WQ0001989_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0001989
Applicant/Permittee Roanoke Rapids Sanitary District
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Drew Matthews
Email Address* Phone Number*
[e-mail] 2528839301
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001989
Has Current Existing permit number
Applicant/Permittee Address* PO Box 308,Roanoke Rapids,NC 27870
Facility Name* Roanoke Rapids Sanitary District Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 RRSD Annual Report.pdf 20.27MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature
Submission Date 2/24/2022

ROANOKE RAPIDS
SANITARY DISTRICT
2021 LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0001989
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
February 24, 2022
SOIL PLUS

SOIL PLUS
February 24,2022
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Re: 2021 LAND APPLICATION ANNUAL REPORT
Roanoke Rapids Sanitary District"Class B" Program
NC Permit No.: WQ0001989
Soil Plus Project No. 202105.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Roanoke Rapids Sanitary District on
behalf of Granville Farms, Inc. Soil Plus compiled this report using data gathered during
the compliance year. This data includes (1) certification form, (2) residual sampling, (3)
field loading calculations, (4) pathogen and vector attraction reduction documentation, (5)
standard soil fertility nutrient analysis.
The Roanoke Rapids Sanitary District conducted application events on permitted fields in
Halifax, Northampton, and Warren counties during 2021. A total of 2,759,061 Gallons or
537.25 Dry Tons of permitted residual biosolids were land applied to permitted fields.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Roanoke Rapids Sanitary District (252-537-9137) for
further assistance.
Respectfully,
*12 ,() NA$1,0/J2
Drew Matthews, Soil Plus
cc: R. Danieley Brown,Roanoke Rapids Sanitary District
Steven Ellis,Roanoke Rapids Sanitary District
Jason Smith, Granville Farms
P.O.Box 1396
Oxford,NC 27565
[phone]
[e-mail]
www.soilplus.net

ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
Roanoke Rapids FORM
Sanitary District Analytical Data
TCLP
2021 Land
Application of
Residual Biosolids FIELD LOADING
Report SUMMARY FORM
WQ0001989
Roanoke Rapids, ANNUAL PATHOGEN &
C VECTOR ATTRACTION
REDUCTION FORM
Fecal Coliform Data
Lime Stabilization Data
SOIL SAMPLES

Roanoke Rapids Sanitary District
2021 Class B Annual Report
WQ Permit# WQ0001989
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0001989 Roanoke Rapids Sanitary District Granville Farms,Inc. Halifax [phone]
Year: 2021
Land application of residuals as allowed by the permit occurred during the past calendar year?If No,skip Part A,and Part Yes No
B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the El a
residuals were handled.
Part A-Residuals Application Summary:
Total number of application fields in the permit: 69
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 537.25
Total number of acres utilizes for land application during the year: 207.18
Part B-Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No -
Including but not limited to items 1-13 below)issued by the Division of Water Quality ❑� ❑i1
If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1.Only residuals approved for this permit were applied to the permitted sites
2.Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6
3.Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory
results are attached
4.Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached
5.All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7.All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities
8.All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503 regulated facilities)
9.All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior authorization was
received from the Division of Water Quality
10.No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11.Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified in the permit.
12.No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13.All buffer requirements as specified by the permit were maintained during each application of residuals.
Part C-Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and
complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations."
R.Danieley Brown,CEO •�"Z
Permittee Name and Title(type or print): Signature of Pe ittee ate
SuAd 2/24/22
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26)
Friday,January 28,2022 •

Source Summary Report
WWTP VolumeApplied Total
RRSD WWTP 2,759,061 537.25
Total 2,759,061 537.25
Friday,January 28,2022 Page 1 of 1

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Roanoke Rapids Sanitary District
2021 Class B Annual Report
WQ Permit# WQ0001989
Residual Sampling Summary Form
Field Loading Calculations
2021 Analytical
2021 TCLP

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v AGMAN FIELD LOADING ESTIMATES
Facility RRSD WW P
Sampling Date 1/11/2021
Solids 3.52
Mineralization Rate 0.3
Gallons per DT 6,812.73
pH 12.27
Sodium Absorpotion 0.16 <5.0 Safe 5.0-10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN(mg/Kg) 41,000 lbs./1,000 gal 12.04 Potassium lbs./1,000 gal 0.88
Ammonia Nitrogen(mg/Kg) 1,300.00 lbs./1,000 gal 0.38 Phosphorus lbs./1,000 gal 5.58
Nitrate-Nitrite(mg/Kg) 114.00 lbs./1,000 gal 0.03 Calcium lbs./1,000 gal 52.84
PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.97
PAN(mg/Kg) 12,674 lbs./1,000 gal 3.72 Manganese lbs./1,000 gal 0.21
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 13,324 lbs./1,000 gal 3.91 Molybdenum lbs./1,000 gal 0.00
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits(mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 8.90 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 0.76 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 300.00 Copper lbs./1,000 gal 0.09
300 840 Lead(mg/Kg) 25.00 Lead lbs./1,000 gal 0.01
17 57 Mercury(mg/Kg) 0.56 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 20.00 Nickel lbs./1,000 gal 0.01
100 100 Selenium(mg/Kg) 4.70 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 620.00 Zinc lbs./1,000 gal 0.18
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 41,000 12,674 25.35 28,326 41,000 13,324 26.65 27,676 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 28,326 4,249 8.50 24,077 27,676 4,151 8.30 23,525 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 24,077 1,806 3.61 22,271 23,525 1,764 3.53 21,760 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 22,271 835 1.67 21,436 21,760 816 1.63 20,944 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 21,436 402 0.80 21,034 20,944 393 0.79 20,552 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 19,966 39.93 Total 20,448 40.90

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Roanoke Rapids VWVTP
Lot Number:WA12001
Date Completed:01/26/2021
—
01/26/2021 1:31 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,_0
, MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WA12001
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low% solids the initial amount of sample -001 was 3 times the standard procedure amount per
PM's request. The LOQ has been adjusted accordingly.
Nitrite
The following sample was diluted due to the nature of the sample matrix: WA12001-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WA12001-001
Description:Roanoke Rapids WWTP Matrix:Solid
Date Sampled:01/11/2021 1045 % Solids: 3.52 01/13/2021 0135
Date Received:01/12/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 01/13/2021 0135 LR1 79363
1 350.1 (Ammonia-N )350.1 1 01/13/2021 1400 CAG2 79167
1 (Nitrate-N )9056A 5 01/13/2021 1730 AMR 79439
1 (Nitrite-N )9056A 5 01/13/2021 1730 AMR 79441
2 (Phosphorus)365.1 25 01/22/2021 1055 DMA 01/20/2021 1747 80124
1 (Soil pH meas)9045D 1 01/12/2021 2346 AAB 79201
1 351.4 (TKN)351.2 2 01/21/2021 1306 DMA 01/20/2021 1747 80122
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 3.52 % 1
Ammonia-N (gas diffusion) 350.1 1300 28 15 mg/kg 1
Nitrate-N (soluble) 9056A 100 71 14 mg/kg 1
Nitrite-N (soluble) 9056A ND 28 14 mg/kg 1
Phosphorus 7723-14-0 365.1 19000 3600 710 mg/kg 2
Soil pH measured in water @ 19.7° C 9045D 11.7 su 1
TKN 351.2 41000 1400 1400 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/21/2021 1209 JAB2 01/20/2021 1110 79538
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.3 0.56 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/13/2021 1858 KSH2 01/13/2021 0648 79212
2 3050B 6010D 1 01/14/2021 1419 KSH2 01/13/2021 0648 79212
3 3050B 6010D 2 01/14/2021 1400 KSH2 01/13/2021 0648 79212
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 15000 190 71 mg/kg 1
Arsenic 7440-38-2 6010D 8.9 7.1 2.4 mg/kg 1
Cadmium 7440-43-9 6010D 0.76 J 2.4 0.60 mg/kg 2
Calcium 7440-70-2 6010D 180000 4700 590 mg/kg 3
Chromium 7440-47-3 6010D 93 4.7 1.2 mg/kg 2
Copper 7440-50-8 6010D 300 4.7 2.1 mg/kg 1
Iron 7439-89-6 6010D 130000 47 22 mg/kg 2
Lead 7439-92-1 6010D 25 4.7 2.1 mg/kg 1
Magnesium 7439-95-4 6010D 3300 2400 300 mg/kg 2
Manganese 7439-96-5 6010D 700 7.1 2.8 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WA12001-001
Description:Roanoke Rapids WWTP Matrix:Solid
Date Sampled:01/11/2021 1045 % Solids: 3.52 01/13/2021 0135
Date Received:01/12/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/13/2021 1858 KSH2 01/13/2021 0648 79212
2 3050B 6010D 1 01/14/2021 1419 KSH2 01/13/2021 0648 79212
3 3050B 6010D 2 01/14/2021 1400 KSH2 01/13/2021 0648 79212
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Molybdenum 7439-98-7 6010D 15 J 19 4.7 mg/kg 1
Nickel 7440-02-0 6010D 20 19 5.0 mg/kg 1
Potassium 7440-09-7 6010D 3000 2400 300 mg/kg 2
Selenium 7782-49-2 6010D 4.7 J 9.5 3.8 mg/kg 1
Sodium 7440-23-5 6010D 1300 J 2400 300 mg/kg 2
Zinc 7440-66-6 6010D 620 24 5.9 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Ch ckllst ISRC)(MEo018C-1S) Rev]sed:W29l2424
rirce�ltialyka't'. issuin Authority_Pace ENV 'IN COI. Page 1 of I
Sample Receipt Checklist (SRC)
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171 ';s C No LIt*€A 4. is fife commercial courier's picking slip attached to leis form'?
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yes INa 19, Was co]lzetiun date&.time listed ten uIl sae a le confiners?
ye4 Chu 10. Did all container label info rmatian(ID,date,tirne)tree with the COO/
p Yes Jj No Were tests ro he T,cr:orrocri]lsted on the CDC? — �-
12. Did all samples s,rF:ve.in the proper containers roc each rat ana:or in good ccndilion
I Er fcs ❑No (unbroken, lids on,etc,)?
••• If Yes l u `I3.V4'oa adequate s3inpic volume available" .
7Yes ❑N cy' 14. 'ere all samp leer .eived within'A the hnldirru time or 4$hours,wt iohe•ier coin first?
CI Yes Le I No 11-Were any sprtlples containers ln:ssinglexcess(cirnlc Ioit)samples Not listed on COO?
16,For VOA and RSK-175 samples,uie bubb[c:pr- ut `pG i}ti"(1/4"or ernes in diemrter)
n'f4s I]?�]a ❑J NA in any of the VOAvials7
"I'm I—I No 'DNA 17. Were all DRO/metals,'nu trim!.samples--ec.ei,red at a QH of<2
Yes Ii No L7A 1S. Wets aJ. LiniciO sant lee rcccireti at a pH> l2_and aullida sainiles received at a H>97
I
�!, 'Gs. 0„IL, r] lA l'1.Were all applicable NH ?cyani phuind.G25,f,'C083 (<E} m.5g.eI,j samples fete of
reside:l chlortre7 171
2[1-Wero•.i hrxi
ient remarkyuests(Le_req'icsted;liFnions,MSIMSE)designations,etc...)
You No correctly transcribed from the CCIX into the comn_4nl scxtion in LTMS?
Yes El No .2l-Was the uote.number..isted,i on th;.container lab d?If yes, mile i# r. _± ,
Svruple Preservation CMust be cornple Jed for any man pies)incorrectly prcacr+'ed or with h eadspace.) 1
SArrole(s) N.n were received iuoorfectly pr,etierved and wore adjusted apgordingly 1
In sample rrax.ivills with E'"A nil.,of circle one! H2501,IThJD3,HCI,NaCH usirg.SR§I KA -
Tim The of prcnter,ratiau NA . ;f more Ian one preservative is I1a LI11j,please n rtl a in the c:ranrrre3,t- oataw. J
aimplc t) uA were received with bubbles>6 mm in diemoLor.
Sarirtless) v_a wereticeived with TRC>0.5 t;reIL(lf#19 isiw)arid'veie
atlausled accordinEly in sample receaviug with 5odiu n lhiosulfate(Na,53Clt)with Shealy '1J:
-
-
SR b¢trcode labels uppl ied by. t''t H _ — Date; O:i tY�42i
_
Comments: — -
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

v AGMAN FIELD LOADING ESTIMATES
Facility RRSD WW P
Sampling Date 4/5/2021
Solids 3.87
Mineralization Rate 0.3
Gallons per DT 6,196.59
pH 11.7
Sodium Absorpotion 0.14 <5.0 Safe 5.0-10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN(mg/Kg) 42,000 lbs./1,000 gal 13.56 Potassium lbs./1,000 gal 1.00
Ammonia Nitrogen(mg/Kg) 1,100.00 lbs./1,000 gal 0.36 Phosphorus lbs./1,000 gal 10.01
Nitrate-Nitrite(mg/Kg) 80.00 lbs./1,000 gal 0.03 Calcium lbs./1,000 gal 67.78
PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 1.16
PAN(mg/Kg) 12,900 lbs./1,000 gal 4.16 Manganese lbs./1,000 gal 0.24
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 13,450 lbs./1,000 gal 4.34 Molybdenum lbs./1,000 gal 0.01
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits(mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 9.60 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 1.00 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 370.00 Copper lbs./1,000 gal 0.12
300 840 Lead(mg/Kg) 36.00 Lead lbs./1,000 gal 0.01
17 57 Mercury(mg/Kg) 0.47 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 32.00 Nickel lbs./1,000 gal 0.01
100 100 Selenium(mg/Kg) 7.00 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 820.00 Zinc lbs./1,000 gal 0.26
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 42,000 12,900 25.80 29,100 42,000 13,450 26.90 28,550 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 29,100 4,365 8.73 24,735 28,550 4,283 8.57 24,268 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 24,735 1,855 3.71 22,880 24,268 1,820 3.64 22,447 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 22,880 858 1.72 22,022 22,447 842 1.68 21,606 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 22,022 413 0.83 21,609 21,606 405 0.81 21,201 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 20,391 40.78 Total 20,799 41.60

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Roanoke Rapids VWVTP
Lot Number:WD08038
Date Completed:04/19/2021
04/28/2021 10:00 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCR,_0
, MILD
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD08038
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample-001 has been digested using three grams of sample. The LOQs have
been changed to reflect the additional disestion mass.
Inorganic Non-Metals
The following sample was diluted due to the nature of the sample matrix: WD08038-001. The LOQ has
been elevated to reflect the dilution.
Subcontracted Analysis
The analysis of CCE has been performed by Waypoint. This data has been ammended to this report
beginning on page 8.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 12

Client:Synagro Laboratory ID:WD08038-001
Description:Roanoke Rapids WWTP Matrix: Solid
Date Sampled:04/05/2021 1000 %Solids: 3.87 04/09/2021 0019
Date Received:04/08/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 04/09/2021 0019 MOM 88462
1 350.1 (Ammonia-N)350.1 1 04/13/2021 1434 KFE 88830
1 (Nitrate-N)9056A 5 04/13/2021 1242 AMR 88909
1 (Nitrite-N)9056A 5 04/13/2021 1242 AMR 88910
2 (Phosphorus)365.1 25 04/13/2021 1544 DMA 04/10/2021 1429 88601
1 (Soil pH meas)9045D 1 04/09/2021 1257 NBW 88539
1 351.4 (TKN)351.2 2 04/15/2021 1006 DMA 04/10/2021 1429 88598
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 3.87 % 1
Ammonia-N (gas diffusion) 350.1 1100 26 13 mg/kg 1
Nitrate-N (soluble) 9056A 67 65 13 mg/kg 1
Nitrite-N (soluble) 9056A ND 26 13 mg/kg 1
Phosphorus 7723-14-0 365.1 31000 3200 650 mg/kg 2
Soil pH measured in water @ 20.3° C 9045D 11.2 su 1
TKN 351.2 42000 1300 1300 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/14/2021 1517 CMS2 04/14/2021 1203 88719
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.0 0.47 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/10/2021 1424 KSH2 04/09/2021 0845 88488
3 3050B 6010D 2 04/12/2021 1145 KSH2 04/09/2021 0845 88488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 23000 170 64 mg/kg 1
Arsenic 7440-38-2 6010D 9.6 6.4 2.1 mg/kg 1
Cadmium 7440-43-9 6010D 1.0 J 2.1 0.54 mg/kg 1
Calcium 7440-70-2 6010D 210000 4300 540 mg/kg 3
Chromium 7440-47-3 6010D 100 4.3 1.1 mg/kg 1
Copper 7440-50-8 6010D 370 4.3 1.9 mg/kg 1
Iron 7439-89-6 6010D 170000 86 39 mg/kg 3
Lead 7439-92-1 6010D 36 8.6 3.9 mg/kg 3
Magnesium 7439-95-4 6010D 3600 2100 270 mg/kg 1
Manganese 7439-96-5 6010D 740 6.4 2.5 mg/kg 1
Molybdenum 7439-98-7 6010D 17 17 4.3 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 12

Client:Synagro Laboratory ID:WD08038-001
Description:Roanoke Rapids WWTP Matrix: Solid
Date Sampled:04/05/2021 1000 %Solids: 3.87 04/09/2021 0019
Date Received:04/08/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/10/2021 1424 KSH2 04/09/2021 0845 88488
3 3050B 6010D 2 04/12/2021 1145 KSH2 04/09/2021 0845 88488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 32 17 4.5 mg/kg 1
Potassium 7440-09-7 6010D 3100 2100 270 mg/kg 1
Selenium 7782-49-2 6010D ND 17 7.0 mg/kg 3
Sodium 7440-23-5 6010D 1200 J 2100 270 mg/kg 1
Zinc 7440-66-6 6010D 820 21 5.4 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 12

PACE ANALYTICAL SERVICES, LLC
Samples Receipt checklist(SRC}(NtE0018C-3.5 Revised:9/29/2020
asArthigical. Issuing Authority:Pace 1;NU-Wan Page 1 of 1
Sample Receipt Checklist (SRC)
Client. _ Cooler Lnspeetcd ldat = • 1 _? L41 Lot o:
Moans of race E; Paw ❑Client. O'UF5 Fe EEK Other: _
Yc Nol 1.Micro custody mils mesa!".on the cooler?
Yes ❑Alo A 2_licustody seals were presetyt,.wertit 1hcy inrstcl rind nnh1 ktar?
pH Strip ID_ ,` Chlorin°Strip 11]: R.J Tested by:._....
lair!ten eiatui-e upon i'ceipt f.cirrcctnrfj lemPerrt,rre Mean reteipt Solid Snap-Cup 1D: i— 4 YI_3
Method:❑Teztipenarura nick Bigainst.13dtles IR Glyn in: . c lit{inn Coax..ism r aeutir: � C
'Method of coolant: L'J wet ice © ice l'acka Tyr Tee [ Nur�c _
Yea ]No' [=J MA 3. If fern perat�ury Amy cuulex cxcseeticd 6,0°C.vas.Pi ojecl Manager Notit iecl?
PM was-Nodliied by phone?email I face-to-face(circle one)-
ts ❑No DNA 4. Is the commercial courier's packing s lip attached to this form?
yes LI Nip: , Were proper custody pi educes(rolinqu[skull-received)followed?
Is ❑No' 6. I4'ere sample 11-is listed on Om
Yes ❑No 7. Were sample Bps listed on all sample containers? _
❑N l. Was collection,dare&time listed on the COCF
i
y o; iffesi
sl L'No 19, Was collection date&time listed on all sample containers?
4-(pi7'y.,to No h Io.Did all container Zabel intarmatian([I},data_time)agree wish the CDC'?J"~
Li Yes 'Nil I I_ Were tests to be performed listed ort the CDC? --
I. Yes �Na 12.Did all samples arrive iu cite proper'.6utt.6-outliners fur each test and/or ire.good 4urltlitiuir
, 5 ((unbroken.,!Ws uu etc_)?
I Ye,1 L_I 3,Jn I 113, Was adequate sample volume available?
led �� 14. Were all samples received w ithin §the holding time or 48]tours,whichever eutrrr [Ina
Yes, L Nu 1.5_ Were any samples caitei.ners inissinv'excess{clam]c one)yen pies Not limed tan COC':
❑ r 116, For VOA rind RSIC-175 eunplas,wtxc;bubble:pr nt>''pea-size"{!."or 6rnm in diameter)
t❑ cs; No I:.,.IfN+ in any of the VOA vials?
Q Ycs U No I.'.J NA 17.WL ra aril DRpfmth iyfnutricut samples received at a pit of C
r 2?
❑Yes-U.Flo 1]'NA I S.Wert a]]cyanide samples raceiwrl at a pit> 12 and sulfide samples received at a p11°9?
19. Were all applicable NUITICNIcyattid 1pfienoil 5.11606,3 (=0,5rn if)stunplcs frco of
❑Yes ❑Ala 17rNA residual c•
hlorine'
E Yes ❑No Lim+A 20_ Were client remarlcsirequests(le_requested dilution%MS,IvtSi] lL i natl0rls.c{c,„)
correctly transcribed from the CDC into the r.omment acc.•hut, in 1.,1M 2
I Yes u ND 21.Was the quote number listed or:the container lobe'?if es,Quote i
.5i mole Preservation (Must be completed for aq sample(2)i:scor melly prescrvad er With hcadspacc.)
:Sample(5) wore re awed incorrectly preserved and were adjusted accordingly
rv,mp[e reoci"it,g with mL of eirclo one:If2SO4,HNO3,HC],1'aOHi using S1tJ _
Time of pres+avation . If more than one preservative is needed,please note iri time euiiiurersts below.
Sattxple(5) _—.werc received with bubbles G nun in diameter.
Samples(s) were received with'l'RC>0.5 ntg/L(If 09 is no)and were
adjusted accordingly in sample riving with sodium Ihiosu 1 Ft1e{Nat ID;S203)with Shealy I
SR h_arcnrle tihels applied hy: nate,
` I
Comments: L,�yy,, . r " k,, � )h eel ( In -t h1e r-
•
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 12

v AGMAN FIELD LOADING ESTIMATES
Facility RRSD WW P
Sampling Date 7/14/2021
Solids 5.73
Mineralization Rate 0.3
Gallons per DT 4,185.13
pH 11.47
Sodium Absorpotion 0.16 <5.0 Safe 5.0-10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN(mg/Kg) 28,400 lbs./1,000 gal 13.57 Potassium lbs./1,000 gal 1.16
Ammonia Nitrogen(mg/Kg) 90.90 lbs./1,000 gal 0.04 Phosphorus lbs./1,000 gal 13.00
Nitrate-Nitrite(mg/Kg) 175.00 lbs./1,000 gal 0.08 Calcium lbs./1,000 gal 80.76
PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.98
PAN(mg/Kg) 8,713 lbs./1,000 gal 4.16 Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 8,759 lbs./1,000 gal 4.19 Molybdenum lbs./1,000 gal 0.00
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits(mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 0.87 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 0.55 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 232.00 Copper lbs./1,000 gal 0.11
300 840 Lead(mg/Kg) 11.10 Lead lbs./1,000 gal 0.01
17 57 Mercury(mg/Kg) 0.22 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 5.50 Nickel lbs./1,000 gal 0.00
100 100 Selenium(mg/Kg) 0.87 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 492.00 Zinc lbs./1,000 gal 0.24
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 28,400 8,713 17.43 19,687 28,400 8,759 17.52 19,641 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 19,687 2,953 5.91 16,734 19,641 2,946 5.89 16,695 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 16,734 1,255 2.51 15,479 16,695 1,252 2.50 15,443 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 15,479 580 1.16 14,898 15,443 579 1.16 14,864 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 14,898 279 0.56 14,619 14,864 279 0.56 14,585 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 13,781 27.56 Total 13,815 27.63

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Ai,
Revised Report: 9/30/2021
Contact: Drew Matthews Report Date: 8/9/2021
Client: Soil Plus
P.O.Box 1396 Project: Roanoke Rapids 3rd Q
Oxford,NC 27565 Date Sample Rcvd: 7/14/2021
Meritech Work Order# 071421184 Sample: RR 071421 Grab 7/14/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 5.73 % 7/15/21 0-100 % SM 2540B
Ammonia, Nitrogen 90.9 mg/kg 8/6/21 10 mg/kg EPA 350.1
TKN 28,400 mg/kg 7/22/21 20 mg/kg EPA 351.1
Nitrate/Nitrite, Nitrogen <175 mg/kg 7/16/21 175 mg/kg EPA 353.2
Aluminum,total 10200 mg/kg 7/26/21 2.50 mg/kg EPA 200.7
Arsenic,total <0.873 mg/kg 7/26/21 0.873 mg/kg EPA 200.7
Cadmium,total 0.550 mg/kg 7/26/21 0.250 mg/kg EPA 200.7
Calcium,total 169,000 mg/kg 7/26/21 10.0 mg/kg EPA 200.7
Copper,total 232 mg/kg 7/26/21 1.00 mg/kg EPA 200.7
Chromium, total 53.2 mg/kg 7/26/21 1.00 mg/kg EPA 200.7
Lead,total 11.1 mg/kg 7/26/21 2.20 mg/kg EPA 200.7
Magnesium,total 2,060 mg/kg 7/26/21 10.0 mg/kg EPA 200.7
Mercury,total 0.218 mg/kg 7/20/21 0.02 mg/kg EPA 245.1
Molybdenum,total 6.14 mg/kg 7/26/21 0.250 mg/kg EPA 200.7
Nickel,total 5.50 mg/kg 7/26/21 2.0 mg/kg EPA 200.7
Phosphorus,total 27,200 mg/kg 7/26/21 2.00 mg/kg EPA 200.7
Potassium,total 2,430 mg/kg 7/26/21 20.0 mg/kg EPA 200.7
Selenium,total <0.873 mg/kg 7/26/21 0.873 mg/kg EPA 200.7
Sodium, total 1,010 mg/kg 7/26/21 20.0 mg/kg EPA 200.7
Zinc,total 492 mg/kg 7/26/21 0.500 mg/kg EPA 200.7
pH 11.4 S.U. 7/15/21 1.0 - 14.0 S.U. SM 4500-HB
I hereby certify that I have reviewed and approve these data. ,,Atnand_a Panceo k ,
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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v AGMAN FIELD LOADING ESTIMATES
Facility RRSD WW P
Sampling Date 11/23/2021
Solids 5.09
Mineralization Rate 0.3
Gallons per DT 4,711.36
pH 12.16
Sodium Absorpotion 0.13 <5.0 Safe 5.0-10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN(mg/Kg) 14,500 lbs./1,000 gal 6.16 Potassium lbs./1,000 gal 0.80
Ammonia Nitrogen(mg/Kg) 1,060.00 lbs./1,000 gal 0.45 Phosphorus lbs./1,000 gal 7.39
Nitrate-Nitrite(mg/Kg) 196.00 lbs./1,000 gal 0.08 Calcium lbs./1,000 gal 60.28
PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.82
PAN(mg/Kg) 4,758 lbs./1,000 gal 2.02 Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 5,288 lbs./1,000 gal 2.24 Molybdenum lbs./1,000 gal 0.00
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits(mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 0.98 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 0.22 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 206.00 Copper lbs./1,000 gal 0.09
300 840 Lead(mg/Kg) 10.50 Lead lbs./1,000 gal 0.00
17 57 Mercury(mg/Kg) 0.41 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 4.83 Nickel lbs./1,000 gal 0.00
100 100 Selenium(mg/Kg) 0.98 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 413.00 Zinc lbs./1,000 gal 0.18
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 14,500 4,758 9.52 9,742 14,500 5,288 10.58 9,212 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 9,742 1,461 2.92 8,281 9,212 1,382 2.76 7,830 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 8,281 621 1.24 7,660 7,830 587 1.17 7,243 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 7,660 287 0.57 7,372 7,243 272 0.54 6,971 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 7,372 138 0.28 7,234 6,971 131 0.26 6,841 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 7,266 14.53 Total 7,659 15.32

Meritech, Inc.
Environmental Laboratory
filk
Laboratory Certification No. 165
140
Contact: Drew Matthews Report Date: 12/8/2021
Client: Soil Plus
P.O. Box 1396 Project: Roanoke Rapids 4th Q
Oxford, NC 27565 Date Sample Rcvd: 11/23/2021
Meritech Work Order# 112321173 Sample: RRSD Grab 11/23/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 5.09 % 11/23/21 0-100 % SM 2540B
Ammonia, Nitrogen 1,060 mg/kg 12/1/21 10 mg/kg EPA 350.1
TKN 14,500 mg/kg 11/30/21 20 mg/kg EPA 351.1
Nitrate/Nitrite, Nitrogen <196 mg/kg 11/24/21 196 mg/kg EPA 353.2
Aluminum,total 3300 mg/kg 12/6/21 2.50 mg/kg EPA 200.7
Arsenic,total <0.982 mg/kg 12/6/21 0.982 mg/kg EPA 200.7
Cadmium,total 0.222 mg/kg 12/6/21 0.100 mg/kg EPA 200.7
Calcium,total 142,000 mg/kg 12/6/21 10.0 mg/kg EPA 200.7
Chromium,total 62.3 mg/kg 12/6/21 0.250 mg/kg EPA 200.7
Copper,total 206 mg/kg 12/6/21 1.00 mg/kg EPA 200.7
Lead,total 10.5 mg/kg 12/6/21 2.25 mg/kg EPA 200.7
Magnesium,total 1,920 mg/kg 12/6/21 10.0 mg/kg EPA 200.7
Mercury,total 0.413 mg/kg 11/30/21 0.02 mg/kg EPA 245.1
Molybdenum,total 9.41 mg/kg 12/6/21 0.250 mg/kg EPA 200.7
Nickel,total 4.83 mg/kg 12/6/21 0.500 mg/kg EPA 200.7
Phosphorus,total 17,400 mg/kg 12/6/21 1.00 mg/kg EPA 200.7
Potassium,total 1,890 mg/kg 12/6/21 20.0 mg/kg EPA 200.7
Selenium,total <0.982 mg/kg 12/6/21 0.982 mg/kg EPA 200.7
Sodium,total 780 mg/kg 12/6/21 20.0 mg/kg EPA 200.7
Zinc,total 413 mg/kg 12/6/21 0.500 mg/kg EPA 200.7
pH 12.4 S.U. 12/7/21 1.0 - 14.0 S.U. SM 4500-HB
I hereby certify that I have reviewed and approve these data. Cbtt
Laboratory Re entative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

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a i' Summit Environmental Technologies,Inc.
inIrg 3310 Win St.
ENVIRONMENTAL TECHNO LOCiES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boraIi rlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
January 25,2021
Chris Wynne
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL:
FAX:
RE: Roanoke Rapids W W TP
Dear Chris Wynne: Order No.: 21010523
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/12/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
/.....?-74424f4 177��
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 35

SUMMIT
Summit Environmental Technologies,Inc.imil*;;:ra Case Narrative
331 Ohio Wm St.
mium
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21010523rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 1/25/2021
CLIENT: Synagro
Project: Roanoke Rapids WWTP
WorkOrder Narrative:
21010523: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21010523-001a CYANIDE,REACTIVES(9014): Below detection level data was reported based on
Total CN data.
21010523-001a TCLP-SVOC-CPest(8081B): High recovery(ies) in the CCV indicate high bias. Data
deemed acceptable as no target analytes were observed in the field sample(s).
Analytical Sequence QC Notes:
CCV VOC-MSTR_NPW(8260): CCV exhibits high recovery for Vinyl chloride. All reported samples
are ND for this analyte.
LCS-47331 TCLP-VOC-MSTR TCLP(8260): Possible high bias for Vinyl chloride due to high
recovery in CCV. Associated samples are N.D. for this analyte.
Original
Page 2 of 35

S
Mt'T Summit Environmental Technologies,Inc.3310 Win St. Case Narrative
ENVIRONMENTAL TECliN❑LOGIES.INC. Cuyahoga Falls,Ohio 44223 WO#: 21010523
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 1/25/2021
CLIENT: Synagro
Project: Roanoke Rapids WWTP
LCS-47347 TCLP-SVOC-CPest(8081B): Possible high bias for Heptachlor and Methoxychlor due to
high recoveries in bracketing CCV's.
MB-47347 TCLP-SVOC-CPest(8081B): High recovery(ies) in the CCV indicate high bias. Data
deemed acceptable as no target analytes were observed in the field sample(s).
Original
Page 3 of 35

•
17 S
Mm iT Summit Environmental Techno3310Wlogies,Ins
Qualifiers and Acronyms
EkiwllxsStJM@N1'nLTecriw❑LOG{ES.rFtI; Cuyahoga Falls,Ohio 442 WO#: 21010523
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 1/25/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 35

S t�' Summit Environmental Technologies,Inc. Workorder
3310 Win St.
1.7 ENVIRONMENTAL TECHNQI. oiEs,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 21010523
Website:http://www.settek.com 25-Jan-21
CLIENT: Synagro
Project: Roanoke Rapids WWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
21010523-001 Roanoke Rapids WWTP 1/11/2021 10:30:00 AM 1/12/2021 11:05:00 AM Sludge
Page 5 of 35

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S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENb1R01JMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010523
Website:http://www.settek.com Date Reported: 1/25/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/11/2021 10:30:00 AM
Lab ID: 21010523-001A
Project: Roanoke Rapids WWTP
Client Sample ID Roanoke Rapids WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200 mg/L 1 1/20/2021 12:22:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 1/19/2021 2:44:28 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 1/19/2021 2:44:28 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/19/2021 2:44:28 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 1/19/2021 2:44:28 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 1/19/2021 2:44:28 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 1/19/2021 2:44:28 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 1/19/2021 2:44:28 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 1/20/2021 1:03:00 AM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 1/20/2021 1:03:00 AM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 1/20/2021 1:03:00 AM
2,4-Dinitrotoluene ND 0.100 mg/L 2 1/20/2021 1:03:00 AM
Cresols,Total ND 10.0 mg/L 2 1/20/2021 1:03:00 AM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 1/20/2021 1:03:00 AM
Hexachlorobenzene ND 0.100 mg/L 2 1/20/2021 1:03:00 AM
Hexachloroethane ND 0.200 mg/L 2 1/20/2021 1:03:00 AM
Nitrobenzene ND 0.200 mg/L 2 1/20/2021 1:03:00 AM
Pentachlorophenol ND 0.500 mg/L 2 1/20/2021 1:03:00 AM
Pyridine ND 0.500 mg/L 2 1/20/2021 1:03:00 AM
Surr:2-Fluorophenol 83.8 10-157 %Rec 2 1/20/2021 1:03:00 AM
Surr: Phenol-d6 94.2 10-169 %Rec 2 1/20/2021 1:03:00 AM
Surr: Nitrobenzene-d5 83.3 32.1 -130 %Rec 2 1/20/2021 1:03:00 AM
Surr:2,4,6-Tribromophenol 115 45.4-166 %Rec 2 1/20/2021 1:03:00 AM
Surr:2-Fluorobiphenyl 71.8 35.7-130 %Rec 2 1/20/2021 1:03:00 AM
Surr:p-Terphenyl-d14 110 74.7-145 %Rec 2 1/20/2021 1:03:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 35

S
it• Summit Environmental Technologies,Inc. Analytical Report
mu 3310 Win St.
ENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010523
Website:http://www.settek.com Date Reported: 1/25/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/11/2021 10:30:00 AM
Lab ID: 21010523-001A
Project: Roanoke Rapids WWTP
Client Sample ID Roanoke Rapids WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 1/19/2021 10:02:00 PM
Toxaphene ND 0.0500 mg/L 1 1/19/2021 10:02:00 PM
Endrin ND 0.00250 mg/L 1 1/19/2021 10:02:00 PM
gamma-BHC ND 0.00250 mg/L 1 1/19/2021 10:02:00 PM
Heptachlor ND 0.00250 QC+ mg/L 1 1/19/2021 10:02:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 1/19/2021 10:02:00 PM
Methoxychlor ND 0.00250 QC+ mg/L 1 1/19/2021 10:02:00 PM
Surr:TCMX 62.6 10-119 %Rec 1 1/19/2021 10:02:00 PM
Surr: DCB 74.0 10-119 %Rec 1 1/19/2021 10:02:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321 SW1311M Analyst: JPG
2,4-D ND 0.500 mg/L 50 1/23/2021 11:15:00 AM
2,4,5-TP ND 0.500 mg/L 50 1/23/2021 11:15:00 AM
Surr:2,4-Dichlorophenylacetic aci 105 70-130 %Rec 50 1/23/2021 11:15:00 AM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
1,2-Dichloroethane ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
MEK ND 5.00 mg/L 50 1/19/2021 3:54:00 AM
Benzene ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
Carbon tetrachloride ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
Chlorobenzene ND 2.50 mg/L 50 1/19/2021 3:54:00 AM
Chloroform ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
Tetrachloroethene ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
Trichloroethene ND 0.250 mg/L 50 1/19/2021 3:54:00 AM
Vinyl chloride ND 0.100 QC+ mg/L 50 1/19/2021 3:54:00 AM
Surr:4-Bromofluorobenzene 97.8 70-130 %Rec 50 1/19/2021 3:54:00 AM
Surr: Dibromofluoromethane 96.3 70-130 %Rec 50 1/19/2021 3:54:00 AM
Surr:Toluene-d8 98.8 70-130 %Rec 50 1/19/2021 3:54:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 35

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECHNOLOGIES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010523
Website:http://www.settek.com Date Reported: 1/25/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/11/2021 10:30:00 AM
Lab ID: 21010523-001A
Project: Roanoke Rapids WWTP
Client Sample ID Roanoke Rapids WWTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: JAP
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.893 mg/Kg 1 1/17/2021 4:20:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: KMW
Ignitability nonflammable mm/sec 1 1/18/2021 10:34:05 AM
RCI SW9045D Analyst: WK
PH (SW9045D)
pH 11.0 s.u.@20.1C 1 1/13/2021 12:15:13 PM
RCI SW9034 Analyst: JAP
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/19/2021
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 9 of 35

S
MM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MI ENVIRONMENTAL TECHNaLOGES,INCCuyahoga Falls,Ohio 44223 J Y
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 21010523
Website:http://www.settek.com 25-Jan-21
Client: Synagro State: NW
Project: Roanoke Rapids WWTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010523-001A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive N
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 10 of 35

S UMM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7tes Report
EN ENWIRONM@NtAL TECHN❑LociEs,i Cuyahoga Falls,Ohio 44223 Analytes
rral}'tiicaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21010523
Website:http://www.settek.com 25-Jan-21
Client: Synagro State: NW
Project: Roanoke Rapids WWTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010523-001A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 11 of 35

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Page 34 of 35

iw SUMMIT
Summit Environmental Technologies,Inc.
OM 3310 Win St.
Arm' OtJMENtALTtiriNOL4Ga S.lFr Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
yt�caf iabora�orJas TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21010523 RcptNo: 1
Logged by: Jesseca E.Westfall 1/12/2021 11:05:00 AM
Completed By: Jesseca E.Westfall 1/12/2021 4:45:53 PM
Reviewed By: Jennifer Woolf 1/12/2021 4:48:02 PM (...710‘.-0.?1' )771'4,aAal'i•-
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no,notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: I Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18.Additional remarks:
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 5.5 Good Not Present
Page 35 of 35

Roanoke Rapids Sanitary District
2021 Class B Annual Report
WQ Permit# WQ0001989
Land Application Field Summary Form

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Roanoke Rapids Sanitary District
2021 Class B Annual Report
WQ Permit# WQ0001989
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Data
Lime Stabilization Data

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 01/01/2021 to 03/31/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 1
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 5,657 10,640.4 23,704 0 Quarterly Grab Samples
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt. 1 (VS reduction)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
Ei requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danielcy Brown,CEO Jason Smith,VP
Preparer Name and Title (type or print) Land Applier Name and Title(if applicable)(type or print)
4 22S r
IL
1 2/24/22
Signature of Prepa r* Da a Signature of Land Applier(if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)
Monday,February 7,2022

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 01/01/2021 to 03/31/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 2
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry
Weight)
Analytical Technique
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt.6 (Alk.Stabilization)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
Ei requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danieley Brown,CEO Jason Smith,VP
Preparer Na and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
202.- C4-41411C
2/24/22
Signature of Prepa r* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102(26)

DIGESTER VSR & 1 MGT FECAL ANALYSIS
1ST. QTR. PRIM DIG. VSR DIG. #2 2ND QTR. PRIM, DIG. VSR DIG. #2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
1/7/21 TS TS TS 73 45 69.7 8735 4/8/21 JP JP JP 88 46 88 60000
1/14/21 JP JP JP 70 45 64.9 23704 4/15/21 BW BW BW 74 46 70 2475
1/21/21 BW BW BW 76 48 70.8 9351 4/22/21 DM DM DM 72 48 64 >243011
2/4/21 TS TS TS 78 45 76.9 7376 4/29/21 HH HH HH 71 47 63 1687
2/11/21 JP JP JP 84 49 81.6 5657 5/6/21 JP JP JP 73 47 67 30948
2/17/21 BW BW BW 70 48 60.4 11579 5/13/21 BW BW BW 72 47 65 3937
2/25/21 DM DM DM 75 47 70.4 16508 5/20/21 DM DM DM 76 47 71 31112
G.M. 10640.4 G.M. 9914.281
MIN. 70 45 60.4 5657 MIN. 71 46 63.0 1687
MAX. 84 49 81.6 23704 MAX. 88 48 88.0 _ 60000
AVER. 75.1 46.7 71 11844.3 AVER. 75.1 46.9 70.8 21693.17
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
1/11/2021 10:45AM 10:50AM 4/5/2021 10:22AM 10:30AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 14.4 °C 12.27 IW 17.8 °C 11.7
I
3RD. QTR. PRIM,I DIG. VSR DIG. #2 4TH. QTR. PRIMI DIG. VSR DIG. #2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
G.M. #NUM! G.M. #NUM!
MIN. 0 0 0 0 MIN. 0 0 0 0
MAX. 0 0 0 0 MAX. 0 0 0 0
AVER. #### #### #### #DIV/0! AVER. #### #### #### #DIV/0!
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
1°C I°c
% VSR CALCULATION: PRIM. %VS--DIG.%VS X 100
MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100)
DIG. #2 FECAL MUST BE BELOW 2,000,000
7 SAMPLES (MINIMUM) REQUIRED PER QUARTER

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 04/01/2021 to 06/30/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 1
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 1,687 9,914.281 60,000 0 Quarterly Grab Samples
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt. 1 (VS reduction)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
0 requirement in 15A NCAC 02T .1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danielcy Brown,CEO Jason Smith,VP
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
ejglit 1 2/24/22
Signature of Pre arer* Date Signature of Land Applier(if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)
Monday,February 7,2022

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 04/01/2021 to 06/30/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 2
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Lime Stabilization
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry
Weight)
Analytical Technique
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt.6 (Alk.Stabilization)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danicicy Brown,CF.() Jason Smith,VP
Preparer Name and Title (type or print) Land Applier Name and Title(if applicable)(type or print)
22 `+, £414L 2/24/22
Signature of Prep er* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)

DIGESTER VSR & 1 MGT FECAL ANALYSIS
1ST. QTR. PRIM DIG. VSR DIG. #2 2ND QTR. PRIM, DIG. VSR DIG. #2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
1/7/21 TS TS TS 73 45 69.7 8735 4/8/21 JP JP JP 88 46 88 60000
1/14/21 JP JP JP 70 45 64.9 23704 4/15/21 BW BW BW 74 46 70 2475
1/21/21 BW BW BW 76 48 70.8 9351 4/22/21 DM DM DM 72 48 64 >243011
2/4/21 TS TS TS 78 45 76.9 7376 4/29/21 HH HH HH 71 47 63 1687
2/11/21 JP JP JP 84 49 81.6 5657 5/6/21 JP JP JP 73 47 67 30948
2/17/21 BW BW BW 70 48 60.4 11579 5/13/21 BW BW BW 72 47 65 3937
2/25/21 DM DM DM 75 47 70.4 16508 5/20/21 DM DM DM 76 47 71 31112
G.M. 10640.4 G.M. 9914.281
MIN. 70 45 60.4 5657 MIN. 71 46 63.0 1687
MAX. 84 49 81.6 23704 MAX. 88 48 88.0 _ 60000
AVER. 75.1 46.7 71 11844.3 AVER. 75.1 46.9 70.8 21693.17
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
1/11/2021 10:45AM 10:50AM 4/5/2021 10:22AM 10:30AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 14.4 °C 12.27 IW 17.8 °C 11.7
I
3RD. QTR. PRIM,I DIG. VSR DIG. #2 4TH. QTR. PRIMI DIG. VSR DIG. #2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
G.M. #NUM! G.M. #NUM!
MIN. 0 0 0 0 MIN. 0 0 0 0
MAX. 0 0 0 0 MAX. 0 0 0 0
AVER. #### #### #### #DIV/0! AVER. #### #### #### #DIV/0!
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
1°C I°c
% VSR CALCULATION: PRIM. %VS--DIG.%VS X 100
MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100)
DIG. #2 FECAL MUST BE BELOW 2,000,000
7 SAMPLES (MINIMUM) REQUIRED PER QUARTER

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 07/01/2021 to 09/30/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 1
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 827 2,004.18 4,339 0 Quarterly Grab Samples
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt. 1 (VS reduction)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danielcy Brown,CEO Jason Smith,VP
Preparer me an Title (type or print) Land Applier Name and Title (if applicable)(type or print)
2/24/22
Signature of Pre arer* ate Signature of Land Applier(if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)
Monday,February 7,2022

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: W(20001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 07/01/2021 to 09/30/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A" only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 2
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry
Weight)
Analytical Technique
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt.6 Alk.Stabilization)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danicicy Brown,CEO Jason Smith,VP
Preparer me and Title (type or print) Land Applier Name and Title(if applicable)(type or print)
- 2 22 1 r""` 2/24/22
Signature of Pre arer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)

DIGESTER VSR & 1MGT FECAL ANALYSIS
1ST. QTR. PRIM DIG. VSR DIG. #2 2ND QTR. PRIM. DIG. VSR DIG.#2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
1/7/21 TS TS TS 73 45 69.7 8735 418121 JP JP JP 88 46 88 60000
1114121 JP JP JP 70 45 64.9 23704 4/15/21 BW BW BW 74 46 70 2475
1/21121 BW BW BW 76 48 70.8 9351 4/22/21 DM DM DM 72 48 64 >243011
2/4121 TS TS TS 78 45 76.9 7376 4/29/21 HH HH HH 71 47 63 1687
2/11/21 JP JP JP 84 49 81.6 5657 5/6/21 JP JP JP 73 47 67 30948
2117121 BW BW BW 70 48 60.4 11579 5/13/21 BW BW BW 72 47 65 3937
2125121 DM DM DM 75 47 70.4 16508 5/20/21 DM DM DM 76 47 71 31112
G.M. 10640.4 G.M. 9914.281
MIN. 70 45 60.41 5657 MIN. 71 46 63.0 1687
MAX. 84 49 81.61 23704 MAX. 88 48 88.01 60000
AVER. 75.1 46.7 71 11844.3 AVER. 75.1 46.9 70.8 21693.17
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
1111/2021 10:45AM 10:50AM 4/5/2021 10:22AM 10:30AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 14.4 I°C 12.27 IW 17.8 1°C 11.7
3RD. QTR. PRIM, DIG. VSR DIG. #2 4TH. QTR. PRIM DIG. VSR DIG. #2
DATE P D F %VS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
7/1/21 JP JP JP 85 49 83 1431!
7/8/21 BW BW BW 79 49 74.4 4339
7/15/21 DM,DM,DM 85 49 83 1819
7/22/21 HH HH HH 79 49 74 827
7/29/21 JP JP JP 78 50 72 4180
8/5/21 BW BW BW 79 50 73 2299
8/12121 DM,DM,DM, 66 491 51 1447
I
G.M. 2004.18 G.M. #NUM!
MIN. 66 49 51 827 MIN. 0 0 0 0
MAX. 85 50 83 4339 MAX. 0 0 0 0
AVER. 78.7 49.3 73.7 2334.57 AVER. #### #### ####j #DIVIO!
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
7/14/2021 9:16AM 9:25AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 24 NC 11:47 ,°C
% VSR CALCULATION: PRIM. %VS--DIG.%VS X 100
MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100)
DIG. #2 FECAL MUST BE BELOW 2,000,000
7 SAMPLES (MINIMUM) REQUIRED PER QUARTER

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WWTP NPDES Number: NC0024201
Monitoring Period: 10/01/2021 to 12/31/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 1
If applicable to alternative performed("Class B" only)indicate"Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 1,022 2,481.35 7,793 0 Quarterly Grab Samples
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt. 1 (VS reduction)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
It.Danicley Brown,CEO Jason Smith,VP
Preparer e and Title (type or print) Land Applier Name and Title(if applicable)(type or print)
4/2Z 40044411' 2/24/22
Signature of Prep rer* Date Signature of Land Applier(if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)
Monday,February 7,2022

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989
WWTP Name: RRSD WW"I'P NPDES Number: NC0024201
Monitoring Period: 10/01/2021 to 12/31/2021
Pathogen Reduction(15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B"Alternative: Alternative 2
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry
Weight)
Analytical Technique
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt.6(Alk.Stabilization)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
R.Danicley Brown,CEO Jason Smith,VP
Preparer me a d Title (type or print) Land Applier Name and Title(if applicable)(type or print)
2 Z"Z jltalecL 2/24/22
Signature of Pr parer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)

DIGESTER VSR & 1 MGT FECAL ANALYSIS
1ST. QTR. PRIM, DIG. VSR, DIG.#2 2ND QTR. PRIM. DIG. VSR DIG.#2
DATE P D F %VS %VS % _ FEC. CT. DATE P D F %VS %VS % FEC. CT.
1/7/21 TS TS TS 73 45 69.7 8735 4/8/21 JP JP JP 88 46 88 60000
1/14/21 JP JP JP 70 45 64.9 _ 23704 4/15/21 Bw BW BW 74 46 70 2475
1/21/21 BW BW BW 76 48 70.8 9351 4/22/21 DM DM DM 72 48 64 >243011
2/4/21 TS TS TS 78' 45 76.9 7376 4/29/21 HH HH HH 71 47 63 1687
2/11/21 JP JP JP 84 49 81.6 5657 5/6/21 JP JP JP 73 47 67 30948
2/17/21 BW BW BW 70 48 60.4 11579 5/13/21 BW BW Bw 72 47 65 3937
2/25/21 DM DM DM 75 47 70.4 16508 5/20/21 DM DM DM 76 47 71 31112
-i
G.M. 10640.4 G.M. 9914.281
MIN. 70 45 60.4 5657 MIN. 71 46 63.0 1687
MAX. 84 49 81.6 23704 MAX. 88 48 88.01 60000
AVER. 75.1 46.7, 71 11844.3 AVER. 75.1 46.9 70.81 21693.17
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
1/11/2021 10:45AM 10:50AM 4/5/2021 10:22AM 10:30AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 14.4 I°C 12.27 IW 17.8 °C 11.7
3RD. QTR. PRIM. DIG. VSR ' DIG. #2 4TH. QTR. PRIM DIG. VSR DIG.#2
DATE P D F `/oVS %VS % FEC. CT. DATE P D F %VS %VS % FEC. CT.
7/1/21 JP JP JP 85 49 83 1431 10/7/21 DM DM DM 82 50 78 1617
7/8/21 BW BW BW 79 49 74.4 4339 10/14/21 Ts Ts TS 78 51 70.6 3368
7/15/21 DM,DM,DM 85 49 83 1819 10/21/21 JP JP JP 79 49 74.4 7793
7/22/21 HH HH HH 79 49 74 827 10/28/21 TS TS TS 74 51 63.4 2717
7/29/21 JP JP JP 78 50 72 4180 11/4/21 DM DM DM 76 50 68.4 1022
8/5/21 BW BW BW 79 50 73 2299 11/18/21 TS TS TS 72 52 57.8 1034
8/12/21 DM,DM,DM, 66 49 51 1447 12/2/21 DM DM DM 86 52 82.3 4753
G.M. 2004.18 G.M. 2481.35
MIN. 66 49 51 827 MIN. 72 49 57.81 v 1022
MAX. 85 50 831 4339 MAX. 86 52 82.3 7793
AVER. 78.7 49.3 73.7 2334.57 AVER. 78.1 50.7 71.2 3186.286
QUARTERLY MGT pH SAMPLE QUARTERLY MGT pH SAMPLE
DATE SAMPLE TIME ANALYSIS TIME DATE SAMPLE TIME ANALYSIS TIME
7/14/2021 9:16AM 9:25AM 11/23/2021 9:28AM 9:36AM
INITIALS SAMPLE TEMP ADJUSTED pH INITIALS SAMPLE TEMP ADJUSTED pH
TS 24 1°C 11:47 TS 19.5 °C 12.16 _
% VSR CALCULATION: PRIM. %VS--DIG.%VS X 100
MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100)
DIG. #2 FECAL MUST BE BELOW 2,000,000
7 SAMPLES (MINIMUM) REQUIRED PER QUARTER

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Roanoke Rapids Sanitary District
2021 Class B Annual Report
WQ Permit# WQ0001989
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