WQ0034688_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0034688
Applicant/Permittee Neuse Regional Water and Sewer Authority
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0034688
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* Neuse Regional WASA Class A Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for NeUse Regional Water and Sewer Authority,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
NeUse NC 2021 Annual Report FINAL.pdf 7.97MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja rotivit5
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0034688
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of Neuse
Regional Water and Sewer Authority, NC.
If you have any questions or need additional information,please do not hesitate to contact
Charlie Colie at(252) 522-2567 or Chris Wynne at 336-909-8627.
Sincerely,
l e't ic& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Charlie Colie, Neuse Regional Water and Sewer Authority
Chris Wynne, Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

NEUSE REGIONAL WATER AND SEWER
AUTHORITY
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0034688
2021 ANNUAL REPORT

Neuse Regional Water and Sewer Authority, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00034688 County Lenoir Year 2021
Facility Name(as shown on permit)Neuse Regional Water Treatment Plant NPDES No.NC00881I 1
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO,skip Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 315.41
Total number of acres utilized for land application during the year: 127.90
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-13 below)issued by the Division of Water Quality X YES NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5_ All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified Iaboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40(..:1FR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals_
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations."
Harold Herring.Executive Director 2/2✓/Z�i
Permittee Name and Title(type or print) ignature of Permittee Date
2/21/2022
Signature of Preparer* Date S e of La Applier Date
(if different from Permittee) (if diffi,reut am Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 12/31/2021
NEUSE REGIONAL WASA,NC
NEUSE REGIONAL WASA,NC WTP LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
October 2021 2,740,500.00 G 315.41 D 286.08
TOTAL 2,740,500.00 G 315.41 D 286.08
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date:2/4/2022 12:10:46 PM

SECTION 2

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Neuse Regional WASA
Lot Number:W109030
Date Completed:09/20/2021
09/22/2021 12:18 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,)0)
MILD
'ye )
ANSI NatonalAccredltatlon Board
ACCREDITEDORA1O,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WI09030
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the initial sample amount used for the following samples was 3X more than
the standard procedure: WI09030-001. The LOQ has been adjusted accordingly.
Inorganic Non-Metals
The following sample was diluted due to the nature of the sample matrix for Nitrate and Nitrite: WI09030-
001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:W109030-001
Description:Neuse Regional WASA Matrix:Solid
Date Sampled:09/08/2021 1430 % Solids: 2.76 09/10/2021 0016
Date Received:09/09/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 09/10/2021 0016 NBW 14920
2 350.1 (Ammonia-N )350.1 1 09/17/2021 1452 MSG 15693
1 (Nitrate-N )9056A 5 09/14/2021 1040 AMR 15374
1 (Nitrite-N )9056A 5 09/14/2021 1040 AMR 15376
1 (Phosphorus)365.1 2 09/10/2021 1612 DMA 09/10/2021 0951 14939
1 (Soil pH meas)9045D 1 09/09/2021 2140 NBW 14917
1 351.4 (TKN)351.2 1 09/17/2021 1124 DMA 09/16/2021 1346 15511
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 2.76 % 1
Ammonia-N (gas diffusion) 350.1 490 36 19 mg/kg 2
Nitrate-N (soluble) 9056A 37 J 90 18 mg/kg 1
Nitrite-N (soluble) 9056A ND 36 18 mg/kg 1
Phosphorus 7723-14-0 365.1 1900 360 72 mg/kg 1
Soil pH measured in water @ 19°C 9045D 6.3 su 1
TKN 351.2 5900 1800 900 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 09/17/2021 1544 CMS2 09/16/2021 1531 15357
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.8 0.69 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/15/2021 0545 JMH 09/14/2021 1046 15134
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 120000 240 90 mg/kg 1
Arsenic 7440-38-2 6010D 9.0 9.0 3.0 mg/kg 1
Cadmium 7440-43-9 6010D ND 3.0 0.76 mg/kg 1
Calcium 7440-70-2 6010D 1500 J 3000 380 mg/kg 1
Chromium 7440-47-3 6010D 18 6.0 1.5 mg/kg 1
Copper 7440-50-8 6010D 120 6.0 2.7 mg/kg 1
Iron 7439-89-6 6010D 26000 60 27 mg/kg 1
Lead 7439-92-1 6010D 16 6.0 2.7 mg/kg 1
Magnesium 7439-95-4 6010D 800 J 3000 380 mg/kg 1
Manganese 7439-96-5 6010D 1100 9.0 3.6 mg/kg 1
Molybdenum 7439-98-7 6010D ND 24 6.0 mg/kg 1
Nickel 7440-02-0 6010D 11 J 24 6.3 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:W109030-001
Description:Neuse Regional WASA Matrix:Solid
Date Sampled:09/08/2021 1430 % Solids: 2.76 09/10/2021 0016
Date Received:09/09/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/15/2021 0545 JMH 09/14/2021 1046 15134
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 780 J 3000 380 mg/kg 1
Selenium 7782-49-2 6010D ND 12 4.9 mg/kg 1
Sodium 7440-23-5 6010D 710 J 3000 380 mg/kg 1
Zinc 7440-66-6 6010D 62 30 7.5 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
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Samples Renalpt Chaddist(SRC)IME 111a3C-15) R€vised:5/29{?_020 c
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Sample Receipt Checklist (SRC)
Cli;,rit- SVNAriRO CO3Ccr Insp0r;kxt byld9it: ft C2 , [91 IVII:r2_ Lot iri,. W1040?0
Means of receipt: ❑ Pace anent El UPS ❑f'eax ❑other:
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_Yes ©No DNA 2. II custody aeaEs.were present,were 11:ey Mint and unbroken?
Jpli Strip JD: E4A-. C11iar..nrStrip ID: al Tested by;NA
Original temperature upon receipt J Derived(Corrected)temperature upon receipt %Solid Snap•Cup ID: 21-1425
5.6 ,r 5.4 ac NA I NA 6t NN A .0 NA oC NA it NA [lc
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1Mdthod ofctiolanL 0 '.Vet lee E ice Packs 0 Dry Ice ❑ None
❑Ycs ❑Nu z NA 3, I f Inn I:.ralture of gray ixl[}IL.Y c.:ccudud 6,0°C, was ProjL t-Manager Notified?
PM4 IN kn.NoIEIi iby;I]irml]L: cinui1 far;4•-lo-Face(c[rcic one).
0 Yes ❑No DNA 4, Is the cott,morciol coiner'*packing slip txlaelled to this form? I k
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J Yrs r j No 7. Were sample Ms listed on all sentp]e containers? I
El Yes ❑No R. WAS collea:[ion 4Ia1.e&lime]i led nn tIi COC'? 1
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n Yes ❑No J I. Wcrc tests to be performed listed on the CUC7
12. Did all 5arr1[rles ordv'c [n the proper contain al;x for each test er-c/or in good coLLLliLioII
0 Yes ❑No {tmbraken,tide on,cto.)? _� I
:Pi Yes Li No 13, Watsadequauk satnokvolLane avai;able~?
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Sample PiTstrt^Itldta (KIS:be 461iiplaCCI Fo.-any sanaple(s) incorrectly preserved or with iir[adspa o.)
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Tirm Urpte.rs rvatEon NA . If more Lime orc preservative is needed,pease ante In thm comments below.
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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SECTION 4

S
a i' Summit Environmental Technologies,Inc.
in7r4 331 Wm St.
Arrary01JMLNTALTECIiNOLOd',i S,IF#C Cuyahoga Falls,Ohio 44223
rralyt�cal iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
September 03,2021
Chris Wynne
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL:
FAX:
RE: Neuse Regional WASA
Dear Chris Wynne: Order No.: 21081554
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/25/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
/.....?-74424f4 177��
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 37

SUMMIT
Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21081554rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 9/3/2021
CLIENT: Synagro
Project: Neuse Regional WASA
WorkOrder Narrative:
21081554: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21081554-OO1A TCLP-SVOC 8270E: CCV exhibits high recovery for 2,4,5-Trichlorophenol. Sample
is ND for this analyte.
21081554-O01A PctSolid S(2540): High RPD due to suspected sample inhomogeneity.
Analytical Sequence QC Notes:
CCV 4OPPM SVOC-MSTR S(8270): CCV exhibits high recovery for 2,4,5-Trichlorophenol. All
associated samples are ND for this analyte. Surrogate outside recovery limits. Minimum method
criterion of one surrogate within established recovery limits was met.
LCS/LCSD-51552 SVOC-BNA TCLP(8270): LCS/LCSD-51552 exceeded calibration range for
surrogate 2,4,6-Tribromophenol. Detection should be considered an estimated concentration. Recovery
Original
Page 2 of 37

SUMMIT
Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21081554rrafyt�caf iaboralorlas TEL:[phone] FAX [phone]
Website:http://www.settek.com Date: 9/3/2021
CLIENT: Synagro
Project: Neuse Regional WASA
was within acceptance criteria. Possible high bias for 2,4,5-Trichlorophenol due to high recovery in
CCV. LCS/LCSD-51552 exhibited high RPD for Pyridine. Both LCS/LCSD-51552 demonstrated
control for this compound individually.
MB-51552 SVOC-BNA TCLP(8270): MB-51552 exceeded calibration range for surrogate 2,4,6-
Tribromophenol. Detection should be considered an estimated concentration. Recovery was within
acceptance criteria.
21081554-001ADUP PctSolid S(2540): High RPD due to suspected sample inhomogeneity.
Original
Page 3 of 37

•
17 S
Mm i or Summit Environmental Techno3310Wlogies,Ins
Qualifiers and Acronyms
EkiwllxsStJM@N1'nLTecriw❑LOG{ES.rF#I; Cuyahoga Falls,Ohio 442 WO#: 21081554
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.co Date: 9/3/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 37

S t�' Summit Environmental Technologies,Inc. Workorder
3310 Win St.
1.7
ENVIRONMENTAL'Melilla WC,3ES,pm,
Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 21081554
Website:http://www.settek.com 03-Sep-21
CLIENT: Synagro
Project: Neuse Regional WASA
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
21081554-001 Neuse Regional WASA 8/24/2021 10:30:00 AM 8/25/2021 10:05:00 AM Sludge
Page 5 of 37

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MM Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
itrgINiM EENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21081554
Website:http://www.settek.com Date Reported: 9/3/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/24/2021 10:30:00 AM
Lab ID: 21081554-001A
Project: Neuse Regional WASA
Client Sample ID Neuse Regional WASA
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: JEB
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200 mg/L 1 8/27/2021 2:50:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010 SW3010A Analyst: MSK
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 8/27/2021 3:41:00 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 8/27/2021 3:41:00 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 8/27/2021 3:41:00 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 8/27/2021 3:41:00 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 8/27/2021 3:41:00 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 8/27/2021 3:41:00 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 8/27/2021 3:41:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS(SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 8/30/2021 8:36:00 PM
2,4,5-Trichlorophenol ND 0.500 QC+ mg/L 2 8/30/2021 8:36:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 8/30/2021 8:36:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 8/30/2021 8:36:00 PM
Cresols,Total ND 10.0 mg/L 2 8/30/2021 8:36:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 8/30/2021 8:36:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 8/30/2021 8:36:00 PM
Hexachloroethane ND 0.200 mg/L 2 8/30/2021 8:36:00 PM
Nitrobenzene ND 0.200 mg/L 2 8/30/2021 8:36:00 PM
Pentachlorophenol ND 0.500 mg/L 2 8/30/2021 8:36:00 PM
Pyridine ND 0.500 mg/L 2 8/30/2021 8:36:00 PM
Surr:2-Fluorophenol 65.4 10-157 %Rec 2 8/30/2021 8:36:00 PM
Surr: Phenol-d6 72.4 10-169 %Rec 2 8/30/2021 8:36:00 PM
Surr: Nitrobenzene-d5 51.8 32.1 -130 %Rec 2 8/30/2021 8:36:00 PM
Surr:2,4,6-Tribromophenol 93.0 45.4-166 %Rec 2 8/30/2021 8:36:00 PM
Surr:2-Fluorobiphenyl 56.8 35.7-130 %Rec 2 8/30/2021 8:36:00 PM
Surr:p-Terphenyl-d14 83.1 70-145 %Rec 2 8/30/2021 8:36:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected OG1
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 37

S
MM Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
itrgINiM EENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21081554
Website:http://www.settek.com Date Reported: 9/3/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/24/2021 10:30:00 AM
Lab ID: 21081554-001A
Project: Neuse Regional WASA
Client Sample ID Neuse Regional WASA
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 8/30/2021 1:10:00 PM
Toxaphene ND 0.0500 mg/L 1 8/30/2021 1:10:00 PM
Endrin ND 0.00250 mg/L 1 8/30/2021 1:10:00 PM
gamma-BHC ND 0.00250 mg/L 1 8/30/2021 1:10:00 PM
Heptachlor ND 0.00250 mg/L 1 8/30/2021 1:10:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 8/30/2021 1:10:00 PM
Methoxychlor ND 0.00250 mg/L 1 8/30/2021 1:10:00 PM
Surr:TCMX 62.3 10-119 %Rec 1 8/30/2021 1:10:00 PM
Surr: DCB 53.9 10-119 %Rec 1 8/30/2021 1:10:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321 Analyst: TM
2,4-D ND 0.500 mg/L 50 9/1/2021 12:52:00 AM
2,4,5-TP ND 0.500 mg/L 50 9/1/2021 12:52:00 AM
Surr:2,4-Dichlorophenylacetic aci 123 70-130 %Rec 50 9/1/2021 12:52:00 AM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
1,2-Dichloroethane ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
MEK ND 10.0 mg/L 100 8/27/2021 8:30:00 PM
Benzene ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
Carbon tetrachloride ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
Chlorobenzene ND 5.00 mg/L 100 8/27/2021 8:30:00 PM
Chloroform ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
Tetrachloroethene ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
Trichloroethene ND 0.500 mg/L 100 8/27/2021 8:30:00 PM
Vinyl chloride ND 0.200 mg/L 100 8/27/2021 8:30:00 PM
Surr:4-Bromofluorobenzene 98.5 70-130 %Rec 100 8/27/2021 8:30:00 PM
Surr: Dibromofluoromethane 100 70-130 %Rec 100 8/27/2021 8:30:00 PM
Surr:Toluene-d8 102 70-130 %Rec 100 8/27/2021 8:30:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected OG1
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 8 of 37

S
M� 331 Win St.Summit Environmental Technologies,Inc. Analytical Report
muEENVIRONMENTAL TECtiNO�OGIES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�cai iaboralorfas TEL:[phone] FAX [phone] WON: 21081554
Website:http://www.settek.com Date Reported: 9/3/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/24/2021 10:30:00 AM
Lab ID: 21081554-001A
Project: Neuse Regional WASA
Client Sample ID Neuse Regional WASA
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide,Reactive ND 12.4 mg/Kg 1 8/27/2021 2:13:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: ALT
Ignitability non flammable mm/sec 1 8/26/2021 5:28:32 PM
PERCENT SOLIDS BY SM2540MOD A2540B Analyst: DHC
Percent Solids 2.84 QDR % 1 8/31/2021 7:00:00 PM
RCI SW9045D Analyst: ALT
PH (SW9045D)
pH 6.5 s.u.@22.2C 1 8/26/2021 3:00:24 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive 40.0 25.0 mg/Kg 1 8/27/2021 2:13:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected OG1
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 9 of 37

SUMMIT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MI ENVIRONMENTAL TECHN❑Lo l 5,i Cuyahoga Falls,Ohio 44223 J Y
rral}'ticaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21081554
Website:http://www.settek.com 03-Sep-21
Client: Synagro State: NW
Project: Neuse Regional WASA Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21081554-001A Sludge Ignitability of Solids(SW-846:1030) Ignitability A
Sludge Percent Solids by SM2540Mod Percent Solids N
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive U
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive U
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Key Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl
Original#1
Page 10 of 37

S UMM'T Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7tes Report
EN ENWIRONM@NtAL TECHNOLociEs,i Cuyahoga Falls,Ohio 44223 Analytes
rral}'ticaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21081554
Website:http://www.settek.com 03-Sep-21
Client: Synagro State: NW
Project: Neuse Regional WASA Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21081554-001A Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl
Original#1
Page 11 of 37

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Page 36 of 37

iw SUMMIT
Summit Environmental Technologies,Inc.
OM 3310 Win St.
Arm' OtJMENtALTtiriNOL4Ga S.lFr Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
yt�caf iabora�orJas TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21081554 RcptNo: 1
Logged by: Christina N.Jager 8/25/2021 10:05:00 AM
Completed By: Christina N.Jager 8/25/2021 5:26:00 PM
Reviewed By: Jennifer Woolf 8/26/2021 10:40:57 AM (...710‘.-0.?1' )771'4,aAal'i•-
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Loa In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no,notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: I Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18.Additional remarks:
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 2.4 Good Not Present
Page 37 of 37

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NC0088111
Monitoring Period: From 01/01/2I To 12/31/21
Pathogen Reduction(40 CFR 503.32/I5A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
It.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt.(1)Fecal Density AIt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter pie Analytical
PERMIT DOES NOT REQUIRE Je Technique
Fecal
Coliform MONITORING FOR PATHOGEN
& VECTOR ATTRACTION
REDUCTION
Salmonella
bacteria(in a111413-,uiy
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable)
(Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT(please check the appropriate statement)
"[certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/1.5A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Herring,Executive Director NRWASA
Preparer N e and Title rint) Land Applier Name and Title(if applicable)(type or print)
Sig re of Prepare* � at Signature of Land Applier(if applicable) Date

SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: Neuse Regional WASA
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (tons/acre) Applied
NC-LN-X6-1 5.8 0.4 0.5 Mar-21
NC-LN-X6-2 5.8 0.4 0.5 Mar-21
NC-LN-X6-3 5.8 0.4 0.5 Mar-21
NC-LN-X6-4 5.8 0.4 0.5 Mar-21
NC-LN-X5-2 5.6 0.4 0.0 n/a
NC-LN-X5-3 5.9 0 0.0 n/a
*Lime will be applied in Spring 2021

SECTION 7

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