Loading...
HomeMy WebLinkAboutWQ0005809_Residual Annual Report 2021_20220223 rl Non-Discharge Branch Upload/Submittal Form NORTH CAROLINA Environment N Qmilelr Version 2-Revised June 23,2020 Initial Review Reviewer Thornburg,Nathaniel D Is this submittal an application?(Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number(IR)* WQ0005809 Applicant/Permittee Colonial Pipeline Company Email Notifications Does this need review by the hydrogeologist?* 0 Yes OO No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Maribeth Hughes Email Address* Phone Number* MHughes@colpipe.com 704-458-3993 Project Information Application/Document Type* New(Fee Required) Modification-Minor Modification-Major(Fee Required) Renewal Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1, Required) NDAR-2 Annual Report Residual Annual Report Additional Information Change of Ownership Other We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High-Rate Infiltration Other Wastewater Reclaimed Water Closed-Loop Recycle Residuals Single-Family Residence Wastewater Other Irrigation Permit Number:* WQ0005809 Has Current Existing permit number Applicant/Permittee Address* 411 Galimore Dairy Road Greensboro NC 27409 Facility Name* Colonial Pipeline Company Class B Residuals Program Please provide comments/notes on your current submittal below. At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form,Engineering Plans,Specifications,Calculations,Etc.) 2021 Annual Report.pdf 11.9MB Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre-review until the fee(if required)has been received by the Non- Discharge Branch.Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order(as specified by the application). Mail payment to: NCDEQ—Division of Water Resources Attn:Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Signature Submission Date 2/23/2022 ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0005809 County: Guilford Year: 2021 Facility Name (as shown on permit): Colonial Pipeline Company Land Application Operator: Faron D. Leigh Phone: 336-669-7903 Land application of residual solids as allowed by the permit occurred during the past calendar year? ❑ Yes p No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied,please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 1-Site, 4-Fields Total number of fields land application occurred duringthe year: 0 PP � Total amount of dry tons applied during the year for all application sites: Total number of acres land application occurred during the year: Part B: Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Resources.p Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Brian L. Smith `Z I Z 3 I 22 Permittee Name and Title(type or print) ature of nittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) DENR FORM ACF (5/2003) A/vt Aref ,�1e ANNUAL DISTRIBUTION AND MARKETING!SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: WQ0005809 FACILITY NAME: Colonial Pipeline Company PHONE: 336-669-7903 COUNTY: Guilford OPERATOR: Faron D,. Leigh FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? ❑ Yes ❑ No No If No skip parts A, B, C and certify form below Part A*: Part B*: Sources s include NPDES #if Volume (dry tons) Recipient Information Month ( Amendment/ Volume (dry applicable) _Bulking Agent Residual In Product Out Name(s) tons) Intended use(s) January February March April May June July August September October November December Totals: Annual (dry tons): 0 0 0 0 Amendment(s) used: Bulking Agent(s) used: * If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year with all conditions of the permit(including but not limited to items 1-3 below) issued by the Division of Water Resources. LI Yes LI No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF(11/2005) • /Ye c4h1e ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0005809 Laboratory: 1) AES, Inc. and Pace Analytical Facility Name: Colonial Pipeline Company 2) NPDES # or N/A 3) WQ#: 4) WWTP Name: N/A 5) Residual Analysis Data Sample or Composite Date Percent Solids _ Arsenic Cadmium Chromium Copper Lead e Mercury Molybdenum Nickel Selenium Zinc ya Total Phosphorus TKN Ammonia-Nitrogen_ Nitrate and Nitrite "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied (Annual): 0 Permit#: WQ0005809 Cation Exchange Capacity(non 503 only): 14 Operator: Owner: Acres Used: 0 Acres Permitted: 1.55 Site#: 1 Field#: 1A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample 1 2 4 5 7 8 9 10 11 12 or Com- posite Date %Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium_ _ Zinc Total Phos- phorus k Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 4 5 6 7 8 9 10 11 12 mid 2. po o. Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0 0 0 0 0 0 0 0 0 0 0 0 0 Chroiniurr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0 0 0 0 0 0 0 0 0 0 0 0 0 _ Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0 0 0 0 0 0 0 0 0 0 0 0 0 v Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0 0 0 0 0 0 0 0 0 0 0 0 0 Total Phos- 0 0 0 0 0 0 0 0 0 0 0 0 0 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" A plie Qa7`or3—,•Z Signature of Land Ap Date *See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (512003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied(Annual): 0 Permit#: WQ0005809 Cation Exchange Capacity (non 503 only): 9.93 Operator: Owner: Acres Used: 0 Acres Permitted: 1.32 Site#: 1 Field#: 1B Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent#): Sample 1 2 3 4 j 7 8 9 10 11 12 or Com- posite Date % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 1 2 4 5 6 7 8 9 10 11 12 y m H rn v O Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0 0 0 0 0 0 0 0 0 0 0 0 0 Chromium 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0 0 0 0 0 0 0 0 0 0 0 0 0 Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0 0 0 0 0 0 0 0 0 0 0 0 0 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0 0 0 0 0 0 0 0 0 0 0 0 0 Total Phos- 0 0 0 0 0 0 0 0 0 0 0 0 0 phorus "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" J ..Zr..Zr . #4;( Off-.0 3--el, OZ Signature of Land Applier Date *See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM° Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied(Annual): 0 Permit#: WQ0005 809 Cation Exchange Capacity(non 503 only): 11.5 Operator: Owner: Acres Used: 0 Acres Permitted: 1.8 Site#: 1 Field#: IC Residual Analysis Data (Heavy Metals and Total Phosphorus use nig/kg, % Solids use Raw Percent#): Sample 1 2 14- 5 6 j 7 8J 9 10 11 12 or Com- posite Date %Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc _ Total Phos- phorus _ Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 4 , 5 6� 7i $j 9i 10 11 12 t7I1 ' o. a d 0 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0 0 0 0 0 0 0 0 0 0 0 0 0 Chromium 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0 0 0 0 0 0 0 0 0 0 0 0 0 v Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum v Nickel 0 0 0 0 0 0 0 0 0 0 0 0 0 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0 0 0 0 0 0 0 0 0 0 0 0 0 Total Phos- 0 0 0 0 0 0 0 0 0 0 0 0 0 phorus "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date *See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF(5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied (Annual): 0 Permit#: WQ0005809 Cation Exchange Capacity(non 503 only): 11.83 Operator: Owner: Acres Used: 0 Acres Permitted: 0.97 Site#: 1 Field#: 1D Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample 1 2 3 4 5 6 7 8 9 10 11 12 or Com- posite Date %Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ,..{ y 1 2 3 4 5 6 7 8 9 10 11 12 o z Y ` y 0 O � Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0 0 0 0 0 0 0 0 0 0 0 0 0 Chrornimr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0 0 0 0 0 0 0 0 0 0 0 0 0 Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0 0 0 0 0 0 0 0 0 0 0 0 0 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0 0 0 0 0 0 0 0 0 0 0 0 0 Total Phos- 0 0 0 0 0 0 0 0 0 0 0 0 0 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" d .r. '( 42�f:?z Signature of La Applier Date *See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit#: WQ0005809 Annual Dry Tons Applied: #DIV/0! Owner: Colonial Pipeline Company Operator: Faron D. Leigh Cation Exchange Capacity (non 503): 14 Site#: 1 Field#: IA Acres Utilized: 0 Acres Permitted: 1.55 :::: Specify Site Must Select Gal. Totals % Cond. Inches AppIi- Vola- Miner Ammo- Ni- q°, ' Cu.Yd. Dry Tons Per Residual Sources Precip. cation tili- all- nia- trate Crop 1 or Crop * o Per Solid Dry, TKN PAN 1 PAN 2 2 * Report Acre (Summarize) Past 24 Meth- zation zation Ni- and Q Totals Acre s Wet, Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gal. Moist #DIV/0! #DIV/0! #DIV/0! #DIV/0! 1 #DIV/0! #DIV/0! _ #DIV/0! #DIV/0! _ #DIV/0! #DIV/0! #DIV/0! #DIV/0! 3 #DIV/0! #D1V/0! #DIV/0! #DIV/0! 4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 6 #DIV/0! #DIV/0! #D1V/0! #DIV/0! 7 #DIV/0! #D1V/0! #DIV/0! #DIV/0! 8 _ #DIV/0! #DIV/0! _ #DIV/0! #DIV/0! 9 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 10 #DIVID! #DIV/0! #DIV/0! #DIV/0! 11 #DIV/0! #D1V/0! #DIV/0! #DIV/0! 12 TOTALS: #Nttt##t As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113.351 0 0 42.1497 0 311.572 Prior Years Cumulative lbs/ac 4.072 143.32 113.351 42.1497 311.572 Permitted C. P. L. R.*** 9 250 1000 250 500 .............. Permit PAN Limit 1 st/2nd Crop ::;; .:::,.:. ::»::::::::::<:: .. .. .. .......... ..... . .... t::::. "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,. ..�_ ", yL, �a - 3 p7A *Application Method: S - Surface,IN-Injection, INC -Incorporation SignatureSignature Applier Date **Volatilization Rate: Surface-0.5, Injection/Incorporation- 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The ESE and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit#: WQ0005809 Annual Dry Tons Applied: #DIV/01 Owner: Colonial Pipeline Company Operator: Faron D. Leigh Cation Exchange Capacity (non 503): 9.93 Site#: 1 Field#: 1B Acres Utilized: 0 Acres Permitted: 1.32 ::: Specify Site Must Select Ni- ,.., JI Gal. Totals % Cond. Inches Appli- Vola- Miner- Ammo- * Tons Per Residual Sources cation tili- aui- nia- trate Crop 1 or Crop * „ d Cu.Yd. Dry Precip. TKN PAN I PAN 2 w o Per Sa1id Dry, 2 Report Acre (Summarize) Past 24 Meth- zation zation Ni- and A Totals Acre s Wet, * Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gal. Moist #DIV/0! _ #DIV/0! #DIV/0! #DIV/0! 1 #DIV/0! #DIV/O! #DIV/0! #DIV/0! 2 #DIV/0! #DIV/0! #DIV/0! #DIV/0!_ 3 #DIV/0! #DIV/0! #DIV/0! #DIVI0! 4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 6 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 7 #DIV/01 #DIV/01 #DIV/0! #DIV/0! 8 #DIV/0! #DIV/01 #DIV/0! #DIV/0! 9 #DIV/0! #DIV/0! #DIV/0! #DIV/01 10 #DIVI0! #DIV/0! #D1V/0! #DIV/0! 11 #DIV/0! #DIV/0! #DEV/0! #DIV/0! 12 TOTALS: #;### As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual lbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113.351 0 0 42.1497 0 311.572 :: •;•:: ::::::::.:. Prior Years Cumulative lbs/ac 4.072_ 143.32 113.351 42.1497 311.572 Permitted C. P. L. R.*** 9 250 1000 250 500 1 t 2nd Crop Permit PAN Limit s/ I I • . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." tti -g- I,. _ 16,2 073- ,,4_A *Application Method: S - Surface, IN-Injection, INC - Incorporation Signature of Latta Applier Date **Volatilization Rate: Surface- 0.5,Iniection/Incorporation- 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit#: WQ0005809 Annual Dry Tons Applied: #DIV/0! Owner: Colonial Pipeline Company Operator: Faron D. Leigh Cation Exchange Capacity (non 503): 11.5 Site#: 1 Field#: 1C Acres Utilized: 0 Acres Permitted: 1.8 Specify site Must Select Gal. Totals % Cond. Inches Appli- Vola- Miner- Ammo- Ni- * d Cu.Yd. Dry Precip. Crop 1 or Crop ;,; Tons Per Residual Sources cation tili- ali- nia- trate o Per Solid Dry, TKN PAN 1 PAN 2 Report Acre (Summarize) Past 24 Meth- zation zation Ni- and 2 Q Totals Acre s Wet, Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gal. Moist #DIV/0! #DIV/0! #DIV/0! #DIV/0! 1 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! 4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 6 #DIV/0! #D1V/01 _ #DIV/0! #DIV/0! 7 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 8 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 9 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 10 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 11 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 12 TOTALS: 1444# As Cd Cr Cu Pb Hg Mo Ni Se Zia P PAN 1 PAN 2 Lime Applied Annual lbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113.351 0 0 42.1497 0 311.572 ' >:: ::::::::: Prior Years Cumulative lbs/ac 4.072 143.32 113.351 42.1497 311.572 `::::..::::.: Permitted C. P. L. R.*** 9 250 1000 250 500 .. ..... .. Permit PAN Limit l st/2nd Crop .... .: ....... ....... . I "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." pbVti• - eV',& .-,pT *Application Method: S- Surface, IN-Injection,INC - Incorporation Signature of Las her Date **Volatilization Rate: Surface- 0.5, Injection/Incorporation- 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie.FSF row#1 to MFLSF column#1. DENR FORM FSF(5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit#: WQ0005809 Annual Dry Tons Applied: #DIV/0! Owner: Colonial Pipeline Company Operator: Faron D. Leigh Cation Exchange Capacity(non 503): 11.83 Site#: 1 Field#: 1D Acres Utilized: 0 Acres Permitted: 0.97 Specify Site Must Select �. Gal. Totals % Cond. Inches Appli- Vola- Miner- Ammo- Ni * - oCrop 1 or Crop * �, b Cu.Yd. Dry Tons Per Residual Sources Precip. cation tili- ali- I nia- trate PAN 1 PAN 2 o Per Solid Dry, 2 * Q Report Acre s Acre (Summarize) Wet, Past 24 Meth- zation zation Ni- and Totals * Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gal. Moist _ #DIV/0! #DIV/0! #DIV/0! #DIVIO! 1 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/O! 4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 6 #DIV/0! #DIV/O! #DIV/O! #DIV/0! 7 #DIV/0! #DIV/0! #DIV/0! #DIV/0! S I #DIV/O! #DIV/0! #DIV/0! #DIV/0! 9 #DIV/O! #DIV/0! #DIVIO! #DIV/0! 10 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 11 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 12 TOTALS: g As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual ibs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac , Current Cumulative lbs/ac 0 _4.072 0 143.32 113.351 0 0 42.1497 0 311.572 ::::::::::::::.: Prior Years Cumulative lbs/ac 4.072 143.32 113.351 42.1497 311.572 :::::::::: Permitted C. P. L. R.*** 9 250 1000 250 5O0 Permit PAN Limit 1 stl2nd Crop .... ......... .. .. "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." O. 0;2 � z *Application Method: S- Surface, IN-Injection, INC - Incorporation Signature of Land Aglier Date **Volatilization Rate: Surface- 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to he entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1. DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Ale f /4//� J,'r g J /La Permit Number: WWTP Name: NPDES Number: Monitoring Period: From To Pathogen Reduction (40 CFR 503.32) -Please indicate level achieved and alternative performed: Class A: Alternative 1❑ Alternative 2 ❑ Alternative 3 ❑ .,,,,,, Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":Compost ❑ Heat Drying❑ Heat Treatment 0 Thermophil is ❑ Beta Ray Cl Gamma Ray❑ Pasteurization ❑ Class B: Alternative 10 Alternative 2 ❑ Alternative 3 ❑ If applicable to alternative performed(Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion❑ I If applicable to alternative performed (CIass A or Class B) complete the following monitoring data: Number of Frequency Analytical Allowable Level Pathogen Density Sample Parameter ExceTech- in Sludge Minimum Geo. MeanMVlaximum Units dencese- of Type niuue Analysis niaue 2 x 10 to the 6th power MEN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFTJ per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vector Attraction Reduction (40 CFR 503,33) - Please indicate option performed: Option 1 ❑ 'Option 2 ❑ Option 3 ❑ Option 4 0 Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 0 Option 10 ❑ No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title(type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier(if applicable) Date DENR FORM RF (5/2003) GW-59A COMPLIANCE REPORT FORM P 't ; 4i11 I�-:...M (Submit one each monitoring period with Uii'-59 for .1 �i I!' Y Enter date monitoring results were due. 0,7-1d ) Will this monitoring report(GW--599 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES",list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information, 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO identification plate,area overgrown,etc.)?If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? S NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is"YES"list the affected wells individually with constituent(s)and concentrations) exceeding standards in the space provided below: II Al -G0 'r Aqd a 4' e5{ lass w• 5 For the constituents identified in question 4 above,have standards been exceeded previously for the YES NO same constituent(s)in the same well(s)in the last two years? If the answer to question 5 is `NO", skip to section 8. If the answer to question 5 is"YES",list in the space provided below, each well with constituent(s) exceeding standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years). /4 GV-J /� ./% x'-, Neu- a?40,Z0.. 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES N If the answer is "YES",a groundwater quality problem may be occurring. CONTACT THE REGIONAL ' OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is"NO", monitoring wells may be improperly located;contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is"YES", describe those actions in the space provided below. If the answer to question 7 is "NO", v reautred to determine the impact the waste disposal system is having at the review and compliance bo.undaries surrogpdine this facility, Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties, 8 The person completing this portion(GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required walls to the address provided at the top of the current GW-59 form. 1 hereby acknowledge that the above information was evaluated and the information submitted in this report(Compliance Report GW-59A) is true and complete the best of my knowledge. 1 - f • q/Z-�12 Sig e of Pormittee(or Authorized Agent) Date — GW-59A l21fi2003 SUBMIT FORM ON fi ar �'�s�.�,� k �' .`,", YELLOW PAPFJ3 ONLY N s • ,, ��PAI R,iTf4! NY�OF� [�tY�f RO h,4EN044,1.4A �JiESti3�1 R a s;$Si k f ,, ., ; ,.: , • Mail original ,� , . R ��� ,�''��,C� • GROUNDWATER QUALITY MONITORING: and I copy to: �° �� 8, L4S t YICE,,FlJ�lERI �c. 7�9916 7 , ( 9�733-3221 Gera COMPLIANCE.-REPORT.FORM • Pno i,s • FACILITY INFORMATION please Print Clearly;or Type •PERMIT Number- .• • Facility Nae: Colonial Pipeline.Com any • NonDischarge ation..Date '.06-30-2022 V m . PermitName(if different) • NPDES Other • Facility,Address; 411:Gallimore Dairy'RoadTYPE OF•PERMITTED OPERATED:. I N BEING MONITORED ,. Greensboro'' NC. 274179 County Guilford ❑ Lagoon O Remediatron Infiltration Gallery {c lyn (shre) Itl) ❑ Spray Field: • . ❑Remediatlon D Leigh • Telephone#:336-669-7903. ❑ Rotary Distributor. ®Land Applicatio Contact Person Faron g n.of Sludge . WellLocation/Site Name:Downgradient No:of wells to be sampled: 5 • Water Source Heat Pump ❑.Other: SAMPLING`INFORMATION MW-1 MIN-1 B) Date sample collected �,3� 7^a7/ ` FIELD ANALYSES ' rmtt � .. H WAS WELL ID NUMBER(from Pe ) aC • DRY'at:Well Depth. 21.2fl"ft.: Well Diameter. • 2 in. P ! ti units Temp. • �� time:of •: iµMhos • Depth torWaterLevel. 15 90 •`fit below measuring point • Screened Interval 5 ft • to 20.ft... Spec:Cond. , .: sampling • Measuring Point is • • • 3 ft above land surface Relative M.P.Elevation ft. Odor check' Volume'of water,pumped/bailed before sampling 7 2,5" gallons • Appearance here; . Samples for.rrietals:were collected unfiltered:`®YES ` ❑•N,O and field acidified ®YES • ❑NO' • .. LABORATORY'IN FORMATION Date sample analyzed: ` (7 -%3' 21-1; r K •''/l3_ 2,.2 Laboratory Name: Analytical Environmental Services Certification No. 562 • PARAMETERS NOTE:.Values'should`:reflect;dissolved and:colloidal,•concentrations. COD • mg/I Nitrite(NO2),as N mgll :Pb-Lead �t/f/ • nag/i • . Coliform: MF Fecal • '1100mI Nitrate(NO3):as N ' • /, 93 mgli -Zinc r •0- 5•g Trig/l Coliform: MF Total " /100m1 ; Phosphorus:Total as P mg/l (Note;Use MPN method foxhighlyturhideamples) Orthophosphate mg/I Other(Specify•Compounds and Concentration Units):,.,• Dissolved Solids:Total 5- 7 mg/I Al Aluminum mg/I p (whenanalyzed) units Ba-Barium mg/l H . TOC mgll Ca-Calcium. mg/I Chloride. `• J 11 mgfl Cd-Cadmium ,, .:.:a�:O ' mg/I Arsenic • mg/l Chromium:;Total 4i. (/, mg/I Grease and Oils mgli Cu-Copper mg/1 ORGANICS:(b GC,`GCIMSy I-IPLC)Iron mg/I (Spec Y ATTACH Phenol mg/I Fe•- if test,'and method#. LAB REPORT:) Sulfate • mgll Hg-Mercury.' mg/I Report Attached? ® 'Yes(1);. ❑ No(0)' ;.Specific Conductance p Mhos • K Potassium • mgll VOC:' method#,$260 • Total Ammonia Mg:.-Magnesium mg/I • ' {Ammonia:Nitrogen NHsas N;Ammonia Nitrogen;`Total) _ • - • - method# Mn,_Man anese.. _ . g. mgll,. method# TKN as'N. mgll NI-Nickel mg/4 method# y( P ) VOCs.::. • mg/L. Effluent:Total•VOCs mg/L VOC Removel o For femediation Systerris Only Elttaclt:;Lab Re .orts -.'• Influent Total I certify that,to the hest of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and thatthe laboratory analytical data was produced using approved methods of analysis bye DWQ-certified laborata I am aware that there are si.nificant•enalGes b for sumittin.false information,,i v lations i - -- ncludin.the possibilify of fines and im.risonment fo r knowing ®Brian L. Smtih' Operations Manager '; ` . • — " 4422—) Permittee,for Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) • • (Date) GW-59 Rev:1f2007 . Date: 5-Apr 2i Analytical Environmental Services,Inc Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/202I 12:45:00 PM Lab ID: 2103D24-001 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchiB Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW503013) 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 312400 I 03/22/2021 14:32 CM 1,i,1-Trichloro ethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,1,2-Triehloroethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,1-Dichloroethane BRL 0,50 ug/L 312400 1 03/22/2021 14:32 CM 1,1-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,1-Dichloropropene BRL , 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,2,3-Tiichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,2,3-Trichloroptopane BRL 0,50 ug/L 312400 1 03/22/2021 14:32 CM 1,2,4-Trichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,2,4-Trimethylbenzene BRL 0.50 ug/L 312400 I 03/22/2021 14:32 CM I,2-Dibromo-3-chloropropane BRL 1.0 ug/L 312400 1 03/22/2021 14:32 CM 1,2-Dibromoethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,2-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,2-Dichloroethane BRL 0.50 ug/i, 312400 1 03/22/2021 14:32 CM 1,2-Dichloropropane BRL 0.50 .ug/L 312400 1 03/22/2021 14:32 CM 1,3,5-Trimethylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 1,3-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/202114:32 CM 1,3-Dichloropropane BRL 0,50 ug/L 312400 1 03/22/2021 14:32 CM 1,4-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 2,2-Dichloropropane BRL 0.50 ug/L 312400 I 03/22/2021 14:32 CM 2-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 4-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM 4-Isopropyitoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Benzene BRL 0.50 ug/L 312400 I 03/22/2021 14:32 CM Bromobenzene BRL 0.50 ug/L, 312400 1 03/22/2021 14:32 CM Bromochloromethane BRL 0.50 ug/L 312400 1 03/22/202114:32 CM Bromodichlorornethane BRL 0.50 ug/L 312400 1 03/22/202114:32 CM Bromofonn BRL 1.0 ug/L 312400 I 03/22/2021 14:32 CM Bromomethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Carbon tetrachloride BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Chlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Chloroethane BRL 1.0 ug/L 312400 1 03/22/2021 14:32 CM Chloroform BRL 0.50 ug/L 312400 1 03/22/202114:32 CM Chloromethane BRL 0.50 ug/L 3i2400 1 03/22/2021 14:32 CM cis-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Dibromoehloromethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Dibromomethane BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Dichlorodifluoromethane BRL 0.50 ug/L 312400 I 03/22/202114:32 CM Ethylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Hexachlorobutadiene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Isopropylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Methylene chloride BRL 5.0 eig/L 312400 I 03/22/2021 14:32 CM n-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM n-Propylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Quallilers; • Value exceeds maximum contaminant level E Estimated{value above quantitation range) BRL. Below reporting limit S Spike Recovery outside limits due to matrix Li Holding tittles for preparation or analysis exceeded Nate See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyse detected in the associated method blank < Less than Result value Greater than Result value ] Estimated value detected below Reporting Limit Page 10 of 56 Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 12:45:00 PM Lab ID: 2103D24-001 Matrix: Aqueous Reporting Dilution Analyses Result Qual Units BatcbID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS 8260D (SW5030B) Naphthalene BRL 1.0 ug/L 312400 1 03/22/2021 14:32 CM see-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Styrene BRL 0.50 uglL 312400 1 03/22/2021 14:32 CM tert-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Tetrachloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Toluene BRL 0.50 ug/L 312400 I 03/22/2021 14:32 CM trans-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Trichlaroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:32 CM Trichlorofluoromethane BRL 0,50 ug/L 312400 1 03/22/2021 14:32 CM Vinyl chloride BRL 0.50 uglL 312400 1 03/22/2021 14:32 CM Surr:4-Bromofluorobenzene 94.9 74.9-127 e%REC 312400 1 03/22/2021 14:32 CM Surr:Dibromofluoromethane 102 78.9-121 %REC 312440 1 03/22/2021 14:32 CM Surr:Toluene-d8 93.3 81.5-120 %REC 312400 I 03/22/2021 14:32 CM Total Phosphorus E365.1 (E365.1) Phosphorus,Total(As P) 0,107 0.050 mg/L 312139 1 03/18/2021 13:24 VB Residue,Dissolved(TDS)by SM2540C Residue,Dissolved(TDS) 257 10 mg/L 311771 I 03/15/2021 13:35 NN 4 Nitrogen,Ammonia(as N) E350.1 (E350.1) Nitrogen,Ammonia(As N) BRL 0.200 mg/L 311281 1 03/18/2021 13:25 TL Inorganic Anions by IC EPA 300.0 Chloride 7.30 1.00 mgei- R449606 1 03/13/2021 14:38 lP Nitrogen,Nitrate(As N) 1.43 0.250 H mg/L R449606 1 03/13/2021 14:38 IP Hydrogen Ion(pH)by SM4500H+B pH 6.06 0.0100 H pH Units R449113 1 03/15/2021 1433 CB Fecal Coliform(MF) SM9222D Fecal Coliform,(MF) BRL 1 H Colonies/100 R449461 I 03/17/2021 11:25 TN ml METALS,TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 mg/L 311837 1 03/17/2021 09:27 JM Chromium BRL 0.0100 mg/L 311837 1 03/17/2021 09:27 JM Lead BRL 0.0100 utg/L 311837 1 03/17/202109:27 JM Zinc 0.0258 0.0200 mg/L 311837 1 03/17/2021 09:27 JM Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitatiou range) BRL Below reporting limit S Spike Recovery outside limits duo to matrix H Holding times For preparation or analysis exceeded Harr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation frost the method F Analyte detected in the associated method blank < Less than Result valise > Greater than Result value J Estimated value detected below Reporting Limit Page 11 of 56 SUBMIT.FORM'-ONYELCOW P.4FER ONLY ` : . . .. • .. . f_ RALI'FM50^l.r,RCESy t'R2 :r." { i tp't u 4;4''' Y :, � ':: — T,�MENiT�`'O'F�ENYt1RON,�VIEIVT�giTI�TAJA' �`,'y,� �i, t� _ ,:r, original;1 ISION'O IT`WATI illl'i Tf.'N :" MA ON pC 5 CIUIV T�fk` ki�,� :,H,V4`A .. Mailorr�r • GROUNDWATER QUALITY MONITORING. . • . and 1 copy to: . A*a..:: . �a :. .s, kp w 4 ,:w, r x . • COMPLIANCE REPORT:FORM . ^t�..1.#1, I=RVICE „�r EtcH,r+rczrs ,,istz�4!o q,is19p7aa a w ,1, FACILITY INFORMATION • PleasePreitClearlyorType PERMIT Number: • Expiration.Date 06 30-2022 Facility.Name: ; Colonial Pipeline Company' Non Discharge WQ00058.09 UIC Permit:Name(if'drfferent) NPDES Other Facilixy Address: 411'Gaffrmore Dairy•Road'., • • • TYPE OF PERMITTED OPERATION BEING MONITORED ' `' Greensboro. Erect) NC 27409 County Guilford ❑ Lagoon ❑Remediation Infiltration'Gallery tcayl; (tar ej. iuP) ❑ Spray•Field 0 Remediation. Faroe.D:.Lei- h Telephone#:336-669-7903. ❑ Rotary Distributor Il land Application of Sludge Contact`Person.,: g • , Well Location/Site Nam.e:Downgradlent No of wells to be sampled:5 •❑ Water Source Heat Pump 0 Other. ' SAMPLING INFORMATION If WELL WAS WELL,ID NUMBER'(from Perm,it). MW-2 Date sample collected tf73 i / FIELD ANALYSES: o DRY.at Weil Depth 25.20.ft Well=Diameter 2i,n.. pH;;. /,(� units- Temp if.• 3 C wMhos time of -W ter::Level• : ft below,measurin oint' Screened Interval 1$ft. to ' 23 ft.' Spec Cont.•:.- sampling . Depth.#o a � :'� g p Measuring.Point is 1.75 ft aborie land surface Relative M.P.Elevation ft.. : Odor • check dlbeiled before'sam lin .w gal • • A earance';' 'Volumerofwater pumpe p g����I/ Ions pp " here:;❑ ySamples for metals were collected'.unfiltered..EYES. ❑NaN and field acidified: I�YES ;. ❑NO �,ABO RATO RY'IN FORMATION Date sample analyzed: t ':%y 74- j.it i'7.,A, Laboratory Name Analytical•Environmental Services Certification Na. 562 PARAMETERS ' ,NOTE:..Values shouldreflect dissolved and colloidal concentratsions. . . . . CO D ,mg!! `: Nitrite(NOz)a N m 11 `.Pb Lead ..‹.a,.. a/e ;,mg/I ' Col,iform: ME Fecal ..' " )•100m.1 Nitrate(NO3:).as N 3..:z'- mgll Zn-Zinc i5, � ,Q� mg/l •Coliform:ME Total `100ml Phosphorus.Total as P mg/l (mote: u•se.MPN method fornlyt,iy turbid sampplles) ;.Orthophosphate -.mgh • Other(:Specify Compounds and Concentration Units): Dissolved.Solids:Total /72// mg/I Al-Aluminum .mg/l • pH(when:analyzed) 'units ' Ba Barium mgli TOC m911 Ca Calcium: mg1l • Chloride .3• / mg/i ' Cd-.Cadmium . " •d•ee, _.mg/l Arsenic •mg/I Chromium:Total -c© ,7/0 • mg11 . .Grease and Oils ...• .mg/l Cu Copper mg/I ORGANICS (by GC,:GC/MS,•HPLC) Phenol mg/I Fe-Iron mg/I (Specify test and method# ATTACH LAB REPORT.) Sulfate irig/I •Hg Mercury mg/I Report Attached? • ® Yes(1).: ❑ No(0) Specific Conductance . .'µMhos K Potassium mg/I VOC • method#::8260 : - Total Ammonia 0. .� ... '�. �' mgll Mg`-magnesium '- mgll , method# (Ammonia Nitrogen;NH1as N;Ammonia Nitrogen,Total) _ gane5t3 mgll method# Mn' Man ... TKN as,N mg/l • Ni .Nickel mg/I method# ' ' /L Effluent Total VOC .: ' mg1,L VOC:Removal% For.Remedtatwm.Systems•Only(Attach;'Lab Reports) Influent Total:'VOCs::' mg .. I certify that,to the best of my knowledge belief,the information submitted in this report is true;accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DN1Q-certified laborato I am aware that there are significant+enalties for submitting false information,including the pas ;bfuiv. fines and im.risonment for knowin.violation;. Brian.•L Smi#h J [ ' Opera#ions Manager = � Permittee(or Authorised Agent)'.Name:and Titles Please print or type SignaturorPermittee{or Authorized A4ent)e GW 59 Rev..112007 [Date) • Date: 5-Apr-21 Analytical Environmental Services,Inc Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 12:30:00 PM Lab ID: 2103D24-002 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchiD • Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW5030B) L,1,1,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/202114:53 CM 1,1,1-Trichloroethane BRL 0.50 ug/L 312900 1 03/22/2021 14:53 CM 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 312400 I 03/22/2021 14:53 CM 1,1,2-Tichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,1-Dichloroethane BRI. 0.50 ug/L 312400 I 03/22/2021 14:53 CM 1,1-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,1-Dichloropropene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,2,3-Tiichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,2,3-Trichloropropane BRL 0.50 ugh 312400 1 03/22/2021 14:53 CM 1,2,4-Trichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,2,4-Trimethylbenzene BRL 0.50 ug/L 3i2400 I 03/22/2021 14:53 CM 1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 312400 1 03/22/2021 14:53 CM 1,2-Dibromoethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM l,2-Diehlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,2-Dichloroethane BRL 0,50 ug/L 312400 1 03/22/2021 14:53 CM 1,2-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,3,5-Trimethylbenzene BRL 0.50 ug/L 312400 I 03/22/2021 14:53 CM 1,3-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,3-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 1,4-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 2,2-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 2-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 4-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM 4-Isopropyltoluene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Benzene BRL 0.50 uga, 312400 1 03/22/2021 14:53 CM Bromobenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Bromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Bromodichloromethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Bromoform BRL 1.0 ug/L 312400 1 03/22/202114:53 CM Bromomethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Carbon tetrachloride BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Chlorobenzene BRL 0.50 ug/L 312400 I 03/22/2021 14:53 : CM Chloroethane BRL 1.0 ug/L 312400 I 03/22/2021 14:53 CM Chloroform BRL 0,50 ug/L 312400 1 03/22/2021 14:53 CM Chloromethane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM cis-1,2-Diehloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Dibromochloromethane BRL 0,50 ug/L 312400 1 03/22/2021 14:53 CM • Dibromomethane BRL 0.50 ug/L 312400 1 03/22/202114:53 CM Dichlorodifluorometbane BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Ethylbenzene BRL 0.50 ug/L 312400 1 03/22/202114:53 CM 14exachlorobutadiene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM lsopropylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Methylene chloride BRL 5.0 ug/L 312400 1 03/22/2021 14:53 CM n-l3utylbenzene BRL 0.50 ug/L 312400 I 03/22/2021 14:53 CM n-Propylbenzene BRL 0.50 ug/L 312400 1 03/22/202114:53 CM Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix it Holding times For preparation or analysis exceeded Barr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value 1 Estimated value detected below Reporting Limit Page 12 of 56 • Analytical Environmental Services,Inc Dater 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 12:30:00 PM Lab ID: 2103D24-002 Matrix: Aqueous Reporting Dilution Analyses. Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GCIMS 8260D (SW5030B) Naphthalene BRL 1.0 ug/L 312400 1 03/22/2021 14:53 CM ' sec-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Styrene BRL 0.50 OWL 312400 1 03/22/2021 14:53 CM tert-Butylbenzene BRL 0.50 ug1L 312400 1 03/22/202114:53 CM Tetrachloroethene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM Toluene BRL 0.50 ug/L 312400 1 03/22/2021 14:53 CM trans-1,2-Dichloroethene BRL 0,50 uglL 312400 I 03/22/2021 14:53 CM Trichloroethene BRL 0.50 ug/L 312400 1 03/22/202114:53 CM Trichlorofluorometlaane BRL 0.50 ug/L 312400 1 03/22/202114:53 CM Vinyl chloride BRL 0.50 usiL 312400 1 03/22/2021 14:53 CM Surr:4-Bromofluorobenzene 92.8 '74.9-127 %REC 312400 1 03/22/2021 14:53 CM Suer:Dibromofluoromethane 94,6 78.9-121 %REC 312400 1 03/22/2021 14:53 CM Suer:Toluene-d8 96.8 81.5-120 %REC 312400 I 03/22/2021 14:53 .CM Total Phosphorus E365.1 (E365.1) Phosphorus,Total(As P) 0.105 0.050 mg/L 312139 1 03/18/2021 13:15 VB Residue,Dissolved(TDS)by SM2540C Residue,Dissolved(TDS) 211 10 mg/L 311771 1 03/15/2021 13:35 NN Nitrogen,Ammonia(as N) E350.1 (E350.1) Nitrogen,Ammonia(As N) BRL 0.200 mg/L 311281 1 03/18/2021 13:27 TL Inorganic Anions by IC EPA 300.0 Chloride 43.1 1.00 mglL R449606 1 03/13/2021 14:49 IP Nitrogen,Nitrate(As N) 3.69 0.250 H mg/L R449606 I 03/13/2021 14:49 LP Hydrogen Ion(pH)by SM4500H+B pH 6.50 0.0100 H p11 Units R449113 1 03/15/2021 14:36 CB Fecal Coliform(MF) SM9222D Fecal Coliform,(MF) 5 1 H Colonies/I00 R449461 1 03/17/2021 11:25 TN ml METALS,TOTAL SW6010D (SW3010A) Cadmium 13RL 0.0050 mg/L 311837 1 03/17/2021 09:30 JM Chromium BRL 0.0100 mg/L 311837 1 03/17/202109:30 JM Lead BRL 0.0100 mg/L 311837 1 03/17/2021 09:30 JM Zinc 0.0204 0.0200 mg/L 311837 I 03/17/2021 09:30 JM Quaafers: c Value exceeds maximum contaminant level E Estimated(value above eluantitotion range) BRI. Below reporting limit S Spike Recovery outside limits due to matrix H holding times For preparation or analysis exceeded Narr See case narrative N Analyte notNELAC certified F Analyzed in the lab which is a deviation From the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value l Estimated value detected below Reporting Limit Page 13 of 56 SUBMIT•FORAAON YFL'i`OW PAPER ONLY • AART(uiE- Mail origin al OFEV�fjLZ6OTEN.H.sERN Gyi4�TUIO�yA N''R,�E:mSCEst�NEp GSnoUNT��tsykf�. p4z�,a a�-sr?a�lu.tItrW�.T �GROUND W ATPR QUAL[TXM and copy to: 3Y���4 � . . R-%::.� a�COMPLIANCE.REPORT'FORl1lf • TY INFORMATION e Print Clearl w;T e . Expiration Date: `0 FACILI - Pleas Y YP ;. PE Company RM1T•Number: ,` '.CO,lonral•Pi elirie p y . N -Discharge WQ000580.9 UIC 63p2022 Faculty Name. p Permit Name(if different). NPDES Other rlit.Address. 41.1:GaRrmoreDairy Road TY PE OFPERMITTED OPERATION BEING MONITORED' Fac y, • Greensboro. s e�i) `, N,C. 27409 County Guilford ❑ Lagoon ❑Remediation Infiltration Gallery iry1. tst to}. (zp� ❑'Spray Field:` ❑Rernediation. Tole hone#:336-609 790'3: ❑ Rotary Distributor •• I Land Application of Sludge • Contact Person : Faron D Leigh p No of wells to be,,sample : - D. Water Source Heat:Pump 0 Other: WeII LocatienlSite Name:DOV+rngradien# d5 iron,aem,n) • If WELL • SAMPLING•INFORMATION • s FIELD ANALYSES: WAS WELL`.ID NUMBER,{from Permit}. MW 3 Date sample collected ��lv^ � • Q • oG DRY f Well Depth ;39..80 ft Well Diameter • 2...in pH 6 0 units:• Temp Z5 time of ft, below measuring poin t Screened Internal 38:5 ft to 43 5 ft` Spec Cond'. µMhos. sampling Depth;to Water Level: /a�'S Measuring Paint is 1:7.3 ft above land surface • Relative M,P:Elevation, ' ft. Odor check allons Appearance here;❑ Volume of water pumpedlbailed..before sampling: f g. _ s a ples for me Sam ` tl :were collected unfiltered.aK�YES „` ❑N ❑NO O and field acidcfied ®YES:, LABORATORY INFORMATION • Date sample analyzedi,. O3'-7/ j�1i err 3^o? Laboratory Name: Analytical Environmental Services Certification No..562 • PARAMETERS NOTE:Values should reflect.dissolved an colloidalconce.ntrations:: COD mg11 ite"(NO2}as mgll Nitr N::, • �d,p/� �mg/l Coliform• .MF Fecal • • /100rn1Pb Lend Nitrate(NO3)(NO3J as N ': %`',�� rngl[ - or. Q�3�r� mgll 4 Coliform MF`: , .Total • �I100rril` • Phosphorus:Total as P m911 Zn Zi nc (Noce: use'.MPN me}hoa for highly Turbid samples) Orthophosphate'' mgll Other(Specify CompoundsConcentration and Con n Units}:.' m ll :. Al-Aluminum mg/l C� q Dissolved Solids:Total / rx ` 9 pH(when analyzed) units Ba-Barium mg/l TOG. mgll Ca-Calcium '. mgll Chloride mgll, Cd Cadmium d_:ad mgll, Arseni•c mg/I Chromium:Total 9 Y mg/I Grease and"Oils mg/I Cu-:Copper. `` mglf :; ORGANICS;:(by GC,;GCIMS; HPLC).. Phenol mgll Fe Iron mgll (Specify test and method#:ATTACH LAB:REPORT:) Sulfate mg/l Hg Mercury mgll Report Attached' ® ', 'Yes(1) '❑- No(0) >. Specific Conductance µMhos: K Potassium mgll VOC method# 8260 • •Total Ammonia mgli Mg Magnesium ": mgli ,method# • (Ammonia..Nitrogan;.NHaas.N;Ammonia Nitrogen Totaq' " • • • _• - • anese' mg/I Mn Mang method:#� TKN as.N mglr... mgll method# • Poi-:Remediat on Systems Only(Attach Lab Reports).',:: Influent Total VOCs: ` mglt: - Effluent Total VOCs: mg/L VOC'Removal% I certify that,to the best of my knowledge and belief.the information submittedin this report is true,acecirate;and complete,and that the laboratory analyiirzi data was produced using approved methods of analysis by a ssibilit of fin s OWQ-certified laborato . ram aware that there are sl nificant.enaities for submittln.false information incruding the o om.resonment fnr knowing wo anon 9 es and � Brian L Smith Operations Manager �., z Perinittee(or Authonzed Pyentl Name:and Title';-.P.lease print or tyrer. 5:gnat ermlttee(orAuth:�edAgentl G1N 59 fRev:1/2Q07 Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-3 • Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 2:15:00 PM Lab ID: 2103D24-003 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatclilD ilu to Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW5030B) 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,1,1-Trichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,1,2,2-Tetrachloroethane BRL 0.50 uglL 312400 1 03/22/2021 15;13 CM 1,1,2-Trichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,1-Dichloroethanc BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,1-Dichioroethene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,1-Dicbloropropene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,2,3-Trichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,2,3-Trichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,2,4-Trichiorobenzene BRL 0.50 uglL 312400 1 03/22/202115:13 CM 1,2,4-Trimethylbenzene BRL 0.50 ug/L 312400 1 03/22/202i 15:13 CM 1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 312400 1 03/22/2021 15:13 CM 1,2-Dibromoethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,2-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,2-Dichloroethane BRL 0,50 ug/L 312400 1 03/22/2021 15:13 CM 1,2-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,3,5-Trimethylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 15;13 CM 1,3-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,3-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 1,4-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 2,2-Dichloropropane BRL 0.50 (TJL 312400 1 03/22/2021 15:13 CM 2-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 4-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM 4-Isopropyltoluene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Benzene BRL 0.50 ug/L 312400 1 03/22/2021 15;13 CM Bromobenzene BRL 0.50 uglL 312400 1 03/22/2021 15:13 CM Bromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Bromodichloromethane BRL 0.50 uglL 312400 I 03/22/2021 15:13 CM Bromoform BRL 1.0 ug/L 312400 1 03/22/202115:13 CM Bromomethane BRL 0.50 uglL 312400 1 03/22/2021 15:13 CM Carbon tetrachloride BRL 0.50 ug/L 312400 1 03/22/2021 15:13 - CM Chlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Chioroethane BRL 1.0 ug/L 312400 1 03/22/2021 15:13 CM Chloroform BRL 0.50 ugh! 312400 I 03/22/2021 15:13 CM Chioroynethane BRL 0.50 ug/L, 312400 1 03/22/2021 15:13 CM cis-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Dibromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Dibromomethane BRL 0.50 ug/L 312400 1 03/22/2021 15;13 CM Dichlorodifluoromethane BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Ethylbenzene BRL 0.50 ug/L 312400 I 03/22/2021 15:13 CM Hexachiorobutadiene BRL 0.50 og/L 312400 1 03/22/202115:13 CM Isopropylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Methylene chloride BRL 5.0 ug/L 312400 1 03/22/2021 15:13 CM n-Butylbenzene BRL 0.50 ug1L 312400 1 03/22/2021 15:13 CM n-Propylbenzene BRL 0.50 uglL 312400 1 03/22/2021 15;13 CM Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitation range) BRL, Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded New See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 14 of 56 . Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-3 Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 2:15:00 PM Lab ID: 2103D24-003 Matrix: Aqueous t Reporting Dilution Analyses Result Qual Units BatchlD Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS 8260D (SW5030B) Naphthalene BRL 1.0 ug/L 312400 1 03/22/2021 15:13 CM sec-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Styrene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM tert-Butylbenzene BRL 0.50 ug/L 312900 1 03/22/2021 15:13 CM Tetrachloroethene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Toluene BRL 0.50 ug/1, 312400 I 03/22/2021 15:13 CM trans-1,2-Diehloroethene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Trichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Trichlorofluoromethane BRL 0.50 ugh 312400 1 03/22/2021 15:13 CM Vinyl chloride BRL 0.50 ug/L 312400 1 03/22/2021 15:13 CM Slur 4-Bromofluorobenzene 93.3 74.9-127 %REC 312400 1 03/22/2021 15:13 CM Surr:Dibromofluoromethane 94.8 78.9-121 %REC 312400 I 03/22/2021 15:13 CM Surr:Toluene-d8 94.3 81.5-120 %REC 312400 1 03/22/2021 15:13 CM Residue,Dissolved(TDS)by SM2540C Residue,Dissolved(TDS) 92 10 nigh 311771 1 03/15/2021 13:35 NN Inorganic Anions by IC EPA 300.0 Nitrogen,Nitrate(As N) 0.465 0.250 H mg/L R449606 1 03/13/2021 15:00 IP Hydrogen Ion(pH)by SM4500H+B pH 6.86 0.0100 H pH Units R449113 1 03/15/2021 14:40 CB Fecal Coliform(MF) SM9222D Fecal Coliform,(MF) 2 1 H Colonies/100 R449461 1 03/17/2021 11:25 TN ml METALS,TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 mg/L 311837 1 03/17/2021 09:32 JM Chromium 0.0209 0.0100 mg/L 311837 1 03/17/2021 09:32 JM Lead BRL 0.0100 mg/L 311837 1 03/17/2021 09:32 JM Zinc 0.0232 0.0200 mg/L 311837 1 03/17/2021 09:32 .1M Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See ease narrative N Analyze not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyto detected in the associated method blank a Less than Result value a Greater titan Result value J Estimated value detected below Reporting Limit Page 15 of 56 SUBMIT FORM:ON YELLOW PAPER ONLY: KE; 0ENYI ,NMEN !N 7U RESOaURCFS § it ..kri' Mail original � ,a�T �nt;.r�q„�, ,�w� ,,�,,,)T ..�/�,��.�, „��.�,�" TY`:MONITORING: • . . .�'.. •o F R U INP(7 .;4 OIL OGla$S, G u � .( " GROUNDWATER:QUAL:.. '! � o ,,and copy t �1�A�• • T ;� 0)Nc 69 0 : ; orre, i91s} s 22..1 0 • COMPLIANCE 'REPORT FORM t � 1=� Prt rt creamy or type, Number.: • •• Expiration Date.;06-30=2022 • J=ACI�jTY INFORMATION , Please, ERMIT '' • P Facility Name:. Colonial:Pipeline Company charge W NPDES O her s Q0005809 C Permit Name,(if different) , .. . Facility Address: 411 Galilmore pairy Raad' • • • • TYPE OF PERMITTED OPERATION BEING MONITORED (st"!'"*. ty ford • " ': ❑ lagoon `❑Remediation Infiltration Gallery Greensboro NC 27409` :-'• Coun Gull ❑Remediation Contact Persorr Far on D. Leigh Telephone#:33 otary Dis 6 669 7903 ❑ R tributor ®Land•Application of Sludge Well Location/Site Name:D.own grad lent ' •;No of wells to be sampled 5 Water Source Heat Pump Other:` SAMPLINGINFORMAT : WAS WELL ID NUMBER(from Permit) ( 35) Date sample collected e.. -/e`off FIELD ANALYSES. MW 4 MV11 1 • 29:5 ft DR oft ` Wel]Depth - Well Dlame#er 2:in. pH � .units 73 to 28 ft`.. Spec. . T emp 34.. erval ft.' .. P sampling, • • • • • µNE os.: •Depth>fo Water:Level. ��.$�5..ft. below measuring point Screened Int Measuring Point is 2 ft.above land surface•: •Relative M.P Elevation •ft: • Odor check Volume of water umpedlbai[ed•":before•sampling: �.�� gallons Appearance• here:LJ • Samples for,metals.were.collected unfiltered. ®YES ❑:NO and field acidified: • ®YES. ❑NO ARORATORY INFORMATION Date sample`.analyzed:- ' •Q3�/� /i,-H •13 07� Laboratory Name: •Analytical Environmental Services Certification.No.`562 olloidal concentrations. • reflect: Nitrite N • mg/1 - PARAMETERS. NOTE Values should • Pb-Lead �Q,Q�d mg/I(NO2)z) COD mgll ( dissolved an c 1100m1: Nitrate(NO3)as•N r{: , mg/l Zn:-Zinc ® %` Conform:.MF Fecal: : � �S m g Colif Coliform MF Total /100ml :Phosphorus:Total as P mg/I P " • c-(Note:•Use MPN method for highly:turbid samples) p p - :and Concentration Units) ;.:: Ortho hos hate , . mgll. Other(Specify.Compounds ,Dissolved Solids:Total 6e, mg/1 Al• :Al-.Aluminum: • mg/I anal p1-I(when yzed) units Ba-13arlum. mg1l TOC mglt . Ca-Calcium ..: mgll .. Chloride. " mgl[ . Cd-Cadmium < .6,, • ,mg/1 Arsenic m•gll Chromium:Total ,1 0 6 rngll Grease and:.Oils • •mgl[ C• u-Copper mg/l ORGANICS:(by GC,:GCIMS,HPLC) Phenol.• • mg/I Fe Iron ' • • • mg/I (Specify test•and method#;ATTACH LAB:REPORT.) Sulfate • mg/I Hg-Mercury mg/I • Report Attached? ®': Yes(1) ❑:No(0) Specific Conductance • i1Mhos K-Potassium _mgll VOC ,method#.8260 Total Ammonia: mgll. Mg Magnesium mg/I • method# • (AmmoniaNitrogen;NI-13as N;Ammonia Nitrogen,Total) - "Mn-Manganese • mgll , method#'" N mgll Ni..'Nickel mg/1 TKN as - method#.: .. , . "!o For Remediation,SystemsOnly(Attach:•Lab Reports).. T > Influent otal VOCsy; .mg/IL :•Effluent Total VOCs mg/L VOC:Removal i certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis bya DWQ-certified laborato . I am aware that there are si.nificant.enalties for submittn false information includin:the.ossihility of fines and im.nsonrnent for knowin.violations Brian,L Smith Operations Manager J � • : °' ' Permit-tee(or Auingnzed Aaent)Name and Title.-.R4ease.gnntor type. Snature -ermittee for.A orized Agent) a !Date) GW 59 Rev.112007 . Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-135(MW-4) Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 2:00:00 PM Lab ID: 2103D24-008 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchiD Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW5030B) 1,1,1,2-Tetrachioroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1,1-Trichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1,2-Trichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1-Dichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,1-Dichloropropane BRL 0.50 OWL 312400 1 03/22/2021 20:12 CM 1,2,3-Triehlorabenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,2,3-Trichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,2,4-Trichlorobenzene BRL 0.50 ug/L, 312400 1 03/22/2021 20:12 CM 1,2,4-Trimethylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,2-Dibromo-3-chloropropane BRL 1.0 ug(L 312400 I 03/22/2021 20:12 CM 1,2-Dibromoethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM l,2-Dichlorobenzene BRL 0.50 OWL 312400 1 03/22/2021 20:12 CM 1,2-Dichloroethane BRL 0.50 uglL 312400 1 03/22/2021 20:12 CM 1,2-Dichloropropane BRL 0.50 uglL 312400 1 03/22/2021 20:12 CM 1,3,5-Trimethylbenzene BRL 0.50 ut 1L 312400 1 03/22/2021 20:12 CM 1,3-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,3-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1,4-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 2,2-Dichloropropane BRL 0.50 ug/L 3i2400 I 03/22/2021 20:12 CM 2-Chlorotoluene BRL 0.50 • ug/L 312400 1 03/22/2021 20:12 CM 4-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 4-Isopropyltoluene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Benzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Bromobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Brolnochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Bromodichloromethane BRL 0.50 ugh., 312400 1 03/22/2021 20:12 CM Bromoform BRL 1.0 ug/L 312400 I 03/22/2021 20:12 CM Bromomethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Carbon tetrachloride BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Chlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Chloroethane BRL 1.0 ug/L 312400 1 03/22/2021 20:12 CM Chloroform BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Chloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM cis-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Dibromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Dibromomethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Dichlorodifluoromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM 1 thylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Hexachlorobutadiene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Isopropylbenzene BRL 0,50 ug/L 312400 1 03/22/2021 20:12 CM Methylene chloride BRL 5.0 ug/L 312400 1 03/22/2021 20:12 CM n-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM n-Prapylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Qualifiers: * Value exceeds maximum contaminant Level E Estimated(value above qudetitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding limes for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 23 of 56 Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-135(MW-4) Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 2:00:00 PM Lab ID: 2103D24-008 Matrix: Aqueous Reporting Dilation Analyses Result Limit Quad Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW5030B) Naphthalene BRL 1.0 ng/l-. 312400 1 03/22/2021 20:12 CM sec-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Styrene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM tert-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Tetrachloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Toluene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM trans-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Trichloroethene BRL 0.50 ug/L 312400 I 03/22/2021 20:12 CM Trichlorofluoromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Vinyl chloride BRL 0.50 ug/L 312400 1 03/22/2021 20:12 CM Surr:4-Bromofluorobenzene 101 74.9-127 %REC 312400 1 03/22/2021 20:12 CM Surr:Dibromofluoromethane 97.9 78.9-121 %REC 312400 1 03/22/2021 20:12 CM Sun:Toluene-d8 91.3 81.5-120 %REC 312400 1 03/22/2021 20:12 CM Residue,Dissolved(TDS)by SM2540C Residue,Dissolved(TDS) 80 10 mg/L 311770 1 03/12/2021 11:50 NN Inorganic Anions by IC EPA 300.0 Nitrogen,Nitrate(As N) BRL 0.250 ma/L R449368 1 03/11/2021 21:23 IP Hydrogen Ion(pH)by SM4500H+B pH 6.70 0.0100 H pH Units R449338 1 03/17/2021 16:44 SK Fecal Coliform(MF) SM9222D Fecal Coliform,(MF) 2 1 H Colonies/100 R448987 1 03/11/2021 13:45 TN m1 METALS,TOTAL SW6010D (SW3010A) Cadmium 13RL 0.0050 mg/L 311837 1 03/17/2021 09:39 JM Chromium 0.0268 0.0100 mg/L 311837 1 03/17/2021 09:39 JM Lead BRL 0.0100 mg1L 311837 1 03/17/202109:39 JM Zinc 0.140 0.0200 mg/L 311837 1 03/17/2021 09:39 JM Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitation range) BRL Below repotting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Annlyte notNELAC certified F Analyzed in the lab which is a deviation from the method B Analyle detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Pape 24 of 56 SUBMITrFORM ONYFLLOW PAPER ONLY ' �:. i D P AfE tVlCov4r otrR��cpp„�U%o1LE Mr t riNiWatFiO IAN t.1/41(�i; ESi36 P.09 1Mn O a3 3-32 0ori*�7t�rct r Mail original GROUNDWATER QUALITY MONITORING: and 1 copyto: El :, ,1sTT� COMPLIANCE:.REPORT:FORM Please.Print Clearly or.Type No PERMIT�NumbeWr~ Expiratio n Date ;Q - - n n Discharge Q0005809 Facility Name Colonial Ripellne Cgpa y NPDES �, : .i Others Permit Name(if different): 411''Gallirr�� ore DairyRoad " TYPE OF PERMITTED OPERATION BEING MONITORED . Facility Address: ❑Remediation Infiltration Gallery NC 2T4Q9 County:Guilford ' ❑"Lagoon Greensboro •0 diation: (City),_ f5tate}:_ '.(Zip) ,'. ❑ $pray Field r; Reme _.,, .. Contact Person: "Faron D. Leigh Telephone#:, 336-669 79.D3' ❑;Rotary Distributor" I Land"Application of Sludge." nt . '` No of wells to be sampled: 5 9 e Water Source Heat Pump ❑Other:; Well Location/Site Name.Down radl,"," f itl L; :❑ If WELL SAMPLING INFORMATION m:Permit :. ':MW-6 MW 183 Date sample collected O3—/ll^,02 WAS ( . � � FIELD ANALYSES: aC DRY:at Well Dep NUMBER(fro ) H o 6 units Temp t7 / Well Depth. 27.O.Q ft Well Diameter: 2 in. P S., time of 25 ft. Spec.Cond: p.Mhos Depth to Water:Level 5,/� 'ft below measuring point Screened Interval 1fl ft to, ch ckng 1:.5Relative M.P.Elevation: ft. Odor �: Measu,ring Point is ft.above land surface Volume of water pumped/bailed before sampling: //+( gallons Appearance> here: Samples for metals were collected unfiltered ®YES ❑NO and field acidified ®"YES: ❑NO LABORATORY INFORMATION •Date sample analyzed Ana] ties[Enviranrnental Services: • Certification No..:562 .`. -�f f A,r'y ,�3—re Laboratory Name y NOTE:Values should reflectc dissolved= an colloidal conentrations:; PARAMETERS`. NO Pb Lead Q �d mg/l COD `-'rngll Nitrite(NO2)as N mg/l Coliform. MF Fecal Zn Zinc" -C 4 rngl! " 1100m1.° Nitrate(NO3)as N C Conform:MF Total 1100m1 Phosphorus:• 'Total as P mgll Nate:.Use MPN method for highly turbid samples) :'Orthophosphate mg/I _ Other(Specify Compounds and Concentration Units): Dissolved Solids Total f S mgll AI Aluminum mgll pH(when analyzed) units l3a-Sanum mgl! TOC mgp Ca-Calcium mgll" Chloride mg/I Cd-Cadmium d= c:76, mg1l Arsenic mg/l Chromium:Total O.,d/� mgll. Grease and Oils mgli " Cu Copper mgll ORGANICS:(by GC;'GCIMS;HPLC); Phenol mgll Fe Iron ' mgh (Specify test and method# ATTACH LAB REPORT.) Sulfate mgll Hg-Mercury mg/I Report Attached? [ l Yes(1) CI No(0) S pacific Conductance '- :.Mhos. K-Potassium" mgh method# 8260 Total Ammonia mgll Mg Magnesium: 9 VOC (Ammonia'Nitrogen;NH3 as N;Ammonia Ndrogen Total) - • Mp-Manganese mgl! - ,method TKN as N, mg/l " method Ni rNtckel ' , m /l orts Influent Total VOCs:; mglL ..:Effluent Total VOCs.. mglL yal°Jo- For Remedla#ion Systems Only. (Attach Lab Rep ) " I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a 'f labarato I am aware that there are significant penalties for submithn false information including the.ossibilit of fees and im.nsonmeni for knowing violations 'I]W�ct;rti fed Brian'L. Smith Operations Manager Coate) ortvge Signature of Pennittee(o. uthorized:Agent) > Pennittee(or Authorized:Agent)Name and print'litle'-:Rlease. ,:.. GW, 59 Rev 5120.07 , Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-183(MW-6) Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 1:45:00 PM Lab ID: 2103D24-009 Matrix: Aqueous Reporting Dilution Result Analyses Limit Qual Units BatchlD Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS 8260D (SW5030B) 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,1,1-Trichloroethane BRA. 0,50 ug/L 312400 1 03/22/2021 20:33 CM 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,1,2-Trichloraethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,1-Dichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,1-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,1-Dichloropropene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2,3-Trichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2,3-Trichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2,4-Tichlorobenzene BRL 0.50 ug/L 312400. 1 03/22/2021 20:33 CM 1,2,4-Trimethylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 312400 1 03/22/2021 20:33. CM 1,2-Dibromoethane BRL ' 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2-Dichlorobenzene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM 1,2-Dichloroethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,2-Dichloropropane BRL 0,50 ug/L 312400 1 03/22/2021 20:33 CM 1,3,5-Trimethylbenzene BRL 0.50 ag/L 312400 1 03/22/2021 20:33 CM 1,3-Dichlorobenzene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM 1,3-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 1,4-Dichlorobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 2,2-Dichloropropane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 2-Chlorotoluene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM 4-Chlorotoluene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM 4-Isopropyltoluene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Benzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Bromobenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Bromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Bromodichloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Bromoforin BRL 1.0 ug/L 312400 1 03/22/202120:33 CM Bromornethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Carbon tetrachloride BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Chlorobenzene BRL 0,50 ug/L 312400 I 03/22/2021 20:33 CM Chloroethane BRL 1.0 ug/L 312400 1 03/22/2021 20:33 CM Chloroform BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Chloromethane 13RL 0.50 ug/L 312400 1 03/22/2021 20:33 CM cis-1,2-Dichloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Dibromochloromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Dibromomethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Dichlorodifluoromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Bthylbenzeene BRL 0,50 ug/L 312400 1 03/22/2021 20:33 CM Hexachlorabutadiene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM Isopropylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Methylene chloride BRL 5.0 ug/L 312400 1 03/22/2021 20:33 CM n-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM n-Propylbenzene BRL 0.50 ug/L, 312400 I 03/22/2021 20:33 CM Qualifiers: a Value exceeds maximum contaminant level . a Estimated(value above guantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or annlysis exceeded Narr See case narrative N Annlyte notNBLAC certified F Analyzed in the lab which is a deviation Corn the method B Analytc detected in the associated method blank < Less than Result value a Greater than Result value .1 Estimated value detected below Reporting Limit Page 25 of 56 Analytical Environmental Services,Inc Date: 5-Apr-21 Client: Colonial Pipeline Client Sample ID: MW-183(MW-6) Project Name: Greensboro Quarterly Sampling Collection Date: 3/10/2021 1:45:00 PM Lab ID: 2103D24-009 Matrix: Aqueous Reporting Dilution Analyses Result Qua' Units BatchlD Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS 8260D (SW5030B) Naphthalene BRL 1.0 ug/L 312400 I 03/22/2021 20:33 CM sec-Butylbenzene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM Styrene BRL 0.50 ug/L 312400 I 03/22/2021 20:33 CM tert-Butylbenzene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Tetraehloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Toluene BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM trans-1,2-Diehloroethene BRL 0.50 ug/L 312400 1 03/22/2021 20;33 CM Trichloroethene BRL 0,50 ug/L 312400 1 03/22/2021 20:33 CM Trichlorofluoromethane BRL 0.50 ug/L 312400 1 03/22/2021 20:33 CM Vinyl chloride BRL 0.50 ug/L 312400 1 03/22/2021 20;33 CM Surr:4-Bronofluorobenzene 92.2 74.9-127 %REC 312400 1 03/22/2021 20:33 CM Surr:Dibromofluoromethane 95.5 78.9-121 %REC 312400 1 03/22/2021 20:33 CM Surf:Toluene-d8 95.4 81.5-120 %REC 312400 1 03/22/2021 20:33 CM I Residue,Dissolved(TDS)by SM2540C Residue,Dissolved(TDS) 154 10 mg/L 311770 1 03/12/2021 11:50 NN Inorganic Anions by IC EPA 300.0 Nitrogen,Nitrate(As N) BRL 0.250 mg/L R449368 1 03/11/2021 21:12 IP Hydrogen Ion(pH)by SM4500H+B pH 6.14 0.0100 H pH Unite R449338 1 03/17/2021 16:46 SK Fecal Coliform(MF) SM9222D Fecal Coliform,(MF) 22 1 H Colonies/100 R448987 1 03/11/2021 13;45 TN ml METALS,TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 ntg/L 311837 1 03/17/2021 09:41 JM Chromium BRL 0.0100 mg/L 311837 1 03/17/2021 09:41 JM Lead BRL 0.0100 mg/L 311837 I 03/17/2021 09:41 JM Zinc BRI, 0.0200 mg/L 311837 1 03/17/202109:41 JM Qualifiers: a Value exceeds maximum contaminant level B Estimated(value above quentitetion range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Neff See case narrative N Acolyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Anelyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 26 of 56 GW-59A COMPLIANCE REPORT FORM Permit# W00005809 (Submit one each monitoring period with GW-59 forms) Enter date monitoring results were due.(AUGUST 31,2021)Will this monitoring report(GW59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES( NO iF the answer to question I or 2 is"YES",list in the space provided below the well identification number(s)and explain the a problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing identificat n YES NO plate,area overgrown,etc.)?If the answer is"Yes",contact the Regional Office for guidance. Some wells need locks gud protective casings. - 4 Are any monitored constituents equal to or above the established standards? `{ YES)NO If the answer to question 4 fs WO",skip to section 8. If the answer to question 4 is"YES"list the affected wells individually with constituent(s)and concentration(s) exceeding standards in the space provided below: pH for all monitor wells sampled was below the range of 6.5-8.5 SU. 5 For the constituents Identified in question 4 above,have standards been exceeded previously for the same YES NO constituent(s)in the same well(s)In the last two years? If the answer to question 5 is WO",skip to section 8. If the answer to question 5 is"YES", list in the space provided below,each well with constltuent(s)exceeding standards,concentration(s)reported,and sample collection date for each occurrence(for the last two years). ltfi MW's had a pH less than 6.5 SU In previous sampling events. 6 Are the monitoring wells listed In section 5 located at or beyond the review boundary? YES - NO If the answer is"YES",a groundwater quality problem may be occurring.CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE.If the answer Is"NO",monitoring wells may be improperly located;contact the Regional Office. 7 Is the permittee Implementing previously approved actions required by the Division involving this groundwater YE( NO quality problem? If the answer to question 7 is"YES',describe those actions in the space provided below. If the answer to question 7Is"NO",contact the Regional Office within 90 days;an evaluation may be required to determine the impact the waste disposal system Is having at the review and compliance boundaries surrounding this facility.Failure to do so may subject the permittee to a Notice of Violation, fines,and/or penalties. 8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current O W-59 form. I hereby acknowledge that the above information was evaluated and the information submitted In this report (Comelianct:_R GW-59A)is true and com to the best of my knowledge. ff Signature of Permittee(or Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY Mail original EP/1RT of Nvl1?rNMEN;3AiC�U,4E.1T�,' f? orwiCf tFLESQl1RCEs GROUNDWATER QUALITY MONITORING: and 1 co to: .:'-, �dN RdcEssING NIT '` r COMPLIANCE REPORT FORM! copy r - r n ail. 'rvicESr , Ra nic zr69s--s» F , � r; FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 ulc Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Daily Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 County Guilford 0 Lagoon 0 Remediation:Infiltration Gallery (city) (state) MO 0 Spray Field ❑Remediation: Contact Person: Brian Smith Telephone# 336-931-6027 0 Rotary Distributor IDLand Application of Sludge Well Location/Site Name:Upgradient of Field No:of wells to be sampled:6 0 Water Source Heat Pump ❑Other: (from Nam) WELL SAMPLING INFORMATION If If WAS WELL ID NUMBER(from Permit): MW-1 Date sample collected:7I30I2021 FIELD ANALYSES: 21.9 f, Well Diameter.2 in. pH 00400:5-7 units Temp.0o010: 17:6 °C DRY at Well Depth: firma of Depth to Water Level 62546:11.61 ft.below measuring point Screened Interval: ft. to ft. Spec.Cond.00094:0.0373 µMhos sampling, Measuring Point is ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ®YES 0 NO and field acidified: ®YES 0 NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform:MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 1.4 mg/L Zn-Zlnc 010s2 <0.01 mg/I. Coliforrn:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for nighty turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 269 mg/L Al-Aluminum 01105 mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug/L Arsenic 01o02 ug!L Chromium:Total 01034<5.0 uglL Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 ug!L Fe-Iron 01045 ug!L (Specify test and method#.ATTACH LAB REPORT.) Sulfate oos4a mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑■ Yes(1) 0 No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen:NL-1 ee N:Ammonia Nitrogen,Total) Mn-Manganese 01055 ug!L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal I certify that,to the best of my knowledge and belief,the information submitted in:his report is true,accurate,and complete and chat:he laboratory analy'cal data'.vas produced using approved methods of analysis by a DWR-certifceo laboratory. I am aware that there are signiricant penalties for submitting false informaicn,including mo poss bility of`ines and irnprlscrcment tor kn wino violations. Brian Smith ____.(-3 ____ Permit a(or Authorized Agent)Name and The-Please print ortype IGS nitre of Perm a(orAuthorized Agent) (Date) GW-59 Rev.06-07-2018 Pace Analytical Services,LLC 9800 kincey Ave. Suite 100 ("1 Huntersville,NC 28078 (704)875 9092 aceAnalyt caf www.pacelabs.cam ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 (dual Lab ID: 92552615001 Collected: O7l30I2109:10 Receive Received: 07130I2A1n1iy ed Mab'CAS No. Sample. MW 1 Report Limit __OF _______Preparex:Water d units �� Parameters Analytical Method:EPA 200.7 Rev 1e.41994 Preparation Method:EPA 200.7 Rev 4 4199 - 200.7 MET IcP Pace Analytical Services Asheville ug/L 1.0 .1 08/04/21 02:00 08104121 18 02. 7440-43 9 <1.0 5.0 1 08/04/21 02:00 08104I21 18 02 7440-47-3 Cadmium <5 0 uglL 5.0 1 08/04/21 02:00 08/04121 18 02 7439-.92-1 Chromium <5.0 ug/L 10.0 1 08/04/21 02:00 08104/21 18:02 7440-66=6 Lead` <10.0 ughL Zinc Analytical Method.EPA 8260D 826UD MSV Low Level Pace Analytical Services Charlotte 25 0 1 08I06121 01 26 67 64-1 <25.0 uglL 08I0612101:20 71�43-2 Acetone ug/L 1'0 1 08/06121 01:26 108 86 1 51.0 1.0 :1 Benzene <1.0 uglL 08/06/21 01;26 74 97-5 1.0 ' ;1 08l06121 01:26 75 27-4 8roinobenzene <1A uglL 1.0 1 Bromachlororometh a <1.0 ug/L 08/06121 01:26 75-25-2 ug/L 1.0_ 1 08/06/21 01:26 74-83-9 v2 Bromodlchlorbmethane <1.0 �.0 1 BromofOrm <2,0 ug/L 08/06/21 01:26 78 93 3 5.0 1 08106/21 0126 56 23 5 Bramomethane. <5.0 uglL 1.0 1 Carbonnone(MEK) <1.0 ugfL 1.0 1 08106I21 01`.26:108-90-7 tetrachloride <1.0 ug/L 08106/21 01:26 75-00-3 1K ugh_ 1.0 1 06I06121 01:26 67-66-3 Ch Chloroform nzene e1.0 1.0 1 Chioroethane e7 0 ug/L 1.0 1 08/06/21 01:26 74 87 3 Chloroform <1.0 uglL 1.0 1 08/06/21 01:26 95-49-8 Chloromethane <1.0 ug/L 1.0 1 08I0612101:26 106-43-4 2-Chlorotoluene <1.0 ugh.- 0 1 08I06121 01:26 96-12-8 4-Chlorotoluene <2.0 ug/L 12.0 1 08/06/21 01:26 124-48-1 Dibro 1,2-Dibromo-3-chloropr0pane <1.0 ugh- 1.0 1 08l06121 01:26 106-93-4 1,2-Di ochloethaneane <1.0 uglL 1.0 1 08/06/21 01:26 74-95-3 1,2-Dibromoethane(Et36) <1.0 ug/L 1.0 1 08106121 01:26 95-50-1 Dlbromomethane <1.0 ug/L 1.0 1 08106/21 01:26 541-73-1 1,2 Dichlorobenzene <1.0 ug/L 1.0 1 08106I21 01:26 106-46-7 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 75-71-8 1,4 lorodirobenxena <1.0 ug/L 10 1 08106/21 01:26 75-34-3 Dichlorodiftuoromethane <1.0 uglL 08/06/21 01:26 107-06-2 ug/L 1.0 1 08/06/21 01:26 75-35-4 1,1-pichloroethane <1.01.0 1 1,2-Dlchloroethane <1.0 ug/L 0B/0612101:26 156-59-2 1.0 1 08106121 01:26 156-60-5 1,1-pichloroethene <1.0 ug/L 1.0 1 cis-1,2-Dich10r0eththe <1.0 ug/L 1.0 1 08/06/21 01:26 78-87-5 trans 1,2-Di prop ethene <1.0 ug/L 08/06I21 01:26 142-28-9 uglL 1.0 1 08106/21 01:26 594-20-7 1,2-Dichloropropane <1.0 1.0 1 1,3-Dichloropropane <1.0 uglL 1.0 1 08106I2101:26 563-58-6 2,2-Dichloropropane <1.0 ug/L 08/06/21 01:26 10061-01-5 1.0 1 08/06/21 01:26 10061-02-6 1,1-Dichloropropene <1.0 uglL 1.0 1 cis-1,3-Dichloropr0pene <1.0 ug/L 08/06/21 01:26 108-20-3 uglL 1.0 1 08I06121 01:26 100-41-4 trans-1,3-Dichloropropene <1,0 1.0 1 Diisopropyl ether <1 0 uglL 06I06121 01:26 3 2.0 1 08/06/21 01:26 7-68-36 Ethylbenzene <2,0 uglL 5 0 1 Hexachloro 1,3 butad'+ene <5.0 uglL 08/06/21 01:26 99-87-6 2-Hexan0ne <1.0 uglL 1.0 1 p-isapropyltoluene REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Page 5of, without the written consent of Pace Analytical Services,LLC. Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 /,P'aceAnaIyticaI® www.pacelahs,cem Huniersville,NC 2807a (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-1 Lab ID: 92552616001 Collected: 07/30/21 09:10 Received: 07/30/21 11:20 Matrix:Water Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte <5.0 uglL 5.0 1 08/06/21 01:26 75-09-2 Methylene Chloride 5 0 1 08I06121 01:26 108-10-1 4-Methyl-2-pentanone(MIBK) <5.0 uglL <1.0 uglL 1.0 1 08/06/21 01:26 1634-04-4 huty!ether <1.0 uglL 1.0 1 08/06/21 01:26 91-20-3 Naphthalene Styrene <1.0 ug/L 1.0 1 08/06/21 01:26 100-42-5 1 0 1 08106I21 01:26 630-20-6 1,1,1,2-Tetrachloroethane <1.0 ug/L <1.0 ug/L 1.0 1 08/06/21 01:26 79-34-5 1,1,2,2-Tetrachloroethane Tetrachioroethene <1.0 uglL 1.0 1 08/06/21 01:26 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 01:26 108-88-3 1 0 1 08/06/21 01:26 87-61-6 1,2,3-Trichlorobenzene <1.0 ug/L <1.0 ug1L 1.0 1 08/06/21 01:26 120-82-1 1,2,4 7richlorobenzene 1 0 1 08/06/21 01:26 71-55-6 1,1,1-Trlchloroethane <1.0 ug/L <1.0 uglL 1.0 1 08/06/21 01:26 79-00-5 1 rich o r ethenethane 1.0 1 08/06/21 01:26 79-01-6 Trichloroethene <1.p ug/L <1.0 uglL 1.0 1 08/06/21 01:26 75-69-4 Triohlorofluoromethane 1 D 1 08/06/21 01:26 96-18-4 1,2,3-Trichloropropane <1.0 ug/L <2.0 ug/L 2.0 1 08/06121 01:26 108-05-4 Vinyl acetate 1 0 1 08/06/21 01:26 75-01-4 Vinyl chloride. <1.0 uglL Xylene(Total) <1.0 ug/L 1.0 1 08I06121 01:26 1330-20-7 <2.0 ug/L 2.0 1 08/06/21 01:26 179601-23-1 m&p-Xylene 1.0 1 08/06/21 01:26 95-47-6 o-Xylene <1.0 ug/L Surrogates 70-130 1 08/06/21 01:26 460-00-4 4-Bromofiuorobenzene(S) 101 %101 % 70-130 1 08/06/21 01:26 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 08/06/21 01:26 2037-26-5 Toluene-d8(S) 2540C Total Dissolved Solids Analytical Method:SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 269 mglL 25.0 1 08/03/21 18:53 353.2 Nitrogen,N021NO3 unpres Analytical Method:EPA 353.2 Rev 2.01993 Pace Analytical Services-Asheville 1.4 mg/L 0.040 1 07/31/21 13:44 14797-55-8 Nitrogen,Nitrate0.040 1 07/31/21 13:44 14797-65-0 Nitrogen,Nitrite <0.040 mglL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, __ __.... ,..11.1-...,,.fro,.,r1tt,n consent of Pace Analytical Services,LLC. Page 6 of 43 =t•% ai OS `� '- Inco cis = N p m co zo < I n 0 v z ° ❑ O o 0.Q ✓ o m a N a_,t7 ct , ` C9 -Npi " Z C _ °, wE v * # * * v_ aV. D U aZ GN Oa a Et a O Oci ca 0 cb v $ is a -- tllEI d 5' H o❑ ❑ ❑ ❑ CO a Wa) � t� EEE Io ~ I- ` v 2, oE N 0 . U O m c°- oapc,) c) `K 0 p 0 o W D rn Z U �C? O E t a. Z "�W. iji X PA o V V 'q C !f n a� o I c m $ o o 5 2 t T. as C IL V) 0 mg V o 0 a m T. 0 \ roan u ns W a v° N D �" U O 40 ° ¢ cno � � a W Qcnpa r5 a o IMg.' lao > . _ W P 4 ❑ ❑ ❑ ❑ ~ O c o E rr a� E E E E E a -it E :m ro '-' .2! Q el L C Ir O ns C3 •0 M U) .J CO E 9 ci) Q. � 100 Li! r I` .N >--. 0 v o e 11. O co N m m o ® L0 . L . o ar 'f m f ' GL �a M V V 2 CS) -a _m E O is e M of t 6 0 o o a o to ti N in 0 ti in ti m o o E7 co 8a -� ui 4 E gg o � 8oggaS2m " ' ' c N - a) C7 ro E o 0 h 0 a © o 0 o °. °i o dcl t z z a m E E E E . 0" c E E m a� j d3 a ' w Cz -. ? 3 (m 0 ° la o ro a = 0 , ' • ai - a m � I- L c U -Ca r in' O as o to Z 0 m c n Ti ? z 0. a al ' f3 c z o _in ° a p a 0) C *J v ., V) `a, o o Z .c U n m E .0 c ❑ a a 'a a �i . N a U LC] U?lij Q , o o `� Y3 -a ...J ,J Li oc _A m 4 e0 to'. Cry A a rn C as rn q^j e" tip C m C .s v co _ EEEELE E c :'N a 2' E " N E ° ® aDi E Z 'i U o 5 E i.. L m rn "'"' w 'Dli. c ii ', `r, m �"� Ql L of O 7 a m } 9 m F.0 _o. 0 0 .� `(i -o H � "N _LI. [L - r .� a5 r V1 3 c .,,, N £ --10 --i I- (� E 1. N L • a) a) O O = . �' o it; m co z a. N m i=N m re • Q '� 00 m0 z .O `0 C ., O E R <C ' '0 04 -o a 0 O o N 0 'n O N N o ? z N F13 0 r- re( E I- C nD W v m sr m o u� m ro z m Q 4' al N cm o en r o O O o .g p E .7.7. 9 al EX a t r 1 m `I` O 3 O d m M o a o 0 o S g Z LLI LLI E U ‘Zr ct 2 Ee Ee rX m E ci 0 6- U ,d E m m E Z o ¢ 0 IT. a iri Qw 3 a a3z _ OU Li- I° E ha r0 '= CO c c o g. a) U1 ° o Z z ai •a u o 0 Z a N o E • m U) L.L. u-' a ro x z c a V] r E z `0 0 -c, '' Q E c 0 - a 0 = _ Tula, , p asW 2 Ec ,p o. U 0 v E a 2 W 2 .Ci Z Atn a. m ca 0. Z k ,2 F- Q m • d. ' ZU [� �. •j N N ttl Q �y V O o '� w tl w3 N ,A E. u) u- _ CICq a Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ® aceAnwwur.pacelahs.cam Huntersville,NC 28078 alytical (704)875 9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No: 92552615 Sample: MW-2 Lab 1D; 92552615002 Collected: 07/30/21 09:30 Received: 07/30/21 11:20 Matrix,Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual ---- 200.7 MET 1CP Analytical ethod:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:12 7440-43-9 Cadmium <5•0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:12 7440-47-3 Cadmium inc Z <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:12 7439-92-1 <10.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:12 7440-66-6 Zinc 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte D8106121 01:45 67 64 1 <25.0 ug/L 25.0 1 08/06/21 01:45 71-43-2 Acetone <1.0 ug/L 1.0 1 08/06/21 01:45 71-43-2108-86-1 Benzene <1.0 ug/L 1.0 1 Bromahenzene 1.0 1 DSIOfi12101:45 74-97-5 <1.0 ug/L08/06/21/ 01:45 75-27-4495 Bromodichlor0meth a <1.0 ug/L 1.0 1 BromoformBromo romethane 1.0 1 08/06/21 01:45 75-25-2 <1.0 ug/L 2.0 1 08106/21 01:45 74-83-9 v2 rnet <2.0 ug/L Bromomethane 5.0 1 08/06/21 01:45 78-93-3 <5.0 ug/L 08/06/21 01:45 78-93-3 2-Butan etr(MEK) <1.0 ug/L 1.0 1 Carbon tetrachloride 1 0 1 08/06/21 01:45 108-90-7 5 <1.0 ug/L 08/06/21 01:45 75-00-3 IK Chloroethanee <1.0 ug/L 1.0 1 1 p 1 08/06/21 01:45 67-66-3 Chloroform <1.0 ug/L 08/06/21 01:45 74-87-3766 Chloroform <1 0 ug/L 1.0 1 Chloromethane 1 0 1 08/06/21 01:45 95-49-8 <1.0 ug/L 08/06/21 01:45 106-43-4 2-Chlorotoluene <i 0 ug/L 1.0 1 4-Chlorotoluene 2 0 1 08/06/21 01:45 96-12-8 <2.0 ug/L 081062101:45 16-12-8 D2-Dmochlor methanropane <1.0 ug/L 1.0 1 Dibromochloromethane 1.0 1 08/06/21 01:45 106-93-4 4-48-1 <1.0 ug/L 08/06/21 01:45 106-93- Dibrom metha a (EDB) <1.0 ug/L 1.0 1 Dibromomethane 0-5-5 1.0 1 08/06/211 01:45 9 74-95-3 <1.0 ug/L 080621 01:45 5-50 1,2-Dichlorabenzene <1.0 ug/L 1.0 1 1,3-Dichlorobenzene1 0 1 08/06/21 01:45 106-46-7 3-1 <1.0 ug/L 08/06/21 01:45 106-46- 75-71-8 Dichl rodifl or0 ene <1.0 ug/L 1.0 1 1,1-Dichloroethmethane 1.0 1 0810612101:45 75-34-3 <1.0 ug/L08/06/21 01:45 107-06-2 1,1-Dichloroethane <1.0 ug/L 1.0 1 1,2-Dichloroethane10 1 08/06/21 01:45 75-35-4 <1.0 ug/L 08/06/21 01:45 15-35 4 cis 1, -Dichl01 etaene <1.0 ug/L 1.0 1 cis-1,2-Dichloroethene 1 0 1 08/06/21 01:45 156-60-5 -2 <1.0 ug/L 080621 01:45 156-605 trans-1Chlor prop ethene <1.0 ug/L 1.0 1 1,2-Dichloropropane -28-4 01:45 9 1.0 1 08/06/2112 <1.0 ug/L 08/06/21 01:45 594-20-7 1,3-Dichloropropane <1.0 ug/L 1.0 1 2,2 Dichloropropane1 0 1 08/06/21 01:45 563-5$-6 <1.0 ug/L 080621 01:45 63-58-6 5 cis 1, -Dichl0r Profpene <1.0 ug/L 1.0 1 cis-1,3-Dichloropropene 1 0 1 08/06/21 01:45 10061-02-6 <1.0 ug/L 08/06/21/ 01:45 10 20-3 Dilsotrans ropyl etheroroprapene <1.0 ug/L 1.0 1 Ethylbe pyl 1.0 1 08/06/21 01:45 100-41-4 <1.0 ug/L 08/06/21 01:45 87-68-3 Ethylbenzene <2.0 ug/L 2.0 1 2 21-lexa oro 1,3-butadiene 5 0 1 08/06/21 01:45 591-78-6 <5.0 ug/L 08/06/21 01:45 99-87-6 p-IIsoproane <1.0 ug/L 1.0 1 p-Isopropyltoluene REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in Lull, Page 8 of 43 Date:08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. ® Pace Analytical Services,LLC aceAnalyica! 9800 KinceyAve. Suite 100 www.pacelahs.com Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-2 Lab ID: 92552615002 Collected: 07/30/21 09:30 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed Y CAS Na. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 08/06/21 01:45 0g 5.0 1 08/06/21 01:45 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 01:45 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 01:45 91-20-3 Styrene <1.0 ug/L 1.0 1 1,1,7,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 30-20-6 6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 79 08/06/21 01:45 9-34-5 Tetrachloroethene4 <1.0 ug/L 1.0 1 08/06/21 01:45 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 01:45 108-88-3 1,2,3-Trich)orobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 1,1,1-Trichloroethane <1.0 ug/L 08/06/21 01:45 120-82-1 g 1.0 1 08/06/21 01:45 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 Trichiaraethene 08/06/21 01:45 79-00-5 <1.0 ug/L 1.0 1 08/06/21 01:45 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 1,2,3-Trichloropropane <1.0 ug/L 08/06/21 01:45 96- 9 1.0 1 08/06/21 01:45 96-18-4 8-4 Vinyl acetate <2.0 ug/L 2.0 1 Vinyl chloride < 08/06/21 01:45 108-05-4 1.0 ug/L 1.0 1 08/06/21 01:45 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 m&p-Xylene < 08/06/21 01:45 1330-20-7 2.0 ug/L 2.0 1 08/06/21 01:45 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 Surrogates 08/06/21 01:45 95-47-6 4-Bromofluorobenzene(S) 101 % 70-130 1 1,2-Dichloroethane-d4(5) 100 /0 08/06/21 01:45 460-00-4 ° 70-130 1 08/06/21 01:45 17060-07-0 Toluene-d8(S) 100 % 70-130 1 08/06/21 01:45 2037-26-5 2540C Total Dissolved Solids Analytical Method:SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 177 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate 3.5 mg/L 0.040 1 07/31/21 13:45 14797-55-8 Nitrogen,Nitrite <0.040 mg/L 0.040 1 07/31/21 13:45 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 43 SUBMIT FORM ON 1QW PAPER ONLY '�t °RESC3URC � 'OEPI Q ' Mail original�� � ,s�'^ i eR��€1�DC S5N,' .: -�kF . ,�� Ind1copy „ r3 GROUNDWATER QUALITY MONITORING: irat;on Date: 6/30I2022 COMPLIANCE REPORT FORM P1easePrirrtcrssrrYorrYpe PERMiTNuntbeWQ0005$09 UIC FA ilityN IAIFDR ColoN Greensboro Junction WINTP Non-Discharge Facility Name: Colonial Pipeline Company NPDI<s over Permit Name(if different): -TYPE OF PERMITTED OPERATION BEING MONITOREDFac;lity Address: 4'i 1 Galiimore Dairy Road - County Guilford ❑ Lagoon 0 Remediation:Infiltration Gallery (slr�t} NC 27409 0 Remediation: Greensboro ❑ Spray Field (sty} (state} MO ®Land Application of Sludge Contact Person: Brian Smith Telepl�ane#: 336-931-6027 0 Rotary Distributor No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other. Well Loc t;onJs;te Name:Upgradien$of d frnmasrmIt) If WELL WAS SAMPLING INORMATION -3 Date sample collected:713©I2021 FIELD ANALYSES, .�8.3 aC DRY at WELL ID NUMBER(from Permit): pH oo4b0: :9 units Temp.000lc: Mhos time of d0.30 R. Well Diameter: 2 in. sampling, D Well Depth: Screened Interval: ft. to Spec.Cond.00094:0.€}OB0 µ 15.62 ft.below measuring point Dods: fVone check Measuringep to Water Levelsz546: Relative M.P.Elevation: ft cheek Point is — ft.above land surface Appearance Giear lbailed before sampling: 8 gallons Volume of water pumped NO and field acidified: ®YES ©NC] Samples for metals were collected unfiltered: in YES ❑ Certification No. 12�, LABORATORY 1NFORMATIDN Laboratory Name: Pace Laboratory Date sample analyzed:8l6l2I}2'l ugr� PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. mglL Pb-Lead 01051 <5.0 COD 0033s mgfL Nitrite(NO2)as N 00615 mglL _Zinc 01092 CO.01 mg/L. /100mL Nitrate(NO3)as N 00620 0.45 Caliform:MF Fecal 31616mg/L. MF Total 31504 1100mL Phosphorus:Total as P 00665 7U507 mg jt Other(Specify Compounds and Concentration Units): (Note:Use AAPN method for highly turbid samples) Orthophosphate Orthophosphate Al-Aluminum 011Y}5 m�- mg/Lu�t Total Xytene- <1.0 ug1L Dissolved SorpH(Lab)al C 0o__ units Ba-Barium 01007 pH a04m Ca-Calcium 00916 m9� TOC cum mg�- mglt Cd-Cadmium 01027 G1-0 ug1L Chloride 0094o !L ug,2 Chromium:Total 01034 ug ORGANICS:(by GC,GC/MS,HPLC) Arsenic 00552 Cu-Copper 01042 m� mglt uglt (Specify test and method#.ATTACH LAB REPORT.) Grease and Oils 00552. Fe-iron o1045 ■ Yes(1) 0 No(0) Phenol 32730 ug/L ug!L Lab Report Attached? ❑ mglL Hg-Mercury 71900 method# 8260D Sulfate 00945 mgtL VOC 7a73 µMhos K-Potassium oa9s7. mglL ,method# Specific andmmonia 00610 mg/L Mg-Magnesium 00927 ,method# Total Ammonia 00610 ug/L Mn-Manganese 01055 ,method# - {Ammonia Nitrogen,Nl{y as N;Ammonia Nitrogen.Tofsl) u�fL mglL Ni-Nickel 01oe7 TICN as N 00625 mgll. VOC Removal9� mg1L Effluent Total VOCs: Systems Only{Attach Lab Deports}: Influent Total VACS: _ - approved methods of analysis by a o�� For Rernediatron Syst ,accurate,and complete,and that the laboratory analytical data was produced using possibility of fines and imprisonment for knowing violations. t r certify that,to the best of my knowledge and belief,the inforrnatiori submitted m this report is true MR-certified laboratory. I am aware that there are significant penalties for submitting false informaticr,including the p y ` (Date) Brian Smith 5iat� 'errn;ttee(or uthorizad Ag Permitter(or Authorized Agent)Name and Title-Please print or type GW-59 Rev.06-07-2018 Ace AnalyticalePace Analytical Services,LLC 9800 Kincey Ave. Suite 100 1-luntersville,WC 28078 (704)875-9092 wompacalabs,cam ANALYTICAL RESULTS Project: CPC Greensboro 216623 07130121 11:20 Matrix:Water Received: Qua1 Pace Project No.: 02562615 CAS No. Lab ID: 92552615044 Collected: 07I30121 10:2 prepared Analyzed ��--� te: MIN-3 Report Limit DP ~�` 5amp Units �� -� Results Parameters .��- Preparation Method:EPA 200.7 Rev 4.4 199 Analytical Method:EPA 200,7 Rev 4.4 1994 Prep 0 08104121 18:25 7440-43-9 200.7 MET tCP Pace Analytical Services-Asheville 1.0 1 0$104121 02:00<1.0 uglL 5.0 1 08104121 02:00 OSl04121 18:25 7440-47-3 ug/L 08/04121 02:00 8/041 1 18:25 5 74 1 Cadmium <5.0 g 5.0 1 <5.0 uglL 10.0 1 0810412102:00 0810412118:25 7440-66-6 Chromiumug1L Lead <10.0 Zinc Analytical Method:EPA B260D p81D6121 02:21 67-64 1 826pp MS)/Low Level Pace Analytical Services-Charlotte 25 0 1 uglL 1 08106/21 02121 71 43 2 <25.0 1.0 08106121 02:21 108 66 1 <1 A uglL 1.0 1 • Acetone ug/L 08106121 02:21 74 97 5 Benzene <1.4 1.0 1 08106l21 02:21 75-27-4 <1.0 uglL 1.0 1 F3romobenzene08106121 02:21 75-25-2 Bromo form methane <1.0 ug1L 1.0 1 08/06/21 02:21 74-83-9 v2 Brom Bromadichlaromefharfe a10 uglL 2.0 1 08/06/21 02:21 73-93-3 Bramoform <2.0 ug1L 5.0 1 081p612102:21 56-23-5 Carbone trs <5.0 uglL 1.0 1 08/06/21 02:21 108-90-7 <1.0 ug/L 1.0 1 allot none(MEK) 08106121 0221 00 3 1 <1.o uglL 1.0 1 Carbon tetrachloride ug/L p8106121 02:21 67-66-3 Ch Chloroform or zsne <7.01.0 1 08/06/21 02:21 674- 6-3 <1.0 uglt 1.0 1 K Chloroet etha ug/L 08I06121 02:21 95 49 8 Chloroform <1.01.0 1 08106121 02:216-49-106-43-4 <1.0 ug/L 1.0 1 4 0h1 methaee ug/L 08106I21 02:2121 96-22-Chlorotoluene e1.0 2.0 1 08106121 02:21 124 48 1 <2.08 ug/L 10 1 DibromOcluene ro one 08l06I21 02:21 106 93 <1.0 uglL 1.0 1 1,2-Dibromo-3-chlorop p uglL D8106121 02:21 74-95-3 Dibrom meth methane <1.0 1.0 1 08/06/21 02:21 95-54-1 <1.0 ug/L 1.0 1 1,,2-Dic lorobe one(EDB) ug/L 081061 02 21 .5 -60-11 Dibromometizane <1.0 1.0 1 08106121 02:21 106 46-7 t1.0 ug/L 1.0 1 Dichlorodifl 1,2A bhliorobe zen ug1L 08106121 02:21 106 46 1,3-Dichloraberizene d1.D 1.0 1 48106121 02:21 75-34-3 <1.0 uglL 1.0 1 1,4-Dichlo oath ne ug/L 08/06/21 02:21 1D7 06 2 1,2-D chioruetomethane <1.01.0 1 0810621 07-06- 8 <7.0 ug/L 1.0 1 1,1-Dich loroethen uglL D8106121 02:21 156 5 4 1,2-Dichioroethane <1.0 1.0 1 08106l2102:21 156-60-5 cis- 2 1,1-1,2-Diroeths th <1.0 uglL 1 p 1 08106I21 02:21 7 trans -Dichlor0eth the <1.0 ug/L 1.0 1 8106121 0221 I42-2 5 trans 1,2j0 opropaneene <1.0 uglL 1.0 1 08106121 02:21 594-20-7 <1.0 -9 uglt 1.0 1 1 2-Dichloo propa0ug/L 08/06/21 0221 94-20 7 1,3-Dichlor0Propen <1.01. 1.0 1 08106121 02:21 503 68-6 5 <1.0 ug/L 1.0 1 cis-1,chloroioropr a 08106I21 10061 02- 1,1-Dichl-0ichIpene <1.0 ug1L 1 0 1 08/06/21 02121 02:21 108-20-3 6 a1.0 ug/L 1.0 1 Dlisopro yl a etherropene ug/L p8106121 100 41 4 Ethylbenzachioropropene <1,p 1.0 1 08/06/21 02:21 02:21 00-4 3 ro i <1.0ug/L L 2.0 1 Diisop Pyug/L 08l0612142:21 591-78-6 Ethylbenzene <2.05.0 1 08106121 02:212 99 87-6 pH sopropylt ,3 butadiene <5.0 ug/L 1.0 1 2-Nexanone <1.4 uglL p-lsopropyltoluene REPORT OF LABORATORY ANALYSIS Page 14 of This report shall not be reproduced,except In full, without the written consent of Pace Analytical Services,LLC. (I Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersviile,NC 28078 www.pacelabs.eem (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: N!W-3 Lab ID: 92552615004 Collected: 07/30/21 10:20 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 02:21 75-09-2 4-Methyl-2-pentanone(MiBK) <5.0 ug/L 5.0 1 08/06/21 02:21 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 02:21 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 02:21 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 02:21 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 02:21 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 79-00-5 Trichioroethene <1.0 ug/L 1.0 1 08/06/21 02:21 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 02:21 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 02:21 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 02:21 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 02:21 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 02:21 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 02:21 95-47-6 Surrogates 4-Bromofluorobenzene(S) 100 °/a 70-130 1 08/06/21 02:21 460-00-4 1,2-Dichloroethane-d4(S) 98 % 70-130 1 08/06/21 02:21 17060-07-0 Toluene-d8(S) 99 % 70-130 1 08/06/21 02:21 2037-26-5 2540C Total Dissolved Solids Analytical Method:SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 363 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2INO3 unpres Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Nitrate 0.45 mg/L 0.040 1 07/31/21 13:50 14797-55-8 Nitrogen,Nitrite <0.040 mg/L 0.040 1 07/31/21 13:50 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 43 SUBMIT FORM ON YELLOW PAPER ONLY Mail original •EP,ARVi! OFz v11z:ONN1Ei3T° QUALITY ADIY6.oFWA RESO`6tltCEs0 GROUNDWATER QUALITY MONITORING: i FORNIAVCI Ro ssi U I -z and 1 copy to: c r �,. 1n xs % COMPLIANCE REPORT FORM ^ Al 4 c=C NrE, ra .Gri cl7699r •a FACILITY INFORMATION Reese Print Clearly sr Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 UIC Permit Name(If different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (s'mt) NC 27409 county Guilford ❑ Lagoon ❑Remediation:Infiltration Gallery (City) (State) OP) ❑ Spray Field 0 Remediation: Contact Person: Brian Smith Telephone#:336-931-6027 0 Rotary Distributor ®Land Application of Sludge Well Location/Site Name:Downgradient of Field No.of wells to be sampled: 6 0 Water Source Heat Pump 0 Other: Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-4 (MW-135) Date sample collected: 7/3012021 FIELD ANALYSES: WAS Well Depth: 29.9 ft. Weil Diameter: 2 in. phi 00400:5.7. units Temp.noon: . °C DRY at Depth to Water Level 82549:19•89 ft.below measuring point Screened Interval: ft. to _fit. Spec.Cond.00094:0.0054 µMhos time of sampling, Measuring Point is ft_above land surface Relative M.P.Elevation: ft. Odor 000s5: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: MI YES ❑ NO and field acidified: RI YES 0 NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mglL Nitrite(NO2)as N o0615 mg/L Pb-Lead o1051 <5.0 ug/L Coliform:MF Fecal 31616 /100mL Nitrate(NO3)as N oo620 <0.040 rrig/L Zn-Zinc 01092 0.0139 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 83.0 mg/L Al-Aluminum 01105 ma Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00016 <1.0 mg/L Chloride 00940 mglL Cd-Cadmium 01027<5.0 uglL Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 uglL Fe-Iron o1045 uglL (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L lig-Mercury 71900 ug1L Lab Report Attached? ial Yes(1) ❑ No(0) Specific Conductance 00095 p:Mhos K-Potassium 00937 mg/L VOC 7873 ,method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH4 as N;Ammonia Nitrogen,Totsi) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that to the best of my knowledge and belief the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a D1n1R-certified laboratory. !am aware that there are significant penalties for submitting false information,including the possibility of fines and Imprisonment for knowing violations. Brian Smith - f 1 Zi Permittee(or Authorized Agent)Name and Title-Please print ortype Sig of Permittee(or Authorized Agent) `' (Date) GW-59 Rev.05-07-2018 Pace Analytical Services,LLG 0800 Kincey Ave. Suite 100 Muntersville,NC 28078 ® (704)875-9092 AceAnalytical wv+w,pacelabe.com ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 W-135 Lab ID: 92552615005 Collected: 07/30/21 10:00 Received: 07/30/21 11:20 Matrix:WS ter Qual Sample: MW4{M } Prepared Analyzed �No� Units R DF ��_ r Results .�-epartLlmit ---- Parameters Analytical Method:EPA 200.7 Rev .41994 Preparation Method:EPA 200.7 Rev 4.4199 200.7 MET ICP 4 Pace Analytical Services-Asheele Cadmium <5 0 ug1L 5.0 1 1.0 1 08104121 02:00 08ID4I2118:28 7440-43-9 <1.0 ug/L 06104I21 02:00 08104121 18:28 7440-47-3 Lead 5,0 1 08104l21 02:00 0810412118:28 7439-92-1 Chromium <5.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:28 7440-66-6 d 3,g uglL Zinc 13. Level Analytical Method:EPA 8260D 82600 MSV Low Pace Analytical Services-Charlotte 08/06/21 02:39 67-64-1 <25.0 ug/L 25.0 1 08/0621 02:39 61-64-1 Acetone <1.0 ug/L 1.0 1 08/06/21 02:39 1-43-21 Benzene <1.0 ugIL 1.0 1 08106/2102:39 108-86- BromOChlOr m <1.0 ug/L 1.0 1 08/06/21 02:39 75-27-4495 Bromodh Moro tetha <1.0 uglL 1.0 1 08/06/21 02:39 75-25-2 Bromoform romethane <7 0 ug/L 1.0 1 08/06/21 02:39 75-23-9 v2 Bromome <2.0 uglL 2.0 1 08/06/21 02:39 78-83-3 2 Sutanone(MEK) <5.0 uglL 5.0 1 08/06/21 02:39 56-23-5 Carbon none <1.0 ug/L 1.0 1 08/06/21 02:39 56235 Carbon tetrachloride ugh.. 1.0 1 08/06/21 02:39 108-90-775-00-3 lK <1.0 1.0 Chlorobenzene <1.0 uglL 08/06/21 02:39 67-66-3 Chloroform <I.0 ug/L 1.0 1 08/06/21 02:39 -86-3 Chloroform ug/L 1.0 1 08/06/21 02:39 75-87-3 <7.0 1.0 1 Chloromethane <1.0 uglL 08/06/21 02:39 106-43-4 8 2-Chlorotoluene <7 0 ug/L 1.0 1 08/06121 02:39 -4-Chlorotoluene2.0 1 08/06/21 02:39 6-12-81 <2.0 ug/L 1.0 1 D2-Dmochlor-chloropropane <1.0 ug/L 1 0 1 08/06/21/ 02:39 1 4- 8-1 4 1,2 D1 r0moethane(E <1.0 ug/L 0806121 02:39 106-93- E bromomethane (EDB} <1.0 ug/L 1.0 1 08106121 02:39 974- 5-3 l,2 Di omethane <1.0 ug/L 1.0 1 08106121 02:39 5-50 1 1,2 Dichlorabenzene <1.0 ug/L 1.0 1 08/06/21 02:39 541- 3-7 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 10 -46- Dlchl rodi0u rom0th <1.0 ug/L 1.0 1 08/06121 02:39 75-71-8 1,1-Dic lor0ethanehane <7 0 ug/L 1.0 1 08106/21 02:39 15 75-34-3 2 1,1-Dichl0r ethane <1.0 ug/L 1.0 1 08I06121 02:39 107-06- 1,2-DichloraetheI <1.0 ugiL 1.0 1 08/06/21 02:39 75 35 4 -2 1,1-1,2 Di hlortene <1.0 ug/L 1.0 1 08106I21 02:39 59 trans-1,2 Dichl roethe <1.0 ugiL 1.0 1 08/06121 02:39 156-60-55 trans c loropropan here <1.0 ug/L 1.0 1 08/06121 02:39 78 87 5 1,2-Dichloropropane <1.0 uglL 1.0 1 0810612102:39 14289 1,3-Dichloropropane <1.0 ug/L 1.0 1 0810612102:39 594-20-75 - -6 2,2-Dichloropropene <1 0 uglL 1.0 1 08106121 02:39 563 58-6 1,1-1,3- ch10r pane <1.0 ug/L 1.0 1 08I06121 02:39 10061-02-65 trans 1,3-DIc ropropene <1.0 ug/L 1.0 1 08/06/21 02:39 10 Dijsopropyl ether ropropene <1.0 uglL 1.0 1 08/06/21 02:39 820-3 Ethyl ropyl ether <1.0 ug/L 1.0 1 08/06/21 02:39 100-41-413 Ethylbenzene <2.0 ug/L 2.0 1 08106/21 02:39 87 683 2H Hexan ro 1,3 butadiene <5.0 uglL 5.0 1 08/06/21 02:39 591-78-69917'6 2-Hexanone <1.0 ug/L 1.0 1 p-lsopropyltoluene REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Page 16 of 43 ,,...,..nRlnRI9021 03:53 PM without the written consent of Pace Analytical Services,LLC. ( ® Pace Analytical Services,LLC _AaaceAnalytical 9800 Kincey Ave. Suite 100 www.pacefahs.com Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-4(MW 135) Lab ID: 92552615005 Collected: 07/30/21 10:00 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared p P Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 02:39 70-09-2 4-Methyl-2-pentanone(MIRK) <5.0 ug/L 5.0 1 08/06/21 02:39 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 Naphthalene <1.0 ug/L 08/06/21 02:39 1634-04-4 Styrene g 1.0 1 08/06/21 02:39 91-20-3 <1.0 uglL 1.0 1 08/06/21 02:39 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 1,1,2,2-Tetrachloroethane 08/0612102:39 630-20-6 <1.0 ug/L 1.0 1 08/06/21 02:39 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 Toluene 08106/21 02:39 127-18-4 <1.0 ug/L 1.0 1 08/06/21 02:39 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 1,2,4-Trichlorobenzene 08/0612102:39 87-61-6 <1.0 ug/L 1.0 1 08/06/21 02:39 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 1,1,2-Trichloroethane 081D6/2102:39 71-55-6 <1.0 ug/L 1.0 1 08/06/21 02:39 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 Trichlorofluoromethane 0810612102:39 79-01-6 <1.0 uglL 1.0 1 08/06/21 02:39 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 Vinyl acetate < 08/46/21 02:39 96-18-4 2.0 ug/L 2.0 1 08/06/21 02:39 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 - XylyTotal) < 08/06/21 02:39 75-01-4 1.0 ug/L 1.0 1 08/06/21 02:39 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 o-Xylene 08106/21 02:39 179601-23-1 Surrogates <1.0 ug/L 1.0 1 08/06/21 02:39 95-47-6 4-Bromofluorobenzene(S) 101 % 70-130 1 1,2-Dichloroethane-d4(S) 100 °/n 70-130 1 08/06/21 02:39 460-00-4 08/06/21 02:39 17060-07-0 Toluene-d8(S) 100 % 70-130 1 08/06/21 02:39 2037-26-5 2540C Total Dissolved Solids Analytical Method:SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 83.0 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2/NO3 unpres Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Nitrate <0.040 mg/L 0.040 1 Nitrogen,Nitrite 07/31/21 13:46 14797-55-8 0.056 mg/L 0.040 1 07/31/21 13:46 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 43 SUBMIT FORM ON YELLOW PAPER ONLY Mail original >="P �,M,6 I O P RO MENT UA7ITY RIViGOVATEI.RESOURCES„,�1. GROUNDWATER QUALITY MONITORING: and 1 co to: , NiSTIO P4ROC SING u�N A ak-a6 , COMPLIANCE REPORT FORM copy g;IMA IP.- R;c ce TER43,11_ N-'2V-W,i,s 7 ,` rh 4 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WVVTF Non-Discharge WQ0005809 Inc Permit Name(if different): - NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (street) NC 27409 County Guilford 0 Lagoon ❑Remediation:infiltration Gallery (cityl (state) (z'rR). - ❑ Spray Field ❑Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 El Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Upgradient of Field No.of wells to be sampled: 6 0 Water Source Heat Pump 0 Other: (from Permits SAMPLING INFORMATION if WELL WELL ID NUMBER(from Permit): 183 Date sample collected: 8/2/2021 FIELD ANALYSES; WAS 25.2 -- - 1$ 9 DRY at Well Depth: ft. Well Diameter: 2 in. pH 00400: 5-5 units Temp.(mow: °c Depth to Water Level 82546:8.76 ft.below measuring point Screened Interval: ft. to_ft. Spec_Cond_00094:0.0129 µMhos time°f sampling, Measuring Point is ft_above land surface Relative RP_Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 8 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: 0 YES ❑NO and field acidified: 0 YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No, 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2 as N 00s15 mg/L Pb-Lead 01051 <5.0 ug/L Coliform:MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 0.19 mg/L Zn-Zinc o1092<0.01 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concenti alien Units): Dissolved Solids:Total 70300 75.0 mg/L Al-Aluminum of io5 mg/L Total Xylene- <1.0 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L TOC 00630 mg/L Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027<1.0 uglL Arsenic 01002 ug/L Chromium:Total 01034<5.0 ug1L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ■❑ Yes(1) 0 No(0) Specific Conductance 00095 Mhos K-Potassium 00937 mg/L VOC 7873 ,method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L method# (Ammonia IYirogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese moss ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01087 ugh ,method# For Remediation Systems Only(Attach Lab Reports): ' Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I catty that,to the best of no,knowledge and belief,the informatinn submitted in this report is true,accurate,and complete,and that the laboratory ana1v cal data was produced using approved methods of analysis by a DV:R-cerified laboratory, I arc aware that there are eignificant penalties for submitting false intormatio^,including the possibility of fines anc imprisonment for:;rror;ing v€orations- ! Brian Smith "�1--�,� AIM' 11111 1( ?i 2-1 Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date) GW-59 Rev.06-07 2018 (ir Pace Analytical Services,LLC e 9800 KinceyAve. Suite 100 7,PceAnaIyticaI Huntersville,NC 28078 www pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08/02/21 10:30 Received: 08/02/21 12:55 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 2540C Total Dissolved Solids Analytical Method:SM 2540C-2011 Pace Analytical Services-Eden Total Dissolved Solids 75.0 mg/L 25.0 1 08/04/21 17:51 200.7 MET ICP. Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.41994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/05/21 13:40 08/06/21 01:23 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/05/21 13:40 08/06/21 01:23 7440-47-3 Lead . <5.0 ug/L 5.0 1 08/05/21 13:40 08/06/21 01:23 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/05/21 13:40 08/06/21 01:23 7440-66-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 uglL 25.0 1 08/10/21 11:40 67-64-1 Benzene <1.0 uglL 1.0 1 08/10/21 11:40 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/10/21 11:40 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/10/21 11:40 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/10/21 11:40 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/10/21 11:40 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-00-3 Chloroform <1.0 ug/L 1.0 1 08/10/21 11:40 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 74-87-3 v2 2-Chlorotoluene <1.0 ug/L 1.0 1 08/10/21 11:40 95-49-8 4-Chlorotoluene <1.0 uglL 1.0 1 08/10/21 11:40 106-43-4 1,2-Dibromo-3-chloropropane <2.0 uglL 2.0 1 08/10/21 11:40 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/10/21 11:40 106-93-4 Dibromomethane <1,0 uglL 1.0 1 08/10/21 11:40 74-95-3 1,2-Dichlorobenzene <1.0 uglL 1.0 1 08/10/21 11:40 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 156-59-2 trans-1,2-Dichloroethene <1,0 ug/L 1.0 1 08/10/21 11:40 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 142-28-9 2,2-Dichloropropane <1.0 uglL 1.0 1 08/10/21 11:40 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 10061-02-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC, Page 4 of 23 (Ir Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ® Huntersville,NC 28078 ace Analytical (704)875-9092 www.paceYa6s.cam ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08(02/21 10:30 Received: 08/02121 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. (Dual_ 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte <1.0 ug/L 1.0 1 08/10/21 11:40 108-20-3 D Ethylbenz ether <1.0 ug/L 1.0 1 08/10/21 11:40 100-41-4 Ethylbenzene 11:4 2.0 1 08/10/210 87-68-3IK <2.0 uglL 081021 11:40 7 Hexachlora 1,3 butadiene <5.0 ug/L 5.0 1 78-6 2-Hexanone1.0 1 08/10/21 11:40 99-87-6 p_ (toluene <1.0 ug/L 08/10/21 11:40 99-87-6 I t yle e <5.0 uglL 5.0 1 Methylene Chloride 5.0 1 08/10/21 11:40 108-10-1 4-Methyl-2-pentanane(MIBK) <5.0 uglL 08/10/21 11:40 108-10 1 -4 <1.0 ug/L 1.0 1 Na h Chalet butyl ether 1 0 1 08/10/21 11:40 91-20-3 Naphthalene <1.0 ug/L 08/10/21 11:40 100-42-5 <1.0 ug/L 1.0 1 Styrene 1.0 1 08/10/21 11:40 630-20-6 <1.0 uglL 08/10/21 11:40 5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 1,1,2,2-Tetrachlaroethane1,0 1 08/10/21 11:40 127-18-4 <1.0 ug/L 081021 11:40 108-88-32714 Toluen oroethene <1.0 ug/L 1.0 1 Toluene 1.0 1 08/10/21 11:40 87-61-6 <1.0 ug/L 08/10/21 11:40 87-61-6120-82-1 l,2,3-Trichlorobenzene <i 0 uglL 1.0 1 1,2,4-Trichlorobenzene 1.0 1 08/10/21 11:40 71-55-6 <1.0 ug/L08/10/21/ 11:40 79-00-516 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 TrichiTrichloroethane1.0 1 08/10/21 11:40 79-01-6 <1.0 ug/L08/10/21 11:40 75-69-4 Trichlorofuoro <1.0 ug/L 1.0 1 Trichlorofluoromethane 1 0 1 08110I21 11:40 96-18-4 <1.0 ug/L 08/10/21 11:40 96 18 4 1 Vinyl acetateopropane <2.0 ug/L 2.0 1 -4 1 0 1 08/10/21 11:40 75-01-4 Vinyl chloride <1.0 uglL 08110121 11:40 1330-20-7 <1.0 uglL 1.0 1 Xylene(Total)m&p-Xylene 2.0 1 08/10/21 11:40 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 <2.0 ug1L 08/10/21 11:40 95-47-6 Surrogates 70-130 1 08/10/21 11:40 46D 00 4 102 % 081021 11:40 46060-4 0 l,2 Dicofluoethane-d4 (S) 106 ova 70-130 1 Toluene-d8 (S) d4(S) 97 % 70-130 1 08/10/21 11:40 2037-26-5 Toluene-d8(S) MBIO 92221)Fecal Coliform RAL Analytical Method:SM 9222D-2006 Preparation Method:SM 9222D-2006 Pace Analytical Services-Raleigh Fecal Coliforms ND CFU/100 mL 1.0 1 08/02/21 14:48 08/03/21 15:41 350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia <0.10 mg/L 0.10 1 08/06/21 11:55 7664-41-7 353.2 Nitrogen,NO21NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Nitrate 0.19 mg/L 0.040 1 08/04/21 01:41 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Page 5 of 23 Date:08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. ( ® Pace Analytical Services,LLC aceAnalytical 9800 KinceyAve. Suite 100 www.pacela6s.cam F tuntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08/02/21 10:30 Received: 08/02/21 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared P Analyzed CAS No. Qual 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus <0.050 mg/L 0.050 1 08/04/21 18:46 08/04/21 23:01 7723-14-0 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 15.3 mg/L 1.0 1 48/09/21 09:54 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC, Page 6 of 23 GW-59A COMPLIANCE REPORT FORM Permit# W00005809 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due.(DECEMBER 31,2021)Wilt this monitoring report(GW-59 and GW-59A) YES NO be submitted after the established due date? 1 2 Was any required information missing on the GW-59 report forms? YES NO fF the answer to question I or 2 is'YES"list in the spate provided below the well Idenlification number(s)and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance(damnged casing,unlocked or missing cap,missing identification YES NO plate,area overgrown,etc.)?Iflhe answer is'Yes',contact the Regional(*cep guidance. Some wells need locks and nrnteetive cosines. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is WO',skip to section 8, If the answer to question 4 is"YES"list the effected wells individually with constituent(s)and concentrations) exceeding standards in the space provided below: pH for all monitor wells sampled was below the range of 6.5-8.5 SU. r ti 5 For the constituents identified in question 4 above,have standards been exceeded previously for the same [ YES) NO constituent(s)In the same well(s)in the last two years? ` lithe answer to question 5 is'NO skip to section 8. If the answer to question 5 is"YES",list in the space provided below,each welt with constituent(')exceeding standards,concentration(s)reported,and sample collection date for each occurrence(for the last two years). All MW's had a pH less than 6.5 SU In previous sampling events. 6 Are the monitoring wells listed in section 5located at or beyond the review boundary? YES NOS if the answer Is"YES",a groundwater quality problem may be occurring.CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is"NO",monitoring wells may be improperly located;contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YE NO quality problem? If the answer to question 7is'YES',describe those actions in the space provided below. If the answer to question 7 is"NO",contact the Regional Office within 90 days;an evaluation may be required to determine the Impact the waste disposal system Is having at the review and compliance boundaries surrounding this facility.Failure to do so may subject the permittee to a Notice of Violation, fines,andlorpenaltfes. 8 The person completing this portion(GW59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59.form. I hereby acknowledge that the above information was evaluated and the Information submitted in this report (Compliant o�-59A1 is true and complete tot be v knowledge. 2_1 Li- Signature of Permit-tee(or Authorized Agent) Date SUBMIT FORM ON YELLOW.PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original Mil. io `eNYrRo,110= tr�4Aign�Di oI•i c_s arro Es cliT' } COMPLIANCE REPORT FORM and fi copy to: c � ( nitt.c t ciN '�i~ o ; ra FACILITY.INFORMATION Pleeee,PrintCleady:or Type. PERMIT Number:: Expiration Date; 6/30I202.2 Facility Name: Colonial Pipeline Company Greensboro Junction\NWTF Non=Discharge WQ0005809 UIC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) -NC 27409 Guilford- Infiltration-Gallery _ _.. _ ry County �❑ Lagoon �Remediation: Inf[Itration Galle (oti:> (were) Cep) ❑ Spray Field 0 Remediation: Contact Person: Brian Smith Telephone* 336-931-6027 ❑ Rotary Distributor W Land Application of Sludge Well Location/Site Name:Upgradient of Field No.of wells to be sampled: 6 ❑Water Source Heat Pump ❑Other (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW 1 Date sample collected: 11130/202/ FIELD ANALYSES: WAS Well Depth: 21.9 ft. Well Diameter: 2 in. pH 0o400f 5.8 units Temp.coon: 18.5 °C DRY at. Depth to Water Level szs4s:14.68 ft:below measuring point Screened Interval- ft. to ft. Spec.Cond.00094:401 KMhos time of sampling,. Measuring Point is _ ft.above land surface Relative M.P.Elevation: ft Odor woes: None check Volume of water pumped/bailed before sampling: 4 gallons Appearance, Clear here:® Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ,E YES 0 NO LABORATORY INFORMATION Date sample analyzed:12/1/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(N05).as N 00615 mg/L Pb-Lead'mom <5M ug/L Coliform:MF Fecal 31516 /100mL Nitrate(NO3)es N aos20 1.2 rnglL Zn-Zinc 01092 0,0453 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as'P 00666 mg/L (Notes User MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 271 mg/L Al-Aluminum 0iyos rngIL Total Xylene- <1.0 ug/L pH(Lab)00403 _ units Ba-Barium o1.007 ug/L TOG ooss0 mg/L Ca-Calcium 00915 mg/L Chloride 00840 mg/L Cd-Cadmium 01027<1-.0 ug/L. Arsenic a1o02 ug/L Chromium:Total 01034 7.8 ug/L Grease and Oils 00552 mg/L Cu-Copper o1042 mg/L ORGANICS:(by GC,GG/MS.HPLC) Phenol 327sa ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ■❑ Yes(1) 0 No(0) Specific Conductance moss ltMhos K-Potassium o0ss7 mg/L VOC 7873' .,Method# 8260D Total Ammonia met o mg/L Mg-Magnesium 00827 mg/L ,method# (Ammonia Nitrogen;NHaas N:Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L NI-Nickel o1o67 ug/L ,-method# For Remediation Systems Only(Attach Lab Reports): influent Total VOCS: mg/L EffltlentTotai'VOCs: mg/L VOC Removal% I Certify that,to the best of my knowledge and belief.the information submitted in this report is troe,accurate.and complete,and that the laboratory analytical data was produced using approved methods of analysis by a D'/ R-certitied laboratory, l am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment forknowing violations. Brian Smith '� J Permittee(or Authorized Agent)Name and Title-Please print ortype Signature of Permittee:(orAuthorized Agent) (Date) GW-59 Rev.06-07-2018 Pace Analytical Services,LLC (__°)I-3/aceAnalytical to 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacolads,com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-1 Lab ID: 92574763001 Collected: 11/30/21 08:15 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 271 mglL 25.0 1 12/01/21 15:18 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 1.2 mg/L 0.040 1 12/01/21 10:13 14797-55-8 MBIO 9222D Fecal Coliform EON Analytical Method: SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms <1.0 CFU/100 mL 1.0 1 11/30/21 15:17 12/01/21 16:12 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4,4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 12/02/21 17:38 12/03/21 17:01 7440-43-9 Chromium 7.8 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:01 7440-47-3 Lead <5.0 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:01 7439-92-1 Zinc 45.3 uglL 10.0 1 12/02/21 17:38 12/03/21 17:01 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 12/04/21 04:04 67-64-1 Benzene <1.0 ug/L 1.0 1 12/04/21 04:04 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 12/04/21 04:04 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 12/04/21 04:04 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 12/04/21 04:04 75-27-4 Bromoform <1.0 ug/L 1.0 1 12/04/21 04:04 75-25-2 Bromomethane <2.0 ug/L 2.0 1 12/04/21 04:04 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 12/04/21 04:04 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 12/04/21 04:04 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 12/04/21 04:04 108-90-7 Chloroethane <1.0 uglL 1.0 1 12/04/21 04:04 75-00-3 Chloroform <1.0 ug/L 1.0 1 12/04/21 04:04 67-66-3 Chloromethane <1.0 ug/L 1.0 1 12/04/21 04:04 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 12/04/21 04:04 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 12/04/21 04:04 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 12/04/21 04:04 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 12/04/21 04:04 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 12/04/21 04:04 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 12/04/21 04:04 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 12/04/21 04:04 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 12/04/21 04:04 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 12/04/21 04:04 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 12/04/21 04:04 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 12/04/21 04:04 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 12/04/21 04:04 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 12/04/21 04:04 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 59 (lir Pace Analytical Services,LLC (ceAnalytical®® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-0092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-1 Lab ID: 92574763001 Collected: 11/30/21 08;15 Received: 11I30121 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 12/04/21 04:04 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 12/04/21 04:04 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:04 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:04 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:04 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 12/04/21 04:04 563-58-6 cis-1,3-Dichloropropene <1.0 ugiL 1.0 1 12/04/21 04:04 10061-01-5 trans-1,3-Dichloropropene <1.0 uglL 1.0 1 12/04/21 04:04 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 12/04/21 04:04 108-20-3 Ethylbenzene <1.0 ugfL 1.0 1 12/04/21 04:04 100-41-4 Hexachloro-1,3-butadiene <2.0 ugfL 2.0 1 12/04/21 04:04 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 12/04/21 04:04 591-78-6 p-Isopropyltoluene <1.0 ug/L 1.0 1 12/04/21 04:04 99-87-6 Methylene Chloride <5.0 uglL 5.0 1 12/04/21 04:04 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 12/04/21 04:04 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 12/04/21 04:04 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 12/04/21 04:04 91-20-3 Styrene <1.0 uglL 1.0 1 12/04/21 04:04 100-42-5 1,1,1,2-Tetrachloroethane <1.0 uglL 1.0 1 12/04/21 04:04 630-20-6 1,1,2,2-Tetrachloroethane <1.0 uglL 1.0 1 12/04/21 04:04 79-34-5 Tetrachloroethene <1.0 uglL 1.0 1 12/04/21 04:04 127-18-4 Toluene <1.0 ugiL 1.0 1 12/04/21 04:04 108-88-3 1,2,3-Trichlorobenzene <1.0 uglL 1.0 1 12/04/21 04:04 87-61-6 1,2,4-Trichlorobenzene <1.0 uglL 1.0 1 12/04/21 04:04 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 12/04/21 04:04 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 12/04/21 04:04 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 12/04/21 04:04 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 12/04/21 04:04 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 12/04/21 04:04 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 12/04/21 04:04 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 12/04/21 04:04 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 12/04/21 04:04 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 12/04/21 04:04 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 12/04/21 04:04 95-47-6 Surrogates 4-Bromofluorobenzene(5) 103 % 70-130 1 12/04/21 04:04 460-00-4 1,2-Dichloroethane-d4(S) 105 % 70-130 1 12/04/21 04:04 17060-07-0 Toluene-d8(S) 103 % 70-130 1 12/04/21 04:04 2037-26-5 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia <0.10 mg/L 0.10 1 12/03/21 10:53 7664-41-7 365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 0.25 mgfL 0.050 1 12/03/21 19:33 12/03/21 22:42 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 59 Pace Analytical Services,LLC aceAnalytical® 9800 KinceyAve, Suite 17 Huntersville,NC 28078 www,pacelabs.cam (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-1 Lab ID: 92574763001 Collected: 11/30/21 08:15 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 11.8 mg/L 1.0 1 12/06/21 09:54 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 59 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non Discharge WQQ006609 UIC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery (cltyt (State) PP) ❑ Spray Field ❑ Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Upgradient of Field No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): M W 2 Date sample collected: 11/30/2021 FIELD ANALYSES: WAS 1 Well Depth: 25.5 ft. Well Diameter: 2 in. pH 00400: 5.6 units Temp.o00ta: 1$• °G DRY at time of Depth to Water Level 82546: 10.70 ft.below measuring point Screened Interval: 18 ft. to 23 ft. Spec.Cond.000s4:220 µMhos sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00065: None check Volume of water pumped/bailed before sampling: 3.5 gallons Appearance Clear here:(--I Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: ❑■ YES ❑NO f I LABORATORY INFORMATION Date sample analyzed:12/1/2021 _ Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 3.1 mg/L Zn-Zinc olos2 <0.01 mg/L Coliform: MF Total 31504 f100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method tor highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): )issolved Solids:Total 70300 168 mg/L Al-Aluminum o1105 mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium cm007 uglL TOO 00680 mg/L Ca-Calcium 00916 mglL Chloride oos40 mglL Cd-Cadmium 01027 <1.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 <5.0 ug!L Grease and Oils 00552 mg/L Cu-Copper 01042 mglL ORGANICS:(by GC, GC/MS, HPLC) Phenol 32730 uglL Fe-Iron 01045 uglL (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mglL Hg-Mercury 71900 uglL Lab Report Attached? CI Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L , method#t (Ammonia Nitrogen;NI1,as N',Ammonia Nitrogen,Total) Mn-Manganese of o55 ug/L , method# TKN as N o0sz5 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: _mg/L VOC Removal% I certify that to the nest of my knowledge and belief the information submitted in this report is true accurate and complete and that the laboratory analytcal data was produced using approved methods of analysis by a UWR-certified laboratory. I am aware that there are significant penalties for submitting false information including the possibility of fines and imprisonment for knowing violations Brian Smith _~ 00r z r 4f zz Permittee(or Authorized Agent)Name and Title-Please print or type Sig nat ermittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 (W Pace Analytical Services,LLC __ P ® 9fioo Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 2807B www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-2 Lab ID: 92574763002 Collected: 11/30/21 08:30 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 168 mg1L 25.0 1 12/01/21 15:18 353.2 N021NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 3.1 mg/L 0.040 1 12/01/21 10:16 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms <1.0 CFU/100 mL 1.0 1 11/30/21 15:17 12/01/21 16:12 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method: EPA200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 uglL 1.0 1 12/02/21 17:38 12/03/21 17:05 7440-43-9 Chromium <5.0 uglL 5.0 1 12/02/21 17:38 12/03/21 17:05 7440-47-3 Lead <5.0 uglL 5.0 1 12/02/21 17:38 12/03/21 17:05 7439-92-1 Zinc <10.0 uglL 10.0 1 12/02/21 17:38 12/03/21 17:05 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 uglL 25.0 1 12/04/21 04:22 67-64-1 Benzene <1.0 ug/L 1.0 1 12/04/21 04:22 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 12/04/21 04:22 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 12/04/21 04:22 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 12/04/21 04:22 75-27-4 Bromoform <1.0 ug/L 1.0 1 12/04/21 04:22 75-25-2 Bromomethane <2.0 ug/L 2.0 1 12/04/21 04:22 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 12/04/21 04:22 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 12/04/21 04:22 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 12/04121 04:22 108-90-7 Chloroethane <1.0 ug/L 1.0 1 12/04/21 04:22 75-00-3 Chloroform <1.0 ug/L 1.0 1 12/04/21 04:22 67-66-3 Chloromethane <1.0 ug/L 1.0 1 12/04/21 04:22 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 12/04/21 04:22 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 12/04121 04:22 106-43-4 1,2-Dibromo-3-chloropropane <2.0 uglL 2.0 1 12/04/21 04:22 96-12-8 Dibromochloromethane <1.0 uglL 1.0 1 12/04/21 04:22 124-48-1 1,2-Dibromoethane(EDB) <1.0 uglL 1.0 1 12/04/21 04:22 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 12/04/21 04:22 74-95-3 1,2-Dichlorobenzene <1.0 uglL 1.0 1 12/04/21 04:22 95-50-1 1,3-Dichlorobenzene <1.0 uglL 1.0 1 12/04/21 04:22 541-73-1 1,4-Dichlorobenzene <1.0 uglL 1.0 1 12/04/21 04:22 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 12/04/21 04:22 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 12/04/21 04:22 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 12104/21 04:22 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 12/04/21 04:22 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 59 Pace Analytical Services,LLC (. .1/ 9800 KinceyAve. Suite 100 eeAnaly rca! Huntersville,NC 28078 www.pacolabs.cum (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No,: 92574763 Sample: MW-2 Lab ID: 92574763002 Collected: 11/30/21 08:30 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte cis-1,2-Dichloroethene <1.0 uglL 1.0 1 12/04/21 04:22 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 12/04/21 04:22 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:22 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:22 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 12/04/21 04:22 594-20-7 1,1-Dichloropropene <1.0 uglL 1.0 1 12/04/21 04:22 563-58-6 cis-1,3-Dichloropropene <1.0 uglL 1.0 1 12/04/21 04:22 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 12/04/21 04:22 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 12/04/21 04:22 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 12/04/21 04:22 100-41-4 Hexachloro-1,3-butadiene <2.0 ug1L 2.0 1 12/04/21 04:22 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 12/04/21 04:22 591-78-6 p-Isopropyltoluene <1.0 ug/L 1.0 1 12/04/21 04:22 99-87-6 Methylene Chloride <5.0 ug/L 5.0 1 12/04/21 04:22 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 12/04/21 04:22 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 12/04/21 04:22 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 12/04/21 04:22 91-20-3 Styrene <1.0 ug/L 1.0 1 12/04/21 04:22 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 12/04/21 04:22 630-20-6 1,1,2,2-Tetrachloroethane <1.0 uglL 1.0 1 12/04/21 04:22 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 12/04/21 04:22 127-18-4 Toluene <1.0 uglL 1.0 1 12/04/21 04:22 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 12/04/21 04:22 87-61-6 1,2,4-Trichlorobenzene <1,0 ug/L 1.0 1 12/04/21 04:22 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 12/04/21 04:22 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 12/04/21 04:22 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 12/04/21 04:22 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 12/04/21 04:22 75-69-4 1,2,3-Trichloroprapane <1.0 ug/L 1.0 1 12/04/21 04:22 96-18-4 Vinyl acetate <2.0 ug/L 2,0 1 12/04/21 04:22 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 12/04/21 04:22 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 12/04/21 04:22 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 12/04/21 04:22 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 12/04/21 04:22 95-47-6 Surrogates 4-Bromofluorobenzene(S) 103 % 70-130 1 12/04/21 04:22 460-00-4 1,2-Dichloroethane-d4(S) 108 % 70-130 1 12/04/21 04:22 17060-07-0 Toluene-d8(5) 102 % 70-130 1 12/04/21 04:22 2037-26-5 350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia <0.10 mg/L 0.10 1 12/03/21 11:00 7664-41-7 365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus <0.050 mg/L 0.050 1 12/03/21 19:33 12/03/21 22:43 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 59 Pace Analytical Services,LLC __ 13 aceAnalytical® 9800 Kincey Ave. Suite 100 Hunteraville,NC 28078 www.pacelabs.cem (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No: 92574763 Sample: MW-2 Lab ID: 92574763002 Collected: 11/30/21 08:30 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limlt DF Prepared Analyzed CAS No. Qual 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 38.1 mgiL 1.0 1 12/06/21 09:56 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 59 SUBMIT FORM ON YELLOW PAPER ONLY Mail original balp!nit r Wst ilR NNIEEtgr '.99, 1Y�"oF rATP zesovRCEs GROUNDWATER QUALITY MONITORING: I oRi IONIP�iocEssl Hula 1: 4 x COMPLIANCE REPORT FORM and copy to: .,,- sir sEf c,c rG. rAst FACILITY INFORMATION please Print Clearly or Type PERMIT Number: Expiration Data: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge W00005809 ufc Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (steal) NC 27409 county Guilfbrd in Lagoon ©Remediation:Infiltration Gallery <Cily) prate} MO , ❑ Spray Field ❑Remediation: Contact Person: Brian Smith Telephone#: 336-931-8027 ❑ Rotary Distributor l Land Application of Sludge Well LocationlSite Name:Upgradient of Field No.of wells to be sampled: 6 ❑.Water Source Heat Pump ❑Other: (from Perm%) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-3 Date sample collected: 11/30/2021 FIELD ANALYSES: WAS Well Depth: 40.30 ft. Well Diameter. 2 in. pH 00400; 6.1 units Temp.Dario_ 17..5'0c DRY at Depth to Water Level 62545:17.69 ft,below measuring point Screened Interval: ft to ft. Spec,Cond.no09I:72 pMhos time of sampling, Measuring Point is ft.above land surface Relative M.P.Elevation: ft. Odor moss: None check. Volume of water pumped/bailed before sampling: 8.0 gallons Appearance: Clear here:i f Samples for metals were collected unfiltered: ID YES ❑ NO and field acidified: ®.YES ❑NO u LABORATORY INFORMATION Date sample analyzed`12/1/202'1 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100rnL Nitrate(NO3)as N 00620 <0.040 mg/L Zn-Zinc ata92<0.01 mglL Coliform:MF Total 31594 /100mL Phosphorus:Total'as P ooass mg/L (Note Use nnant.method for highly turbid sues) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): ?Dissolved Solids:Total 70300 85.0 mg/L Al-Aluminum auras mglL pH(Lab)aoaos units Ba-Barium o1007 ugli,. Total.Xylene- <1.0 ug/L TOG Doss° mg/L Ca-Calcium loots mg/L Chloride 00940 mg/L Cd-Cadmium.ol027<1.0 uglL Arsenic a1002 ug/L Chromium;Total n1034 <6.0 ug/L Grease and Oils 00552 mg/L Cu-Copper.01042 mglL ORGANICS:.(by GC,GC/MS, I-IPLC) Phenol 327so uglL Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-.Mercury 71900 ug/L Lab Report Attached? ❑■ Yes(1) ❑ No(0) Specific Conductance 0009s pMhoe K-Potassium 00937 mg/L VOC 7873 , method it 8260D Total Ammonia coat o mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NHgas N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel.of 057 uglL ,method# ' For Remediation Systems Only(Attach Lab Reports): lrifinentTo'tal VOCs:, mg/L Effluent TbtalVOCS mg/L VOG Removal% I certify that,Io the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,site that the facoratory analyt cal data was produced using approved methods of analysis by a [MR-certified laboratory I am aware that there are significant penalties for suomitting false information,including the possibility of`Ines and impnsonnfent;;or knowing violations. Brian Smith ,- Z/ L ) Z "` Permittee(or Authored Agent)Name and Title-Please print or type Signatur-. ittee(or Authorized Agent) (Date) GW-58 Rev.€06-07-2018 (1111- Pace Analytical Services,LLC aceAnalytical__ F ® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacalabs,com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-3 Lab ID: 92574763009 Collected: 11/30/21 09:35 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 85.0 mg/L 25.0 1 12/01/21 15:19 353.2 N021NO3 unpres EI]N Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen, Nitrate <0.040 mg/L 0.040 1 12/01/21 10:25 14797-55-8 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method:EPA200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 12/02/21 17:38 12103/21 17:19 7440-43-9 Chromium <5.0 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:19 7440-47-3 Lead <5.0 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:19 7439-92-1 Zinc <10.0 ug/L 10.0 1 12/02/21 17:38 12/03/21 17:19 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 12/03/21 16:51 67-64-1 Benzene <1.0 ug/L 1.0 1 12/03/21 16:51 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 12/03/21 16:51 74-97-5 Bromodichloromethane <1,0 uglL 1.0 1 12/03/21 16:51 75-27-4 Bromoform <1,0 uglL 1.0 1 12/03/21 16:51 75-25-2 Bromomethane <2.0 ugiL 2.0 1 12/03/21 16:51 74-83-9 2-Butanone(MEK) <5.0 uglL 5.0 1 12/03/21 16:51 78-93-3 Carbon tetrachloride <1,0 uglL 1.0 1 12/03/21 16:51 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 108-90-7 Chloroethane <1.0 ug/L 1.0 1 12/03121 16:51 75-00-3 Chloroform <1.0 ug/L 1.0 1 12/03/21 16:51 67-66-3 Chloromethane <1.0 uglL 1.0 1 12/03/21 16:51 74-87-3 2-Chlorotoluene <1.0 ugiL 1.0 1 12/03/21 16:51 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 12103/21 16:51 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 12103/21 16:51 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 12/03/21 16:51 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 12/03/21 16:51 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 12/03/21 16:51 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 12/03/21 16:51 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 16:51 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 16:51 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 12/03/21 16:51 75-35-4 cis-1,2-Dichloroethene <1,0 ug/L 1.0 1 12/03/21 16:51 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 12/03/21 16:51 156-60-5 1,2-Dichloropropane <1.0 uglL 1.0 1 12/03/21 16:51 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 16:51 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 59 (.' Pace Analytical Services,LLC _ ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-3 Lab ID: 92574763009 Collected: 11/30/21 09:35 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte 2,2-Dichlorapropane <1.0 ug/L 1.0 1 12/03/21 16:51 594-20-7 1,1-Dichlorapropene <1.0 ug/L 1.0 1 12/03/21 16;51 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 12/03/21 16:51 10061-01-5 trans-1,3-Dichloropropene <1,0 ug/L 1.0 1 12/03/21 16:51 10061-02-6 Diisopropyl ether <1.0 ug1L 1.0 1 12/03/21 16:51 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 12/03/21 16;51 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 12/03/21 16:51 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 12/03/21 16:51 591-78-6 p-Isopropyltoluene <1.0 ug/L 1.0 1 12/03/21 16:51 99-87-6 Methylene Chloride <5.0 ugh. 5.0 1 12/03/21 16:51 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 12/03/21 16:51 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 12/03/21 16:51 1634-04-4 Naphthalene 1.3 ug/L 1.0 1 12/03/21 16:51 91-20-3 Styrene <1.0 ug/L 1.0 1 12/03/21 16:51 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 12/03/21 16:51 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 12/03/21 16:51 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 12/03/21 16:51 127-18-4 Toluene <1.0 ug/L 1.0 1 12/03/21 16:51 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:51 120-82-1 1,1,1-Trichlaroethane <1.0 ug/L 1.0 1 12/03/21 16:51 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 12/03/21 16:51 79-00-5 Trichloraethene <1.0 ug/L 1.0 1 12/03/21 16:51 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 12/03/21 16:51 75-69-4 1,2,3-Trichlaropropane <1.0 ug/L 1.0 1 12/03/21 16:51 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 12/03/21 16:51 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 12/03/21 16:51 75-01-4 Xylene(Total) <1.0 ug/L 1,0 1 12/03/21 16:51 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 12/03/21 16:51 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 12/03/21 16:51 95-47-6 Surrogates 4-Bromofluorobenzene(S) 105 % 70-130 1 12/03/21 16:51 460-00-4 1,2-Dichloroethane-d4(S) 97 % 70-130 1 12/03/21 16:51 17060-07-0 Toluene-d8(S) 100 % 70-130 1 12/03/21 16:51 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 28 of 59 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: and I Col?y to INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 2769E-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 ulc Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 County Guilford - ❑ Lagoon ❑ Remediation: Infiltration Gallery (clly) (Stare) (zip) ❑ Spray Field ❑ Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Downgradient of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-4 (MW-1 35) Date sample collected: 11/30/2021 FIELD ANALYSES: WAS Well Depth: 29.9 ft. Well Diameter: 2 in. pH 00a0o: 6.4 units Temp.mom 14.9 °C DRY at Mhos time of Depth to Water Level 62545:22.06 ft. below measuring point Screened Interval: ft. to _ft. Spec.Cond. 00094: 57 11 sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 4-0 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: l]YES ❑ NO and field acidified: l]YES ❑ NO LABORATORY INFORMATION Date sample analyzed:12/1/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00515 mg/L Pb-Lead o1051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 0.39 mg/L Zn-Zinc 01092 0.0115 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P oases mg/L (Note: UseMPN method for highly turbid simples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 78.0 mg/L Al-Aluminum o11os mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium ot0o7 ug!L TOC ooseo mg/L Ca-Calcium 00916 <1.0 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 6.1 uglL Arsenic 01002 ug/L Chromium:Total 01034 uglL Grease and Oils 00552 rng/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron at045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? © Yes(1) ❑ No(0) Specific Conductance 00095 ftMhos K-Potassium 00937 mg/L VOC 7673 method# 8260D Total Ammonia onto mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen;NN3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01087 ug!L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true accurate,and complete,and that the laboratory analytcal data was produced using approved methods of analysis by a DWR-certi@ed laboratory. I am aware that there are significant penalties for submitting false information,including Ire possibility of fines and imprisonment for knowing violations. Brian Smith l 219 f ZZ---- Perrnittee(or Authorized Agent)Name and Title-Please print or type Signature of ee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 Pace Analytical Services,LLC 7P'aceAnaIyticaI(___----Pil � 9800Kuntarsvlle,NC1 te 100 t 28078 www,pacelabs.cam (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-4 Lab ID: 92574763010 Collected: 11/30/21 09:20 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 78,0 mg/L 25.0 1 12/01/21 15:19 353.2 NO21NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 0.39 mg1L 0.040 1 12/01/21 10:21 14797-55-8 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200,7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 uglL 1.0 1 12/42/21 17:38 12/03/21 17:23 7440-43-9 Chromium 6.1 uglL 5.0 1 12/02/21 17:38 12/03/21 17:23 7440-47-3 Lead <5.0 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:23 7439-92-1 Zinc 11.5 ug/L 10.0 1 12/02/21 17:38 12/03/21 17:23 7440-66-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 12/03/21 17:08 67-64-1 Benzene <1.0 ug/L 1.0 1 12/03/21 17:08 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 12/03/21 17:08 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 12/03/21 17:08 75-27-4 Bromoform <1.0 ug/L 1.0 1 12/03/21 17:08 75-25-2 Bromomethane <2.0 ug/L 2.0 1 12/03/21 17:08 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 12/03/21 17:08 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 12/03/21 17:08 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 108-90-7 Chloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 75-00-3 Chloroform <1.0 ug/L 1.0 1 12/03/21 17:08 67-66-3 Chloromethane <1,0 ug/L 1.0 1 12/03/21 17:08 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 12/03/21 17:08 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 12/03/21 17:08 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 12/03/21 17:08 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 12/03/21 17:08 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 12/03/21 17:08 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 12/03/21 17:08 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 12/03/21 17:08 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 12/03/21 17:08 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 12/03/21 17:08 156-59-2 trans-1,2-Dichloroethene <1.0 uglL 1.0 1 12/03/21 17:08 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 17:08 78-87-5 • 1,3-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 17:08 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 29 of 59 Pace Analytical Services,LLC 9800 Klncey Ave. Sulte 100 (Sr_,Pace Analytical') Huntersville,NC 28078 wmpacelabs.com {704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: Mw-4 Lab ID: 92674763010 Collected: 11/30/21 09:20 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte 2,2-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 17:08 594-20-7 1,1-Dichloropropene <1.0 uglL 1.0 1 12/03/21 17:08 563-58-6 cis-1,3-Dichloropropene <1.0 uglL 1.0 1 12/03/21 17:08 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 12/03/21 17:08 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 12/03/21 17:08 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 12/03/21 17:08 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 12/03/21 17:08 87-68-3 2-Hexanane <5.0 ug/L 5.0 1 12/03/21 17:08 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 12/03/21 17:08 99-87-6 Methylene Chloride <5.0 ug/L 5.0 1 12/03/21 17:08 75-09-2 4-Methyl-2-pentanone(MIRK) <5.0 ug/L 5.0 1 12/03/21 17:08 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 12/03/21 17:08 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 12/03/21 17:08 91-20-3 Styrene <1.0 ug/L 1.0 1 12/03/21 17:08 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 12/03/21 17:08 127-18-4 Toluene <1.0 ug/L 1.0 1 12/03/21 17:08 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 87-61-6 1,2,4Trichlorobenzene <1.0 ug/L 1.0 1 12/03/21 17:08 120-82-1 1,1,1:crichloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 71-55-6 1,1,2 Trichloroethane <1.0 ug/L 1.0 1 12/03/21 17:08 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 12/03/21 17:08 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 12/03/21 17:08 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 12/03/21 17:08 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 12/03/21 17:08 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 12/03/21 17:08 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 12/03/21 17:08 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 12/03/21 17:08 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 12/03/21 17:08 95-47-6 Surrogates 4-Bromofluorobenzene(S) 103 % 70-130 1 12/03/21 17:08 460-00-4 1,2-Dichloroethane-d4(S) 104 % 70-130 1 12/03/21 17:08 17060-07-0 Toluene-d8(S) 101 % 70-130 1 12/03/21 17:08 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 30 of 59 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: and 1 co tO: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 ulc_ Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (struts NC 27409 County Guilford ❑ Lagoon Li Remediation:Infiltration Gallery (C. ) (stele) tzip) ❑ Spray Field ❑ Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor 0 Land Application of Sludge Well Location/Site Name:Upgradient of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): 183 Date sample collected: 11/30/2021 FIELD ANALYSES: WAS Well Depth: 252 ft. Well Diameter: 2 in. pH 00400: 55.0 units Temp.0om1o: 1 8.7 °C DRY at time of Depth to Water Level 82546:14.72 ft.below measuring point Screened Interval: ft. to _ft. Spec. Cond. oo094: 98 pMhos sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor moss. None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:(— Samples for metals were collected unfiltered: l■�. YES ❑ NO and field acidified: ❑■ YES ❑NO I I LABORATORY INFORMATION Date sample analyzed:12/1/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead oio51 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 0062a <0.040 mg/L Zn-Zinc 01092 <0.01 rng/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 53.0 mg/L Al-Aluminum altos mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium ot007 ug/L TOC ease° mglL Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 <5.0 ug/L Grease and Oils oos52 mglL Cu-Copper 01042 mglL ORGANICS:(by GC, GC/MS, HPLC) Phenol 32730_ ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 7100 ugIL Lab Report Attached? ❑M Yes(1) ❑ No(0) Specific Conductance 000s5 µMhos K-Potassium 00937 mg/L VOC 7673 method# 8260D _ Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen;NH,asN;Ammonia Nitrogen,Total) Mn-Manganese lot 055 ugll_ , method# TKN as N 00625 mg/L Ni-Nickel 01 067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is tree.accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware That there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.Brian Smith / 2 Jf127 Permittee(or Authorized Agent)Name end Title-Please print or type Signature or Permittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 (W Pace Analytical Services,LLC Kincey Ave, aceAnalytrcal® 9800 te 100 Hunte sOle,C1280778 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-183 Lab ID: 92574763007 Collected: 11/30/21 09:30 Received: 11/3D/21 13:20 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 53.0 mg/L 25.0 1 12/01/21 15:18 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate <0.040 mg/L 0.040 1 12/01/21 10:24 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method:SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms <1.0 CFU/100 mL 1.0 1 11/30/21 16:19 12/01/21 16:12 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 12/02/21 17:38 12/03/21 17:12 7440-43-9 Chromium <5.0 ug/L 5.0 1 12/02/21 17:38 12/03/21 17:12 7440-47-3 Lead <5.0 ug1L 5.0 1 12/02/21 17:38 12/03/21 17:12 7439-92-1 Zinc <10.0 ug/L 10.0 1 12/02/21 17:38 12/03/21 17:12 7440-66-6 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 12/03/21 16:15 67-64-1 Benzene <1.0 ug/L 1.0 1 12/03/21 16:15 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 12/03/21 16:16 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 12/03/21 16:15 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 12/03/21 16:15 75-27-4 Bromoform <1.0 ug/L 1.0 1 12/03/21 16:15 75-25-2 Bromomethane <2.0 ug/L 2.0 1 12/03/21 16:15 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 12/03/21 16:15 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 12/03/21 16:15 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:15 108-90-7 Chloroethane <1.0 uglL 1.0 1 12/03/21 16:15 75-00-3 Chloroform <1.0 uglL 1.0 1 12/03/21 16:15 67-66-3 Chloromethane <1.0 ug/L 1.0 1 12/03/21 16:15 74-87-3 2-Chlorotoluene <1,0 ug/L 1.0 1 12/03/21 16:15 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 12/03/21 16:15 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 12/03/21 16:15 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 12/03/21 16:15 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 12/03/21 16:15 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 12/03/21 16:15 74-95-3 1,2-Dichlorobenzene <1.0 uglL 1.0 1 12/03/21 16:15 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:15 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:15 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 12/03/21 16:15 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 16:15 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 12/03/21 16:15 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 12/03/21 16:15 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 59 Pace Analytical Services,LLC (1::PiceAnaIy icaI® 9800 Kincey Ave, Suite 100 www.pacelabs.com Nuntersviile,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No,: 92574763 Sample: MW-183 Lab ID: 92574763007 Collected: 11/30/21 09:30 Received: 11/30/21 13:20 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method:EPA 8260D Pace Analytical Services-Charlotte cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 12103/21 16:15 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1,0 1 12/03/21 16:15 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 16:15 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 16:15 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 12/03/21 16:15 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 12/03/21 16:15 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 12/03/21 16:15 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 12/03/21 16:15 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 12/03/21 16:15 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 12/03/21 16:15 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2,0 1 12/03/21 16:15 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 12/03/21 16:15 591-78-6 p-Isopropyltoluene <1.0 ug/L 1.0 1 12/03/21 16:15 99-87-6 Methylene Chloride <5.0 ug/L 5.0 1 12/03/21 16:15 75-09-2 4-Methyl-2-pentanone(MMBK) <5.0 ug/L 5.0 1 12/03/21 16:15 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 12/03/21 16:15 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 12/03/21 16:15 91-20-3 Styrene <1.0 ug/L 1.0 1 12/03/21 16:15 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 12103/21 16:15 630-20-6 1,1,2,2-Tetrachloroethane <1.0 uglL 1.0 1 12/03/21 16:15 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 12/03/21 16:15 127-18-4 Toluene <1.0 ug/L 1.0 1 12/03/21 16:15 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 12/03/21 16:15 87-61-6 1,2,4-Trichlorobenzene <1.0 uglL 1.0 1 12/03/21 16:15 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 12/03/21 16:15 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 12/03/21 16:15 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 12/03/21 16:15 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 12/03/21 16:15 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 12/03/21 16:15 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 12/03/21 16:15 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 12/03/21 16:15 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 12/03/21 16:15 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 12/03/21 16:15 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 12/03/21 16:15 95-47-6 Surrogates 4-Bromofluorobenzene(S) 94 % 70-130 1 12/03/21 16:15 460-00-4 1,2-Dichloroethane-d4(S) 101 % 70-130 1 12/03/21 16:15 17060-07-0 Toluene-d8(S) 104 % 70-130 1 12/03/21 16:15 2037-26-5 350.1 Ammonia • Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia <0.10 mg1L 0,10 1 12/03/21 11:07 7664-41-7 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus <0.050 mg/L 0.050 1 12/03/21 19:33 12/03/21 22:48 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 22 of 59 (IF Pace Analytical Services,LLC Kincey te 100 Ace Analytical® 9800Hunte sville,NC1280778 www.pacelabs.com {704)875-9092 ANALYTICAL RESULTS Project: CPC-Greensboro Junction Spray Pace Project No.: 92574763 Sample: MW-183 Lab ID: 92574763007 Collected: 11/30/21 09:30 Received: 11/30/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 14.7 mglL 1,0 1 12/06/21 10.03 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 12/08/2021 04:30 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 59