WQ0003035_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0003035
Applicant/Permittee City of Eden
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0003035
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* City of Eden Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for City of Eden,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Eden NC 2021 Annual Report FINAL.pdf 22.98MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja TM/WO
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No. WQ0003035
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Eden, NC.
If you have any questions or need additional information,please do not hesitate to contact
Melinda Ward at(336) 627-1009 ext. 130 or Ryan Copeland at(336) 607-4494.
Sincerely,
l e't ic& Sfiiva'G 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Melinda Ward—City of Eden
Ryan Copeland—Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

CITY OF EDEN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003035
2021 ANNUAL REPORT

City of Eden, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms & Metals Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit y: WQ00Q3035 County gockineham Year 2�1
Facility Name las shown on permit)Mebane Bridge WWTP NPDES N,. \(thi2 I
Land Application Operator Synagto Phoney. i336199x-7150
Land application ot'residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO.skip Part A.and Part B and proceed to Part C. Also,if residuals were generated but not land applied.
please attach an explanation on how the residuals were handled.
;'art A-Residuals Application Summary:
Total number of application fields in the permit: 12
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: p97.91
Total number of acres utilized for land application during the year: 155.50
Part)3-Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-13 below)issued by the Division of Water Quality X YES NO.
If no,please provide a u ritten description why the facility was not compliant.the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites_
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three 13)copies of
laboratory results are attached.
4. Annual TCLP analysis i if requital)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(31
copies of certified laboratory results arc attached.
6, The facility did not exceed any of the Pollutant Concentration Limits in 1 SA NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1 105(h)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with tapplicable to 40 CFR Part 503
regulated facilities).
All monitoring and reporting requirements in i 5A NCA('02T.11 1.1 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the ease of a deviation,prior
authorization was received from the Division of Water Quality.
10. \o contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remcdiations.
II. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runotTof residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C-Certification:
"1 certify.under penalty of law.that the above information is,to the hest of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of lines and imprisonment for
knowing violations." •
f
Melinda Ward.Utility Manager 1 t(f_e( ,dg i4j?4. 2 6
1� U
Permit-tee Name and Title Hype or print) Signature of e dice Date
_ 2/18/2022
Signature of Preparer• Date " nature of La Applier Date
{ifdiffemnt from Pennitteo) (if different from Penmitee and Preparers
•Preparcr is defined in 40 CFR Part 503.9(r)and I5A NCAC 02T.1102(261 DENR FORS! ACF(I_'2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 12/31/2021
EDEN,NC
EDEN,NC MEBANE BRIDGE WWTP AEROB.DIGESTED CAKE
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
March 2021 480.00 W 99.84 D 90.55
April 2021 516.00 W 91.33 D 82.84
June 2021 264.00 W 46.73 D 42.38
July 2021 924.00 W 174.64 D 158.39
August2021 588.00 W 111.13 D 100.80
November 2021 276.00 W 52.16 D 47.31
December 2021 120.00 W 22.08 D 20.03
TOTAL 3,168.00 W 597.91 D 542.31
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 1/24/2022 1:34:58 PM

SECTION 2

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Wapoi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
2/24/2021
Synagro Central LLC/Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 21-036-0006
Project Description: Eden WWTP
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/5/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�auA.r,t 11 c &fvaiyl
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
VS/aypoint - 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401 o Fax [phone]
ANALYTICAL www.waypointanalyticalcom
Sample Summary Table
Report Number: 21-036-0006
Client Project Description: Eden WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 SM-4500-NH3C WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 9045D WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 4500NO3F-2011 WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 6010D WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 SW-7471B WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 SM-4500-NH3C-TKN WP MTN
74924 Eden WWTP Solids 02/04/2021 11:45 02/05/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN
Page 2 of 6

v
•
7621 Whitepine Road,Richmond,VA 23237
�y��I I�� Main 804-743-9401 o Fax [phone]
ANALYTICAL www.waypointanalyticalcom
46452
Synagro Central LLC/Eden Project Eden WWTP
Mary Brewer Report Date : 02/24/2021
284 Boger Road Information : Received :02/05/2021
Mocksville , NC 27028
awie frl Grow
Report Number :21-036-0006 REPORT OF ANALYSIS Pauric Mc Groary Ph.D.,CPA
Agronomist
Lab No : 74924 Matrix: Solids
Sample ID : Eden WWTP Sampled: 2/4/2021 11:45
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 79.2 % 0.010 1 02/11/21 16:39 FMM SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 3410 mg/Kg-dry 481 1 02/23/21 12:00 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 36.5 mg/Kg-dry 24.0 1 02/12/21 13:33 ZBD 4500NO3F-2011
Organic N 42900 mg/Kg-dry 1200 1 02/22/21 15:30 CALCULATION
pH 7.4 s.u. 1 02/12/21 16:40 CxC 9045D
Total Solids 20.8 % 0.010 1 02/11/21 16:39 FMM SM-2540G
Total Kjeldahl Nitrogen 46300 mg/Kg-dry 1200 1 02/22/21 15:30 JPJ ;M-4500-NH3C-TKI`
Phosphorus 20000 mg/Kg-dry 24.0 1 02/13/21 01:40 TJS 6010D
Aluminum 53400 mg/Kg-dry 240 10 02/13/21 16:35 JTR 6010D
Arsenic 8.80 mg/Kg-dry 2.40 1 02/13/21 16:30 JTR 6010D
Calcium 9090 mg/Kg-dry 240 1 02/13/21 01:40 TJS 6010D
Cadmium 2.13 mg/Kg-dry 0.481 1 02/13/21 01:40 TJS 6010D
Chromium 50.5 mg/Kg-dry 1.20 1 02/13/21 01:40 TJS 6010D
Copper 1880 mg/Kg-dry 2.40 1 02/13/21 01:40 TJS 6010D
Iron 31400 mg/Kg-dry 48.1 1 02/13/21 01:40 TJS 6010D
Lead 47.5 mg/Kg-dry 1.44 1 02/13/21 01:40 TJS 6010D
Magnesium 3050 mg/Kg-dry 24.0 1 02/13/21 01:40 TJS 6010D
Manganese 625 mg/Kg-dry 2.40 1 02/13/21 01:40 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

w•
7621 Whitepine Road,Richmond,VA 23237
\A/aypoint Main 804-743-9401 o Fax [phone]
ANALYTICAL www.waypointanalyticalcom
46452
Synagro Central LLC/Eden Project Eden WWTP
Mary Brewer Report Date : 02/24/2021
284 Boger Road Information : Received :02/05/2021
Mocksville , NC 27028
awie frl Grow
Report Number :21-036-0006 REPORT OF ANALYSIS Pauric Mc Groary Ph.D.,CPA
Agronomist
Lab No : 74924 Matrix: Solids
Sample ID : Eden WWTP Sampled: 2/4/2021 11:45
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Mercury 0.740 mg/Kg-dry 0.0730 1 02/12/21 12:04 DDB SW-7471B
Molybdenum 8.89 mg/Kg-dry 1.20 1 02/13/21 01:40 TJS 6010D
Nickel 33.1 mg/Kg-dry 1.20 1 02/13/21 01:40 TJS 6010D
Potassium 3200 mg/Kg-dry 48.1 1 02/13/21 01:40 TJS 6010D
Selenium 10.4 mg/Kg-dry 2.40 1 02/13/21 01:40 TJS 6010D
Sodium 615 mg/Kg-dry 120 1 02/13/21 01:40 TJS 6010D
Zinc 986 mg/Kg-dry 6.01 1 02/13/21 01:40 TJS 6010D
Sulfur 6680 mg/Kg-dry 48.1 1 02/13/21 01:40 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 6

s YV
Wa4pOiflt.. 7621 Whitepine Read,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytica l.com
Shipment Receipt Form
Customer Number:46452
Customer Name: Synagro Central LLC/ Eden
Report Number: 21-036-0006
Shipping Method
O Fed Ex O US Postal O Lab O Other :
® UPS 0 Client O Courier Thermometer ID:
Shipping container/cooler uncompromised? ® Yes O No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler? O Yes O No ® Not Present
Custody seals intact on sample bottles? 0 Yes O No ® Not Present
Chain of Custody(COC) present? ® Yes 0 No
COC agrees with sample label(s)? ® Yes O No
COC properly completed ® Yes O No
Samples in proper containers? ® Yes O No
Sample containers intact? ® Yes O No
Sufficient sample volume for indicated test(s)? ® Yes O No
All samples received within holding time? ® Yes 0 No
Cooler temperature in compliance? ® Yes O No
Cooler/Samples arrived at the laboratory on ice. ® Yes O No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No ® N/A
Water- VOA vials free of headspace 0 Yes 0 No ® N/A
Trip Blanks received with VOAs 0 Yes 0 No ® N/A
Soil VOA method 5035—compliance criteria met O Yes 0 No ® N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: Samantha Clarke Date &Time: 02/05/2021 13:23:58
Page 5 of 6

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Eden VVVVTP
Lot Number:WC26029
Date Completed:04/02/2021
04/06/2021 8:26 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,_0
MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WC26029
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WC26029-001
Description:EDEN WWTP Matrix:Solid
Date Sampled:03/25/2021 1110 % Solids: 17.7 03/29/2021 2117
Date Received:03/26/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 03/29/2021 2117 MOM 87239
1 350.1 (Ammonia-N )350.1 25 04/01/2021 1400 KFE 87597
1 (Nitrate-N )9056A 1 03/31/2021 0241 AMR 87625
1 (Nitrite-N )9056A 1 03/31/2021 0241 AMR 87626
1 (Phosphorus)365.1 100 03/30/2021 1247 DMA 03/27/2021 0820 87068
1 (Soil pH meas)9045D 1 03/31/2021 1334 NBW 87485
1 351.4 (TKN)351.2 10 03/30/2021 1905 DMA 03/27/2021 0820 87067
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 17.7 % 1
Ammonia-N (gas diffusion) 350.1 2800 140 73 mg/kg 1
Nitrate-N (soluble) 9056A 2.9 2.8 0.56 mg/kg 1
Nitrite-N (soluble) 9056A ND 1.1 0.56 mg/kg 1
Phosphorus 7723-14-0 365.1 24000 2800 560 mg/kg 1
Soil pH measured in water @ 19.8° C 9045D 6.4 su 1
TKN 351.2 42000 1400 1400 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/01/2021 1812 CMS2 04/01/2021 1540 87571
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 1.0 0.42 0.10 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 03/31/2021 1447 KSH2 03/30/2021 1157 87144
2 3050B 6010D 3 03/31/2021 2005 KSH2 03/30/2021 1157 87144
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 51000 96 36 mg/kg 1
Arsenic 7440-38-2 6010D 11 3.6 1.2 mg/kg 1
Cadmium 7440-43-9 6010D 2.2 1.2 0.30 mg/kg 1
Calcium 7440-70-2 6010D 9800 1200 150 mg/kg 1
Chromium 7440-47-3 6010D 51 2.4 0.60 mg/kg 1
Copper 7440-50-8 6010D 2200 7.2 3.2 mg/kg 2
Iron 7439-89-6 6010D 35000 24 11 mg/kg 1
Lead 7439-92-1 6010D 52 2.4 1.1 mg/kg 1
Magnesium 7439-95-4 6010D 3400 1200 150 mg/kg 1
Manganese 7439-96-5 6010D 780 3.6 1.4 mg/kg 1
Molybdenum 7439-98-7 6010D 10 9.6 2.4 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WC26029-001
Description:EDEN WWTP Matrix:Solid
Date Sampled:03/25/2021 1110 % Solids: 17.7 03/29/2021 2117
Date Received:03/26/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 03/31/2021 1447 KSH2 03/30/2021 1157 87144
2 3050B 6010D 3 03/31/2021 2005 KSH2 03/30/2021 1157 87144
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 34 9.6 2.5 mg/kg 1
Potassium 7440-09-7 6010D 3000 1200 150 mg/kg 1
Selenium 7782-49-2 6010D 9.9 4.8 1.9 mg/kg 1
Sodium 7440-23-5 6010D 450 J 1200 150 mg/kg 1
Zinc 7440-66-6 6010D 1200 12 3.0 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
•
Samples Receipt Cbee:klist(5RC)(MEOD1EC-151 Revised:9129/2D20
.. . ac9Araafyt,a:al issuing Authority: Pace eNV-WCUL Page 1 of 1
Sample Receipt Checklist (SRC)
Client: SYN GRO Conte:Ins ecced bqdate: ri1ru r ;YL6ltin 1 Lot li: Wc2to29
Me;firis efrece;f' I: Pace LLC1ierit j lIPS ® PedEx fl Other:
Yes n No '1_ Were custody seals present on the cooler?
h'Yes ❑No NA[2- If cangundy Beals wore prey ni,WOW.lhL'y intact arnr_ien1-rrrkcn? ,
pH$drip ID; NA Chlorine Strip ID_ 2'''It Teste_d by:NA .
Original teI perotlu a upon receipt f Decked(Corrected)temperature'upon receipt %Solid Snap. up ID: MA _-_-__.
4,5 1r 4,,1 oc Nei 11A ',c NA 11+3A GC NA ,NA oic
lvIct%nu:EiT'cJnperHL1Jrc RIHnk FAD—Lin/4 13e11I.c- ER film ID: 6 1R Cron Cnrrcclicin Fsjr;lcor: C °C
Ma'am':of saoole.at: IL Wot Ice © Ice recta ❑ Dry Ica © None •
❑Yes 0'1al OT1,rt 3. [f temperature of any cooler exceeded 6.0°C,was Project Manager Notified? •
_ [VT xras Notitied by:piioe e/err ail i face-cr-race(circle one).
inns 0Net ©NA4. Es the coer.rtiarcial courier's?acid ng slip fitac:ie1to this form?
Q Yes Li No 5. Were prOpert.untaly proeedure.A(rclinquir,€Jeclrreeeiwed)Followed?
J y4, 0 No 6. Wert HillOple i17t]ijted uo tilt COG?
/ Yes [No LL 7_ Were sample ii]s listed on all sample aantainers?
'
jf Yes � lr} -- 8_ Was cal:ectiae7 date&time listed a:i the COC?
Le--
es I I vN0 9_ Was col:ectioudate&tine:isut:lCHI all lamp le containers?
. Ye5 ❑No I(L Did all container laiel information([D,date,tine)agree with.tile COC?
C `Yes IT No 11_ Welt tests to be performed listed on the CCJC? ,
D Yes ❑ #i l2_laid all samples arrive u]ale.proper iamlBin fir cry upµ F 11.A1:..HEIKIVOr in good candid on ,
(unm-nkrm,lids ern r.rc..)? •
Z Ycs LiNo 13_ Was adequate sample volume riven la'alc9
Zi Yes ❑No I4_Were,.all tiareplts5 received within !A the holding time or48 aours,whichever comes firs_? •
DYea /JI No 15,Wareuny Hateplesmoleinerrmisain y°excess(circle ono)s�immlcs Nol listed on CUC:':
16_For VOA and RSK-l75 Sat'riplez,ware bubbles proscrt>° aa-size"[J..-Vor GJnm in diameter)
Yes ❑ 10 DNA.iri env of l:te°VOA vials?
Yes I I N° NA 17,Wzrc 8 El DROlr]1 etalsinutricnt samples reca=ved at a jiI-I of<2?
l
E
Yes Li No 7NA II Wcre ell cyanide saoneles received at a I-I> !2 and mil Flee sarilplc6l ectived at a pH?9?
E ❑ lrr Q�IA 19_ Were allapplicnble7M,,"TKNfcytuil a p emu/625,115t78.3(<O,5mg'L)9tunpics frac of
Yns
residual chlorine?
- - t1_ Were cliegt r narlssJrcquss (Lc.requested dilutions,MSJMSD desigiatione,,etc...)
U`fesl ❑�10 E1NJ
correctly lrariscriIs d from lEic CCIC into the comment section in LIMP
l Y. ❑No 21.Way Ithe ii,oule nu+nber Eistxxi on tho coa,aincr label?If yes,Qnote;t
Sample Presenimiuu (Must be completed for any sample(s) incorrectly preserved or wit 1]eadcp ce.)
Samples) NA were received ineonecrly preserved a:id vieee o lj:esshid uocr,rdinLEy
:i m p1Et r#,rk,iving with NA mL of circle OM H2SO4,HN 03,HC1,NnO H using SR# t`A .
Tim;o:preservation r' . ]f inoi a than c li preser 'ativLt is recdodc please note in the com]nea3 below.
'Sample(s) • were:ecehod wilEi bubbles>6:i_n in diameter.
Samples(s) hn wereJtx:eivex[witE. TRC'L.-0.c m t1..(If#]9 isun)and were
adjusted accordingly nl sample receiving,With so lwi c Ili w a]FiLo(NA,320j)with She;ly ID;D, Ni•
•
SR_6erc ela1>,eEsappliedby; Ri:12_ — [dare 3r2f 02]
Comments: — -_
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Eden
Lot Number:WG01035
Date Completed:07/12/2021
Project Manager:Lucas Odom
07/12/2021 4:00 PM
Approved and released by:
Project Manager II: Kathy E. Smith
MILD
'ye I ANSI NatlonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety,without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WG01035
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals
The method blank associated with batch 97691 had Potassium and Sodium detected at a concentration
that was above the MDL but below '%the PQL. All samples associated with this method blank that have
detections for Potassium and Sodium have been flagged with a "B".
Pace Analytical Services,LLC(formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WG01035
Sample Number Sample ID Matrix Date Sampled Date Received
001 EDEN Solid 06/30/2021 1310 07/01/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:WG01035-001
Description:EDEN Matrix: Solid
Date Sampled:06/30/2021 1310 %Solids: 18.9 07/01/2021 2335
Date Received:07/01/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 350.1 (Ammonia-N)350.1 25 07/07/2021 1117 KFE 97967
1 (Nitrate-N)9056A 1 07/07/2021 1405 AMR 98232
1 (Nitrite-N)9056A 1 07/07/2021 1405 AMR 98238
1 (Phosphorus)365.1 100 07/08/2021 1535 DMA 07/07/2021 1615 98126
1 (Soil pH meas)9045D 1 07/04/2021 1806 NBW 97864
1 351.4 (TKN)351.2 10 07/09/2021 1242 DMA 07/07/2021 1535 98116
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ammonia-N (gas diffusion) 350.1 2400 130 69 mg/kg 1
Nitrate-N (soluble) 9056A 9.4 2.6 0.53 mg/kg 1
Nitrite-N (soluble) 9056A ND 1.1 0.53 mg/kg 1
Phosphorus 7723-14-0 365.1 23000 2600 530 mg/kg 1
Soil pH measured in water @ 19.7° C 9045D 7.0 su 1
TKN 351.2 33000 2600 1300 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:WG01035-001
Description:EDEN Matrix: Solid
Date Sampled:06/30/2021 1310 %Solids: 18.9 07/01/2021 2335
Date Received:07/01/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 07/07/2021 1709 CMS2 07/06/2021 1320 97801
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.59 0.42 0.10 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:WG01035-001
Description:EDEN Matrix: Solid
Date Sampled:06/30/2021 1310 %Solids: 18.9 07/01/2021 2335
Date Received:07/01/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 07/06/2021 1452 JMH 07/06/2021 0413 97691
2 3050B 6010D 5 07/07/2021 1312 KSH2 07/06/2021 0413 97691
3 3050B 6010D 10 07/08/2021 1045 JMH 07/06/2021 0413 97691
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 51000 160 59 mg/kg 2
Arsenic 7440-38-2 6010D 7.3 1.2 0.39 mg/kg 1
Cadmium 7440-43-9 6010D 1.7 0.39 0.099 mg/kg 1
Calcium 7440-70-2 6010D 8700 390 49 mg/kg 1
Chromium 7440-47-3 6010D 40 0.79 0.20 mg/kg 1
Copper 7440-50-8 6010D 2300 7.9 3.5 mg/kg 3
Iron 7439-89-6 6010D 30000 39 18 mg/kg 2
Lead 7439-92-1 6010D 46 3.9 1.8 mg/kg 2
Magnesium 7439-95-4 6010D 2600 390 49 mg/kg 1
Manganese 7439-96-5 6010D 510 1.2 0.47 mg/kg 1
Molybdenum 7439-98-7 6010D 8.5 3.1 0.79 mg/kg 1
Nickel 7440-02-0 6010D 27 3.1 0.83 mg/kg 1
Potassium 7440-09-7 6010D 2300 B 390 49 mg/kg 1
Selenium 7782-49-2 6010D 7.8 J 7.9 3.2 mg/kg 2
Sodium 7440-23-5 6010D 590 B 390 49 mg/kg 1
Zinc 7440-66-6 6010D 1000 20 4.9 mg/kg 2
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
samples Re eipt CheddJst{SRC; (Mroo113C..15) Rewised:9Jz9/2020
./.2veAnalieliarl I5.5 a i 1f Authority:Pace ENV•WCOL Page 1 of 1
Sample Receipt lie c ist (SRC)
Cliti]t; SYNAGRO _Cooler Enspecied_bvidarc: KD r o-ruIr2c2! Lot i: VTO'o}i
Means of receipt: Pace — C[iu,i - LIPS 1•-odLx )iher' -
Yts. d 14� '1. Were.cu.s.tcdyaea[€present orl Use.Luplcrr — — —
❑Ye-s No ,, NA-2. If custody se-u[s wcr prewen v.cr4 ih y*act arid wthrr.ken'f -
pH Strip ID: FA Chtorino Strip ID: NA "i ested by:i'..-Lai.--.
Original tetnpvratu,e upoir reecdpi f] iced.(Conned)tempera =upon roceipt %Solis Snap-Cup]T3: °1-24.'
i- i 1.,3 uc NA 1 NA NA i NA cc NA ,NA ae
Me,hod: ❑lemperatt]re Blank IThiainst 13otticx IR Gun ID: 5 1R. ri'.rr]Co-ection Factor: l] c,
Method of coolant: E Wet Ice U Tex.PaMks ❑ D]xr tee ElNone J I '
3_ Ir tYmpend:arc of arty cooler exceeded 6-0°T,WM Ptoj wet Manage,.Notified? i
❑Yew n Na LINA PM was NaLi led by:phone,'email I taco to-fcce(circle one). •
Q Yes No ❑NA 4. Ts the commercial touricr'S racking slip attached ce this fe}rrr?
❑] Yes !Ni . We=c proper custody procedures(re:lnqu shod/received', followed?
/ les, J N:, 6. W.=sani pie]D :fisted ao the COC? -'flii Yes: n Al_, 7. Wcr,san,plc;=r]a:isnei an all sun*a ntuiners?
❑J YeN D Flo' 8. Was collection data 3t time listed an the O L?
1-�Yee No� 5►. Was collection el to&fine listed.a_r an i u,1p le r:;a:ltaincrs7 j
0 Yer. ❑Ro ,[0-Did ewll container label information(ID,r0at;t=De)agree with Ow CDC?
aYe3 flTs-o I.I.Wcre tests to be pm-Farmed]iet.:J an toe'oc
0>i a l2,Did ail saeu pl es arrive in the proper contain e.r3 for each rasT aacVor in good condition
(unbroken, t'ds OD:etc.)?
i.IDeY T1� u ;]3, WOttdor{tl le sample volume atiniltible —
I Ycs No! 14. Were air sampies received within 14 the holding time or 4g hours.,whichever comes first?
12 Yeti 77/1No _ IS. Were any 2i]nplcs c:]n1Iin.1. missing/excess(circle orm)semples Not listed on CO 2 i
1[6. For'VOA and [tSK-173 sanip[es,WON.babbles presant>"pea-s[ze"(1.4"frr Cm m in inmeter)
]]Yes; ❑No n V, m any of the VOA vials'?
r Yes. U No I NA 17. Were all D1 C,'rtlel alsr'n;rticnt samples r€echoed in-a pH cf'2? .I
1e 1 I No; jNA 1 S-Were ah cyan i(IC a impl es received at a p-1> 12 and su f fide samplsw re.ue i v;.d At x pH} 9? S1
19. Wee all applicab;e NH3J1.1{Alley[IicleIplrenm11625-li608.3 (V 0.3rng'[)samRf riac of
E]Yes ©No riNA
residual chlorine?
n 20, Were Clinch:remarks1requesls(Le.requcs.ed dilutions,MSJMSii designations,etc.--)
❑Ye.9 El Na NA1 i
Correctly transcribed fro n Ih4 COC into the commenr Fe( inn in LIMB?
0 Yesi El Ma 21, Was thequote 1ursilwr]istvd on the VON VONQ ur�t,:it _ —
ample PreseruatInio (Must be completed for env sumpfr:(s)incorr:c:ly preserved ix with]teadspace
.)
am p:c(s) "•4 were_e]:e]wed ncorrectly piegervetl hod wra-es adius ed tic„orJingly ,
in sample receiving with NA ma,of oirtJe or-e: FI2SC4,I1NO3, HCl. NaOH using bR 0 NA
'Time of preservation NJA _- If more r'] ,t one preserwat:vc is fleeted,pJeawe nol C in the comments below.,
l
Sun 1' were rcceivcd with 1 iibbles>I mm dim in di 'platcr.
u
Sarnpte;,(s) a WCrs reoeiv with TRC 0,5 ma.([f419 is rrv)and erc
• ad_WIcd uuordingly in sample llroeivinn,will.' fioditim t:tiosilfate(NarS 03)with Shoaly II): NA
SR barcade IuLclx applied hy_ K.Drvkr - T]atr; O7J61ii2 0=:
,--.—.J.
Conon:10 x:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 9

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Eden
Lot Number:WK03056
Date Completed:11/21/2021
Ola
11/22/2021 3:24 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,c_0‘
MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WK03056
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the following samples have an initial weight that is 3x greater
than standard procedure: WK03056-001. The LOQ has been adjusted accordingly.
Inorganic Non-Metals
The following sample was diluted due to the nature of the sample matrix: WK03056-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WK03056-001
Description:EDEN Matrix: Solid
Date Sampled:11/01/2021 1340 %Solids: 18.4 11/04/2021 0111
Date Received:11/02/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 11/04/2021 0111 MOM 21214
1 350.1 (Ammonia-N)350.1 25 11/20/2021 2038 DRD 22997
1 (Nitrate-N)9056A 5 11/10/2021 1518 AMR 22147
1 (Nitrite-N)9056A 5 11/10/2021 1518 AMR 22153
1 (Phosphorus)365.1 120 11/04/2021 1717 DMA 11/04/2021 1019 21253
1 (Soil pH meas)9045D 1 11/07/2021 1755 NBW 21588
1 351.4 (TKN)351.2 10 11/05/2021 1233 DMA 11/04/2021 1312 21269
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 18.4 % 1
Ammonia-N (gas diffusion) 350.1 2200 140 71 mg/kg 1
Nitrate-N (soluble) 9056A 17 14 2.7 mg/kg 1
Nitrite-N (soluble) 9056A ND 5.4 2.7 mg/kg 1
Phosphorus 7723-14-0 365.1 24000 3300 650 mg/kg 1
Soil pH measured in water @ 20.8° C 9045D 7.1 su 1
TKN 351.2 36000 2700 1400 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 11/16/2021 1708 JAB2 11/15/2021 1536 22152
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.62 0.41 0.099 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 11/09/2021 1438 KSH2 11/09/2021 0403 21598
2 3050B 6010D 3 11/09/2021 1652 KSH2 11/09/2021 0403 21598
3 3050B 6010D 10 11/09/2021 1656 KSH2 11/09/2021 0403 21598
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 46000 100 39 mg/kg 2
Arsenic 7440-38-2 6010D 9.4 1.3 0.43 mg/kg 1
Cadmium 7440-43-9 6010D 1.8 0.43 0.11 mg/kg 1
Calcium 7440-70-2 6010D 8700 430 54 mg/kg 1
Chromium 7440-47-3 6010D 38 0.86 0.22 mg/kg 1
Copper 7440-50-8 6010D 2200 8.6 3.9 mg/kg 3
Iron 7439-89-6 6010D 30000 26 12 mg/kg 2
Lead 7439-92-1 6010D 51 2.6 1.2 mg/kg 2
Magnesium 7439-95-4 6010D 2300 430 54 mg/kg 1
Manganese 7439-96-5 6010D 590 1.3 0.51 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WK03056-001
Description:EDEN Matrix: Solid
Date Sampled:11/01/2021 1340 %Solids: 18.4 11/04/2021 0111
Date Received:11/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 11/09/2021 1438 KSH2 11/09/2021 0403 21598
2 3050B 6010D 3 11/09/2021 1652 KSH2 11/09/2021 0403 21598
3 3050B 6010D 10 11/09/2021 1656 KSH2 11/09/2021 0403 21598
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Molybdenum 7439-98-7 6010D 10 3.5 0.86 mg/kg 1
Nickel 7440-02-0 6010D 26 3.5 0.91 mg/kg 1
Potassium 7440-09-7 6010D 1600 430 54 mg/kg 1
Selenium 7782-49-2 6010D 9.3 5.2 2.1 mg/kg 2
Sodium 7440-23-5 6010D 550 430 54 mg/kg 1
Zinc 7440-66-6 6010D 1800 13 3.2 mg/kg 2
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Sarni,leS Receipt Checklist(SRC)(14INiniac-isa Revised: /29f2020
t'rl,y? •al. Issuing Autharvy:Pace ENV-WCOL Rage;:of 1
Sample Receipt Checklist (SRC)
Client 4w6;101ro
Gaoler Irtspeclai byidate: JR[:2 1 L11A73!201 Lot,, . V1 030 n
Way orft"lpt: ,7 Para Clicnt ' UPS / FcdEx f.]the3•7 —
Yeg Iv' No 1. Were custody seal -o ent on tht cooler
Ye,; L . o. ..._ If s to y r+ea Is WI' pes cot,were#hc•intact and u u brok en 7 —
p]1 Ship 1D_ N . Clt]orine Strip ID: NA L _ Tested by —
Original temperature upon receipt/Derived(Corrected)temperature upon receipt %So]id$no-9p.o.ip [D: 21-192s
4.5 .0.5 et NA +rc or-+ NA INA ec NA /NA oc —
Mcihod:©Ts,rllxarlture 13]unk IapirotBo tlee 2l.Gun 11.1: d Ili Cam Correct ill Factor: {' u•C
iWetLtuJ cofroolanl ❑ Wet Ice r I Ice 1'aeks� 1D]y ke CI None
U y43 �]No[I f1tiA 3_ if[,emptrature of flay cooker exceeded 6,0"C, o i Prnjert mans •N.06i, d?
PM ve Notified iy:phone i emril 1 f'nu-to-face(circ:io one),
7es — No ❑N 4 4- Is the c rnrrxrcia]courir.-'s puking ing slip atracheri to this furm7
cs _No 5_ V4'erc pauper cnstod�larurcdtn S(r HnquisliCdfnccived)followed?
c5 No6. 1Cre3 `kICJl3sIlgta Orl the CI?C7es Not 7. 1+Lre sample Ii. :it;kx]on all sample cxant rincrs7 �I
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Ye.: l'o _ $. Was col dale&drne listed ea the COC7
Yes ❑No 19. Was coup.:ion date&time Liam/on all sample co.itaine m? —
cs II-�No •='J Did a:l container lalacl information(10,date,4mc)a wiI i die CDC? .
fl Yes ]� o 1 1_Were testy to be performed listod on the COG?
Yea ©No 12. DM Lill sum riles arrive in[he proper armlrine s for each[Est andf r in p.00d condition
1(.111417'Oken, [ids on,ctc,)'/ - - —
0 Yes LJ No 13.Wii ude re!mrple volume avaiiab lc?
ED Yes LN0 14. Were all Sfziplcs received witltite V.the holding time orlt$hours,whichever comes first? .
Yes U Na 15. Werc any sample3 containers issfn execs[circle one)flduiplcs Nog Iis[ed an COC?
LiYeg ONo [71+1,4 I . per VOA and RSK-173 santplca,were blIMILes pr&boit-"pea- ize"(Arar6rrtrn in dimmer) '
in any of the YOA vials':
Yes I]hl a 0 NA I;_ Were all D1 QhnetalsJn u lrietat r 'r.s received a!:P pl.!of<3'r'
Yes MI No d NA'18- Wor:all t rrnide 3ai i i plcn recei.vcd at a pH> 12 and suIfido sa,n 'es rceicivd all t,pH>9?
]fa3 I]No 17II A 1`-Wc:a all applierIble NJ-1 cyanid r.1ry cool: 25,I U,5tiigr2., sam plen free of
ie'thIti9I chlorine?
Dyes Leto M' NAi2a. Wire client remarks+rOqucsts(Lc.. requested cliltotior_s, MS/MSD design.atioims,plc,,,)
ix/Treaty transi;ribcd born the COC into rye comments :Lion in LIMB?
1Yes I Pi No 2], Was[fee gIune number listed on the eoetc,incr I abt1? If yes,Quote Ili —
Sample Freservution (Mist be completed for any sam] Lo(h)incorree.r v pose(vaxl or whh hudspare_)
Satnple(s). `41. 7 _ were FM:Lived incorrectly prc1crrcd and WIC'adjuslctl acco:rdirtr.ry .
i n saml le r{x;niving with N mL of eiEC]C one: !J2SO4,HNO3,HCI,NaOF using SR# N.' _
Time of pre5erval,ion 14A If Ilion:than erie preserv1L;vc is needed,please 7aie in the comments below,
Samp]°(s) MA — — — war:I ete=wed wilt bubbles:}
6 mm in di_ arncr.
Sarriplos(sl were received with TC C>0 5 m/L(I I#l9 is ran)and were
adjusted accordingly iessamplee;Toth inl with sodiumilii[_1sult2[e(Na257D3)with Shealy]D: NA
Sli l rcvde labels applied by;
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Comments` —
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 19.12
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Michael Nichols Owner: Michael Nichols Predominant Soil Series: Clifford
Acres Used: 2.6 Acres Permitted: 2.6 Site#: NC RC 00005 Field#: RC 00005 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use rng/kg, % Solids use Raw Percent#):
Sample or 1 2 , 3 41 5 6 8 91 10 j 11: 121
Cam-
posite
Date 3/25/21
%Solids 17.7
Arsenic 11
Cadmium 2.2
Copper 2200
Chromium 5I
Lead 52
Mercury_ 1
Molyb- 10
denum _
Nickel 34
Selenium 9.9
Zinc 1200
Total
Phos- 24000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 'J 2. 3 4 5 6 71 8 1 _9 10 11 12
DT/Ac./
App. a_
Event 7.35
Arsenic 0.162 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.162
Cadmium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
Copper 32.349 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.349
Chromium 0.750 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.750
Lead . 0.765 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.765
Mercury 0.015 0.000 0.000 0.000 0.000 0.000 0.00(1 0.000 0.000 _ 0.000 0.000 0.000 0.015
Molyb- 0.147 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.147
denum
Nickel 0.500 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.500
Selenium 0.146 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.146
Zinc 17.645 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 17.645
Total
Phos- 352.896 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 352.896
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Rt Ctce ��J fZ7
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Dry Tons Applied (Annual): 25.49
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Michael Nichols Owner: Michael Nichols Predominant Soil Series: Clifford
Acres Used: 18.7 Acres Permitted: 18.7 Site#: NC RC 00005 Field#: RC 00005 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 , '2(1 3 4 5' 6 7 j 81 _9 1 10 11 12
Com-
posite
Date 3/25/21
%Solids 17.7 _
Arsenic 11
Cadmium 2.2
Copper 2200
Chromium 5 I
Lead 52
Mercury I
Molyb- 10
denum
Nickel 34
Selenium 9.9 _
Zinc 1200
Total
Phos- 24000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 3 41 5 6 7 8 9 10 11 121
DT/Ac./
App.
Event 1.36
Arsenic 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030
Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006
Copper 5.997 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.997
Chromium 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139
Lead 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.142
Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb- 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
denum
Nickel 0.093 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093
Selenium 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Zinc 3.271 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.271
Total
Phos- 65.424 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 65.424
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
VYM 1,r,P6CA44 2.41107-3
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Drp Tons Applied(Annual): 46.48
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Clover
Acres Used: 9.1 Acres Permitted: 9.1 Site#: NC RC 00011 Field#: RC 00011 D001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2i 3 P4 5 6 8 9 1Q 11 12]
Com-
posite
Date 3/25/21 6/30/21
%Solids 17.7 18.9
Arsenic 11 7.3
Cadmium 2.2 1.7
Copper 2200 2300
Chromium 51 40
Lead 52 46
Mercury 1 0.59
Molyb- 10 8.5
denum _
Nickel 34 27 _
Selenium 9.9 7.8 _
Zinc 1200 1000
Total
Phos- 24000 23000
phorus _
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 _ 2' 31 41 5 6 ' 71 8 9 '10 11 12 ;
DT/Ac./
App.
Event 1.87 3.24
Arsenic 0.041 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.088
Cadmium 0.008 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019
Copper 8.215 14.904_ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 23.119
Chromium 0.190 0.259 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.450
Lead 0.194 0.298 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.492
Mercury 0.004 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.008
Molyb 0 037 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.092
denum Nickel 0.127 0.175 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.302
Selenium 0.037 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.088
Zinc 4.481 6.480 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.961
Total
Phos- 89.616 149.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 238.656
phorus _
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1ZYCW CIWK-3W)
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 79.38
Permit#: WQ0002035 Cation Exchange Capacity (non 503 only):
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Clover
Acres Used: 17.1 Acres Permitted: 17.1 Site#: NC RC 00011 Field#: RC 00011 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 21 3 4 5 6 I 7 81 91 10 1- 11 12
Com-
posite
Date 6/30/21
%Solids 18.9
Arsenic 7.3
Cadmium 1.7
Copper 2300
Chromium 40
Lead 46
Mercury 0.59
Molyb-
8.5
denum
Nickel 27
Selenium 7.8
Zinc 1000
•
Total
Phos- 23000
phorus
Annual Heavy Metal Field Loadings(Calculated in lbs/acre):
Total 1( ' 2 31 41 51 6 7J 8 91 10 11 12
DTIAc./
App.
Event 4.64
Arsenic 0.068 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _0.000 0.000 0.000 0.068
Cadmium 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016
Copper 21.353 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 21.353
Chromium 0.371 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.371
Lead 0.427 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.427
Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Molyb- 0 079 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.079
denum
Nickel 0.251 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.251
Selenium 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072
Zinc 9.284 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.284
Total
Phos- 213.532 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 213.532
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
APJ 60(t1 Z(e/ZZ
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 24.95
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Clover
Acres Used: 16.8 Acres Permitted: 16.8 Site#: NC RC 00011 Field#: RC 00011 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 11 21 31 41 5 6 7' 8 91 10 12
Corn-
posite
Date 6/30/21
Solids 18.9
Arsenic 7.3
Cadmium 1.7
Copper 2300
Chromium 40
Lead 46
Mercury 0.59
Molyb-
8.5
denum _
•
Nickel 27 _
Selenium 7.8
Zinc 1000
Total
Phos- 23000
phorus ,
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 2 3 5 6 71 8 9 10 11 12_1
DT/Ac./ 0-3
App.
Event 1.49
Arsenic 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ` 0.000 0.000 0.000 0.022
Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Copper 6.831 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.831
Chromium 0.119 _0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119
Lead 0.137 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.137
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025
denum
Nickel 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.080
Selenium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023
Zinc 2.970 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.970
Total
Phos- 68.310 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.310
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
PPis• (pA Zi lel zz
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied (Annual): 59.22
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only);
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Lackwtown
Acres Used: 12.8 Acres Permitted: 12.8 Site#: NC RC 00011 Field#: RC 00011 0004
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2. ±I 4 5J 6 7 8 9 10 11 12
Com-
posite
Date 3/25/2 1 6/30/21
%Solids 17.7 18.9
Arsenic 11 7.3
Cadmium 2.2 1.7 J
Copper 2200 2300
Chromium 51 40
Lead 52 46
Mercury 1 0.59
Molyb- 10 8.5
denum
Nickel 34 27
Selenium 9.9 7.8
Zinc 1200 I000
Total
Phos- 24000 23000
phorus
Annual Heavy Metal Field Loadings(Calculated in lbs/acre):
Total _� j 2 ' 3 ' 4] 5 6 7 8 9 10 11 12 '
DT/Ac.I - o
App.
Event 2.32 2.31
Arsenic 0.051 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.085
Cadmium 0.010 0.008 0.000 0.000 0.000 0.000 0.000 0.000 _0.000 0.000 0.000 0.000 0.018
Copper 10.221 10.612 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.833
Chromium 0.237 0.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.422
Lead 0.242 0.212 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.454
Mercury 0.005 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Molyb 0.046 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.086
denum
Nickel 0.158 0.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.283
Selenium 0.046 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.082
Zinc 5.575 4.614 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.189
Total
Phos- 111.504 106.122 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 217.626
phorus
"I certify,under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
ilki/V\) 601)e1.14\-n
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 9.07
Permit#: WQ0002035 Cation Exchange Capacity (non 503 only):
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Lacwtown
Acres Used: 2.3 Acres Permitted: 2.3 Site#: NC RC 00011 Field#: RC 00011 0005
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2 3' 4 5 6 j 7 8 910 11 12
Com-
posite
Date 6/30/21
°o Solids 18.9
Arsenic 7.3
Cadmium 1.7 _
Copper 2300
Chromium 40
Lead 46
Mercury 0.59
Molyb-
8.5
denum _
Nickel 27
Selenium 7.8
Zinc 1000
Total
Phos- 23000
phorus _
Annual Heavy Metal Field Loadings(Calculated in Ibs/acre):
Total ._1 ; 2 ' 3J 4J 6 7j 8 9 10 1 i i 12
DT/Ac./
App.
Event 3.94
Arsenic 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058
Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 18.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 18.142
Chromium 0.316 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.316
Lead 0.363 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.363
Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Molyb- 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067
denum
Nickel 0.213 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.213
Selenium 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062
Zinc 7.888 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.888
Total
Phos- 181.424 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 181.424
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1Z-rAlo Meek;: %' -21(fILZ
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Dry Tons Applied(Annual): 45.36
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Gray Tuttle Owner: Gray Tuttle Predominant Soil Series: Clover
Acres Used: 11.6 Acres Permitted: 11.6 Site#: NC RC 00011 Field#: RC 00011 0006
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1. 2 3_ 41 5 ; 6 7_1 8 9 101 11 12
Com-
posite
Date 6/30/21
%Solids 18.9
Arsenic 7.3
Cadmium 1.7
Copper 2300
Chromium 40
Lead 46
Mercury 0.59
Molyb-
8.5
denum _
Nickel 27
Selenium 7.8
Zinc 1000
Total i
Phos- 23000
phorus
Annual Heavy Metal Field Loadings(Calculated in lbs/acre):
Total ' 1 1 _2 31 4] 5 6 i 8 9 10 11 12
DT/Ac./
App.
Event 3.91
Arsenic 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057
Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 17.986 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 17.986
Chromium 0.313 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.313
Lead 0.360 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.360
Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Molyb- 0 066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066
denum
Nickel 0.211 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.211
Selenium 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.061
Zinc 7.820 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.820
Total
Phos- 179.860 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 179.860
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
!2`;4"J C9p0"^-49 4977Z,
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Dry Tons Applied (Annual): 57.41
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Claude French Owner: Claude French Predominant Soil Series: FRD2
Acres Used: 20.4 Acres Permitted: 20.4 Site#: NC RC 00026 Field#:RC 00026 0001B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 3 4 i 5 6 7 8 9 j i D 11 12 r
Com-
posite
Date 2/4/21
%Solids 20.8
Arsenic 8.8
Cadmium 2.13
Copper 1880
Chromium 50.5
Lead 47.5
Mercury 0.74
Molyb- 8.89
denum
Nickel 33.1
Selenium i 0.4
Zinc 986
Total
Phos- 20000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 ' 2 ' 3 4; 5 6 7 8 9 10 1i 12
DT/Ac./
App.
Event 2.81
Arsenic 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050
Cadmium 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012
Copper 10.581 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.581
Chromium 0.284 0.000 0.000 0.000 0.000 0.000 0.000 r 0.000 0.000 0.000 0.000 0.000 0.284
Lead 0.267 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.267_
Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Molyb- 0 050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050
denum
Nickel 0.186 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.186
Selenium 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059
Zinc 5.549 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.549
Total
Phos- 112.560 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 112.560
phorus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
gyAAAJ CAP 017 z
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Dry Tons Applied (Annual): 46.73
Permit#: WQ0002035 Cation Exchange Capacity (non 503 only):
Operator: Michael Nichols Owner: Elmer Dickerson Predominant Soil Series: Clifford
Acres Used: 9 Acres Permitted: 9 Site#: NC RC 00028 Field#: RC 00028 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2 1 3 4 5 , 6J 71 8 9 101 11 121
Com-
posite
Date 3/25/21
%Solids 17.7
Arsenic 11
Cadmium 2.2
Copper 2200
Chromium 51
Lead 52
Mercury I
Molyb- 10
denum
Nickel 34
Selenium 9.9
Zinc 1200
Total
Phos- 24000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total L1.] 2' 3 I 4J 5 6 7 8 9 10 11 12
DT/Ac./
App.
Event 5.19 `•
Arsenic 0.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.114
Cadmium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023
Copper 22.845 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 22.845
Chromium 0.530 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.530
Lead 0.540 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.540
Mercury 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010
Molyb- 0104 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104
denum
Nickel 0.353 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.353
Selenium 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103
Zinc 12.461 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.461
Total
Phos- 249.216 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 249.216
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/44\-)
(,,OFELA-kr) 2/irv12Z
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden,NC Total Dry Tons Applied(Annual): 74.24
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Tommy Strader Owner: Tommy Strader Predominant Soil Series: Banister
Acres Used: 8.9 Acres Permitted: 8.9 Site#: NC RC 00045 Field#:RC 00045 0001A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 3 4J 5 6 8 91 10 11 12 j
Com-
posite
Date 6/30/21 1 1/1,2 I _
%Solids 18.9 18.4 _
Arsenic 7.3 9,4
Cadmium 1.7 I.8
Copper 2300 2200
Chromium 40 38 _
_ Lead 46 51
Mercury 0.59 0.62
Molyb-
denum 85 10
Nickel 27 26
Selenium 7.8 9.3
Zinc 1000 1800
Total
Phos- 23000 24000
phorus _
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total _1 21 3 _4i 5 61 71 8 9 10 11 12
DT/Ac./ V o
App. m_
Event 5.86 2.48
Arsenic 0.086 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.132
Cadmium 0.020 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029
Copper 26.956 10.912 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 37.868
Chromium 0.469 0.188 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.657
Lead 0.539 0.253 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.792
Mercury 0.007 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010
Molyb- 0100 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.149
denum
Nickel 0.316 0.129 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.445
Selenium 0.091 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.138
Zinc 11.720 8.928 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 , 0.000 20.648
Total
Phos- 269.560 119.040 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 388.600
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1 (c(uzA10 2 OP
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 68.04
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Tommy Strader Owner: Tommy Strader Predominant Soil Series: Clifford
Acres Used: 12.8 Acres Permitted: 12.8 Site#: NC RC 00045 Field##: RC 00045 0002
Residual Analysis'' 'Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or I-1 3r 5 6 7' ` 8I 9, 10 11 ; 12
Com-
posite
Date 6/30/21 _
%Solids 18.9
Arsenic 7.3
Cadmium 1.7
Copper 2300
Chromium 40
Lead 46
Mercury 0.59
Molyb-
8.5
denum
Nickel 27 _
Selenium 7.8
Zinc 1000
Fula!
Phos- 23000
phorus
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total 1j 2 1 3' 4 5. 6 7 8 9 10 11 12
DT/AcJ
App. LT
Event 5.32
Arsenic 0.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.078
Cadmium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018
Copper 24.454 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 24.454
Chromium 0.425 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.425
Lead 0.489 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.489
Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006
Molyb- 0 090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090
denum _
Nickel 0.287 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.287
Selenium 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.083
Zinc 10.632 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.632
Total
Phos- 244.536 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 244.536
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/` V 6p'VOcht
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden.NC Total Dry Tons Applied(Annual): 42.43 _
Permit#: WQ0002035 Cation Exchange Capacity(non 503 only):
Operator: Charles O'Bryant,Jr. Owner: Charles O'Bryant, Jr. Predominant Soil Series: Clifford
Acres Used: 13.4 Acres Permitted: 13.4 Site#: NC RC 00117 Field#: RC 00117 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or I I 2 3J 4I 51 6J f7j SI 91 10 11 12{
Corn-
posite
Date 2/4/21 _
%Solids 20.8 _
Arsenic 8.8 _
Cadmium 2.13
Copper 1880
Chromium 50.5
Lead 47.5
Mercury 0.74
Molyb- $ $9
denum
Nickel 33.1
Selenium 10.4
Zinc 986
Total 1
Phos- 20000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1F ; 2 3 4 5' 7 B 9' 10. 11 12', '
App.
F
Event 3.17
Arsenic 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 11.908 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.908
Chromium 0.320 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.320
Lead 0.301 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.301
Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Molylr 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
denum
Nickel 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210
•
Selenium 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066
Zinc 6.245 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.245
Total
Phos- 126.680 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 126.680
phorus
"I certify,under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
K-4 irri C�� 4/3/ZZ
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

S
a i' Summit Environmental Technologies,Inc.
inIrg 3310 Win St.
ENVIRONMENTAL TECHNO LOCiES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boraIi rlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
December 30, 2020
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL: [phone]
FAX: [phone]
RE: Eden-REVISED
Dear Ryan Copeland: Order No.: 20121120
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/18/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 37

5 M�'� Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraioriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 20121120rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 12/30/2020
CLIENT: Synagro
Project: Eden-REVISED
WorkOrder Narrative:
20121120: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20121120-001a TCLP-SVOC-CPEST(8081B): Possible low bias for Methoxychlor due to poor
recovery in ending CCV. Other ending CCV's, including on confirmation column(R121734) exhibit
similar results. Compound demonstrates adequate sensitivity in RLC.
Analytical Sequence QC Notes:
20121120-001AMS/MSD TCLP-SVOC-CPEST(8081B): Possible low bias for Methoxychlor due to
poor recovery in ending CCV. Other ending CCVs, including on confirmation column (R121734)
exhibit similar results. Compound demonstrates adequate sensitivity in RLC.
MB/LCS-46981 TCLP-SVOC-CPEST(8081B): Possible low bias for Methoxychlor due to poor
recovery in ending CCV. Other ending CCVs, including on confirmation column (R121734) exhibit
Revision vl
Page 2 of 37

Summit Environmental Technologies,Inc.
5I.I1u1Lf1I1 3310 Win St. Case Narrative
mu
ENVIRONMENTAL TECHN❑LOCI $,INC. Cuyahoga Falls,Ohio 44223 WO#: 20121120
rrafy0cal yt�caf Laboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 12/30/2020
CLIENT: Synagro
Project: Eden-REVISED
similar results. Compound demonstrates adequate sensitivity in RLC.
REVISED REPORT 12/30/20: Includes QC Summary Report pages for TCLP Herbicices.
Revision vl
Page 3 of 37

•
17 S
Mm iT Summit Environmental Techno3310Wlogies,Ins
Qualifiers and Acronyms
EkiwllxsStJM@N1'nLTecriw❑LOG{ES.INC Cuyahoga Falls,Ohio 442 WO#: 20121120
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 12/30/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 37

S t�' Summit Environmental Technologies,Inc. Workorder
3310 Win St.
1.7 ENVIRONMENTAL TECHNQI.QC,3ES,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 20121120
Website:http://www.settek.com 30DeC-20
CLIENT: Synagro
Project: Eden-REVISED
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
20121120-001 Eden TCLP 12/17/2020 9:52:00 AM 12/18/2020 10:20:00 AM Sludge
Page 5 of 37

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it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENb1R01JMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 20121120
Website:http://www.settek.com Date Reported: 12/30/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/17/2020 9:52:00 AM
Lab ID: 20121120-001A
Project: Eden-REVISED
Client Sample ID Eden TCLP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00500 mg/L 1 12/23/2020 4:29:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 12/23/2020 12:19:38 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 12/23/2020 12:19:38 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 12/23/2020 12:19:38 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 12/23/2020 12:19:38 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 12/23/2020 12:19:38 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 12/23/2020 12:19:38 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 12/23/2020 12:19:38 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 12/22/2020 8:33:00 PM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 12/22/2020 8:33:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 12/22/2020 8:33:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 12/22/2020 8:33:00 PM
Cresols,Total ND 10.0 mg/L 2 12/22/2020 8:33:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 12/22/2020 8:33:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 12/22/2020 8:33:00 PM
Hexachloroethane ND 0.200 mg/L 2 12/22/2020 8:33:00 PM
Nitrobenzene ND 0.200 mg/L 2 12/22/2020 8:33:00 PM
Pentachlorophenol ND 0.500 mg/L 2 12/22/2020 8:33:00 PM
Pyridine ND 0.500 mg/L 2 12/22/2020 8:33:00 PM
Surr:2-Fluorophenol 78.4 10-157 %Rec 2 12/22/2020 8:33:00 PM
Surr: Phenol-d6 88.2 10-169 %Rec 2 12/22/2020 8:33:00 PM
Surr: Nitrobenzene-d5 80.0 32.1 -130 %Rec 2 12/22/2020 8:33:00 PM
Surr:2,4,6-Tribromophenol 95.0 45.4-166 %Rec 2 12/22/2020 8:33:00 PM
Surr:2-Fluorobiphenyl 91.2 35.7-130 %Rec 2 12/22/2020 8:33:00 PM
Surr:p-Terphenyl-d14 125 74.7-145 %Rec 2 12/22/2020 8:33:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Revision v1
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 37

S
it• Summit Environmental Technologies,Inc. Analytical Report
mu 3310 Win St.
ENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 20121120
Website:http://www.settek.com Date Reported: 12/30/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/17/2020 9:52:00 AM
Lab ID: 20121120-001A
Project: Eden-REVISED
Client Sample ID Eden TCLP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 12/22/2020 8:10:00 PM
Toxaphene ND 0.0500 mg/L 1 12/22/2020 8:10:00 PM
Endrin ND 0.00250 mg/L 1 12/22/2020 8:10:00 PM
gamma-BHC ND 0.00250 mg/L 1 12/22/2020 8:10:00 PM
Heptachlor ND 0.00250 mg/L 1 12/22/2020 8:10:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 12/22/2020 8:10:00 PM
Methoxychlor ND 0.00250 mg/L 1 12/22/2020 8:10:00 PM
Surr:TCMX 68.0 10-119 %Rec 1 12/22/2020 8:10:00 PM
Surr: DCB 85.2 10-119 %Rec 1 12/22/2020 8:10:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321A Analyst: TM
2,4-D ND 1.00 mg/L 100 12/24/2020 10:42:00 AM
2,4,5-TP ND 1.00 mg/L 100 12/24/2020 10:42:00 AM
Surr:2,4-Dichlorophenylacetic aci 107 70-130 %Rec 100 12/24/2020 10:42:00 AM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
1,2-Dichloroethane ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
MEK ND 5.00 mg/L 50 12/24/2020 3:28:00 AM
Benzene ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
Carbon tetrachloride ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
Chlorobenzene ND 2.50 mg/L 50 12/24/2020 3:28:00 AM
Chloroform ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
Tetrachloroethene ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
Trichloroethene ND 0.250 mg/L 50 12/24/2020 3:28:00 AM
Vinyl chloride ND 0.100 mg/L 50 12/24/2020 3:28:00 AM
Surr:4-Bromofluorobenzene 96.7 70-130 %Rec 50 12/24/2020 3:28:00 AM
Surr: Dibromofluoromethane 102 70-130 %Rec 50 12/24/2020 3:28:00 AM
Surr:Toluene-d8 99.4 70-130 %Rec 50 12/24/2020 3:28:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Revision v1
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 37

S
it• Summit Environmental Technologies,Inc. Analytical Report
mu 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 20121120
Website:http://www.settek.com Date Reported: 12/30/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/17/2020 9:52:00 AM
Lab ID: 20121120-001A
Project: Eden-REVISED
Client Sample ID Eden TCLP
Analyses Result RL Qual Units DF Date Analyzed
RCISOLID-W/IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.490 mg/Kg 1 12/21/2020 2:38:00 PM
PAINT FILTER FREE LIQUIDS TEST(SW-846: 9095) SW9095 Analyst: DHC
Free Liquid pass 1 12/24/2020 9:10:00 AM
RCI-SOLID-W/IGNITABILITY1030 SW1030 Analyst: CXS
IGNITABILITY OF SOLIDS(SW-846: 1030)
Ignitability nonflammable mm/sec 1 12/29/2020 3:03:57 PM
RCISOLID-W/IGNITABILITY1030 SW9045D Analyst: WK
PH (SW9045D)
pH 7.0 s.u.@20.3C 1 12/22/2020 11:31:06 AM
RCISOLID-W/IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 12/21/2020 2:38:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Revision v1
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 9 of 37

S
MM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MI ENVIRONMENTAL TECHNaLOGES,iri Cuyahoga Falls,Ohio 44223 J Y
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 20121120
Website:http://www.settek.com 30-Dec-20
Client: Synagro State: NW
Project: Eden-REVISED Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
20121120-001A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge Paint Filter Free Liquids Test(SW-846:9095) Free Liquid A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive N
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Version#2
Page 10 of 37

S UMM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7tes Report
EN ENWIRONM@NtAL TECHN❑LociEs,i Cuyahoga Falls,Ohio 44223 Analytes
rral}'0caf iaboralorlas TEL:[phone] FAX [phone] WO#: 20121120
Website:http://www.settek.com 30-Dec-20
Client: Synagro State: NW
Project: Eden-REVISED Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
20121120-001A Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Version#2
Page 11 of 37

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Page 36 of 37

SUMMIT
Summit Environmental Technologies,Inc.
OMra 3310 Win St.
Arm' OtJMENtALTtiriNOL4Ga S.lFr Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
yt�caf iabora�orJas TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 20121120 RcptNo: 1
Logged by: Christina N.Jager 12/18/2020 10:20:00 AM
Completed By: Christina N.Jager 12/18/2020 1:16:17 PM
Reviewed By: Jennifer Woolf 12/18/2020 1:24:30 PM (...710‘.-0.?1' )771'4,aAal'i•-
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no,notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑d No ❑ NA ❑
Person Notified: 'Ryan Copeland Date: 12/18/2020
By Whom: 'Jennifer Woolf Via: 0 eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: state
Client Instructions: NC
18.Additional remarks:
NC
project address not included
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 0.6 Good Not Present
Page 37 of 37

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
Monitoring Period: From 01/01/21 To 03/31/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2xl0to the 6th MPN MPN/g
Coliform power per gram
of total solids
CFU 12821 37647 52133 CFU/g 0 4/yr Grab 9222D
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake) X
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward,WWTP Superintendent
Prep rer Name sand Title(type or p ) Land Applier Name and Title(if applicable)(type or print)
14fft
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Meritech, Inc,
.r/ Environmental Laboratory
ill
1
�" Laboratory Certification No. 165
lel
Page 1
Contact: Ryan Copeland Report Date: 2/3/2021
Client: Synagro
284 Boger Road Project: Eden
MocksviIle, NC 27028 Date Sample Rcvd: 1/25/2021
Meritech Work Order# 01252134 Sample: Eden 1 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 23.4 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 12,821 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
Meritech Work Order# 01252135 Sample: Eden 2 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.3 % 1/26/21 0-100 % SM 2540E
Fecal Coliform (Sludge) 51,813 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
Meritech Work Order# 01252136 Sample: Eden 3 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.5 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 35,897 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
Meritech Work Order# 01252137 Sample: Eden 4 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 21.1 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 52,133 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
Meritech Work Order# 01252138 Sample: Eden 5 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.4 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 46,392 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

iiik
Meritech, Inc.
Environmental Laboratory
OF
Laboratory Certification No. 165
-2e
Page 2
Contact: Ryan Copeland Report Date: 2/3/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 1/25/2021
Meritech Work Order# 01252139 Sample: Eden 6 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 20.5 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 39,024 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
Meritech Work Order# 01252140 Sample: Eden 7 Grab 1/25/21
Parameters Results Analysis Date Reporting Limit Method
0/0 Total Solids 27.3 % 1/26/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 47,619 col/g dry wt 1/25/21 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. O 00 [rt.,
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result Log
12821 4.11 Min 12821
51813 4.71 Max 52133
35897 4.56 Geometric Mean 37647
52,133 4.72
46392 4.67
39024 4.59
47619 4.68
Average 4.58

Specific Oxygen Uptake Rate
SOUR
Facility Name: Mebane Bridge
Biosolids Permit Number: WQ0003035
Date: 3/22/2021
Digester Temperature:
Sampling Date/Time: 3/22/21 1611
Sampled By: M Ward
Analysis Date/Time: 3/22/21 1614
Analyzed By: M Ward
Total Solids: 0.84 % Dry Solids
Beginning Temperature: 14.9 degrees Celsius
End Temperature: 15.9 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/I)
0 9.63
1 9.6
2 9.51
3 9.45
4 9.37
5 9.31
6 9.24
7 9.18
8 9.11
9 9.05
10 8.99
11 8.9
12 8.85
13 8.8
14 8.7
15 8.64
Slope: 0.07
Intercept: 9.6
Correlation Coefficient: 1.00
Oxygen Uptake Rate: 4.00 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.48 mg Oxygen/hr/g
Average Temperature: 15 degrees Celsius
Temperature Correction Factor: 1.40
Temperature Corrected Specific Oxygen Uptake Rate: 0.67 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 4/01/21 To 06/30/21
Pathogen Reduction(40 CFR 50332/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10 to the 6'h MPN CFU/g
Coliform power per gram of
total solids
CFU 65217 94443 183784 CFU/g 0 4 (irah 9222 D
1000 MPN per gram of total MPN/g
solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake) X
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met"(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward,WWTP Superintendent
,)P7rer ame An Titl ( e or print) Land Applier Name and Title(if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Meritech, Inc.
oti
Environmental Laboratory
n Laboratory Certification No. 165
0
Page 1
Contact: Ryan Copeland Report Date: 3/18/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville,NC 27028 Date Sample Rcvd: 3/15/2021
Meritech Work Order# 03152115 Sample: Eden 1 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.4 % 3/15/21 0-100 % SM 254DB
Fecal Coliform (Sludge) 100,543 col/g dry wt 3/15/21 130 coI/g dry wt SM 9222D
Meritech Work Order# 03152116 Sample: Eden 2 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.9 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 89,947 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
Meritech Work Order# 03152117 Sample: Eden 3 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.5 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 183,784 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
Meritech Work Order# 03152118 Sample: Eden 4 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.8 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 90,426 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
Meritech Work Order# 03152119 Sample: Eden 5 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.6 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 96,774 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
A Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Ryan Copeland Report Date: 3/18/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 3/15/2021
Meritech Work Order# 03152120 Sample: Eden 6 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.4 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 70,652 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
Meritech Work Order# 03152121 Sample: Eden 7 Grab 3/15/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.4 % 3/15/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 65,217 col/g dry wt 3/15/21 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data, J'irrrtrilarr1 kj
Laboratory Representative
642 Tamco Road,Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result Log
100543 5.00 Min 65217
89947 4.95 Max 183784
183784 5.26 Geometric Mean 94443
90,426 4.96
96774 4.99
70652 4.85
65217 4.81
Average 4.98

Specific Oxygen Uptake Rate
SOUR
Facility Name: Mebane Bridge
Biosolids Permit Number: WQ0003035
Date: 4/14/2021
Digester Temperature:
Sampling Date/Time: 4/14/21 1440
Sampled By: M. Tuttle
Analysis Date/Time: 4/14/21 1442
Analyzed By: M. Tuttle
Total Solids: 0.38 % Dry Solids
Beginning Temperature: 18.1 degrees Celsius
End Temperature: 19 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/I)
0 7.18
1 7.13
2 7.11
3 7.07
4 7.05
5 7.02
6 6.99
7 6.96
8 6.93
9 6.9
10 6.87
11 6.85
12 6.83
13 6.79
14 6.77
15 6.74
Slope: 0.03
Intercept: 7.2
Correlation Coefficient: 1.00
Oxygen Uptake Rate: 1.71 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.45 mg Oxygen/hr/g
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.48 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 7/01/21 To 09/30/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10 to the 6th MPN CFU/g
Coliform power per gram of
total solids
CFU 10152 37010 194805 CFU/g 0 4 r Grab 9222 D
1000 MPN per gram of total \1PN/g
solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake) X
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward,WWTP Superintendent
Prep er Np..te And Titl (tupriily Land Applier Name and Title(if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Meritech, Inc.
Adlilik Environmental Laboratory
4 Laboratory Certification No. 165
Page 1
Contact: Ryan Copeland Report Date: 7/1/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Revd: 6/23/2021
Meritech Work Order# 06232143 Sample: Eden 1 Grab 6/23/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.2 % 6/25/21 0-100 % SM 2540E
Fecal Coliform (Sludge) 194,805 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
Meritech Work Order# 06232144 Sample: Eden 2 Grab 6/23/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.1 % 6/25/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 52,356 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
Meritech Work Order# 06232145 Sample: Eden 3 Grab 6/23/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.0 % 6/25/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 63,158 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
Meritech Work Order# 06232146 Sample: Eden 4 Grab 6/23/21
Parameters Results Analysis Date ReportingLimit Method
%Total Solids 19.6 % 6/25/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 25,510 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
Meritech Work Order# 06232147 Sample: Eden 5 Grab 6/23/21
Parameters Results AnaIysis Date Reporting Limit Method
%Total Solids 19.4 % 6/25/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 20,619 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

imp4iMeritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Or
Page 2
Contact: Ryan Copeland Report Date: 7/1/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 6/23/2021
Meritech Work Order# 06232148 Sample: Eden 6 Grab 6/23/21
Parameters Results Analysis Date Reporting Limit Method
%TotaI Solids 21.7 % 6/25/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 27,650 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
Meritech Work Order# 06232149 Sample: Eden 7 Grab 6/23/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 19.7 % 6/25/21 0-100 % SM 2540E
Fecal Coliform (Sludge) 10,152 col/g dry wt 6/23/21 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. 6.2?-1-- --
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result Log
194,805 5.29 Min 10152
52,356 4.72 Max 194805
63,158 4.80 Geometric Mean 37010
25,510 4.41
20,619 4.31
27,650 4.44
10,152 4.01
Average 4.57

Specific Oxygen Uptake Rate
SOUR
Facility Name: Mebane Bridge
Biosolids Permit Number: WQ0003035
Date: 7/6/2021
Digester Temperature:
Sampling Date/Time: 7/6/21 0850
Sampled By: M. Tuttle
Analysis Date/Time: 7/6/21 0853
Analyzed By: M. Tuttle
Total Solids: 0.35 % Dry Solids
Beginning Temperature: 24.3 degrees Celsius
End Temperature: 23.8 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/I)
0 7.4
1 7.3
2 7.2
3 7.14
4 7.08
5 7.03
6 6.96
7 6.9
8 6.85
9 6.79
10 6.73
11 6.67
12 6.61
13 6.55
14 6.48
15 6.42
Slope: 0.06
Intercept: 7.3
Correlation Coefficient: 1.00
Oxygen Uptake Rate: 3.72 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.06 mg Oxygen/hr/g
Average Temperature: 24 degrees Celsius
Temperature Correction Factor: 0.82
Temperature Corrected Specific Oxygen Uptake Rate: 0.88 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
From
Monitoring Period: 10/01/21 To 12/31/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10 to the 6th MPN CFU/g
Coliform power per gram of
total solids
CFt'' 12994 20277 35294 CFU/g 0 4/yr Grab 9222D
1000 MPN per gram of total MPN/g
solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake) X
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward,Utility Manager e arer ame And itle e r print) Land Applier Name and Title(if applicable)(type or print)
SiSi ature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Meritech, Inc.
Environmental Laboratory
I� Laboratory Certification No. 165
Page 1
Contact: Ryan Copeland Report Date: 11/3/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 10/28/2021
Meritech Work Order# 10282123 Sample: Eden 1 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.7 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 12,994 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
Meritech Work Order# 10282124 Sample: Eden 2 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.3 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 28,902 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
Meritech Work Order# 10282125 Sample: Eden 3 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.8 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (SIudge) 18,539 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
Meritech Work Order# 10282126 Sample: Eden 4 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.0 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (SIudge) 35,294 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
Meritech Work Order# 10282127 Sample: Eden 5 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.0 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 23,529 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

loilk0 Meritech, Inc.
Environmental Laboratory
0
Laboratory Certification No.165
Page 2
Contact: Ryan Copeland Report Date: 11/3/2021
Client: Synagro
284 Boger Road Project: Eden
Mocksville,NC 27028 Date Sample Revd: 10/28/2021
Meritech Work Order# 10282128 Sample: Eden 6 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.7 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 13,559 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
Meritech Work Order# 10282129 Sample: Eden 7 Grab 10/28/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.8 % 10/29/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 17,978 col/g dry wt 10/28/21 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. Jirilifyia i n cnrk,
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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FECAL DATA SHEET
Lab result Log
12994 4.11 Min 12994
28902 4.46 Max 35294
18539 4.27 Geometric Mean 20277
35,294 4.55
23529 4.37
13559 4.13
17978 4.25
Average 4.31

Specific Oxygen Uptake Rate
SOUR
Facility Name: Mebane Bridge
Biosolids Permit Number: WQ0003035
Date: 11/3/2021
Digester Temperature:
Sampling Date/Time: 11/3/2021 1345
Sampled By: M. Tuttle
Analysis Date/Time: 11-3-21 1347
Analyzed By: M.Tuttle
Total Solids: 0.48 % Dry Solids
Beginning Temperature: 18.3 degrees Celsius
End Temperature: 18.8 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/I)
0 8.44
1 8.42
2 8.41
3 8.4
4 8.38
5 8.37
6 8.35
7 8.31
8 8.3
9 8.3
10 8.29
11 8.28
12 8.26
13 8.24
14 8.23
15 8.21
Slope: 0.02
Intercept: 8.4
Correlation Coefficient: 0.99
Oxygen Uptake Rate: 0.91 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.19 mg Oxygen/hr/g
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.20 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: EDEN
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied
NC-RC-5-1 7.1 0.0 tons/ac.
NC-RC-5-2 7.0 0.0 tons/ac.
NC-RC-28-1 7.1 0.0 tons/ac.
NC-RC-26-1 B 6.9 0.0 tons/ac.
NC-RC-117-2 5.7 0.3 tons/ac.
NC-RC-01-1 6.6 0.0 tons/ac.
NC-RC-01-2 6.6 0.0 tons/ac.
NC-RC-01-3 6.6 0.0 tons/ac.
NC-RC-01-4 6.3 0.0 tons/ac.
NC-RC-01-5 6.9 0.0 tons/ac.
NC-RC-01-6 6.9 0.0 tons/ac.
NC-RC-45-1A 6.5 0.0 tons/ac.
NC-RC-45-2 6.5 0.0 tons/ac.
*Ag lime will be applied once field and crop conditions are suitable

SECTION 7

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