WQ0003698_Groundwater Monitoring Report November 2021_20211216

GW-59A COMPLIANCE REPORT FORM Permit # 1W Q 0003(dt8
(Submit one each monitoring period with GIV-59 jornte.)
I
Enter date monitoring results were due. (D86 21 I Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question t or 2 is "YES" list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Officefor guidance.
x
4
Are any monitored constituents equal to or above the established standards?
E
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
See. A+}ba��A
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO" skip to section 8. ff^^,
If the answer to question 5 is "YES", list in the space provided below, each well with constittak— i�t�eir
standards, concentration(s) date for the last two
repotted, and sample collection each occurrence (for years).
Sew A DEC 3.0 202
/
Q'Aia,WTtQ4
R'FO�MATIt�ar•,�,,r;;:cgl;
(31JIJI'�
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
x
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
e910W O--FFic� Coh4-ar-4ed
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
x
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be
refit uired to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the Permittee to a Notice of Violation
fines, and/or penalties.
1QAton2.1 Off.Rl Con{44:�
>
t
�
c
m �
-
g
The person completing this portion (GW-59A) of the monitoring report should sign below and sd mit this
form
with G W-59 forms for required wells to the address provided at the top of the cum nt GW-« l p}m.
146 gwledoethatthe: above information, ns.evaluated and the information submitted irk tt5�s
r
t ` , , t( Qfltplla ce•RSRoit GIN 59A) is true_and eo plate to the best of my knowledge.
_ I
r'
_
Signature f Permittee (or Authoriz A nt) Dated
GW-59A 12/8/2003

Question #4
LAB DATA WHICH EXCEEDS PERMIT
DATE
MONITORING WELL#
PARAMETER
REPORTED
DATA
11.30.21
1
PH
5.9
2
Ammonia
6.0 mg/L
Iron
28.4mg/L
Manganese
1080 ug/L
PH
6
3
Nitrate
12.1mg/L
Manganese
132 ug/L
PH
5
4
Manganese
119 ug/L
PH
5.1

QUESTION #5
LAB DATA WHICH EXCEEDS PERMIT FOR LAST 2 PREVIOUS YEARS
I'll 4Z*]11A411
DATE MW # PARAMETER DATA
5/9/2018
1
pH
5.9
2
Iron
6.8 mg/L
Manganese
642 ug/L
ph
6.3
3
Nitrate
25 mg/L
Iron
4.6 mg/L
Manganese
370 ug/L
4
Iron
3.3 mg/L
pH
4.9
11/12/2018
1
pH
5.9
2
Ammonia
6.2 mg/L
Iron
32 mg/L
Manganese
1300 ug/L
pH
6.3
3
Nitrate
34.6 mg/L
Iron
0.62 mg/L
Manganese
360 ug/I
4
Iron
5.1 mg/L
Manganese
130 ug/L
pH
4.9
5/13/2019
1
Iron
3.5 mg/L
Manganese
81 ug/L
pH
5.8
2
Ammonia
7.2 mg/L
Iron
36 mg/L
Manganese
960 ug/L
3
Nitrate
39 mg/L
Iron
2.5 mg/L
pH
4.6
4
Iron
15 mg/L
Manganese
120 ug/L
pH
4.9
11/20/2019
1
Iron
0.34 mg/L
pH
59
2
Ammonia
5.0 mg/L
Iron
17 mg/L
Manganese
1100 ug/L
3
Nitrate
39.2
Iron
2.3 mg/L
`�' Je-sIV t 0 ZU[1
Water O;jal;;y Reglcnal Operations
Asheville Regional Office

Manganese
5800 ug/L
pH
4.8
4
Iron
1.1 mg/L
Manganese
93 ug/L
pH
5.1
5/19-27/2020
1
Iron
0.34 mg/L
pH
5.2
2
Ammonia
6.7 mg/L
Iron
43 mg/L
Manganese
1360 ug/L
3
Nitrate
40.5 mg/L
Iron
0.5 mg/L
Manganese
1 573 irg/L
pH
4.7
4
Manganese
149 ug/L
pH
4.5
11/16/2020
1
Iron
0.691 mg/L
Manganese
50.6 ug/L
pH
6
2
Ammonia
5.6 mg/L
Iron
21.6 mg/L
Manganese
1490,ug/L
pH
6.4
3
Nitrate
32.1 mg/L
Iron
1.07 mg/L
Manganese
434 ug/L
pH
5
4
Manganese
127 ug/L
pH
5i1
5/18 & 6/1/2021
1
Iron
0.948,mg/L
pH
5,9
2
Ammonia
7.3 mg/L
Iron
39.5mg/L
Manganese
1060 ug/L
3
Nitrate
21.2mg/L
Iron
0.937mg/L
Manganese
265 ug/L
pH
4.9
4
Manganese
207 ug/L
pH
5
��j---
1 �
�. 1AN 1 n null
Water Qualay Rccponal Operations
Asheville Regional Office

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"' Analytical
www.pacelabe.com
i
December 14, 2021
Mr. Tim Horton
City of Marion
3982 NC Hwy 226 South
Marion, NC 28752
RE: Project: CITY OF MARION
Pace Project No.: 92574920
Dear Mr. Horton:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
��- JAN 10LU11
Water Quality Regional Operations
Asheville Regional Office
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

Analytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CITY OF MARION
Pace Project No.: 92574920
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cart. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CITY OF MARION
92574920
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92574920001
MWAR
EPA 200.7 Rev 4.41994
JOR
5
PASI-A
SM 6200B
SAS
63
PASI-C
SM 254OC-2015
MJP
1
PASI-A
SM 254OD-2015
MJP
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92574920002
MW-2
EPA 200.7 Rev 4.41994
JOR
5
PASI-A
SM 6200B
SAS
63
PASI-C
SM 254OC-2015
MJP
1
PASI-A
SM 254OD-2015
MJP
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353,2 Rev 2.0 1993
MFO
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 531 OB-2014
MDW
1
PASI-A
92574920003
MW-3
EPA 200.7 Rev 4.41994
JOR
5
PASI-A
SM 6200B
SAS
63
PASI-C
SM 2540C-2015
MJP
1
PASI-A
SM 254OD-2015
MJP
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92574920004
MW-4
EPA 200.7 Rev 4.41994
JOR
5
PASI-A
SM 6200B
SAS
63
PASI-C
SM 254OC-2015
MJP
1
PASI-A
SM 254OD-2015
MJP
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 531OB-2014
MDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 33

�va'u Analytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-1R
ANALYTICAL RESULTS
92674920001 Collected: 11/30/21 09:45 Received: 11/3012116:30 Matrix: Water
Parameters
Results
Units
PQL
DF
Prepared
Analyzed
CAS No.
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
12/14/21 16:30
Collected By
RMB
1
12/14/21 16:30
Collected Date
11/30/21
1
12/14/21 16:30
Collected Time
09:45
1
12/14/21 16:30
pH
5.9
Std. Units
1
12/14/21 16:30
Temperature
10.3
deg C
1
12/14/21 16:30
Static Water Level
24.32
feet
1
12/14/21 16:30
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
NO
ug/L
10.0
1
12/07/2101:52
12/09/21 19:23
7440-38-2
Cadmium
ND
ug/L
1.0
1
12107/2101:52
12/09/21 19:23
7440-43-9
Iron
71.6
ug/L
50.0
1
12/07/21 01:52
12109/2119:23
7439-89-6
Lead
NO
ug/L
5.0
1
12/07/21 01:52
12/09/21 19:23
7439-92-1
Manganese
10.6
ug/L
5.0
1
12/07/21 01:52
12/09/21 19:23
7439-96-5
6200E MSV
Analytical Method:
SM 6200B
Pace Analytical Services - Charlotte
Benzene
NO
ug/L
0.50
1
12/0912118:29
71-43-2
Bromobenzene
NO
ug/L
0.50
1
12109/2118:29
108-86-1
Bromochloromethane
NO
ug/L
0.50
1
12/09/21 18:29
74-97-5
Bromodichloromethane
NO
ug/L
0.50
1
12/09/21 18:29
75-27-4
Bromoform
ND
ug/L
0.50
1
1210912118:29
75-25-2
Bromomethane
NO
ug/L
5.0
1
1210912118:29
74-83-9
n-Butylbenzene
NO
ug/L
0.50
1
12/09/21 18:29
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
12109/2118:29
135-98-8
tert-Butylbenzene
NO
ug/L
0.50
1
12109/2118:29
98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
12/09/21 18:29
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
12/09/21 18:29
108-90-7
Chloroethane
NO
ug/L
1.0
1
12109/2118:29
75-00-3
Chloroform
NO
ug/L
0.50
1
12/09/21 18:29
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/09/21 18:29
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
12109/2118:29
95-49-8
4-Chlorotoluene
NO
ug/L
0.50
1
12109/2118:29
106-43-4
1,2-Dibromo-3chloropropane
NO
ug/L
1.0
1
12/09/21 18:29
96-12-8
Dibromochloromethane
NO
ug/L
0,50
1
12/09/21 18:29
124-48-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
12/09/21 18:29
106-93-4
Dibromomethane
NO
ug/L
0.50
1
12/09/21 18:29
74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
12/09/21 18:29
95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
1210912118:29
541-73-1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
12/09/21 18:29
106-46-7
Dichlorodifluoromethane
NO
ug/L
0.50
1
12/09/21 18:29
75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
12/09/21 18:29
75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
1
12/09/21 18:29
107-06-2
1,1-Dichloroethene
NO
ug/L
0.50
1
12/0912118:29
75-35-4
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -I-C. Page 4 of 33

® Pace Analytical Services, LLC
arc`Analytical 2225 Riverside Dr.
Asheville, NC
28804
www.pacele6s.com
[phone]-7176
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MWAR Lab ID: 92674920001 Collected: 11/30/2109:45 Received: 11/30/2116:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qua]
6200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
12/09/21 18:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
12/09/21 18:29
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
12/09/21 18:29
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
12/09/21 18:29
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
12/09/21 18:29
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
12/09/21 18:29
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
12/09/21 18:29
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
12109/2118:29
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
12/09/21 18:29
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
12/09/21 18:29
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
12109/2118:29
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
12/09/21 18:29
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
12/09/21 18:29
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
12/09/21 18:29
1634-04-4
Naphthalene
ND
ug/L
2.0
1
1210912118:29
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
12/09/21 18:29
103-65-1
Styrene
ND
ug/L
0.50
1
12/09/21 18:29
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
12/09/21 18:29
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
1210912118:29
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
12/09/21 18:29
127-18-4
Toluene
ND
ug/L
0.50
1
12/09/21 18:29
108-88-3
1,2,3-Tdchlorobenzene
ND
ug/L
2.0
1
12/09/21 18:29
87-61-6
1,2,4-Trichlorobenzene
NO
ug/L
2.0
1
12/09/21 18:29
120-82-1
1, 1. 1 -Trichloroethane
ND
ug/L
0.50
1
12109/2118:29
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
12/09/21 18:29
79-00-5
Trichloroethene
ND
ug/L
0.50
1
12/09/21 18:29
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12109/2118:29
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
12109/2118:29
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
12/09/21 18:29
95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
1
12/09/21 18:29
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
12/09/21 18:29
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
12/0912118:29
179601-23-1
o-Xylene
ND
ug/L
0.50
1
12/09/21 18:29
9547-6
Surrogates
1,2-Dichloroethaned4 (S)
108
%
70-130
1
12/09/21 18:29
17060-07-0
4-Bromofluorobenzene (S)
101
%
70-130
1
12/09/21 18:29
460-00-4
Toluene-d8 (S)
102
%
70-130
1
12/09/21 18:29
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical
Services -Asheville
Total Dissolved Solids
30.0
mg/L
25.0
1
12/06/21 12:13
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical
Services -Asheville
Total Suspended Solids 4.5 ni 2.6 1 12/06/21 10:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the wriuen consent of Pace Analytical Services, LLC. Page 5 of 33

� accAnalytica!®
www.pacelabsxom
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-1R
Lab ID: 92574920001 Collected: 11/30/2109:45
Received: 11/30/2116:30 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed CAS No, Qual
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
12/10/21 10:42 7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 3532 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.10 mg/L 0.040
1
12/01/21 01:12 14797-55-8
420.4 Phenolics, Total
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable
ND mg/L 0.020
1
12/07/21 10:38 12/07/21 15:06 64743-03-9
5310E TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
12/14/21 02:40 7440-44-0
Date: 12/14/2021 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 33

aceAnalytical
wwv.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-2
Lab ID: 92574920002 Collected:
11/30/21 13:00
Received: 11/30/21 16:30 Matrix: Water
Parameters
Results
Units PQL
OF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
12/14/21 16:31
Collected By
RMB
1
12/14/21 16:31
Collected Dale
11/30/21
1
12/14/21 16:31
Collected Time
13:00
1
12/14/21 16:31
pH
6.4
Std. Units
1
12/14/21 16:31
Temperature
17.2
deg C
1
12/14/21 16:31
Static Water Level
18.72
feet
1
12/14/21 16:31
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND
ug/L
10.0
1
12/07/2101:52
12/09/2119:27
7440-38-2
Cadmium
ND
ug/L
1.0
1
12107/2101:52
12109/2119:27
7440-43-9
Iron
28400
ug/L
50.0
1
12107/2101:52
12109/2119:27
7439-89-6
Lead
ND
ug/L
5.0
1
12/0712101:52
12/09/2119:27
7439-92-1
Manganese
1080
ug/L
5.0
1
12/0712101:52
12109/2119:27
7439-96-5
6200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
0.50
1
12/09/21 18:46
71-43-2
Bromobenzene
ND
ug/L
0.50
1
12/09/21 18:46
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
12109/2118:46
74-97-5
Bromodichloromethane
NO
ug/L
0.50
1
12109/2118:46
75-27-4
Bromoform
ND
ug/L
0.50
1
12/09/21 18:46
75-25-2
Bromomethane
ND
ug/L
5.0
1
12/09/21 18:46
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
12109/2118:46
104-51-8
sec-Butylbenzene
ND
ug/L
0.60
1
12/09/21 18:46
135-98-8
tert-Butylbenzene
NO
ug/L
0.50
1
12109/2118:46
98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
12/09/21 18:46
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
12/09/21 18:46
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/09/21 18:46
75-00-3
Chloroform
ND
ug/L
0.50
1
12109/2118:46
67-66-3
Chloromethane
NO
ug/L
1.0
1
12109/2118:46
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
12/09/21 18:46
9549-8
4-Chlorotoluene
ND
ug/L
0.50
1
12/09/21 18:46
10643-4
1,2-01bromo-3-chloropropane
ND
ug/L
1.0
1
12/09/21 18:46
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
12109/2118:46
12448-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
12/09/21 18:46
106-934
Dibromomethane
NO
ug/L
0.50
1
12109/2118:46
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
12109/2118:46
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
12109/2118:46
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
12109/2118:46
10646-7
Dichlorodifluoromethane
NO
ug/L
0.50
1
12/09/21 18:46
75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
12/09/21 18:46
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
12/09/21 18:46
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
12/09/21 18:46
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 33

W aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW2
6200B MSV
ANALYTICAL RESULTS
Lab ID: 92574920002 Collected: 11/30/21 13:00 Received: 11/30/21 16:30 Matrix: Water
Parameters Results Units
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropen e
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1. 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroelhene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Tri methylbenzene
1,3, 5-Tdmelhylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
2540D Total Suspended Solids
Total Suspended Solids
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
PQL DF Prepared Analyzed CAS No. Qual
NO
ug/L
0.50
1
12109/2118:46
156-59-2
NO
ug/L
0.50
1
12/09/21 18:46
156-60-5
ND
ug/L
0.50
1
12/09/21 18:46
78-87-5
NO
ug/L
0.50
1
12/09/21 18:46
142-28-9
NO
ug/L
0.50
1
1210912118:46
594-20-7
NO
ug/L
0.50
1
1210912118:46
563-58-6
NO
ug/L
0.50
1
12/09/21 18:46
10061-01-5
NO
ug/L
0.50
1
12/09/21 18:46
10061-02-6
NO
ug/L
0.50
1
12109/2118:46
108-20-3
NO
ug/L
0.50
1
12/0912118:46
100-414
NO
ug/L
2.0
1
12/09/21 18:46
87-68-3
NO
ug/L
0.50
1
12/09/21 18:46
98-82-8
NO
ug/L
2.0
1
12109/2118:46
75-09-2
NO
ug/L
0.50
1
1210912118:46
1634-04-4
ND
ug/L
2.0
1
12/0912118:46
91-20-3
NO
ug/L
0.50
1
12/09/21 18:46
103-65-1
ND
ug/L
0.50
1
12/09/21 18:46
10042-5
NO
ug/L
0.50
1
12/09/21 18:46
630-20-6
NO
ug/L
0.50
1
12/0912118:46
79-34-5
ND
ug/L
0.50
1
12/0912118:46
127-18-4
NO
ug/L
0.50
1
12/09/21 18:46
108-88-3
NO
ug/L
2.0
1
12/09/21 18:46
87-61-6
NO
ug/L
2.0
1
12109/2118:46
120-82-1
NO
ug/L
0.50
1
12/09/21 18:46
71-55-6
NO
ug/L
0.50
1
12/09/21 18:46
79-00-5
NO
ug/L
0.50
1
12/09/21 18:46
79-01-6
ND
ug/L
1.0
1
12109/2118:46
75-69-4
NO
ug/L
0.50
1
12109/2118:46
96-18-4
NO
ug/L
0.50
1
12/0912118:46
95-63-6
NO
ug/L
0.50
1
12/09/21 18:46
108-67-8
NO
ug/L
1.0
1
1210912118:46
75-01-4
NO
ug/L
1.0
1
12109/2118:46
179601-23-1
NO
ug/L
0.50
1
12/0912118:46
95-47-6
112
%
70-130
1
12/09/21 18:46
17060-07-0
101
%
70-130
1
12109/2118:46
460-00-4
102
%
70-130
1
12/09/21 18:46
2037-26-5
Analytical Method: SM 254OC-2015
Pace Analytical Services -Asheville
121 mg/L 25.0 1 12106/2112:13
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
35.7 mg/L 8.3 1 12/06/21 10:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-2
Lab ID: 92574920002 Collected: 11/30/21 13:00
Received: 11/30/21 16:30 Matrix: Water
Parameters
Results Units PQL DF
Prepared Analyzed CAS No. Qual
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
6.0 mg/L 0.10 1
12/10/21 10:43 766441-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040 1
12/01/21 01:30 14797-55-8
420.4 Phenolics, Total
Analytical Method: EPA420.4 Rev 1.0 1993 Preparation Method: EPA420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable
ND mg/L 0.020 1
12/07/21 10:38 12/07/21 15:11 64743-03-9
5310E TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
1.9 mg/L 1.0 1
12/14/21 02:59 7440-44-0
Date: 12/14/2021 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 33

aceAnalytical
www.pacelabf.cam
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-3
Parameters
ANALYTICAL RESULTS
Lab ID: 92574920003 Collected: 11/30/21 11:40 Received: 11/30/21 16:30 Matrix: Water
Results Units POL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
12/14/21 16:33
Collected By
RMB
1
12/14/21 16:33
Collected Date
11/30/21
1
12/14/21 16:33
Collected Time
11:40
1
12/14/21 16:33
pH
5.0
Std. Units
1
12/14/21 16:33
Temperature
13.9
deg C
1
12/14/21 16:33
Static Water Level
31.34
feel
1
12/14/21 16:33
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND
ug/L
10.0
1
12/07/21 01:52
12/09/21 19:37
7440-38-2
Cadmium
0.96.1
ug/L
1.0
1
12/07/2101:52
12/0912119:37
7440-43-9
Iron
246
ug/L
50.0
1
12/07/2101:52
12109/2119:37
7439-89-6
Lead
ND
ug/L
5.0
1
12/07/21 01:52
12/09/21 19:37
7439-92-1
Manganese
132
ug/L
5.0
1
12107/2101:52
12109/2119:37
7439-96-5
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
0.50
1
12109/2119:04
7143-2
Bromobenzene
NO
ug/L
0.50
1
12/09/21 19:04
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
12109/2119:04
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
12/09/21 19:04
75-27-4
Bromoform
ND
ug/L
0.50
1
12/09/21 19:04
75-25-2
Bromomethane
ND
ug/L
5.0
1
12109/2119:04
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
12/09/21 19:04
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
12/09/21 19:04
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
12109/2119:04
98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
12/09/21 19:04
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
12/0912119:04
108-90-7
Chloroelhane
ND
ug/L
1.0
1
12/09/21 19:04
75-00-3
Chloroform
ND
ug/L
0.50
1
12109/2119:04
67-66-3
Chloromethane
ND
ug/L
1.0
1
12109/2119:04
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
12/09/2119:04
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
12109/2119:04
106-43-4
1,2-Dibromo-3chloropropane
NO
ug/L
1.0
1
12/0912119:04
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
12/0912119:04
124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
0.50
1
12/09/21 19:04
106-93-4
Dibromomethane
ND
ug/L
0.50
1
12109/2119:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
12/09/21 19:04
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
12109/2119:04
541-73-1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
12/09/21 19:04
106-46-7
Dichlorodifluoromethane
NO
ug/L
0.50
1
12/09/21 19:04
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
12/09/21 19:04
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
12/09/21 19:04
107.06-2
1,1-Dichloroethane
ND
ug/L
0.50
1
12109/2119:04
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 33

(1*coAnalyticalt
www.pacelabs.cam
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-3 Lab ID: 92574920003 Collected: 11/30/21 11:40 Received: 11/30/21 16:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
cis-1,2-Dichloroelhene
ND
ug/L
0.50
1
12/09/21 19:04
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
12/09/21 19:04
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
12/09/21 19:04
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
12109/2119:04
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
12109/2119:04
594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
12/09/21 19:04
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
12/09/21 19:04
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
12/09/21 19:04
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
12/09/21 19:04
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
12/09/21 19:04
100-41-4
Hexachloro-1,3-buladiene
ND
ug/L
2.0
1
12/09/21 19:04
87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
12/09/21 19:04
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
12/09/21 19:04
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
12/09/21 19:04
1634-04-4
Naphthalene
ND
ug/L
2.0
1
12109/2119:04
91-20-3
n-Propylbenzene
NO
ug/L
0.50
1
12/09/21 19:04
103-65-1
Styrene
ND
ug/L
0.50
1
12/0912119:04
100412-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
12/09/21 19:04
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
12/09/21 19:04
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
12109/2119:04
127-18-4
Toluene
NO
ug/L
0.50
1
12/09/21 19:04
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
12/09/21 19:04
87-61-6
1,2,4-Trichlorobenzene
NO
ug/L
2.0
1
12/09/21 19:04
120-82-1
1,1,1-Trichloroelhane
ND
ug/L
0.50
1
12109/2119:04
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
12/0912119:04
79-00-5
Trichloroelhene
NO
ug/L
0.50
1
12/0912119:04
79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
1
12/09/21 19:04
75-69-4
1,2,3-Trichloropropane
NO
ug/L
0.50
1
12/09/21 19:04
96-18-4
1,2,4-Tdmethylbenzene
ND
ug/L
0.50
1
12109/2119:04
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
1210912119:04
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
12/09/21 19:04
75-01-4
m&p-Xylene
NO
ug/L
1.0
1
12/09/21 19:04
179601-23-1
o-Xylene
ND
ug/L
0.50
1
12109/2119:04
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
112
%
70-130
1
12/09/21 19:04
17060-07-0
4-Bromofluorobenzene (S)
101
a/
70-130
1
12/09/21 19:04
460-00-4
Toluene-d8 (S)
101
%
70-130
1
12/09/21 19:04
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical
Services -Asheville
Total Dissolved Solids
123
mg/L
25.0
1
12/06/21 12:13
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical
Services -Asheville
Total Suspended Solids
8.2
mg/L
2.5
1
12/06/21 10:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 33

' g6"nalytical e
ieww.pacelr6r.con
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-3
Parameters
Lab ID: 92574920003 Collected: 11/30/21 11:40
Results Units PQL DF
Received: 11/30/21 16:30 Matrix: Water
Prepared Analyzed CAS No. Qual
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
NO mg/L 0.10 1
12/10/21 10:45 7664-41-7
363.2 Nitrogen, NO2IN03 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
12.1 mg/L 0.40 10
12/01/21 01:50 14797-55-8
420.4 Phenolics, Total
Analytical Method: EPA420.4 Rev 1.0 1993 Preparation Method: EPA420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable
ND mg/L 0.020 1
12/07/21 10:38 12/07/21 15:13 64743-03-9
531013 TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
0.52J mg/L 1.0 1
12/14/21 03:17 744044-0
Date: 12/14/2021 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 33

j aceAnalytical
(f www.pacelabs.com
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-4
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92574920004 Collected: 11/30/21 14:10 Received: 11/30/21 16:30 Matrix: Water
Parameters
Results
Units
PQL
DF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
12/14/21 16:34
Collected By
RMB
1
12/14/21 16:34
Collected Dale
11/30/21
1
12/14/21 16:34
Collected Time
14:10
1
12/14/21 16:34
pH
5.1
Std. Units
1
12/14/21 16:34
Temperature
14.7
deg C
1
12/14/21 16:34
Static Water Level
20.16
feel
1
12/14/21 16:34
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND
ug/L
10.0
1
12/0712101:52
12/0912119:41
7440-38-2
Cadmium
NO
ug/L
1.0
1
12/07/2101:52
1210912119:41
7440-43-9
Iron
ND
ug/L
50.0
1
12107/2101:52
1210912119:41
7439-89-6
Lead
ND
ug/L
5.0
1
12/07/2101:52
12109/2119:41
7439-92-1
Manganese
119
ug/L
5.0
1
12/07/21 01:52
12/09/21 19:41
7439-96-5
8200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
0.50
1
12/09/21 19:22
71-43-2
Bromobenzene
ND
ug/L
0.50
1
12/09/21 19:22
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
12/0912119:22
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
12/09/21 19:22
75-27-4
Bromoform
ND
ug/L
0.50
1
1210912119:22
75-26-2
Bromomethane
ND
ug/L
5.0
1
12109/2119:22
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
12/09/21 19:22
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
12/09/21 19:22
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
12/09/21 19:22
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
12/09/21 19:22
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
12/09/21 19:22
108-90-7
Chloroethane
NO
ug/L
1.0
1
12109/2119:22
75-00-3
Chloroform
ND
ug/L
0.60
1
12109/2119:22
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/09/21 19:22
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
12/09/21 19:22
9549-8
4-Chlorotoluene
ND
ug/L
0.50
1
1210912119:22
10643-4
1,2-Dibromo-3chloropropane
ND
ug/L
1.0
1
12/09/21 19:22
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
12109/2119:22
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
12/09/21 19:22
106-93-4
Dibromomethane
ND
ug/L
0.50
1
12/09/21 19:22
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
12/09/21 19:22
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
12/0912119:22
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
1210912119:22
10646-7
Dichlorodinuoromethane
ND
ug/L
0.50
1
1210912119:22
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
12/09/21 19:22
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
12109/2119:22
107-06-2
1,1-Dichloroelhene
ND
ug/L
0.50
1
12109/2119:22
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 33

aceAnalytical
www.pacelebs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MWd Lab ID: 92574920004 Collected: 11/30/21 14:10 Received: 11/30/21 16:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
6200B MSV
cis-1,2-Dich lorcethene
trans-1,2-Dich lorcethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Telrachloroelhane
Tetrachloroethene
Toluene
1,2,3-Trlch lorobenzene
1,2,4-Tdchlorobenzene
1,1.1-Trichloroelhane
1,1,2-Trichloroethane
Trichloroethene
Trichloro0uoromethane
1,2,3-Trich loropropane
1,2,4-Trimethylbenzene
1,3, 5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-BromoOuorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
2540D Total Suspended Solids
Total Suspended Solids
Date: 12/14/2021 04:36 PM
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
ND
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
112 %
100 %
103 %
Analytical Method: SM 254OC-2015
Pace Analytical Services -Asheville
NO mg/L
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
0.50
1
12/09/21 19:22
156-59-2
0.50
1
12/09/21 19:22
156-60-5
0.50
1
12/09/21 19:22
78-87-5
0.50
1
12/09/21 19:22
142-28-9
0.50
1
12/09/21 19:22
594-20-7
0.50
1
12/09/21 19:22
563-58-6
0.50
1
12/09/21 19:22
10061-01-5
0.50
1
12/09/21 19:22
10061-02-6
0.50
1
12/09/21 19:22
108-20-3
0.50
1
12/09/21 19:22
10041-4
2.0
1
12/09/21 19:22
87-68-3
0.50
1
12109/2119:22
98-82-8
2.0
1
12/09/21 19:22
75-09-2
0.50
1
12/09/21 19:22
1634-04-4
2.0
1
12/09/21 19:22
91-20-3
0.50
1
12/09/21 19:22
103-65-1
0.50
1
12/09/21 19:22
10042-5
0.50
1
12109/2119:22
630-20-6
0.50
1
12109/2119:22
79-34-5
0.50
1
12/09/21 19:22
127-18-4
0.50
1
12/09/21 19:22
108-88-3
2.0
1
12/09/21 19:22
87-61-6
2.0
1
12/09/21 19:22
120-82-1
0.50
1
1210912119:22
71-55-6
0.50
1
12109/2119:22
79-00-5
0.50
1
12/09/21 19:22
79-01-6
1.0
1
12/09/21 19:22
75-69-4
0.50
1
12/09/21 19:22
96-18-4
0.50
1
12109/2119:22
95-63-6
0.50
1
12/09/21 19:22
108-67-8
1.0
1
12/09/2119:22
75-01-4
1.0
1
12/09/21 19:22
179601-23-1
0.50
1
12/09/21 19:22
9547-6
70-130
1
12/09/21 19:22
17060-07-0
70-130
1
1210912119:22
460-00-4
70-130
1
12/09/21 19:22
2037-26-5
25.0
1
12/06/21 12:13
ND mg/L 2.5 1 12/0612110:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Page 14 of 33

' aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CITY OF MARION
Pace Project No.: 92574920
Sample: MW-4
Lab ID: 92574920004 Collected: 11/30/21 14:10
Received: 11/30/21 16:30 Matrix: Water
Parameters
Results Units PQL OF
Prepared Analyzed CAS No. Qual
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.17 mg/L 0.10 1
12/10/2110:46 7664A1-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
1.9 mg/L 0.040 1
12/01/21 01:31 14797-55-8
420.4 Phenolics, Total
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable
ND mg/L 0.020 1
12/07/21 10:38 12/07/21 15:14 64743-03-9
53108 TOC
Analytical Method: SM 53108-2014
Pace Analytical Services -Asheville
Total Organic Carbon
0.591 mg/L 1.0 1
12/14/21 03:34 7440-44-0
Date: 12/14/2021 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 33

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Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Balch: 664118
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3478756
Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
NO 10.0
12/07/2119:41
Cadmium
ug/L
NO 1.0
12/0712119:41
Iron
ug/L
NO 50.0
12/0712119:41
Lead
ug/L
NO 5.0
12/07/21 19:41
Manganese
ug/L
NO 5.0
12107/2119:41
LABORATORY CONTROL SAMPLE:
3478757
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Arsenic
ug/L
500
469
94 85-115
Cadmium
ug/L
500
479
96 85-115
Iron
ug/L
5000
4780
96 85-115
Lead
ug/L
500
482
96 85-115
Manganese
ug/L
500
458
92 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3478758
3478759
MS
MSD
92571755002
Spike
Spike MS
MSD MS MSD
%Rec
Parameter
Units Result
Conic.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Arsenic
ug/L <100
500
500 473
488 88 91
70-130
3
Cadmium
ug/L <10.0
500
500 494
490 99 98
70-130
1
Iron
ug/L 1930
5000
5000 7740
7550 116 112
70-130
2
Lead
ug/L <50.0
500
500 493
484 99 97
70-130
2
Manganese
ug/L <50.0
500
500 506
499 97 96
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3478760
3478761
MS
MSD
92574920002
Spike
Spike MS
MSD MS MSD
%Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Arsenic
ug/L NO
500
500 459
454 92 91
70-130
1
Cadmium
ug/L NO
500
500 461
457 92 91
70-130
1
Iron
ug/L 28400
5000
5000 34300
33400 118 100
70-130
3
Lead
ug/L NO
500
500 453
448 91 90
70-130
1
Manganese
ug/L 1080
500
500 1580
1550 99 93
70-130
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -I-C.
Page 16 of 33

(�aceAnalj4icalo
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QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 664244 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3479432 Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
12/09/21 14:52
1,1,1-Tichooroethane
ug/L
ND
0.50
12109/2114:52
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
12109/2114:52
1,1,2-Trichloroethane
ug/L
ND
0.50
12/09/21 14:52
1,1-Dichloroethane
ug/L
ND
0.50
12/09/21 14:52
1,1-Dichloroelhene
ug/L
ND
0.50
12/09/21 14:52
1,1-Dichloropropene
ug/L
ND
0.50
12/09/21 14:52
1,2,3-Trichlorobenzene
ug/L
ND
2.0
12/09/21 14:52
1,2,3-Tiichloropropane
ug/L
ND
0.50
12/0912114:52
1,2,4-Trichlorobenzene
ug/L
NO
2.0
12/09/21 14:52
1,2,4-Trimethylbenzene
ug/L
ND
0.50
12/09/21 14:52
1,2-Dibromo-3chloropropane
ug/L
ND
1.0
1210912114:52
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
12/09/21 14:52
1,2-Dichlorobenzene
ug/L
ND
0.50
12109/2114:52
1,2-Dichloroethane
ug/L
ND
0.50
12/09/21 14:52
1,2-Dichloropropane
ug/L
ND
0.50
12/0912114:52
1,3,5-Tdmethylbenzene
ug/L
NO
0.50
12/09/21 14:52
1,3-Dichlorobenzene
ug/L
ND
0.50
12/09/21 14:52
1,3-Dichloropropane
ug/L
ND
0.50
12/09/21 14:52
1,4-Dichlorobenzene
ug/L
ND
0.50
12109/2114:52
2,2-Dichloropropane
ug/L
ND
0.50
12/0912114:52
2-Chlorotoluene
ug/L
NO
0.50
12/09/21 14:52
4-Chlorotoluene
ug/L
ND
0.50
12/09/21 14:52
Benzene
ug/L
ND
0.50
12/09/21 14:52
Bromobenzene
ug/L
ND
0.50
12109/2114:52
Bromochloromethane
ug/L
ND
0.50
12109/2114:52
Bromodichloromethane
ug/L
ND
0.50
12/09/21 14:52
Bromoform
ug/L
ND
0.50
12/0912114:52
Bromomethane
ug/L
ND
5.0
12/09/21 14:52
Carbon tetrachloride
ug/L
ND
0.50
12/09/21 14:52
Chlorobenzene
ug/L
ND
0.50
12109/2114:52
Chloroethane
ug/L
ND
1.0
12/09/21 14:52
Chloroform
ug/L
ND
0.50
12/09/21 14:52
Chloromethane
ug/L
ND
1.0
12/09/21 14:52
cis-1,2-Dichloroelhene
ug/L
ND
0.50
12/09/21 14:52
cis-1,3-Dichloropropene
ug/L
ND
0.50
12/09/21 14:52
Dibromochloromethane
ug/L
ND
0.50
12/09/21 14:52
Dibromomethane
ug/L
ND
0.50
12/09/21 14:52
Dichlorodifiuoromethane
ug/L
ND
0.50
12/09/21 14:52
Diisopropyl ether
ug/L
ND
0.50
12/09/21 14:52
Qualifiers
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -LC. Page 17 of 33

aceAnalytical
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Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
METHOD BLANK: 3479432 Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units Result Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
12/09/21 14:52
Hexachloro-1,3-butadiene
ug/L
ND
2.0
12/09/21 14:52
Isopropylbenzene (Cumene)
ug/L
ND
0.50
12/09/21 14:52
m&p-Xylene
ug/L
ND
1.0
12109/2114:52
Methyl-tert-butyl ether
ug/L
ND
0.50
12/09/21 14:52
Methylene Chloride
ug/L
ND
2.0
12/09/21 14:52
n-Butylbenzene
ug/L
ND
0.50
12/09/21 14:52
n-Propylbenzene
ug/L
ND
0.50
12109/2114:52
Naphthalene
ug/L
ND
2.0
12/0912114:52
o-Xylene
ug/L
ND
0.50
12/09/21 14:52
sec-Butylbenzene
ug/L
ND
0.50
12/0912114:52
Styrene
ug/L
ND
0.50
12/09/21 14:52
tert-Butylbenzene
ug/L
ND
0.50
12109/2114:52
Tetrachloroethene
ug/L
ND
0.50
12109/2114:52
Toluene
ug/L
ND
0.50
12/09/21 14:52
trans-1,2-Dichloroethene
ug/L
ND
0.50
12/09/21 14:52
trans-1,3-Dichloropropene
ug/L
ND
0.50
12/09/21 14:52
Trichloroethene
ug/L
ND
0.50
12109/2114:52
Trichlorofluoromethane
ug/L
ND
1.0
12109/2114:52
Vinyl chloride
ug/L
NO
1.0
12/09/21 14:52
1,2-Dichloroethane-d4 (S)
%
109
70-130
12/09/21 14:52
4-Bromofluorobenzene (S)
%
100
70-130
12/09/21 14:52
Toluene-d8 (S)
%
100
70-130
12/09/21 14:52
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3479433
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rec
Limits
1,1,1,2-Telrachloroethane
ug/L
50
55.0
110
60-140
1, 1, 1 -Trichloroethane
ug/L
50
56.6
113
60-140
1, 1,2,2-Tetrach loroethane
ug/L
50
54.7
109
60-140
1,1,2-Trichloroethane
ug/L
50
58.7
117
60-140
1,1-Dichloroethane
ug/L
50
58.1
116
60-140
1,1-Dichloroethene
ug/L
50
57.9
116
60-140
1,1-Dichloropropene
ug/L
50
56.5
113
60-140
1,2,3-Tdchlorobenzene
ug/L
50
57.4
115
60-140
1,2,3-Trichloropropane
ug/L
50
50.0
100
60-140
1,2,4-Trichlorobenzene
ug/L
50
58.4
117
60-140
1,2,4-Trimethylbenzene
ug/L
50
57.6
115
60-140
1,2-Dibromo-3chloropropane
ug/L
50
50.4
101
60-140
1,2-Dibromoethane (EDB)
ug/L
50
57.7
115
60-140
1,2-Dichlorobenzene
ug/L
50
56.3
113
60-140
1,2-Dichloroethane
ug/L
50
55.3
111
60-140
1,2-Dichloropropane
ug/L
50
54.9
110
60-140
1,3,5-Trimethylbenzene
ug/L
50
58.2
116
60-140
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 33

aceAnalytical
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Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
LABORATORY CONTROL SAMPLE:
Parameter
3479433
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
65.8
112
60-140
1,3-Dichloropropane
ug/L
50
55.7
111
60-140
1,4-Dichlorobenzene
ug/L
50
55.0
110
60-140
2,2-Dichloropropane
ug/L
50
61.3
123
60-140
2-Chlorotoluene
ug/L
50
58.9
118
60-140
4-Chlorotoluene
ug/L
50
56.3
113
60-140
Benzene
ug/L
50
56.1
112
60-140
Bromobenzene
ug/L
50
55.0
110
60-140
Bromochloromethane
ug/L
50
58.7
117
60-140
Bromodichloromethane
ug/L
50
56.2
112
60-140
Bromoform
ug/L
50
57.9
116
60-140
Bromomethane
ug/L
50
64.7
129
60-140
Carbon tetrachloride
ug/L
50
54.5
109
60-140
Chlorobenzene
ug/L
50
57.1
114
60-140
Chloroethane
ug/L
50
50.5
101
60-140
Chloroform
ug/L
50
57.7
115
60-140
Chloromethane
ug/L
50
54.8
110
60-140
cis-1,2-Dichloroethene
ug/L
50
53.9
108
60-140
cis-1,3-Dichloropropene
ug/L
50
56.1
112
60-140
Dibromochloromethane
ug/L
50
59.8
120
60-140
Dibromomethane
ug/L
50
58.3
117
60-140
Dichlorodifluoromelhane
ug/L
50
58.1
116
60-140
Diisopropyl ether
ug/L
50
52.4
105
60-140
Ethylbenzene
ug/L
50
57.5
115
60-140
Hexachloro-1,3-butadiene
ug/L
50
58.9
118
60-140
Isopropylbenzene (Cumene)
ug/L
50
60.2
120
60-140
m&p-Xylene
ug/L
100
116
116
60-140
Methyl-tert-butyl ether
ug/L
50
55.7
111
60-140
Methylene Chloride
ug/L
50
57.3
115
60-140
n-Butylbenzene
ug/L
50
59.3
119
60-140
n-Propylbenzene
ug/L
50
58.0
116
60-140
Naphthalene
ug/L
50
54.3
109
60-140
o-Xylene
ug/L
50
56.9
114
60-140
sec-Butylbenzene
ug/L
50
58.4
117
60-140
Styrene
ug/L
50
56.3
113
60-140
tert-Butylbenzene
ug/L
50
48.3
97
60-140
Tetrachloroethene
ug/L
50
51.8
104
60-140
Toluene
ug/L
50
58.4
117
60-140
trans-1,2-Dichloroethene
ug/L
50
59.0
118
60-140
trans-1,3-Dichloropropene
ug/L
50
58.9
118
60-140
Trichloroethene
ug/L
50
57.5
115
60-140
Trichlorofluoromethane
ug/L
50
51.6
103
60-140
Vinyl chloride
ug/L
50
58.1
116
60-140
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
102
70-130
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -LC. Page 19 of 33

(7WceAnalytical'
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CITY OF MARION
Pace Project No.: 92574920
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3479434
3479435
MS
MSD
92575770003
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rao
Limits
RPD Qua[
1,1,1,2-Tetrach[orcethane
ug/L
ND
20
20
13.6
13.4
68
67
60-140
2
1,1,1-Tdch[oroethane
ug/L
ND
20
20
14.0
13.9
70
70
60-140
1
1,1,2,2-Telrach[oroethane
ug/L
ND
20
20
12.9
13.3
65
66
60-140
3
1,1,2-Trichloroethane
ug/L
ND
20
20
14.6
14.6
73
73
60-140
0
1,1-Dichloroethane
ug/L
ND
20
20
15.0
14.6
75
73
60-140
3
1,1-Dichloroethene
ug/L
ND
20
20
16.1
14.7
80
74
60-140
9
1,1-Dichloropropene
ug/L
ND
20
20
14.6
14.1
73
71
60-140
4
1,2,3-Trich[orobenzene
ug/L
ND
20
20
16.8
15.3
84
77
60-140
9
1,2,3-Trichloropropane
ug/L
ND
20
20
12.2
13.0
61
65
60-140
7
1,2,4-Trich[orobenzene
ug/L
ND
20
20
16.2
15.6
81
78
60-140
3
1,2,4-Trimethy[benzene
ug/L
0.74
20
20
15.7
15.4
75
73
60-140
2
1,2-Dibromo-3chloropropane
ug/L
ND
20
20
11.9
11.5
60
57
60-140
4 M1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
13.8
14.0
69
70
60-140
1
1,2-Dichlorobenzene
ug/L
ND
20
20
14.3
13.5
71
68
60-140
5
1,2-Dichloroethane
ug/L
ND
20
20
14.2
14.1
71
71
60-140
0
1,2-Dich[oropropane
ug/L
ND
20
20
13.6
13.8
68
69
60-140
2
1,3,5-Trimethylbenzene
ug/L
NO
20
20
15.4
15.0
77
75
60-140
3
1,3-Dichlorobenzene
ug/L
ND
20
20
14.1
13.6
70
68
60-140
3
1,3-Dich[oropropane
ug/L
ND
20
20
13.9
13.8
70
69
60-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
13.6
13.3
68
67
60-140
2
2,2-Dichloropropane
ug/L
NO
20
20
15.7
15.4
79
77
60-140
2
2-Chloroto[uene
ug/L
ND
20
20
14.6
14.0
73
70
60-140
4
4-Chlorotoluene
ug/L
NO
20
20
13.7
13.5
69
67
60-140
2
Benzene
ug/L
15.3
20
20
29.8
29.7
73
72
60-140
0
Bromobenzene
ug/L
ND
20
20
14.2
13.7
71
68
60-140
4
Bromochloromethane
ug/L
NO
20
20
14.8
14.4
74
72
60-140
2
Bromodichloromethane
ug/L
NO
20
20
13.8
14.1
69
71
60-140
3
Bromoform
ug/L
ND
20
20
13.3
13.1
67
66
60-140
1
Bromomethane
ug/L
ND
20
20
18.0
16.8
90
84
60-140
7
Carbon tetrachloride
ug/L
ND
20
20
13.7
14.1
69
71
60-140
3
Chlorobenzene
ug/L
NO
20
20
14.4
14.5
72
73
60-140
1
Chloroethane
ug/L
ND
20
20
16.9
16.9
84
84
60-140
0
Chloroform
ug/L
ND
20
20
14.6
14.5
73
73
60-140
1
Chloromethane
ug/L
ND
20
20
13.3
12.6
67
63
60-140
5
cis-1,2-Dichloroethene
ug/L
NO
20
20
14.0
13.9
70
69
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
13.4
13.8
67
69
60-140
3
Dibromochloromethane
ug/L
ND
20
20
14.0
14.4
70
72
60-140
3
Dibromomethane
ug/L
ND
20
20
14.3
14.6
72
73
60-140
2
Dichlorodifluoromelhane
ug/L
NO
20
20
12.8
13.1
64
66
60-140
2
Diisopropyl ether
ug/L
6.0
20
20
19.1
18.8
65
64
60-140
1
Ethylbenzene
ug/L
1.8
20
20
16.6
16.7
74
74
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
18.4
17.0
92
85
60-140
8
Isopropylbenzene (Cumene)
ug/L
ND
20
20
15.6
15.4
78
77
60-140
1
m&p-Xy[ene
ug/L
6.9
40
40
37.4
37.1
76
76
60-140
1
Methyl-tert-butyl ether
ug/L
2.7
20
20
16.4
16.6
68
70
60-140
1
Methylene Chloride
ug/L
ND
20
20
12.2
11.7
61
59
60-140
4 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 33

(�aceAnalytical'
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QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3479434
MS
92575770003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3479435
MS
Result
MSD
Result
MS
e/ Rao
MSD
%Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
NO
20
20
16.5
15.3
83
77
60-140
7
n-Propylbenzene
ug/L
ND
20
20
15.4
14.9
77
74
60-140
3
Naphthalene
ug/L
ND
20
20
14.5
13.4
71
66
60-140
8
o-Xylene
ug/L
3.6
20
20
18.3
17.9
73
72
60-140
2
sec-Butylbenzene
ug/L
ND
20
20
15.9
15.1
80
76
60-140
5
Styrene
ug/L
ND
20
20
13.5
13.5
68
68
60-140
0
tert-Butylbenzene
ug/L
ND
20
20
12.9
12.5
64
62
60-140
3
Tetrachloroethene
ug/L
ND
20
20
13.5
13.3
67
67
60-140
1
Toluene
ug/L
26.2
20
20
41.6
41.7
77
77
60-140
0
trans-1,2-Dichloroethene
ug/L
NO
20
20
15.3
15.0
76
75
60-140
2
trans-1,3-Dichloropropene
ug/L
NO
20
20
13.9
14.1
70
70
60-140
1
Trichloroethene
ug/L
ND
20
20
14.3
14.3
71
71
60-140
0
Trichlorofluoromethane
ug/L
ND
20
20
14.1
14.2
71
71
60-140
1
Vinyl chloride
ug/L
ND
20
20
14.8
14.4
74
72
60-140
2
1,2-Dichloroethane-d4 (S)
%
102
104
70-130
4-Bromofluorobenzene (S)
e/
101
101
70-130
Toluene-d8 (S)
%
100
102
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 33

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 664054 Analysis Method: SM 254OC-2015
QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3478315 Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L NO 25.0 12t06/21 12:12
LABORATORY CONTROL SAMPLE:
3478316
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250
260 104 90-110
SAMPLE DUPLICATE: 3478317
92574627001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 46.0 54.0 16
SAMPLE DUPLICATE: 3478318
92575165002 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L NO ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, I.I.C.
Page 22 of 33

aceAnalytical
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Pace Analytical services, LLC
2225 Riverside Or.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 664056 Analysis Method: SM 254OD-2015
QC Balch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3478322 Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/06/21 10:53
LABORATORY CONTROL SAMPLE:
3478323
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 246 98
90-110
SAMPLE DUPLICATE: 3478347
92575224001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mg/L
278 234
17
SAMPLE DUPLICATE: 3478348
92574920002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 35.7 36.3 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 33

aceAnalj6cal
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 665204
Analysis Method: EPA
350.1 Rev 2.0 1993
QC Batch Method: EPA 3%1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3484900
Matrix: Water
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
12/10/2110:21
LABORATORY CONTROL SAMPLE: 3484901
Spike LCS
LCS % Rae
Parameter Units
Cone. Result
%Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 4.8
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3484902 3484903
MS MSD
92574468002
Spike Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Cone. Cone. Result
Result %Rec %Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 22.1
5 5 26.8
27.2 93 100
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3484904 3484905
MS MSD
92674755001
Spike Spike MS
MSD MS MSD
% Rae
Parameter Units Result
Cone. Cone. Result
Result % Rae % Rae
Limits RPD Qual
Nitrogen, Ammonia mg/L 1.7
5 5 6.6
6.6 98 98
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 33

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 662970
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2,0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92574920001
METHOD BLANK: 3473033
Matrix: Water
Associated Lab Samples: 92574920001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.040 12/01/21 00:43
LABORATORY CONTROL SAMPLE: 3473034
Spike LCS LIDS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
1.5 1.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473035 3473036
MS MSD
92574833006
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conic. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L NO
1.5 1.5 1.5 1.4 97 96
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473037 3473038
MS MSD
92574833011
Spike Spike MS MSD MS MSD
%Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L ND
1.5 1.5 1.5 1.5 102 103
90-110 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -I-C.
Page 25 of 33

/�'aceAnalytical
www.pacelebs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project:
CITY OF MARION
Pace Project No.:
92574920
QC Batch:
662971
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method:
EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92574920002, 92574920003, 92574920004
METHOD BLANK: 3473039 Matrix: Water
Associated Lab Samples: 92574920002, 92574920003, 92574920004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L NO 0.040 12/01/21 01:15
LABORATORY CONTROL SAMPLE: 3473040
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473041 3473042
MS MSD
92574796002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 3.3 1.5 1.5 5.1 5.5 119 147 90-110 8
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 33

////��aceAnalytical
www.pacelabs.com
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project:
CITY OF MARION
Pace Project No.:
92574920
QC Batch:
664085
Analysis Method:
EPA420.4 Rev 1.0 1993
QC Batch Method:
EPA420.4 Rev 1.0 1993
Analysis Description:
420.4 Phenolics
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92574920001, 92574920002, 92574920003, 92574920004
METHOD BLANK: 3478507
Matrix: Water
Associated Lab Samples: 92574920001, 92574920002,
92574920003, 92574920004
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Phenolics, Total Recoverable mg/L
ND 0.020
12/07/21 14:05
LABORATORY CONTROL SAMPLE: 3478508
Spike
LCS
LCS % Rae
Parameter Units
Cone.
Result
%Rec Limits
Qualifiers
Phenolics, Total Recoverable mg/L
0.05
0.051
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3478509
3478510
MS
MSD
92574920001
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rae
% Rae
Limits RPD Qua]
Phenolics, Total Recoverable mg/L NO
0.05
0.05 0.051
0.051 103
102
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3478511
3478512
MS
MSD
92574920002
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rae
e/ Rae
Limits RPD Qual
Phenolics, Total Recoverable mg/L ND
0.05
0.05 0,052
0.053 105
105
90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, -I-C.
Page 27 of 33

/,PaceAnalytical
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Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CITY OF MARION
Pace Project No.: 92574920
QC Batch: 665769
Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531OB-2014
Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574920001, 92574920002,
92574920003, 92574920004
METHOD BLANK: 3488019
Matrix: Water
Associated Lab Samples: 92574920001, 92574920002,
92574920003, 92574920004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
12/13/21 18:40
LABORATORY CONTROL SAMPLE: 3488020
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 25.7
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3488021 3488022
MS MSD
73100961001
Spike Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc. Conc. Result
Result %Rec %Rec
Limits RPD Qual
Total Organic Carbon mg/L 52.0
25 25 80.5
80.1 114 112
90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3488023 3488024
MS MSD
92573480001
Spike Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 25.4
25.5 101 102
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Dale: 12/14/2021 04:36 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 33

�i
aceAnalj4ical�
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Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: CITY OF MARION
Pace Project No.: 92574920
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL -Adjusted Method Detection Limit.
PQL - Practical Quantilation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CITY OF MARION
92574920
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92574920001
MW-1R
92574920002
MW-2
92574920003
MW-3
92574920004
MW4
92574920001
MW-1R
EPA 200.7 Rev 4.41994
664118
EPA 200.7 Rev 4.41994
664269
92574920002
MW-2
EPA 200.7 Rev 4.4 1994
664118
EPA 200.7 Rev 4.4 1994
664269
92574920003
MW-3
EPA 200.7 Rev 4.4 1994
664118
EPA 200.7 Rev 4.4 1994
664269
92574920004
MW-4
EPA 200.7 Rev 4.4 1994
664118
EPA 200.7 Rev 4.4 1994
664269
92574920001
MW-1R
SM 6200B
664244
92574920002
MW-2
SM 6200B
664244
92574920003
MW-3
SM 6200B
664244
92574920004
MW4
SM 6200B
664244
92574920001
MW-1R
SM 2540C-2015
664054
92574920002
MW-2
SM 254OC-2015
664054
92574920003
MW-3
SM 254OC-2015
664054
92574920004
MW4
SM 254OC-2015
664054
92574920001
MWAR
SM 2540D-2015
664056
92574920002
MW-2
SM 254OD-2015
664056
92574920003
MW-3
SM 254OD-2015
664056
92574920004
MW-4
SM 2540D-2015
664056
92574920001
MW-1R
EPA 350.1 Rev 2.01993
665204
92574920002
MW-2
EPA 350.1 Rev 2.01993
665204
92574920003
MW-3
EPA 350.1 Rev 2.0 1993
665204
92574920004
MW-4
EPA 350.1 Rev 2.0 1993
665204
92574920001
MW-1R
EPA 353.2 Rev 2.01993
662970
92574920002
MW-2
EPA 353.2 Rev 2.0 1993
662971
92574920003
MW3
EPA 353.2 Rev 2.01993
662971
92574920004
MW-4
EPA 353.2 Rev 2.0 1993
662971
92574920001
MW-11R
EPA 420.4 Rev 1.0 1993
664085
EPA 420.4 Rev 1.0 1993
664370
92574920002
MW-2
EPA 420.4 Rev 1.0 1993
664085
EPA 420.4 Rev 1.0 1993
664370
92574920003
MW-3
EPA 420.4 Rev 1.0 1993
664085
EPA 420.4 Rev 1.0 1993
664370
92574920004
MW-4
EPA 420.4 Rev 1.01993
664085
EPA 420.4 Rev 1.01993
664370
92574920001
MWAR
SM 53108-2014
665769
92574920002
MW-2
SM 531OB-2014
665769
92574920003
MW-3
SM 531OB-2014
665769
92574920004
MW-4
SM 531OB-2014
665769
Date: 12/14/2021 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 33

Document Name: Document Revised: November I5, 2021
e Sample Condition U on Recel t (SCUR Page 1 of 2
.- aceAnalykaj Document No.: IssuingAuthorlty:
f•CAR•CS-033•Rev.OB Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville❑ Eden[] Greenwood[] Huntersvilledl'�Ralelgh❑ Mechaniciville❑ Atlanta❑ Kernersville❑
Client Na IIMWII 1 ' e /- 1 � i-�xt Pr ject 1 wo# . 4920
❑Courier. Fed EKC ❑UPS ❑LISPS �]]Cllent II�II"II II'�I�'III'II
Commercial []Pace ❑Other:_ '
92574920
Custody Seal Present? []Yes :—❑No Seats intact? ❑Yes --�❑No
Date/InleaiS Perron Wmining Contents.
Packing Material: -. ❑Bubble wrap ❑llubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermomett '.- Type of Ira:
Des es
D IE Gun ID: P ZCi� / Qwet ❑Blue ❑Nant ❑No �N/A
Correction Factor:
Cooler Temp: � Add/Subtract ('Cj Temp should be above free2ing to 6'C
-EoolerTemp-Corrected{'[{ 1 - 139mpler out of temp uhena Samples an ice Coaling process
USDA Regulated � 8 (❑ N/A�,water.sample(
Did samples arit7nate In a gdarantine cone whin the United States: CA, NY, or SC (check maps I? Old samples originate from a foreign
❑Yes rNro rource pntemationaliy,
muuamnlnawananaruenoRiml?LIYes No
Comments/Discrepancy:
- Chain of Custody Present?
er
ONO
EINJA
1.
Sam les Arrived within Hold Timer
Qyft
No
N/A
2.
Short Hold Time Anatysis <72 hr.?
13yes
ONo
N/A
3.
Rush Turn Around Time nested?Elfes
No[]N/A
4.
SuMcientYolume?
ves
o
N/a
5.
Correct Containers Used?
��
❑No
❑N/A
6.
-Pace Containers Used?
ves
No
N/A
Containers Intact?
yes
No
N/A
7.
Dissolved anal is: Samples Field Filtered?
ves
No
p/,t'
a.
Sample Labels Match COC?
❑Y&'
[]No❑N/A
9.
Indudes Date /ID/Analysis Matrik:
���
Heads au Ia VOA Vials >5.6mm17
ves
Flo
. N)A
10.
Trip Blank Present?.
❑yes
❑yo
N/A .
it.
Trip BlankCustooy Seals Present?
yes
No
N p
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spit containers:
CUENTNOTIFIG710N/gESOLUnON
Person contacted:
Project Manager SCURF Review:
Project Manager:SRF Review:
Date/rime:
Field Data RequIred? ❑Yes []NO
Date:
Date:
Page 31 of 33

Document Name:
Document
Document Revised: November 15, 2021
Pape 2 of 2
*Check mark top half of box if pH and/or dechlorination is project
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Collform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
PM: UP Due Dalee: 12/14/21
CLIIENT: 83-MRRION
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pH Adjustment Log for Preserved Samples
Sample to
Type of Preservative
pH upon receipt
Date preservation adju;ted
Time preservtllon
Amount of preservative
Lot
adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be lent to the North Carolina OEHNR CeniRcatlon Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 32 of 33

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OOZE OOA
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DaaumentNnme: Fled Ma Sheet
Date Issued: March &, 20W
rare:. 1 of
ABAIh71yNCal
Oocumeal. Number P-CAIt-DIA-001-rev:Q3
lssuht Authority:Pace Httntersville ualil
8 Y
Office
Field Data Sheet
Client: 4:+-4 o r
Name and Affiliation (Sampler(5): RI^ 6 Pa I e
Name and Affiliation (inspector): N I A
Well Information
Well ID: MV/'�(Z
Welt Diameter: Z: n
Total Well Depth: b0' b 5 ft
Static Water Level: 24.1 Z ft
Height of Wate1• Colurtin. 36.3 3 ft
­-, Proeet4: c:+ti o� Niws.� f:;n go...aor/
Id Data Sheet Review:
Date: ! j 1�{ �a By: U` -L,
Well Locked: 'YES NO / lushmoun
Construction: Qyg^teel/Stainless Steel)
Multi Factor*:0.163 r(Radius/12)2x3rt4x7.481
CasingVolume: 5.1Z gallons
Cal. 3 Volumesi _ 17,71 gallons
PumpIntake: ~ S 6 ft
Purge Information
Date Purged: 11 / l0 Start: 042o Finish: 0g40 Purge Rate: ioo^111^,.1
Purging Method: Pens+elhtr P&k,-P Tota]VolumePtArged:,. Z001D (gallons mis .)
Sampling Information.
Dabe Collected: 11 / ?o/ 2 1 Time Collected; _a9 45 _,,: (am in)
Sainplingl?quipmentUsed: POP,34-4:r P%mp InstrumentlD: Y)r0S&9/TPW6092.__,____
Bottle Type Preservation
Field Measurements/Observations
Analysis Required
AAAae; a, N: r
t44A41T-J k , T b 5
1' 51 Vol 6200
Sample Temp (C): i 0. 3 Time: 09 4 s _Turbidity (ntu): 1- b Time: o g 4 5
Diss Oxy (mg/L): S • 5 Time: Fe 2+ mg/ L: N ID Time: 1
Specific Cond: (uS): 2 7 5 Time: Res. Cl'--
Sample pH. (s.u.):—°i —_--._Time: Odor:_._._ NO Ae _..—_Time:._ an 4 5 --
ReDox (mV): — Time: '— Appearance G 12e r `rime:
ReDox (EH valile):YSI ProPlus.+200mV Other: Time:
General/Weather
Temp. 3 aCF) Wind 0-$ (mph)
SamplerSignature:.... RY e A 6y aI Date: l (/ i o/2 I
Stabilization Test
Volume
Time
Temp.
Diss Oxy:
Coed,
pH (s.u.)
ReDOx
Turbidity
removed
Water
Other
Purged
(mC)
(mg/L)
(us)
(mV)
(ntu)
(gallons nils
level (ft)
L
4Dgi5
9.8
8.1
27.6
5.5
5*.1
500
24. 5
nu,
9.g
g,
17
5.
5.
Soo
2t,.
oQ90
10.0
8.85
:7.7
54
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loop
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1 2000
2

ry
DDcument Name: Field data Sheet.
Date Inued: March B, 2019
r?GG'/Irh7iIKlCeV
Page: 1 of 1
fhxuncenl Number FCAR-fLI>-0Ol mv,0$
Issuing Authority: bete Huntersville ualit Y
-
,.
Office
Field Data Sheet
Name and Affiliation(Sampler(s): RMg Pare Field Data Sheet Review.:
Name and Affiliation (Inspector):, M /A
Date:. la1 �lly�
Well Information a j
Well ID: M W 2 Well Locked: YES NO / Flushmount )'
Well Diameter: 2 ' n Construction '(+ems^ teel/Stailrless Steel)
Total Well Depth: ;$• O 2 ft
Static Water Level: Ig .7 2 ft
Height of Water Column: 19.3a ft
Multi Factof*: o• I b 3 r+(Rrdiva112)2 x 3a4 x 7a81
Casing Volume: 3.1 S gallons
Cal. $ Volumes: A.44 gallons
Pomp intake: ~ 3S ft
Purge information,
Date Purged; I I /_ 33 0 '( /__t_ Start: 12 4 o Finish:_ 1'2.5 5 Purge Ratc: 100 ANn r1
Purging Method: f2r154e:1+4_ P0.mf Total Volume Purged: 1510,0 (gallons
Sampling Information
Date Collected: Il /J*-/ 21 Time Collected ._ 13W (a pm
Sampling Equipment Used: fsr3*>I4;LPuthP instrument ID: YOo56at`/Pw6o$3
Bottle Type
Field Measurements/Observations
Preservation
Analysis Required
_ roei..15 2oo. �10t_
ArA^oA; o, N;}rafP
eh0Aet,704e•l� T b 3
T5I, VOL G,200
mw'io.AT6A9 N0V.242/
Sample Temp (eq:. ) 7• Z Time; 13o9__Turbidity
(Atu): 2 • `J
Time:
13O0
Diss Oxy (mg/L): 0•'1 Time;
Fe 2+ mg/L: N ()
Time:
Specific Cond: (uS): -53 7.3 Time:,
Res. Cl�—
Sample pH (s.u.):. (0• Time: _
Odor:_ N o Ne
_Thue:
_. 309
ReDox (mV): Time:
Appearance: Ltee.
Time:
�-
ReDox (EH value):YSI ProPlus +200mV�
Other:
Time:
General/Weather Observations:
Temp. S °t (OF) Wind 0'
Sampler Signature: RYo A gyaq _Date: tl/10/ ZI _
Stabilization Test
Spec.
---Volume
Time
Temp.
Diss Oxy.
Cond.
pi -I (s.u.)
R`eDox
Turbidity
remove
Water
Other
Purged
CC)
(mg/L)
(us)
(mV)
(ntu)
(gallons/ Is
level (ft)
L
1245
b.
rx b
33717
---
6.-
Soo
19
b.
'3318
Soo
19. 9 Ll
115 a
I Vq
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33b.1
6.14
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" .1
eeAnrl/ytiCal
Document Name: Field data Shef.
Date Issued: March 8; 2019
P. er 1 of a
Document Number F•CAR-FI,D-0p1-rev;Q'i
Issuing Authority: Pace Huntersville Quality
Office
Field Data Sheet
Nov 702-1
Name and Affiliation (Sampler(s): RA18 Pose
Name and Affiliation (Inspector): N A
Well Information
Well ID: 1% W -3
Well Diameter: 2 t n
.Id Data Sheet Review:
12.Iy•2t M�,IL
Date:By:Tnf
Well Locked: C5) NO / Mishmount )
Construction: Steel/.Stateless Steel)
Total Well Depth: S0, OZ ft MultlFact00: 0'163 r(ttadiu8/12)2x3rt4x7.481
Static Water Leveli 41. 3y., ft Casing Volume: _5.0N gallons
Height of Water Column; Ib.b-S ft Cal. 3 Volumes: 9 l gallons
Pump Intake: /%- 147 ft
Purge Information.
Date Purged: 11 / 30 J Z1 .Start: iO3S Fb-dsh: 1135 Purge Rate: !OLQ /m ,1
Purging Method: laalw noftsoo^ PAM? . �Total Volume Purged: b000 (gallons, ails/ )
Sampling.lnformation
Date Collected: +I /_jo/ 11 Time Collected:_.) l'10am rn)
Sampling Equipment Used: Me5 > mea. 3oe /1 Pu A P Instrument ID: Y sz 05 bei /T ow Do e 3
Bottle Type Preservation Analysis Required:
Mg4gl5 Zoo.7, T4L __v
r�.o,.ol79 tat Tb 5
'755yoc blop
Field Measurements/Observations
Sample Temp CC):. 13, '9 Time: 11 _Turbidity (ntu): q . 7 Time: l 14 0
Diss Oxy (mg/L): 3. l Time., Fe 2+ mg/L: N O Time:
SpecificCond, (uS): I S 3. t{ Time: Res. Ct (nig/L)J(µg/L):� — Thee;
Sample pH (s.u.): 5 -10 .___. Time: Odor:..,_— N o AP _ Time:...._ \ I H fj_ _
ReDox (mV):: Time: %Appearance:. Glem r Time:
ReDox (EH value);YSI ProPlus +200uiV Other: Time: .�
General/Weather Observations-,
Temp.52 ff) Wind lo-I (mph)
Sampler Signature: RY&%A h y qt$ �._ __DAte: 11 /3o421 --
Stabilization Teat
Time
Temp.
Dins Oxy.
Spec.
Cond.
pH (s.u.)
ReDox
Turbidity
o ume
remov
Water
Other
Purged
(C)
(mg/L)
(US)
(MV)
(ntu)
(gallons ,Is
level (ft)
L
typo
li•4
4.Z
208,5
4.
"„
59.6
5A0
6tt
11.E
y Z
2oS,
�—
54.6
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3 552
io45
4,
2.
5•0
8).
loop
31.015
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12.7
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1105
132
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132.Oq

Document Name Field data Sheet.
Date Issued: March 8, 2019:
<CBArh7lyflCN
Page: iufI
Document Number FCAR-BI..n-001-rcv:03
Issuing Aullimityt Pace Huntersville Quality
_
l
Office
Field Data Sheet
i-r o 0
Name and Affiliation(Sampler(s):.&AIR Para
Name and Affiliation (Inspector) N /A
Well Information
Well ID: ^ W • 4 Well Locked:
Well Diameter: 2 i n
Total Well Depth: 3 5. 37 It
Static Water Level: 2O- 16 ft
Height of Water Colunyn: 15.21 ft
Puree Information
Construction:
tid Data Sheet Review:
IL.Ih.2+
Date: lad Mk-2\
Steel)
Multi Factor*:0+ 1 h3 P(Radius/12)2 x.3.14 x 7.481
Casing Volume; 2.48 gallons
Cal, 3 Volumes: -7 • 4 4 gallons
Pump Intake: /" 3 3 ft
M
Jk�E+2.
By; T yt-
Date Purged: 11 ,/ 3 o /_11 Start: 13 qS Firdsh; Ill. -I T_ Purge Rate: 100AIIIA ; N
Purging Method':_P.&. ii�H''c ar .J! Total Volume Purged: 10010 (gallons nits
at
Date Collect drtn-11_/3o / 2I Time Collected; 4io (am jim)
Sampling Equipment Used: fe.IlYml .L0unp lnstrumentlD: yfLa56gITPwboL?3_.,
Bottle Type Preservation Analysis Required
d±4fi 15 200.7 /.?4_�._...- -
A , N,;yreyt
f1ero1, Total /� D f
75if VoLb2o0
Field Measurements/Observations
Sample Temp Cc);
) L 7 Time:�l
412__Turbidity (ntu): I , Z Time: 141,2
Diss O m L
xy ( gJ)
1. 1 Time:
N
Fe 2+ mg/ U. O Time:
SO' 4
Specific Cond. (uS):
Tlme:
Res. d (nlg/L)/(µg/L): "'— Tillie: —
Sample pH (s,u,),
5 ��Time:
Odor:_ Eo-r� ► xTime: _ 1410
ReDox (mV):
-- Time:
-- — Appearance: L 1Q dt rime:
ReDox (EH value):YS.1 ProPlus +2110niV Other:
General/Weather Observations,•
Time:
Temp. b i (°F)
v
Sampler Signature: RYon Ho- _Dot: 11/30/2
Stabilization Test
Spec.
Volume
Time
Purged
Temp.
CC)
Diss Oxy,
(mg/L)
Cond.
PH (s.u.)
ReDox
V)
("IV)
Turbidity
(ntu)
(ntu)
removed
gallons/
(gallons/6
Water
level (ft)
Other
L
135a
S
T4
54 .o
I
10.3
Sao
2.o.4Z
QK
tS
S4.o
.1
--
ml
50A
2p,42
1 55
is
a
loov
ao.5
JUDO
14,
1,0
50
5.0
--
150o
zD p
14oS
1N.6
i.o
fa0.3
----
1.5
1
D.b
Nov. 20V

Document Name:
Document Issued: March 8, 2019
aceAnr2lylical -
Field Data Sheet
Paget of I
Document Number:
lssuehig Aufirority:
_,.
f
F-CAR-FLD-001,rev.03
Pace Huntersville Quality Offiee
Client: L��y "u M.,-Toll
Location; Air ;on, N L
Project; [.;iy or- AWS�yGnj itlov, 202)
Well ID:
Reviewed Date and By: 11�f a�a� In
Stabilization Test 12 I M L( M EL&
FVell Diameter
Multiplication Factor"
1
0.0408
1.2
0.0918
1.625
0.1050
2
0.1630
3
0.3670
4
0.6530
6
1.4680
3
2.6100
Time
Purged
Temp.
(°C)
Diss Oxy.
(.mg/L)
Spec.
Cond.
(u5)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume RemovedWater
(gal rcle one )
circle one
level
( )
other
Ills
13.5
3,6
i%6.5
5. o
a5, 6
4004
112S
13,&
3 3
fay•7
5.0
--
lq.B
Soaq
31.23
1130
13,
3 Z
1642
5.0
7 b
SSoo
32 a r0
435
13.1
3.1
W3.6
S,o
--
9.
(0000
32,3