540 RE: Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Dear Mr. Clifton: Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Enclosed are the analytical results for sample(s) received by the laboratory on May 24, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - WestVirginia • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Stacy Heasley stacy.heasley@pacelabs.com 800-999-0105 Project Manager Enclosures cc: Ms. Kimberly Wickemeyer, INFRAMARK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 (eAnaIYtica/ e www.pacelabs.com CERTIFICATIONS Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Pace Analytical Services Beaver 225 Industrial Park Drive, Beaver, WV 25813 Virginia VELAP 460148 West Virginia DEP 060 West Virginia DHHR 00412CM North Carolina DEQ 466 Kentucky Wastewater Certification KY90039 Pennsylvania DEP 68-00839 Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 (eAnaIYtica/ e www.pacelabs.com SAMPLE SUMMARY Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Matrix Date Collected Date Received 7372432001 CATWALK Al #7 Solid 05/24/21 08:05 05/24/21 12:25 7372432002 CATWALK A2 #1 Solid 05/24/21 07:30 05/24/21 12:25 7372432003 CATWALK A3 #6 Solid 05/24/21 08:00 05/24/21 12:25 7372432004 CATWALK A4 #3 Solid 05/24/21 07:40 05/24/21 12:25 7372432005 CATWALK A5 #5 Solid 05/24/21 07:55 05/24/21 12:25 7372432006 CATWALK A6 #4 Solid 05/24/21 07:45 05/24/21 12:25 7372432007 CATWALK A2 #2 Solid 05/24/21 07:35 05/24/21 12:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 (eAnaIYtica/ e www.paeelabs.enm SAMPLE ANALYTE COUNT Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID Method Analytes Analysts Reported Laboratory 7372432001 CATWALK Al #7 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432002 CATWALK A2 #1 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432003 CATWALK A3 #6 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432004 CATWALK A4 #3 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432005 CATWALK A5 #5 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432006 CATWALK A6 #4 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV 7372432007 CATWALK A2 #2 SM 9222D - 2006 JCD 1 PASI-LX SM 2540G-11 KRP 1 PASI-BVWV PASI-BVWV = Pace Analytical Services - WestVirginia PASI-LX = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK Al #7 Lab ID: 7372432001 Collected: 05/24/21 08:05 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <1961 CFU/g 1960 1.961 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 94.9 % 0.10 1 05/25/21 15:27 Sample: CATWALK A2 #1 Lab ID: 7372432002 Collected: 05/24/21 07:30 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <4167 CFU/g 4170 4.167 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.6 % 0.10 1 05/25/21 15:28 Sample: CATWALK A3 #6 Lab ID: 7372432003 Collected: 05/24/21 08:00 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <1754 CFU/g 1760 1.755 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 94.3 % 0.10 1 05/25/21 15:29 Sample: CATWALK A4 #3 Lab ID: 7372432004 Collected: 05/24/21 07:40 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <2381 CFU/g 2380 2.381 05/24/21 15:50 05/25/21 16:15 REPORT OF LABORATORY ANALYSIS Date: 06/04/2021 03:36 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 10 (eAnaIYtica/ e www.pacelabs.com ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Sample: CATWALK A4 #3 Lab ID: 7372432004 Collected: 05/24/21 07:40 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.8 % 0.10 1 05/25/21 15:30 Sample: CATWALK A5 #5 Lab ID: 7372432005 Collected: 05/24/21 07:55 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms 94000 CFU/g 2000 2 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.0 % 0.10 1 05/25/21 15:31 Sample: CATWALK A6 #4 Lab ID: 7372432006 Collected: 05/24/21 07:45 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <2128 CFU/g 2130 2.128 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 95.3 % 0.10 1 05/25/21 15:31 Sample: CATWALK A2 #2 Lab ID: 7372432007 Collected: 05/24/21 07:35 Received: 05/24/21 12:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006 Pace Analytical Services - Lexington Fecal Coliforms <3333 CFU/g 3330 3.334 05/24/21 15:50 05/25/21 16:15 Percent Moisture Analytical Method: SM 2540G-11 Pace Analytical Services - WestVirginia Percent Moisture 97.0 % 0.10 1 05/25/21 15:32 REPORT OF LABORATORY ANALYSIS Date: 06/04/2021 03:36 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 (eAnaIYtica/ e www.pacelabs.com QUALIFIERS Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS Date: 06/04/2021 03:36 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 10 (eAnaIYtica/ e www.paeelabs.enm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK-DANVILLE (92-618203) Pace Project No.: 7372432 Pace Analytical Services, LLC 225 Industrial Park RD Beaver, WV 25813 (800)999-0105 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 7372432001 CATWALK Al #7 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432002 CATWALK A2 #1 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432003 CATWALK A3 #6 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432004 CATWALK A4 #3 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432005 CATWALK A5 #5 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432006 CATWALK A6 #4 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432007 CATWALK A2 #2 SM 9222D - 2006 70821 SM 9222D - 2006 70822 7372432001 CATWALK Al #7 SM 2540G-11 70183 7372432002 CATWALK A2 #1 SM 2540G-11 70183 7372432003 CATWALK A3 #6 SM 2540G-11 70183 7372432004 CATWALK A4 #3 SM 2540G-11 70183 7372432005 CATWALK A5 #5 SM 2540G-11 70183 7372432006 CATWALK A6 #4 SM 2540G-11 70183 7372432007 CATWALK A2 #2 SM 2540G-11 70183 REPORT OF LABORATORY ANALYSIS Date: 06/04/2021 03:36 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 aceAnalytical CHAIN -OF -CUSTODY Analytical Request Document Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields e Billing Information: Inframark-Danville WWTP nville, VA 24540 229 Northside Drive Danville, VA 24540 Company: Inframark-Danville Address: 229 Northside Dr., Da Report To: Robert.Clifton@Inframark.com Copy To: Kimberly.Wickemeyer@Inframark.com Customer Project Name/Number: Inframark-Danville (client #: 92-618203) Email To: Stephanie.Mosko@Inframark.com Site Collection Info/Address: Danville VA WWTP 229 Northside, Dr., Danville, VA 24540 State: County/City: Time Zone Collected: VA /Danville [ jPT[ ]MT[ ICI VET Phone: 434-799-5137 Email: Kimberly.wickemeyer@inframark.com Collected By (print): Robert Clifton Site/Facility ID #: Compliance Monitoring? Danville, VA WWTP permit VA0060593 [ keYes [ ] No Cc)4ec ed By (signature): Sample Disp al: Dispose as appropriate [ ] Return [ ] Archive: [ ] Hold: Purchase Order#: Quote #: 00091909 a 1 Turnaround1 Date 0Required: 06/ 121 DW PWS ID #: DW Location Code: Immediately Packed on Ice: [Yes [ ] No Rush: [ ] Same Day [ j Next Day [ ] 2 Day [ ] 3 Day [ j 4 Day [ ] 5 Day (Expedite Charges Apply) Field Filtered (if applicable): [ ] Yes 1/1 No Analysis: * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID -Catwalk Al #7 Catwalk A2 #1 Catwalk A3 #6 Catwalk A4 #3 Catwalk A5 #5 Catwalk A6 #4 Catwalk A2 #2 Matrix * SL* SL* SL* SL* SL* SL* SL* Comp / Grab Grab Grab Grab Grab Grab Grab Grab Customer Remarks / Special Conditions / Possible Hazards: *Biosolids for Fecal Coliform Bottles: 150 mL Sterile plastic for microbio Ogy Radchem sample(s) screened (<500 cpm): Y N NA Collected (or Compos to Start) Composite End Date 05/24/21 05/24/21 05/24/21 05/24/21 05/24/21 05/24/21 05/24/21 Time o8o5 D730 0800 o740 0755 0745 0735 Date Time Res CI No No No WOtt:7372432 71111,72432 IIII III IIIIIIIIIII III ** Preservative Types: (1) nitric acid, (2) sulfuric acid, O hydiochonaciu, (4) sooium Pydroxr e, (5) Zirc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other _ # of Ctns , No 1 No 1 No No Type of Ice Used: We Blue Dry Packing Material Used: 1 1 None Relinquished by/Company: (Signature) Date/Time: Received by/C mpany: (Signature) etv- Relinquished by/Company: (Signature) Date/Time: 2elinquished by/Company: (Signature) Received by/Company: (Signature) Ana yses cJ 0 Z I + i fA Z '. 0 a To cf) 0 O co Z:F-1Go F- 1 )SHORT HOLDS PRESENT (<72 hours Lab Tracking #: Samples received via: FEDEX UPS Che Date/Time: Date/Time: /22 Date/Time: Received by/Company: (Signature) Date/Time: 0 0 cp LL Courier Pace Courier MTJL LAB USE ONLY Table #: 'Acctnum: Template: IPrelogin: PM: IPB: Lab Sample Temperature Info: Temp Blank Received: Y N NA Therm ID#: Lkl, 1 2 t/ Cooler 1 Temp Upon Receipt: 2 , ebC Cooler 1 Therm Corr. Factor:^ 0.1ZC Cooler 1 Corrected Temp: i - 2 oC Comments: Trip Blank Received: Y N NA HCL McOH TSP Other Non Conformance(s): Page: YES / NO of: 1 WO#:7372432 Thermometer Used Cooler Temperature Comments: LIMS73 Lab Sample Condition Upon Receipt (West Virginia aceAnalytical Client Name: reel% •••‘1,414. Courier: ❑ Fed Ex ❑ UPS ❑ USPS Client ❑ Commercial ❑ Pace ❑ Other: Tracking #: Custody Seal on Cooler/Box/Containers Present: ❑ yes ,,,rno Type of Ice: L k?M tH PM: SDH Due Date: 06/04/21 CLIENT: INFRAMARK Seals intact: ❑ yes ❑ no Blue None Observed Temp 3 . 0 ° C Correction Factor: - 0.7 ° C Final Temp: 2.3 °C IpH paper Lot# Date and Initials of person examining I contents: Yes No N/A Chain of Custody Present: Chain of Custody Filled Out: Chain of Custody Relinquished: Sampler Name & Signature on COC: Sample Labels match COC: -Includes date/time/ID Matrix: SL Samples Arrived within Hold Time: Short Hold Time Analysis (<72hr remaining): Rush Turn Around Time Requested: Sufficient Volume: 2. 3. 4. 5. 6. 7. 8. 9. Correct Containers Used: -Pace Containers Used: 7 10. Containers Intact: 11. Orthophosphate field filtered: Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (If yes, indicate acid lot #) Filtered volume received for Dissolved tests: 12. 13. All containers have been checked for preservation: exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous mat ix All containers meet method preservation requirements: 14. 15. '/ Initial when completed) �J (provided Date/time samples to lab �- 4; r 12 Zr Tests not preserved: Headspace in VOA Vials: 16. Trip Blank Present: Trip Blank Custody Seals Present: Client Notification/ Resolution: Person Contacted: Comments/ Resolution: 17. Initial when /� completed: VJ J 'Date: s-' 214' Z1 Date/Time: Contacted By: ❑ A check in this box indicates that additional information has been stored in ereports. *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. SCUR_WV - rev.08 10 of 10 At* Contact: Brent Collins Client EMA Resources, Inc 755 YadkinvilIe Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: 9/27/2021 Date Sample Revd: 8/24/2021 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 08242105 Sample: Danville 2 Composite 8/24/21 Total Solids Volatile Solids % Volatile Solids Week 1 1.35 0.660 0.488 Week 2 1.37 0.690 0.505 Week 3 1.26 0.630 0.500 Week 4 1.14 0.570 0.503 Week 5 0.980 0.480 0.493 Van Kleek Reduction (a/o): -2.27 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass %)dtrtt„&a d-hrkact. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 Analyst: j/l) Date: Recorded By: p (( I 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample rN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C 13 - A x 100 = % TOTAL SOLIDS C I3 - D x 100 = % VOLATILE SOLIDS C lst Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE g USED DISH # o 6 at(z r_ ©, 5 Novi. le I5,75 60 1st TARE WT. (g) 2tJ-2273 2nd TARE Wt (g) Tare WT Diff (As) 1st Dry Wt (g) 2U-2273 0 ZZ -43iu 2nd Dry Wt (g) 2,t1.k31 i Dry Wt Diff (final -initial) % TOT SOLIDS SA PLE MPLE W13516 g USED DISH # g USED 1'S:o33'5 g USED DISH # DISH # (initial ignition 550°C for 1 hour) (repeat lginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (AO (initial ignition 550°C for 1 hour) (repeat iginition 550°C for I hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) (initial ignition 550°C for 1 hour) (repeat'ginition 550°C far 1 hour) 1st TARE WT. (g) 2z.16611 2nd TARE Wt (g) 2 L- 1 bqq Tare WT Diff (Ag) C (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 21-1.3 17$ Z •31; 0 ;a,71 1 1st Dry Wt (g) 2?-0 7-?2- 2nd Dry Wt (g) Dry Wt Diff (final -initial) 0 TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS Z1• 95 79 .2 .` 5 __o 4v 1st Dry Wt (g) Zi-YCt?Q 2nd Dry Wt (g) Zi. 0 Dry Wt Diff (final -initial) % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 2I,7)Q 9 4. 1c9 G:646 Dry Wt Diff (final -initial) 22-37 'I D TOT SOLIDS lst Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 22sU 21,27E D 0, PERCENT TOTAL SOLIDS / PERCENT VOLATII SOLIDS SM 2540 B-2011 Analyst: WI) Date: 131 Recorded By: lst Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C C A B - A x 100 = % TOTAL SOLIDS C I3 - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C lst Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C SAMPLE g USED DISH # 0 "zll 2-I- or.; P014v11? ? 1 ,30� 1st TARE WT. (g) cI.? 31,543- 2nd TARE Wt (g) Tare WT Diff (Ag) 36?.5243 . 0 1st Dry Wt (g) 3'7•7 13 2nd Dry Wt (g) JL753 Dry Wt Diff (final -initial) % TOT SOLIDS SAN; I, G PLE S4 MVMPLE WB516 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff Oh) (initial Ignition 550°C for I hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT Diff (Ag) (initial ignition 550°C for 1 hour) (repeat iginition 5S0°C for I hour) 1st TARE WT. (g) 2nd TARE Wt (g) Tare WT DIff (Ag) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 3Ll 1 •7 .7 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 34,6A .39.6.53 0 _ ..„ _ '°. 1st Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt DIIf (final -initial) % VOL SOLIDS 410_71-60 0o 2/60. o o. 7 1st Dry Wt (g) 2nd Dry Wt (g) Dry WtDiff (final -initial) TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1st Dry Wt (g) 2nd Dry Wt (g) D TOT SOLIDS lst Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1 Analyst: Date: Retarded By: SAMPLE Zil lI - o %DanV\ le 2 WB516 1st Sample IN 104°C lst Sample OUT 104°C 2nd Sample IN 104°C 2nd Sample OUT 104°C g USED Itt-6:S ++}}gUSED f . DISH # DISH # 1st TARE WT. (g) 2nd TARE Wt (g) SM 2540 B-2011 v"."-- 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) 2nd TARE Wt (g) 3'1_5111- (initial ignition 550°C for 1 hour) (repeat iginition 559°C for 1 hour) 1st TARE WT. 2nd TARE Wt DISH # (g) (g) IL.R' g USED .13 j 3,-1Lt i-1 LI3,92-i (initial ignition 550°C for 1 hour) (repeat Iginition 550°C for 1 hour) 2nd TARE Wt (g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) A 1st Sample IN 550°C 2nd Sample IN 550°C B-A x 100 = %TOTAL SOLIDS C B - D x 100 = % VOLATILE SOLIDS 1st Dry Wt (g) Lid- 7-95 1st Ignition Wt(g) 1st Dry Wt (g) 1st Ignition Wt (g) 44/4 4133 1st Ignition Wt (g) 11•01 1 1st Dry Wt (g) 1st Ignition Wt (g) 31;-35 1st Sample OUT 550°C 2nd Sample OUT 550°C 2nd Dry Wt (g) D 2nd Ignition Wt (g) 2nd Dry Wt (g) 2nd Ignition Wt (g) 2nd Dry Wt(g) Dry Wt Diff (final -initial) Ignite Wt Diff (final -initial) Dry Wt Diff (final -Initial) Ignite D [f (final -initial) % TOT SOLIDS % VOL SOLIDS % TOT SOLIDS % VOL SOLIDS % TOT SOLIDS 2nd Ignition Wt (g) 2nd Dry Wt (g) Dry Wt (final -Initial) Ignite Wt Diff (final -initial) Dry Wt Diff (final -initial) Ignite WtD ff (final -initial) % VOL SOLIDS % TOT SOLIDS % VOL SOLIDS Analyst: AIl} Date: ql Recorded By: SAMPLE PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT 104°C 2nd Sample 1N 104°C 2nd Sample OUT 104°C g USED DISH # 0 ?U'21_05 Azov,` ! 2 15. '53 SA PLE C 1st TARE WT. (g) a. 3T.30; g USED DISH # 1' =3143S 2nd TARE Wt (g) A Tare WT Diff (Ag) 3?3e3 0 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) u- r truly 277 SAMPLE g USED DLSH # 15 S MPLE WB516 g USED lea-3303 DISH # 4 2nd TARE Wt (g) Tare WT Diff (AO 0 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 2nd TARE Wt (g) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TAKE WT. (g) '3 Qin 2nd TARE Wt (g) Tare WT Diff (as) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Sample IN 550°C 2nd Sample IN 550°C 1st Dry Wt (g) 1st Ignition Wt (g) 3e_cr6 q@ 1st Dry Wt (g) LILT . o33 B - A x 100 = % TOTAL SOLIDS C B-Dx100=%VOLATILE SOLIDS C lst Sample OUT 550°C 2nd Sample OUT 550°C 2nd Dry Wt (g) Dry Wt Diff (Gnat -initial) TOT SOLIDS 1'13 2nd Ignition Wt (g) 2nd Dry Wt (g) �r' u 033 Ignite Wt Diff (£nai -initial) Dry Wt Diff (final.initiai) 0 VOL SOLIDS % TOT SOLIDS 114 1st Ignition Wt (g) OIL :7-161g. I. 2nd Ignition Wt (g) zrr -71ti Ignite Wt Diff (final -initial) 0 VOL SOLIDS 047 lst Dry Wt (g) 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS 1st Ignittion Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1 uo.E5. l5 3z_ u o B 3Z G fi 1st Dry Wt (g) 2nd Dry Wt (g) 3-19 1st Ignitian Wt (g) 3g-1037- 2nd Ignition Wt (g) 3 R. (o 3 Dry Wt Diff (final -initial) Ignite Wt Diff (final -initial) VD TOT SOLIDS %° VOL SOLIDS Analyst: �C Date: 1/Li Recorded By: PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 1st Clean IN 550°C 1st Clean OUT 550°C 2nd Clean IN 550°C 2nd Clean OUT 550°C 1st Sample IN 104°C 1st Sample OUT I04°C 2nd Sample IN 104°C 2nd Sample OUT 104°C SAMPLE c zj —95 '/CciL, Zr g USED l 1-1,13 DISH # z.� C A 1st TARE WT. (g) 33-.5OU 2nd TARE Wt (g) -6.50zz B-A x 100 = %TOTAL SOLIDS C - D x 100 = % VOLATILE SOLIDS C 1st Sample IN 550°C 1st Sample OUT 550°C 2nd Sample IN 550°C 2nd Sample OUT 550°C Tare WT Diff (ag) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) SAMPLE SAMPLE SAMPLE WB516 g USED g USED g USED '1..210 DISH # 5 DISH # DISH 15 1st TARE WT. 2nd TARE Wt Tare WT Diff (g) (g) (aal 143.1Z i5 Lf 9L55 (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) Ist TARE WT. (g) 1st Dry Wt (g) 2nd Dry Wt (g) 31- 650, D Dry Wt Diff (final -initial) c TOT SOLIDS 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1st Dry Wt (g) 2nd DryWt(g) Dry Wt Diff (final -initial) 0 % TOT SOLIDS 1st Ignition Wt (g) 2nr1 Ignition Wt (g) Ignite Wt Dlff (fins sinitial) %VOL SOLIDS i13.9 CI 2_ ? u 3 ‘ c62R ((- ` 7 0. 9 2nd TARE Wt (g) jAli ttl.1�I1G Tare WT Diff (As) (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st TARE WT. (g) , -I30 2nd TARE Wt (g) .13.341LB Tare WT Diff (as) .000Z (initial ignition 550°C for 1 hour) (repeat iginition 550°C for 1 hour) 1st Dry Wt (g) 70616 2nd Dry Wt (g) Dry Wt Diff (final -initial) %° TOT SOLIDS 0.99 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS a1,21. ur.z14� 0 O.: 1st Dry Wt (g) U3 M3 2nd Dry Wt (g) Dry Wt Diff (final -initial) % TOT SOLIDS .00.. 1st Ignition Wt (g) 2nd Ignition Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS / 13. L(�!'7 r43, 2475 0 it y 5-9-2016 Chain of Custody Record (COC) NPDES#:. EMA Resources Inc. Phone: 336 751 1441 ME R I T E C H / INC.Client: Address:_ 755 Yadkinville Rd Fax: 336-751-1442 ENVIRONMENTAL LABORATORIES Mocksviile NC 27028 Email: brentcallins@emaresourcesinc,com 642 Tamco Rd. Phone: 336-342-4748 Project: ' , Reidsville NC 27320 Fax: 336-342-1522 P,O,#: Email: info@meritechlabs.com Attention:_ Brent Collins Turn Around Time* *RUSH How would you like your report sent? work needs prior approval. www.meritechlabs.com Circle all that std 1Dda s, 3-.5Days 24-48Hrs apply: (preferred) , Fax, Mail Sample Sampling Dates & Times Person Taking Sample (Sign/print): AnF (. It c/1s Lab Use Only Location and/or ID # Start End Comp? #of Ice? pH OK? D Date Time Date Time Grab? Cont. Test(s) Required es Yes / No CI OK? �, i� 44r4 a. 0'24 ro;15 ( ( , o T3c1.7 r..r•►ct ir.): p eJ1.e.A. (J + Temperature Upon Receipt: Method of *** Dechiorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.*** l ,- 'it Shipment: Comments: lcio4.0-7 _g Compositor # ❑ UPS ?tease snc/ C aw y Jug# • Fed Ex Are these results for regulatory purposes? Yes U' No ❑ Report results in: rng/L ❑ mg/kg ug/L ❑ ❑ Hand Delivery Relinquished by: Date: Ti Fr��Nme: ��; bs Received by: Time: Date: Other Relinquished by: Date: Time: Received by:Date: Time: Relinquished by: Date: Time: e by L 1pat j,t TrQ: G NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL003417 k5i I"14'4+ . via Predictive °± f' Soil Report Mehlich-3 Extraction "'yiii..r' Links to Helpful Information Client: Glen Hodges, Jr. 2388 Allison Rd. Pelham, NC 27311 Sampled County : Caswell Client ID: 523434 Advisor: Brent Collins EMA Resources Inc 755 Yadkinville Rd Mocksville, NC 27028 Advisor ID: 405413 Sampled: Received: 09/02/2021 Completed: 09/13/2021 Farm: CS09 Sample ID: 00003 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 K2O Mg S Mn Zn 0 0 0 0 0 Cu B 0 0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.46 1.10 10.0 91 0.9 6.5 171 136 66 18 S-I 51 Soil Class: Mineral Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-AI 626 385 518 518 Cu-I Na ESP SS -I NO3-N 189 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tolbacci., Truk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL011175 k5 i I"14 - . via Predictive °± f' Soil Report Mehlich-3 Extraction "'y,ii..r' Links to Helpful Information Client: Marc Thomas 730 Old Satterfield Rd. Milton, NC 27305 Sampled County : Caswell Client ID: 523433 Advisor: Brent Collins EMA Resources Inc 755 Yadkinville Rd Mocksville, NC 27028 Advisor ID: 405413 Sampled: Received: 10/25/2021 Completed: 11/08/2021 Farm: CS10 Sample ID: 00001 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tons/acre) N P2O5 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 K2O Mg S Mn Zn 100 0 20 pH$ 0 Cu B 0 0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.36 1.13 10.0 94 0.6 6.8 72 22 63 29 S-I 23 Soil Class: Mineral Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al 911 551 408 408 Cu-I Na ESP SS -I NO3-N 226 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Truk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL003415 k5 i I"14 - . via Predictive °± f' Soil Report Mehlich-3 Extraction "'y,ii..r' Links to Helpful Information Client: Marc Thomas 730 Old Satterfield Rd. Milton, NC 27305 Sampled County : Caswell Client ID: 523433 Advisor: Brent Collins EMA Resources Inc 755 Yadkinville Rd Mocksville, NC 27028 Advisor ID: 405413 Sampled: Received: 09/02/2021 Completed: 09/13/2021 Farm: CS10 Sample ID: 00005 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 K2O Mg S Mn Zn 40 0 0 0 0 Cu B 0 0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.32 1.12 10.2 88 1.2 6.2 322 48 60 25 S-I 59 Soil Class: Mineral Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al 194 130 1120 1120 Cu-I Na ESP SS -I NO3-N 437 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tolbacci., Truk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL003416 k5 i I"14 --- 1• . via Predictive °± f' r Soil Report Mehlich-3 Extraction "'y,ii..r' Links to Helpful Information Client: Client ID: David Sartin 3404 Park Springs Rd Providence, NC 27315 Sampled County : Caswell 347847 Advisor: Brent Collins EMA Resources Inc 755 Yadkinville Rd Mocksville, NC 27028 Advisor ID: 405413 Sampled: Received: 09/02/2021 Completed: 09/13/2021 Farm: CS14 Sample ID: 00001 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 K2O 0 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.27 1.02 12.8 93 0.9 6.5 375 154 64 23 S-I 68 Mn-I 346 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 217 1176 1176 Cu-I 629 Na ESP SS -I NO3-N 0.2 2 Sample ID: 00002 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.0 120-200 120 2 - 0.0 K2O 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.22 1.07 6.0 81 1.2 5.9 11 21 53 26 S-I 34 Mn-I 97 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 75 76 76 Cu-I 145 Na ESP SS -I NO3-N 0.1 2 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Truk fund Cixninlbskm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL003416 David Sartin Page 2 of 3 Sample ID: 00003 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.7 120-200 0 2 - 0.0 K2O 80 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.46 0.93 8.2 80 1.6 5.5 84 31 55 23 S-I 60 Mn-I 248 Soil Class: Mn-AI1 Mn-Al2 166 Mineral Zn-I Zn-AI 462 462 Cu-I 321 Na 0.0 ESP SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL011174 k5 i I"14 --- 1• . via Predictive °± f' :. Soil Report Mehlich-3 Extraction oyiiF.r' Links to Helpful Information Client: Client ID: James Poindexter Etree LLC 9193 McGhees Mill Rd Semora, NC 27343 Sampled County : Person 14303 Advisor: Brent Collins EMA Resources Inc 755 Yadkinville Rd Mocksville, NC 27028 Advisor ID: 405413 Sampled: Received: 10/25/2021 Completed: 11/08/2021 Farm: P502 Sample ID: 00002 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, M 0.7 120-200 0 2 - 0.0 K2O 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.36 1.31 6.6 77 1.5 5.5 92 19 56 19 S-I 59 Mn-I 589 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-Al 370 526 526 Cu-I 207 Na ESP SS -I NO3-N 0.2 3 Sample ID: 00003 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tons/acre) N P2O5 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 K2O 90 Mg S Mn Zn 0 0 pH$ 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% 0.36 1.11 10.4 93 0.7 6.8 82 24 64 29 S-I 26 Mn-I 870 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 528 464 464 Cu-I 236 Na ESP SS -I NO3-N 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tatlariw Truk fund Coininissksn