WQ0003902_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0003902
Applicant/Permittee City of Newton
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0003902
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* City of Newton Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for City of Newton,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Newton NC 2021 Annual Report FINAL.pdf 15.71 MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja rotivit5
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0003902
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Newton, NC.
If you have any questions or need additional information,please do not hesitate to contact Eric
Jones at(828) 695-4345 or Alex Fox at(336) 703-8681.
Sincerely,
l e't ic& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Eric Jones—City of Newton
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

CITY OF NEWTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003902
2021 ANNUAL REPORT

City of Newton, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#:W00003902 County Catawba Year 2021
Facility Name(as shown on permit)City of Newton,Clark Creek WWTP NPDES No.NC0036196
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO,skip Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: 50
Total number of fields utilized for land application during the year: 11
Total amount of dry tons applied during the year for all application sites: 948.61
Total number of acres utilized for land application during the year:367.80
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-13 below)issued by the Division of Water Quality X YES NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in I5A NCAC 02T.1105(6)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in I5A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations." 1 tom
lames Wentz;Public Works Director
Permittee Name and Title(type or print) Signature of Pe ittee ate
022
Signature of Preparer" Date Si a an pplier Date
(if different from Permittee) (if different m Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 7/31/2021
NEWTON,NC
NEWTON,NC CLARK CREEK LIME STABILIZED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
January 2021 468,000.00 G 170.18 D 154.35
March 2021 606,000.00 G 220.36 D 199.86
April 2021 774,000.00 G 224.96 D 204.04
May 2021 96,000.00 G 27.90 D 25.31
June 2021 624,000.00 G 181.36 D 164.50
TOTAL 2,568,000.00 G 824.76 D 748.06
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 1/28/2022 1:25:57 PM

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 9/1/2021 - 12/15/2021
NEWTON,NC
NEWTON,NC CLARK CREEK LIME STABILIZED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
September 2021 480,000.00 G 64.85 D 58.82
October 2021 54,000.00 G 7.30 D 6.62
December 2021 252,000.00 G 51.70 D 46.89
TOTAL 786,000.00 G 123.85 D 112.33
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 1/28/2022 1:28:41 PM

SECTION 2

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Newton
Lot Number:WA05053
Date Completed:01/21/2021
01/21/2021 4:00 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,_0
, MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WA05053
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: WA05053-001, due to low% solids the initial amount of these samples was 3 times the
standard procedure amount. The LOQ has been adjusted accordingly.
TKN
Sample -001 was run at reduced volume due to sample sludge matrix. The LOQ has been adjusted
accordingly.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WA05053-001
Description:Newton Matrix:Solid
Date Sampled:01/04/2021 0930 % Solids: 8.72 01/07/2021 0115
Date Received:01/05/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 01/07/2021 0115 MOM 78694
1 350.1 (Ammonia-N )350.1 2 01/08/2021 1014 DRD 78739
1 (Nitrate-N )9056A 1 01/08/2021 1203 AMR 79020
1 (Nitrite-N )9056A 1 01/08/2021 1203 AMR 79022
1 (Phosphorus)365.1 5 01/08/2021 1113 DMA 01/07/2021 1936 78800
1 (Soil pH meas)9045D 1 01/07/2021 2328 AAB 78814
2 351.4 (TKN)351.2 1 01/14/2021 1231 DMA 01/13/2021 1905 79348
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 8.72 % 1
Ammonia-N (gas diffusion) 350.1 770 23 12 mg/kg 1
Nitrate-N (soluble) 9056A 100 5.7 1.1 mg/kg 1
Nitrite-N (soluble) 9056A 4.0 2.3 1.1 mg/kg 1
Phosphorus 7723-14-0 365.1 5500 290 57 mg/kg 1
Soil pH measured in water @ 19.6° C 9045D 12.2 su 1
TKN 351.2 13000 290 290 mg/kg 2
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/07/2021 1001 JAB2 01/07/2021 0400 78580
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 0.91 0.22 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/08/2021 1650 KSH2 01/08/2021 0311 78587
2 3050B 6010D 2 01/11/2021 1435 KSH2 01/08/2021 0311 78587
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 7700 76 28 mg/kg 1
Arsenic 7440-38-2 6010D 1.4 J 2.8 0.95 mg/kg 1
Cadmium 7440-43-9 6010D ND 0.95 0.24 mg/kg 1
Calcium 7440-70-2 6010D 2700 1900 240 mg/kg 2
Chromium 7440-47-3 6010D 11 1.9 0.47 mg/kg 1
Copper 7440-50-8 6010D 63 1.9 0.85 mg/kg 1
Iron 7439-89-6 6010D 5800 19 8.6 mg/kg 1
Lead 7439-92-1 6010D 5.5 1.9 0.85 mg/kg 1
Magnesium 7439-95-4 6010D 2400 950 120 mg/kg 1
Manganese 7439-96-5 6010D 220 2.8 1.1 mg/kg 1
Molybdenum 7439-98-7 6010D ND 7.6 1.9 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WA05053-001
Description:Newton Matrix:Solid
Date Sampled:01/04/2021 0930 % Solids: 8.72 01/07/2021 0115
Date Received:01/05/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/08/2021 1650 KSH2 01/08/2021 0311 78587
2 3050B 6010D 2 01/11/2021 1435 KSH2 01/08/2021 0311 78587
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 8.8 7.6 2.0 mg/kg 1
Potassium 7440-09-7 6010D 510 J 950 120 mg/kg 1
Selenium 7782-49-2 6010D ND 3.8 1.5 mg/kg 1
Sodium 7440-23-5 6010D 530 J 950 120 mg/kg 1
Zinc 7440-66-6 6010D 310 9.5 2.4 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Ch cldist[SRC}[MEUC1HC-1S) Revised:9/29/102Q
. aceAr> +ytieN Issuing A:attlority:pace FN -WCO1 Page 1 of 1.
Sample Receipt Checklist (SRC)
Client: $4NAG:t0 Cooler Inspected byidate• i*1_l: + 41.O5/241 Lot#I: w^` c53
7�`earis of rece[pt: E Pace ❑Client • UPS MI FedEx Other: _
❑Yes fl lido 1. Ware cottony wcsiEr prt2ticnil i+u Lhi.txiu Icy
❑Y:::f ❑No ❑NA 2.if custody seals were presert,were tIi y-rOicr;end i Inh-oken? .
pH Strip ID. NA Chlorine Strip TD; N — Tested by: _--
Origkwt i mpereitnw upon r:xeipl. ( rivyJ(iCiorrectiftij Len grcraturnupon ii ]pt %Solid Soap-Cup ID: 2t}875
2.7 i 2.7 c{ NA I NA oc NA 1 NA �C t9A ;NA
Method! ✓❑temperature Blank❑ILgaitist Boles IR tin'] €l): 55y ER Gunf orreetion.Facror; c `e
Method of coolant ❑ Wet Ica El lee Packs ❑ Dry ]ce [� Tome
Ftcmpertlurc or any cinder exceeded t,0 ,was p'r'ujec1 [NanngerNnufed?
❑files FM" n]A TPM vira.5 Notified by: phone I email f fact-en-fact(circle one).
❑Yes ❑Nn ❑, NA 4, Is Eho commercial courier's packing slip acmclx-d to this fblin?
Yes ON S_ Were proper custody 7rncetJivas(reEinquishedlraceived)Followed?
J Yes Were sample IOs listed on the COCA
J Yes ❑No 7_ Were sample'Ds listed on .II sample containers?
1❑Yes LINr) 3_ R+ c a;.IllIc..tion data& !loc.listed on COC?
Yes; FIND 9. Was calleutiondate&.time listed on al:sample containers?
EYesi ❑No I(]_ Did al]container label r.rtormatinn(I]7, date,time)n tee with th,e(:OC?
ayes: ❑No_ I I. Were C,i to b.y perfornr d listed pn Iho COC.'?
,Cs ©N 12, Did all samples arrive in the proper containers tbr each test andlor in good cond itioa
{unbroken,lids on,c*.)?
Yes ❑Na •I1_ Was adequaltttrmple volume avAllahle?
❑Yes n N a 14. Were all samples received within•$:the]io]d in i little rr 48 1 wu.N.wliic3t0ver comes first°
❑Yes D 15. Were any samples containers misstngfcxccss(circle onc)samEles Not listed ott COC?
16. For VOA andRSK-]75 5arnplen,were bubbles present>"pea-si2c"(Wei-6r_im:ndisircter)
❑Yes FIN DNA in urn.v ifie VOA iria[5?
Yes ❑ND r EN A: 7. Wc�e all 1JRUlmetals{nutrient samples recei,,er:at pi] :f 2?
▪Yc5 �]D 1 1 I NA. 1 R_ Were:,II cyanide i:mplm rrcc:vrd at a pH> 12 and swlfide samp]cs received at a pH>r}?
19_ Were all app]iciibl;2NE4 TF(N,'uyinidelptenn1?i425.I1FlD8.3 oirnplcsiiccof
❑Yes ❑ND 0 A
rcSlt[uul i]7lorine? _ _
El yes ❑Nu ENA 20- Were dicntrcmru-Icsf:-c€{uese, requested dilutions. M5lMSD deli cations,etc___)
c xrrcctly LrUiiscribxl from the COC into the oDmmcnt section in LL 7S7
❑Yips Q Ni 2I I. Wus the woo:ee_imhcr listed ern the container 1rl'el"r IFye ,Qiio 9 4 nW,
Sample Pr ertratipu (NMI.be corr;p]eLet1 roe any yt1mple(s)incorrectly preserveC t r with hcad:pacc.)
Sampla(s) were received inc redly preserved and wore adjusted tt;.cerdingly
in sample receiving with. Nn mL of circle one:].12SU1, F1Ni}3 ]�Ct,NaOH using SR Il >~A
"finite orp,t a tiatie_e N,h . If tii❑in thpn Line pie eivtt:ivc is eieedc 1,plt.use note in thu c ri:Timis below.
Samples] NA were received with bubbles>6 MIA ire diti ieier.
crop Imo) NA were received with-LNG?0.5 mg{L(1f 419 is no)and wen]
adjuatad accatxlinnfv in sample rceeivingwi h sodium thiosulfatc(I,2a3`iO3)with Shealy
SR barcode labels applied by: "Ill Dote:. 011U5r'ro2t
Comments:
•
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED 1/4/2021 1/1/2021 -3/31/2021 0.5258
LIQUID
Na mg/I =(Na mg/kg x %Solids) = 100= (530 x 8.7200) = 100=46.216
Ca mg/I =(Ca mg/kg x %Solids) = 100= (2700 x 8.7200) = 100 =235.44
Mg mg/I =(mg mg/kg x% Solids) = 100 =(2400 x 8.7200) = 100=209.28
Na meq= Na mg/I = Molec.Wgt.Na =46.216=23=2.00939
Ca meq=Ca mg/I = Molec.Wgt.Ca =235.44=20= 11.772
Mg meq= Mg mg/I = Molec.Wgt.Mg=209.28= 12 = 17.44
SAR = Na meq =SgrRoot[0.5 x(Ca meq + Mg meq)] =2.00939=SgrRoot[0.5(11.772+17.44)] =0.525774

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Newton
Lot Number:WD06081
Date Completed:04/19/2021
04/19/2021 11:23 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye )
ANSI NatonalAccredltatlon Board
ACCREDITEDORA1O,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD06081
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Sample -001 has been prepared using three grams of sample mass due to low percent solids. The LOQs
have been changed to reflect the additional volume.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WD06081-001
Description:Newton Matrix: Solid
Date Sampled:04/06/2021 0930 %Solids: 6.97 04/06/2021 2311
Date Received:04/06/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 04/06/2021 2311 MOM 88169
1 350.1 (Ammonia-N)350.1 5 04/07/2021 1208 KFE 88135
1 (Nitrate-N)9056A 1 04/08/2021 1141 AMR 88521
1 (Nitrite-N)9056A 1 04/08/2021 1141 AMR 88522
2 (Phosphorus)365.1 100 04/13/2021 1544 DMA 04/10/2021 1429 88601
1 (Soil pH meas)9045D 1 04/07/2021 1919 NBW 88303
1 351.4 (TKN)351.2 3 04/09/2021 1737 MSG 04/07/2021 1700 88277
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 6.97 % 1
Ammonia-N (gas diffusion) 350.1 2400 72 37 mg/kg 1
Nitrate-N (soluble) 9056A 33 7.2 1.4 mg/kg 1
Nitrite-N (soluble) 9056A 14 2.9 1.4 mg/kg 1
Phosphorus 7723-14-0 365.1 44000 7200 1400 mg/kg 2
Soil pH measured in water @ 21.7° C 9045D 11.2 su 1
TKN 351.2 20000 1100 1100 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471B 1 04/09/2021 1835 CMS2 04/09/2021 1308 88366
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471 B ND 1.1 0.27 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/08/2021 1409 JMH 04/07/2021 1012 88194
2 3050B 6010D 4 04/10/2021 1026 KSH2 04/07/2021 1012 88194
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 19000 93 35 mg/kg 1
Arsenic 7440-38-2 6010D 2.9 J 3.5 1.2 mg/kg 1
Cadmium 7440-43-9 6010D 0.65 J 1.2 0.29 mg/kg 1
Calcium 7440-70-2 6010D 170000 4600 580 mg/kg 2
Chromium 7440-47-3 6010D 36 2.3 0.58 mg/kg 1
Copper 7440-50-8 6010D 240 9.3 4.2 mg/kg 2
Iron 7439-89-6 6010D 13000 23 11 mg/kg 1
Lead 7439-92-1 6010D 16 2.3 1.0 mg/kg 1
Magnesium 7439-95-4 6010D 4800 1200 140 mg/kg 1
Manganese 7439-96-5 6010D 550 3.5 1.4 mg/kg 1
Molybdenum 7439-98-7 6010D 5.8 J 9.3 2.3 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WD06081-001
Description:Newton Matrix: Solid
Date Sampled:04/06/2021 0930 %Solids: 6.97 04/06/2021 2311
Date Received:04/06/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/08/2021 1409 JMH 04/07/2021 1012 88194
2 3050B 6010D 4 04/10/2021 1026 KSH2 04/07/2021 1012 88194
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 39 9.3 2.4 mg/kg 1
Potassium 7440-09-7 6010D 1300 1200 140 mg/kg 1
Selenium 7782-49-2 6010D 3.9 J 4.6 1.9 mg/kg 1
Sodium 7440-23-5 6010D 840 J 1200 140 mg/kg 1
Zinc 7440-66-6 6010D 1400 12 2.9 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Chedcli9t(SRC' [OIAfOu18C-1 1 Re4'Ised'3/29{2020
7 e.4rraMicaf' •59.1 iv.Authority:Pat ENV-WCOL ring.=0`1
Sample Receipt Checklist (SRC)
Client: "S•`'n""n' Cooler Inspected byitifitu, JRG2 f L 17U'203L Lot ilk WL46In I
Moans of rueoipc; ri P[1Ce (JClieut Q OP • lied;a: • Other; __..
Yes d I No 'I. Were.custody Weals prcmcnt on !NC cooler? --
Ycs •No ®NA 2. Jf custDuir seals wcr.;present,were LJ1 intact and unbrokeiiV . ---
aH Strip ED: l'`^ Chlorine Strip 1[ . NA -.-.--- 'Tese(1 by;IA
OriLinal temperature upon reeeipt I Derived({ tr:ected)temperature upon RC;Lpt :iSulicl Snap-Cup ID: -'1-112
1.4 fLA ec NA /I'IA oc-+ VA /Nft cc NA fHA. oe
Mcthed:❑7 cmperaturc Blank Q :inst Bottles IR Gan ID: 5ER Gun Cnirecric n Farrar. _ ;
Mcncerl ofooiant- El We:ice 0 're Packs I]. Tory Ice None
r al. Iftelnperature ofu'iy cooler exceeded b.0°C,was Project EvIenagerN{1ified?
• ❑ N�
Yes � o E. NA
PM was Notified by: phone/email?fact-to-face(circle one).
U Y,�y [Ti t'o fNA 4- Is the a nrneinial courier's packing slip atea.ehnd to this C„ijn?
Q-• 17- o i. Vv'en proper custody arocixiur (rtlillyu.die�freC:ivec]) RAI:+sea? I
iRYes EIN0 6, Wcrc sampkc]l s list'1 on the COC?
Yes_ - - 'V rc km ap]c lt7w tisu;d am di sample conL-liners? _
El Yes Erc,
7
o 8. '4'us ocllcaion dale&time I:sted on the COC? _
U Ye., I1 NcF 9. Was co[I ction date&time I;sted an al:sample containers'?
❑Y^P. ..❑Nn, 10.bid aft ction:ainer laacl information ion(ID.dalk,4itlle);brie wall ille COC?
Q Yes IT c! 11. Wore toss to bo performed listed on tho COC
12-Did al:samples arrive in the proper containers for call test andkw In good aaiditlon
Yin. []No (iiihroken, lids in,etc.)? _-- . .__.
l Yes 1 I No [3-Was adequate sample volume available?
❑J Ycs 0No 14. Were al:Sam7les received wi'hiu'.•5 tiie holding time or 48 hours,whichever oamcs:rat°
D Yes ilk° E5.Were any samples containers inissingexccss(conic ono)samples Not listed on COC?
16, For VOA and 1tSK-]75 samples,were bcbb]cs pr1icnt>"pea-s Tom"('/+"car 6rrnn ill diameter)
❑Yes ON° 14A in any ofthe VOA vials?
Yes ... Nu ?d NA 11 Were all DROhne[a:s,i'nutrieut wimples received at a p1-1 of- 2?
©Yes I No 2NA 18. Were all,yyan.ide samples rac:eived at a pH> 12 and sulfidePI1K IS�l1 Ins received at A ]-]>9 r 1
o l�NA 19.Wcre all applicable NI-1 Nfc}�anidrir,I,a,iEf 25.I/60g.:,( 0-:5u! L)samples.tree o
❑Yes El
` — - tesi.dua,chlorine? _
❑Yes ❑No QhA AI, Were client remarks/requests(i.e.requested dilmions,?'fIS!MSD dzsigrurtions,etc.,.)
Correetiy trrmSCribed frnrn the t C into the camnlen-sectors in L[AMS'f
❑Yes LINE.: 21, Was the quote number l i stet:OrL the container label''If 'es,Quote#
Sample Presel'vatioa (1l st be completed fir ary sampic{s)incotrecdy'rreLm ed or with headspa€e.)
Sample(s) r'* _ wee received incorrectly prcscrvcd and wcrc adjusted accordingly
i n s,c utpie recei+rirri with NA- rr.l.n r circle nne: E I2SO4,11NO3,!ICI.NaOU i using SR li NA
Time of preservation NA ' 1Frnr}re than one preservative is needed,please note in the comments ly,kuw.
Sarno:As) NA __.. . wr rcc :vcd with bnubbles>6 imnl in diameter,
Saumpl 4s) 14" were received with TR >0 5 mg/LW#I L9 is u )acid were
t€djnsted accardinsly in samplo receiving with sodium ytlosutfilte(ria2S7iN with Shcaly ID; NA
R nilrecxlc li:helx;•riplicd',Ay: .IR{if Date: 84+ P(L
Comments:
--
•
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED 4/6/2021 4/1/2021 -6/30/2021 0.1445
LIQUID
Na mg/I =(Na mg/kg x %Solids) = 100= (840 x 6.9700) = 100=58.548
Ca mg/I =(Ca mg/kg x %Solids) = 100= (170000 x 6.9700) = 100= 11849
Mg mg/I =(mg mg/kg x% Solids) = 100 =(4800 x 6.9700) = 100=334.56
Na meq= Na mg/I = Molec.Wgt.Na =58.548=23=2.54557
Ca meq=Ca mg/I = Molec.Wgt.Ca = 11849 =20 =592.45
Mg meq= Mg mg/I = Molec.Wgt.Mg=334.56= 12 =27.88
SAR = Na meq =SgrRoot[0.5 x(Ca meq + Mg meq)] =2.54557=SgrRoot[0.5(592.45+27.88)] =0.14454

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Newton
Lot Number:WG14143
Date Completed:07/27/2021
07/28/2021 10:19 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,c_0‘
MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WG14143
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WG14143-001
Description:Newton Matrix: Solid
Date Sampled:07/14/2021 0930 %Solids: 3.24 07/15/2021 0012
Date Received:07/14/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 07/15/2021 0012 AAB 98917
1 350.1 (Ammonia-N)350.1 10 07/19/2021 1543 KFE 99305
1 (Nitrate-N)9056A 1 07/20/2021 1629 AMR 99555
1 (Nitrite-N)9056A 1 07/20/2021 1629 AMR 99558
1 (Phosphorus)365.1 10 07/23/2021 1200 DMA 07/21/2021 1635 99611
1 (Soil pH meas)9045D 1 07/19/2021 2050 NBW 99378
1 351.4 (TKN)351.2 2 07/27/2021 1404 DMA 07/21/2021 1523 99586
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 3.24 % 1
Ammonia-N (gas diffusion) 350.1 13000 S 310 160 mg/kg 1
Nitrate-N (soluble) 9056A 53 S 15 3.1 mg/kg 1
Nitrite-N (soluble) 9056A 8.9 6.2 3.1 mg/kg 1
Phosphorus 7723-14-0 365.1 15000 S 1500 310 mg/kg 1
Soil pH measured in water @ 19.2° C 9045D 7.2 su 1
TKN 351.2 46000 S 3100 1500 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 07/22/2021 1416 CMS2 07/21/2021 1058 99142
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.71 J 2.4 0.57 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 07/17/2021 1400 KSH2 07/16/2021 1042 98936
2 3050B 6010D 1 07/19/2021 1811 JMH 07/16/2021 1042 98936
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 24000 560 210 mg/kg 1
Arsenic 7440-38-2 6010D ND 21 7.0 mg/kg 1
Cadmium 7440-43-9 6010D ND 7.0 1.8 mg/kg 1
Calcium 7440-70-2 6010D 220000 7000 880 mg/kg 1
Chromium 7440-47-3 6010D 37 14 3.5 mg/kg 1
Copper 7440-50-8 6010D 270 14 6.3 mg/kg 1
Iron 7439-89-6 6010D 16000 140 64 mg/kg 1
Lead 7439-92-1 6010D 21 14 6.3 mg/kg 1
Magnesium 7439-95-4 6010D 7200 7000 880 mg/kg 2
Manganese 7439-96-5 6010D 600 21 8.3 mg/kg 1
Molybdenum 7439-98-7 6010D ND 56 14 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WG14143-001
Description:Newton Matrix: Solid
Date Sampled:07/14/2021 0930 %Solids: 3.24 07/15/2021 0012
Date Received:07/14/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 07/17/2021 1400 KSH2 07/16/2021 1042 98936
2 3050B 6010D 1 07/19/2021 1811 JMH 07/16/2021 1042 98936
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 15 J 56 15 mg/kg 1
Potassium 7440-09-7 6010D 1500 J 7000 880 mg/kg 1
Selenium 7782-49-2 6010D ND 28 11 mg/kg 1
Sodium 7440-23-5 6010D 2100 J 7000 880 mg/kg 1
Zinc 7440-66-6 6010D 1100 70 18 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
i
Samples keceipt Checklist(SRC}(ME0012C-0) ar,icised=51/79f2420
2eArr i€af• Iss:AIng Authority;Pace ENV-WCOL j Pav 1 of 1
•
Sample Receipt Checklist (SRC)
Client: SYNfs;rRJ _ Cooler Inspect-A by/dal : :SM i air.i'2U' ] LLLk; 11ici14143
Mesas ut'reccipt; 0 1'aaco Delienr UPS PedLht Other,, 7
i Yes I No 11.Were custody seals present on the aoaer ; —
MEE ,No is NA. 2_If custody seals were preterit,were the •intact aru21.u-113r at7 I
'pH Str'pID: \Fa —alfr}rin Strip ID_ NA _— L'SE bb ern
Original temperaature upon receipt/Derived(CorreClyd)aanpera re upon receipt 1%.nlic!Saifrp-Cup]D; 2141
I2.6 12.E •r . NA 1NA, GC NA ;11 o • NA /NA aC
fwt¢thcd:O'Te mperat�rre>'3Iink [ Icinst E3o tEes IR Ginn ID: 5 _IR Guns Correction,E'ac o : 0 _{:C
:Method af coolant; ®V1fa�t[c Ice Packs � f]i} Ice ❑ None
13- Ir temperature of any cooler en.gccdcd 6-floc:,was Proju.L Ivlanager Notified?Yes ❑No !DNA
PM was Notified by:phone 2'email/face-ro-roue(;.hell*En le;),
Yes ❑Now. is the commercial couri,ur'c rack slip angel Led to th[ firm?
k4 Yes No 5, Were proper custody procetkres(retinae,ishcdlrccei ved/ d?foil awe
{ Yc:x No 6. Were narmple ID3]Jaacd on the COc. 1
✓• 'ems �No 7. Wets S JC II)R li3rell on all skunple containers 1
Yes L No S. Was oollectior date&time][sted on the.flC,' .
1 Y,4 J No 9, Was cnJJcctim.datC&time lismnrl on ail sample co itain#rs?
J 'C5 Na PO,Did all container lahttl infarmcitiun(1D,dal-C.,time)agP4L:with dm COO? -
J J I`fee No I I.Were tesrs to be ps,T ormed I iL7ed ou the COC;' 1 —
Yes El :+. IAA all samples arrive in tho pioper containers t'or eachlieSt aadlar In gaol condition No
(unbroken, lids on,ere,)? J
Yes No I.;. Was adewate sample volume available?
d Yes No .14, Were all samples receivedwithin the Etalding time it;i16 hours.whichever comes t rsL4
D
[�Yera o I5. Were Itn}r sa�rplcs containers missiatg/cxcess(circle INA)samples No`Eist .on CPC?
Yoe No 1G-For VOA and I S1K-175 samples,were bubbles la -size"('li'ur 6mut in d meter)
�D in any ua the VOA vials/ J
IYci _No d R`A 17- Wcra ail DROftt;etalalnatric:e[surnpJo.s receiver,araI of<2? I
Li Yes —.1 Nu. J NA.18, Ware al]eyuniac Rarnples ierek vial at a H ]2 arid [ :de camp:cs reoeivcrl at a p14 }9?
0 Yes' ON° ©NAe19. Y re all a p�i NI-I f1•KNec}anidelpberio1/625.1.16GI 3(•:17.5rng L)samples face of
residual chlorine?
y o 0 Ne n N 20.Weer client r'e131arksh'egi nets(i.e. cgiicsted dilutions, SorMSD des[ r'.atians,.etc,,.)
_ correctly transcribed from the COC into Inc comment semi n in LIMS?
Yes QNo �21-V4`sls the q',lulu number listed On t[lo container label'?II ell a,Qua(c ' P'p.
naiplc Prcuervaflon CAM.oe completed for anv'arnple(s)incorrectly prmeJ-ed v(with headspace-)
S�amlrle(s) " �_wcre Teceived.incorrectly pre4eryCd and wens adjusted 1::cordirigly
in sample recei iiig with N:A . n]L of circle one; 1-12SO1, IiNO3,NCI,NaOET using E.[f 1) ' __
"rime of presercatian NA [Imam than one prea-ervarive is.tkcdcd.:slam not, in the carnI Brits bej , '
Samples) N'A
w4:wrec receiver' bubbles $trim in d1arrder-
Samp'os(s) NA wCre rdcei ae l with TIC-01$rngJL(If#19 is w!)and w •.e
djo ied accordingly in sattnpJe receiving with 7
so,�iiuirt tFiosu]fate(l fr:2%03)wielf SI`.ea4y ID: NA
SR barcodelafaels applied by_ 15 4 DAt,E: 11.112G2I '
._
.II .- - _i
Comments.: i
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED 7/14/2021 7/1/2021 - 10/31/2021 0.2158
LIQUID
Na mg/I =(Na mg/kg x %Solids) = 100= (2100 x 3.2400) = 100 =68.04
Ca mg/I =(Ca mg/kg x %Solids) = 100= (220000 x 3.2400) = 100=7128
Mg mg/I =(mg mg/kg x% Solids) = 100 =(7200 x 3.2400) = 100=233.28
Na meq= Na mg/I = Molec.Wgt.Na =68.04=23=2.95826
Ca meq=Ca mg/I = Molec.Wgt.Ca =7128 =20=356.4
Mg meq= Mg mg/I = Molec.Wgt.Mg=233.28= 12 = 19.44
SAR = Na meq =SgrRoot[0.5 x(Ca meq + Mg meq)] =2.95826=SgrRoot[0.5(356.4+19.44)] = 0.215799

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Newton
Lot Number:WK02067
Date Completed:11/29/2021
Ola
11/30/2021 4:40 PM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WK02067
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample has an initial weight that is 3x greater than standard
procedure: WK02067-001. The LOQ has been changed to reflect the additional mass.
Inorganic Non-Metals
The pH of sample WK02067-001 came to 11.10 which is outside the range of the pH meter. Therefore a
pH 12 Buffer Standard was read, but it failed to meet its temperature corrected value. Results will be
reported.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WK02067-001
Description:Newton Matrix: Solid
Date Sampled:11/02/2021 0830 %Solids: 4.92 11/03/2021 0152
Date Received:11/02/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 11/03/2021 0152 MOM 21051
1 350.1 (Ammonia-N)350.1 10 11/20/2021 2010 DRD 22997
1 (Nitrate-N)9056A 1 11/10/2021 1112 AMR 22147
2 (Nitrite-N)9056A 1 11/26/2021 1210 AMR 23954
1 (Phosphorus)365.1 25 11/04/2021 1701 DMA 11/04/2021 1019 21253
1 (Soil pH meas)9045D 1 11/07/2021 1730 NBW 21588
1 351.4 (TKN)351.2 1 11/05/2021 1219 DMA 11/04/2021 1312 21269
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 4.92 % 1
Ammonia-N (gas diffusion) 350.1 6000 S 200 110 mg/kg 1
Nitrate-N (soluble) 9056A 37 10 2.0 mg/kg 1
Nitrite-N (soluble) 9056A ND 4.1 2.0 mg/kg 2
Phosphorus 7723-14-0 365.1 12000 2500 510 mg/kg 1
Soil pH measured in water @ 20.8° C 9045D 11.1 su 1
TKN 351.2 26000 1000 510 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 11/16/2021 1647 JAB2 11/15/2021 1536 22152
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.53 J 1.6 0.39 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 11/04/2021 1342 JMH 11/04/2021 0126 21089
2 3050B 6010D 1 11/05/2021 1756 KSH2 11/04/2021 0126 21089
3 3050B 6010D 5 11/05/2021 1800 KSH2 11/04/2021 0126 21089
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 28000 130 49 mg/kg 1
Arsenic 7440-38-2 6010D 4.1 J 4.9 1.6 mg/kg 1
Cadmium 7440-43-9 6010D 0.92 J 1.6 0.41 mg/kg 1
Calcium 7440-70-2 6010D 340000 8200 1000 mg/kg 3
Chromium 7440-47-3 6010D 52 3.3 0.82 mg/kg 1
Copper 7440-50-8 6010D 380 16 7.4 mg/kg 3
Iron 7439-89-6 6010D 18000 33 15 mg/kg 1
Lead 7439-92-1 6010D 19 3.3 1.5 mg/kg 1
Magnesium 7439-95-4 6010D 6900 1600 200 mg/kg 1
Manganese 7439-96-5 6010D 760 4.9 1.9 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WK02067-001
Description:Newton Matrix: Solid
Date Sampled:11/02/2021 0830 %Solids: 4.92 11/03/2021 0152
Date Received:11/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 11/04/2021 1342 JMH 11/04/2021 0126 21089
2 3050B 6010D 1 11/05/2021 1756 KSH2 11/04/2021 0126 21089
3 3050B 6010D 5 11/05/2021 1800 KSH2 11/04/2021 0126 21089
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Molybdenum 7439-98-7 6010D 7.2 J 13 3.3 mg/kg 1
Nickel 7440-02-0 6010D 20 13 3.4 mg/kg 1
Potassium 7440-09-7 6010D 1300 J 1600 200 mg/kg 2
Selenium 7782-49-2 6010D 7.1 6.6 2.7 mg/kg 1
Sodium 7440-23-5 6010D 1400 J 1600 200 mg/kg 1
Zinc 7440-66-6 6010D 1100 16 4.1 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
J
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt ChecklistISRC)(ME]04i3C-15) RC4isee_9j29fQO p
9i1 i4Irc71 Issuing Authority: 7a c 5E1 V-WOO L 1325e 1 of 1
Sample Receipt Checklist (SRC)
C]ie_u, Synrgro Cooler inspected hylirlzic- <DRW i ii 1203E Lot ff: 4VKG?ix,7
Means of receipts ❑ Pace lient UPS FeclIN Other
,F Yes ❑,f Nti ,_ Were custodv seals aresert on the cooler? -- —
Yex,❑Ncr, ONA 7, It:custo Jy s••:als w4r4_, r fi ; ent,were they intact aria unbroken?
phi Slip FDr, NA Chlorine Strip 11); NA Tested by:NA ._ •
•�
Original Iempffature upon,cceipir+Derived(Correcte ).tempeeratureuponrercipt %Solid5nap-Cup ID; 2L-1 Kg
2.4 f•L4 DC NA rN.A NA fNA DC NA 1NA oC
I Method_[iTernpe..rdwrE E3lank inst]3oulc5 IR Gun ID: s aRGM]Correction Factor; 0
lMethod 0-coolairt: 0 Wd lei E Ice pa., Eal Dry Ice ❑ was!
13_ ]f tettlpesr lture of ails,�;oolcr exceeded
6.0°C,was Project Mattuger Nail fired?
i n 'cs nND DN +
PM was Nod fled by_phone 1 email f race-to-face(circle out).
fl'r.cs 7 No Q 4. Is the commercial courier's packing slip auached m this form?
FQ Yes No 5. Were pnapercustody procedures(rellLlr[LLishedireckivedj followed/
Yes E No 6. Were samp]C IDs l isted on the CDC? _
Yes 7. Weres:unp"e 1fx%listed on all sarnp.e cao�.taiJiers?
Yes No�Nco R. Was collection date&,time]iered on the(2CC?
•LIJYes ❑240 9, Was collection date&time listed on all sample coma]ner5?
fir Yes • No TO- Did an container label information(ID,date,time)agree.with the CCC?
FA Yrt 0No I I_Were Lesim to he performed listed to the(IOC?
17Yes ❑Na 12. Dld all samples at:ivn in the proper crintainerR for each test Endrcle in good wild iNoll
I
(unbroken,]ids an,etc_)' _
No 13, Was adequatesurnple valurna available?
El Yes MI No 14. Were all samples received within the holding time or 4$hours,wh;citover comes first?
• Yes ✓ No 1.5_1174PC any sample;ECM hiiner3 mitsittlr'Cxoess(circle one)ss,mples Not listed out COC?
Yes Ala t 16.I or VOA and RSK =15 samples,were bubbles present "pea-sins"(V°'ar Gnim in diameter)
in any afthe VO.1 vials'!
• Yes ]No FA NA 17.Were all DROhttetilsfnulriunt sample rft.eF. red at a pHI(IF<2?
MO . Nro, /NA.I R. Woe ail cyn,diee Namples received al a pH 12 rend.au]fisic samples a civod mi a II[ 9 •
] 19_Wury all apri icable 1Hy''r ,cymtitl;:fphe fi25,i.,6(1 . ( O.Sin.G�I.)r:arnples tree of
❑ ,cs IT!No 17
:residual chlorine?
❑yes ❑N0 "DNA 20' Wore c]iertt rcm&rk.slregi a (i.e.requested dilutions,M5JMSD designations,etc,„)
• correctly"ratis rtbcd from the COC into the comment section in LIMtS'i
• yes Lid No _ 21. 14 rs qu `x the o �twnr bc 1 fisted on tF a c�ant:.]itcr labs 12 If •vs,( ri.4,tr i l€
sample Preservation (Must be corall•kted.far any somp[c(s) incnrrecl'y preserved or with h idspace.)
Sainple(sj •c were fteo vcd incowectiv pr reed and were Euijustcd accordingly ,•
I
in sump[e receiving with r"A mL of circle one t 147.504,HNO3,HO[,Na01 1 using SR U NA
me afpreservatiar. , If more/ran one preservatiNo is meted,please note intke arlrncnis botow.
4;uupEe(s) NA — wero received will-. aubbles>6 mere in diameter.
urnplcsi M _ wca+e recr.hvrd with TRC>0.5 rnglL(If0lr9 is no)and were
'auljiisted accordingly in sattsple receiving.wit:a SAdium th lost]lfale([ atS2D3)with Shealy ID: N
—!
SR barcade]ab•Qls applied by. t`DR' ` Dow; 11132rt1n;
Comments: .. — —
•
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED 11/2/2021 11/1/2021 - 0.1440
LIQUID 12/31/2021
Na mg/I =(Na mg/kg x %Solids) = 100= (1400 x 4.9200) = 100 =68.88
Ca mg/I =(Ca mg/kg x %Solids) = 100= (340000 x 4.9200) = 100= 16728
Mg mg/I =(mg mg/kg x% Solids) = 100 =(6900 x 4.9200) = 100=339.48
Na meq= Na mg/I = Molec.Wgt.Na =68.88=23=2.99478
Ca meq=Ca mg/I = Molec.Wgt.Ca = 16728 =20 =836.4
Mg meq= Mg mg/I = Molec.Wgt.Mg=339.48= 12 =28.29
SAR = Na meq =SgrRoot[0.5 x(Ca meq + Mg meq)] =2.99478=SgrRoot[0.5(836.4+28.29)] = 0.144029

SECTION 3

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SECTION 4

S
a i' Summit Environmental Technologies,Inc.
inIrg 3310 Win St.
ENVIRONMENTAL TECHNO LOCiES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boraIi rlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
January 12,2021
Alex Fox
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL:
FAX:
RE: Newton
Dear Alex Fox: Order No.: 21010090
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/5/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
/.....?-74424f4 177��
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 42

5 M�'� Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21010090rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 1/12/2021
CLIENT: Synagro
Project: Newton
WorkOrder Narrative:
21010090: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Original
Page 2 of 42

•
17 S
Mm iT Summit Environmental Techno3310Wlogies,Ins
Qualifiers and Acronyms
EkiwllxsStJM@N1'nLTecriw❑LOG{ES.INC Cuyahoga Falls,Ohio 442 WO#: 21010090
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 1/12/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 42

S t�' Summit Environmental Technologies,Inc. Workorder
I'll3310 Win St.
OM=
ENVIRONMENTAL TECHNQI. oiEs,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 21010090
Website:http://www.settek.com 12-Jan-21
CLIENT: Synagro
Project: Newton
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
21010090-001 Newton 1/4/2021 8:50:00 AM 1/5/2021 10:15:00 AM Sludge
Page 4 of 42

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S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENb1R01JMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010090
Website:http://www.settek.com Date Reported: 1/12/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2021 8:50:00 AM
Lab ID: 21010090-001A
Project: Newton
Client Sample ID Newton
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00500 mg/L 1 1/8/2021 12:31:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 1/11/2021 12:41:05 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 1/11/2021 12:41:05 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/11/2021 12:41:05 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 1/11/2021 12:41:05 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 1/11/2021 12:41:05 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 1/11/2021 12:41:05 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 1/11/2021 12:41:05 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 1/8/2021 12:49:00 AM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 1/8/2021 12:49:00 AM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 1/8/2021 12:49:00 AM
2,4-Dinitrotoluene ND 0.100 mg/L 2 1/8/2021 12:49:00 AM
Cresols,Total ND 10.0 mg/L 2 1/8/2021 12:49:00 AM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 1/8/2021 12:49:00 AM
Hexachlorobenzene ND 0.100 mg/L 2 1/8/2021 12:49:00 AM
Hexachloroethane ND 0.200 mg/L 2 1/8/2021 12:49:00 AM
Nitrobenzene ND 0.200 mg/L 2 1/8/2021 12:49:00 AM
Pentachlorophenol ND 0.500 mg/L 2 1/8/2021 12:49:00 AM
Pyridine ND 0.500 mg/L 2 1/8/2021 12:49:00 AM
Surr:2-Fluorophenol 89.4 10-157 m %Rec 2 1/8/2021 12:49:00 AM
Surr: Phenol-d6 81.0 10-169 %Rec 2 1/8/2021 12:49:00 AM
Surr: Nitrobenzene-d5 89.1 32.1 -130 %Rec 2 1/8/2021 12:49:00 AM
Surr:2,4,6-Tribromophenol 107 45.4-166 %Rec 2 1/8/2021 12:49:00 AM
Surr:2-Fluorobiphenyl 87.0 35.7-130 %Rec 2 1/8/2021 12:49:00 AM
Surr:p-Terphenyl-d14 110 74.7-145 %Rec 2 1/8/2021 12:49:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 6 of 42

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010090
Website:http://www.settek.com Date Reported: 1/12/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2021 8:50:00 AM
Lab ID: 21010090-001A
Project: Newton
Client Sample ID Newton
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 1/11/2021 10:04:00 PM
Toxaphene ND 0.0500 mg/L 1 1/11/2021 10:04:00 PM
Endrin ND 0.00250 mg/L 1 1/11/2021 10:04:00 PM
gamma-BHC ND 0.00250 mg/L 1 1/11/2021 10:04:00 PM
Heptachlor ND 0.00250 mg/L 1 1/11/2021 10:04:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 1/11/2021 10:04:00 PM
Methoxychlor ND 0.00250 mg/L 1 1/11/2021 10:04:00 PM
Surr:TCMX 69.2 10-119 %Rec 1 1/11/2021 10:04:00 PM
Surr: DCB 82.8 10-119 %Rec 1 1/11/2021 10:04:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321A Analyst: JPG
2,4-D ND 0.500 mg/L 50 1/8/2021 7:48:00 PM
2,4,5-TP ND 0.500 mg/L 50 1/8/2021 7:48:00 PM
Surr:2,4-Dichlorophenylacetic aci 106 70-130 %Rec 50 1/8/2021 7:48:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
MEK ND 5.00 mg/L 50 1/7/2021 5:55:00 PM
Benzene ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
Chlorobenzene ND 2.50 mg/L 50 1/7/2021 5:55:00 PM
Chloroform ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
Tetrachloroethene ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
Trichloroethene ND 0.250 mg/L 50 1/7/2021 5:55:00 PM
Vinyl chloride ND 0.100 mg/L 50 1/7/2021 5:55:00 PM
Surr:4-Bromofluorobenzene 93.8 70-130 %Rec 50 1/7/2021 5:55:00 PM
Surr: Dibromofluoromethane 102 70-130 %Rec 50 1/7/2021 5:55:00 PM
Surr:Toluene-d8 99.2 70-130 %Rec 50 1/7/2021 5:55:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 42

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECHNOLOGIES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010090
Website:http://www.settek.com Date Reported: 1/12/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/4/2021 8:50:00 AM
Lab ID: 21010090-001A
Project: Newton
Client Sample ID Newton
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.481 mg/Kg 1 1/7/2021 4:50:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: SEE
Ignitability nonflammable mm/sec 1 1/6/2021 2:27:57 PM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 11.9 s.u.@19.7C 1 1/6/2021 12:50:00 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/7/2021 4:50:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 42

it SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MI ENVIRONMENTAL TECHNaLOGES,INC Cuyahoga Falls,Ohio 44223 J Y
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 21010090
Website:http://www.settek.com 12-Jan-21
Client: Synagro State: NW
Project: Newton Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010090-001A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive N
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Original#1
Page 9 of 42

S UMM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7tes Report
EN ENWIRONM@NtAL TECHN❑LociEs,i Cuyahoga Falls,Ohio 44223 Analytes
rral}'tiicaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21010090
Website:http://www.settek.com 12-Jan-21
Client: Synagro State: NW
Project: Newton Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010090-001A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
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1f5t2421 Summit Environmental Technologies Mail-Ike;send data from MFP12072737 01fO5/2071 12;24
iir+� SUMMIT Jennifer Woolf=[e-mail]>
;I H;h41ii.•:::-.oafs i.f
M1 1.1 J,111'1%Wl
Re: Send data from MFP12072737 0110512021 12:24
1 message
Alex Fox [e-mail] _ — Tue,Jan 5,2021 at 1:01 PM
To: Jennifer Woolf<[e-mail]>
They are all inn NC and yes that's part of TGGp.
Thanks,
Alex Fox
TSS Western NC
336-703-6681 •
afoxe synagro.corn
On Jan 5,2021,at 12:39 PM,Jennifer Woolf.jw❑[e-mail]>wrote:
Could you resend them with the state included in the Project Address box? Also,could you indicate that
the Pest/Herb are TCLP also.
thanks!
jen
N
Jennifer Woolf o
Project Manager (NI
JWoolf@settek,com cm
33'10 Win St. c_
Cuyahoga Falls, Ohio 44223
Summit Environmental Technologies, Inc.
TEL; [phone]
FAX: [phone]
h ttp:/Iwww.set tok.c o m
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that may only be reviewed by the intended recipient.Any distribution or use of this
communication by anyone other than the intended recipient is strictly prohibited and may be
unlawful. If this email has been received in error, please notify the sender immediately by
replying to this message and delete the contents of this email from your files.
Please let us know how we are doing by participating in an online survey at
https://www.surveymonkey.comfriSBC3DYM.
On Tue,Jan 5,2021 at 12:31 PM Alex Fox<[e-mail]>wrote:
Here are the COG,
You can take Will,Marshall and Melvin of the list they no longer work for Synagro
Thanks,
Alex Fox
TSS Western NC •
336-703-8681
afox c@synagro.00m
Mips:flmall.google.cornfmailiu/Vik=ca79t59241&view=pt&search=all&pawn[hid=thread-f'AM1688068831$27378652%7Cmsg-f9Mo3A16880707515188..- 117
Page 41 of 42

iw SUMMIT
Summit Environmental Technologies,Inc.
OM 3310 Win St.
Arm' OtJMENtALTtiriNOL4Ga S.lFr Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
yt�caf iabora�orJas TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21010090 RcptNo: 1
1.f'
Logged by: Jesseca E.Westfall 1/5/2021 10:15:00 AM , G
Completed By: Jesseca E.Westfall 1/5/2021 4:14:14 PM �{ G
Reviewed By: Jennifer Woolf 1/5/2021 4:22:09 PM (...710‘.-0.?1' )771'4,aAal'i•-
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no,notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: I Date:J
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18.Additional remarks:
COC emailed
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 3.6 Good Not Present
Page 42 of 42

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Newton WQ Permit Number: WQ 0003902
WWTP Name: Newton Clark Creek WWTP NI'DES Number: NC 0036196
Monitoring Period: From 01/0121 To 3/31/2021
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt.1/A(time/temp) Alt.2/6(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior'lest) Alt.5/Process to Further Reduce Pathogens All.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Bela Ray Gamma Ray Pasteurization
Class It:
Alt.(1)Fecal Density Alt.(2)Process to Significantly Reduce Pathogens x
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data: _
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
tixeec- of Type Technique
Minimum Geo.Mean Maximum Units denser Analysis
Fecal 2x I0 to the 6h MPN MPN/g
Coliform power per gram
of total solids
CFU CFU/g
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
conform)
Vector Attraction Reduction(40 CFR 503.32/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt.1 Option/Alt.2 Optian/Alt.3 Option/Alt.4
(VS reduction) (40-day hench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(I 4-Day Aerobic) (AIk Stabilization) x (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt.10
(injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1I 07 have been met."
"I certify,under penalty of law,that the pathogen req9uirements in 40 CFR 503.32/15A NCAC 02T,1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 021.1107 have not been met"(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
James Wentz PWIJ Director
Prepare,nName and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
Signaturr`�/f sf Preparcr* Date Signature of land Applier(if applicable) Date
*Prep aitfr is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1 i 02(26)

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ANN UAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Roles)
Facility Name: Ci of Newton WQ Permit Number: WQ 0003902
WWTP Name: Newton Clark Creek WWTP NPDES Number: NC 0036196
Monitoring Period: From 04/01/21 To 6/30/2021
Pathogen Reduction(4U CFR 50332/ISA NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt.t!A(time/temp) Alt.2/B(AR Treatment) Alt.3/C(Prior'resting)
Ail.4/D(No Prior Test) All.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray — Pasteurization _
Class R:
Alt.(1)Fecal Density Alt.(2)Process to Significantly Reduce Pathogens x
if applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitorin;data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excce- of Type Technique
Minimum Geo.Mean Maximum Units dances Analysis
Fecal 2x10to the 6th MPN MPN/g
Coliform power per gram
of total solids
CPU CFU/g
1000 MPN per grant of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(thy weight)
lieu of fecal
conform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt.1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.S
(14-Day Aerobic) (AlkStabilization) x (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt.10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
'9 certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.I107 have been met."
"1 certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/I5A NCAC 027,1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 021'.1107 have not been met."(Please note if you check this statement attach ao
explanation why you have not met one or both of the requirements.)
'This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the p tdtogen and vector attraction reduction requirements have
been met. 1 am aware that there are significant penalties for false certification including fine and imprisonment."
James Wentz PWU Director
Prepare am and Title(type or print) Land ApplicrName and Title(if applicable)(type or print)
Vibe
Signat of Preparer* Date Signature of Land Applier(if applicablc) Date
*Pre er is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Newton WQ Permit Number: WQ 0003902
WWTP Name: Newton Clark Creek WWTP NPDIBS Number: NC 0036196
Monitoring Period: From 07/01/21 To 9/30/2021
Pathogen Reduction(40 CFR 50332/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt.i/A(time temp) Mt.2/13(Aik Treatment) Alt.3/C(Prior Tasting)
Alt.4/L)(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophi lie
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density AIL(2)Process to Significantly Reduce Pathogens x
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Clam A or Class R)complete the following monitoring data:
• Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x I0 to the 6't' MPN MPN/g
Coliform power per gram
of total solids
CFU CFU/g
1000 MPN per gram of MPNlg —
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt 1 Option/Alt.2 Option/Alt.3
(VS reduction) (40-day bench) (30-day bench) c.02 Option/Alt.4
(Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.S
(14-Day Aerobic) (Alk Stabilization) x (Drying—Stable) (Drying Unstable)
Option/Alt,9 Option/Alt.10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/I5A NCAC 02T.1 106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 021.1107 have not been met."(Please note if you check this statement attach au
_ explanation why you have not met one or both of the requirements.)
"This determination has been madc under my direction and supervision in accordance with the system designed to ensure that qualified
personnel pIr oampe rawheart a tnhde reev araleu astieg tnfin rmpenatialotn su sfeodr fa sdee tecmitnea dant the 1puahnogg fienn ea nadn dv emctporri sara
nmcetinotneduction requirements have
James Wentz PWU Director
Proper N ea .Title(type or print) Land Applier Name and Title(if applicable)(type or print)
Si Lure ofPreparcr* Date Signature of Land Applier(if applicable) Date
* rcparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 27.1102(26)

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•
ANNUAL.PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Newton WQ Permit Number: WQ 0003902
WWTP Name: Newton Clark Creek WWTP NPDES Number: NC 0036196
Monitoring Period: From 10/01/21 To 12/31/2021
Pathogen Reduction(411 CFR 503.321I5A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt.1/A(time/temp) _ Alt.2/13(Alk Treatment) Alt.3/C(Prior'resting)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens All.6(l3quivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Bela Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density Alt.(2)Process to Significantly Reduce Pathogens x
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(ass A,or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excco- of Type Technique
Minimum Geo.Mean Maximum Units denccs Analysis
Fecal 2x10 to the 6th MPN MPN/g
Conform power per gram
of total solids
CPU CFUIg -
1000 MPN per gram of MPN/g
total solids(thy weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
conform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T,1107)-Please indicate option/alternative performed:
Option/Alt.I Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/AR 7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization). x (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt,10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"1 certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1 l06 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"1 certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.I106 and the vector attraction
reduction requirement as 40 Cl
R 503.33/15A NCAC 021.I 107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
`"Phis determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I arts aware that there are significant penalties far false certification including fine and imprisonment."
James Wentz.PWU Director
Prep er Name and Title(type or print) Land Applicr Name and Title(if applicable)(type or print)
41/0/7
Si attire of Prepare Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

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SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: Newton
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied(CCE Eq.)
CA-16-1 7.7 0.0T/Ac.
CA-16-2 7.0 0.0T/Ac.
CA-21-1 7.0 0.0 T/AC
CA-21-2 6.9 0.0T/Ac.
CA-20-10 6.0 0.0T/Ac.
CA-20-7 6.8 0.0T/Ac.
CA-20-8 7.4 0.0T/Ac.
CA-36-3 4.9 0.0T/Ac.
CA-36-4 6.2 0.0T/Ac.
LT-119-5 6.4 0.0T/Ac.
CA-32-1 6.3 0.0T/Ac.
CA-32-2 6.9 0.0T/Ac.
They get their lime in the sludge since Newton is Lime stabalized.

SECTION 7

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