WQ0003351_2021 Residual Annual Report_20220228

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer EADS\ndthornburg
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0003351
Applicant/Permittee Town of Mocksville
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Brent Collins
Email Address* Phone Number*
[e-mail] 336-399-3646
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0003351
Has Current Existing permit number
Applicant/Permittee Address* 171 Clement Street,Mocksville,NC 27028
Facility Name* Town of Mocksville Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 Mocksville Annual Report-WO0003351.pdf 12.13MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature
ate- -ad
Submission Date 2/28/2022

February 28, 2022
DENR/Water Quality Section
Non-Discharge Compliance Unit
1617 Mail Service Center
Raleigh,NC 27699-1617
Re: 2021 Annual Report-Mocksville
Treatment and Land Application of Residuals
Permit No. WQ0003351
Dear Sir or Madam:
Enclosed is one copy of the 2021 Annual Report for the above referenced land
application permit.
During 2021 EMA Resources, Inc. land applied 29.12 dry tons of wastewater residuals to
23.7 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
[e-mail]

EMA
---Resources, Inc.
Town of Mocksville
2021 Annual Report
Residuals Land Application
Permit No. WQ0003 3 51
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd— Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0003351 County: Davie Year: 2021
Facility Name (as shown on permit): Town of Mocksville
Land Application Operator: EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
Q Yes ❑ No -If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A-Residuals Application Summary:
Total number of application fields in the permit: 10
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 29.12
Total number of acres utilizes for land application during the year: 23.7
Part B-Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. In Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied(if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4) Annual TCLP analysis (if required)was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b)(applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C- Certification:
"I certify, under penalty of law,that the above information is, to the best of my knowledge and belief,true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
6Gtivb/2 Feb 18, 2022
Ken Gamble-Town Manager Ken Gamble(Feb 18,202212:31 EST)
Permittee Name and Title(type or print) Signature of Permittee Date
7MG(ab/2/1-0// Feb 9, 2022 2/8/2022
Todd Robinson(Feb 9,2022 10:00 EST)
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

Pages from 2021 Mocksville Annual Report -
WQ0003351
Final Audit Report 2022-02-18
Created: 2022-02-18
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAmmMEDV-qgJRKnAboJi727E3CZ79AnQDn
"Pages from 2021 Mocksville Annual Report - WQ0003351 " Hist
ory
Document created by Brent Collins ([e-mail])
2022-02-18-3:53:14 PM GMT-IP address:206.85.202.26
P-► Document emailed to Ken Gamble ([e-mail]) for signature
2022-02-18-3:53:41 PM GMT
Email viewed by Ken Gamble ([e-mail])
2022-02-18-5:30:29 PM GMT-IP address:67.213.52.2
Document e-signed by Ken Gamble ([e-mail])
Signature Date:2022-02-18-5:31:07 PM GMT-Time Source:server-IP address:67.213.52.2
Agreement completed.
2022-02-18-5:31:07 PM GMT
Eal Adobe Sign

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF- B
WQ Permit Number: WQ0003351 Laboratory: 1) Waypoint Analytical
Facility Name: Town of Mocksville 2)
Residual Source WQ #or NC0021491 3)
NPDES#: 4)
WWTP Name: Dutchman's Creek WWTP 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit
(mg/kg) (mg/kg)a 2i24i21 8i26i21
Percent Solids (%) NA 1.45 1.1
Arsenic 75 17.1 21.8
Cadmium 85 1.43 1.82
Copper 4,300 148 247
Chromium NA 22.8 38
Lead 840 17.8 16.4
Mercury 57 0.433 0.622
Molybdenum 75 9.64 12.3
Nickel 420 20.3 21.3
Selenium 100 22.9 29.1
Zinc 7,500 351 722
Total Phosphorus NA 18700 25600
TKN NA 40600 60900
Ammonia-Nitrogen NA 13900 12600
Nitrate and Nitrite NA 386 18500
a For surface disposal facilities the ceiling concentration limits listed in this foul'are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
7,ad, /,h/MfOI7 Feb 9 2022
Todd Robinson(Feb 9,2022 10:00 EST)
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102(26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0003351 Laboratory: 1) Waypoint Analytical
Facility Name: Town of Mocksville 2)
Residual Source NC0021491 3)
NPDES# or WQ#: 4)
WWTP Name: Dutchman's Creek WWTP 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg) 2/24/21 8/26/21
Aluminum 18100 22500
Calcium 17700 75200
Potassium 4610 7930
pH 7.9 7.2
Magnesium 2970 6130
Sodium 6590 14000
PAN 15346 39290
SAR 1.45 1.38
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Tcfcf, Db11,1:011 Feb 9, 2022
Todd Robinson(Feb 9,202210:00 EST)
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied(Annual): 19.20
Permit#: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Clarence Rupard Owner: Clarence Rupard Predominant Soil Series: MsB -Mocksville
Acres Used: 15 Acres Permitted: 15 Site #: NC-MK01 Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or I-1 L? L 3 15 1 L L 10 11 12
Corn- 8/26/21
posite
Date
% Solids 1.1
Arsenic 21.8
Cadmium 1.82
Copper 247
Chromium 38
Lead 16.4
Mercury 0.622
Molyb- 12.3
denum
Nickel 21.3
Selenium 29.1
Zinc 722
Total
Phos- 25600
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 L? a 41 u 6 7 I L$ L 9 10 11 112
1-3
DT/Ac./
App. CA
Event 1.28
Arsenic 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Copper 0.632 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.632
Chromium 0.097 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097
Lead 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031
denum
Nickel 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055
Selenium 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074
Zinc 1.848 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.848
Total
Phos- 65.536 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 65.536
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowingg violations".
Z.4.?
1/4/2022
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit#: WQ0003351 Field#: 2 Acres Utilized: 15
Land Owner: Clarence Rupard Annual Dry Tons Applied: 19.20 Site#: NC-MK01 Acres Permitted: 15
Operator: Clarence Rupard Predominant Soil Series: MsB-Mocksville Cation Exchange Capacity(non 503):
Crop 1 Name: Fescue-Pasture Crop 1 Max.PAN: 167 Crop 2 Name: Crop 2 Max.PAN:
Volume applied Volume Residual Sources Soil Precip. a o Z Nitrate Name of Crop Type
p Cond. ; PAN Applied
(enter one)Solids/ % Applied per (NPDES#,WQ#, Past 24 r '� w . r, TKN o and Receiving Residual
a� o wry, - a o (lbs/acre)
c� Liquid Solids Acre Fert.,Animal Hrs. w : * N. S E. Nitrite Application
Q o
Wet, : w
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches E. * o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
8/30/21 63000 1.1 0.193 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 15.139 NA Fescue
8/31/21 90000 1.1 0.275 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 21.627 NA Fescue
9/3/21 36000 1.1 0.110 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 8.651 NA Fescue
9/7/21 72000 1.1 0.220 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 17.301 NA Fescue
9/10/21 40500 1.1 0.124 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 9.732 NA Fescue
9/11/21 49500 1.1 0.151 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 11.895 NA Fescue
9/13/21 67500 1.1 0.206 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 16.220 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
II I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 0 418500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 100.565 0.000 Lime Applied
Annual lbs/acre 0.0558 0.0047 0.6323 0.0973 0.0420 0.0016 0.0315 0.0545 0.0745 1.8483 65.536 Date lbs/ac
Prior Years Cumulative lbs/ac 0.2242 0.1569 11.4674 0.8987 2.2613 0.0527 0.6647 1.1036 0.2793 42.2857
Current Cumulative lbs/ac 0.2800 0.1616 12.0997 0.9960 2.3033 0.0543 0.6962 1.1581 0.3538 44.1340
Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498
Peunit PAN Limit lst/2nd Crop 167
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
dd *Application Method: S-Surface,IN-Injection,INC-Incorporation
1/4/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied(Annual): 6.58
Permit#: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Jeff Smith Owner: Town of Mocksville Predominant Soil Series: CeB2 - Cecil
Acres Used: 4.7 Acres Permitted: 4.7 Site #: NC-MK05 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample orlL 5 L3 15 1 L6 L 10 11 12
Corn-
2/
ite 24/21 8/26/21
Date
% Solids 1.45 1.1
Arsenic 17.1 21.8
Cadmium 1.43 1.82
Copper 148 247
Chromium 22.8 38
Lead 17.8 16.4
Mercury 0.433 0.622
Molyb- 9.64 12.3
denum
Nickel 20.3 21.3
Selenium 22.9 29.1
Zinc 351 722
Total
Phos- 18700 25600
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total [ L 31 41 51 71 L 10 11 112
1-3
DT/Ac./
App. CA
Event 0.52 0.88
Arsenic 0.018 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
Cadmium 0.001 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Copper 0.154 0.434 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.588
Chromium 0.024 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090
Lead 0.019 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047
Mercury 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.010 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
denum
Nickel 0.021 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059
Selenium 0.024 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075
Zinc 0.366 1.268 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.634
Total
Phos- 19.485 44.954 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 64.439
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Z~e 1/4/2022
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit#: WQ0003351 Field#: 1 Acres Utilized: 4.7
Land Owner: Town of Mocksville Annual Dry Tons Applied: 6.58 Site#: NC-MK05 Acres Permitted: 4.7
Operator: Jeff Smith Predominant Soil Series: CeB2-Cecil Cation Exchange Capacity(non 503):
Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 209 Crop 2 Name: Crop 2 Max.PAN:
Volume applied Volume Residual Sources Soil Precip. a o Z a Nitrate Name of Crop Type
p Cond. ; PAN Applied
(enter one)Solids/ % Applied per (NPDES#,WQ#, Past 24 r '� ,, r, TKN o and Receiving Residual
a� o wry, - a o (lbs/acre)
c� Liquid Solids Acre Fert.,Animal Hrs. w N S E. Nitrite Application
Q
Wet, * o
w
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches °� * o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
2/24/21 36000 1.45 0.463 Dutchman's Creek Dry <.5" S 0.5 0.3 40600 13900 386 14.215 NA Fescue
2/25/21 4500 1.45 0.058 Dutchman's Creek Dry <.5" S 0.5 0.3 40600 13900 386 1.777 NA Fescue
9/3/21 36000 1.1 0.351 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 27.609 NA Fescue
9/10/21 27000 1.1 0.264 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 20.706 NA Fescue
9/13/21 4500 1.1 0.044 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 3.451 NA Fescue
9/14/21 22500 1.1 0.220 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 17.255 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0 0 I I 0.000 I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): 0.000 0.000
TOTALS: 0 130500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 85.013 0.000 Lime Applied
Annual lbs/acre 0.056 0.005 0.588 0.090 0.047 0.002 0.032 0.059 0.075 1.634 64.439 Date lbs/ac
Prior Years Cumulative lbs/ac 0.484 0.112 10.979 1.906 1.543 0.053 0.393 1.379 0.543 35.321
Current Cumulative lbs/ac 0.540 0.117 11.567 1.996 1.590 0.055 0.425 1.438 0.618 36.955
Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498
Peunit PAN Limit 1st/2nd Crop 209
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
dAZ
*Application Method: S-Surface,IN-Injection,INC-Incorporation
1/4/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied(Annual): 3.34
Permit#: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Jeff Smith Owner: Town of Mocksville Predominant Soil Series: CfB2
Acres Used: 4 Acres Permitted: 4 Site #: NC-MK05 Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample orlL 5 L3 15 1 L6 L 10 11 12
Corn- 2/24/21 8/26/21
posite
Date
% Solids 1.45 1.1
Arsenic 17.1 21.8
Cadmium 1.43 1.82
Copper 148 247
Chromium 22.8 38
Lead 17.8 16.4
Mercury 0.433 0.622
Molyb- 9.64 12.3
denum
Nickel 20.3 21.3
Selenium 22.9 29.1
Zinc 351 722
Total
Phos- 18700 25600
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total [ L 31 41 51 71 L 10 11 112
1-3
DT/Ac./
App.
Event 0.68 0.16
Arsenic 0.023 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030
Cadmium 0.002 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 0.201 0.077 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.278
Chromium 0.031 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043
Lead 0.024 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029
Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Molyb 0.013 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017
denum
Nickel 0.028 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034
Selenium 0.031 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040
Zinc 0.477 0.224 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.701
Total
Phos- 25.432 7.936 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 33.368
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Z~e 1/4/2022
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit#: WQ0003351 Field#: 2 Acres Utilized: 4
Land Owner: Town of Mocksville Annual Dry Tons Applied: 3.34 Site#: NC-MK05 Acres Permitted: 4
Operator: Jeff Smith Predominant Soil Series: CfB2 Cation Exchange Capacity(non 503):
Crop 1 Name: Fescue-Hay Crop 1 Max.PAN: 209 Crop 2 Name: Crop 2 Max.PAN:
Volume applied Volume Residual Sources Soil Precip. a o Z a Nitrate Name of Crop Type
p Cond. ; PAN Applied
(enter one)Solids/ % Applied per (NPDES#,WQ#, Past 24 r '� ,, r, TKN o and Receiving Residual
a� o wry, - F"D a o (lbs/acre)
c� Liquid Solids Acre Fert.,Animal Hrs. w * N Nitrite Application
Q
Wet o
, * w
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches E. * o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
2/25/21 45000 1.45 0.680 Dutchman's Creek Dry <.5" S 0.5 0.3 40600 13900 386 20.878 NA Fescue
9/14/21 13500 1.1 0.155 Dutchman's Creek Dry <.5" S 0.5 0.3 60900 12600 18500 12.165 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
II I Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 0 58500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 33.043 0.000 Lime Applied
Annual lbs/acre 0.030 0.003 0.278 0.043 0.029 0.001 0.017 0.034 0.040 0.701 33.368 Date lbs/ac
Prior Years Cumulative lbs/ac 1.847 0.245 3.265 12.234 12.024 0.407 0.141 3.751 1.468 10.861
Current Cumulative lbs/ac 1.877 0.248 3.543 12.277 12.053 0.408 0.158 3.785 1.508 11.562
Permitted C. P. L. R.**** 36 34 1338 267 15 374 89 2498
Peunit PAN Limit 1st/2nd Crop 209
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
dAZ
*Application Method: S-Surface,IN-Injection,INC-Incorporation
1/4/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

`.O
Vv
Waypoint,,, 2790 Whitten Road, Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
3/4/2021
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 21-056-0185
Client Project Description: Mocksville, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 2/25/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '--' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
0/-No LiaCa-Q 0J-3-Q--
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

,.4.,
. .iD
\Alaypoint. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalyticalcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2022
Arkansas State Program 88-0650 02/07/2021
California State Program 2904 06/30/2021
Florida State Program - NELAP E871157 06/30/2021
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2021
Illinois State Program - NELAP 200078 10/10/2021
Kentucky State Program 80215 06/30/2021
Kentucky State Program KY90047 12/31/2021
Louisiana State Program - NELAP LA037 12/31/2021
Louisiana State Program - NELAP 04015 06/30/2021
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2021
Oklahoma State Program 9311 08/31/2021
Pennsylvania State Program - NELAP 68-03195 05/31/2021
South Carolina State Program 84002 06/30/2021
South Carolina State Program 84002 06/30/2021
Tennessee State Program 02027 02/11/2023
Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021
Texas State Program - NELAP T104704180 09/30/2021
Virginia State Program 00106 06/30/2021
Virginia State Program - NELAP 460181 09/14/2021
Page 1 of 1 00001/21-056-0185
Page 2 of 8

•
\P4.'arIoIflt 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-056-0185
Client Project Description: Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
85671 Dutchmans Creek WWTP Solids 02/24/2021 11:30 02/25/2021
Page 3 of 8

�O
Waypoi nt N 2790 Whitten Road, Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Client: EMA Resources Inc CASE NARRATIVE
Project: Mocksville, NC
Lab Report Number: 21-056-0185
Date: 3/4/2021
Metals Analysis Method 6010D
Sample 85671 (Dutchmans Creek VVWTP)
Analyte: Aluminum
QC Batch No: L538520/L538262
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

a • VV
2790 Whitten Road,Memphis,TN 38133
My I�� Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 03/04/2021
755 Yadkinville Rd Information : Received : 02/25/2021
Mocksville , NC 27028
Report Number :21-056-0185 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No : 85671 Matrix: Solids
Sample ID : Dutchmans Creek WWTP Sampled: 2/24/2021 11:30
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 98.6 % 0.010 1 03/01/21 16:17 FMM SW-DRYWT
Ammonia Nitrogen 13900 mg/Kg-dry 1790 7140 1 03/04/21 14:30 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 386 mg/Kg-dry 357 357 1 02/26/21 14:22 ZBD 4500NO3F-2011
Organic N 26710 mg/Kg-dry 1786 7143 1 03/04/21 14:11 DH CALCULATION
pH 7.9 s.u. 1 03/03/21 16:30 ADM 9045D
Total Solids 1.45 % 0.010 0.010 1 03/01/21 16:17 FMM 2540G-2011
Total Volatile Solids 71.9 % 0.010 0.010 1 03/01/21 16:17 FMM 2540G-2011
Total Kjeldahl Nitrogen 40600 mg/Kg-dry 3570 1 03/04/21 14:11 CLP 4500NORGD-2011
Phosphorus 18700 mg/Kg-dry 197 357 1 03/01/21 19:44 JTR 6010D
Aluminum 18100 mg/Kg-dry 330 357 1 02/27/21 10:52 JADS 6010D
Arsenic <17.1 mg/Kg-dry 17.1 35.7 1 03/01/21 19:44 JTR 6010D
Cadmium <1.43 mg/Kg-dry 1.43 7.14 1 02/27/21 10:52 JADS 6010D
Calcium 17700 mg/Kg-dry 2760 3570 1 02/27/21 10:52 JADS 6010D
Chromium 22.8 mg/Kg-dry 16.9 17.9 1 02/27/21 10:52 JADS 6010D
Copper 148 mg/Kg-dry 22.1 35.7 1 02/27/21 10:52 JADS 6010D
Iron 19400 mg/Kg-dry 609 714 1 02/27/21 10:52 JADS 6010D
Lead 17.8] mg/Kg-dry 12.9 21.4 1 02/27/21 10:52 JADS 6010D
Magnesium 2970 mg/Kg-dry 184 357 1 02/27/21 10:52 JADS 6010D
Manganese 1170 mg/Kg-dry 23.2 35.7 1 02/27/21 10:52 JADS 6010D
Mercury <0.433 mg/Kg-dry 0.433 0.993 1 03/02/21 17:07 DDB 7471A
Molybdenum <9.64 mg/Kg-dry 9.64 17.9 1 02/27/21 10:52 JADS 6010D
Nickel 20.3 mg/Kg-dry 8.57 17.9 1 02/27/21 10:52 JADS 6010D
Potassium 4610 mg/Kg-dry 441 714 1 02/27/21 10:52 JADS 6010D
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 5 of 8

\A/aypoint.
Main 901.213.2400°fax [phone]
ANALYTICAL www.waypointanalyticalcom
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 03/04/2021
755 Yadkinville Rd Information : Received : 02/25/2021
Mocksville , NC 27028
Report Number :21-056-0185 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No : 85671 Matrix: Solids
Sample ID : Dutchmans Creek WWTP Sampled: 2/24/2021 11:30
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <22.9 mg/Kg-dry 22.9 35.7 1 03/01/21 19:44 JTR 6010D
Sodium 6590 mg/Kg-dry 929 1790 1 02/27/21 10:52 JADS 6010D
Zinc 351 mg/Kg-dry 57.9 89.3 1 02/27/21 10:52 JADS 6010D
Sulfur 9140 mg/Kg-dry 370 714 1 03/01/21 19:44 JTR 6010D
Sodium Absorption Ratio 1.42 Ratio 0.01 0.01 1 02/27/21 10:52 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions
Page 6 of 8

vi.
\P1(aYpOl ut ' 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46245
Customer Name: EMA Resources Inc
Report Number: 21-056-0185
Shipping Method
• Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: T102
Shipping container/cooler uncompromised? • Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed • Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes 0 No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No • N/A
Water- VOA vials free of headspace 0 Yes 0 No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: Makayla Weaver Date &Time: 02/25/2021 16:16:33
Page 7 of 8

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Page 8 of 8

2/24/2021
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 6590 95.555 23 4.154565
Calcium 17700 256.65 20 12.8325
Magnesium 2970 43.065 12 3.58875
Percent Solids 1.45 Na
SAR =
I2(Ca2+ + Mg2 I )
SAR 1.45 �/

`.O
Vv
Waypoint,,, 2790 Whitten Road, Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
9/8/2021
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 21-239-0005
Client Project Description: Mocksville, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/27/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '--' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Randy Thomas
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

,.4.,
. .iD
\Alaypoint. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalyticalcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2022
Arkansas State Program 88-0650 02/07/2022
California State Program 2904 06/30/2022
Florida State Program - NELAP E871157 06/30/2022
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2022
Illinois State Program - NELAP 200078 10/10/2022
Kentucky State Program 80215 06/30/2022
Kentucky State Program KY90047 12/31/2021
Louisiana State Program - NELAP LA037 12/31/2021
Louisiana State Program - NELAP 04015 06/30/2022
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2021
Pennsylvania State Program - NELAP 68-03195 05/31/2022
South Carolina State Program 84002 06/30/2022
South Carolina State Program 84002 06/30/2022
Tennessee State Program 02027 02/11/2023
Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021
Texas State Program - NELAP T104704180 09/30/2021
Virginia State Program 00106 06/30/2022
Virginia State Program - NELAP 460181 09/14/2021
Page 1 of 1 00001/21-239-0005
Page 2 of 7

•
\P4.'arIoIflt 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-239-0005
Client Project Description: Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
95935 Mocksville Solids 08/26/2021 08:05 08/27/2021
Page 3 of 7

a • VV
2790 Whitten Road,Memphis,TN 38133
My I�� Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 09/08/2021
755 Yadkinville Rd Information : Received : 08/27/2021
Mocksville , NC 27028
Report Number :21-239-0005 REPORT OF ANALYSIS Randy Thomas
Project Manager
Lab No : 95935 Matrix: Solids
Sample ID : Mocksville Sampled: 8/26/2021 8:05
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 98.9 % 0.010 1 08/30/21 16:35 FMM SW-DRYWT
Ammonia Nitrogen 12600 mg/Kg-dry 1450 9090 1 08/31/21 13:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 18500 mg/Kg-dry 441 441 1 08/31/21 15:54 ZBD 4500NO3F-2011
Organic N 48270 mg/Kg-dry 1455 9091 1 08/27/21 11:00 DH CALCULATION
pH 7.2 s.u. 1 08/31/21 15:37 DRS 9045D
Total Solids 1.10 % 0.010 0.010 1 08/30/21 16:35 FMM 2540G-2011
Total Volatile Solids 56.2 % 0.010 0.010 1 08/30/21 16:35 FMM 2540G-2011
Total Kjeldahl Nitrogen 60900 mg/Kg-dry 909 22700 1 08/27/21 11:00 JPJ iM-4500-NH3C-TKP
Phosphorus 25600 mg/Kg-dry 251 455 1 09/03/21 02:59 TJS 6010D
Aluminum 22500 mg/Kg-dry 420 455 1 09/03/21 02:59 TJS 6010D
Arsenic <21.8 mg/Kg-dry 21.8 45.5 1 09/03/21 02:59 TJS 6010D
Cadmium <1.82 mg/Kg-dry 1.82 9.09 1 09/03/21 02:59 TJS 6010D
Calcium 75200 mg/Kg-dry 3520 4550 1 09/03/21 02:59 TJS 6010D
Chromium 38.0 mg/Kg-dry 21.5 22.7 1 09/03/21 02:59 TJS 6010D
Copper 247 mg/Kg-dry 28.2 45.5 1 09/03/21 02:59 TJS 6010D
Iron 25000 mg/Kg-dry 775 909 1 09/03/21 02:59 TJS 6010D
Lead <16.4 mg/Kg-dry 16.4 27.3 1 09/03/21 02:59 TJS 6010D
Magnesium 6130 mg/Kg-dry 235 455 1 09/03/21 02:59 TJS 6010D
Manganese 1220 mg/Kg-dry 29.5 45.5 1 09/03/21 02:59 TJS 6010D
Mercury <0.622 mg/Kg-dry 0.622 1.43 1 08/30/21 12:10 TJS 7471A
Molybdenum <12.3 mg/Kg-dry 12.3 22.7 1 09/03/21 02:59 TJS 6010D
Nickel 21.33 mg/Kg-dry 10.9 22.7 1 09/03/21 02:59 TJS 6010D
Potassium 7930 mg/Kg-dry 562 909 1 09/07/21 17:07 JADS 6010D
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 4 of 7

\A/aypoint.
Main 901.213.2400°fax [phone]
ANALYTICAL www.waypointanalyticalcom
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 09/08/2021
755 Yadkinville Rd Information : Received : 08/27/2021
Mocksville , NC 27028
Report Number :21-239-0005 REPORT OF ANALYSIS Randy Thomas
Project Manager
Lab No : 95935 Matrix: Solids
Sample ID : Mocksville Sampled: 8/26/2021 8:05
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <29.1 mg/Kg-dry 29.1 45.5 1 09/03/21 02:59 TJS 6010D
Sodium 14000 mg/Kg-dry 1180 2270 1 09/03/21 02:59 TJS 6010D
Zinc 722 mg/Kg-dry 73.6 114 1 09/03/21 02:59 TJS 6010D
Sulfur 13300 mg/Kg-dry 471 909 1 09/03/21 02:59 TJS 6010D
Sodium Absorption Ratio 1.38 Ratio 0.01 0.01 1 09/03/21 02:59 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions
Page 5 of 7

vi.
\P1(aYpOl ut ' 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46245
Customer Name: EMA Resources Inc
Report Number: 21-239-0005
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: T135
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present
Custody seals intact on sample bottles? 0 Yes 0 No # Not Present
Chain of Custody(COC) present? # Yes 0 No
COC agrees with sample label(s)? #Yes 0 No
COC properly completed # Yes 0 No
Samples in proper containers? # Yes 0 No
Sample containers intact? # Yes 0 No
Sufficient sample volume for indicated test(s)? # Yes 0 No
All samples received within holding time? # Yes 0 No
Cooler temperature in compliance? # Yes 0 No
Cooler/Samples arrived at the laboratory on ice. # Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Makayla Weaver Date &Time: 08/27/2021 08:51:18
Page 6 of 7

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8/26/2021
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 14000 154 23 6.695652
Calcium 75200 827.2 20 41.36
Magnesium 6130 67.43 12 5.619167
Percent Solids 1.1 Na
SAR =
I2(Ca2+ + Mg2 I )
SAR 1.38 �/

aceAnaiica�® A \ ALYTICAL REPORT
National Center forTesting&Innovation March 09, 2021
2
Tc
3
SS
EMA Resources
a
Sample Delivery Group: L132O228 Cn
Samples Received: 02/25/2021 5Sr
Project Number: MOCKSVILLE
5
Description: Sludge Qc
GI
Report To: Mr. Brent Collins
755 Yadkinville Road r-Al
Mocksville, NC 27028
9
SC
Entire Report Reviewed By:
,....
Cassandra Foster
' Project Manager
Results relate only to the items tested or calibrated and are reported as rounded valves.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
• Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided,
and as the samples are received.
4 a
ii.• .
•c. IN' 411....1" aT -
r
1
i
.11. I"51 41, ....
L y
ti
_.4.11.111111110fr
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 1 of 21

TABLE OF CONTENTS ONE LAB.NATIONWIDE. AO
Cp:Cover Page 1
Cp
Tc:Table of Contents 2
Ss:Sample Summary 3 1
Tc
Cn:Case Narrative 4
3
Sr:Sample Results 5 Ss
DUTCHMANS CREEK WWTP L1320228-01 5 4
Cn
Qc:Quality Control Summary 7
Wet Chemistry by Method 9012 B 7 5Sr
Wet Chemistry by Method 9034-9030B 8
5
Wet Chemistry by Method 9045D 9 Qc
Wet Chemistry by Method D93/1010A 10
GI
Mercury by Method 7470A 11
Metals(ICP) by Method 6010D 12 8AI
Volatile Organic Compounds(GC/MS) by Method 8260D 13
9
Chlorinated Acid Herbicides(GC) by Method 8151A 15 Sc
Pesticides(GC) by Method 8081E 16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 17
GI: Glossary of Terms 19
Al:Accreditations& Locations 20
Sc:Sample Chain of Custody 21
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 2 of 21

SAMPLE SUMMARY ONE LAB.NATIONWIDE. al
Collected by Collected date/time Received date/time
DUTCHMANS CREEK WWTP L1320228-01 Waste Roy Whitaker 02/24/2111:30 02/25/2109:50 1 C
p
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Preparation by Method 1311 WG1627600 1 03/01/2113:13 03/01/2113:13 TM Mt.Juliet,TN
Preparation by Method 1311 WG1628245 1 03/02/2115:28 03/02/2115:28 IDW Mt.Juliet,TN
Wet Chemistry by Method 9012 B WG1629603 2 03/04/2116:26 03/07/21 01:52 SDL Mt.Juliet,TN Ss
Wet Chemistry by Method 9034-9030B WG1628802 1 03/03/2123:00 03/03/2123:00 LDT Mt.Juliet,TN
Wet Chemistry by Method 9045D WG1627250 1 02/28/2117:56 02/28/21 21:08 KPS Mt.Juliet,TN 4
Cn
Wet Chemistry by Method D93/1010A WG1629797 1 03/05/21 07:58 03/05/21 07:58 CAT Mt.Juliet,TN
Mercury by Method 7470A WG1628343 1 03/02/2119:04 03/03/2111:52 ABL Mt.Juliet,TN 5
Metals(ICP)by Method 6010D WG1628115 1 03/02/2119:58 03/03/21 00:49 EL Mt.Juliet,TN Sr
Volatile Organic Compounds(GC/MS)by Method 8260D WG1628754 1 03/03/2119:03 03/03/2119:03 ACG Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 8260D WG1628754 1 03/04/2115:12 03/04/2115:12 JHH Mt.Juliet,TN 5
Qc
Chlorinated Acid Herbicides(GC)by Method 8151A WG1629916 1 03/05/2111:29 03/08/2112:29 MTJ Mt.Juliet,TN
Pesticides(GC)by Method 8081B WG1627083 1 03/04/21 09:45 03/04/2119:16 HMH Mt.Juliet,TN
Semi Volatile Organic Compounds (GC/MS)by Method 8270E WG1628367 1 03/02/21 22:50 03/03/2116:26 LEA Mt.Juliet,TN GI
8
Al
9
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 3 of 21

CASE NARRATIVE ONE LAB.NATIONWIDE. AO
Cp
All sample aliquots were received at the correct temperature, in the proper containers,with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL(LOD) and RDL(LOQ)values reported for environmental samples zTc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form 3
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been a
knowingly withheld that would affect the quality of the data. Cn
5
Sr
5
Qc
GI
Cassandra Foster
Project Manager
9
Sc
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 4 of 21

DUTCHMANS CREEK WWTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. al
Collected date/time: 02/24/21 11:30 L1320228
Preparation by Method 1311 1
Result Qualifier Prep Batch Cp
Analyte date/time
2
TCLP Extraction - 3/1/2 0 21 1:13:11 PM WG1627600 Tc
TCLP 7HE Extraction - 3/2/2021 3:23:20 PM WG1628245
Fluid 1 3/1/20211:13:11 PM WG1627600 3
SS
Initial pH 7.34 3/1/20211:13:11 PM WG1627600
Final pH 4.88 3/1/20211:13:11 PM WG1627600 4
Cn
Wet Chemistry by Method 9012 B
5
Result Qualifier RDL Dilution Analysis Batch Sr
Analyte mg/kg mg/kg date/time
Reactive Cyanide ND 0.500 2 03/07/2021 01:52 WG1629603 5
Qc
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL Dilution Analysis Batch GI
Analyte mg/kg mg/kg date/time
s
Reactive Sulfide ND 25.0 1 03/03/2021 23:00 WG1628802 Al
Wet Chemistry by Method 9045D Sc9
Result Qualifier Dilution Analysis Batch
Analyte su date/time
Corrosivity by pH 7.41 T8 1 02/28/2021 21:08 WG1627250
Sample Narrative:
L1320228-01 WG1627250:7.41 at 21.3C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg.F date/time
Ignitability DNI at 170 1 03/05/2021 07:58 WG1629797
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Mercury ND 0.0100 0.20 1 03/03/202111:52 WG1628343
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Arsenic ND 0.100 5 1 03/03/2021 00:49 WG1628115
Barium 0.125 0.100 100 1 03/03/2021 00:49 WG1628115
Cadmium ND 0.100 1 1 03/03/2021 00:49 WG1628115
Chromium ND 0.100 5 1 03/03/2021 00:49 WG1628115
Lead ND 0.100 5 1 03/03/2021 00:49 WG1628115
Selenium ND 0.100 1 1 03/03/2021 00:49 WG1628115
Silver ND 0.100 5 1 03/03/2021 00:49 WG1628115
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Benzene ND 0.0500 0.50 1 03/03/202119:03 WG1628754
Carbon tetrachloride ND 0.0500 0.50 1 03/03/202119:03 WG1628754
Chlorobenzene ND 0.0500 100 1 03/03/202119:03 WG1628754
Chloroform ND 0.250 6 1 03/03/202119:03 WG1628754
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 5 of 21

DUTCHMANS CREEK WWTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. al
Collected date/time: 02/24/21 11:30 L1320228
Volatile Organic Compounds (GC/MS) by Method 8260D
1
Result Qualifier RDL Limit Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
1,2-Dichloroethane ND 0.0500 0.50 1 03/03/202119:03 WG1628754 z
Tc
1,1-Dichloroethene ND 0.0500 0.70 1 03/03/202119:03 WG1628754
2-Butanone(MEK) ND 0.500 200 1 03/04/202115:12 WG1628754 3
Tetrachloroethene ND 0.0500 0.70 1 03/03/202119:03 WG1628754 SS
Trichloroethene ND 0.0500 0.50 1 03/03/202119:03 WG1628754
Vinyl chloride ND 0.0500 0.20 1 03/03/202119:03 WG1628754 4
Cn
(S)Toluene-d8 105 80.0-120 03/04/202115:12 WG1628754
(S)Toluene-d8 111 80.0-120 03/03/202119:03 WG1628754 5
(S)4-Bromofluorobenzene 102 77.0-126 03/03/202119:03 WG1628754 Sr
(S)4-Bromofluorobenzene 102 77.0-126 03/04/202115:12 WG1628754
(S)1,2-Dichloroethane-d4 93.7 70.0-130 03/04/202115:12 WG1628754 5
QC
(S)1,2-Dichloroethane-d4 106 70.0-130 03/03/202119:03 WG1628754
Chlorinated Acid Herbicides (GC) by Method 8151A GI
Result Qualifier RDL Limit Dilution Analysis Batch a
Analyte mg/I mg/I mg/I date/time Al
2,4,5-TP(Silvex) ND 0.00200 1 1 03/08/202112:29 WG1629916
2,4-D ND 0.00200 10 1 03/08/202112:29 WG1629916 9
SC
(S)2,4-Dichlorophenyl Acetic Acid 95.8 14.0-158 03/08/202112:29 WG1629916
Pesticides (GC) by Method 8081B
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Chlordane ND 0.00500 0.03 1 03/04/202119:16 WG1627083
Endrin ND 0.00500 0.02 1 03/04/202119:16 WG1627083
Heptachlor ND 0.00500 0.0080 1 03/04/202119:16 WG1627083
Lindane ND 0.00500 0.40 1 03/04/202119:16 WG1627083
Methoxychlor ND 0.00500 10 1 03/04/202119:16 WG1627083
Toxaphene ND 0.0100 0.50 1 03/04/202119:16 WG1627083
(S)Decachlorobiphenyl 80.9 10.0-128 03/04/202119:16 WG1627083
(S)Tetrachloro-m-xylene 75.4 10.0-127 03/04/202119:16 WG1627083
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
1,4-Dichlorobenzene ND 0.100 7.50 1 03/03/202116:26 WG1628367
2,4-Dinitrotoluene ND 0.100 0.13 1 03/03/202116:26 WG1628367
Hexachlorobenzene ND 0.100 0.13 1 03/03/202116:26 WG1628367
Hexachloro-1,3-butadiene ND 0.100 0.50 1 03/03/202116:26 WG1628367
Hexachloroethane ND 0.100 3 1 03/03/202116:26 WG1628367
Nitrobenzene ND 0.100 2 1 03/03/202116:26 WG1628367
Pyridine ND 0.100 5 1 03/03/202116:26 WG1628367
364-Methyl Phenol ND 0.100 400 1 03/03/202116:26 WG1628367
2-Methylphenol ND 0.100 200 1 03/03/202116:26 WG1628367
Pentachlorophenol ND 0.100 100 1 03/03/202116:26 WG1628367
2,4,5-Trichlorophenol ND 0.100 400 1 03/03/202116:26 WG1628367
2,4,6-Trichlorophenol ND 0.100 2 1 03/03/202116:26 WG1628367
(S)2-Fluorophenol 113 10.0-120 03/03/202115:26 WG1628367
(S)Phenol-d5 277 10.0-120 03/03/202115:26 WG1628367
(S)Nitro benzene-d5 71.9 10.0-127 03/03/202115:26 WG1628367
(S)2-Fluorobiphenyl 76.8 10.0-130 03/03/202115:26 WG1628367
(S)2,4,6-Tribromophenol 87.5 10.0-155 03/03/202115:26 WG1628367
(S)p-Terphenyl-d14 84.8 10.0-128 03/03/202115:26 WG1628367
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 6 of 21

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GLOSSARY OF TERMS ONE LAB.NATIONWIDE. AO
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, Tc
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
3
Abbreviations and Definitions Ss
MDL Method Detection Limit.
4
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery. 5
RPD Relative Percent Difference. Sr
SDG Sample Delivery Group.
5
Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and Qc
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable). GI
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
s
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the Al
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor. 9
These are the target%recovery ranges or,difference value that the laboratory has historically determined as normal SC
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
T8 Sample(s)received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 19 of 21

ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. 11111
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as
accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing Cp
turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
*Not all certifications held by the laboratory are applicable to the results reported in the attached report.
*Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2
Tc
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN, 37122
Alabama 40660 Nebraska NE-OS-15-05 3
SS
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey—NELAP TN002 4Cn
Cn
California 2932 New Mexico' TN00003
Colorado _ TN00003 _ New York 11742
Connecticut PH-0197 North Carolina Env375 5
Sr
Florida E87487 North Carolina' DW21704
Georgia NELAP North Carolina' 41
—
Georgia' 923 North Dakota R-140 6
QC
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002 GI
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky'6 KY90010 South Carolina 84004002
Kentucky' 16 South Dakota n/a
Louisiana A130792 Tennessee'4 2006
Louisiana LA018 Texas T104704245-20-18 9
SC
Maine TN00003 Texas' LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA—ISO 17025' 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources MOCKSVILLE L1320228 03/09/21 09:22 20 of 21

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Mocksville WQ Permit Number: WQ0003351
WWTP Name: Dutchman's Creek WWTP PWS Number: NC0021491
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑
AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1)Fecal Density ❑ Alt. (2)Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization 0 Air Drying ❑ Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of
Parameter gExcee-
in Frequency Sample Analytical
Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type Tech-nique
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU 327 342 348 col/g 0 Annually Grab SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(thy
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107) -Please indicate alternative performed:
Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) r2 Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying- Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
O "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Todd Robinson -Assistant Area Manager Brent Collins - Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
TadRob/` *Ii Feb 9,2022 dti Todd Robinson(Feb 9,2022 10:00 EST) 2/8/2022
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
10,F40.
Page 1
Contact: Brent Collins Report Date: 3/2/2021
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 2/23/2021
Meritech Work Order# 022321107 Sample: Dutchman Creek WWTP D-1 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 2.66 % 2/24/21 0-100 % SM 2540E
Fecal Coliform (Sludge) <342 col/g dry wt 2/23/21 342 col/g dry wt SM 9222D
Meritech Work Order# 022321108 Sample: Dutchman Creek WWTP D-2 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
0/0 Total Solids 2.62 % 2/24/21 0-100 % SM 2540B
Fecal Coliform (Sludge) <347 col/g dry wt 2/23/21 347 col/g dry wt SM 9222D
Meritech Work Order# 022321109 Sample: Dutchman Creek WWTP D-3 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 2.62 % 2/24/21 0-100 % SM 2540B
Fecal Coliform (Sludge) <347 col/g dry wt 2/23/21 347 col/g dry wt SM 9222D
Meritech Work Order# 022321110 Sample: Dutchman Creek WWTP D-4 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%TotaI Solids 2.61 % 2/24/21 0-100 % SM 2540B
Fecal Coliform (Sludge) <348 col/g dry wt 2/23/21 348 col/g dry wt SM 9222D
Meritech Work Order# 022321111 Sample: Dutchman Creek WWTP D-5 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 2.62 % 2/24/21 0-100 % SM 2540B
Fecal Coliform (Sludge) <347 col/g dry wt 2/23/21 347 col/g dry wt SM 9222D
642 Tamco Road, Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

44 Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
101":
Ali
Page 2
Contact: Brent Collins Report Date: 3/2/2021
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 2/23/2021
Meritech Work Order# 022321112 Sample: Dutchman Creek WWTP D-6 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 2.78 % 2/24/21 0-100 % SM 2540B
Fecal CoIiform (Sludge) <327 col/g dry wt 2/23/21 327 col/g dry wt SM 9222D
Meritech Work Order# 022321113 Sample: Dutchman Creek WWTP D-7 Grab 2/23/21
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 2.71 % 2/24/21 0-100 % SM 2540E
Fecal Coliform (Sludge) <335 col/g dry wt 2/23/21 335 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. -_,41)andcit. licuncoo.IL
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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Analytical Results STATESVILLE
ANALYTICAL
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 02/24/2021
Reported: 03/31/2021
For: DUTCHMAN
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210224-16-01 30 Day Benchscale DUTCHMAN 11.3 % EPA625-R-92/0 02/24/2021 MD
Respectfully submitted,
1
Melissa Myers
NC Cert#440,
NCDW Cert#37755,
EPA#NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 210224-16-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 5

STATESVILLE
ANALYTICAL
Analytical Results
EMA RESOURCES, INC. For: DUTCHMAN
755 Yadkinville Rd
Mocksville, NC 27028
Entered: 2/24/21
Reported: 3/31/21
Sample ID: 210224-16-01
PARAMETER:Vector Attraction Reduction/Aerobically Digested Sludge(30day)
Total Solids Volatile Solids %Volatile Solids
Week 1 1.38 0.72 0.5217
Week 2 1.36 0.69 0.5074
Week 3 1.31 0.67 0.5115
Week 4 1.24 0.63 0.5081
Week 5 1.26 0.65 0.5159
Week 6 1.2 0.59 0.4917
Volatile Solids Reduction: 0.5217 - 0.4917 X 100 = 11.3
0.5217-(0.5217 X 0.4917)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.#440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID#210224-16
WEEK 1
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.37 0.71
2 1.38 0.72
3 1.38 0.726
Average: 1.38 0.72 0.5217
WEEK 2
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.37 0.69
2 1.35 0.70 •
3 1.35 0.69
Average: 1.36 0.69 0.5074
WEEK 3
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.32 0.67
2 1.32 0.68
3 1.30 0.67
Average: 1.31 0.67 0.5115
WEEK 4
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.25 0.64
2 1.24 0.63
3 1.24 0.63
Average: 1.24 0.63 0.5081
WEEK 5
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.25 0.65
2 1.26 0.65
3 1.27 0.66
Average: 1.26 0.65 0.5159
WEEK 6
Samples Total Solids Volatile Solids %Volatile Fraction
1 1.19 0.59
2 1.19 0.59
3 1.21 0.6
Average: 1.2 0.59 0.4917
Van Kleeck Reduction: 0.5217-0.4917 X 100= %
0.5217-(0.5217 X 0.4917)
Final Result: 11.3%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

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2021 Mocksville Annual Report - WQ0003351
Final Audit Report 2022-02-09
Created: 2022-02-09
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAheowZhzM0VZD79G6oSu5V0Eb8C0j69f1
"2021 Mocksville Annual Report - WQ0003351 " History
t Document created by Brent Collins ([e-mail])
2022-02-09-2:49:18 PM GMT-IP address:206.85.202.26
2p Document emailed to Todd Robinson ([e-mail])for signature
2022-02-09-2:51:31 PM GMT
e Email viewed by Todd Robinson ([e-mail])
2022-02-09-2:54:11 PM GMT-IP address:66.44.247.179
>o Document e-signed by Todd Robinson ([e-mail])
Signature Date:2022-02-09-3:00:33 PM GMT-Time Source:server-IP address:66.44.247.179
Agreement completed.
2022-02-09-3:00:33 PM GMT
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