WQ0001800_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0001800
Applicant/Permittee Town of Yadkinville
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001800
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* Town of Yadkinville Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for Town of Yadkinville,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Yadkinville NC 2021 Annual Report FINAL.pdf 15.17MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja TM/WO
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0001800
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Yadkinville, NC.
If you have any questions or need additional information,please do not hesitate to contact Jacob
Swaim at(336) 403-2444 or Alex Fox at(336) 703-8681.
Sincerely,
l e't ic& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc:Jacob Swaim—Town of Yadkinville
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

TOWN OF YADKINVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001800
2021 ANNUAL REPORT

Town of Yadkinville, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms & Metal Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00001800 County Yadkin Year 2021
Facility Name(as shown on permit)Town of YadkinviUe WWTP&WTP NPDES No.NC0020338,NC0079260 G�
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO,skip Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: 19
Total number of fields utilized for land application during the year: 11
Total amount of dry tons applied during the year for all application sites: 92.25
Total number of acres utilized for land application during the year: 62.00
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-13 below)issued by the Division of Water Quality YES_X NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in I SA NCAC 02T.1105(b)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in I 5A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9, All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
!I. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations."
Jacob Swaim.Director of Public Wojks — t I0
Permittee Name and Title(type or print) Si of a Date
)9?-liC5 �—�4— 2/10/2022
Signature oeparer* Date Si and tier Date
(if different from Permittee) (if different fr m Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(112006)

SYNAGRO
July 28, 2021
N.C. Department of Environmental Quality
Division of Water Resources
450 W.Hanes Mill Rd. Suite 300
Winston Salem,NC 27105
ATTENTION: Mr. Lon Snider
REFERENCE: RESPONSE: NOTICE OF VIOLATION
NOV-2021-PC-0359
2020 ANNUAL REPORT REVIEW
Town of Yadkinville, Residuals Land Application Program
Permit No. WQ0001800
Yadkin County
Dear Mr. Snider:
On behalf of the Town of Yadkinville, Synagro is responding to your letter dated July 23rd,2021,and
received July 26th, 2021 regarding the review and comments on the 2020 annual report for this
program. The response to each item listed in the violation are below:
1. During the 2020 calendar year, a total of 78.73 dry tons was land applied from the Yadkinville
WTP which exceeds the currently permitted maximum of 30 dry tons. This is a result of
elevated percent solids and an increased amount of material being land applied.As a
corrective action,the maximum permitted dry tonnage will be increased in the upcoming
permit renewal to accommodate any fluctuation in solids content or overall residuals
production.
2. Additionally,when analyzing the Yadkinville WWTP nonhazardous results, it was observed
that 2 constituents listed in the required analysis were reported at detection limits above the
acceptable regulatory limit. It is understood that a reporting limit above the regulatory limit
cannot confirm compliance with required maximum concentrations. As a corrective action,the
current lab completing this testing will be informed of the necessary detection limits to be able
to display permit compliance.
If you require additional information or have further questions,please contact me at 336-703-8681 or
[e-mail].
Sincerely,
Alex Fox
Cc: Lon Snider,Regional Supervisor,Division of Water Resources,NCDEQ-WSRO—[e-mail]
Jacob Swaim,Director of Public Works,Town of Yadkinville—[e-mail]
284 Boger Road, Mocksville, NC 27028 • Phone: [phone]

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 12/31/2021
YADKINVILLE,NC
YADKINVILLE,NC WWTP LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
July 2021 359,600.00 G 41.84 D 37.95
November 2021 257,400.00 G 29.95 D 27.16
TOTAL 617,000.00 G 71.78 D 65.11
YADKINVILLE,NC WTP LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
March 2021 17,500.00 G 1.20 D 1.09
April 2021 70,000.00 G 4.82 D 4.37
July 2021 91,000.00 G 6.26 D 5.68
September 2021 66,500.00 G 4.58 D 4.15
December 2021 52,500.00 G 3.61 D 3.28
TOTAL 297,500.00 G 20.47 D 18.57
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date:2/2/2022 3:08:10 PM

SECTION 2

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Yadkinville
Lot Number:WD20039
Date Completed:04/30/2021
05/03/2021 3:36 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,c_0‘
MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD20039
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WD20039-001
Description:Yadkinville WWTP Matrix:Solid
Date Sampled:04/19/2021 1130 % Solids: 2.79 04/21/2021 0002
Date Received:04/20/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 04/21/2021 0002 SJL 89669
1 350.1 (Ammonia-N )350.1 5 04/26/2021 1340 DRD 90225
2 (Nitrate-N )9056A 1 04/30/2021 1102 AMR 90829
1 (Nitrite-N )9056A 1 04/28/2021 2338 AMR 90650
1 (Phosphorus)365.1 25 04/26/2021 1446 DMA 04/24/2021 1139 90119
1 (Soil pH meas)9045D 1 04/26/2021 2203 NBW 90278
1 351.4 (TKN)351.2 2 04/26/2021 1253 DMA 04/24/2021 1116 90116
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 2.79 % 1
Ammonia-N (gas diffusion) 350.1 5500 180 93 mg/kg 1
Nitrate-N (soluble) 9056A 80 18 3.6 mg/kg 2
Nitrite-N (soluble) 9056A 6.3 J 7.2 3.6 mg/kg 1
Phosphorus 7723-14-0 365.1 25000 4500 900 mg/kg 1
Soil pH measured in water @ 18.7° C 9045D 6.9 su 1
TKN 351.2 44000 1800 1800 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/27/2021 1544 CMS2 04/27/2021 1035 90176
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.8 0.66 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/23/2021 1618 KSH2 04/22/2021 1217 89730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 58000 200 74 mg/kg 1
Arsenic 7440-38-2 6010D 5.8 J 7.4 2.5 mg/kg 1
Cadmium 7440-43-9 6010D 0.99 J 2.5 0.62 mg/kg 1
Calcium 7440-70-2 6010D 11000 2500 310 mg/kg 1
Chromium 7440-47-3 6010D 55 4.9 1.2 mg/kg 1
Copper 7440-50-8 6010D 390 4.9 2.2 mg/kg 1
Iron 7439-89-6 6010D 23000 49 22 mg/kg 1
Lead 7439-92-1 6010D 26 4.9 2.2 mg/kg 1
Magnesium 7439-95-4 6010D 2800 2500 310 mg/kg 1
Manganese 7439-96-5 6010D 3800 7.4 2.9 mg/kg 1
Molybdenum 7439-98-7 6010D 7.1 J 20 4.9 mg/kg 1
Nickel 7440-02-0 6010D 50 20 5.2 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WD20039-001
Description:Yadkinville WWTP Matrix:Solid
Date Sampled:04/19/2021 1130 % Solids: 2.79 04/21/2021 0002
Date Received:04/20/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/23/2021 1618 KSH2 04/22/2021 1217 89730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 4200 2500 310 mg/kg 1
Selenium 7782-49-2 6010D 8.5 J 9.9 4.0 mg/kg 1
Sodium 7440-23-5 6010D 3000 2500 310 mg/kg 1
Zinc 7440-66-6 6010D 1800 25 6.2 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Reclipt uheekti5t(SRC){Tr1Eooi.5C-151 lievised:9{29{24
' 20.01+afyric.r? Issuing Authority;'ace ENV-WCOL PaRe l ail
Sample Receipt Cheeidist (SRC)
Client: Synagro Cools'Inspected , :IJax: TIU-' f 04.9.c..+202! Lott+: 1.11p2003)
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3. If temperature of tLrty cooler exceeded 6.0=C, was Project IvtanaRer Notified?
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77 yd5 ❑No NA i. is the commercial 4uurier's packing Slip attacked to lima form?
El Yes!: 0 N0 5- Were pro1.''er cusludy procedures(relinquishcd,'rccelved)tollo vod?
Fg Yes El No .6. Were sample!Ds listed 0r the LOC? —
Ii Ye; 1No J. Were sample]Ds lisr_�rI fin, all sample containers?
Y_AsNo S. Itime
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I 'es R No, 10-Did all container label infodmatin r{:T7,date,time)agree with the OC)C? ...
n Yrs No I l. Wwrc orals to ba parf4rnt ed listed to E3e COC'?
Yes I- Na 12-Did all sum pits u._iwe in the proper oontainec for each tear and+or in red condition
511 I . pr.br oken,lids on,ctr-)?
I�Yes I I No 13.1V0 s adequate sample volume available?
Z yes DNO 11.Wt:rc all samples received within V.the]toidirEr,Time or(-1I tours, whichever refines first7 —
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7]Yes pi Nu
❑NA in arty of the VDA vials?• _
Yes ❑Nu [1NAI t7. Were al'.1)I(Oh.netaksinutricnt samples received at a pH of<T
Yes LJt o r]NA'1S., Were all ,�nicIcxHn_l,lesre civaial aFIi> 12w.ralsulfidesamplYsreceived ttupH-9?
❑Yp� El ]o ❑+ N 9.Vibe a applic.ahie N111ft7c r aide phone 11625-lifiUS.3(. 0,517i samples free of
residual c[)lcrine'i _
20. .Vcrc cligtt i+elrarks(reg1 e5ts(Le.requnicci dilutions,!4Sf,MSF)designations e.-.)
❑Yaq ❑No ONAcorrectly taansedIxLl from the COG into the eminent section in L11k4 ?
•0 yys I . I21_Was the gloom number listed on the container la1-1e17 Tr yes,Quoit it
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'nscrip'a receiving witty ' ._rd.,ofcir}cle.one:1-1'7.Ste, ITN03, HCi,Nat?I[using .1t]r11A -_
ime of preservati<n tx15` _. . it mere than one p e ervative is neviteJ,please note it,the cornma:1is boLc r.
Sample(s) NA _ _ were received with bubbles>6 mini in diameter.
S:a;r,ples(a) NA _were received'with TRC '0.5 mg+L(If#1.9 i IMP)aiul were
adju_<tedaccnrd'lglyin sample receiving with sodium thiose]lfale(NaAU)with Shealyil); "•r
p barrcode labcks ayplied by: 3:t6-2 Date; 0dt200. 1
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Comments:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Yadkinville WTP
Lot Number:WC26085
Date Completed:04/07/2021
04/08/2021 11:44 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WC26085
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WC26085-001
Description:Yadkinville WTP Matrix: Solid
Date Sampled:03/25/2021 1000 %Solids: 1.65 03/27/2021 1535
Date Received:03/26/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 03/27/2021 1535 AAB 87070
1 350.1 (Ammonia-N)350.1 1 04/01/2021 1404 KFE 87597
1 (Nitrate-N)9056A 1 03/31/2021 0319 AMR 87625
1 (Nitrite-N)9056A 1 03/31/2021 0319 AMR 87626
1 (Phosphorus)365.1 1 03/30/2021 1242 DMA 03/27/2021 0820 87068
1 (Soil pH meas)9045D 1 03/31/2021 1339 NBW 87485
3 351.4 (TKN)351.2 1 04/06/2021 1623 MSG 04/03/2021 0859 87839
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 1.65 % 1
Ammonia-N (gas diffusion) 350.1 40 J 61 32 mg/kg 1
Nitrate-N (soluble) 9056A 44 30 6.1 mg/kg 1
Nitrite-N (soluble) 9056A ND 12 6.1 mg/kg 1
Phosphorus 7723-14-0 365.1 1200 300 61 mg/kg 1
Soil pH measured in water @ 19.9° C 9045D 6.6 su 1
TKN 351.2 4600 1500 1500 mg/kg 3
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/01/2021 1817 CMS2 04/01/2021 1540 87571
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 4.7 1.1 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 03/31/2021 1502 KSH2 03/30/2021 1157 87144
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 200000 370 140 mg/kg 1
Arsenic 7440-38-2 6010D 6.7 J 14 4.6 mg/kg 1
Cadmium 7440-43-9 6010D ND 4.6 1.2 mg/kg 1
Calcium 7440-70-2 6010D 1000 J 4600 580 mg/kg 1
Chromium 7440-47-3 6010D 42 9.2 2.3 mg/kg 1
Copper 7440-50-8 6010D 40 9.2 4.2 mg/kg 1
Iron 7439-89-6 6010D 29000 92 42 mg/kg 1
Lead 7439-92-1 6010D 33 9.2 4.2 mg/kg 1
Magnesium 7439-95-4 6010D 1000 J 4600 580 mg/kg 1
Manganese 7439-96-5 6010D 3800 14 5.5 mg/kg 1
Molybdenum 7439-98-7 6010D ND 37 9.2 mg/kg 1
Nickel 7440-02-0 6010D 18 J 37 9.7 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WC26085-001
Description:Yadkinville WTP Matrix: Solid
Date Sampled:03/25/2021 1000 %Solids: 1.65 03/27/2021 1535
Date Received:03/26/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 03/31/2021 1502 KSH2 03/30/2021 1157 87144
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 770 J 4600 580 mg/kg 1
Selenium 7782-49-2 6010D 8.5 J 18 7.5 mg/kg 1
Sodium 7440-23-5 6010D 910 J 4600 580 mg/kg 1
Zinc 7440-66-6 6010D 160 46 12 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Sample Receipt Checklist 1.SPC)IMEOO18C-151 R.etitsCCI:9123/2020
.."ceA+k*;4i:3! IssulnP,A1:ftority_Pace Er V-WEDL Page'of 3.
Sample Receipt Checklist (SRC)
C:ient: 'Y°"gra Cooler Inspect d byAlm: ICtG2 r + 7(11( . .. Lot 14: c2r;os5
11 Megrtsr,=receipt; Parma Client !J[' ]kdEx 4l!]cr;
Yes , L Were cusrndy seals prnr 1 ore the cooler?
Yo No ❑J NA 2. if custody seas k+_er UNS4 nt,were eh�:y
w ims.:t Hod unbroken?
pH Strip ID: r -- Chlari-'e Strip]!]_ NA Tesled ley;I'A
Original,temperature upon receipt 1 Derived(Corroded)temperature upon receipt %Suiid Snap-Cep 1fl' 2.'462
,3.7 '3.7 ac, NA f NA. oc NA 1 i4h_ oC h111 ;h'r'. oc
,Method: J❑reniDcaature Mack lest Bolles lR-Gun ID; 6 -- . . ,- IR Gur.Correction Facwr; 0 `C:
'Method of coolant; 0 We 1]ee Yee Pacts ❑ Thy lee ❑ None
., If temperature of any c ooler�cxcaodod 6-U`C,'r++rxs 1'rpieCt lama er Notifiecl?
yes
❑No DMA PM was Notifizd by-Ta;,onc I•:imuil 1 Cstcr-Lo-face(circle o,te)_
El Yes ❑No __1 A 14., Is[he commercial courier's pecking slip LittLc]ed to this form?
151 Yes ❑No. 5, Arem proper custody procedures(relinquishedirzccivtd)followid?
at Yes 0 No 4, WCre•5p04)1 c IDS I is.tec on the COL"?
- --
Yes ONO 7, Were sample Ms listed on ail sample containers? ..
A Yes 1i No 8. Was collection date&time listed on the COG? .--
Yes ID No . Was uullectiun date&time fisted on all sanip'c[.orrteiners?
'1Yes ONo 10.Did all container label informscion(ID,dHlz,time;tic\with Inc COC?
•
. Y ID No 1 I.Were tots L3 he pefori ted lisped ou the COC7�
❑Yes 17 No 12_Did all samples arrive:o the Kock':cortuirrcrs :or ouch Lust rrud/er in gt•3od condition
Off hrukun, Iirs jai,cLc.1?.i _ —
n Yes ❑Nt} l3.Wasadcquatc sample volt u xtva3lualc?
✓ L`42 El NaI&Were all t mplcs:ecelvCtl w;thin'la the'inkling time or 4 hours,which:acr conics First?
0 yes El tip 15.VL'e;r any tirmp ,r lai s;ontaiuers rui sin eaxcess(clrc]e(nx)samples Not listed on COC?
n 4'cs Nu NA I�x,For Y0 And RSK-l75 samples,were laul�blc�s pra 'l›-pea-size"('VV"ar 6niin iu 11iarneLet)
i n tty of the YQA v ia:s"?
YrA 0 NO II NA 17. Werc all DROrmotalskuttricni s8mp]K rcoeiv'ed al )`I a or‹2?
R___
y� LiN J NA'!S, Were all c`uide saEnples rerr'.ived irk H pI4 x I7 Hn{€suIfide xrvurIes iCsrivecl al.a Ill]>9?
•
'19, Were all applicable 14H,SI3licyauide+phonoU625_].r(OR3(<QSma/L)samples free of
©Yes ID No. ❑, NAi
__ re9idetol'Morino?
No EN , ,Vero client reurxrks?requests(i.e.reques-eddilutions, NIS/MEL)designations,etc,,,)Ycs Licurnx:l]y..r;ulscribrxl fain flue COC uito Lire conrmeunt section is Lila?
LIT/c,5l 0 No ....!i, Wus Lie yuate nLeml,er listed on the container label?If yes.Quote ii
Sample Preservation (Must be oomploied for airy Saurple(s) incorrectly preserved or with Lod 50 .)
&rruple(s) NA — wear rr.c;civr l iricnrrectly j ese1ved and were adjusted accordingly
jut bwriple receiving will' NA .. nil.ce circle one: H2SO4,I iNO3,T1C€,NR01d using.SR 4 14'^
'l iinc of preservation NA___ , If mom than one preservative is needed,please noie in the moments helcrw_
Sample([) NA —.-- were received with bubbles'›b nun in diameter.
•Saniplas(s) n - WIZ IC L'CLCivcd with TRC>0.5 rng/L(If 019:s Igo)c.nd wore
adjusted accordingly in sample re;oeivin jr with sodium thinsu€fiae(Nat52f;)with Shealy ID: '1''N
SF 1)arcode Ia eLsappliedl]y t z� t}Ktr; 43126J202.1
Conrmcnls:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied(Annual): 7.89
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: Poplar Forest
Acres Used: 4.2 Acres Permitted: 4.2 Site#: NC YK 00008 Field#: YK 00008 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample orL U U LJ J 1 8 I __9i II°_i 1111 12
Com-
posite
Date 4/19/21
Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum 7.1
Nickel 50
_Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total _.2 J 3 ' 4 51 6J 7 I S 1 91 10 11 12
DT/Ac./ o
rr
App. 1
Event 1.88
Arsenic 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022
Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Copper 1.465 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.465
Chromium 0.207 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.207
Lead 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.098
T
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
denum _ J
Nickel 0.188 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.188
Selenium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
Zinc 6.761 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.761
Total
Phos- 93.900 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 93.900
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprison ent for knowing violations".
.1' X (-7-- ------ 2- 6?_ 77
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 5.58
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: Poplar Forest
Acres Used: 3.2 Acres Permitted: 3.2 Site#: NC YK 00008 Field#: YK 00008 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample orJ .J (J 4 1_,L ± u u i0 1111 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum 7.1
Nickel 50
Selenium 8.5
Zinc _ 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 J j 4 1 6_1 1 7 1 81 9 10 ; 11 '12 1
DT/Ac./ o
App.
Event 1.75 "
Arsenic 0.020 0.000 0.000 0.000 0.000 0.000 0.000_ 0.000 0.000 0.000 0.000 0.000 0.020
Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 1.361 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.361
Chromium 0.192 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.192
Lead 0.091 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.091
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0 025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025
denum
Nickel 0.175 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.175
T
Selenium 0.030 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030
Zinc 6.282 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.282
Total
Phos- 87.250 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 87.250
phorus .
"I certify,under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonm t or knowing violations".
'----7
z z
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 3.61
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: Poplar Forest
Acres Used: 2.1 Acres Permitted: 2.1 Site#: NC YK 00008 Field#: YK 00008 0003
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample on 11 121 f 3 .J J .6_1 2_1 U 19 10 11 112 I
Com-
posite
Date 4/1901
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66 _
Molyb-
7.1
denum
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 I J 3 La I 51 6 _ 71 s I s J 10 11 11
DT/Ac./ a
App. z
Event 1.72
Arsenic 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020
Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 1.339 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.339
Chromium 0.189 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.189
Lead 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0 024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024
denum
Nickel 0.172 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.172
Selenium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.029
Zinc 6.181 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.181
Total
Phos- 85.850 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 85.850
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonm nt for knowing violations".
t/--;,__ ,__c_ z
Z._
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 6.38
Permit#: WQ000I800 Cation Exchange Capacity (non 503 only):
Operator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: Poplar Forest
Acres Used: 4.2 Acres Permitted: 4.2 Site#: NC YK 00008 Field#: YK 00008 0004
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample u J $f 9 10 11 112
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum
7.1
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total U 1 2 I ._3-I 41 5J 6..1 7j 8 9 10 11 12
DT/Ac./ o'
App.
Event 1.52
Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018
Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 1.184 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.184
Chromium 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.167
Lead 0.079 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.079
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022
denum
Nickel 0.152 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.152
Selenium 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026
Zinc 5.465 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.465
Total
Phos- 75.900 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 75.900
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
1)/6,,
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 2.16
Permit#: WQ0001800 Cation Exchange Capacity (non 503 only):
Operator: Billy Griffin Owner: Larry Styers Predominant Soil Series: Clifford
Acres Used: 2.1 Acres Permitted: 2.1 Site#: NC YK 00008 Field#:YK 00008 0006A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or i [ 2 l L _5_[ ±I [?i J . ) 11 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury _ 0.66
Molyb-
denum 7.1
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 1 U 3 4 J l 5 l 6 L U 9 10 Ili 12 y
DT/Ac./ o
App. As
c.
Event 1.03
Arsenic 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012
Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Copper 0.803 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.803
Chromium 0.113 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.113
_ Lead 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054
Mercury 0.00I 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Molyb- 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015
denum
Nickel 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103
-
Selenium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018
Zinc 3.708 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.708
Total
Phos- 51.500 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 51.500
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonmen r knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 1.44
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: Clifford
Acres Used: 1 Acres Permitted: 1 Site#: NC YK 00008 Field#:YK 00008 0006B
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 1 U U J I [ J 9 f i 0 11 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb- 71
denum
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total U 3 4_ 5J 6 17 8 9J 10 11 J 12
DT/Ac./
App. °r
Event 1.44
Arsenic 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017
Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 1.126 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.126
Chromium 0.159 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.159
Lead 0.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.002
Molyb- 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020
denum
Nickel 0.144 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.144
Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025
Zinc 5.195 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 5.195
Total
Phos- 72.150 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 72.150
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
113AX/
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

N
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville,NC Total Dry Tons Applied(Annual): 2.89
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Jack Adams Owner: Jack Adams Predominant Soil Series: Clifford
Acres Used: 7.5 Acres Permitted: 7.5 Site#: NC YK 00009 Field#: YK 00009 0001
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 i I 2 1 J U (J J J U U 1,31 1111 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum► 7.1
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11I 2 3 ': _41 71 8_1 9 10 11 12
DT/Ac./ o
K
App. w
Event 0.39 "
Arsenic 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Copper 0.300 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.300
Chromium 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042
Lead 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.000 0.020
Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Malyb 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
denum
Nickel 0.039 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.039
Selenium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Zinc 1.386 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1.386
Total
Phos- 19.250 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 19.250
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonme t for knowing violations".
il (.----77,„
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied(AnnuaI): 20.47
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Town of Yadkinville Owner: Town of Yadkinville Predominant Soil Series: Clifford
Acres Used: 11.5 Acres Permitted: 11.5 Site#: NC YK 00029 Field#: YK 00029 0001
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, °A) Solids use Raw Percent#):
Sample on 1 I 1 3 j 4 5 6J U 9 f 10 lin 12
Com-
posite
Date 3/25/21
%Solids 1.65
- Arsenic 6.7
Cadmium 1.2 _
Copper 40
Chromium 42
Lead 33
Mercury 1.1
Molyb- 9 2
denum
Nickel 18
Selenium 8.5
Zinc 160
Total
Phos- 1200
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 121 J 4 5 61 71 F 8 9( 10 11 12 y
DT/Ac./ o
App.
Event 1.78
Arsenic 0.024 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024
Cadmium_ 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Copper 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.142
Chromium 0.150 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.150
Lead 0.117 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.117
Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Molyb- 0 033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033
denum
Nickel 0.064 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.064
Selenium 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030
_ Zinc 0.570 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.570
Total
Phos- 4.272 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.272
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonmen for knowing violations".
2_9_ 7-_
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied(Annual): 14.43
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: James Hobson Owner: Kenneth Hobson Predominant Soil Series: Clifford
Acres Used: 7.6 Acres Permitted: 7.6 Site#: NC YK 00033 Field#: YK 00033 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or± I 21 U U U 61 8 9 10 11 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8 _
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
7.1
denum
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 I 21 4 i 5_1 6 li 9 10 11 j 12
DT/Ac./
App.
Event 1.90
Arsenic 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022
Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Copper 1.480 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 1.480
Chromium 0.209 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.209
Lead 0.099 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099
Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb- 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
denum
Nickel 0.190 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.190
Selenium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
Zinc 6.833 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.833
Total
Phos- 94.900 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 94.900
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonme t for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied(Annual): 7.94
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: James Hobson Owner: Kenneth Hobson Predominant Soil Series: Clifford
Acres Used: 6.4 Acres Permitted: 6.4 Site#: NC YK 00033 Field#: YK 00033 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or�. 1 21 U 5 J 6 J 7J L8 J 10l 11_11 1 j
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8 _
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum 7.1
Nickel 50
Selenium 8,5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 ; 31 4 J -6 L 7 8 u 10 11 12 I
DT/Ac./ "
O
App. a_
Event 1.24
Arsenic 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014
Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Copper 0.967 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.967
Chromium 0.136 0.000 ^0.000 0.000 ^0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.136
T
Lead 0.064 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.064
Mercury 0.002 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018
denim _
Nickel 0.124 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.124
Selenium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021
Zinc 4.464 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 4.464
Total
Phos- 62.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 62.000
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonme f or knowing
violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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)IX

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied(Annual): 19.48
Permit#: WQ0001800 Cation Exchange Capacity(non 503 only):
Operator: Roger Davis Owner: Roger Davis Predominant Soil Series: Clifford
Acres Used: 12.2 Acres Permitted: 12.2 Site#: NC YK 00035 Field#: YK 00035 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2 3 LL J L U _9i10 I31 , 12
Com-
posite
Date 4/19/21
%Solids 2.79
Arsenic 5.8
Cadmium 0.99
Copper 390
Chromium 55
Lead 26
Mercury 0.66
Molyb-
denum 7'1
Nickel 50
Selenium 8.5
Zinc 1800
Total
Phos- 25000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total L _3_1 4 1 _J 6 _7] .8 j 9 10 11 I 12
DT/Ac./ "
0
App. cp
Event 1.60
Arsenic 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019
Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Copper 1.245 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.245
Chromium 0.176 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.176 _
Lead 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.083
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023
denum
Nickel 0.160 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.160
Selenium 0.027_ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Zinc 5.746 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.746
Total
Phos- 79.800 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 79.800
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment or knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

S
a i' Summit Environmental Technologies,Inc.
EIrg 3310 Win St.
MUM ENVIRONMENTAL TECHNOLOCIES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
April 02,2021
Alex Fox
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL:
FAX:
RE: Yadkinville
Dear Alex Fox: Order No.: 21031808
Summit Environmental Technologies, Inc. received 2 sample(s) on 3/26/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
1...v10.144,01 )77��
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 39

SUMMIT
Summit Environmental Technologies,Inc.3310 Win 2t. Case Narrative
itira ENVIRONMENTAL TECliN❑LOGIES.INC. Cuyahoga Falls,Ohio 44223 WO#: 21031808
MI 4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 4/2/2021
CLIENT: Synagro
Project: Yadkinville
WorkOrder Narrative:
21031808: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report,Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or"wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21031808-001A TCLP-VOC-MSTR 8260D: Corresponding QC exhibited high recovery for Vinyl
chloride. Sample is ND
21031808-002A TCLP-VOC-MSTR 8260D: Corresponding QC exhibited high recovery for Vinyl
chloride. Sample is ND
Analytical Sequence QC Notes:
Pest CCV1 500ppb TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater
than 40%.
CCV VOC-MSTR NPW(8260): CCV exhibits high recovery for Vinyl chloride. Associated samples
Original
Page 2 of 39

5Mt'T Summit Environmental Technologies,Inc. Case Narrative
mu 3310 Ohio Win St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21031808rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 4/2/2021
CLIENT: Synagro
Project: Yadkinville
are N.D. for this analyte.
LCS-48669 TCLP-VOC-MSTR TCLP(8260): LCS exhibits high recovery for Vinyl chloride.
Associated samples are N.D. for this analyte. Possible high bias for Vinyl chloride due to high recovery
in CCV.
Original
Page 3 of 39

•
17 S
Mm iT Summit Environmental Technologies,In Qualifiers and Acronyms
331 i Wm 5 `C
Arralytiica @N1 L orator iN❑cOG{ S.INC Cuyahoga Falls,Ohio 442 WO#: 21031808rral}'t�caf iaboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 4/2/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLv1 Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 39

S
��'� Summit Environmental Technologies,Inc. Workorder
3310 Win St.
1.7611 ENVIRONMENTAL TECHNQI. oiEs,it c, Cuyahoga Falls,Ohio 44223 Sample Summary
rralyt�cal iaboralorlas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com 02-Apr-21
CLIENT: Synagro
Project: Yadkinville
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
21031808-001 Yadkinville WWTP 3/25/2021 9:00:00 AM 3/26/2021 4:00:00 PM Sludge
2 1 03 1 808-002 Yadkinville WTP 3/25/2021 10:00:00 AM 3/26/2021 4:00:00 PM Sludge
Page 5 of 39

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S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 9:00:00 AM
Lab ID: 21031808-001A
Project: Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200 mg/L 1 4/2/2021 3:08:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: DNS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 4/2/2021 1:22:23 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 4/2/2021 1:22:23 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 4/2/2021 1:22:23 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 4/2/2021 1:22:23 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 4/2/2021 1:22:23 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 4/2/2021 1:22:23 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 4/2/2021 1:22:23 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 4/1/2021 7:22:00 PM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 4/1/2021 7:22:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 4/1/2021 7:22:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 4/1/2021 7:22:00 PM
Cresols,Total ND 10.0 mg/L 2 4/1/2021 7:22:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 4/1/2021 7:22:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 4/1/2021 7:22:00 PM
Hexachloroethane ND 0.200 mg/L 2 4/1/2021 7:22:00 PM
Nitrobenzene ND 0.200 mg/L 2 4/1/2021 7:22:00 PM
Pentachlorophenol ND 0.500 mg/L 2 4/1/2021 7:22:00 PM
Pyridine ND 0.500 mg/L 2 4/1/2021 7:22:00 PM
Surr:2-Fluorophenol 86.5 10-157 %Rec 2 4/1/2021 7:22:00 PM
Surr: Phenol-d6 91.4 10-169 %Rec 2 4/1/2021 7:22:00 PM
Surr: Nitrobenzene-d5 80.0 32.1 -130 %Rec 2 4/1/2021 7:22:00 PM
Surr:2,4,6-Tribromophenol 113 45.4-166 %Rec 2 4/1/2021 7:22:00 PM
Surr:2-Fluorobiphenyl 79.5 35.7-130 %Rec 2 4/1/2021 7:22:00 PM
Surr: p-Terphenyl-d14 112 70-145 %Rec 2 4/1/2021 7:22:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 39

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 9:00:00 AM
Lab ID: 21031808-001A
Project: Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 4/1/2021 8:10:00 PM
Toxaphene ND 0.0500 mg/L 1 4/1/2021 8:10:00 PM
Endrin ND 0.00250 mg/L 1 4/1/2021 8:10:00 PM
gamma-BHC ND 0.00250 mg/L 1 4/1/2021 8:10:00 PM
Heptachlor ND 0.00250 mg/L 1 4/1/2021 8:10:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 4/1/2021 8:10:00 PM
Methoxychlor ND 0.00250 mg/L 1 4/1/2021 8:10:00 PM
Surr:TCMX 72.2 10-119 %Rec 1 4/1/2021 8:10:00 PM
Surr: DCB 91.1 10-119 %Rec 1 4/1/2021 8:10:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321 SW1311M Analyst: TM
2,4-D ND 0.500 mg/L 50 4/1/2021 11:00:00 PM
2,4,5-TP ND 0.500 mg/L 50 4/1/2021 11:00:00 PM
Surr:2,4-Dichlorophenylacetic aci 72.9 70-130 %Rec 50 4/1/2021 11:00:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
MEK ND 5.00 mg/L 50 4/1/2021 8:51:00 PM
Benzene ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
Chlorobenzene ND 2.50 mg/L 50 4/1/2021 8:51:00 PM
Chloroform ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
Tetrachloroethene ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
Trichloroethene ND 0.250 mg/L 50 4/1/2021 8:51:00 PM
Vinyl chloride ND 0.100QC+QL+mg/L 50 4/1/2021 8:51:00 PM
Surr:4-Bromofluorobenzene 91.6 70-130 %Rec 50 4/1/2021 8:51:00 PM
Surr: Dibromofluoromethane 99.2 70-130 %Rec 50 4/1/2021 8:51:00 PM
Surr:Toluene-d8 100 70-130 %Rec 50 4/1/2021 8:51:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 39

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES.IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 9:00:00 AM
Lab ID: 21031808-001A
Project: Yadkinville
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.490 mg/Kg 1 3/31/2021 2:55:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: KMW
Ignitability nonflammable mm/sec 1 4/1/2021 11:13:20 AM
RCI SW9045D Analyst: ALT
PH (SW9045D)
pH 7.2 s.u.@16.9C 1 3/29/2021 5:36:55 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 3/31/2021 2:55:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 9 of 39

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 10:00:00 AM
Lab ID: 21031808-002A
Project: Yadkinville
Client Sample ID Yadkinville WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.0100 mg/L 1 4/2/2021 3:22:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: DNS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 4/2/2021 1:26:24 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 4/2/2021 1:26:24 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 4/2/2021 1:26:24 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 4/2/2021 1:26:24 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 4/2/2021 1:26:24 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 4/2/2021 1:26:24 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 4/2/2021 1:26:24 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.500 mg/L 5 4/1/2021 7:54:00 PM
2,4,5-Trichlorophenol ND 1.25 mg/L 5 4/1/2021 7:54:00 PM
2,4,6-Trichlorophenol ND 1.25 mg/L 5 4/1/2021 7:54:00 PM
2,4-Dinitrotoluene ND 0.250 mg/L 5 4/1/2021 7:54:00 PM
Cresols,Total ND 25.0 mg/L 5 4/1/2021 7:54:00 PM
Hexachloro-1,3-butadiene ND 0.100 mg/L 5 4/1/2021 7:54:00 PM
Hexachlorobenzene ND 0.250 mg/L 5 4/1/2021 7:54:00 PM
Hexachloroethane ND 0.500 mg/L 5 4/1/2021 7:54:00 PM
Nitrobenzene ND 0.500 mg/L 5 4/1/2021 7:54:00 PM
Pentachlorophenol ND 1.25 mg/L 5 4/1/2021 7:54:00 PM
Pyridine ND 1.25 mg/L 5 4/1/2021 7:54:00 PM
Surr:2-Fluorophenol 71.6 10-157 %Rec 5 4/1/2021 7:54:00 PM
Surr: Phenol-d6 85.4 10-169 %Rec 5 4/1/2021 7:54:00 PM
Surr: Nitrobenzene-d5 82.2 32.1 -130 %Rec 5 4/1/2021 7:54:00 PM
Surr:2,4,6-Tribromophenol 104 45.4-166 %Rec 5 4/1/2021 7:54:00 PM
Surr:2-Fluorobiphenyl 81.8 35.7-130 %Rec 5 4/1/2021 7:54:00 PM
Surr: p-Terphenyl-d14 111 70-145 %Rec 5 4/1/2021 7:54:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 10 of 39

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 10:00:00 AM
Lab ID: 21031808-002A
Project: Yadkinville
Client Sample ID Yadkinville WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 4/1/2021 8:32:00 PM
Toxaphene ND 0.0500 mg/L 1 4/1/2021 8:32:00 PM
Endrin ND 0.00250 mg/L 1 4/1/2021 8:32:00 PM
gamma-BHC ND 0.00250 mg/L 1 4/1/2021 8:32:00 PM
Heptachlor ND 0.00250 mg/L 1 4/1/2021 8:32:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 4/1/2021 8:32:00 PM
Methoxychlor ND 0.00250 mg/L 1 4/1/2021 8:32:00 PM
Surr:TCMX 71.9 10-119 %Rec 1 4/1/2021 8:32:00 PM
Surr: DCB 80.1 10-119 %Rec 1 4/1/2021 8:32:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321 SW1311M Analyst: TM
2,4-D ND 0.500 mg/L 50 4/1/2021 11:57:00 PM
2,4,5-TP ND 0.500 mg/L 50 4/1/2021 11:57:00 PM
Surr:2,4-Dichlorophenylacetic aci 85.4 70-130 %Rec 50 4/1/2021 11:57:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
MEK ND 5.00 mg/L 50 4/1/2021 8:23:00 PM
Benzene ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
Chlorobenzene ND 2.50 mg/L 50 4/1/2021 8:23:00 PM
Chloroform ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
Tetrachloroethene ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
Trichloroethene ND 0.250 mg/L 50 4/1/2021 8:23:00 PM
Vinyl chloride ND 0.100QC+QL+mg/L 50 4/1/2021 8:23:00 PM
Surr:4-Bromofluorobenzene 92.0 70-130 %Rec 50 4/1/2021 8:23:00 PM
Surr: Dibromofluoromethane 98.0 70-130 %Rec 50 4/1/2021 8:23:00 PM
Surr:Toluene-d8 99.1 70-130 %Rec 50 4/1/2021 8:23:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 11 of 39

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES.IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com Date Reported: 4/2/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/25/2021 10:00:00 AM
Lab ID: 21031808-002A
Project: Yadkinville
Client Sample ID Yadkinville WTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.476 mg/Kg 1 3/31/2021 2:55:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: KMW
Ignitability nonflammable mm/sec 1 4/1/2021 11:13:20 AM
RCI SW9045D Analyst: ALT
PH (SW9045D)
pH 6.8 s.u.@17.2C 1 3/29/2021 5:36:55 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 3/31/2021 2:55:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 12 of 39

�� SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
1. 3310 Win St. Anal�7teS RenOrt
ENVIRONMENTAL TECHNOLOGIES,INC
Cuyahoga Falls,Ohio 44223 J Y
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com 02 Apr 2l
Client: Synagro State: NW
Project: Yadkinville Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
2 1 03 1 808-00 1A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive U
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive U
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Original#1
Page 13 of 39

� SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal teS Report
um ENVIRONMENTAL TECHN❑w oes,INC Cuyahoga Falls,Ohio 44223 3' P
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com 02 Apr 2l
Client: Synagro State: NW
Project: Yadkinville Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
2 1 03 1 808-00 1A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
2 1 03 1 808-002A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive U
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive U
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Original#1
Page 14 of 39

�� SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
1. 3310 Win St. Anal teS Report
ENVIRONMENTAL TECHN❑w oes,INC Cuyahoga Falls,Ohio 44223 3' P
rral}'ticaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21031808
Website:http://www.settek.com 02 Apr 2l
Client: Synagro State: NW
Project: Yadkinville Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
2 1 03 1 808-002A Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Original#1
Page 15 of 39

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Page 37 of 39

;74700,1summIT Summit Environmental Techn3310ologiesW,in Inc.St.
II a
ENVIRONMENTAL TEC„NOLOGaS,INC Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
ArrafyOcaf Laborator/as TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21031808 RcptNo: 1
Logged by: Christina N.Jager 3/26/2021 4:00:00 PMrxx
Completed By: Jacqueline Rasile 3/28/2021 11:39:11 AM
Reviewed By: Jennifer Woolf 3/29/2021 1:26:08 PM (...710‘7*.?1' M''oaL011,--
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? UPS
Log In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no, notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑d No ❑ NA ❑
Person Notified: 'Alex Fox Date:I 3/29/2021
By Whom: 'Jennifer Woolf Via: 0 eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: both bottles labeld as WWTP
Client Instructions: 'the Brown one is WTP and the Blacker one is WWTP.
18.Additional remarks:
the Brown one is WTP and the Blacker one is WWTP.
samples not labeled
both lids labled as WWTP
Cooler Information
Page 38 of 39

iiiiiw S
M M'T Summit Environmental Technologies,Inc.
3310 Win St.
MN ENVIRONMENTAL TECHNOLOQ4S,ihi Cuyahoga Falls,Ohio 44223 Sample Log-In Check List
Arrafy1k of iaboralorJas TEL:[phone] FAX [phone]
Website:http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21031808 RcptNo: 1
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 2.6 Good Not Present
Page 39 of 39

TCLP data is not included in the 2021 Annual Report for Yadkinville WTP. A TCLP sample was
taken in 2019 and is only required to be taken once per permit cycle.

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Town of Yadkinville WQ Permit Number: WQ 00001800
WWTP Name: Yadkinville WWTP NPDES Number: -NOMA-I.90—�� NCoO 2O 33 a
Monitoring Period: From 01/01/2021 To 12/31/21
Pathogen Reduction(40 CFR 503.32/ISA NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP) _
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Gee,Mean Maximum Units deuces Analysis
Fecal 2x10 to the 6'1' MPN 7,667 8364 10,101 MPNig 0 Annual Grab Sm9221C
Coliform power per gram E
of total solids
CFU CFUig
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/ISA NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) _ __ (30day bench) ___ (Spec.02 uptake)
OptioniAlt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying-Stable) (Drying-Unstable)
Option/Alt.9 Option/Alt.10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met.'
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of tht requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel property gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. 1 am aware that there are significant penalties for false certification including fine and imprisonment."
Grant Trivette Plant Manager
Pre Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
Si attire of Pteparer• Date Signature of Land Applier(if applicable) Date
'Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1 102(26)

Analytical Results STATESVILLE
Ibt ANALYTICAL
Town of Yadkinville
PO Box 816
Yadkinville, NC 27055
Receive Date: 04/29/2021
Reported: 05/03/2021
For: Holding Tank Fecals
Comments: Geometric Mean: 8364 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210429-10-01 Fecal Coliforms HT#1 7692 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-01 Percent Solids HT#1 2.99 % SM2540B-2011 04/29/2021 MD
210429-10-02 Fecal Coliforms HT#2 7667 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-02 Percent Solids HT#2 3.0 % SM2540B-2011 04/29/2021 MD
210429-10-03 Fecal Coliforms HT#3 7823 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-03 Percent Solids HT#3 2.94 % SM2540B-2011 04/29/2021 MD
210429-10-04 Fecal Coliforms HT#4 10101 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-04 Percent Solids HT#4 2.97 % SM2540B-2011 04/29/2021 MD
210429-10-05 Fecal Coliforms HT#5 8070 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-05 Percent Solids HT#5 2.85 % SM2540B-2011 04/29/2021 MD
210429-10-06 Fecal Coliforms HT#6 9901 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-06 Percent Solids HT#6 3.03 % SM2540B-2011 04/29/2021 MD
210429-10-07 Fecal Coliforms HT#7 7692 MPN/g SM92210E-2006 04/29/2021 MD
210429-10-07 Percent Solids HT#7 2.99 % SM2540B-2011 04/29/2021 MD
Respectfully submitted,
% L j. 1,-
Melissa Myers
NC Cert#440,
NCDW Cert#37755,
EPA#NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210429-10-01 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-02 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-03 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-04 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-05 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-06 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210429-10-07 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

(0) rD
voblialesoids.xit 2/2106 %TOTAL SOLIDS %VOLATILE SOLIDS
SM 2540 G
Analyzed By calculated Sy: SA
Date in 103-105 oven: ., —30 —02. 1 Date In 550 furnace: 3—
Tine In 103-105 oven: I itm Time In 550 furnace: 1 „.491.6r),A
Time Out 103-105 oven: 0 Lo SI< Time Out 550 furnace: A a,t 4 j,-, obAk_,
itmenAL , -NMAL
gitaPPe ID ,7643 LAch 14 I -meow r4ch ±) 2
13rtstt wt. -"-1 U. c) (1) i-i- i 1 -/. 0 (scec0
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V&V % hv %adage %volatile Intl&
-Tsch t\ 5 2 fraction 0, 4- i r3 *wen AVERAGE:
C ,
Caltzdadon for TS%and VS%: Dry wt.-Deb wt. X 100
Sample vol.
0\1 €_,Ie)
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0 GD Iit. .C2) --to 0., -,
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USE INITIAL AND FINAL AVERAGES OF YOUR%VOLATILE FRACTION TO CALCULATE THE
PERCENT REDUCTION(USE THE VAN KLEECK FORMULA)
Van Kieeck Reduction: Initial%vol.frac.-Final%vol. frac. X 100=%reduction
Initial%vol.frac.-(Initial%vol.frac x Final%vol.frac.)
( 0, (-P 51 ) minus ( 6 , i-i a c 1 ) x too = (� 2_tizi
( 6 , (e Lt S ( ) minus [( ( , 4 (.4. 5 I times C. 1-0_`i 1 )1
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*Do multiplication inside[( )} before you subtract on bottom of equation.
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6i31 -765t/
__

SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: Yadkinville WWTP
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied(CCE Eq.)
YK-08-1 5.9 .5 T/AC *
YK-08-2 5.7 .5 T/AC *
YK-08-3 5.8 .5 T/AC *
YK-08-4 5.4 .5 T/AC *
YK-08-6A 5.7 .5 T/AC *
YK-08-6B 5.7 .5 T/AC *
YK-09-1 5.4 .5 T/AC *
YK-33-1 5.7 .5 T/AC 1 T/AC 09/05/21
YK-33-2 6.3 0.0T/AC 0.0
YK-35-1 5.0 .5 T/AC *
YK-29-1 6.1 0.0 0.0T/AC
*Lime will be applied when conditions improve.

SECTION 7

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