WQ0003487_Residual Annual Report 2021_20220211

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0003487
Applicant/Permittee Novozymes North America, Inc.
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer
Raleigh

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Scott Creech
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
9194960862
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0003487
Has Current Existing permit number
77 Perry Chapel Church Rd Franklinton, NC 27525
Novozymes Class A Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2021 SBM Annual Report.pdf 16.81 MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/11/2022

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: 3487 Novozymes North America, Inc.
PHONE: [phone] Franklin OPERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): J Surface Disposal (complete Part A(Source(s) and "Residual In" Volume Only) and Part C)
El Distribution and Marketing ( complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes No [] J If No skip parts A, B, C and certify form below
Part A*: Part B*:
Month
January
Sources(s) (include NPDES # if
applicable)
Amendment/
Bulking Agent
Volume (dry tons)
Residual In
WAS
SBM
Product Out
Name(s)
Recipient Information
Volume (dry tons)
Intended use(s)
February
March
April
May
June
July
August
September
October
November
Deeember
Totals:
82
124
114
175
165
213
110
193
164
173
148
143
108
68
113
145
137
109
166
101
140
112
88
101
486
847
1283
1727
1035
546
497
873
1310
1163
1109
934
676
1039
1510
2047
1337
868
773
1167
1614
1448
1345
1178
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
see attached DMSDF (Supp)
0 0
15002 15002
13ulking Agent(sl used: None
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Numhcr of 1' >nn DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit (including Eyes
but not limited to items 1-3 below) issued by the Division of Water Quality: © No If No, Explain in Narrative
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality,
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
9
Total from FORM DMSDF (sup)
Signature of Permittee
Annual (dry tons): 1804
Amendment(s) used:I 1 lydrated Lime
**Preparer is defined in 40 CFR Part 503.9(r) and
15A NCAC 2T .1102 (26)
0
1388
11810
2J/o%2
Date Signature of Preparer**
(if different from Permittee)
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
Nnynrvmes North America. Inc.
WQ PERMIT #: 3487 FACILITY NAME:
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
17 Distribution and Marketing (complete Parts A, and B)
Part A*
Part B*:
Month
NPDES # if
Volume (dry tons)
Recipient Information
Sources(s) (include
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)tons}
Volume (dry
Intended use(s)
January
DANNY BOLTON
146
Agricultural
January
SHELBY DAVIS
34
Agricultural
January
TIM DUKE
26
Agricultural
Agricultural
January
MADISON HEDGECOCK
83
January
ROBERT JOHNSON
13
Agricultural
January
DOUG MAY
31
Agricultural
January
THOMAS PERDUE
26
Agricultural
Agricultural
January
MIKE SMITH
37
January
JOE THARRINGTON
18
Agricultural
January
TOM TRAYLOR
93
Agricultural
February
RC CREECH
68
Agricultural
February
DONALD EDWARDS
31
Agricultural
Agricultural
February
WILLIAM GRIFFEN
26
February
LEE INSCOE
57
Agricultural
February
ALPHEUS JONES
58
Agricultural
February
EMERY KEETER
125
Agricultural
February
RANDY MARTIN
51
Agricultural
February
NOVOZYMES
360
Agricultural
February
MIKE SMITH
70
Agricultural
Totals:
Annual (dry tons):
0
0
0 1,333
Amendment(s) used:I
Bulking Agent(s) used:
DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
9
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America, Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): L I Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
P1 Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
# if
Volume (dry tons)
Recipient Information
Sources(s) (include NPDES
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
March
MARTEZ ALSTON
64
Agricultural
Agricultural
March
WAYNE CLEATON
173
March
EARLY JOURNIGAN
106
Agricultural
March
EMERY KEETER
124
Agricultural
Agricultural
March
ROBERT LOYD
64
March
REX MURPHY
47
Agricultural
March
HENRY NELMS
120
Agricultural
March
DELTON NELMS
32
Agricultural
March
THOMAS PERDUE
163
Agricultural
March
PHILLIP SMITH
57
Agricultural
Agricultural
March
MIKE SMITH
64
March
JOE THARRINGTON
11
Agricultural
March
TOM TRAYLOR
125
Agricultural
Agricultural
March
BILLY WOOD
131
April
RICKY AYCOCK
19
Agricultural
April
TALMADGE BURGESS
37
Agricultural
April
HERMAN COLLIER
195
Agricultural
April
STEVE COLLINS
27
Agricultural
Agricultural
April
RC CREECH
.15
April
DONALD EDWARDS
35
Agricultural
Totals:
Annual (dry tons):
0
0
0 1639
Amendment(s) used:I
Bulking Agent(s) used:
DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
9
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Nnvozymes North America, Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): U Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
A Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Volume (dry tons)
Recipient Information
Sources(s) (include NPDES # if
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
April
GREG HOLTZMAN
13
Agricultural
April
EARLY JOURNIGAN
71
Agricultural
April
DAVID KEMP
385
Agricultural
April
ROBERT LOYD
84
Agricultural
April
DOUG MAY
17
Agricultural
Agricultural
April
HENRY NELMS
22
April
TROY NELMS
86
Agricultural
April
JEREMY PASCHALL
90
Agricultural
April
THOMAS PERDUE
131
Agricultural
April
RAYMOND SEAMAN
208
April
PHILLIP SMITH
106
April
MIKE SMITH
28
Agricultural
April
JOE THARRINGTON
19
Agricultural
Agricultural
April
TOM TRAYLOR
91
April
DWIGHT WILLIAMS
17
Agricultural
JAMES ALLEN
26
Agricultural
May
May
HERMAN COLLIER
89
Agricultural
Agricultural
Agricultural
May
DONALD EDWARDS
64
May
CRAIG FAULKNER
1 17
May
PHILLIP FLEMING
23
Agricultural
Agricultural
May
_ ANDY GARRETT
37
Totals:
Annual (dry tons):
0
0
0 1724
Amendment(s) used:
Bulking Agent(s) used:
* If mnre snace is reauired. attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
9
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America. inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): LJ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
�I Distribution and Marketint (complete Parts A and 13)
Part A*:: v
Part B*:
Month
Volume (dry tons)
Recipient Information
Sources(s) (include NPDES # if
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
May
MADISON HEDGECOCK
22
Agricultural
May
JOHNNIE KING
25
Agricultural
May
ROBERT LOYD
3(1
Agricultural
May
SPENCER MARSHALL
10
Agricultural
May
HENRY NELMS
201
Agricultural
May
DELTON NELMS
23
Agricultural
May
EDDIE NEWTON
19
Agricultural
May
MARK PERKINS ON
59
Agricultural
May
JUSTYN PHELPS
32
Agricultural
May
LEE SHORT
166
Agricultral
Agricultural
May
PHILLIP SMITH
22
May
BILLY WOOD
69
Agricultural
June
DANNY BOLTON
64
Agricultural
June
CALVIN BRODIE
8
Agricultural
June
TALMADGE BURGESS
82
Agricultural
June
HUNTER CHOPL1N
10
Agricultural
June
GLEN COLEMAN
6
Agricultural
June
JONNETTE COLLINS
26
Agricultural
June
OSCAR DAVIS
9
Agricultural
June
LEON DILLARD
36
Agricultural
June
WILLIE EDWARDS
17
Agricultural
June
PHILLIP FLEMING
38
Agricultural
Totals:
Annual (dry tons):...
0
0
0 ... 974
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
otal Number of Form DMSDF {Supp
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America. Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
[] Distribution and Marketing (complete Parts A, and B)
Month
June
June
June
June
June
June
June
June
July
July
July
July
July
July
July
July
July
July
July
July
July
Totals:
Part A*.
Sources(s)( (include NPDES # if I
applicable)
Volume (dry tons)
Part B*:
Recipient Information
Annual (dry tons):
Amendment(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Amendment/
Bulking Agent
0
Residual In
Product Out
0
Bulking Agent(s) used:
0
Name(s)
Volume (dry
tons)
Intended use(s)
ANDY GARRETT 36 Agricultual
MADISON HEDGECOCK 49 Agricultual
RANDY MARTIN 30 Agricultual
HENRY NELMS 37 Agricultual
DELTON NELMS 10 Agricultual
GLENN RIGGAN 10 Agricultual
MARTY ROOKER 73 Agricultual
BILLY WOOD 2 Agricultual
DANNY BOLTON 17 Agricultual
TALMADGE BURGESS 63 Agricultral
TOMMY BURTON 29 Agricultral
HUNTER CHOPLIN 17 Agricultral
WILLIE EDWARDS 56 Agricultual
FRANK GANTT 10 Agricultual
RUSSELL GUPTON 35 Agricultual
HERMAN HAWKINS 13 Agricultual
JUSTIN LEONARD 11 Agricultual
LESLIE LONG 6 Agricultual
ED MOORE 16 Agricultual
HENRY NELMS 18 Agricultual
JEREMY PASCHALL 60 A ricultual
598
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America, Inc.
Franklin OPERATOR: Novozymes North America, Inc
PHONE: [phone] COUNTY:
FACILITY TYPE (please check one): 'J Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
0
Distribution and Marketing (com)lete Parts A, and B)
Part A*:
Part B':
Month
Sources(s) (include NPDES
applicable)
# if
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)Volume
{dry
tons)
Intended use(s)
July
WILLIAM PEOPLES
23
Agricultual
Agricultual
July
BRANDON PERNELL
54
July_
GLENN RIGGAN
24
Agricultual
July
LARRY THOMAS
11
Agricultual.
Agricultual
July
TOM TRAYLOR
35
August
JASON AYCOCK
68
Agricultual
August
SIDNEY BURTON
38
Agricultual
August
DAVID CLARY
57
Agricultual
August
SEAN FALLON
20
Agricultual
August
FRANK FURLOW
21
Agricultual
August
JOHN GARRETT
52
Agricultual
August
JOEL HARRIS
40
Agricultual
August
HERMAN HAWKINS
27
Agricultual
August
EMERY KEETER
72
Agricultual
August
KEN KREGER
20
Agricultual
Agricultual
August
ROBERT MILLER
40
August
MIKE NORWOOD
44
Agricultual
Agricultual
Agricultual
August
DANNY PAYNTER
185
August
NICHOLAS PEDIADITAKIS
47
August
LEE SHORT
90
Agricultual
August
GOINS SNEED
34
Agricultual
August
DARYL THARRINGTON
18
Agricultual
Totals:
Annual (dry tons):
t1
0
0 1020
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
9
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America, Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
I] Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
# if
Volume (dry tons)
Recipient Information
Sources(s) (include NPDES
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume {dry
tons)
Intended use(s)
September
JASON AYCOCK
71
Agricultual
September
CALVIN BRODIE
22
Agricultual
September
SHELBY DAVIS
32
Agricultual
September
JAMES DAVIS
10
Agricultual
September
SPENCER DEAN
355
Agricultual
September
WILSON FLEMING
114
Agricultual
September
CHARLES GRAINGER
48
Agricultual
September
JOEL HARRIS
61
Agricultual
September
STEVE HICKS
41
Agricultual
September
EMERY KEETER
140
Agricultual
September
MIKE NEWTON
64
Agricultual
September
LEE SHORT
72
Agricultual
September
CECIL WILSON
169
Agricultual
September
ALFRED WORTHAM
13
Agricultual
September
GREG WRIGHT
98
Agricultual
October
LYN BRYAN
58
Agricultual
October
EDDIE CAUDLE
14
Agricultual
October
JAMES DAVIS
156
Agricultual
October
WILSON FLEMING
250
Agricultual
October
JOHN GARRETT
38
Agricultual
Agricultual
October
MARTHA MOBLEY
420
October
MIKE PREDDY
22
Agricultual
October
LARRY SHORT
94
Agricultual
Totals:
Annual (dry tons):
0
0
0 2362
.
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
9
DENR FORM DMSDF (Supp) (12/2006)

Part A*:
Sources(s) (include NPDES # if
applicable)
Annual (dray tons):
Amendment(s) used:I
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America, Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc
FACILITY TYPE (please check one): L1 Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
p Distribution and Marketing (complete Parts A, and B)
Month
October
November
November
November
November
November
November
November
November
November
November
November
December
December
December
December
December
December
December
Totals:
Volume (dry tons)
Amendment/
Bulking Agent
0
Residual In
0
Product Out
Part B*:
Recipient Information
Name(s)
CECIL WILSON
MICHAEL CLOPTON
BILLY FAULKNER
WILSON FLEMING
BILL GARDNER
ROBERT LAND
MARTHA MOBLEY
DALE MOSS
MIKE NORWOOD
SHERBY SLAUGHTER
ROBERT SOUTHERLAND
JC WILSON
RUSSEL BOTTOMS
ANN BRAGG
RONNIE BURNETTE
DAVID CLARY
WESTER FARMS
WILSON FLEMING
GREG HOLTZMAN
Volume (dry
tons)
110
53
142
142
27
29
279
86
9
188
65
47
27
32
111
45
310
36
27
0 - 1765
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Intended use(s)
Agricultual
Agricultual
Agricultual
Agricultual
Agricultual
Agricultual
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
Agricutural
9
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: Novozymes North America, Inc.
PHONE: [phone] COUNTY: Franklin OPERATOR: Novozymes North America, Inc
FACILITY TYPE (please check one): U Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
p Distribution and Marketing (complete Parts A, and B)
Part A*:
Part BY':
Month
Volume (dry tons)
Recipient Information
Sources(s) (include NPDES # if
applicable)
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
December
SHANE MITCHELL
56
Agricultual
December
TYLER POLLOCK
38
Agricultual
December
LARRY POPE
29
Agricultual
December
1H SMITH
68
Agricultual
Agricultual
December
LARRY WILLIAMS
98
December
JC WILSON
57
Agricutural
Totals:
Annual (dry tons):
0
0
0 346
Amendment(s) used:
Bulking Agent(s) used:
* If more space is reauired_ attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
9
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
3487
Novozymes North America, Inc.
Laboratory: 1)
2)
3)
4)
5)
ENCO
Parameter
(mgfkg)
Ceiling
Conc.
Limit
Sample or Composite Date
Jan
Feb
Mar
Apr
May
Jun
Jul
Aug
Sep
Oct
Nov
Dec
Percent Solids (%)
NA
3.40
4.60
5.50
4.80
4.40
1.80
2.00
2.60
4.30
4.60
4.00
4.10
Arsenic
75
2.24
1.65
1.38
1.58
1.73
4.22
3.80
2.92
1.77
1.65
1.90
1.85
Cadmium
85
0.11
0.08
0.07
0.07
0.08
0.20
0.18
0.14
0.08
0.08
0.09
0.09
Copper
4,300
0.47
12.07
1.17
0.33
0.36
0.89
0.80
0.62
8.51
0.35
0.40
0.39
Chromium
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Lead
840
1.14
0.82
0.56
0.65
0.70
1.72
1.55
1.19
0.72
0.67
0.77
0.76
Mercury
57
0.04
0.03
0.03
0.02
0.02
0.01
0.08
0.03
0.02
0.02
0.02
0.00
Molybdenum
75
0.74
0.45
0.59
0.57
1.94
1.59
1.36
0.92
0.54
0.63
0.61
Nickel
420
1.14
_1.03
1.95
0.64
0.73
0.97
2.26
1.81
1.46
1.89
0.48
0.57
0.54
Selenium
100
1.82
1.35
1.13
1.29
1.41
3.44
3.10
2.38
1.44
1.35
1.55
1.51
Zinc
7,500
11.97
38.48
5.15
2.62
23.86
11.67
4.00
6.00
35.12
1.99
3,70
1.07
Total Phosphorus
NA
1,029
5,000
7,455
5,208
7,045
11,111
26,000
6,923
8,605
6,957
13,250
6,341
TKN
NA
11,765
14,783
38,182
29,167
29,545
8,333
85,000
33,077
22,093
26,087
12,000
8,049
Ammonia -Nitrogen
NA
2,471
2,000
2,000
3,750
2,955
8,333
4,650
5,000
2,163
2,609
4,500
1,829
Nitrate and Nitrite
NA
300
220
178
523
115
72236
397
443
154
194
138
211
a For surface disposal faclities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
3487
Novoyzmes North America, Inc.
Laboratory:
1)
2)
3)
4)
5)
ENCO
Sample or Composite Date
Parameter
(mg/kg)
Jan
Feb
Mar
Apr
May
Jun
Jul
Aug
Sep
Oct
Nov
Dec
Aluminum
2,333
7.294
544
134
2,426
126
1,852
246
7,068
1,618
75
132
Magnesium
733
1.163
378
42
464
389
20
233
1,246
53
411
29
Calcium
55,111
60,196
20,000
55,769
56,596
55,652
71,379
57,917
65,424
68,529
43,947
46,042
Potassium
9,778
10,961
4,600
7,885
8,830
12,370
19,138
12,000
6,458
13,618
10,342
8,208
Sodium
4.622
6,020
2,400
4,769
4,957
5,848
12,069
7,354
4,017
10,382
5,079
5,521
PAN
12,816
29,618
5,300
13,628
11,554
13,216
26,044
8,797
12,764
17330
10,664
25,427
SAR
1.15
1.50
1.52
1.27
1.23
1.45
1.64
1.83
1.03
1.56
1.29
1.55
pH
12.29
11.93
11.92
12.49
12.14
12.15
12.2
12.1
12.1
12.1
12.1
12.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
an*, Tnrv�._
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Z//o/z.t
Date
DENR FORM RSSF - B (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Novozymes North America, Inc. WQ Permit Number: 3487
WWTP Name: NPDES Number:
Monitoring Period: From 1/1/2021 To 3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Alt. A (time/temp) Li I Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing)p
Process to Further Reduce Pathogengs ❑
Class A:
AIt.D (No Prior Test) 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Thermophilic ❑
Compost ❑
B eta Ray ❑
Heat Drying 0
Gamma Ray ❑
Heat Treatment 0
Pasteurization ❑
Alt. (I) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens L=I
Class B:
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Digestion ❑
Lime Stabilization ❑
Anaerobic Digestion ❑
If applicable to alternative perfo
Number of
Allowable Level
Excee-
in Sludge dences
Air Drying ❑
Composting ❑
Parameter
Fecal Coliform
2x10tothe
bth power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative per formea:
Al 4 (Spec.02uptake) ❑
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Alt.1 (VS reduction)
LI
Alt. 5 (I4-Day Aerobic) ❑
Alt. 9 (Injection) ❑
Pathogen Density
Minimum
Geo. Mean
Maximum
Units
<3.0
MPN/4g
Alt. 2 (40-day bench) ❑
Alt. 6 (Alk. Stabilization ID
Alt. 10 (Incorporation) El
0
El
QTLY
G
EPA 1682
Alt. 3 (30-day bench) t.
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Chase McGee Environmental Manager
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
O'>L 914/Q/ 2/%/12.
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Signature of Preparer*
Facility Name: Novozymes North America, Inc.
WWTP Name:
Monitoring Period: From
4/1/2021
To
WQ Permit Number:
NPDES Number:
6/30/2021
3487
tion (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
a
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ■
Alt. C (Prior Testing)12
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ■
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying❑
Heat Treatment
■
Thermophilic
•
Beta Ray •
Gamma Ray❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly
Reduce Pathogens
•
•
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization •
Air Drying ■
Composting ❑
Aerobic Digestion •
Anaerobic Digestion 0
I
_
If applicable to alternative performed (Class A or Class B) complete the following monitoring. data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Excee-
,it_.,,`c,s
Frequency
Analysis
Y
Sample
T pe
y
Analytical
Tech-nique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2xI0tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
<3.0
MPN/4g
0
QTLY
G
EPA 1682
raction Reduction (1 SA NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench)
j
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
Ll
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
12
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
0
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
,.,,,
No vector attraction reduction alternatives were performed
U
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Chase McGee Environmental Manager
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
aV1/1-- 7/44AA-- 71A/2
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Novozymes North America, Inc. WQ Permit Number:
WWTP Name: NPDES Number:
Monitoring Period: From 7/1/2021 To 9'30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Alt. C (Prior Testing)8
3487
Class A:
Alt. A (time/temp) ❑
A1t.D (No Prior Test) 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Thennophilic ❑ j
Compost ❑
Beta Ray ❑
Gamma Ray❑
Pasteurization ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Digestion
Class B:
Alt. (1) Fecal Density ❑
Lime Stabilization ❑ l
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Number of
Frequency Sample
Excee-
of Analysis Type
denres
Parameter
Fecal Coliform
Allowable Level
in Sludge
2 x 10 to the
6th power
per gram of
total solids
\ 1PN
CFU
1000 mpn per gram
of total solid (dry
weight)
Minimum
Pathogen Density
Geo. Mean
Maximum
Units
Analytical
Tech-nique
3 MPN per 4 grams
total solid (dry MPN 4g
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 4 (Spec. O, uptake) ❑
Alt. 8 (Drying - Unstable) 0
No vector attraction reduction alternatives were performed ❑
Salmonella bacteria
(in lieu of fecal
coliform)
A lt.1 (VS reduction)
Alt. 5 (14-Day Aerobic) ❑
Alt. 9 (Injection)
CERTIFICATION STATEMENT (please check the appropriate statement)
U "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Chase McGee Environmental Manager
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
<3.0
Alt. 2 (40-day bench) ❑
Alt. 6 (Alk. Stabilization p
Alt. 3 (30-day bench) ❑
Alt 7 (Drying - Stable) 0
J
Signature of Preparer*
Heat Drying❑
Alt B (Alk Treatment) ❑
Process to Further Reduce Pathogengs ❑
Heat Treatment ❑
Air Drying ❑ { Composting ❑
0
QTLY
G
EPA 1682
Alt. 10 (Incorporation) ❑
Cam- /14/1/kt ZIP&
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Lime Stabilization Cl
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Discstinn
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Sample
Type
Parameter
Fecal Coliform
Compost ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Thermophilic ❑
Beta Ray ❑
Facility Name: Novozym.es North America, Inc.
WWTP Name:
Monitoring Period: From
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Alt. C (Prior Testing)0
10/1/2021
WQ Permit Number:
NPDES Number:
12.`31/2021
3487
Class A:
Alt. A (time/temp) .3
Alt.D (No Prior Test)
Alt B (Alk Treatment)C
Process to Further Reduce Pathogengs ❑
Heat Drying❑
Gamma Ray❑
Pasteurization El
Class B: Alt. (1) Fecal Density ❑ I Alt. (2) Process to Significantly Reduce Pathogens ❑
Allowable Level
in Sludge
2x10tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 4 (Spec. O, uptake) Li
Minimum
Heat Treatment ❑
Air Drying ❑ IComposting ❑
Pathogen Density
Geo. Mean
To
Maximum
Units
Number of
Excee-
rlenres
Frequency
of Analysis
Analytical
Tech-nique
Salmonella bacteria
(in lieu of fecal
coliform)
Alt.1 (VS reduction)
Alt. 5 (14-Day Aerobic) ❑
Alt. 9 (Injection) ❑
<3.0
Alt. 2 (40-day bench)
Cl
Alt. 6 (Alk. Stabilization 0
Alt. 10 (Incorporation) ❑
MPN/4g
Alt. 3 (30-day bench)
Alt 7 (Drying - Stable)
0
QTLY
G
EPA 1682
Alt. 8 (Drying - Unstable) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Chase McGee Environmental Manager
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
21114
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

AKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Novozymes North America Inc.
Date
FFI 96 (SBM Initial)
FHG 409(SBMIWAS Initial)
FHG 407A (>2 Hour pH)
FLF 96 24 Hour pH
Operator
initials
pH
Temp *C
Corr.
Factor
Corr.
pH
Time
pH
Temp 'C
Corr.
Factor
Corr
pH
Time
pH
Temp "C
Corr.
Factor
Corr.
pH
Time
pH
Temp `C
Corr.
Factor
Corr.
pH
Time
1/9/2021
12.26
25.00
0.00
12.26
4:00 AM
12.31
25.00
0.00
12,31
4:00 AM
12.23
25.00
0.00
12.23
6:03 AM
socr
1/10/2021
12.23
15.00
-0.3
11.93
8:00 AM
socr
4/16/2021
12.42
25.00
0.00
12.42
6:05 PM
12.10
25.00
0.00
12.10
6:05 PM
12.47
25.00
0.00
12.47
8:14 PM
socr
4/17/2021
12.69
17.00
-0.24
12.45
7:00 PM
socr
7/2/2021
12.02
25.00
0.00
12.02
11:00 AM
12.10
25.00
0.00
12.10
11:00 AM
12.12
25.00
0.00
12.12
1:19PM
socr
7/3/2021
12.17
26.00
0.03
12.20
1:00 PM
socr
10/2/2021
12.2
25
0.00
12.20
2:30 PM
12.40
25
0.00
12.40
2:30 PM
12.1
25
0.00
12.10
4:46 PM
socr
10/3/2021
12.20
24.00
-0.03
12.17
1:00 PM
socr
0,w4A,
Signature
FFI 96, FHG409, and FHG407 readings are from pH probes
FLF 96 pH is manually read from lab pH meter within 15 min. of taking sample
7/iezt,
Date

HOOSIER MICROBIOLOGICAL
H TT A I
TM
L A BOR A T o R Testing • Research • Consulting
Multiple Analysis Report
Sample: 403966
February 8, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:21 AM,
1/6/2021, and collected at 10:00 AM, 1/5/2021:
TEST - METHOD RESULT MDLk Date Complete
Solids, total-SM 2540G 4.49% 0.005% 1/13/2021
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 1/8/2021
*Minimum Detection Level
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincere) `` —
Donald A. Hendrickson, Ph.D.
President.- Micropiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN47303-1702 Phone: [phone] Fax:[phone]
E-mail: 102255.I52L7a compuserve. com Web Site: http://www.hmicom
Page: 1

HOOSIER MICROBIOLOGICAL
LVA
L A BOR A TOR Y
Sample: 403967
February 8, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
Testing •
Multiple Analysis Report
Research • Consulting
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:21 AM,
1/6/2021, and collected at 10:00 AM, 1/5/2021:
TEST - METHOD
Solids, total-SM 2540G
Salmonella -EPA 1682
Helminth Ova-EPA/625/R-921013
*Minimum Detection Level
RESULT
1.56%
<3 MPN/4 g dry
<1 ovum/4g dry
MDL*
0.005%
3 MPNl4 g dry
1 ovum/4 g dry
Date Complete
1/13/2021
1/12/2021
2/5/2021
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Plunge: [phone] Fax: [phone]
E-mail:. [e-mail] Web Site: lttip://www.lrml.com
Page: 1

HOOSIER MICROBIOLOGICAL
Hi.v A I
Th1
L ABOR ATORY
Sample: 408424
May 18, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:07 AM,
04/20/2021, and collected at 10:00 AM, 04/19/2021:
TEST - METHOD RESULT MDL* Date Complete
Solids, total-SM 2540G 4.23% 0.005% 04/22/2021
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 04/22/2021
'Minimum Detection Level
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincerely,elN
,f/rn,.de-s a.. Ai.... o -J... _
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone]
E-mail: 102255.152®compuserve.com Web Site: http://www.hml.cam
Page: 1

HOOSIER MICROBIOLOGICAL
LYA
L A B OR A T 0 Iz x Testing •
Multiple Analysis Report
Sample: 408423
May 18, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
Research • Consulting
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:07 AM,
04/20/2021, and collected at 10:00 AM, 04/19/2021:
TEST - METHOD
Solids, totat-SM 2540G
Salmonella -EPA 1682
Hetminth Ova-EPA/625/R-92/013
*Minimum Detection Level
RESULT
1.51 %
<3 MPN/4 g dry
<1 ovum/4g dry
MDL*
0.005%
3 MPN/4 g dry
1 ovum/4 g dry
Date Complete
04/22/2021
04/22/2021
05/18/2021
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincerely,
re/Y,N.-o- mot_ N-a 1 d-
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGailierd, Muncie, IN 47303.1702 Phone: [phone] Fax: [phone]
E-mail:102255.152Qcompuserve.com Web Site: http://www.hmtcom
Page: 1

HOOSIER MICROBIOLOGICAL
HI v A 4
7r�1
L A B O R ATORY
Sample: 412847
August 9, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Testing • Research • Consulting
Multiple Analysis Report
Dear Sir/Madam:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:02 AM,
7/8/2021, and collected at 9:00 AM, 7/7/2021:
TEST - METHOD RESULT MDL* Date Complete
Solids, total-SM 2540G 4.68% 0.005% 7/14/2021
Salmonella -EPA 1682 <3 MPNI4 g dry 3 MPN/4 g dry 8/12/2021
*Minimum Detection Level
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone]
E-mail: [e-mail] Web Site: http://www.11ml. com
Page: 1

HOOSIER MICROS IOLOGI CAL
L'A
L
1
4
1111
L ABOR A T 0 R Y Testing • Research • Consulting
Multiple Analysis Report
Sample: 412848
August 9, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:02 AM,
7/8/2021, and collected at 9:00 AM, 7/7/2021:
TEST - METHOD RESULT MDL* Date Complete
Solids, total-SM 2540G 1.34% 0.005% 7/14/2021
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 8/13/2021
Helminth Ova-EPA/625/R-92/013 <1 ovuml4g dry 1 ovum/4 g dry 8/5/2021
*Minimum Detection Level
This testing was completed by T.K. Please feel free to contact us if we can be of further service to you.
Sincerely,
1 61. ,tr,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone]
E-mail: [e-mail] Web Site: http://www.hml.coni
Page: 1

HOOSIER MICROBIOLOGICAL
H LTA LEI
L A BOR AT O R x Testing • Research • Consulting
Multiple Analysis Report
Sample: 419069
November 1, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Sir/Madam:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 12:39 PM,
10/05/2021, and collected at 10:00 AM, 10/04/2021:
TEST - METHOD RESULT MDL* Date Complete
Solids, total-SM 2540G 3.74% 0.005% 10/08/2021
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 10/07/2021
*Minimum Detection Level
This testing was completed by T.K. and K.L. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone]
E-mail: I02255.152@a compuserve.cofn Web Site: http://www.hmLcon:
Page: 1

HOOSIER MICROBIOLOGICAL
Hli
L ,A B OR A T () R Y
Sample: 419068
November 1, 2021
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Testing •
Multiple Analysis Report
Research • Consulting
Dear Sir/Madam:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 12:39 PM,
10/05/2021, and collected at 10:00 AM, 10/04/2021:
TEST - METHOD
Solids, total-SM 2540G
Salmonella -EPA 1682
Heiminth Ova-EPA/625/R-92/013
*Minimum Detection Level
This testing was completed by T.K. and K.L. Please feel free to contact us if we can be of further service to you.
Sincerely,
Q _ 1•f .
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
RESULT
1.34%
<3 MPN/4 g dry
<1 ovum/4g dry
MDL*
0.005%
3 MPN/4 g dry
1 ovum/4 g dry
Date Complete
10/08/2021
10/07/2021
10/29/2021
912 West McGalfiard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone]
E-mail: 102255.152 a@compuserve. com Web Site: http://www.hmt com
Page: 1

ENCO Laboratories
Accurate. Timely. .Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, January 19, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD20533
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, January 5, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable, This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL
This report relates only to the sample as received b/ the laboratory, and may only be reproduced in full. Page 1 of 13

www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CO20533-01
Sampled: 01/05/21 03:50
Received: 01/05/21 09:50
Parameter Preparation
CSU Method NO PREP
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 {CAL[}
EPA 353.2 NO PREP
EPA 6010D EPA 3005A
EPA 7470A EPA 7470A
SM 2540B-2011 NO PREP
SM 2540D-2011 NO PREP
SM 5210 8-2011 NO PREP
SM 5220D-2011 Same
Hold DatelTlme(sl
10/01/23
02/02/21
02/02/21
01/07/21 03:50
01/07/21 03:50
02/02/21
07/04/21
02/02/21
01/12/21
01/12/21
01/07/21 03:50
02/02/21
prey DatelTime(s).
Analysis Date/Time(sk
01/06/21 08:30 01/06/21 13:49
01/07/21 08:15 01/07/21 11:08
01/06/21 07:16 01/12/21 10:29
01/05/21 15:20 01/05/21 17:16
01/14/21 08:50 01/14/21 12:48
01/14/21 08:50 01/19/21 12:48
01/06/21 08:30 01/06/21 12:53
01/07/21 10:34 01/08/21 10:00
01/07/21 17:25 01/07/21 17:25
01/07/21 16:12 01/07/21 16:12
01/06/21 11:30 01/06/21 11:30
01/08/21 09:06 01/08/21 15:28
Client ID: SBM
Lab ID: CD20533-01RE 1
Parameter Preparation
EPA 365.4 Same
Hold DateIT1me(s1
02/02/21
Sampled: 01/05/21 03:50
prep Date/Time(s)
01/06/21 07:17
Received: 01/05/21 09:50
Analysis Date/Timers)
01/12/21 13:04
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 2 of 13

www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CD20533-01
Analvte
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Lead - Total
Magnesium - Total
Nickel - Total
Nitrate as N
Nitrate/Nitite as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
Results En MDL POL DIM
105 0.420 1.00 mg/L
84 D 4.0 9.0 mg/L
12000 2.0 2.0 mg/L
2480 0.390 1.00 mg/L
33000 800 800 mg/L
0.0386 I 0.0310 0.100 mg/L
33.0 0.290 1.00 mg/L
0.0388 I 0.0220 0.100 mg/L
10 D 0.82 2.0 mg/L
10 D 0.82 2.0 mg/L
0.20 0.017 0.10 mg/L
440 1.50 5.00 mg/L
208 4.00 5.00 mg/L
1.15 [blank]
400 D 52 96 mg/L
3.4 0.12 0.12 % by Volume
2700 250 250 mg/L
0.407 0.0440 0.100 mg/L
Method
EPA 6010D
EPA 350.1
SM 5210 8-2011
EPA 6010D
SM 5220D-2011
EPA 6010D
EPA 6010D
EPA 6010D
EPA 353.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 6010D
CSU Method
EPA 351.2
SM 25408.2011
SM 2540D-2011
EPA 60100
Client ID: SBM Lab ID: CD20533-01RE1
Analrte Results Flag !7f?!. EOL units Notes
Phosphorus 35 D 0.50 2.0 mg/L EPA 365.4
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 3 of 13

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID: CD20533-01
Sampled:01/05/21 03:50
Sampled By:Ray Dixon
Received: 01/05/21 09:50
Work Order: CD20533
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified araahte [NC 591]
pnalvte FCAS Numberl
Mercury [7939-97-6]^
Results E1ag
0.00150 U
WADE
mg/L
PE M01 PQ.L Batch
10 0,00150 0.00200 1A07025
Method
EPA 7470A
Analyzed RV =RE
01/08/21 10:00 KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certiVedanaNteINC 591]
Anatvte FCAS Numberl
Aluminum [7429-90-5]^
Arsenic [7490-38-2]^
Cadmium [7440-43-9]"
Calcium [7440-70-2]^
Copper[7440-50-8]^
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nidcel[7440-02-0]^
Potassium [7440-09-7]"
Selenium [7782-49-21"
Sodium [7440-23-5]^
Zinc [7440-66-6] ^
Results Eiia Llitl la MIL r'% Elm Method Aiabrassi !fix
105 mg/L 10 0.420 1.00 1A05030 EPA 6010D 01/06/21 12:53 JDH
0.0760 U mg/1 10 0.0760 0.100 1A05030 EPA 6010D 01/06/21 12:53 JDH
0.00360 U mg/1. 10 0.00360 0.0100 1A05030 EPA 60100 01/06/21 12:53 JDH
2480 mg/L 10 0.390 1.00 1A05030 EPA 6010D 01/06/21 12:53 JDH
0.0160 U mg/L 10 0.0160 0-100 1A05030 EPA 6010D 01/06/21 12:53 3DH
0.0386 3 mg/L 10 0.0310 0.100 1A05030 EPA 6010D 01/06/21 12:53 3DH
33.0 mg/L 10 0.290 1.00 1A05030 EPA 6010D 01/06/21 12:53 JDH
0.0250 U mg/L 10 0.0250 0.100 1A05030 EPA 60100 01/06/21 12:53 3DH
0.0388 J mg/L 10 0.0220 0.100 1A05030 EPA 6010D 01/06/21 12:53 3DH
440 mg/L 10 1.50 5.00 1A05030 EPA 6010D 01/06/21 12:53 3DH
0,0620 U mg/L 10 0.0620 0.100 1A05030 EPA 6010D 01/06/21 12:53 JDH
208 mg/L 10 4.00 5.00 1A05030 EPA 6010D 01/06/21 12:53 JDH
0.407 mg/L 10 0.0440 0.100 1A05030 EPA 6010D 01/06/21 12:53 3DH
Classical Chemistry Parameters
^ - ENCO Cary certified anaryte INC 591]
gpalvte FCAS Numberl ROrdill2 flag Molts /2E MJ POI, Batdt Method An.s]]tzg B1 Eisacs
Ammonia as N [7664-41-7]^ 84 D mg/L 90 4.0 9,0 1A07012 EPA 350.1 01/07/21 11:08 JAH
Biochemical Oxygen Demand^ 12000 mg/L 1 2.0 2.0 1A06009 SM 521013-2011 01/06/21 11:30 JOC
Chemical Oxygen Demand^ 33000 mg/L 80 800 800 1A08004 SM 5220D-2011 01/08/21 15:28 JOC
Nitrate as N [14797-55-8] 10 D mg/L 20 0.82 2.0 [CALC] EPA 353,2 01/19/21 12:48 JAH
Nitrate/Nitrite as N^ 10 D mg/L 20 0.82 2.0 1A14006 EPA 353.2 01/14/21 12:98 JAH
Nitrite as N [14797-65-0]^ 0.20 mg/L 1 0.017 0.10 1A05034 EPA 353.2 01/05/21 17:16 JAH
Phosphorus [7723-14-0] ^ 35 D mg/L 20 0.50 2.0 1A06008 EPA 365.4 01/12/21 13:04 JAH
Sodium Adsorption Ratio 1.15 [blank] 1 1A05030 C51I Method 01/06/21 13:49 JDH
Total Kjeldahl Nitrogen,' 400 D mg/L 200 52 96 1A06007 EPA 351.2 01/12/21 10:29 JAH
Total Solids^ 3.4 % by Volume 25 0.12 0.12 1A07023 SM 254013-2011 01/07/21 17:25 DMJ
Total Suspended Solids^ 2700 mg/L 100 25D 250 1A07022 SM 2540D-2011 01/07/21 16:12 DMJ
FINAL This report relates only to the sample es received Dy the laboratory, and may only be reproduced In Cut. Page Al of 13

QUALITY CONTROL DATA
Metals by EPA 6(100/7000 Series Methods - Quality Control
Batch 1A07025 - EPA 7470A
[Blank (1A07025-BLK1)
Prepared: 01/07/2021 10:34 Analyzed: 01/08/2021 09:15
1
Analvte
Mercury
Spike Source
Result Ma POI. 1JniSg Level Result
0.000150 U 0.000200 mg/L
1_,LCS(1A07025-BS1)
Analvte
Mercury
&suit flan ROL Units
0.00503 0.000200
mglL
%REC RPD
%REC Limns RPD Limit Ng
Prepared: 01/07/2021 10:34 Analyzed: 01/08/202109:22
1
Spike
Level
0.00500
Source
Result
%REC
%REC Limits
101
80-120
RPD
RPD Limit
Matrix Spike (1A07025-MS1)
Prepared: 01/07/2021 10:34 Analyzed: 01/08/2021 09:27
Source: CD20320-03
Analvte
Mercury
Result Elan PQL
0.00524 0.000200
Unite
mg/L
Spike Source
Level Result
0.00500 0.000150 U
%REC RPD
%REC Limits RPD Limit Note&
105
75-125
Matrix Spike Dup (1A07025-MSD1)
Prepared: 01/07/2021 10:34 Analyzed: 01/08/2021 09:30
Source: CD20320-03
Anakke
Mercury
Result Has P l Units
0.00545 0.000200
mg/L
Spike
Level
0.00500
Source
8.2.10
0.000150 U
%REC
%REC mi RPD
109
75-125
4
Post Spike (1A07025-PS1)
Prepared: 01/07/2021 10:34 Analyzed: 01/08/2021 09:33
Source: CD20320-03
Anal
Mercury
Spike Source %REC
Result Elan P_QL Units Level Result %REC Limits RPD
5.90
0.200
ug/L
5.00 -0.149 118 75-125
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1A05030 - EPA 3005A
RPD
Lit&
25
RPD
Limit
Notes
1
Blank (1A05030-BLKI)
Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 10:50
1
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result Else POL Units Level Result %REC limits RPD Limit Notes
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 rn9/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
RPD
LCS (1A05030-B51) Prepared: 01/05/2021 13:19 Analyzed; 01/06/2021 10:56
jatifte
Aluminum
Arsenic
FINAL
Spike Source
Result Els P.QL Units Level EMIL
1.98 0.100 mglL 2.00
0.188 0.0100 rn9/L 0.200
%REC
%REC Limits
99 80-120
94 80-120
This report relates only to the sample as received by the laboratory, and may miry be reproduced in fuK.
RPD
RPD Limit itiQl�i
Page 5 of 13

www.encolabs.com
QUALITY CONTROL DATA
G.
•
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1A05030 - EPA 3005A - Continued
LCS (1A05030-BS1) Continued
Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 10:56
1
Analvte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Mut PDL Units Level
0.0191 0.00100 mg/L 0.0200
1.99 0.100 mg/L 2.00
0.189 0.0100 m9/1- 0.200
0.198 0.0100 mg/L 0.200
1.97 0.100 mg/L 2.00
0.187 0.0100 mg/L 0.200
0.198 0.0100 mg/L 0.200
10.1 0.500 mg/L 10.0
0.194 0.0100 mg/L 0.200
10.1 0.500 mg/L 10.0
0.193 0.0100 mg/L 0.200
Source
lit
%REC
%REC limits
96 80-120
100 80-120
95 80-120
99 80-120
98 80-120
93 80-120
99 80-120
101 80-120
97 80-120
101 80-120
96 80-120
RPD
RPD Limit
Matrix Spike (1A05030-MS1)
Source: CD20532-01
�BDaiXYR
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Racer}
9.92
0.938
0.0941
118
0.937
0.960
14.0
0.946
0.972
413
0.975
459
0.990
Elan POL
0.500
0.0500
0.0050E
0.500
0.0500
0.0500
0.500
0.0500
0.0500
2.50
0.0500
2.50
0.0500
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 10:59
Spike Source %REC RPD
Level g %REC Units RPD L!m!I N" otes
10.0 0.210 U 99 75-125
1.00 0.0380 U 94 75-125
0.100 0.00180 U 94 75-125
10.0 106 118 75-125
1.00 0.00800 U 94 75-125
1.00 0.0155 U 96 75-125
10.0 4.22 98 75-125
1.00 0.0125 U 95 75-125
1.00 0.0110 U 97 75-125
50.0 357 110 75-125
1.00 0.0310 U 98 75-125
50.0 403 112 75-125
1.00 0.0220 U 99 75-125
Matrix Spike Dup (1A05030-MSD1) Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 11:08
1
Source:CD20532-01
ltnnlbcrP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Flaa POI Units Level Result %REC Lrmits RPD Limit NOM
9.76 0.500 mg/L 10.0 0.210 U 98 75-125 2 20
0.895 0.0500 mg/L 1.00 0.0380 U 90 75-125 5 20
0.0913 0.00500 mg/L 0.100 0.00180 U 91 75-125 3 20
103 0.500 mg/L 10.0 106 NR 75-125 13 20 QM-07
0.913 0.0500 mg/L 1.00 0.00800 U 91 75-125 3 20
0.937 0.0500 mg/L 1.00 0.0155 U 94 75-125 2 20
13.2 0.500 mg/L 10.0 4.22 90 75-125 6 20
0.920 0.0500 mg/L 1.00 0.0125 U 92 75-125 3 20
0.940 0.0500 mg/L 1.00 0.0110 U 94 75-125 3 20
366 2.50 mg/L 50.0 357 17 75-125 12 20 QM-07
0.914 0.0500 mg/L 1.00 0.0310 U 91 75-125 7 20
407 2.50 mg/L 50.0 403 9 75-125 12 20 QM-07
0.947 0.0500 mg/L 1.00 0.0220 U 95 75-125 4 20
FINAL
Thls report relates only to the sample es received by the laboratory, and may only be reproduced in full. Page 6 of 13

QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
www.encolabs.com
Batch 1A05030 - EPA 3005A - Continued
Post Spike (1A05030-PS1)
Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 11:11
Source: CD20532-01
Analyte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
1.95
0.202
0.0194
21.7
0.193
0.200
2.67
0.198
0.201
77.0
0.201
85.3
0.204
MR POI
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0,200
10.0
0.200
Source
Result
0.0198
-0.00470
-9.96E-5
21.2
-0.000146
0.00132
0.814
-0.000242
0.000891
71.5
-0.000473
80.6
0,000293
%REC
%REC Limits
96 80-120
101 80-120
97 80-120
25 80-120
96 80-120
99 80-120
91 80-120
99 80-120
100 80-120
55 80-120
102 80-120
48 80-120
102 80-120
RPD
RPD Limit ht4LefL
QM-08
QM-08
QM-08
Classical Chemistry Parameters - Quality Control
Batch 1405030 - EPA 3005A
[Blank (1A05030-BLKI)
Prepared: 01/05/2021 13:19 Analyzed: 01/06/2021 13:50
1
Acolyte
Sodium Adsorption Ratio
Batch 1A05034 - NO PREP
Resit Mu PQL Unita
0.00 U [blank]
Spike
Level
Source
Result
%REC RPD
%REC Limits RPD Limit
Blank (1A05034-BLK1)
Prepared: 01/05/2021 15:20 Analyzed: 01/05/2021 17:11
1
Analyte
Nitrite as N
Result Ilan
0.017 U
Spike Source
PO- Units Level Rest %REC Limits RPD Limit -
0.10 mg/L
%REC
RPD
[LCS(1A05034-BS1)
Prepared: 01/05/2021 15:20 Analyzed: 01/05/2021 17:27
1
Analvte
Nitrite as N
Result Hog
1.0
P2
0.10
Units
mg/L
Spike Source %REC RPD
Level RIB& %REG MailRPD Limit EMIL
1.00
105
90-110
Matrix Spike (1A05034-MS1)
Prepared: 01/05/2021 15:20 Analyzed: 01/05/2021 17:13
Source: CD20532-01
Analvte
Nitrite as N
Spike Source
Result Hag POI Units Level Result
1.6 0.10 mg/L 1.00 0.61
Matrix Spike Dup (1A05034-MSD1)
Source: CD20532-01
%REC
%REC Limits
100 90-110
RPD
RPD Limit Notes_
Prepared: 01/05/2021 15:20 Analyzed: 01/05/2021 17:14
Spike Source %REC RPD
_MAIM Elae PQL S1nRIB Level Ewa %REC Limits RPD Limit
Nitrite as N 1.6 0.10 mg/L 1.00 0.61 100 90-110 0.04 10
Batch 1A06007 - Same
FINAL
This report relates only to the sample as received by the laboratory, and may onry be reproduced in full. Page 7 of 13

www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1A06007 - Same - Continued
Blank (1A06007-BLK1)
9nande
Total Kjeldahl Nitrogen
Prepared: 01/06/2021 07:16 Analyzed: 01/12/2021 09:58
1
Result Eke
U
0.26
PQL
0.48
Spike Source
Units Level Result %REC Limits RPD lima Notes
mg/L
%REC
RPD
-LCS(1A06007-BS1)
Total Kjeldahl Nitrogen
BesuIt Elea PQL
13
0.48
Units
mg/L
Prepared: 01/06/2021 07:16 Analyzed: 01/12/2021 10:19
Spike
Level
12.0
Source
jtesult
%REC
%REC Limits
107
90-110
1
RPD
RPD Limit NOTAL
[Matrix Spike (3A06007-MS1)
Source: CD19545-01
_Mahan
Total Kjeldahl Nitrogen
Prepared: 01/06/2021 07:16 Analyzed: 01/12/2021 10:22
1
Result EI ga POL
6.7
0.48
Molts
mg/L
Spike
Level
4.80
Source
Result
1.7
%REC
%REC Limits RPD
106
90-110
RPD
Limit
Notes
Matrix Spike (1A06007-MS2)
Prepared: 01/06/2021 07:16 Analyzed: 01/12/2021 10:28
Source: CDi9586-01
Analvte
Total Kjeldahl Nitrogen
Result Bps Pn&
0.26 U
0.48
Units
mg/L
Spike
Level
4.80
Source
Bead
0.26 U
%REC
%REC limits
90-110
RPD
RPD Limit Notes
QM-07
Matrix Spike Dup (1A06007-MSD1)
Source: CD19545-01
Analvte
Total Kjeldahl Nitrogen
Batch 1406008 - Same
Prepared: 01/06/2021 07:16 Analyzed: 01/12/2021 10:24
Spike Source
Re511F BOB .ink Units Level Regal
5.2 0.48 mg/L 4.80 1.7
1
%REC RPD
%REC L ti_ RPD -mit Notes
72 90-110 27 10 QM-07,
QM-11
Blank (1A06008-BLK1)
Prepared: 01/06/2021 07:17 Analyzed: 01/12/2021 11:53
Y
Amble
e
Phosphorus
Spike Source
Result Bag PAL Units Level Result %REC Limits RPD Limit Notes
0.025 U
0.10
mg/L
%REC
RPD
f LCS (1A06008-851)
Analvte
Phosphorus
Prepared: 01/06/2021 07:17 Analyzed: 01/12/2021 11:54
Spike Source
Result Flag PQL ry jeel Level Result
1.6 0.10 mg/L 1.60
%REC
%REC Limits
102 80-120
RPD
RPD Limit )
1
Matrix Spike (1A06008-MS1) Prepared: 01/06/2021 07:17 Analyzed: 01/12/2021 11:57 1
Source: CD19545-01
Analvte
Phosphorus
EMAIL Hag
5.1 D
PQL
1.0
Spike
Unita Level
mg/L
0.640
Source
1m!
4.8
%REC
53
%REC
Liles
B0-120
RPD
RPD Ling fIS
QM-07
[Matrix Spike Dup (1A06008-MSD1)
Source: CD19545-01
Phosphorus
Batch 1A06009 - NO PREP
Prepared: 01/06/2021 07:17 Analyzed: 01/12/2021 11:59
Spike Source
Bond Elan PQL il.Oi3a Level ABIlt %REG
5.3 D 1.0 mg/L 0,640 4.8
%REC
Limits
1
RPD
RPD Limit M1[otes
85 80-120 4 25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In lull.
Page 8 of 13

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
EMMI
Batch 1A06009 - NO PREP - Continued
Blank (1A06009-BLK1)
•••••••• m
Analvte
Prepared &Analyzed: 01/06/2021 11:30
Biochemical Oxygen Demand
Remelt S4
2.0 U
PQL Units
2.0 mg/L
Spike Source
Level Result
www.encolabs.com
%REC
%REC Limits RPD
LCS (1A06009-BS1)
Prepared &Analyzed: 01/06/202i 11:30
Analvte
Biochemical Oxygen Demand
Spike
Result Elan Pal Unita Level
200
2.0
mg/L
198
source
Result
%REC
%REC Limits RPD
103
85-115
RPD
Limit
NAM
RPD
Limit motes
Duplicate (1A06009-DUP1)
Prepared & Analyzed: 01/06/2021 11:30
Source: CD19591-01
Analvte
Biochemical Oxygen Demand
Batch 1A07012 - NO PREP
Result Ilan
180
POL units
2.0 mg/L
Spike
Level
Source
Result
180
1
%REC RPD
%REC Limits RPD Limit Noteet
0.3 30
Blank (1A07012-BLK1)
Prepared: 01/07/2021 08:15 Analyzed: 01/07/2021 10:51
Analvte
Ammonia as N
Result BOA
0.045 U
ROL Units
mg/L
0.10
Spike Source
Level )result
%REC
%REC Limits RPD
RPD
Lim Notes
[LCS (1A07012-BS1)
Prepared: 01/07/2021 08:15 Analyzed: 01/07/2021 10:53
Anaivte
Ammonia as N
Result Elan
1.0
PS8. Units
mg/L
0.10
Spike Source
Level Result
1.01
%REC
104
%REC
Limits RPD
90-110
RPD
Limit
Matrix Spike (1A07012-MSI)
Prepared: 01/07/2021 08:15 Analyzed: 01/07/2021 10:56
1
Source: CD20532-01
Anglixte
Ammonia as N
Spike
Result Elan PQL Units Level
3.1
[Matrix Spike (1A07012-MS2)
Source: CD20532-0I
Analvte
Ammonia as N
Matrix Spike Dup (1A07012-MSD11
Source: CD20532-01
Analvte
Ammonia as N
Batch 1A07022 - NO PREP
0.10
mg/L
0.393
Source
Result
2.8
%REC
%REC Limits RPD
78
90-110
RPD
Limit !L
QM-07
Prepared: 01/07/2021 0B:15 Analyzed: 01/07/2021 11:05
1
Spike
Remit Elasi POL Units Level
Blank (1A07022-BLK1)
Total Suspended Solids
0.42 0.10 mg/L
Result Man
3.1 E
POI Units
0.10 mg/L
0.393
Source
Bann
0.12
%REC
77
%REC
kW& RPD
90-110
RPD
Limi
Notes
QM-07
Prepared: 01/07/2021 08:15 Analyzed: 01/07/2021 10:58
1
Spike Source
Level &RA
0.393 2.8
%REC
%REC Limits RPD
88 90-110 1
RPD
Limit
10
NOM
QM-07
Prepared & Analyzed: 01/07/2021 16:12
Spike
&milt Idea AIL Units Level
2.5 U
2.5 mg/L
Source %REC
leesult %REC JUMLIE RPD
RPD
Litlit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 13

www.encolabs.com
QUALITY CONTROL DATA
1
Classical Chemistry Parameters - Quality Control
Batch 1A07022 - NO PREP - Continued
LCS(1A07022-851)
Prepared & Analyzed: 01/07/2021 16:12
Analvte
Total Suspended Solids
Result Flan ErL Units
110
2.5
mg/L
Spike
Level
100
Source
R211 it
%REC
%REC Linajja
108
80-120
RPD
RPD Limit
Duplicate (1A07022-DUP1)
Prepared & Analyzed: 01/07/2021 16:12
Source: CO20996-01
Analvte
Total Suspended Solids
Result Elan
98
PAL Units
50 mg/L
Spike Source
Level Result %REC Limits RPD
110
%REC
8
RPD
Laaa
20
Duplicate (1A07022-DUP2)
Source:CD19591-01
Analyte
Total Suspended Solids
Batch 1A07023 - NO PREP
Prepared & Analyzed: 01/07/2021 16:12
Spike Source
Result Bag PQL Units Level R u %REC jimits RPD MBA Notes
97 83 mg/L 120 19 20
1
%REC
RPD
[Blank (1A07023-BLK1)
Prepared & Analyzed: 01/07/2021 17:25
1
Attabde
Total Solids
Result Elora
0.0050 U
POL Units Level
0.0050 % by Volume
Spike Source
RR¢u ft
%REC
RPD
%REC Limits RPD Lima Natal_
LLC5(1A07023-BS1)
Prepared & Analyzed: 01/07/2021 17:25
Total Solids
Result flag
1100
PQ.L
50
Units
mg/L
Spike
Level
1100
Source
3 1t
%REC RPD
%REC Limits RPD Limit Notes
101
90-110
Duplicate (1A07023-DUP1)
Prepared & Analyzed: 01/07/2021 17:25
1
Source: CD19567-01
Analvte
Total Solids
Batch IA011004 - Same
Remit Flan
0.028
Spike Source
POL Units Level Result
0.010 % by Volume
0.026
%REC RPD
%REC Limits RPD Limit
4
5
[Blank (1A08(104-BLK1)
Prepared: 01/08/2021 09:06 Analyzed: 01/08/2021 15:28
1
Analvte
Chemical Oxygen Demand
@sash! Elan
10 U
Spike
�4L Units Level
10
mg/L
Source
Result
%REC RPD
%REC Limits RPD LILLt Notes
LLCS(1A08004-B51)
Analvte
Chemical Oxygen Demand
Prepared: 01/08/2021 09:06 Analyzed: 01/08/2021 15:28
1
Spike
Result Elan PQL Units Level
520
10
mg/L
500
Source
%REC RPD
%REC imi RPD Limit N,_Qt
104
90-110
Matrix Spike (1A08004-MS1)
Prepared: 01/08/2021 09:06 Analyzed: 01/08/2021 15:28
Source: CD17371-01
Analvte
Chemical Oxygen Demand
$pike Source
Result Elm PQI Units Level BASIS
1800 20 mg/L 1000 790
%REC
%REC Limits
101 90-110
RPD
RPD L(plit
Note_
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 10 of 13

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1A08004 - Same - Continued
www.encola bs.com
Matrix Spike Dup (1A08004-MSD1)
Prepared: 01/08/2021 09:06 Analyzed: 01/08/2021 15:28
Source: CD17371-01
Analvte
Chemical Oxygen Demand
Batch 1A14006 - NO PREP
Blank (1A14006-BLk1)
Analvte
Nitrate/Nitrite as N
Spike Source %REC RPD
Result Elfin POL Units Level Result %REC Limits RPD Limit Notes_
1800 20 mg/L 1000 790 99 90-110 1 5
Prepared: 01/14/2021 08:50 Analyzed: 01/14/2021 I2:24
1
Result Elan
0.041 U
Spike Source WoREC RPD
PAL Millis Level Result %REC Limits RPD Limit Naies.
0.10 mg/L
LCS(.414006-BS3)
Prepared: 01/14/2021 08:50 Analyzed: 01/14/2021 12:26
1
Analvte
Nitrate/Nitrite as N
Spike
Result Elea POI Units Level
1.3
0.10
mg/L
1.25
Source
Result
%REC
%REC Limits RPD
104
90-110
RPD
VAdt
Nobel
Matrix Spike (1A14006-MS1)
r.
Prepared: 01/14/2021 08:50 Analyzed: 01/14/2021 12:30
1
Source: CD19647-01
Analvte
Nitrate/Nitrite as N
Result Flea P01 Quits
1.0
0.10
mg/L
Spike
Level
0.521
Source
Result
0.41
a/%REC RPD
%REG grail RPD Limit
112
90-110
Notes
QM-07
Matrix Spike (1A14006-M52)
Prepared: 01/14/2021 08:50 Analyzed: 01/14/2021 12:35
1
Source: CD19648-01
Analvte
Nitrate/Nitrite as N
Result Flea EQL. Quits
0.57
0.10
mg/L
Spike Source
Level Result
0.041 U
0.521
%REC
%REC Lindu
109
90-110
RPD
RPD Limit Notes
Matrix Spike Dup (1A14006-MSDI)
Prepared: 01/14/2021 08:50 Analyzed: 01/14/2021 12:32
1
Source: CD19647-01
Analvte
Nitrate/Nitrite as N
Spike Source
Result Etas PQ1. Units Level Result
0.98 0.10 mg/L 0.521 0.41
%REC
%REC Llmlt5
109 90-110
RAD
RPD Limit
2 10
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 af 13

FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
{CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
F1NAL This report relates only to the sample as received by the I;3horate-;, and may only be reproduced in full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY � RECORD
10775 Central Port Dr 4810 Executive Park Court Suite 117
CI
Orlando. FL 32824 Jacksonvtue- FL 32218.6069 Cary NC 27511
(4071826-5314 1904)250-3007 Fax )9041296.6210 19191407.30E0 Fax [phone]
Client Name
Novezy mee North America (NOON)
Address
77 Perry Chapel Church Road
CilyfSTrzip
Fraf>tdintfDn, NC 27625
Fax
Protect Humber
jnonel
Propel Name Disc
Monthly - Week One - SBM
rd
(919) 494-30
Po r Birttnq Into
3800465333
Reporting Cornet
5amp''edal Na •, AIhl 'nnq
aottl
Samplers =1 S
Scab: Creech
Wang Canted
Accounts Payable
Site Location I Time Zone
www.encolabs.com
Page _ of _
Requested Anelysee
11
§ § F
Preservation (See Codes) ICorfSna as names, 1
11em$
Sample ID (Field Idenulicahonl
SBM
Collection Dale
Collection
Tame
frfitifilw
1Aalnx
Comp / Grab Iwo cedes)
Tate) a of
Contemn
x
x
x
x
x
htequesie0 I Df natDuilu
Times
Ncre Rush requests subfect to
acceptance by the facility
Standard
Expedited
Due / /
Lab Workorder
CD20533
Sample Comments
e Kd Prup<rred fay
Co ants/Special Rapmting Requirements
D` atte vinery
1l1 i V
Rail mpg By
Rea
-- Total ri of Containers
Dnerfrrre � Received 8� ��/ s ��l i
" Ica 4r -
Da.teiflme Reamed 8y
Melt
ReIe qurshed 0y
GOder Is 6 Temps On Receipt
Gate/Time
Received By
Gr(,�-ill
Date/Tana • 5
DatelT,e L? S V
Delerfime
Receipt
Acceptable _ Unacceptable
Matrix OW -Groundwater SO-SaI OW -Drinking Water SE4ote s Smpes sabr tiedWatl EN VlLebs are
A -Air dance th the et c s nentsid co
Preorvauon: r-rrr H.HCI N-HNO3 S-H2594 NO-Ne1JH 0-other (delel In comments)
Nola AN samples s+rbmdtad 10 F1VG0 Labs are in accordance with the terms and conditions Yeted on the rrverse of this brm, unless prior wreten agreements exist

Sample Preservation Verification
ENCO Cary
Work Order CD20533 Project: Monthly - Week One - SBM
Client Novozymes North America (NO008) Project #: [none]
Logged By: John C King
Date/Time: / `) 2 / /'f
Logged in 05-Jan-21 10:25
Preservation Check Performed By:
5�1
CD20533-01
Cont
Type
1
2
250mLP+H2SO4
250mLP+HNO3
Reagent Name
ffu'3
t17SoLf
Pres (pH)
Requirement
<2
<2
pH Checked 1
In Control
Y/ i NA
Y11N]lNA
pH Adjusted
Date/Time
Adjusted
�Y r N / NA f.S'.21 /[�!
Y Icy NA
ID Reagent Name
{ "o Vo(1)'.
pH Strip ID: CY0i ) "5-
3
ID
5
6
Reagent Used/Comments
L //256'/
) 7j v L H4/L/3
Reagent Name ID
C:IELMNT1Printlwko_PreservationCheck. rpt
Page 1 of 1

ENCO Laboratorks
Accurate. Timely. Responsive. _Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, February 15, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CEOI.077
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, February 2, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosu re(s)
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
1
Client ID: SBMN Lab ID: CE01077-01
Sampled: 02/02/21 08:40 Received: 02/02/21 09:15
Parameter Preparation
CSU Method NO PREP
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 [CALC]
EPA 353.2 NO PREP
EPA 365.4 Same
EPA 6010D EPA 3005A
EPA 7470A EPA 7470A
SM 2540B-2011 NO PREP
SM 25400-2011 Same
SM 5210 B-2011 NO PREP
SM 52200-2011 Same
paid Date/Time(s]
10/29/23
03/02/21
03/02/21
02/04/21 08:40
02/04/21 08:40
03/02/21
03/02/21
0B/01/21
03/02/21
02/09/21
02/09/21
02/04/21 08:40
03/02/21
Prep Date(Time(s) Analysis Date/Times]
02/03/21 08:40 02/03/21 14:54
02/10/21 09:12 02/12/21 13:39
02/04/21 11:59 02/11/21 12:11
02/02/21 15:29 02/02/21 18:11
02/09/21 08:04 02/09/21 12:13
02/09/21 08:04 02/09/21 12:13
02/04/21 12:00 02/11/21 14:48
02/03/21 08:40 02/03/21 13:37
02/04/21 11:01 02/05/21 17:24
02/05/21 13:03 02/05/21 13:03
02/08/21 14:53 02/09/21 09:11
02/03/21 11:35 02/03/21 11:35
02/08/21 11:35 02/08/21 15:07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 2 of 13

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SAMPLE DETECTION SUMMARY
r
Client ID: SUM Lab ID: GEO1077-01
Malybe Results Flag MDL PQL Units Mtn
Aluminum - Total 372 0.420 1.00 mg/L EPA 6010D
Ammonia as N 92 D 4.0 9.0 mg/L EPA 350.1
Biochemical Oxygen Demand 11000 2.0 2.0 mg/L SM 5210 B-2011
Calcium - Total 3070 0.390 1.00 mg/L EPA 6010D
Chemical Oxygen Demand 37000 800 800 mg/L SM 5220D-2011
Copper - Total 0.555 0.0160 0.100 mg/L EPA 6010D
Lead - Total 0.0377 3 0.0310 0.100 mg/L EPA 6010D
Magnesium - Total 59.3 0.290 1.00 mg/L EPA 6010D
Molybdenum - Total 0.0976 3 0.0250 0.100 mg/L EPA 6010D
Nickel - Total 0.0898 3 0.0220 0.100 mg/L EPA 6010D
Nitrate as N 9.9 D 0.41 1.0 mg/L EPA 353.2
Nitrate/Nitrite as N 10 D 0.41 1.0 mg/L EPA 353.2
Nitrite as N 0.23 0.017 0.10 mg/L EPA 353.2
Phosphorus 230 D 12 50 mg/L EPA 365.9
Potassium - Total 559 1.50 5.00 mg/L EPA 6010D
Sodium - Total 307 4.00 5.00 mg/L EPA 6010D
Sodium Adsorption Ratio 1.50 [blank] CSU Method
Total Kjeldahl Nitrogen 680 D 52 96 mg/L EPA 351.2
Total Solids 4.6 0,0050 0.0050 % by Volume SM 2540B-2011
Total Suspended Solids 22000 2.5 2.5 mg/L SM 2540D-2011
Zin: - Total 1.77 0.0440 0.100 mg/L EPA 6010D
FINAL
This report relates only to the sample as received try the laboratory, and may only be reproduced In Full. Page 3 of 13

ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID: CE01077-01
Sampled:02/02/21 08:40
Sampled By:John C Hilliard Jr
Metals by EPA 6000/7000 Series Methods
^ . ENCO Cary certified anaiyte INC 591]
pnalvt@ [CAS Numbed
Mercury [7439-97-6]^
Resulhs nig
0.00150 U
Units
mg/L
www.encolabs.com
Received: 02/02/21 09:15
Work Order: CE01077
PE EQL IWO
10 0.00150 0.00200 11303021
Method
EPA 7470A
Analyzed lilt Notes
02/05/21 17:24 KAH
i
[Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyse INC 591]
Analvte [CAS Numbed
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Calrrum [7440-70-2]^
Copper[7440-50-8]^
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel[7440-02-0]^
Potassium [7440-09-7]^
Seenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc [7440-66-61^
Results Elan Units DF MU PQL Batch Method Analyzed I}JC
372 mg/L 10 0,420 1.00 1802028 EPA 6010D 02/03/21 13:37 JDH
0.0760 U mg/L 10 0.0760 0.100 1802028 EPA 6010D 132/03/21 13:37 JDH
0.00360 U mg/L 10 0.00360 0.0100 1802028 EPA 6010D 02/03/21 13:37 JDH
3070 mg/L 10 0.390 1.00 1602028 EPA 6010D 02/03/21 13:37 JDH
0.555 mg/L 10 0.0160 0.100 11302028 EPA 6010D 02/03/21 13:37 3DH
0.0377 J mg/L 10 0.0310 0.100 11302028 EPA 6010D 02/03/21 13:37 JDH
59.3 mg/L 10 0.290 1.00 1802028 EPA 601013 02/03/21 13:37 JDH
0.0476 3 mg/L 10 0,0250 0.100 1802028 EPA 6010D 02/03/21 13:37 JDH
0.0898 J m9/L 10 0,0220 0.100 1802028 EPA 6010D 02/03/21 13:37 JDH
559 mg/L 10 1.50 5.00 1802028 EPA 60100 02/03/21 13:37 JDH
0.0620 U mg/L 10 0.0620 0.100 1802028 EPA 6010D 02/03/21 13:37 JDH
307 mg/L 10 4.00 5.00 1802028 EPA 6010D 02/03/21 13:37 3DH
1.77 mg/L 10 0.0440 0.100 1802028 EPA 6010D 02/03/21 13:37 JDH
Classical Chemistry Parameters
- ENCO Cary certified anal* INC 591]
Analvte [CAS Number'[
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand^
Chemical Oxygen Demand"
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus [7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
•
Notes
kesulis BBB Units DF hiPL EQL hatch Method he81Md ay Notes
92 D mg/L 90 4.0 9.0 11310015 EPA 350.1 02/12/21 13:39 JAH
11000 mg/L 1 2.0 2.0 1803003 SM 5210 B-2011 02/03/21 11:35 30C
37000 mg/L 80 800 800 11308006 SM 52200-2011 02/08/21 15:07 JOC
9.9 D mg/L 10 0.41 1.0 [CALC] EPA 353.2 02/09/21 12:13 JAH
10 D mg/L 10 0.41 1.0 1809005 EPA 353.2 02/09/21 12:13 JAH
0.23 mg/L 1 0.017 0.10 11307039 EPA 353.2 02/02/21 18:11 JAH
230 D mg/1 500 12 50 1804025 EPA 365.4 02/11/21 14:48 JAH
1.50 [blank] 1 1B02028 CSU Method 02/03/21 14:54 3DH
680 D mg/L 200 52 96 1804024 EPA 351.2 02/11/21 12:11 JAH
4.6 % by Volume 1 0.0050 0.0050 1805008 SM 25405-2011 02/05/21 13:03 LJI
Classical Chemistry Parameters
Analvte [CAS Number]
Total Suspended Solids
r � -
Results flag Unit DF ]yQJ. POI, B8.til Method Air alvaed fl Notes
22000 mg/L 1 2.5 2.5 1808014 SM 2540D-2011 02/09/21 09:11 AMP
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
1
Batch 1E103022 - EPA 7470A
Blank (1803021-BLK1)
Prepared: 02/03/2021 11:01 Analyzed: 02/05/2021 16:59
1
Analvte
Mercury
Spike
Result Elan P_QL Units Level
0.000150 U 0.000200
mg/L
Source
Result
%REC
%REC Limits RPD
RPD
Limit
Notes
LCS(1B03021-BS1)
Prepared: 02/03/2021 11:01 Analyzed: 02/05/2021 17:02
Analvte
Mercury
Result Ban PQL
0.00563 0.000200
Units
mg/L
Spike
Level
0.00500
Source
13t
%REC
%REC Limits
113
80-120
RPD
RPD Limit Notes
[Matrix Spike (1B03021-MS1)
Source: CE01204-01
Analvte
Mercury
Prepared: 02/03/2021 11:01 Analyzed: 02/05/2021 17:07
Result
0.00548
Elast PQL
0.000200
Units
mg/L
Spike Source
Level Result 44REC
0.00500 0.000150 U 110
%REC
Limits
75-125
RPD
RPD Ld 4
N9L
[Matrix Spike Dup (1B03021-MSD1)
Prepared: 02/03/2021 11:01 Analyzed: 02/05/2021 17:09
Source: CE01204-01
nal
Mercury
Result Etas POI Units
0.00551 0.000200
mg/L
Spike
Level
0.00500
Source %REC RPD
Result %REC inkiltA RPD Limit Notes_
0.000150 U 110
75-125
0.6
25
Post Spike (11303021-PS1)
Prepared: 02/03/2021 11:01 Analyzed: 02/05/2021 17:12
Y
Source: CE01204-01
Analvte
Mercury
Result Mg
6.05
FQL
0.200
Spike
Molts Level
ug/L
5.00
Source
Result
-0.0600
%REC RPD
%REC -mi RPD Limit Nobel
121
75-125
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1802028 - EPA 3005A
Blank (11302028-BLK1)
Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 12:52
1
Analvte
Aluminum
Arsenic
Cadmium
Calaum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result Flan EQL Units Level Ancuu
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
RPD
%REC Limits RPD Limit n2.ni
LCS (1B02028-BS1) Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 12:58
1
Analvte
Aluminum
Arsenic
FINAL
Spike Source
Result Mao PQL lints Level ggg g
2.10 0.100 mg/L 2.00
0.195 0.0100 mg/L 0.200
%REC
%REC Limits
105 80-120
98 80-120
This report relates only to the sample as received ny the laboratory, and may only he reproduced In full.
RPD
RPD limit Notes
Page 5of13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
1
Batch 1E02028 - EPA 3005A - Continued
LCS(11302028-BSI) Continued
Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 12:58
Aoalvte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result Elan POI Units Level BMA& %REC Li RPD
0.0198 0.00100 mg/L 0,0200 99 80-120
2.05 0.100 mg/L 2.00 102 80-120
0.201 0.0100 mg/L 0.200 101 80-120
0.206 0.0100 mg/L 0.200 103 80-120
2.10 0.100 mg/L 2.00 105 80-120
0.197 0,0100 mg/L 0.200 98 80-120
0.208 0.0100 mg/L 0.200 104 80-120
10.8 0.500 mg/L 10.0 108 80-120
0.200 0.0100 mg/L 0.200 100 80-120
10.8 0.500 mg/L 10.0 108 80-120
0.204 0.0100 mg/L 0.200 102 80-120
[Matrix Spike (1802028-MS1)
Source: CE01204-01
Anal vte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
RPD
mi
Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 13:01
Spike Source %REC
Result Elam PQL Units Level Result %REC lamlts RPD
2.17 0.100 mg/L 2.00 0.113 103 75-125
0.194 0.0100 mg/L 0.200 0.00760 U 97 75-125
0.0191 0.00100 mg/L 0.0200 0.000360 U 95 75-125
6.61 0.100 mg/L 2.00 4.83 89 75-125
0.258 0,0100 mg/L 0.200 0.0659 96 75-125
0.195 0.0100 mg/L 0.200 0.00310 U 98 75-125
3.81 0.100 mg/L 2.00 1.85 98 75-125
0.298 0.0100 mg/L 0,200 0.111 93 75-125
0.202 0.0100 mg/L 0.200 0.00220 U 101 75-125
13.8 0.500 mg/L 10.0 3.63 102 75-125
0.194 0.0100 mg/L 0.200 0.00620 U 97 75-125
80.4 0.500 mg/L 10.0 73.1 72 75-125
0.232 0.0100 mg/L 0.200 0.0303 101 75-125
RPD
Limit
Notea
QM-07
[Matrix Spike Dup (1B02028-MSD1) Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 13:03
Source: CE01204-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %RISC
Result Flan P4L !!nits Level gesuft %REC Limits RPD
2.20 0.100 mg/L 2.00 0.113 104 75-125 2
0.198 0.0100 mg/L 0.200 0.00760 U 99 75-125 2
0.0195 0.00100 mg/L 0.0200 0.000360 U 98 75-125 2
6.77 0.100 mg/L 2.00 4.83 97 75-125 2
0.265 0.0100 mg/L 0.200 0.0659 99 75-I25 2
0.197 0.0100 mg/L 0.200 0.00310 U 99 75-125 1
3.90 0.100 mg/L 2.00 1.85 102 75-125 2
0.305 0.0100 mg/L 0.200 0.111 97 75-125 3
0.207 0.0100 mg/L 0.200 0.00220 U 103 75-125 2
14.0 0.500 mg/L 10.0 3.63 104 75-125 1
0.199 0.0100 mg/L 0.200 0.00620 U 99 75-125 2
82.4 0.500 mg/L 10.0 73.1 93 75-125 2
0.238 0.0100 mg/L 0.200 0,0303 104 75-125 3
RPD
limit
20
20
20
20
20
20
20
20
20
20
20
20
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1B02028 - EPA 3005A - Continued
Post Spike (1802028-P51)
Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 13:06
Source: CE01204-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
2.22
0.199
0.0203
6.75
0.265
0.203
3.95
0.310
0.212
14.0
0.201
81.0
0.243
flan POL
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
Classical Chemistry Parameters - Quality Control
Batch .1802028 - EPA 3005A
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike Source %REC
Level Result %REC Limits
2.00 0.113 106 80-120
0.200 0.00198 99 80-120
0.0200 1.11E-6 101 80-120
2.00 4.83 96 80-120
0.200 0.0659 100 80-120
0.200 -0.000456 102 80-120
2.00 1.85 105 80-120
0.200 0.111 99 80-120
0.200 0.00196 105 80-120
10.0 3.63 104 80-120
0.200 0.00261 99 80-120
10.0 73.1 79 80-120
0.200 0.0303 106 80-120
RPD
RPD Limit 1131321..
QM-08
[Blank (1B02028-BLK1)
Prepared: 02/02/2021 12:47 Analyzed: 02/03/2021 14:55
1
Analvte
Sodium Adsorption Ratio
Batch 1802039 - NO PREP
Result flag POI L!nhta
0.00 U [blank]
Spike Source
Level Result
%REC RPD
%REC Limits RPD ii lit:
Blank(1802039-BLK1)
Prepared: 02/02/2021 15:29 Analyzed: 02/02/2021 18:03
Ansilite
Nitrite as N
134611it Elan
0.017 U
Spike
POL Units Level
0.10
mg/L
Source
$!&slit
%REC
RPD
%REC Limits RPD Limit
NoteL
ILCS (1B02039-B51)
Prepared: 02/02/2021 15:29 Analyzed: 02/02/2021 18:15
i
Anaivte
Nitrite as N
Result 1 POL
0.95
0.10
Units
mg/L
Spike Source
Level Eesult
1.00
%REC RPD
%REC Limits RPD mi Note_
95
90-110
Matrix Spike (1802039-MS1)
Prepared: 02/02/2021 15:29 Analyzed: 02/02/2021 18:05
1
Source: CE00946-01
MaMe
Nitrite as N
Spike Source
Result Elan PM !Hilts Level ROM
1.00 0.017
1.0
0.10
mg/L
%REC RPD
%REC Limits RPD Limit l ei
100
90-110
[Matrix Spike Dup (1B02039-MSD1)
Prepared: 02/02/2021 15:29 Analyzed: 02/02/2021 18:06
1
Source: CE00946-01
Analvte
Nitrite as N
Batch IB03003 - NO PREP
Spike Source %REC RPD
$snit Flan PQL Units Level &Ea %REC Limits RPD 12mi
1.0 0.10 mg/L 1.00 0.017 100 90-110 0.5 10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1803003 - NO PREP - Continued
[Blank (1B03003-BLK1)
Prepared & Analyzed: 02/03/2021 11:35
1
Analvte
Biochemical Oxygen Demand
Spike
Result NAP PQL Units Level
2.0 U
2.0
mg/L
Source
Result %REC RPD Limit Notes
%REC
RPD
[LCS(1B03003-BS1)
Prepared & Analyzed: 02/03/2021 11:35
1
Analvte
Biochemical Oxygen Demand
Result fIM
190
P9L
2.0
Units
mg/L
Spike Source
Level Result
198
%REC RPD
%REC Limits RPD limit flaw_
94
85-115
Duplicate (1B03003-DUP1)
Prepared &Analyzed: 02/03/2021 11:35
Source: CD12371-01
jalvW
Biochemical Oxygen Demand
Batch 1504024 - Same
Spike Source %REC RPD
Result flan PQL Units Level Result %REC Limits RPD Ling Notes
2.1 2.0 mg/L 2.2 4 30
[Blank (1804024-BLK1)
Prepared: 02/04/2021 11:59 Analyzed: 02/11/2021 11:28
1
Analvte
Total Kjeldahl Nitrogen
Result Elam
0.26 U
Spike
PDL Moils Level
0.48
mg/L
Source
Result
%REC
%REC limit*
RPD
RPD Limit Notes
1LCS(1B04024-BS1)
Analvte
Total Kjeldahl Nitrogen
Prepared: 02/04/2021 11:59 Analyzed: 02/11/2021 11:30
Result Egg
13
Spike Source
PAL Units Level Result
0.48 mg/L
12.0
%REC
%REC Limits
110
90-110
RPD
RPD Linii
Matrix Spike (1B04024-MSL)
Prepared: 02/04/2021 11:59 Analyzed: 02/11/2021 11:33
Source: CD19650-01
Analvte
Total Kjeldahl Nitrogen
Result flan
54 D
PAL
4.8
liras
mg/L
Spike Source
Level Result %REC
4.80 48
138
%REC RPD
Limits RPD L n!
90-110
Notes.
QM-07
[Matrix Spike (1804024-M52)
Source: CE00106-01
AnAlitIF
Total Kjeldahl Nitrogen
Bssult Flag PAL
120 D
4.8
Units
mg/L
Prepared: 02/04/2021 11:59 Analyzed: 02/11/2021 11:38
Spike Source
Level Result
4.80
110
%AEC
%REC Limits
205
90-110
RPD
RPD limit
i
Notes_
QM-07
Matrix Spike Dup (1B04024-MSD1)
Prepared: 02/04/2021 11:59 Analyzed: 02/11/21321 11; 35
Source: CD19650-01
_naly e
Total Kjeldahl Nitrogen
Batch 1804025 - Same
Spike Source %REC RPD
Result Pion Units Level ague %REC Limits RPD Limit Notes
52 0 4.8 mg/L 4.80 48 95 90-110 4 10
Blank (1B04025-BLK1)
Prepared: 02/04/2021 12:00 Analyzed: 02/11/2021 14:20
1
Analvte
Phosphorus
Result 1E180 P24 Units
0.025 U 0.10 mg/L
Spike Source
Level BM&lt
%REC
%REC Limits
RPD
RPD Unlit NQt8L
FINAL This report relates only to the sample es received by the laboratory, and may only be reproduced in full.
Page 8ui13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1E04025 - Same - Continued
LCS(11304025-0S1)
Prepared: 02/04/2021 12:00 Analyzed: 02/11/2021 14:21
Anah�
Phosphorus
Result Hag
1.6
P91. Units
mg/L
0.10
Spike
Level
1.60
source
Result
%REC
%REC Limits
100 80-120
RPD
RPD Limit Nlli;�
Matrix Spike (1804025-MS1)
Source: CD19650-01
Analvte
Phosphorus
Result lag PQL
7.4 D
1.0
Units
mg/L
Prepared: 02/04/2021 12:00 Analyzed: 02/11/2021 14:24
Spike
Level
0.640
Source
Bradt
6.6
%REC RPD
%REC Lam¢ RPD Wit Notes
128
80-120
QM-07
',Matrix Spike Dup (1804025-MSD1)
Source: CD19650-01
Analvte
Phosphorus
Batch 1805008 - NO PREP
Prepared: 02/04/2021 12:00 Analyzed: 02/11/2021 14:25
Spike Source
Result Han PQL Units Level Result
7.8 D 1.0 mg/L 0.640 6.6
9+aREC RPD
%REC Limits RPD inrr it
196 80-120 6
25
Notes-
QM-07
Blank (1B05008-BLK1)
Prepared & Analyzed: 02/05/2021 13:03
Analvte
Total Solids
Result Ban POI llnitS Level
0.0050
U 0.0050 % by Volume
Spike Source
Boat
%REC RPD
%REC lmi RPD Limit Nei
LCS(1805008-BS1)
Prepared & Analyzed: 02/05/2021 13:03
1
Total Solids
Result fiso PQL Units
1100
50
mg/ L
Spike Source
Level Result %REC
1100
99
%REC
Limits
90-110
RPD
RPD Limit
Duplicate (11305008-DUP1)
Prepared & Analyzed: 02/05/2021 13:03
Source: CE01108-04
Analvte
Total Solids
Batch 11308006 - Same
Spike
Result Flit PQL Units Level
0.039
0.0050 % by Volume
Source
Result
0.039
%REC RPD
%REC Limits RPD Limit Notes.
0 5
Blank (0B013006-BLK1)
Prepared: 02/08/2021 11:35 Analyzed: 02/08/2021 15:07
1
Analvte
Chemical Oxygen Demand
LCS (1808006-BS1)
ADaivie
Chemical Oxygen Demand
Result Flan
10 U
Spike Source
Units Level Result %REC Limits RPD Limit No s
10 mg/L
%REC
Prepared: 02/08/2021 11:35 Analyzed: 02/08/2021 15:07
Spike
Result Flag PS& Units Level
530
10
mg/L
500
Source
B!
%REC
%REC Limits RPD
106
90-110
RPD
RPD
Umit
Notes
Matrix Spike (11308006-MS1)
Source: CD21052-01
Analvte
Chemical Oxygen Demand
Prepared: 02/08/2021 11:35 Analyzed: 02/08/2021 15:07
Spike Source
Result gag ROL Units Level MEd
580 10 mg/L 526 33 104 90-110
1
%REC RPD
%REC limits RPD Limit NQts
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fut.
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1608006 - Same - Continued
Matrix Spike Dup (1B08006-MSD1)
Prepared: 02/08/2021 11:35 Analyzed: 02/08/2021 15:07
1
Source: CD21052-01
Analvte
Chemical Oxygen Demand
Batch 1809005 - NO PREP
Spike Source %REC RPD
Result Flag P_01. Units Level Result 0/%REC Limits RPD Limit Notes
570 10 mg/L 526 33 102 90-110 1 5
Blank (1B09005-BLK1)
Prepared: 02/09/2021 08:09 Analyzed: 02/09/2021 11:39
1
Nitrate/Nitrite as N
Result Bag
0.041 U
Spike Source
P21 Units Level Bela %REC Limits RPD
0.10 mg/L
%REG
RPD
Limit
NAIL
LCS(1B09005-BS1)
Prepared: 02/09/2021 08:04 Analyzed: 02/09/2021 11:40
•
Analvte
Nitrate/Nitrite as N
Result
1.3
Spike
Flee P01. Units Level
0.10
mg/L
1.25
Source
Result
%REC RPD
%REC Limits RPD Limit
107
90-110
Matrix Spike (11309005-MS1)
Prepared: 02/09/2021 08:04 Analyzed: 02/09/2021 11:44
Source: CD15610-01
Andlvte
Nitrate/Nitrite as N
Remit Flan PQL omits
0.74
0.10
mg/L
Spike
Level
0.521
Source
Emit
0.19
%REC RPD
%REC Limits RPD i n t Noses,
104
90-110
[Matrix Spike (1B09005-M52)
Source: CD15610-02
Analvte
Nitrate/Nitrite as N
Prepared: 02/09/2021 08:04 Analyzed: 02/09/2021 11:49
Result ilia PQL Units
1.0
0.10
mg/L
Spike
Level
0.521
Source
Result
0.47
%REC
%REC Lines
103
90-110
RPD
RPD Limit Notes
Matrix Spike Dup (1B09005-MSD1)
Prepared: 02/09/2021 08:09 Analyzed: 02/09/2021 11:46
Source: CD15610-01
Analvte moult Flan PS2L
Nitrate/Nitrite as N 0.72
Batch 1910015 - NO PREP
Source
Result
0.10 mg/L 0.521 0.19
ni
Spike
Level
1
%RFC RPD
%REC UnftsRPD "mi Notes
101 90-110 2 10
Blank (1B10015-BLK1)
Prepared: 02/10/2021 09:12 Analyzed: 02/12/2021 13:06
1
Analvte
Ammonia as N
Result Elag
0.045 U
Spike
EQ1 units Level
0.10
mg/L
Source
Result
%REC
%REC Limits
RPD
RPD Li ri Notes
LCS(1B10015-BS1)
Prepared: 02/10/202109:12 Analyzed: 02/12/2021 13:08
r
Analvte
Ammonia as N
Result Flse PQL Units
1.0
0.10
mg/L
Spike
Level
1.01
Source
Result
%REC
%REC Lim
101
90-110
RPD
RPD Limit Notes
Matrix Spike (1B10015-MS1)
Prepared: 02/10/2021 09:12 Analyzed: 02/12/2021 13:11
1
Source:CE00105-01
Analvte
Ammonia as N
Spike Source
Result Fise PQL Units Level Result
7.9 1.0 mg/L 4.04 3.9 98 90-110
%REC
%REC Limits
RPD
RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fun.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1B10015 - NO PREP - Continued
Matrix Spike (1610015-MSZ)
Prepared: 02/10/2021 09:12 Analyzed: 02/12/2021 13:16
Source: CE00590-02
Analvte
Ammonia as N
Spike Source %REC RPD
Result Etas P.4L Units Level gilt %REG Limits RPD Limit Notes_
0.86
0.10
MIL
0.393 0.47
100
90-110
Matrix Spike Dup (1B10015-MSD1)
Prepared: 02/10/2021 09:12 Analyzed: 02/12/2021 13:13
1
Source: CE00105-01
Analvte
Ammonia as N
Remit flan P L
7.9
1.0
Spike
Units Level
mg/L
4,04
Source
BFPO
3.9
%REC RPD
%REC Limits RPD Limit NOYeS_
99
90-110
0.4
10
Classical Chemistry Parameters - Quality Control
Batch1B08014 - NO PREP
Blank (1608014-BLK1)
Prepared: 02/08/2021 14:53 Analyzed: 02/09/2021 09:11
Analvte
Total Suspended Solids
Result Flan
2.5 U
Spike Source
pf! Units Level Result %REC Limits RPD
2.5
mg/L
%REC
RPD
Limit
WM.
LCS(1608014-BS1)
Prepared: 02/08/2021 14:53 Analyzed: 02/09/2021 09:11
na
Total Suspended Solids
Result
95
Spike Source
Rau p94 Units Level Rglyjt
2.5 mg/L
100
%REG
%REC im
95
80-120
RPD
RPD Umit
Duplicate (11108014-DUP1)
Source: AE00820-01
Analvte
Total Suspended Solids
Prepared: 02/08/2021 14:53 Analyzed: 02/09/2021 09:11
1
Spike Source %REC RPD
Result Flag EQL Units Level Result %REC Lin_fik RPD Limit Notes,
380 2.5 mg/L 380 0 20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 13

(eisiEr4
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
iD The sample was analyzed at dilution.
3 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 12 of 13

aigeidaooeu f
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U1:1003L1 AUOISfI3-AO-NIVHO S31aOlVaO81/1 NOIIVAlGSNO01VIN31AINOEI1AN3

Sample Preservation Verification
ENCO Cary
Work Order: CE01077
Client: Novozymes North America (N0008)
Logged In 02-Feb-21 12:02
Preservation Check Performed By:
Cti
Project: Monthly - Week One - SBM
Project # [none]
Logged By: Rachel Ann Y ni t r� �f�,
Date/Time. 2.�h
1- L L�'O I \
CE01077-01
Cunt
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments
D
250rnLP+H2SO4
<2
/ / N / NA
Y/ N / NA Z4Z�j.I 125O
/J
Z Ci j
(l�L �`1
E
250mLP+HNO3
<2
Y 1' N / NA
,'j/ N 1 NA
_ - 7 L � alp"T
1
2
Reagent Name
ID Reagent Name
\A-NO3
pH Strip ID:
PH Strips C0F0555
C-Ielmnt1Prir«vvvp.u_r 1 e ur VdilUll�.necK.rpt
3
4
ID
Reagent Name
5l
H
6
Page 1

ENCO Laboratorws
Accurate. Timely. Responsive Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, March 16, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE03078
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, March 2, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosures)
FINAL
This report relates only to the sample as received 1y the I:bn-• and may only be reproduced In full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CE03078-01
Sampled: 03/02/21 02:00
Received: 03/02/21 08:15 I
Parameter Preparation
CSU Method EPA 3005A
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 (CALL]
EPA 3S3.2 NO PREP
EPA 6010D EPA 3005A
EPA 7470A EPA 7470A
SM 25408-2011 NO PREP
SM 25400-2011 NO PREP
SM 5210 6-2011 NO PREP
SM 5220D-2011 Same
Hold Date/Tme(sl
11/26/23
03/30/21
03/30/21
03/04/21 02:00
03/04/21 02:00
03/30/21
08/29/21
03/30/21
03/09/21
03/09/21
03/04/21 02:00
03/30/21
Prep Date/Time(sl Analysis Date/Time(s1
03/03/71 08:45
03/08/71 08:15
03/08/21 06:55
03/02/21 14:35
03/05/21 09:04
03/05/21 09:04
03/03/21 08:45
03/03/21 10:29
03/09/21 13:38
03/09/21 08:59
03/03/21 11:19
03/05/21 09:52
03/03/21 14:00
03/98/21 12:44
03/09/21 11:54
03/02/21 16:52
03/05/21 14:01
03/05/21 14:01
03/03/21 13:10
03/03/21 16:17
03/09/21 13:38
03/10/21 11:40
03/03/21 11:19
03/05/21 12:45
Client ID: SBM Lab ID: CE03078-01RE1
Sampled: 03/02/21 02:00 Received: 03/02/21 08:15
Parameter Preparation
EPA 365.4 Same
Hold Date/Time(s1
03/30/21
Prep Date/Tlme(sl
03/08/21 06:59
Analysis Date/Time(s]
03/09/21 15:55
FINAL
This report relates only to the sample as received by the iataratory, and may only be reproduced `n full. Page 2 of 13

Client ID: 58M
Anal e
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Copper - Total
Magnesium - Total
Nickel - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
www.encolabs.com
SAMPLE DETECTION SUMMARY
Lab ID: CE03078-01
1
Resu_ Ea.2 MDL Lc& Units Mood Nws
59.8 0.420 1.00 mg/L EPA 6010D
110 D 4.0 9.0 mg/L EPA 350.1
19000 2.0 2.0 mg/L SM 5210 B-2011 8-07
2200 0.390 1.00 m8/L EPA 6010D
38000 800 800 mg/L SM 52200-2011
0.0642 3 0.0160 0.100 mg/L EPA 6010D
41.6 0.290 1.00 mg/L EPA 6010D
0.0352 3 0.0220 0.100 mg/L EPA 6010D
9.6 D 0.41 1.0 mg/L EPA 353.2
9.8 D 0.41 1.0 mg/L EPA 353.2
0.20 0.017 0.10 mg/L EPA 353.2
506 1.50 5.00 mg/L EPA 6010D
264 4.00 5.00 mg/L EPA 6010D
1.52 [blank] CSUI Method
2100 D 26 48 mg/L EPA 351.2
5.5 0.0050 0.0050 % by Volume 5M 2540B-2011
200000 2.5 2.5 mg/L SM 2540D-2011
0.283 0.0440 0.100 mg/L EPA 6010D
_ Client ID: SBM Lab ID: CE03078-01RE1
ReEutts Ela4 t. PAL !l111ts ELet 141. Ego
AMMO
Phosphorus
410 D 5.0 20 mg/L
EPA 365.4
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

ANALYTICAL RESULTS
L
Description: SBM
Matrix: Sludge
Project Monthly - Week One - SBM
Lab Sample ID: CE03078-01
Sampled: 03/02/21 02:00
Sampled By:HUNTER WILSON
www.encolabs.com
Received: 03/02/21 08:15
Work Order: CE03078
Metals by EPA 6000/7000 Series Methods
- ENCO Cary certified analyte INC 591]
ppalvte FCAS Numbed
Mercury [7439-97-6]^
Results nig Mn!
MDL fQ1. 1 h Method
0.00150 U mg/L 10 0.00150 0.00200 1CO2019 EPA 7470A
Ana v ed
03/03/21 16:17
8Y Notes
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyteINC 591]
Aoalvte !CAS Number'[
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Calcium (7440-70-2]^
Copper[7440-50-8]^
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel[7440-02-0]^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc[7440-66-6]^
Results Boa Units RE Ma iQL MIA Method Analysed Ix Wm
59.8 mg/L 10 0.420 1.00 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.0760 U mg/L 10 0.0760 0.100 1CO2017 EPA 6010D 03/03/21 13:10 ]DH
0.00360 U mg/L 10 0.00360 0.0100 1CO2017 EPA 6010D 03/03/21 13:10 ]DH
2200 mg/L 10 0.390 1.00 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.0642 3 mg/L 10 0.0160 0.100 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.0310 U mg/L 10 0.0310 0.100 1CO2017 EPA 60101) 03/03/21 13:10 JDH
41.6 m9/L 10 0.290 1.00 1CO2017 EPA 60100 03/03/21 13:10 JDH
0.0250 U mg/L 10 0,0250 0.100 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.0352 3 mg/L 10 0.0220 0.100 1CO2017 EPA 6010D 03/03/21 13:10 JDH
506 mg/L 10 1.50 5.00 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.0620 U mg/L 10 0.0620 0.100 1CO2017 EPA 6010D 03/03/21 13:10 JDH
264 mg/L 10 4.00 5.00 1CO2017 EPA 6010D 03/03/21 13:10 JDH
0.283 mg/L 10 0.0440 0.100 1CO2017 EPA 6010D 03/03/21 13:10 JDH
Classical Chemistry Parameters
^ - ENCO Cary certified aralyte (NC 591]
Anaivte FCAS Numberl
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand^
Chemical Oxygen Demand^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Roads 1i4
110 D
19000
38000
9.6
9.6
0.20
410
1.52
2100
5.5
Classical Chemistry Parameters
Apaivte rCAS Number'{
Total Suspended Solids
Mk Of 11214 fQL =b. Method Analysed k Ms§
mg/L 90 4.0 9.0 1C08009 EPA 350.1 03/08/21 12:44 JAH
mg/L 1 2.0 2.0 1C03015 SM 5210 B-2011 03/03/21 11:19 JOC 8-07
mg/L 80 800 800 1C05006 SM 52200-2011 03/05/21 12:45 JOC
D mg/L 10 0.41 1.0 [CALC] EPA 353.2 03/05/21 14:01 JAH
0 mg/L 10 0.41 1.0 1C05005 EPA 353.2 03/05/21 14:01 JAH
mg/L 1 0,017 0.10 1CO2025 EPA 353.2 03/02/21 16:52 JAH
D mg/L 200 5.0 70 1C08004 EPA 365.4 03/09/21 15:55 3AH
[blank] 1 1CO2017 CSU Method 03/03/21 14:00 JDH
D mg/L 100 26 48 1C08003 EPA 351.2 03/09/21 11:54 JAH
% by Volume 1 0.0050 0.0050 1C09018 SM 25408-2011 03/09/21 13:38 U1
Reeklia ..e R.n1LE RE MU LQL Rohl Method &tined $Y MU
200000 mg/1 1 2.5 2.5 1C09008 SM 25400-2011 03/10/21 11:40 AAL
F1r4AL
This report relates only to the sample as ,e .cued by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1CO2019 - EPA 7470A
Blank(1CO2019-BLK1)
Prepared: 03/02/2021 11:45 Analyzed: 03/03/2021 15:54
1
Analvte
Mercury
Spike
Result Rao PAL Units Level
0.000150 U 0.000200
mg/L
Source
Result
%REC
%REC
RPD
RPD Limit l
LCS(1CO2019-BS1)
Prepared: 03/02/2021 11:45 Analyzed: 03/03/2021 16:01
Analvte
Mercury
Result Flag POL Units
0.00533 0.000200
mg/L
Spike
Level
0.00500
Source
Result
%REC RPD
%REC Limits RPD Limit
107
80-120
Oka -
Matrix Spike (1CO2019-M51)
Prepared: 03/02/2021 11:45 Analyzed: 03/03/2021 16:05
Source: CE03536-08
Analvte
Mercury
0.00517
Spike
Re�rrIt Flan PQL Units Level
0.00500
0.000200
mg/L
l
Source %REC RPD
Result %RFC Limits RPD Limit Notes
0.000150 U 103
75-125
Matrix Spike Dup (1CO2019-MSD1)
Prepared: 03/02/2021 11:45 Analyzed; 03/03/2021 16:08
Source: CE03536-OS
Analvte
Mercury
Result 17ao P._4L Units
0.00509 0.000200
mg/L
Spike Source
Level ksaWL
0.00500 0.000150 U
%REC
%REC Limits RPD
102
75-125
1
RPD
Limit Liao_
25
Post Spike (1CO2019-PS1)
Prepared: 03/02/2021 11:45 Analyzed: 03/03/2021 16:10
Source:CE03536-08
Analvte
Mercury
Spike
Result Flag PQL Units Level
5.65
0.200
ug/L
5.00
Source
Result
-0.0700
%REC
%REC Limits
113
75-125
RPD
RPD Limit
Notes
Meta15 (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1CO2017 - EPA 3005A
1
Blank (1CO2017-BLKL)
Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 10:10
1
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result Flag P0!. !nit!Mita Level ROWS %REC Limits RPD Limit
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0,0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
RPD
LCS (1CO2017-BS1) Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 10:26
Analvte
Aluminum
Arsenic
FINAL
Spike Source
Result Elm P01. Units Level Ewalt
2.01 0,100 mg/L 2.00
0.179 0.0100 mg/L 0.200
%REC RPD
WoREC Limits RPD Limit
100 80-120
89 80-120
This report relates only to the sample as received by the laboratory, and may ordy be reproduced in full.
Page 5 of 13

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QUALI1Y CONTROL. DATA
6
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1CO2017 - EPA 3005A - Continued
[LCS(1CO2017-851)Continued
Prepared: 03/02/2021 11:30 Anaiyzed:03/03/2021 10:26
Anatvte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %/oREC RPD
Result Rao P01< Units Level Real& D/nREC Limit RPD 'mit Notes.
0.0193 0.00100 mg/L 0.0200 97 80-120
1.98 0.100 mg/L 2.00 99 80-120
6.185 0.0100 mg/L 0,200 92 80-120
0.192 0.0100 mg/L 0.200 96 80-120
1.99 0.100 mg/L 2.00 99 80-120
0.183 0.0100 mg/L 0.200 91 80-120
0.194 0.0100 mg/L 0.200 97 80-120
10.2 0,500 mg/L 10.0 102 80-120
0.189 0.0100 mg/L 0.200 94 80-120
10.2 0.500 mg/L 10.0 102 80-120
0.193 0.0100 mg/L 0.200 97 80-120
[Matrix Spike (1CO2017-MS1)
Source: CE03185-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Poassium
Selenium
Sodium
Zinc
Result
2.33
0.201
0.0193
57.2
0.226
0.195
3.64
0.194
0.198
19.0
0.197
18.9
0.433
Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 10:29
1
•
Spike Source %REC RPD
Elan POL Unit. Level ESED t 9/%REC Limits RPD Limit Notes
0.100 mg/L 2.00 0.459 94 75-125
0.0100 mg/L 0.200 0.0115 95 75-125
0.00100 mg/L 0.0200 0.600360 U 96 75-125
0.100 mg/L 2.00 55.9 69 75-125
0.0100 mg/L 0.200 0.0375 94 75-125
0.0100 mg/L 0.200 0.00310 U 97 75-125
0.100 mg/L 2.00 1.75 94 75-125
0.0100 m9/L 0.200 0,00403 95 75-125
0.0100 mg/L 0.200 0.00220 U 99 75-125
0.500 mg/L 10.0 9.09 99 75-125
0.0100 mg/L 0.200 0.00620 U 99 75-125
0.500 mg/L 10.0 9.07 98 75-125
0.0100 mg/L 0.200 0.232 100 75-125
QM-07
[matrix Spike Dup (1CO2017-MSD1) Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 10:31
Source:CE03185-01
Anailde
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Batt POL Units Level Result WDREC Limits RPD Limit
2.41 0.100 mg/L 2.00 0.459 97 75-125 3 20
0.196 0.0100 mg/L 0.200 0.0115 92 75-125 2 20
0.0189 0.00100 mg/L 0.0200 0.000360 U 95 75-125 2 20
56.3 0.100 mg/L 2.00 55.9 21 75-125 2 20 QM-07
0.224 0,0100 m9/L 0.200 0.0375 93 75-125 0.6 20
0.187 0.0100 mg/L 0.200 0.00310 U 94 75-125 4 20
3.59 0.100 mg/L 2.00 1.75 92 75-125 1 20
0.192 0.0100 mg/L 0.200 0.00403 94 75-125 0.8 20
0.195 0.0100 mg/L 0.200 0.00220 U 98 75-125 2 20
18.9 0.500 mg/L 10.0 9.09 98 75-125 0.9 20
0.194 0.0100 mg/L 0.200 0.00620 U 97 75-125 1 20
18.8 0.500 mg/L 10.0 9.07 97 75-125 0.7 20
0.423 0.0100 mg/L 0.200 0.232 96 75.125 2 20
NOtgL
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 13

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QUALITY CONTROL DATA
'MetzIs (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1CO2017 - EPA 30054 - Continued
1
[Post Spike(1CO2017-PS1)
Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 10;33
Source: CE03185-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result flag P91 Units Level Result %REC im'
2.66 0.100 mg/L 2.00 0.459 1I0 80-120
0.207 0.0100 mg/L 0.200 0.0115 98 80-120
0.0199 0.00100 mg/L 0.0200 -0.000302 100 80-120
56.0 0.100 mg/L 2.00 55.9 5 80-120
0.231 0.0100 mg/L 0.200 0.0375 97 80-120
0.197 0.0100 mg/L 0.200 0.00132 98 80-120
3.74 0.100 mg/L 2.00 1.75 100 80-120
0.202 0.0100 mg/L 0,200 0.00403 99 80-120
0.203 0.0100 mg/L 0,200 0.00176 101 80-120
19.3 0.500 mg/L 10.0 9.09 102 80-120
0.202 0.0100 mg/L 0.200-0.000167 101 80-120
19.2 0.500 mg/L 10.0 9,07 142 80-120
0.416 0.0100 mg/L 0.200 0.232 92 80-120
Classical Chemistry Parameters - Quality Control
Batch 1CO2017 - EPA 3005A
RPD
RPD Limit Notes
QM-08
1
Blank (1CO2017-BLK1)
Prepared: 03/02/2021 11:30 Analyzed: 03/03/2021 14:00
1
ADaI]f�
Sodium Adsorption Ratio
Batch 1CO2025 - NO PREP
Result Etas 1PQL Units
0.00 U [blank]
Spike Source
Level Result %REC Limits RPD
%REC
RPD
Limit
MAL
Blank(1CO2025-BLK1)
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 16:34
Analvte
Nitrite as N
Result fin
0.017 U
PQ
0.10
spike Source
Units Level Result %REC Limits RPD
mg/L
%REC
RPD
Limit
Nn6es
[LCS(1CO2025-BS1)
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 17:01
1
AnallLhe
Nitrite as N
Resll flag
0.99
Spike Source
g1�1 Units Level Result
0.10
mg/L
1.00
%REC RPD
%REC Limits RPD L#mi Notes
99
90-110
[Matrix Spike (1CO2025-MS1)
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 16:36
1
Source: CE01362-01
Analvte
Nitrite as N
Result !flag}
0.92
POI Units
mg/L
0.10
Spike Source
Level Result
0.017 U
1.00
%REC
%REC Ala RPD
92
90-110
RPD
Limit
Matrix Spike (1CO2025-MS2)
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 16:39
Y
Source: CE01363-01
Analvte
Nitrite as N
Spike Source
Result Hut PQ1 Units Level Result %REC Limits RPD
1.1
%REC
0.10 mg/L 1.00 0.083 97 90-110
Matrix Spike Dup (1CO2025-MS01)
RPD
Unit Notes
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 16:37 1
Source: CE01362-01
Analvte
FINAL
Spike Source %REC RPD
Result Elm PM Units Level Result %ROC Limas RPD Limit Notes
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 7 of 13

r
� 1
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QUALITY CONTROL DATA
[assical Chemistry Parameters - Quality Control
1
Batch 1CO2025 - NO PREP - Continued
I Matrix Spike Dup (1CO2025-MSD1) Continued
Prepared: 03/02/2021 14:35 Analyzed: 03/02/2021 16:37
Source: CE01362-01
Anahte Result
Nitrite as N 0.95
Batch 1C030,15 - NO PREP
Flan I'QL Units
0.10 mg/L
Spike
Level
1.00
Source
Result
0.017 U
%REC
%REC Limits RPD
95 90-110 2
RPD
Limit
10
Rojas_
Blank(1C03015-BLK1)
Prepared & Analyzed: 03/03/2021 11:19
1
na
Biochemical Oxygen Demand
Result Elm
2.0 U
POI Units
2.0 mg/L
Spike Source
Level Result
a/AEC
%REC Limits RPD
LCS (1C03015-BS1)
Prepared & Analyzed: 03/03/2021 11:19
Analvte
Biochemical Oxygen Demand
Result Mao
230
Spike
PQL Units Level
2.0
mg/L
198
Source
Result
%REC
%REC Mao RPD
118
85-115
Duplicate (1C03015-DUP1)
Prepared & Analyzed: 03/03/2021 11:19
Source: CE00059-01
An IAN
Biochemical Oxygen Demand
Batch 2C05005 - NO PREP
Result Flag
2700
Spike
POL Units Level
2.0 mg/L
Blank (1C05005-BLK1)
Source
Result
%REC
%REC Limits RPD
2600 3
RPD
Limit
NL
B-03
1
RPD
Ojai
RPD
Limit !
30 B-07
Prepared: 03/05/2021 09:04 Analyzed: 03/05/2021 13:27
Analvte
Nitrate/Nitrite as N
Result
0.041
Flag Poi.
u
0.10
Units
mg/L
Spike Source
Level Result %REC Limits RPD
%REC
RPD
Unlit l
rLCS(1C05005-BS1)
Analvte
Nitrate/Nitrite as N
Result Elaq
1.2
EDI
0.10
Units
mg/L
Prepared: 03/05/2021 09:09 Analyzed: 03/05/2021 13:29
$pike Source
Level Result
1.25
%REG
%REC Limits RPD
93
90-110
RPD
mi
1
Notes
Matrix Spike (1005005-MS1)
Prepared: 03/05/2021 09:04 Analyzed: 03/05/2021 13:33
Source:CE02188-01
Anal
Nitrate/Nitrite as N
Result
8.4
Flag P9l
1.0
Units
mg/L
Spike
Level
5.00
Source
Bela
3.7
%REC
%REC Limi
95
90-110
RPD
RPD Li i
[Matrix Spike (1C05005-M52)
Source: CE02194-01
Allta14te
Nitrate/Nitrite as N
Prepared: 03/05/2021 09:04 Analyzed: 03/05/2021 13:38
Result
8.5
Elas P91:
1.0
Units
mg/L
Spike
Level
5.00
Source
3.7
%REC
a/oREC Limits RPD
96
90-110
RPD
mi
NOT
[Matrix Spike Dup (1C05005-MSD1)
Source: CEOZ168-01
Nitrate/Nitrite as N
Batch 1C05006 - Same
Result Ban
8.5
Prepared: 03/05/2021 09:04 Analyzed: 03/05/2021 13:34
Spike
PQL Vilna Level
1.0 mg/L 5.00
Source
Rac A
3.7
%REC
%REC 'Adis RPD
96 90-110 0.7
RPD
10
1
NALL
FINAL
This report relates only to the sample as received trf the laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1C05006 - Same - Continued
l
Blank (1C05006-BLK1)
Analvte
Chemical Oxygen Demand
Prepared: 03/05/2021 09:52 Analyzed: 03/05/2021 12:45
1
Result Flan
10 U
PQL Unites
10 mg/L
Spike Source
Level gay
%REC
RPD
%REC }unit RPD unit
LCS(1C05006-BSI)
Prepared: 03/05/2021 09:52 Analyzed: 03/05/2021 12:45
1
Analvte
Chemical Oxygen Demand
Result nog
520
l
Matrix Spike (1C05006-MS1)
Source: CE01429-01
Analvte
Chemical Oxygen Demand
Pl3L YAM
10 mg/L
Spike Source
Level Result
500
%REC
%REC Limits RPD
104
90-110
RPD
ItLutf
Notes
Prepared: 03/05/2021 09:52 Analyzed: 03/05/2021 12:45
esult PQL
630
10
Spike
Units Level
mg/L
526
Source
Resu
76
%REC
%REC "Limits RPD
105
90-110
RPD
limit
Notes
[Matrix Spike Dup (1C05006-MSD1)
Source: CE01429-01
Anibete
Chemical Oxygen Demand
Batch IC08003 - Same
Prepared: 03/05/2021 09:52 Analyzed: 03/05/2021 12:45
Result Etas PQL Units
620
10 mg/L
Spike
Level
526
Source
Raid
76
%REC
%REC Limit RPD
104 90-110 0.4
RPD
Limit
5
1
Blank (1C08003-BLK1)
Prepared: 03/08/2021 06:55 Analyzed: 03/09/2021 11:16
1
Analvte
Total Kjeldahl Nitrogen
Result Flag
0.26 U
PQL Units
mg/L
0.48
Spike Source
Level Result
%REC
%REC Limits RPD
RPD
Limit Notes
LLCS (1C08003-BS1)
Analvte
Total Kjeldahl Nitrogen
Prepared: 03/08/2021 06:55 Analyzed: 03/09/2021 11:18
Spike
Result Elan P01. Units Level
13
0.48
mg/L
12.0
Source
Result
%REC
%REC Limits RPD
105
90-110
RPD
mit Rom
Matrix Spike (1C08003-MS1)
Prepared: 03/08/2021 06:55 Analyzed: 03/09/2021 11:22
Source: CE01408-01
Analvte
Total Kjeldahl Nitrogen
ROAR Flagt P.QL
93 D
4.8
Spike
Units Level
mg/L
4.80
Source
Sett
97
%RFC
%REC Lido RPD
NR
90-110
RPD
Limit
1
Nobel
QM-07
Matrix Spike (1C08003-M52)
Prepared: 03/08/2021 06:55 Analyzed: 03/09/2021 11:30
Source: CE01409-01
lid
Total Kjeldahl Nitrogen
Result Mae
33 D
spike
PEn. Units Level
0.96
mg/L
4.80
Source
Result
30
%REC
%REC Limits RPD
83
90-110
RPD
Lint
Notes
QM-07
Matrix Spike Dup (1C08003-MSD1)
Source: CE01408-01
Analvte
Total Kjeldahl Nitrogen
Batch 1C08004 - Same
Result Elea
100 D
P0L Units
4.8 mg/L
Prepared: 03/08/2021 06:55 Analyzed: 03/09/2021 11:23
Spike
Level
4.80
Source
BelaR %REC
97 141
%REC
Limits RPD
90-110 11
RPD
Limit
10
1
NDtrs
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1C08004 - Same - Continued
[Blank(1C08004-8LK1)
Prepared: 03/08/2021 06:59 Analyzed: 03/09/2021 14:04
Analvte
Phosphorus
Result Flag
0.025 U
Spike Source
P9L Units Level Result %REC Limits RPD Lg_ni.1
0.10 mg/L
%REC
RPD
NobeL
�LCS(iC08004-B51)
Analvte
Phosphorus
Prepared: 03/08/2021 06:59 Analyzed: 03/09/2021 14:05
Matrix Spike (1C08004-MS1)
Result Rae
1.6
PQL Units
mg/L
0.10
Spike Source
Level Result
1.60
%REC
99
%REC RPD
Limits RPD Limit
80-120
Prepared: 03/08/2021 06:59 Analyzed: 03/09/2021 14:08
Source: CE01408-01
.Analvte
Phosphorus
Result Flag
4.9 D
EQL Units
mg/L
0.50
Spike Source
Level Result
0.640
5.1
%REC
NR
%REC RPD
Limits RPD Mild
80-120
QM-07
i Matrix Spike Dup (1C08004-MSD1)
source:CE01408-01
Analvte
Phosphorus
Batch.1C08009 - NO PREP
Prepared: 03/08/2021 06:59 Analyzed: 03/09/2021 14:09
Spike Source
Result Men PQL Units Level Result
4.7 0 0.50 mg/L 0.640 5.1 NR 80-120 4
%REC RPD
%MEC ',WAS RPD Limit
25
1
Kolas
QM-07
Blank (1C08009-BLK1)
Prepared: 03/08/2021 08:15 Analyzed: 03/08/2021 11:37
1
Analvte
Ammonia as N
Result F124
0.045 U
Spike Source
ER, Units Level Result
0.10 mg/L
%REC RPD
%REC Limits RPD Limit MO_
LCS(1C08009-051)
Prepared: 03/08/2021 08:15 Analyzed: 03/08/2021 11:39
1
Analvte
Ammonia as N
Spike Source
Resift Flag PQL Units Level Rylt
0.10 mg/L
1.1
1.01
%REC
%REC Limits
108
90-110
RPD
RPD Limit Notes
Matrix Spike (1C08009-MS1)
Prepared: 03/08/2021 08:15 Analyzed: 03/08/2021 11:43
Source: CE00059-02
Analvte
Ammonia as N
Result Elan
3.8 is
PQL Units
mg/L
0.10
Spike Source
Level Result
0.393
3.3
%REC RPD
%REC Limi:e4 RPD Up=nk
112
90-110
NotOS-
QM-07
Matrix Spike (1C08009-M52)
Prepared: 03/08/2021 08:15 Analyzed: 03/08/2021 11:51
Source: CE01007-01
Analvte
Ammonia as N
Spike
Result Elan PQL Units Level
0.39
0.10
mg/L
0.393
source
Result
0.045 U
%REC
%REC Linn sP
99 90-110
RPD
RPD Limit i4otee
Matrix Spike Dup (1C08009-MSD1)
Prepared: 03/08/2021 08:15 Analyzed: 03/08/2021 11:44
1
Source: CE00059-02
Anaivffi
Ammonia as N
Batch 1C09018 - NO PREP
Spike Source %REC
Result Han POL Units Level gg %REC Limits RPD i3 Notes
3.7 E 0.10 mg/L 0.393 3.3 104 90-110 0.8 10
RPD
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 10 of 13

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1C09018 - NO PREP - Continued
I Blank (1C09018-BLK1)
Analvte
Total Solids
LCS (1C09018-BS1)
www.encolabs.com
1
Prepared & Analyzed: 03/09/2021 13:38
Spike Source
Result Elan POI Units Level Result
0.0050 u 0.0050 % by Volume
%REC
RPD
%REC Llmi RPD Limit Notea
Prepared & Analyzed: 03/09/2021 13:38
Spike
Result nen PM. 11*s Level
Total Solids 1100 50 mg/L 1100
Source %REC RPD
Result %REC Limits RPD Lima Kot&L
102
90-110
[Duplicate (1C09018-DUP1)
Prepared & Analyzed: 03/09/2021 13:38
i
Source: CE01438-01
Analvte
Total Solids
Result
Spike Source
0.42 0.0050 % by Volume 0,42
Rau PAL rUAb Level
Classical Chemistry Parameters - Quality Control
Batch 1C09008 - ND PREP
%REC
RPD
%REC Limits RPD Limit Notes
0.2 5
Blank (1C09008-BLK1)
Prepared: 03/09/2021 08:59 Analyzed: 03/10/2021 11:40
1
Analvte
Total Suspended Solids
Result Elan
2.5 U
Spike Source
P41 Unita Level Result %REC limns RPD mi Now
2.5 mg/L
%REC
RPD
ILCS(1C09008-BS2)
nalvte
Total Suspended Solids
Result Elan
89
P01. Units
2.5 mg/L
Prepared: 03/09/2021 08:59 Analyzed: 03/10/2021 11:40
Spike Source
Level Result
100
%REC
%REC Limits
89
80-120
1
RPD
RPD Limit Notes
Duplicate (11;09008-DUP1)
Prepared: 03/09/2021 08:59 Analyzed: 03/10/2021 11:40
Source: AE01744-01
Anahrte
Total Suspended Solids
Spike Source
Result ELa9 POI Units Level R4 1L
1200 2.5 mg/L 1100
%REG RPD
%REC Limits RPD 'mi Notes-
13 20
FINAL This report relates only to the sample as received by the laboratory, and may oriy be reproduced In full.
Page S1of13

www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MRL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-03 Blank exceeds the method required oxygen depletion of <0.20 mg/L.
B-07 LCS exceeded control limits for this test. The test can not be repeated due to method constraints. The
result should be considered an estimated value.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

10775 Central Port Dr
Orlando FL 32624
1407) 5213-5314
4510 Executive Park Court Suite 111
JacksormIte, FL 32216.60e9
{904) 296-3007 Fax [phone]
102-A Woodwindslndus1na CI
Cary. NC 275 t
0191457-3090 Fax {919)467.3515
Page of
CIIE,il Name
Novozyrnes North America (N0009)
Address
77 Perry Chapel Church Road
Crly'Si2iP
Fr ankknton, NC 27525
Prajeci Number
inenel
Project Narne/Desc
Monthly - Week One - SBIM
PO r r Biting Ina
3700044905
Tel
[phone]
Fax
Reparang Canted
Scott Creech
Serriplerlsl Name Alfiebon {Pint)
J1 tit II-8rC Ii
Samplerfsi Signalure
13111:nq Contact
Accounts Payable
60.1.ocebon Time Zane
rift o is 07100, AA,
m
0
Q0
0
Requested
Preservation (See Coder) (Combine as necessary
Requested Turnaround
Times
Nola Rush requests subject to
acceptance by the lankly
Standard
Expedited
Due II
Lob Workorder
C E030 f 8
Items Sample ID IFleld Idenkecefion)
SBM
Collection Date
Collection
Time
Comp r GOO
6(647
NUM.
Ise' codes)
Total a of
Container'
7
x
x
x
x
x
x
Sample Comments
<-- Total N of Containers
Sample Kn Prepared By
Per Tf(rne
Relinquished By r
tit ?
DeleYrme
0342/.2,1
4.27
Re sented By
.. '
L
DatsRlme
L, a L ...77 Al �5 /S
Cnnanin rSpecaf R
g
equlremenls
,'^fj}iTh4)"-1141j
Relrngisshed By
Dale/Timm
Received By
OeteTTrme ,
Rolinqueshed By
DalaTrme
Received By
De erMine
Cooler e s & Tampa an Recaipl
c
- 0 L
Condition U ecelpl
Acceptable — Unacceptable
iMatnx GW-Groundwater SO-SoIIOW-Dunking Water SE -Sediment SW-SurteceWater WW-Wa.rer:ater A-Av O.Otller Meted ncomments) Prefervsllon:4Ice H-HCI N-HNO3 5-H2SOa NO-NaOH O.Oitter(041ar
Note AN samples submitted le ENCO Labs are in accordance with the terms and condmone listed on the reverse of This form unless prior melon agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CE03078
Client: Novozymes North America (N0008)
Logged In: 02-Mar-21 10:18
Preservation Check Performed By:
Project: Monthly - Week One - SBM
Project # [nonej
Logged By: John C King
Date/Time 3.' ( (1•L)
CE03078-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
1n Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
D
250mLP+H2SO4
<2
Y /�NA
C
/l! / N / NA �0 [
ZdnL_ 4 �7SU►-IE
25QmLP+I-tNO3
<2
Y INN) NA
Y I (�V.YNA4
ti...,(
2 vn ` -v�o7
1
2
Reagent Name
ID Reagent Name
([00 5
1-17am
pH Strip ID: c 0 555
3
4
ID
5
6
Reagent Name ID
C:IELM NT\Print\wko_P reservationC heck. rpt
Page 1

ENCO Labrn'atorks
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102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, April 20, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE04310
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, April 6, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL. This report relates only to the sample as received by the laboratory, and may only be reproduced to €ul[. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM Lab ID: CE04310-01
Parameter
CSU Method
EPA 351.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 7470A
SM 2540B-2011
SM 2540D-2011
SM 5210 B-2011
SM 5220D-2011
Preparation
EPA 3005A
Same
NO PREP
[CALC]
EPA 3005A
EPA 7470A
NO PREP
NO PREP
NO PREP
Same
Hold Date/Time(s)
12/31/23
05/04/21
04/08/21 00:50
04/08/21 00:50
10/03/21
05/04/21
04/13/21
04/13/21
04/08/21 00:50
05/04/21
Sampled: 04/06/21 00:50 Received: 04/06/21 08:15
Pren Date/Timers). Analysis DatelTime(s)
04/07/21 08:37 04/07/21 15:31
04/07/21 05:17 04/12/21 10:44
04/06/21 15:29 04/06/21 17:15
04/15/21 08:52 04/15/21 14:45
04/07/21 08:37 04/07/21 13:47
04/10/21 14:57 04/12/21 17:06
04/13/21 11:15 04/13/21 11:15
04/12/21 09:42 04/13/21 11:18
04/07/21 15:07 04/07/21 15:07
04/12/21 09:50 04/12/21 13:55
Client ID: SBM Lab ID: CE04310-01RE1
Sampled: 04/06/21 00:50 Received: 04/06/21 08:15
Parameter
EPA 350.1
EPA 353,2
EPA 365.4
Preparation
NO PREP
NO PREP
Same
Hold DatePfime(sl
05/04/21
05/04/21
05/04/21
Prep Date/Time(s) Analysis Date/Tim-eft!
04/19/21 10:06 04/19/21 16:52
04/15/21 08:52 04/15/21 14:45
04/07/21 05:19 04/12/21 15:31
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 2of13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Limennwollo
Analyte
Aluminum - Total
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Magnesium - Total
Molybdenum - Total
Nickel - Total
Nitrate as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
Lab ID: CE04310-01
Results Flag MD l L uni
6.99 0.420 1.00 mg/L
10000 2.0 2.0 mg/L
2900 0.390 1.00 mg/L
29000 800 800 mg/L
2.17 0.290 1.00 mg/L
0.0281 J 0.0250 0.100 mg/L
0.0351 J 0.0220 0.100 mg/L
25 D 2.0 4.8 mg/L
0.12 0.017 0.10 mg/L
410 1.50 5.00 mg/L
248 4.00 5.00 mg/L
1.27 [blank)
1900 0 26 48 mglL
4.8 0,0050 0.0050 % by Volume
260000 2.5 2.5 mg/L
0.126 0.0490 0.100 mg/L
_ Client ID: SBM Lab ID: CE04310-01RE1
&suits flag MIX PQL units Method
180 D 9.0 20 mg/L EPA 350.1
25 0 2.0 4.8 mg/L EPA 353.2
250 D 2.5 10 mg/L EPA 365.4
Method Ply
EPA 6010D
SM 5210 B-2011
EPA 6010D
SM 52200-2011
EPA 60100
EPA 6010D
EPA 6010D
EPA 353.2
EPA 353.2
EPA 6010D
EPA 60100
CSU Method
EPA 351.2
SM 2540B-2011
SM 2540D-2011
EPA 6010D
ADa1.1te
Ammonia as N
Nitrate/Nitrite as N
Phosphorus
1
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - 58M
Lab Sample ID:CE04310-01
Sampied:04/06/21 00:50
Sampled By:VINCE WILKINS
Received: 04/06/21 08:15
Work Order: CE04310
Metals by EPA 6000/7000 Series Methods
- ENCC' Cary certified ara/yte [NC 591]
Analvte ICAS Numbed
Mercury [7439-97-6]^
Results Flag ni
0.000750 U mg/L
Pi MDL P_QL Bitch Method Analyzed BY Moira
5 0.000750 0.00100 1D10004 EPA 7470A 04/12/21 17:06 KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - 519(0 Cary certified arta44e pc 591]
Analvte Kg§ Numberl
Aluminum 17429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Calcium [7440-70-2]^
Copper [7440-50-8]^
Lead [7439-92-1]^
Magnesium [7439-95-4]"
Molybdenum [7439-98-7]^
Nickel [7440-02-0]^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc [7440-66-6]^
BMsults Elia
6.99
0.0760
0.00360
2900
0.0160
0.0310
2.17
0,0281
0.0351
410
0.0620
248
0.126
Classical Chemistry Parameters
^ - ENCO Cary, certified anary2e PC 591]
Analvte rCAS Numberl
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand"
Chemical Oxygen Demand"
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Results
180
10000
29000
25
25
0.12
250
1.27
1400
4.8
Units DF MQL PQL fiat P4ethod Apalrzed BY
mg/L 10 0.420 1.00 1006015 EPA 6010D 04/07/21 13:47 JDH
U mg/L 10 0.0760 0.100 1D06015 EPA 6010D 04/07/21 13:47 3DH
U mg/L 10 0.00360 0.0100 1D06015 EPA 6010D 04/07/21 13:47 JDH
mg/L 10 0.390 1.00 1D06015 EPA 6010D 134/07/21 13:47 3DH
U mg/L 10 0.0160 0.100 1D06015 EPA 6010D 04/07/21 13:47 JDH
U mg/L 10 0.0310 0.100 1006015 EPA 6010D 04/07/21 13:47 JDH
mg/L 10 0.290 1.00 1D06015 EPA 6010D 04/07/21 13:47 JDH
J mg/L 10 0.0250 0.100 1D06015 EPA 6010D 04/07/21 13:47 JDH
mg/L 10 0.0220 0.100 1D06015 EPA 6010D 04/07/21 13:47 JDH
mg/L 10 1.50 5.00 1D06015 EPA 6010D 04/07/21 13:47 JDH
U mg/L 10 0.0620 0.100 1D06015 EPA 601013 04/07/21 13:47 JDH
mg/L 10 4.00 5.00 1D06015 EPA 6010D 04/07/21 13:47 JDH
mg/L 10 0.0440 0.100 1D06015 EPA 6010D 04/07/21 13:47 JDH
_m im • .
1V5
1
Etas Units DF j2112.1. EQL Aatsb Method Analyzed j1:y 14otts
D 111g/L 200 9.0 20 1D19016 EPA350.1 04/19/21 16:52 JAH
mg/L 1 2.0 2.0 1D07015 SM 5210 B-2011 04/07/21 15:07 JOC
mg/L 80 800 800 1D12005 SM 52200-2011 04/12/21 13:55 JOC
D mg/L 4B 2.0 4.8 [CALC] EPA 353.2 04/15/21 14:45 JAH
D mg/L 48 2.0 4.8 1D15006 EPA 353.2 04/15/21 14:45 JAH
mg/L 1 0.017 0.10 1006034 EPA 353.2 09/06/21 17:15 JAH
D mg/L 100 2.5 10 1D07006 EPA 365.4 04/12/21 15:31 JAH
[blank] 1 1D06015 C5U Method 04/07/21 15:31 JDH
D mg/L 100 26 48 1D07005 EPA 351.2 04/12/21 10:44 JAH
% by Volume 1 0.0050 0.0050 1D13012 SM 25400-2011 04/13/21 11:15 LH
. . _ __ - A
Classical Chemistry Parameters
Analvte ICAS Numberl
Total Suspended Solids
Result Bag ALAI [I p.% Batch Method Analyzed fy fiats
260000 mg/L 1 2.5 2.5 1D12010 SM 25400-2011 04/13/21 11:18 AAL
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1010004 - EPA 7470A
Blank (1010004-BLK1)
Anaticte
Mercury
LCS (1D10004-BS1)
Prepared: 04/10/2021 14:57 Analyzed: 04/12/2021 16:31
i
Spike
Result Elan PQL Units Level
0.000150 U 0.000200 mg/L
Source
Result
%REC RPD
%REC Mmits RPD Limit N
Analvte
Mercury
Matrix Spike (1D10004-MS1)
Prepared: 04/10/2021 14:57 Analyzed: 04/12/2021 16:34
Result Elan PQL Units
0.00500 0.000200
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
0,00500
100
80-120
Prepared: 04/10/2021 14:57 Analyzed: 04/12/2021 16:40
1
Source: CE03590-03
Analvte
Mercury
Result Rae POL Units
0.00490 0.000200
mg/L
Spike
Level
0.00500
Source
Result %REC
0.000150 U 98
%REG
Linllt1
75-125
RPD
RPD Limit Notes
Matrix Spike Dup (1D10004-MSD1)
Prepared: 04/10/2021 14:57 Analyzed: 04/12/2021 16:42
Source: CE03590-03
Analvte
Mercury
0.00497
Result Elan PQL units
mg/L
0.000200
Spike Source
Levet BURR
0.00500 0.000150 U
%REC
%REC Limits
99
75-125
RPD
RPD Chit
1
25
Notes
Post Spike (1D10004-PS1)
Prepared: 04/10/2021 14:57 Analyzed: 04/12/2021 16:44
Source: CE03590-03
AnRli►le
Mercury
Spike Source
Result Hoe P01. Units Level Result
5.67 0.200 ug/L 5.00-0.0230
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1006015 - EPA 3005A
%REC
%REC Imits
113
75-125
RPD
RPD Limit
Notes
[Blank (1D06015-BLK1)
Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:08
1
JUsdide
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Elea P01. Ilnita Level
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0,00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
Source
Result %REC Limits RPD Chilli Notes_
%REC
Blank (1D06015-BLK2) Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:10
Analyte
Aluminum
Arsenic
FINAL
Spike Source
Result Nag P01. Units Level Rpm+1}
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
%REC
%REC Limits
RPD
RPD
RPD Li0]ii Nam.
Page 5 of 13

@-4111-1816.
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1D06015 - EPA 3005A - Continued
Blank (1D06015-BLK2) Continued
9ealltfi&
Cadmium
Calcium
ale
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
www.encolabs.com
Prepared: 04/06/2021 10:38 Analyzed: 09/07/2021 12:10
Result Flan P91 Units
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
Spike Source
Level ! %REC Limits RPD Limit
%REC
RPD
LCS (1D06015-BS1) Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:15
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Sault Eau PQL Units Level
1.82 0.100 mg/L 2.00
0.181 0.0100 mg/L 0.200
0.0182 0.00100 mg/L 0.0200
1.89 0.100 mg/L 2.00
0.177 0.0100 mg/L 0.200
0.186 0.0100 mg/L 0.200
1.84 0.100 mg/L 2.00
0.178 0.0100 mg/L 0.200
0.189 0.0100 mg/L 0.200
9.43 0.500 mg/L 10.0
0.186 0.0100 mg/L 0.200
9.51 0.500 mg/L 10.0
0.188 0.0100 mg/L 0.200
Source
Result
%REC
91
90
91
95
88
93
92
89
94
94
93
95
94
%REC
Limits RPD
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
RPD
Limit
Matrix Spike (tDO6015-MS1)
Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:17
1
Source: CE04214-12
Mobile
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result Flag P0.1 Unita Level &Ka %REC Liao
2.27 0.100 m9/L 2.00 6.35 NA 75-125
0.182 0.0100 mg/L 0.200 0.00760 U 91 75-125
0.0184 0.00100 mg/L 0.0200 0.000360 U 92 75-125
8.30 0.100 mg/L 2,00 6.51 89 75-125
0.179 0.0100 mg/L 0.200 0.00213 88 75-125
0.184 0.0100 mg/L 0.200 0.00310 U 92 75-125
4.06 0.100 mg/L 2.00 2.61 72 75-125
0.180 0.0100 m9/L 0.200 0.00250 U 90 75-125
0.189 0.0100 mg/L 0.200 0.00220 U 94 75-125
10.9 0.500 mg/L 10.0 2.33 86 75-125
0.189 0.0100 mg/L 0.200 0.00620 U 94 75-125
24.2 0.500 mg/L 10.0 15.3 89 75.125
0.194 0.0100 mg/L 0.200 0.0102 92 75-125
RPD
RPD mi
Moto,
QM-07
QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Pave 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1D06015 - EPA 3005A - Continued
Matrix Spike Dup (1006015-M5D1)
Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:19
1
Source: CE04214-12
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result i:ia4 P0L !dnit9 Level Haze %REC Limits RPD imi Notes
2.87 0.100 mg/L 2,00 6.35 NR 75-125 23 20 QM-07,
QM-11
0.185
0.0181
8.19
0.177
0.184
4.06
0.179
0.188
10.9
0.191
24.0
0.193
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.200 0.00760 U 92 75-125 2 20
0.0200 0,000360 U 90 75-125 2 20
2.00 6.51 84 75-125 1 20
0.200 0.00213 87 75-125 1 20
0.200 0.00310 U 92 75-125 0.2 20
2.00 2.61 72 75-125 0.01 20 QM-08
0.200 0.00250 U 89 75-125 0.6 20
0.200 0.00220 U 94 75-125 0.5 20
10.0 2.33 86 75-125 0.1 20
0.200 0.00620 U 96 75-125 1 20
10.0 15.3 87 75-125 0.9 20
0.200 0.0102 91 75-125 0.4 20
Post Spike (1006015-PS1) Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 12:21
Source: CE04214-12
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
8.15
0.191
0.0189
8.26
0.184
0.195
4.45
0.187
0.198
11.8
0.202
24.4
0.208
Flan PS&
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Source
Result
6.35
0.00190
-2.91E-5
6.51
0.00213
0.00270
2.61
0.000371
0.00191
2.33
0.00527
15.3
0.0102
%REC RPD
%REC Limits RPD limit
90 80-120
95 80-120
95 80-120
88 80-120
91 80-120
96 80-120
92 80-120
93 80-120
98 80-120
95 80-120
99 80-120
90 80-120
99 80-120
a
flitteL
Classical Chemistry Parameters - quality Control
Batch 1006015 - EPA 3005A
[Blank (1006015-BLK1)
Prepared: 04/06/2021 10:38 Analyzed: 04/07/2021 15:31
Analvte
Sodium Adsorption Ratio
Result Man P01.
0.00
U
Unit5
[blank]
Spike Source
Level Result
%REC RPD
%REC Limits RPD 'mit yams_
Blank(1D06015-SLK2)
Prepared: 04/06/2021 10:38 Analyzed: 04)07/2021 15:31
Analvte
Sodium Adsorption Ratio
Batch 11106034 - NO PREP
Result Bag PQL ldniM
0.00 U [blank]
Spike
Level
EWA
Source
%REG RPD
%REC Limits RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Pese7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1D06034 - NO PREP - Continued
Blank(1D06034-BLK1)
Prepared: 04/06/2021 15:29 Analyzed: 04/06/2021 17:11
Analvte
Nitrite as N
Result Else
0.017 U
Spike
PAL Units Level
0.I0
mg/L
Source
Poe&
%REC
%REC Limits RPD
RPD
Limit
Notes
(ICS(1D06034-851)
Prepared: 04/06/2021 15:29 Analyzed: 04/06/2021 17:27
■
Analvte
Nitrite as N
Result Flan
0.99
EQi: Units
mg/L
0.10
Spike
Level
1.00
Source
Result
%REC
99
%REC
Limits RPD
90-110
RPD
Limit
Matrix Spike (1D06034-MS1)
Prepared: 04/06/2021 15:29 Analyzed: 04/06/2021 18:03
Source: CE04309-01
Analvte
Nitrite as N
Result FIa4
61 DE
2.7
ni
mg/L
Spike Source
Level Result
1.00
61
%REC
4
%REC
Limits
90-110
RPD
RPD !jimAt
Note
QM-07
',Matrix Spike Dup (1D06034-MSD1)
Source: CE04309-01
Analvte
Nitrite as N
Batch 1D07005 - Same
Prepared: 04/06/2021 15:29 Analyzed: 04/06/2021 17:44
&tilt Flan
13 D
PQL Units
0.50 mg/L
Spike
Level
1.00
Source
Result
61
%REC
%REC Jamb RPD
NR 90-110 129
RPD
Limit
10
Note -
QM-07,
QM-11
Blank (1D07005-BLK1)
Prepared: 04/07/2021 05:17 Analyzed: 04/12/2021 10:09
1
.Anab to
Total Kjeldahl Nitrogen
Remit Elan
U
0.26
EQL
0.48
Spike
Molts Level
mg/L
Source
lZesult
%REC
%REC Limits RPD
RPD
Limit Mr&
LCS(1D07005-BSI)
Prepared: 04/07/2021 05:17 Analyzed: 04/12/2021 10:11
Analvte
Total Kjeldahl Nitrogen
Result Flag EQL
12
0.48
Spike Source
Units Level
mg/L
12.0
Result
%REC
%RFC Limits RPD
104
90-110
RPD
u_mB.
MIL
Matrix Spike (1007005-MS1)
Prepared: 04/07/2021 05:17 Analyzed: 04/12/2021 10:14
Source: CE00086-01
Analvte
Tool Kjeldahl Nitrogen
Result
65
Flag
D
Spike
PDT. IIJi Level
4.8
mg/L
4.80
Source
Result
64
%REC
%REC Limits RPD
17
90-110
RPD
Limit
Notes
QM-07
Matrix Spike (1007005-MS2)
Source: CE03080-04
Analvle
Total Kjeldahl Nitrogen
Result Ela4
63 E
Matrix Spike Dup (1D07005-MSD1)
Source: CE00086-01
Analvte
Total Kjeldahl Nitrogen
Batch 1007006 - Same
Result Eon
67 D
PS?L Units
0.48 mg/L
Prepared' 04/07/2021 05:17 Analyzed: 04/12/2021 10:20
Spike
Level
4.80
Source
Remit
64
%REC
%REC Limits RPD
NR
90-110
1
RPD
Limit Notes
QM-07
Prepared: 04/07/2021 05:17 Analyzed: 04/12/2021 10:16
•
EQL Units
4.8 mg/L
Spike Source
Level Result
4.80 64
%REC
%REC Limits RPD
62 90-110 3
RPD
Limit
10
Notes
QM-07
FINAL.
This report rela6 only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1007006 - Same - Continued
Blank (1D07006-BLK1)
Prepared: 04/07/2021 05:19 Analyzed: 04/12/2021 11:58
AnabrIV
Phosphorus
Result Has
0.025 U
Spike Source %REC
P321. Units Level
0.10
mg/L
Result DARK Limits
RPD
RPD Lima ROIL
ILCS(1D07006-BS1)
Analyte
Phosphorus
[Matrix Spike (1D07006-MS1)
Source: CE00086-01
Analvte
Phosphorus
Relit Dam
1.6
P2
0.10
Units
mg/L
Prepared: 04/07/2021 05:19 Analyzed: 04/12/2021 12:00
Spike Source
Level Elea %REC
100
1.60
%REC RPD
rmi RPD mi Hotel
80-120
Prepared: 04/07/2021 05:19 Analyzed: 09/12/2021 12:02
1
Matrix Spike Dup (1D07006-MSD1)
Result
7.7
Bug
0
Spike
P9� Units Level
1.0
mg/L
0.640
Source
Result
7.2
%REC RPD
%REC limits RPD LInilt Notes
88
80-120
Prepared: 04/07/2021 05:19 Analyzed: 04/12/2021 12:04
Source: CE000B6-01
Analvte
Phosphorus
Batch 1007015 - NO PREP
Spike Source %REC RPD
Result Elm P01. Units Level Result %REC atlas RPD Limit Notes
7.8 D 1.0 mg/L 0.640 7.2 95 80-120 0.6 25
L
Blank (1D07015-BLK1)
Prepared &Analyzed: 04/07/2021 15:07
Analvte
8iodiemical Oxygen Demand
[LCS (1D07015-BS1)
Result Flag
2.0 U
Spike
PSL Units Level
2.0
mg/L
Source
Result
%REC
%REC Limits
Prepared & Analyzed: 04/07/2021 15:07
RPD
RPD Limit Notes_
Arable
Biochemical Oxygen Demand
Result flag
200
P0L Units
2.0 mg/L
Spike Source
Level R %REC
198
99
%REC
Limits
85-115
RPD
RPD limit Notes
Duplicate (1D07015-DUP1)
Prepared & Analyzed: 04/07/2021 15:07
1
Source: CE04810-18
Biochemical Oxygen Demand
Batch 1012005 - Same
Spike Source
Result Elan PQL Units }.ever gegult
2.0 U 2.0 mg/L 2.0 U
%REC RPD
%REC Limits RPD mit Notes
30
Blank (1D12005-BLK1)
.Anande
Chemical Oxygen Demand
Prepared: 04/12/202109:50 Analyzed: 04/12/2021 13:55
Y
Spike Source %REC RPD
Result Flaq P01 Units Level EMU %REC Limits RPD Limit Note_
10
[LCS(1D12005-B51)
Analvte
Chemical Oxygen Demand
l 10 mg/L
Prepared: 04/12/2021 09:50 Analyzed: 04/12/2021 13:55
Spike
Result Elam JIM Unite Level
520 10 mg/L 500
Source
Bella
%REC
%REC Ljmlts
104 90-110
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9.of13

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1D12005 - Same - Continued
Matrix Spike (1D12005-MS1)
Source: CE04810-18
Analde
Chemical Oxygen Demand
Matrix Spike Dup (1D12005-MSD1)
Source: CE04810-18
Analvte
Chemical Oxygen Demand
Batch 1D13012 - NO PREP
Result 1]ao
550
www.encolabs.com
1
Prepared: 04/12/2021 09:50 Analyzed: 04/12/2021 13:55
PU1. Units
10 rng/L
Besult F189 Elk Units
560 10 mg/L
Spike Source
Level Result
526
26
%REC RPD
%REC Limits RPD wit
100
90-110
Prepared: 04/12/2021 09:50 Analyzed: 09/12/2021 13:55
Spike Source
Level Result
%REC RPD
%REC Limits RPD Limit
526 26 101 90-110 0.9 5
Notes_
Blank (1D13012-SLK1)
Prepared & Analyzed: 04/13/2021 11:15
Analvte
Total Solids
LCS(1D13012-BS1)
Result flan
U
0.0050
Spike Source
POL Units Level Result %REC Limits RPD
0.0050 % by Volume
Prepared & Analyzed: 04/13/2021 11:15
RPD
mi
Analvte
Total Solids
BR;ult Elea
1100
Duplicate (1D13012-DUP1)
Source:CE04309-01
Total Solids
Batch 1D15006 - NO PREP
Spike Source
POL Units Leve! dtegult
50 mg/L 1100
%REC
%REC Limits RPD
100
90-110
RPD
Limit
Notes
Prepared & Analyzed: 04/13/2021 11:15
Spike Source
Result flail POL units Level
0.27
0.27 0.0050 % by Volume
Blank (1D15006-BLK1)
Analvte
Nitrate/Nitrite as N
LCS (1D15006-BS1)
t.
AnahrSB
Nitrate/Nitrite as N
%REG RPD
%REG Limits RPD that Mgt
0.07 5
Prepared: 04/15/2021 08:52 Analyzed: 04/15/2021 11:45
R un Etas LOL
0.041 U
0.10
units
mg/L
Spike
Level
Source
Result
%REC
RPD
%REC Lj01ita RPD Lllnit Notes
Prepared: 04/15/2021 08:52 Analyzed: 04/15/2021 11:47
Spike
Result Eiae POL Units Level
1.3
0.10
mg/L
1.25
Source
Result
%REC
%REC Limits
101
90-110
1
RPD
RPD Iknia Notes
`Matrlx Spike (1D15006-MS1)
Source: CE04403-01
Analvte
Nitrate/Nitrite as N
Result Hall PQL
Prepared: 04/15/202108:52 Analyzed: 04/15/2021 11:51
Spike
Units Level
0.51 0.10 mg/L 0.521
Source
Bela
0.041 U
%REC RPD
%REC Limits RPD Ljnilt NotL
98 90-110
[Matrix Spike (1D15005-MS2)
Source: CE04403-02
%REC
Prepared: 04/15/2021 08:52 Analyzed: 04/15/2021 11:56
■
Spike Source %REC RPD
Analvi;e Result Asa E24 .UnilA Level %REC Limits RPD Must Mittei-
Nitrete/Nltrite as N 0.33 0.10 mg/L 0.521 0.041 U 64 90-110 QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1015006 - NO PREP - Continued
Matrix Spike Dup (1D15006-MSD1)
Prepared: 04/15/2021 0B:52 Analyzed: 04/16/2021 11:52
Source: CE04403-01
AnaM
Nitrate/Nibite as N
Batch 1D19016 - NO PREP
Result Mao PQL
0.52
0.10
Units
mg/L
Spike
Level
Source
Rend %REC
0.521 0.041 U 99
%REC
Litllil RPD
90-110 1
RPD
Limit Notes
10
Blank (1019016-BLK1)
Prepared: 04/19/2021 10:06 Analyzed: 04/19/2021 14:20
1
Anithitte
Ammonia as N
&Milt Mao
U
0.045
PQL
0.10
Units
mg/L
Spike Source %REC
Result %REC Lim
Level
RPD
RPD Limit
Notes
I LCS (1D19016-BS1)
Prepared: 04/19/2021 10:06 Analyzed: 04/19/2021 14:22
Bn htte
Ammonia as N
Result Qa.9
1.1
PQL in11
mg/L
0.10
Spike Source
Level Result
1.01
%REC
104
%REG
Limits RPD
90-110
RPD
Limit
(Matrix Spike (1D19016-MS1)
Prepared: 04/19/2021 10:06 Analyzed: 04/19/2021 14:25
Source: CE04730-01
Analvte
Ammonia as N
Result Fiaa
0.82
Spike
PQL Units Level
0.10
mg/L
0.393
Source
Emit
0.45
%REC
%REC Uzz its RPD
95
90-110
RPD
Limit
Notes
Matrix Spike (1D19016-MS2)
Prepared: 04/19/2021 10:06 Analyzed: 04/19/2021 14:31
i
Source: CE04731-01
Analvte
Ammonia as N
Result fl04
0.36
PQL Units
mg/L
0.10
Spike
Level
0.393
Source
Result
0.045 U
%REC
92
%REC
lj RPD
90-110
RPD
Limit
Notes
Matrix Spike Dup (1D19016-MSD1)
Prepared: 04/19/2021 10:06 Analyzed: 04/19/2021 14:27
Source: CE04730-01
Analvte
Ammonia as N
Result Finn
0.79
PQL Units
0.10 mg/L
Classical Chemistry Parameters - Quality Control
Batch 1012010 - NO PREP
Spike
Level
0.393
Source
Result
0.45
%REC
87
%REC
li BA
90-110
RPD
4
RPD
Limit
10
Notes
QM-07
1
[Blank(1D12010-BLK1)
Prepared: 04/12/2021 09:42 Analyzed: 04/13/2021 11:18
Analvte
Total Suspended Solids
Result F109
2.5 U
EQL
2.5
Units
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
ILCS(1D12010-B51)
Prepared: 04/12/2021 09:42 Analyzed: 04/13/2021 11:18
Analvte
Total Suspended Solids
Result Eau
87
IMAL Valls
2.5 mg/L
Spike
Level
100
Source
BMA
%REC
%REC Limits RPD
B7
80-120
RPD
Limit
1
Duplicate (1D12010-DUP1)
Prepared: 04/12/2021 09:42 Analyzed: 04/13/2021 11:18
Source: AEO2E107-01
Anahrte
Total Suspended Solids
the
360
Spike
EQL Units Level
2.5 mg/L
source
NUMB
460
%REC
%REC Limil RPD Unit
24 20
RPD
Notes
QM-12
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
6 The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
l The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
tJ The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
(CALC] Calculated analyte MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
10775 Central Port Dr 4810 Executive Park Court, Suite 111
Orlando. FL 32824 Jacksonville FL 32218.8089
1407)82E-5314 1;J04)208.3007 Fax [phone]
102-A Wadi:Nanda Indueirel Ct
Cary NC 2751 I
1919) 467.3090 Fax [phone]
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Page
of
Client Name
No► o ymes North America (N0009)
Profacl Number
!none'
Requested Anayse+
Requested Turnaround
Times
Note Ruh requests wised to
acceptance by the facility
Standard
_ Expedited
Due l l_
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k.I
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Address Church Road
77 Perry Chapel I turc r
Prolact NameeDesc
Monthly - Week One - SBM
Ctly ST2q
Frank nion, NC 27525
PO a 1 Baling Into
3700044905
Tel
(919) �194-3t )U
Fax
Reporting Contact
Scott Crew
semphr{■j Name. Affiliation {Pont)
!
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'Arc
Bang Contact
Accounts Payable
Lab Workorder
fi�r. 0 {
LrE l
Samp�r(■i
Lta ,<�lf�v?
see Loraean 1 Time zone
Prasarvs0an I See Coded (Combine as necessary)
Item r
Sample ID (Feld Idenehcaeoni
Gollecton Date
Collection
Tame
crimp rGro)
Malnx
tsee wlesi
Total a ni
Containers
r Sample Comments
r
SBM
f% Gs- 44
&mi.
7
X
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7
<-- Total # of Containers
Sample 10 Prepared By
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DatNrime ;e to Alf,
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Received By i
Get -'Tr
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Comments/Sewall Reporting Requirements
Relinquished By
Dale/Time
DalalTema
Relinquished By
DatefTkne
Received By
Deleffime
Copier x's S Temps on Receipt
• C
Condition Upon Receipt
& Acceptable _ _ Unacceptable
Matrix • OW -Groundwater SO -Soil OW-Dnnklng Water SE -Sediment SW-Surfaos Water W W-Wee1sweler A -Air 0 0 her {detail in oommental Preservation: I -Ice H-HGI N-HNO3 S-H2504 NO-NaOH 0.01her (datail+n commanlel
Nola . All samples aubmilleed le ENCO Labs are in accordance wnih the terms and condtltona Wed on Ilia revert@ al this form. unleee prior wntten agreements exist

Sample Preservation Verification
ENCO Cary
Work Order CE04310 Project: Monthly - Week One - SBM
Client' Novozyrnes North America (NO008) Project #' [none]
Logged In: 06-Apr-21 10.26 Logged By Rachel Ann Y niI17,1
��
Preservation Check Performed By Date/Time:
L-
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted Date/Time
dtusted
Reagent Used/Comments
D
250mLP+H2SO4
<2
Y .1 N / NA
Y'/ N / NA 4-k kl (lug]
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250mLP+HNO3
<2
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pH Strip ID:
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C:lelmnt\Pn1 „�.�vrieservationuneCK.rpt
3
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Reagent Name
ID
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Reagent Name ID
Page 1 of 1

ENCO Laboratories
Accurate, Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, May 14, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE05806
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, May 4, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL
This report relates only to the sample as recesved by the laboratory, and may only be reproduced In fui.. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Parameter Preparation
CS() Method EPA 3005A
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 [CALC]
EPA 353.2 NO PREP
EPA 365.4 Same
EPA 601013 EPA 3005A
EPA 7470A EPA 7470A
SM 2540B-2011 NO PREP
SM 2540D-2011 NO PREP
SM 5210 8-2011 NO PREP
SM 5220D-2011 Same
Lab ID: CE05806-01
Hold DatelTime(sl
01/28/24
06/01/21
06/01/21
05/06/21 01:20
05/06/21 01:20
06/01/21
06/01/21
10/31/21
06/01/21
05/11/21
05/11/21
05/06/21 01:20
06/01/21
Sampled: 05/04/21 01:20 Received: 05/04/21 08:00
Prep pate/Time(5) Analysis Date(Time(s1
05/06/21 13:38 05/10/21 14:58
05/10/21 08:50 05/10/21 12:38
05/06/21 08:22 05/11/21 11:59
05/04/21 15:24 05/04/21 16:31
05/12/21 09:35 05/12/21 13:46
05/12/21 09:35 05/12/21 13:46
05/06/21 08:23 05/11/21 13:19
05/06/21 13:38 05/10/21 11:19
05/11/21 09:44 05/12/21 14:21
05/06/21 13:50 05/06/21 17:13
05/11/21 16:42 05/12/21 11:28
05/05/21 14:24 05/05/21 14:24
05/04/21 14:02 05/05/21 07:55
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 2 of 13

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SAMPLE DETECTION SUMMARY
1
Client ID: 5BM
Lab ID: CE05806-01
Aaalvte Results Flaa JMDL EQL_ Units Meitsg 11 s.
Aluminum - Total 114 0.420 1.00 mg/L EPA 6010D
Ammonia as N 130 D 4.0 9.0 mg/L EPA 350.1
Biochemical Oxygen Demand 11000 2.0 2.0 mg/L SM 5210 8-2011 B-07
Calcium - Total 2660 0.390 1.00 mg/L EPA 6010D
Chemical Oxygen Demand 30000 800 800 mg/L SM 5220D-2011
Magnesium - Total 21.8 0.290 1.00 mg/L EPA 6010D
Nickel- Total 0.0428 ] 0.0220 0.100 mg/L EPA 6010D
Nitrate as N 4.8 D 0.82 2.0 mg/L EPA 353.2
Nitrate/Nitrite as N 5.1 D 0.82 2.0 mg/L EPA 353.2
Nitrite as N 0.24 0.017 0.10 mg/L EPA 353.2
Phosphorus 310 0 2.5 10 mg/L EPA 365.4
Potassium - Total 415 B 1.50 5.00 mg/L EPA 6010D
Sodium - Total 233 4.00 5.00 mg/L EPA 6010D
Sodium Adsorption Ratio 1.23 [blank] 1 SU Method
Total Kjeldahl Nitrogen 1300 D 26 48 mg/L EPA 351.2
Total Solids 4.4 0.12 0.12 % by Volume SM 2540B-2011
Total Suspended Solids 30000 2.5 2.5 mg/L SM 2540D-2011
Zinc - Total 1.05 0.0440 0.100 mg/L EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproducer] in full.
Page 3of13

ANALYTICAL RESULTS
1
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID:CE05806-01
Sampled:05/04/21 01:20
Sampled By: Elbert Alston
m ^m NMI
IN
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certr rigid arelyte INC 591]
Analvte iCAS Number(
Mercury [7439-97-6]^
Results Flag
0.000750 U
units
mg/L
PE PLM. Batch
5 0.000750 0.00100 1E11009
Method
EPA 7470A
www.encolabs.com
Received: 05/04/21 08:00
Work Order: CE05806
Baabsad Bx Notes
05/12/21 14:21 KAl-I
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary cer(16ed ana/yte [NC 591]
Analvte jCAS Numberl
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-91^
Calcium [7440-70-2]^
Copper [7440-50-8]"
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-71^
Nickel [7440-02-01"
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc [7440-66-6]^
Bsa1111i fin ni OF p]pL PAL Bakb. !Method An Jl<1[ Nates
114 mg/L 10 0.420 1.00 1E06026 EPA 6010D 05/10/21 11:19 JDH
0.0760 U mg/L 10 0.0760 0.100 1E06026 EPA 60100 05/10/21 11:19 JDH
0.00360 U mg/L 10 0.00360 0.0100 1E06026 EPA 60100 05/10/21 11:19 JDH
2660 mg/L 10 0,390 1.00 1E06026 EPA 6010D 05/10/21 11:19 JDH
0.0160 U mg/L 10 0.0160 0.100 1E06026 EPA 6010D 05/10/21 11:19 JDH
0.0310 U mg/L 10 0.0310 0.100 1E06026 EPA 6010D 05/10/21 11:19 JDH
21,8 mg/L 10 0.290 1.00 1E06026 EPA6010D 05/10/21 11:19 JDH
0.0250 U mg/L 10 0.0250 0.100 1E06026 EPA 6010D 05/10/21 11:19 3DH
0.0428 J mg/L 10 0.0220 0.100 1E06026 EPA 6010D 05/10/21 11:19 JDH
415 B mg/L 10 1.50 5.00 1E06026 EPA 6010D 05/10/21 11:19 JDH
0.0620 U mg/1. 10 0.0620 0.100 1E06026 EPA 6010D 05/10/21 11:19 3DH
233 mg/L 10 4.00 5.00 1E06026 EPA 6010D 05/10/21 11:19 JDH
1.05 mg/L 10 0.0440 0.100 1E06026 EPA 6010D 05/10/21 11:19 JDH
Classical Chemistry Parameters
�. �..
^ - ENCO Cary certrfted analyte AC 591]
Analvte !CAS Number( Results nu Units BE Ma EDI l Method Anal ad BY Notes
Ammonia as N [7664-41-7]^ 130 D mg/L 90 4.0 9.0 1E10008 EPA 350.1 05/10/21 12:38 JAH
Biochemical Oxygen Demand^ 11000 mg/L 1 2.0 2.0 1E05007 SM 5210 B-2011 05/05/21 14:24 JOC B-07
Chemical Oxygen Demand^ 30000 mg/L 80 800 B00 1E04031 SM 5220D-2011 05/05/21 07:55 JOC
Nitrate as N [14797-55-8] 4.8 D mg/L 20 0.82 2.0 [CALC] EPA 353.2 05/12/21 13:46 JAR
Nitrate/Nitrite as N^ 5.1 D mg/L 20 0.82 2.0 1E12009 EPA 353.2 05/12/21 13:46 JAH
Nitrite as N [14797-65-0]^ 0.24 mg/L 1 0.017 0.10 1E04040 EPA 353.2 05/04/21 16:31 JAH
Phosphorus [7723-14-0]^ 310 0 mg/L 100 2.5 10 1E06012 EPA 365.4 05/11/21 13:19 JAH
Sodium Adsorption Ratio 1.23 [blank] 1 1E06026 CSU Method 05/10/21 14:58 JDH
Total Kjeldahl Nitrogen^ 1300 D mg/L 100 26 48 1E06011 EPA 351.2 05/11/21 11:59 JAH
Total Solids" 4.4 %by Volume 25 0.12 0.12 1E06027 SM 25408-2011 05/06/21 17:13 DMJ
Classical Chemistry Parameters
Analvte TCAS Numberl
Total Suspended Solids
Results ilas !!Hilo 12E MPL EQL j l Method ° w
30000 mg/L 1 2.5 2.5 1E11075 SM 25400-2011 05/12/21 11:28 AAL
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
1
Batch 1E11009 - EPA 7470A
Blank (1E11009-BLK1)
Analvte
Mercury
0.000150 U 0.000200
Prepared: 05/11/2021 09:44 Analyzed: 05/12/2021 13:33
Spike Source %REC RPD
Result E{ay EQL Units Level EMIR %REC )Limits RPD i !i
mg/L
ILCS (1E11009-BS1)
Analvte
Mercury
Prepared: 05/11/2021 09:44 Analyzed: 05/12/2021 13:35
Matrix Spike (1E11009-MSI)
Source: CE06766-03
Analvte
Mercury
Result Etas P_Q.1. units
0.00525 0,000200
Result Hen Q01.
0.00502
0.000200
mg/L
Spike
Level
0.00500
Source
MAI
%REC
%REC Limits
105
80-120
RPD
RPD ,Limit 1.
Prepared: 05/11/2021 09:44 Analyzed: 05/12/2021 13:40
Spike
Units Level
0.00500
mg/L
Source %REC RPD
Result %REC lisnis RPD Lin*
0.000150 U 100
75-125
Matrix Spike Dup (1E11009-MSD1)
Prepared: 05/11/2021 09:44 Analyzed: 05/12/2021 13:42
Source: CE06766-03
Analvte
Mercury
Result Flag PAX
0.00509 0.000200
Spike Source
Units Level Result %REC
mg/L
0.00500 0.000150 U 102
%REC
jimita RPD
1
75-125
RPD
Urn
25
Post Spike (1E11,009-PS1)
Prepared: 05/11/2021 09:44 Analyzed: 05/12/2021 13:44
Source: CE06766-03
Analvte
Mercury
Spike
Result Elan P01, Units Level
5.41
0.200
ug/L
5.00
Source
Result
-0.00800
%REC RPD
%REC Limi RPD imi Notes
108
75-125
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1E06026 - EPA 3005A
Blank (1E06026-BLK1)
Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 10:07
na
Aluminum
Arsenic
Cadmium
Calcium
Capper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result Elan PM. Units Level &Ault %REC Limits RPD
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00229 3 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.190 3 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
RPD
Limit
Notes
LCS (1E06026-BS1) Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 10:18
1
Aluminum
Arsenic
FINAL
Spike Source
Result Elan Mk Units Level gn,Eyg
2.16 0.100 mg/L 2.00
0.207 0.0100 mg/L 0.200
%REG
%REC Limit6
108 80-120
104 80-120
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
RPD
RPD Mat
Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1E06026 - EPA 3005A - Continued
LCS(1E06026-BS1)Continued
Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 10:18
Analvte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Elm P91 Units Level
0.0206 0.00100 mg/L 0.0200
2.26 0.100 mg/L 2.00
0.207 B 0.0100 mg/L 0.200
0.211 0.0100 mg/L 0.200
2.23 0.100 mg/L 2.00
0.203 0.0100 mg/L 0.200
0.214 0.0100 mg/L 0.200
11.1 B 0.500 mg/L 10.0
0.211 0.0100 mg/L 0.200
11.1 0.500 mg/L 10.0
0.212 0.0100 mg/L 0.200
Source
Result
%REC
%REC Limits
103 80-120
113 80-120
104 80-120
105 80-120
112 80-120
102 80-120
107 80-120
111 80-120
105 80-120
111 B0-120
106 80-120
RPD
RPD Limit Notes
Matrix Spike (1E06026-MS1) Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 10:21
Source:CE05398-02
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Elan PQL Units Level
1.72 0.100 mg/L 2.00
0.158 0.0100 mg/L 0.200
0.0162 0.00100 mg/L 0.0200
2.62 0.100 mg/L 2.00
0.154 B 0.0100 mg/L 0,200
0.162 0.0100 mg/L 0.200
2.52 0.100 mg/L 2.00
0.157 0.0100 mg/L 0.200
0.168 0.0100 mg/L 0.200
11.1 B 0.500 mg/L 10.0
0.171 0.0100 mg/L 0.200
13.9 0.500 mg/L 10.0
0.171 0.0100 mg/L 0.200
Source
Emit
0.0420 U
0.00760 U
0.000360 U
0.997
0.00160 U
0.00310 U
0.816
0.00250 U
0.00220 U
2.31
0.00620 U
5.34
0.00731
%REG
%REC Lim112
86 75-125
79
81
81
77
81
85
79
84
87
86
85
82
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
RPD
RPD Mina Nat9E..
Matrix Spike Dup (1E06026-MSD1) Prepared: 05/06/2021 13:38 Ana[yzed: 05/10/2021 10:23
Source: CE05398-02
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Flag P.OL Units Level Result %REC Limits RPD Llmit Notes
1.73 0.100 mg/L 2.00 0.0420 U 87 75-125 0.5 20
0.162 0.0100 mg/L 0,200 0.00760 U 81 75-125 3 20
0.0164 0.00100 mg/L 0.0200 0.000360 U 82 75-125 0.8 20
2.64 0.100 mg/L 2.00 0.997 82 75-125 0.9 20
0.157 B 0.0100 mg/L 0.200 0.00160 U 78 75-125 2 20
0.164 0.0100 mg/L 0.200 0.00310 U 82 75-125 1 20
2.56 0.100 mg/L 2.00 0.816 87 75-125 2 20
0.160 0.0100 mg/L 0.200 0.00250 U 80 75-125 2 20
0.171 0.0100 mg/L 0.200 0.00220 U 85 75-125 2 20
11.2 B 0.500 mg/L 10.0 2.31 89 75-125 1 20
0.169 011100 mg/L 0.200 0.00620 U 85 75-125 1 20
14.0 0.500 mg/L 10.0 5.34 87 75-125 1 20
0.174 0.0100 mg/L 0.200 0.00731 83 75-125 2 20
FINAL This report relates only to the sample as received by the Laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
MetaIs (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1 E06026 - EPA 3005A - Continued
[Post Spike (1E06025-PS1)
Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 10:26
Source: CE05398-02
Analvte
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result BAU P91. Units Level Result %REC Limits RPD
1.7B 0.100 mg/L 2.00 0.0236 BB 80-120
0.168 0.0100 mg/L 0.200 -0.00126 84 80-120
0.0169 0.00100 mg/L 0,0200 0.000151 84 80-120
2.71 0.100 mg/L 2.00 0.997 85 80-120
0.161 8 0.0100 mg/L 0.200 -0.00181 80 80-120
0.171 0.0100 mg/L 0.200 -0.00217 85 80-120
2.61 0.100 mg/L 2.00 0,816 90 80-120
0.166 0.0100 mg/L 0.200 0.000499 83 80-120
0.176 0.0100 mg/L 0.200 0.00158 87 80-120
11.4 B 0.500 mg/L 10.0 2.31 91 80-120
0.170 0,0100 mg/L 0.200 0.00143 84 80-120
14.3 0.500 mg/L. 10.0 5.34 90 80-120
0.180 0.0100 mg/L 0.200 0.00731 87 80-120
Classical Chemistry Parameters - Quality Control
Batch 1E04031 - Seine
RPD
Limit
Blank (1 E04031-BLK1)
Prepared: 05/04/2021 14:02 Analyzed: 05/05/2021 07:55
AnakW
Chemical Oxygen Demand
LC5(1E04031-BS1)
Analvte
Chemical Oxygen Demand
[Matrix Spike (1E04031-MS1)
Source: CE00741-01
Analvte
Chemical Oxygen Demand
Matrix Spike Dup (1E04031-M5D1)
Source: CE00741-01
Iv+
Chemical Oxygen Demand
Batch 1E04040 - NO PREP
lLesult flag
10 U
Result Elan
510
Rases BAR
640
Result
630
I
Blank (1E04040-BLK1)
Analvte
Nitrite as N
Result
LCS (1E04040-851)
Analvte
0.017
Result
POL Units
10 mg/L
JIM
10
MAW
mg/L
PQL Units
10 mg/L
Spike Source
Level Result
%REC
%REC Limits
RPD
RPD Unlit
Prepared: 05/04/2021 14:02 Analyzed: 05/05/2021 07:55
Spike Source
Level Result
500
%REC
%REC Limits
103
90-110
RPD
RPD Limit
Prepared: 05/04/2021 14:02 Analyzed: 05/05/2021 07:55
Spike
Level
526
Source
Result
98
%REC
%REC Limits RPD
103
90-110
Prepared: 05/04/2021 14:02 Analyzed: 05/05/2021 07:55
Spike
Mass PQL units Level
10 mg/L 526
Elan
u
Source
Result
98
%REC
%REC Limits RPD
101 90-110 1
Notes_
N
RPD
LIMB Notes.
RPD
Limit
5
R
Prepared: 05/04/2021 15:24 Analyzed: 05/04/2021 16:24
P9L Units
0.10 mg/L
Spike Source
Level Result
%REC
%REC Limits RPD
RPD
Lind
Met
Prepared: 05/04/2021 15:24 Analyzed: 05/04/2021 16:37
Spike Source
POL Units Level gesult
%REC
%REC Limit& RPD
RPD
Limit RAM
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1EO4014O - NO PREP - Continuer!
[LCS(1E04040-BS1)Continued
Prepared: 95/04/2021 15:24 Analyzed: 05/09/2021 16:37
1
Anali to
Nitrite as N
Result nag
1.1
P0L !Hilts
mg/L
0.10
Spike
Level
1.00
Source
Result
%REC
%REC Limits RPD
108
90-110
RPD
Limit
Matrix Spike (1E04040-MSJ)
Prepared: 05/04/2021 15:24 Analyzed: 05/04/2021 16:26
Source: CE06009-01
Analvte
Nitrite as N
Remit Elan
1.0
Spike
P.41. LInll$ Level
0.10
mg/L
1,00
Source
Bann
0.017 U
%REC
%REC Limits
102
90-110
RPD
RPD Limit
Matrix Spike Dup (1E04040-MSD1)
Prepared: 05/09/2021 15:24 Analyzed: 05/04/2021 16:co
Source: CE06009-01
Analvte
Nitrite as N
Batch 1EO50O7 - NO PREP
Result Eno
1.0
Spike
12 Units Level
0.10 mg/L 1.00
Source
Result
0.017 U
%REC
%REC Limits
104 90.110
RPD
RPD
2
10
Notes
BOISE
[Blank (1E05007-BLK1)
Prepared & Analyzed: 05/05/2021 14:24
Analvte
Biochemical Oxygen Demand
Result Elan
2.0 U
PO.L !Units
2.0 mg/L
Spike Source
Level Result
%REC
%REC Limits RPD
RPD
LI[Dit
LCS(1E05007-SS1)
Prepared & Analyzed: 05/05/2021 19:24
Analvte
Biochemical Oxygen Demand
R of Flan
140
Spike
P9L Units Level
2.0
mg/L
198
Source
Result %REC
71
%REC
Limits
85-115
RPD
RPD
Limit
B-07
Duplicate (1E05007-DUP1)
Prepared & Analyzed: 05/05/2021 14:24
Source: CE01412-01
Analvte
Biochemical Oxygen Demand
Batch 1EO6O11 - Same
R u Rao
500
Spike
P01. Units Level
2.0 mg/1
Source
Result
480
%REC
%REC Limits RPD
3
RPD
Limit
30
Notes
B-07
Blank (1E06011-BLK1)
Prepared: 05/06/2021 08:22 Analyzed: 05/11/2021 11:26
1
Analvte
Total Kjeldahl Nitrogen
Result
0.26
Flag
u
Spike
P01. Units Level
0.48
mg/L
source
Rs llr
%REC
%REC Lmttb
RPD
RPD Limit Notes
LLCS (1E06011-BSI)
Analvte
Total Kjeldahl Nitrogen
ReAUit Elan
12
Prepared: 05/06/2021 08:22 Analyzed: 05/11/2021 11:28
Spike
P91 Untls Level
0.48
mg/L
12.0
Source
R9:sllt
%REC
%REC Limits RPD
103
90-110
RPD
limit
1
Notes
Matrix Spike (1E06011-MS1)
Source: CE00741-01
Analvte
Total Kjeldahl Nitrogen
Result Flag
6.2
P01. Units
0.48 mg/L
Prepared: 05/06/2021 08:22 Analyzed: 05/11/2021 11:31
Spike
Level
4.80
Source
Remit
1.4 101 90-110
%REC
%REC Limits RPD
RPD
Limit
Now
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page B o(13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1E06011 - Same - Continued
Matrix Spike (1E06011-MS2)
Prepared: 05/06/2021 08:22 Analyzed: 05/11/2021 11:37
1
Source: CE01412-01
Analvte
Total Kjeldahl Nitrogen
Result flag
85 0
PQL !MRS
4.8 mg/L
Spike
Level
4.80
Source
Result
83
%REC
%REC Ljmita
49
90-110
RPD
RPD Limit 1
QM-07
`Matrix Spike Dup (1E06011-MSD1)
Source:CE00741-01
Analvte
Total Kjeldahl Nitrogen
Batch 1E06012 - Same
Prepared: 05/06/2021 08:22 Analyzed: 05/11/2021 11:33
1
Spike Source %REC
Resttltt Elam P9.I. linl!E Level Result %REC 11110 g
6.7 0.48 mg/L 4.80 1.4 110 90-110
RPD
RPD Una lochs_
7 10
Blank (1E06012-BLK1)
Prepared: 05/06/2021 08:23 Analyzed: 05/11/2021 12:58
Anatde
Phosphorus
Result BM
0.025 U
Spike Source
Et& WAS Level Begat
0.10
mg/L
%REC
%REG lamitg
RPD
RPD timjt Nan
LCS (1E06012-BS1)
Prepared: 05/06/2021 08:23 Analyzed: 05/11/2021 13:00
Analvte
Phosphorus
Result flag
1.6
E41 Units
mg/L
0.10
Spike Source
Level Result
1.60
%REC
%REC Limits
101
80-120
RPD
RPD Limit Notes_
[Matrix Spike (1E06012-MS1)
Source: CE00741-01
Analvte
Phosphorus
Result flag
1.1
EQL Units
mg/L
0.10
Prepared: 05/06/2021 08:23 Analyzed: 05/11/2021 13:03
Spike Source
Level R
0.640
0.25
%REC
%REC Limits
137
80-120
RPD
RPD Limit
1
Notes
QM-07
[Matrix Spike Dup (1E06012-MSD1)
Source: CE00741-01
Amide
Phosphorus
Batch 1E06026 - EPA 3005A
Prepared: 05/06/2021 0B:23 Analyzed: 05/11/2021 13:04
1
Spike Source %REC RPD
Rwilt Elan INg Units Level newit %REC Limits RPD !jai N2tSC
0.79 0.10 mg/L 0.640 0.25 84 80-120 35 25 QM-11
[Blank(1E06026-BLK1)
Prepared: 05/06/2021 13:38 Analyzed: 05/10/2021 15:00
1
Analvte
Sodium Adsorption Ratio
Batch 1E06027 - NO PREP
Result flan Ell Units
0.00 ll (blank]
Spike Source
Level Result %REC Limits RPD Limit M es
%REC
RPD
Blank (1E06027-BLK1)
Prepared: 05/06/2021 13:50 Analyzed: 05/06/2021 17:13
MAMA
Total Solids
tit Eke
0.0050 U
Spike
PAL Units Level
0.0050 % by Volume
Source
Rpi..kt
%REC
RPD
%REC Limits RPD Limn
LCS (1E06027-BS1)
Prepared: 05/06/2021 13:50 Analyzed: 05/06/2021 17:13
A
Total Solids
Spike Source
Result flan P_Q.L Units Level Rperd}
1000 50 mg/L 1100
%REC RPD
%REC Limits RPD Limit Notes
91 90-110
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in fun.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1E06027 - NO PREP - Continued
[Duplicate (1E06027-DUP1)
Prepared: 05/06/2021 13:50 Analyzed: 05/06/2021 17:13
Source:CE05805-01
Analvte
Total Solids
Batch 1E10008 - NO PREP
Spike Source
Result Elan P9L Units Level gIBB
0.22
0.22 0,0050 % by Volume
RPD
%REC Limits RPD Unlit Notes_
2 5
%REC
Blank (1E10008-BLKI)
Prepared: 05/10/2021 08:50 Analyzed: 05/19/2021 12:22
1
Analvte
Ammonia as N
Result Han POI
0.045 U
0.10
units
mg/L
Spike
Level
Source
Re8uIt•
%REC RPD
%REC L+mils RPD Unit Rotes
LLCS(1E1000B-BS1)
Anal][te
Ammonia as N
Prepared: 05/10/2021 08:50 Analyzed: 05/10/2021 12:24
Spike Source
Result Elan P.M Units Level )result
1.0
0.10
mg/L
1.01
%REC
104
%REC RPD
Limits RPD l.lmt
90-110
Moto_
Matrix Spike (1E10008-MS1)
Prepared: 05/10/2021 0B:59 Analyzed: 05/10/2021 12:28
Source; CE06009-01
Analvte
Ammonia as N
Result Elan FM
0.38
0.10
Units
mg/L
Spike
Level
0.393
Source
)1 L
0.045 U
%REC
%REC Limit# RPD
96
90-110
RPD
Lima Notes_
[Matrix Spike (1E1000B-MS2)
Source: CE06010-01
Analvte
Ammonia as N
Prepared: 05/10/2021 0B:50 Analyzed: 05/10/2021 12:36
1
Blurt HBO PPOL NUBS
0.41 0.10 mg/L
Spike
Level
0.393
Source
Result
0.095 U
%REC RPD
%REC Limits RPD )limit {�Entes
105
90-110
Matrix Spike Dup (1E10008-MSD1)
Source: CE06009-01
Analvte
Ammonia as N
Hatch 1E12009 - NO PREP
Result Else
Prepared: 05/10/2021 08:50 Analyzed: 05/10/2021 12:29
Spike Source %REC
units Level Result %REC Limit
RPD
RPD !LUAU
0.38 0.10 mg/L 0.393 0.045 U 96 90-110 0.4 10
Notes.
Blank(1E12009-BLKI)
Prepared: 05/12/202109:35 Analyzed: 05/12/2021 13:18
Analvte
Nitrate/Nitrite as N
LCS (1E12009-BS1)
1lnallte
Nitrate/Nitrite as N
Matrix Spike (1E12009-MS1)
Source:CE00741-01
Amble
Nitrate/Nitrite as N
Result Elan
0.041 U
Spike
PQL Level
0,10
mg/L
Source
Roma
%REC
%REC Limits
RPD
RPD Li Lt Naas.
Prepared: 05/12/2021 09:35 Analyzed: 05/12/2021 13:20
Spike
Result Mao ink Units Level
1.3
0.10
mg/L
1.25
Source
ROSIN
1
%REC RPD
%REC Limits RPD Lmit Notts.
101
90-110
Prepared: 05/12/2021 09:35 Analyzed: 05/12/2021 13:24
Spike Source
Result Elan PAL Links Level ESSyIt
1.0 0.10 mg/L 0.521 0.47 106 90-110
%REC RPD
%REC Limitg RPD limit Notes_
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1E12009 - NO PREP - Continued
Matrix Spike (1E12009-MS2)
Prepared: 05/12/2021 09:35 Analyzed: 05/12/2021 13:29
Source: CE01412-01
Anaivte
Nitrate/Nitrite as N
Matrix Spike Dup (1E12009-MSD1)
Spike
Result Elan P91 Units Level
0.74
0.10
mg/L
0.521
Source
Relat
0.21
W%REC RPD
%REC Limits RPD Limit Notes
102
90-110
Prepared: 05/12/2021 09:35 Analyzed: 05/12/2021 13:26
Source: CE00741-01
Analvte
Nitrate/Nitrite as N
Result Etas P91 I1nits
1.0
0.10
mg/L
Spike
Level
0.521
Source
0.47
W°REC
WoREC Limits RPD
105
90-110
0.5
RPD
Limit
10
Classical Chemistry Parameters - Quality Control
Batch 1E11075 - NO PREP
1
Blank (1E11075-BLK1)
Prepared: 05/11/2021 16:42 Analyzed: 05/12/2021 11:28
Atryte
Total Suspended Solids
Result Fag
2.5 U
PQL U it
2.5 mg/L
Spike Source
Level Result %REC Limits RPD
%REC
RPD
Limit
Rolm_
LCS (1E11075-BS1)
Prepared: 05/11/2021 16:42 Analyzed: 05/12/2021 11:28
Anal
Total Suspended Solids
Spike
Result Elam PQL Sly Level
120
2.5
mg/L
100
Source
Result
WaREC
118
%REC RPD
Limits RPD inimkt Notes
80-120
Duplicate (1E11075-DUP1)
Prepared: 05/11/2021 16:42 Analyzed: 05/12/2021 11:28
.1
Source: CE05806-01
.Analite
Total Suspended Solids
Spike Source
Result Elan P units Level Result
28000 2.5 mg/L 30000
%REC RPD
°/aREC Limns RPD Limit t 2 s
6 20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 11 of 13

www.encotabs.com
FLAGS/NOTES AND DEFINITIONS
1
B The analyte was detected in the associated method blank.
ID The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 250/0 concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-07 LCS exceeded control limits for this test. The test can not be repeated due to method constraints. The
result should be considered an estimated value.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may ordy be reproduced In fuh. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
10775 Cannel Pprt Dr 4810 Executive Peat Court, SOS 111 102•A Woodwinds ktduslnal CI
Ortondo. FL 32624 Jacksoninile FL 3 216-6069 Cary NC 27511
1407)628.5314 I9041296-3007 Fax f904}296-6210 nil 91487•3090 FaxIMF 467.3515
www.encolabs.com
Page of
Client Nuns
Nanozyn es North America (N0008)
Project Number
[none]
Requested Ana tyaas
Requested Turnaround
Times
Noie Rush requests WNW t0
acceptance by the Iadrly
_ Standard
_ Expedited
Due _II_
i i.
mo
'1.'.„'
§
8
co3
{3)
G
i
I
A
g
Z
B
Z
TSS SM2540D
Address
77 Perry Chapel Church Road
Propel NamaiDesc
Mont* - Week One - WM
Crty'ST.Z,Fr
Franklintion, NC 27525
PO s I Meng Inlo
3700044905
Tal
[phone]
Fax
Reporting Contact
Scott Creech
Sam, lorl' I Name, Alk"Il.11on (PrrntfLib ekt
1(� 11
Bitting Contact
Accounts Rayabhe
Lab 11ii0rkOrefer
CE05806
Samplerlsl ire
Mb
See location 'Tune Zane
�
P.rvr�Co , Ise. d.el
bnecessary)
)Cofn,a.. nessary)
ilim 8
sample ID [Field Ideneltoellonj
Collect on Dale
Colt ctlan
Time
Comp r Grab
Waal
isee eotlesl
Total M of
Containers
Sample Comments
x
x
x
x
X
x
7
r- s4
SBM
✓.y- t)
`
b WI>
6
_X__.
1
1
<-- Total # of Containers
Semple Kr! Prepared By
Deus -Tune
ReknqurshW
C
DefelTxne
5- ,,t� �
Received By
Delarrune
c 4/-ter ostk)
Relinquished By
Dale/Time
Aec By
Da1WTime
Cornmenta/Spsciel Repodelp Requirements
Relinquished By
Det&Trme
Rocerred By
Date/Time
Cooler e'u & Temps on Receipt
1 • i
Condition Upon I
, cceptable _ Unacceptable
yletrix OW-Groundwelar SO-Scil OW-Dnieung Wafer SE -Sediment SWSurtace Water WWWesiewater A -Air O•0ttiner [detail en cons r I j Preservation: Mee k•WCJ N-FIN03 S-1i2SOS NO-NaOR 0.01her IWlei
Note' Ali samples submitted 10 ENCO tabs are m accordance with the tams and conditions listed On the reverse of Ibis toxin union. prior written agreements cost

Sample Preservation Verification
ENCO Cary
Work Order CE05806
Client Novozymes North America (N0008)
Logged In 04-May-21 10 33
Preservation Check Performed By:
Project: Monthly - Week One - SBM
Project #: [none]
Logged By Samantha L Hy {tt cr��
Date/me: 7� Lt (-)0
CE05806-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
^Y
pH Adjusted Datefrme
Adjusted
Reagent Used/Comments
G_
D
250mLP+H2SO4
<2
1 N / NA
4.XJ 1 N / N \LAW Ct(
4 1 0CWA
E
250mLP+HNO3
<2
,i..1) N / NA
Yl N f NA5 ��z ( goo
4 2 �) �.S
1
2
Reagent Name
03 6
ID Reagent Name
(J\CDt c\
Cilipkis
pH Strip ID: CO S S
3
ID Reagent Name
5
6
ID
C:IELMNTIPrintlwko_PreservationCheck_ rpt
Page 1 of 1

2�Sp PCVrENCO Laboratorws
v4e0,77
Accurat Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, June 28, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE06532
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, June 1, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL
This report relates only to the sample as received by the laWratory, and may only be reproduced to fu6. Page 1 of 14

www.encalabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client Ill: SBM Lab ID: CE06532-01.
Sampled: 06/01/21 06:00 Received: 06/01/ 21 08:00
Parameter
CSU Method
EPA 350.1
EPA 351.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 7470A
SM 25408-2011
SM 2540D-2011
SM 5210 B-2011
SM 5220D-2011
preparation
EPA 3005A
NO PREP
Same
NO PREP
[CALL]
EPA 3005A
EPA 7470A
NO PREP
NO PREP
NO PREP
Same
Hold Date/Time(s1
02/25/24
06/29/21
06/29/21
06/03/21 06:00
06/03/21 06:00
11/28/21
06/29/21
06/08/21
06/08/21
06/03/21 06:00
06/29/21
prep Date/Time(s1
06/02/21 10:32
06/09/21 10:27
06/04/21 10:46
06/01/21 15:07
06/10/21 09:26
06/02/21 10:32
06/11/21 09:55
06/08/21 17:42
06/07/21 14:13
06/02/21 09:42
06/03/21 08:14
Analysis Date/Time(51
06/07/21 13:50
06/09/21 14:06
06/07/21 13:33
06/02/21 09:04
06/10/21 14:52
06/07/21 11:01
06/14/21 09:25
06/08/21 17:42
06/08/21 13:50
06/02/21 09:42
06/03/21 15:32
Client ID: SBM
Lab ID: CE06532-01RE2
Sampled: 06/01/21 06:00 Received: 06/01/21 08:00
Parameter
EPA 353.2
Preparation
NO PREP
Mold Date/Time(s)
06/29/21
Pre& Date/ropes}
06/10/21 09:26
Analysis Date/Time(s1
06/10/21 14:52
Client ID: SBM
Lab ID: CE06532-01RE3 Sampled: 06/01/21 06:00
Received: 06/01/21 08:00
parameter
EPA 365.4
Preparation
Same
Hold Date/Time(s)
06/29/21
Prep Date/Time(s1 Analysis Date!Time(s1
06/24/21 10:28 06/25/21 14:22
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In lull.
Page 2of14

SAMPLE DETECTION SUMMARY
L
(E-41E
www.encolabs.com
41
Client ID: SBM Lab ID: CE06532-01
Ana
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium -Total
Chemical Oxygen Demand
Magnesium - rota
Molybdenum - Total
Nickel - Total
Nitrate as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
Client ID: SBM
Nitrate/Nitrite as N
Resultg Flag, MDIW P2 LIT
5.79 0.920 1.00 mg/L
150 D 4.0 9.0 mg/L
9800 2.0 2.0 mg/L
2560 0.390 1.00 mg/L
26000 800 800 mg/L
17.9 0.290 1.00 mg/L
0.0349 3 0.0250 0.100 mg/L
0.0407 3 0.0220 0.100 mgjL
1300 D 41 100 mg/L
0.24 0.017 0.10 mg/L
569 1.50 5.00 mg/L
269 4.00 5.00 mg/L
1.45 [blank]
150 D 26 48 mg/L
1.8 0,0050 0.0050 % by Volume
32000 2.5 2.5 mg/L
0.210 0.0440 0.100 mg/L
Lab ID: CE06532-01RE2
Methad
EPA 6010D
EPA 350.1
SM 5210 B-2011
EPA 6010D
SM 5220D-2011
EPA 6010D
EPA 6010D
EPA 6010D
EPA 353.2
EPA 353.2
EPA 6010D
EPA 6010D
CSU Method
EPA 351.2
SM 2540B-2011
SM 7540D-2011
EPA 6010D
NNu
Client ID: SBM
Analvte
Phosphorus
1300 D
Results Elm NUL
200 D
2.5
41
QL Units
100 mg/L
Lab ID: CE06532-01RE3
10
Units
mg/L
Method
EPA 353.2
Method
EPA 365.4
MOE
Notes
1
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 3 of 14

ANALYTICAL RESULTS
Description: SBM
(Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID:CE06532.01
Sampled:06/01/21 06:00
Sampled By:Elvin C Williamson
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary cettifed anaht [NC 591]
Analvte 'CAS Number)
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Caldum [7440-70-2]^
Copper [7440-50-8]"
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel[7440-02-0]^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-51"
Zinc [7440-66-6]^
Results
5.79
0.0760
0.00360
2560
0.0160
0.0310
17.9
0.0349
0.0407
569
0.0620
269
0.210
Flog ni PF
mg/L 10
U mg/L 10
U mg/L 10
mg/L 10
U mg/L 10
U mg/L 10
mg/L 10
] mg/L 10
] mg/L 10
mg/L 10
U mg/L 10
mg/L 10
mg/L 10
r
bP1 11Q1 JIB Method
0.420 1.00 1F02017 EPA 6010D
0.0760 0.100 1F02017 EPA 6010D
0.00360 0.0100 1F02017 EPA 6010D
0.390 1.00 1F02017 EPA 6010D
0.0160 0.100 1F02017 EPA 6010D
0.0310 0.100 1F02017 EPA 6010D
0.290 1.00 1F02017 EPA 6010D
0,0250 0.100 1F02017 EPA 6010D
0,0220 0.100 1F02017 EPA 6010D
1.50 5.00 1F02017 EPA 6010D
0.0620 0.100 1F02017 EPA 6010D
4.00 5.00 1F02017 EPA 6010D
0.0440 0.100 1F02017 EPA 6010D
www.enmlabs.com
Received: 06/01/21 08:00
Work Order: CE06532
Anslvzed $II Reira
06/07/21 11:01 3DH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
06/07/2111:01 JDH
06/07/21 11:01 3DH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
06/07/21 11:01 3DH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
06/07/21 11:01 JDH
Classical Chemistry Parameters
^ • ENCo Cary certified anah'e INC 5911
Mesta [CAS Number)
Ammonia as N [7664-41-71^
Biochemical Oxygen Demand"
Chemical Oxygen Demand^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Remits flag PALE QE
150 D mg/L 90
9800 mg/L 1
26000 mg/L 80
1300 D mg/L 1000
1300 D mg/L 1000
0.24 mg/L 1
200 D mg/L 100
1.45 [blank] 1
150 D mg/L 100
1.8 % by Volume 1
1
M4 pQL Patch Method Analyzed ¢y
4.0 9.0 1F09021 EPA 350.1 06/09/21 14:06 JAH
2.0 2.0 1F02003 SM 5210 B-2011 06/02/21 09:42 JOC
800 800 1F03003 5M 52200-2011 06/03/21 15:32 30C
41 100 [ICI EPA 353.2 06/10/21 14:52 JAH
41 100 1F10010 EPA 353.2 06/10/21 14:52 JAH
0.017 0.10 1F01032 EPA 353,2 06/02/21 09:04 JAH
2.5 10 1F24015 EPA 365.4 06/25/21 14:22 JAH
1F02017 CSIJ Method 06/07/21 13:50 JDH
26 48 1F04015 EPA 351.2 06/07/21 13:33 JAH
0.0050 0.0050 1F08021 SM 25408-2011 06/08/21 17:42 DM]
Metals by EPA 6000/7000 Series Methods
- EucO Orlando canned analyte (NC 424]
Analvte !CAS Number) R�,gyl_tf Ig Units DF Mph PQL Batch Method Analyzed 43t
MAE
Mercury [7439-97-6]^ 0,000115 U mg/L 5 0.000115 0.00100 1F10034 EPA 7470A 06/14/21 09:25 NRB
Classical Chemistry Parameters
Analvte 'CAS Number)
Total Suspended Solids
BOUM Flag PAtri Ef]4�„L ]a Batch Method Analyzed 1],y 18gt
32000 mg/L 1 2.5 2.5 1F07005 SM 25400-2011 06/08/21 13:50 AAL
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 14

QUALITY CONTROL DATA
Metals (total recoverable} by EPA 6000/7000 Series Methods - Quality CoPr^^r
Batch 1F02017 - EPA 3005A
L
Blank (1F02017-BLK1)
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
0.0420
0.00760
0.000360
0.0390
0.00160
0.00310
0.0290
0.00250
0.00220
0.150
0.00620
0.400
0.00440
Flaw
u
u
u
U
u
U
u
u
u
u
u
PQL
0.100
0.0100
0.00100
0.100
0.9100
0.0100
0.100
0,0100
0.0100
0.500
0.0100
0.500
0.0100
www.encolabs.com
Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 10:26
Spike
Units Level
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Source
Result
%REC RPD
0/%REC Limits RPD Limit
[LCS (1F02017-BS1) Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 10:38
■
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Hau P_4.L Units
2.04 0.100 mg/L
0.202 0.0100 mg/L
0.0200 0.00100 mg/L
2.00 0.100 mg/L
0.196 0.0100 mg/L
0.202 0.0100 mg/L
2.06 0.100 mg/L
0.199 0.0100 mg/L
0.208 0.0100 mg/L
10.2 0.500 mg/L
0.205 0.0100 mg/L
10.3 0.500 mg/L
0.208 0.0100 mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Source
Result
%REC
102
101
100
100
98
101
103
99
104
102
102
103
104
%REC
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
RPD
RPD mi
Matrix Spike (1F02017-M51) Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 10:41
Source: CE07727-91
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Res A am put Unites Level Result %REC Limits
2.24 0.100 mg/L 2.00 0.125 106 75-125
0.202 0.0100 mg/L 0.200 0.00760 U 101 75-125
0.0201 0.00100 mg/L 0.0200 0.000360 U 100 75-125
5.41 0.100 mg/L 2.00 3.64 88 75-125
0.202 0.0100 mg/L 0.200 0.00325 100 75-125
0.205 0,0100 mg/L 0.200 0.00364 101 75-125
2.87 0.100 m9/1- 2.00 0.927 97 75-125
0.200 0.0100 mg/L 0.200 0.00250 U 100 75-125
0.213 0.0100 mg/L 0,200 0.00277 105 75-125
10.6 0.500 mg/L 10.0 0.485 101 75-125
0.207 0.0100 mg/L 0.200 0.00620 U 103 75-125
69.1 0.500 mg/L 10.0 62.4 67 75-125
0.240 0.0100 mg/1- 0.200 0.0271 107 75-125
RPD
RPD Limit =M.
QM-07
FINAL
This report relatrs only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 14

L
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1F02017 - EPA 3005A - Continued
Matrix Spike Dup (1F02017-MSD1)
Source: CE07727-01
_Anaheim
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
2.12
0.207
0.0207
5.51
0.206
0.211
2.94
0.205
0.219
10.7
0.212
70.3
0.247
Flan POL
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 10:43
1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Spike Source
Level RPSIII}
2.00 0.125
0.00760 U
0.000360 U
3.64
0.00325
0.00364
0.927
0.00250 U
0.00277
0.485
0.00620 U
62.4
0.0271
%REC
%REC Limits
100 75.125
104 75-125
104 75-125
94 75-125
102 75-125
104 75-125
100 75-125
103 75-125
108 75-125
102 75-125
106 75-125
79 75-125
75.125
110
RPD
5
2
3
2
2
3
2
2
3
1
2
2
3
RPD
Limit
20
20
20
20
20
20
20
20
20
20
20
20
20
mows
Post Spike (1F02017-PS1) Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 10:45
Source: CE07727-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
2.11
0.198
0.0198
5.47
0.202
0.203
2.86
0.198
0.220
10.5
0.200
69.7
0.241
Elan PQL
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0.500
0.0100
0.500
0.0100
Unit*
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Source
Rana
0.125
0.000740
4.04E-5
3.64
0.09325
0.00364
0.927
0.000191
0.00277
0.485
-0.00343
62.4
0,0271
%REC
%REC LitOilA
99 80-120
99 80-120
99 80-120
91 80-120
99 80-120
100 80-120
97 80-120
99 80-120
109 80-120
100 80-120
100 80-120
73 80-120
107 80-120
RPD
RPD 'mit Notes_
QM-08
Classical Chemistry Parameters - Quality Control
Batch 1F01032 - NO PREP
Blank (1F01032-BLK1)
Prepared: 06/01/2021 15:07 Analyzed: 06/02/2021 08:57
1
Analvte
Nitrite as N
Result Eas
u
0.017
Spike Source
PQL Units Level Result %REC limits RPD
0.10
mg/L
%REC
RPD
Limit
[LCS(1F01032-BSI)
Prepared: 06/01/2021 15:07 Analyzed: 06/02/2021 09:08
1
.Analvte
Nitrite as N
Spike Source
Result flag Ka Malts Level Result
1.0 0.10 mg/L 1.00
%REC
%REC SUE
101 90-110
RPD
RPD Limit Notes
Matrix Spike (1F01032-MS1) Prepared: 06/01/2021 15:07 Analyzed: 06/02/2021 08:59
Source:CE06358-01
Analvte
FINAL
Spike Source %REC RPD
Result Elan POL Units Level Emit %REC Limits RPD LIn i NAM
"this report relates only to the sample as received try the laboratory, and may orgy be reproduced in full.
Page 6 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1F01031- NO PREP - Continued
Matrix Spike (1F01032-MS1) Continued
Prepared: 06/01/2021 15:07 Analyzed: 06/02/2021 OB:59
1
Source: CE06358-01
AnalleP
Nitrite as N
Result
1.1
Spike
Flag POI Units Level
0.10
mg/L
1.00
Source
Result
0.017 U
%REC
o/oREC Lim€ts
106
90-110
RPD
RPD limit Notes
Matrix Spike Dup (1F01032-MSD1)
Source:CE0635B-01
ARAM
Nitrite as N
Batch 1F02003 - NO PREP
Result kiag
1.1
PIM Units
0.10 mg/L
Prepared: 06/01/2021 15:07 Analyzed: 06/02/2021 09:00
Spike
Level
1.00
Source
Result
0.017 U
%REC
108
%REC
that RPD
90-110 1
RPD
'm€
10
1
[Blank (1F02003-BLK1)
Prepared & Analyzed: 06/02/2021 09:42
1
Analvte
Biochemical Oxygen Demand
Spike
Result Flag ROL Molls Level
2.0 U
2.0
mg/L
Source
%REC
%REC L€m€ts RPD
RPD
Ling
Kolas
LCS(1F02003-BS1)
Prepared & Analyzed: 06/02/2021 09:42
1
1.11PUte
Biochemical Oxygen Demand
Result nag
180
PQL Units
2.0 mg/L
Spike Source
Level &Eat
198
%REC
91
%REC
Lim€ts
85-115
RPD
RPD m€t Notes
Duplicate (1F02003-DUP1)
Prepared & Analyzed: 06/02/2021 09:42
1
Source: CE03343-01
Analvte
Biochemical Oxygen Demand
Batch .I F02017 - EPA 3005A
Result nag
2.0 U
Spike
POL !A01� Level
2.0 mg/L
Source
Result
2.0 U
%REC
%REC Limitf RPD
RPD
Limit
30
Nam_
Blank (1F02017-BLK1)
Prepared: 06/02/2021 10:32 Analyzed: 06/07/2021 13:50
MAAR
Sodium Adsorption Ratio
Batch 1F03003 - Same
Result Flag
0.00 U
201. Units
[blank}
Spike
Level
Source
Rasa
%REC
%REC Limit& RPD
RPD
Unlit HOW_
[Blank (1F03003-BLK1)
Prepared: 06/03/2021 08:14 Analyzed: 06/03/2021 15:32
Analvte
Chemical Oxygen Demand
ILCS (1F03003-BS1)
Analvte
Chemical Oxygen Demand
Result
10
Spike Source %REC
Bag )'41 clods Level Result %REC Limits
U 10 mg/L
Result Elan
510
PQL Units
10 mg/L
RPD
RPD LimiS Notes
Prepared: 06/03/2021 0B:14 Analyzed: 06/03/2021 15:32
Spike Source
Level Result
500
%REC
%REC 3mmit6 RPD
102
90-110
RPD
Limit
1
Ma„
',Matrix Spike (1F03003-MS1)
Prepared: 06/03/2021 08:14 Analyzed: 06/03/2021 15:32
Source: CE06319-01
„Aluidg
Chemical Oxygen Demand
Result
670
Spike
EQL Units Level
10 mg/L 526
Source
Result
140
%REC
%REC gooks_
101 90-110
RPD
RPD Limit Nobel_
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Pape 7 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1F03003 - Same - Continued
Matrix Spike Dup (1F03003-MSD1)
Prepared: 06/03/2021 08:14 Analyzed: 06/03/2021 15:32
1
Source: CE06319-01
Analvte
Chemical Oxygen Demand
Batch 1F04014 - Same
Result Nan
670
PQL Unit
10 mg/l.
Spike
Level
526
Source
Result
140
%REC
100
%REC
Limits
90-110
RPD
RPD Limit Notes
0.7
5
Blank (1F04014-BLK1)
Prepared: 06/04/2021 10:33 Analyzed: 06/07/2021 15:59
Analvte
Phosphorus
Result
0.025
Elan
U
Spike Source
Ent UJ1it4 Level Result %REC Limit RPD
0.10
mg/L
%REC
RPD
Limit
[LCS (1F04014-BSI)
Analvte
Phosphorus
Result Flag
1.7
POL Units
mg/L
0.10
Prepared: 06/04/2021 10:33 Analyzed: 06/07/2021 16:01
Spike Source
Level Result
1.60
%REC
%REC Limits RPD
108
80-120
RPD
-mi
Notes
Matrix Spike (1F04014-M51)
Prepared: 06/04/2021 10:33 Analyzed: 06/07/2021 16:03
1
Source: CE06358-01
Analvte
Phosphorus
Result EIa9
3.6 E
Spike
PQL Units Level
0.10
mg/L
0.640
Source
Result
3.3
%REC
%REC Limits RPD
36
80-120
RPD
limit
Notes
QM-07
I Matrix Spike Dup (1F04014-MSD1)
Prepared: 06/04/2021 10:33 Analyzed: 06/07/2021 16:05
1
Source: CE06358-01
.Anahie
Phosphorus
Batch 1F04015 - Same
Result Elan
3.3 E
Spike
pQL Units Level
0.10 mg/L 0.640
Source
Result
3.3
%REC
%REC Lr,� mils RPD
NR 80-120 7
RPD
mil
25
Hotel
QM-07
Blank (1F04015-SLK1)
Prepared: 06/04/2021 10:46 Analyzed: 06/07/2021 13:10
1
Total Kjeldahl Nitrogen
LCS (1F04015-BSI)
.ADande
Total Kjeldahl Nitrogen
Matrix Spike (1F04015-MS1)
Source: CE06358-01
Aaallde
Total Kjeldahl Nitrogen
Result Ela9
0.26 U
Result flag
13
Result Bas
5.6
PQL
0.48
Spike Source
Units Level Result %REC Limits RPD
mg/L
EOL Units
mg/L
0.48
POL Units
mg/L
0.48
%REC
Prepared: 06/04/2021 10:46 Analyzed: 06/07/2021 13:12
Spike Source
Level Result
12.0
%REC
%REC Limits
110
90-110
RPD
Limit
RPD
RPD Limit Kole
Prepared: 06/134/2021 10:46 Analyzed: 06/07/2021 13:15
Spike
Level
4.80
Source
Result
0.66
%REC
%REC Limits RPD
103
90-110
RPD
Unit
1
',Matrix Spike (1F04015-MS2)
Source:CE06531-02
Total Kjeldahl Nitrogen
Prepared: 06/04/2021 10:46 Analyzed: 06/07/2021 13:21
Result flag
23 D
PQL
Wit$
2.4 mg/L
Spike Source
Level BOA
4.80 18
%REC
%REC Limits RPD
103 90-110
RPD
Limit Natal
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in fut.
Page 13of14

:
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1F04015 - Same - Continued
Matrix Spike Dup (1F04015-MSD1)
Prepared: 06/04/2021 10:46 Analyzed: 06/07/2021 13:17
Source: CE06358-01
Total Kjeldahl Nitrogen
Batch 1E08017 - NO PREP
Spike Source %REC RPD
Result flan ED3 llnits Level Result: %REC Limits RPD Limit Notes
4.1 0.48 mg/L 4,80 0.66 71 90-110 33 10 QM-07,
QM-11
[Blank (1F08017-BLK1)
Prepared: 06/08/2021 13:48 Analyzed: 06/08/2021 14:57
1
Analvte
Nitrate/Nitrite as N
Spike Source
Result Flag Ell Units Level Result %REC Limits RPD IBnit
0.041 Li
0.10
mg/L
%REC
RPD
[LCS(1F08017-BS1)
-AuallLte
Nitrate/Nitrite as N
Prepared: 06/08/2021 13:48 Analyzed: 06/08/2021 14:59
Spike
Result Ban pm. Units Level
1.2
0.10
mg/L
1.25
Source
Result
%REC
%REC Limits
92
90-110
RPD
RPD amjt
1
Matrix Spike (1F08017-MS1)
Prepared: 06/08/2021 13:48 Analyzed: 06/08/2021 15:02
Source: CE05822-01
Analvte
Nitrate/Nitrite as N
Result !Flag
15
P01 Units
1.0 mg/L
Spike Source
Level Result
5.00
11
%REC RPD
%REC limits RPD i i t
91
90-110
[Matrix Spike (1F08017-MS2)
Source:CE05822-02
Analvte
Nitrate/Nitrite as N
Prepared: 06/08/2021 13:48 Analyzed: 06/08/2021 15:08
Result flag PM Units
12
1.0
mg/L
Spike
Level
5.00
Matrix Spike Dup (1F08017-MSD1)
Source: CE05822-01
.Analvte
Nitrate/Nitrite as N
Batch 1E011021 - NO PREP
Source
EIS=
7.3
%REC RPD
%REC Limits RPD Limit Notes
103
90-110
Prepared: 06/08/2021 13:48 Analyzed: 06/08/2021 15:04
Spike Source
Result flan PO1. Units Level Result
15 1.0 mg/L 5.00 11
%REC RPD
%REC =Its RPD Limit Noi
83 90-110 2 10 QM-07
[
Blank (1F08021-BLK1)
Prepared & Analyzed: 06/08/2021 17:42
Analvte
Total Solids
Result Elan
u
0.0050
Spike Source
POL Units Level
0.0050 % by Volume
Result
%REC
RPD
%REC Limits RPD
LCS (1F08021-BS1)
Prepared & Analyzed: 06/08/2021 17:42
1
Analvte
Total Solids
Result
1100
Spike
flag P41 Unim Level
1100
50
mg/L
Source
&:Suit
%REC
%REC Limits
101 90-110
RPD
RPD Limit 1(012s-
Duplicate (1F08021-DUP1)
Prepared & Analyzed: 06/08/2021 17:42
Source:CE06531-01
,Ara Lte Result flan
Total Solids 022
Batch 1F09021- NO PREP
0.0050 % by Volume
Spike Source
POI. Units Level Result
0.22
%REC RPD
%REC Limits RPD Limit N
a 5
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full
Page9 of 14

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QUALITY CONTROL DATA
Iassical Chemistry Parameters - Quality Control
Batch 1F09021 - NO PREP - Continued
LB1ank(1F09021-BLK1)
Prepared: 06/09/2021 10:27 Analyzed: 06/09/2021 13:42
Analvte
Ammonia as N
Result Rag
0.045 LI
Spike
PQL Units Level
0.10
mg/L
Source
Result
%REC
%REC Limits RPD
RPD
Limit
Rotes
LCS(1F09021-BS1)
Prepared: 06/09/2021 10:27 Analyzed: 06/09/2021 13:44
nal
Ammonia as N
i Matrix Spike (1F09021-MSI)
Result flag P
1.0
0.10
Units
mg/L
Spike Source
Level Result
1.01
%REC
%REC Limits
99
90-110
RPD
RPD Li ni
Prepared: 06/09/2021 10:27 Analyzed: 06/09/2021 13:47
1
Source: CE03343-01
Analyte
Ammonia as N
Result Fiaa POL Lini
0.35
0.10
mg/L
Spike
Level
0.393
Source
Boat
0.045 U
%REG
%REC Limits RPD
90
90-110
RPD
Limit
Matrix Spike (1F09021-MS2)
Source: CE05038-01
Anallde
Ammonia as N
[Matrix Spike Dup (1F09021-MSD1)
Source: CE03343-01
Analvte
Ammonia as N
Batch 1F10010 - NO PREP
tZ t flag
0.37
Prepared: 06/09/2021 10:27 Analyzed: 06/09/2021 13:56
Spike
PQL Units Level
0.10
mg/L
0.393
Source
0.045 U
%REC
%REC Omits RPD
95
90-110
Prepared: 06/09/2021 10:27 Analyzed: 06/09/2021 13:49
RPD
Limit
1
Notes
Result Flan
0.36
Spike
SQL Units Level
0.10 mg/L
Source
Result
0,393 0.095 U
%REC RPD
%REC Limits RPD Limit NQ 55
92 90-110 3 10
Blank (1F10010-BLK1)
Prepared: 06/10/2021 09:26 Analyzed: 06/10/2021 13:36
Analyte
Nitrate/Nitrite as N
Result Flag
U
0.041
Spike Source
PQL Uni14 Level gInt %REC Limits RPD
0.10 mg/L
%REC
RPD
Limit
LCS(1f10010-B51)
Analvte
Nitrate/Nitrite as N
',Matrix Spike (1F10010-MS1)
Source: CE07725-05
Analvte
Nitrate/Nitrite as N
Result €Ins PQL Units
1.2
0.10
mg/L
Prepared: 06/10/2021 09:26 Analyzed: 06/10/2021 13:37
Spike Source
Level BOO
1.25
%REC
%REC 1 It5 RPD
98
90-110
Prepared: 06/10/2021 09:26 Analyzed: 06/10/2021 13:41
RPD
VAR MSS -
1
Spike
Mtn& Flag PQL Units Level
mg/L 0.521
0.68
0.10
Source
Mud
0.11
%REC
%REC Limits RPD
109
90-110
RPD
Limit
[Matrix Spike (IF10010-MS2)
Source: CE07725-06
.Anavte
Nitrate/Nitrite as N
Prepared: 06/10/2021 09:26 Analyzed: 06/10/2021 13:47
Result Flag
0.64
Spike Source
PQL !lnjts Level
0.10 mg/L 0.521
%REC
%REC limits RPD
0.085 107 90-110
RPD
l �rlt
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 10of14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1E10010 - NO PREP - Continued
Matrix Spike Dup (1F10010-MSDL)
Prepared: 06/10/2021 09:26 Analyzed: 06/10/2021 13:43
Source: CE07725-05
Analvte
Nitrate/Nitrite as N
Batch 1F24015 - Same
Result Flag
0.67
PQL Units
0.10 mg/L
Spike Source
Level Result
0.521 0.11
%REC
%REC Li i RPD
107 90-110 2
RPD
LiB1i5 spans
10
Blank (1F24015-BLK1)
Prepared: 06/24/2021 10:28 Analyzed: 06/25/2021 14:13
1
_PoSaftte
Phosphorus
LCS (1F24015-BS1)
ABalmte
Phosphorus
Result Elan
0.025 U
Spike
E.0.1 Units Level
0.10
Result flag P01
1.7
0.10
mg/L
Units
mg/L
Source
gala
%REC
%REC Limits RPD
Prepared: 06/24/2021 10:28 Analyzed: 06/25/2021 14:14
Spike Source
Level Result
1.60
%REC
%REC Limits RPD
105
80-120
RPD
Limit
RPD
Limit
N
1
[Matrix Spike (1F24015-MS1)
Source: CE06539-01
Analvte
Phosphorus
Prepared: 06/24/2021 10:28 Analyzed: 06/25/2021 14:17
1
Kermit flag
3.9 i)
Spike
P0. Units Level
0.50
mg/L
0.640
Source
Result
3.1
%REC
%REC Linllti RPD
122
80-120
RPD
Limit
Notes
QM-07
Matrix Spike Dup (1F24015-MSD1)
Prepared: 06/24/2021 10:28 Analyzed: 06/25/2021 14:18
Source: CE06539-01
Analvte
Phosphorus
Result Flat
3.9 D
P01 Units
0.50 mg/L
Spike Source
Level Result %REC
0.640 3.1
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1F10034 - EPA 7470A
%REC
Limits
RPD
133 80-120 2
RPD
Limit
25
Notes
QM-07
[Blank (1F10034-BLK1)
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 09:10
.An:tb[l:e
Mercury
Blank(1F10034-BLK2)
Result
2.30E-5
Flan NM
u 0.000200
Units
mgfl.
Spike Source
Level Sat&
%REC
%REC Limlilt RPD
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 09:37
RPD
Limit
1
Analvte
Mercury
Remit Has P01
2.30E-5 U 0.000200
Spike Source %REC RPD
WAS Level Result %REC Limits RPD Limit Notes
mg/L
r LC5 (1F10034-BS1)
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 09:13
Analvte
Mercury
Result
0.00545
Ban P41.
0.000200
Units
mg/L
LCS(1F10034-B52)
Analvte
Mercury
Rend Elam PQL.
0.00571 0.000200
Units
mg/L
Spike
Level
0.00500
Source
Result
%REC
%REC Limits RPD
109
80-120
RPD
Limit Notes
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 10:14
Spike
Level
0.00500
Source
Result
%REC
%REC 1[LLLtEE RPD
114 80-120
RPD
Limit
Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11of14

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1F10034 - EPA 7470A - Continued
Matrix Spike (1F10034-MS1)
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 09:19
Source: AE05003-02
ADabt#&
Mercury
Matrix Spike Dup (1F10034-MSD1)
Source: AE05003-02
Apalvte
Mercury
Spike Source
Result Flag PM. Units Level Result
0.00564 0.000200 mg/L 0.00500 2.30E-5 U
Result Elea P91. Unita
0.00575 0.000200
mg/L
%REC
%REC Limits RPD
113
75-125
Prepared: 06/11/2021 09:55 Analyzed: 06/14/2021 09:22
Spike
Level
0.00500
Source
Result
2.30E-5 U
%REC
%REC Limps
115
75-125
RPD
2
RPD
Limit Naffs
RPD
Lim
20
lassical Chemistry Parameters - Quality Control
Batch 1E07005 - NO PREP
1
Blank (1F07005-BLK1)
Prepared: 06/07/2021 14:13 Analyzed: 06/G8/2021 13:50
1
Anal
Total Suspended Solids
Result Firma
U
2.5
PAL
2.5
Spike Source
Units Level Result
mg/L
%REG
%REC Limits RPD
RPD
Lift
Notes
LCS (1F07005-BS1)
Prepared: 06/07/2021 14:13 Analyzed: 06/08/2021 13:50
Anaivte
Total Suspended Solids
Duplicate (1F07005-DUP1)
Sou rce: AE04202-01
Analvie
Total Suspended Solids
Spike
Result flag PBL Units Level
mg/L 100
92
2.5
Source
Result
%REC RPD
%REC Limits RPD mi lY
92
80-120
Prepared: 06/07/2021 14:13 Analyzed: 06/08/2021 13:50
■
Spike Source %REC RPD
Result Bali PQL Units Level Resu tl %REC Limits RPD -mit Notes
3.0 2.5 mg/L 3.0 0 20 LP-02
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
tl The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
fE The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC1 Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
LP-02 Filtered residue did not meet 2.5 - 200mg range.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in foil. Page 13 of 14

Standard
aoKZWS Etsl
Sample Comments
X
Ieasays SJTCC • N se IN
Lt
O$sti UO dJOSpV EMI Le
❑oasvis Goo
eo6Z5WS 008 I
WI1'd"i£9e XON'1'096 Y
et-
tosNierIh(1N'orferi ruOir '.oWFr
X
X
X
X
X
X
A
1
Li
CD
r
Oa
i
og
ti
ai
w
co
0
E
0
i
s
1
a
as
a
IU
00

Sample Preservation Verification
ENCO Cary
Work Order- CE06532
Client: Novozymes North America (NO008)
Logged In: 01-Jun-21 11:08 •
Preservation Check Performed By.
Project: Monthly - Week One - SBM
Project #: [none]
Logged By- Rachel Ann Ycinisth `` r
DatelTime: _
Cant
T
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTime
Adiusted
Reagent Used/Commentsype
D
250mLP+H2SO4
<2
/Y ! N / NA
N / NA WI y L 4
k.JC-�0
1-
YY1L C1Z.SC --1
E
250mLP+HNO3
<2
N / NA
Y
N / NA
.�
4-nAL
k-\(\ 03
1
2
Reagent Name
ID Reagent Name
0,IC ocrSci
\ DvM
pH Strip ID
PH Strips COF0555
_ rpt
3
4
1D
5
6
Reagent Name ID
Page 1 of 1

ENCO Laboratorks
Accurate. Timely. Responsive. Innovative.
ve.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, July 15, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none), Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE08079
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, July 6, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosu re(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduces in full. Page 1 of 13

Client ID: SBM
Parameter
CSU Method
EPA 350.1
EPA 351.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 7470A
SM 25408-2011
SM 2540D-2011
SM 5210 B-2011
SM 5220D-2011
Client ID: SBM
parameter
EPA 365.4
SAMPLE SUMMARY/LABORATORY CHRONICLE
Preparation
EPA 3005A
NO PREP
Same
NO PREP
[CALC]
NO PREP
EPA 3005A
EPA 245.1
NO PREP
NO PREP
NO PREP
NO PREP
Lab ID: CE08079-01
Hold Date/Timersl
03/31/24
08/03/21
08/03/21
07/08/21 00:30
07/08/21 00:30
08/03/21
01/02/22
08/03/21
07/13/21
07/13/21
07/08/21 00:30
08/03/21
07/07/21
07/12/21
07/09/21
07/07/21
07/09/21
07/09/21
07/07/21
07/08/21
07/12/21
07/13/21
07/07/21
07/09/21
www.encolabs.com
Sampled: 07/06/21 00:30 Received: 07/06/21 08:00
Prep Date/Time(sl
10:10
10:08
11:55
15:41
10:39
10:39
10:10
10:22
18:30
21:00
15:04
10:06
Apalvsls Date/Time(sl
07/08/21 15:49
07/12/21 12:57
07/12/21 17:22
07/07/21 17:20
07/09/21 14:25
07/09/21 14:25
07/08/21 11:06
07/09/21 14:03
07/12/21 18:30
07/13/21 21:00
07/07/21 15:04
07/09/21 13:04
Lab ID: CE08079-01RE1
preparation Bold Date/Time(s)
Same 08/03/21
Sampled: 07/06/21 00:30 Received: 07/06/21 08:00
prep Date/Time(s)
07/09/21 11:55
Analysis Date/Time(sl
07/13/21 12:54
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 2 af 13

SAMPLE DETECTION SUMMARY
1
www.encolabs.com
Client ID: SBM
Lab ID: CE08079-01
Analvbe
Aluminum - Total
Ammonia as N
8lochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Magnesium - Total
Molybdenum - Total
Nickel - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
Results nest
53.7
93
6100
2070
26000
0.571
0.0318
0.0363
7.8
7.9
0.14
555
350
1.64
1700
2.0
29000
0.0800
MDL j ni Method
0.420 1.00 mg/L EPA 6010D
D 4.0 9.0 mg/L EPA 350.1
2.0 2.0 mg/L SM 5210 8-2011
0,390 1.00 mg/L EPA 6010D
800 800 mg/L SM 52200-2011
3 0.290 1.00 mg/L EPA 6010D
3 0.0250 0.100 mg/L EPA 6010D
3 0.0220 0.100 mg/L EPA 6010D
D 0.82 2.0 mg/L EPA 353.2
D 0.82 2.0 mg/L EPA 353.2
0.017 0.10 mg/L EPA 353.2
1.50 5.00 mg/L EPA 6010D
4.00 5.00 mg/L EPA 6010D
[blank] CSU Method
D 26 48 mg/L EPA 351.2
0.12 0.12 % by Volume SM 25408-2011
500 500 mg/L SM 2590D-2011
3 0.0440 0.100 mg/L EPA 6010D
Client ID: SBM Lab ID: CE08079-01RE1
ARAM Results flag MIL
1Q4 e�
Phosphorus 520 D 12 50 mg/L
Notes
Mathes! haw
EPA 365.4
FINAL This report relates only to the sample as received ay the laboratasy, and may only be reproduced in full.
Page 3 of 13

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID:CE08079-01
Sampled:07/06/21 00:30
Sampled By:John C Hilliard Ir
Received: 07/06/21 08:00
Work Order: CE08079
Metals by EPA 6000/7000 Series Methods
^ - ENCCD Cary cerbhed artalyfe INC 591]
Analyte FCAS Numberl
Mercury [7439-97-6]^
RessiiI[e Ea unite QE MDL E4.L fiat.h
0.00150 U mg/L
10 0.00150 0.00200 1G08023
Method
EPA 7470A
Maimed MX rotes
07/09/21 14:03 KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary coifed analyte (MC 591]
Analvte FCAS Numberl
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Calmum [7440-70-2]^
Copper [7440-50-8]^
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel [7440-02-01"
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc [7440-66-6]^
Results fj g
53.7
0.0760
0.00360
2070
0.0160
0.0310
0.571
0.0318
0.0363
555
0.0620
350
0.0800
ryjjg IN MEL PQL Batch Method Analyzed �]C
mg/L 10 0.420 1.00 1G06017 EPA 6010D 07/08/21 11:06 JDH
U mg/L 10 0.0760 0.100 1G06017 EPA 6010D 07/08/21 11:06 JDH
U mg/L 10 0.00360 0.0100 1G06017 EPA 6010D 07/08/21 11:06 JDH
mg/L 10 0.390 1.00 1006017 EPA 6010D 07/08/21 11:06 JDH
U mg/L 10 0.0160 0.100 1G06017 EPA 6010D 07/08/21 11:06 JDH
U mg/L 10 0.0310 0.100 1006017 EPA 6010D 07/08/21 11:06 JDH
J mg/L 10 0.290 1.00 1006017 EPA 6010D 07/08/21 11:06 3011
] mg/L 10 0.0250 0.100 1G06017 EPA 6010D 07/08/21 11:06 JDH
] mg/L 10 0.0220 0.100 1G06017 EPA 6010D 07/08/21 11:06 JDH
mg/L 10 1.50 5.00 1G06017 EPA 6010D 07/08/21 11:06 JDH
U mg/1. 10 0,0620 0.100 1G06017 EPA 60100 07/08/21 11:06 3011
mg/L 10 4.00 5.00 1G06017 EPA 6010D 07/08/21 11:06 JDH
] mg/L 10 0.0440 0.100 1G06017 EPA 6010D 07/08/21 11:06 JDH
Classical Chemistry Parameters
Notes
- ENCO Gary certified artalyte [NC 5911
Anahrte [CAS Numbed
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand"
Chemical Oxygen Demand^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Total Suspended Solids^
Bards Flag Units PE Ma fQ1. Batch Method Anaivzed Ily Mau
93 D mg/L 90 4.0 9.0 1012013 EPA 350.1 07/12/21 12:57 JAH
6100 mg/L 1 2.0 2.0 1G07013 SM 5210 8-2011 07/07/21 15:04 JOC
26000 mg/L 80 800 800 1G09009 SM 52200-2011 07/09/21 13:04 JOC
7.8 D mg/L 20 0.82 2.0 [CALC] EPA 353.2 07/09/21 14:25 Ali
7.9 D mg/L 20 0,82 2.0 1G09022 EPA 353.2 07/09/21 14:25 JAH
0.14 mg/L 1 0.017 0.10 1G07020 EPA 353.2 07/07/21 17:20 }AH
520 0 mg/L 500 12 50 1G09020 EPA 365.4 07/13/21 12:54 JAH
1.64 [blank] 1 1G06017 CSU Method 07/08/21 I5:49 JDH
1700 D mg/L 100 26 98 1G09018 EPA 351.2 07/12/21 17:22 JAH
2.0 % by Volume 25 0.12 0.12 1G12046 SM 2540B-2011 07/12/21 18:30 DM)
29000 mg/L 200 500 500 1G09007 SM 25400-2011 07/13/21 21:00 ZGW
FINAL This report relates only to the sample as received try the laboratory, and may only be reproduced in full.
Page 4 of 13

www.encolabs.com
QUALITY CONTROL DATA
jetals by EPA 6000/7000 Series Methods - Quality Control
Batch 1G08023 - EPA 243.1
[Blank(1G08023-BLK1)
Prepared: 07/08/2021 10:22 Analyzed: 07/09/2021 13:03
tialitte
Mercury
Blank (1G08023-BLK2)
Ana
Mercury
Spike Source
Result Etas EDI Units Level
0.000150 U 0.000200
mg/L
Result E1e P93. Units
0.00300 U 0.00400
mg/L
%REC
RRgauit< %REC Limits RPD
Prepared: 07/08/2021 10:22 Analyzed: 07/09/2021 13:05
Spike Source
Level Result
%REC
%REC Limits RPD
RPD
limit
RPD
Limit
N
LLCS(1G08023-BS1)
Analvte
Mercury
Result Ftwi PQL
0.00516
0.000200
Units
mg/L
Prepared: 07/08/2021 10:22 Analyzed: 07/09/2021 13:07
Spike Source
Level Result
0.00500
%REC
%REC Lints RPD
103
80-120
RPD
Limit
Matrix Spike (1G08023-MS1)
Prepared: 07/08/2021 10:22 Analyzed: 07/09/2021 13:10
1
Source: CE09426-05
Ailablll!
Mercury
Result Flan POL
0.00496 0.000200
Units
mg/L
Source
Result %REC
0.00500 0.000150 U 99
Spike
Level
%REC
Limits RPD
75-125
RPD
OAR
Notes.
Matrix Spike Dup (1G08023-MSD1)
Prepared: 07/08/2021 10:22 Analyzed: 07/09/2021 13:17
1
Source: CE09426-05
Ana!yte
Mercury
Result Elan PC& Units
0.00489 0.000200
mg/L
Spike
Level
0.00500
ource
Result
0.0S00150 U
%REC
%REC Limits RPD
98
75-125
Post Spike (1G08023-PSI)
Prepared: 07/08/2021
10:22 Analyzed: 07/09/202
Source: CE09426-05
Analvte
Mercury
Spike
Result Flag P91. Units Level
4.95
0.200
ug/L
5.00
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1006017 - EPA 3005A
Source
Rona
0.0348
%REC
%REC
98
75-125
RPD
Lin -
1 25
1 13:19
RPD
RPD lim
Notes
Blank (1006017-BLK1)
Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 10:31
_Amble
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Flan MIL Units
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
Spike Source
Level Rs6SIIt
%REC
%REC Limits RPD
RPD
Lk&
1
FINAL This report relates only to the sample as reeved by the leboratoty, and may only be reproduced in full.
Page 5 of 13

www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1G06017 - EPA 3005A - Continued
LCS(1G06017-BSI)
Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 10:37
i_AiWyto
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result D8u W. Units
1.98 0.100 mg/L
0.200 0.0100 mg/L
0.0201 0.00100 mg/L
2.05 0.100 mg/L
0.191 0.0100 mg/L
0.203 0.0100 mg/L
1.92 0.100 mg/L
0.202 0.0100 mg/L
0.208 0.0100 mg/L
9.96 0.500 mg/L
0.207 0.0100 mg/L
9.96 0.500 mg/L
0.209 0.0100 mg/L
Spike Source %REC
Level Emit %REC Limits
2.00 99 80-120
0.200 100 80-120
0.0200 100 80-120
2.00 102 80-120
0.200 96 80-120
0.200 101 80-120
2.00 96 80-120
0.200 101 80-120
0.200 104 80-120
10.0 100 80-120
0.200 103 80-120
10.0 100 80-120
0.200 104 80-120
RPD
RPO Unfit Notes
Matrix Spike (1G06017-MS1) Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 10:40
Source: CE10039-37
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Eis14 ES& units
2.10 0.100 mg/L
0.211 0.0100 mg/L
0.0201 0.00100 mg/L
66.9 0.100 mg/L
0.197 0.0100 mg/L
0.205 0.0100 mg/L
10.2 0.100 mg/L
0.217 0.0100 mg/L
0.219 0.0100 mg/L
25.1 0.500 mg/L
0.206 0.0100 mg/L
16.3 0,500 mg/L
0.225 0.0100 mg/L
Spike Source %REC
Level ggjt %REC Limits
2.00 0.0563 102 75-125
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
0.00760 U 105
0.000360 U 100
63.5 144
0.00235 97
0.00310 U 103
7.95 110
0.0107 103
0.00294 106
14.6 105
0.00620 U 103
6.09 102
0.0102
107
75-125
75.125
75-125
75-125
75-125
75-125
75-I25
75-125
75-125
75-125
75-125
75-125
RPD
RPD Limit Notes
Matrix Spike Dup (1G06017-MSD1) Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 10:42
Source: CE10039-37
Analvde
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
QM-07
Spike Source %REG RPD
Result 1 PPP Units Level Result %REC timitii RPD alai ai =IL
2.02 0.100 mgJL 2.00 0.0563 98 75-125 4 20
0.201 0.0100 mg/L 0.200 0.00760 U 101 75-125 5 20
0.0191 0.00100 mg/L 0.0200 0.000360 U 95 75-125 5 20
63.9 0.100 mg/L 2.00 63.5 17 75-125 4 20 QM-07
0.199 0.0100 mg/L 0.200 0.00235 96 75-125 2 20
0.193 0.0100 mg/L 0.200 0.00310 U 96 75-125 6 20
9.66 0.100 mg/L 2.00 7.95 86 75-125 5 20
0.204 0,0100 mg/L 0.200 0.0107 97 75-125 6 20
0.201 0.0100 mgJL 0.200 0.00294 99 75-125 6 20
29.3 0.500 mg/L 10.0 14.6 97 75-125 3 20
0.196 0.0100 mg/L 0.200 0.00620 U 98 75-125 5 20
15.8 0.500 mg/L 10.0 6.09 97 75-125 3 20
0.211 0.0100 mg/L 0.200 0.0102 100 75-125 7 20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 13

QUALITY CONTROL DATA
www.encolabs.com
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1606017 - EPA 3005A - Continued
Post Spike (1G06017-PS1)
Source:CE10039-37
Analrtte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
2.08
0.185
0.0181
64.7
0.199
0.182
9.68
0.195
0.191
24.8
0.186
16.2
0.203
Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 10:45
Spike Source %REC
Elan EQL Units Level BOO %REC Limits
0.100 mg/L 2,00 0.0563 101 80-120
0.0100 mg/L 0.200 2.75E5 93 80-120
0.00100 mg/L 0,0200 -0.000325 90 80-120
0.100 mg/L 2.00 63.5 56 80-120
0.0100 mg/L 0.200 0.00235 98 80-120
0.0100 mg/L 0.200 -0.00117 91 80-120
0.100 mg/L 2.00 7.95 86 80-120
0.0100 mg/L 0.200 0.0107 92 80-120
0.0100 mg/L 0.200 0.00244 94 80-120
0.500 mg/L 10.0 14.6 102 80-120
0.0100 mg/L 0.200 -0.00210 93 80-120
0.500 mg/L 10.0 6.09 102 80-120
0.0100 mg/L 0.200 0.0102 96 80-120
Classical Chemistry Parameters - Quality Control
Batch 1606017 - EPA 3005A
RPD
RPD Limit l
QM-0B
Blank (1G06017-BLK1)
Prepared: 07/06/2021 14:18 Analyzed: 07/08/2021 15:50
Analvte
Sodium Adsorption Ratio
Batch 1607013 - NO PREP
Result Etas
0.00 U
PQL Units
[blank]
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD Limit Notes.
Blank (1607013-BLK1)
Prepared & Analyzed: 07/07/2021 15:04
1
Analvte
Biochemical Oxygen Demand
Result flag P01.
2,0
u
2.0
Units
mg/L
Spike Source
Level EMAIL
%REC
%REC Limits
RPD
RPD Limit lyres.
LCS(1G07013-BS1)
Analyte
Biochemical Oxygen Demand
Duplicate (1G07013-DUP1)
Source: CE08078-01
AoalYke
Biochemical Oxygen Demand
Batch 16070.20 - NO PREP
Result EIRO
170
Prepared & Analyzed: 07/07/2021 15:04
Spike
LOL Units Level
2.0
mg/L
198
Source
Result
%REC
87
%REC
Limits
85-115
Prepared & Analyzed: 07/07/2021 15:04
Spike Source
Result Hag POI Units Level Result %REC Limits
18 2.0 mg/L 18
%REC
1
RPD
RPD Limit lyotes-
RPD
2
1
RPD
Limit 1Votes
30
[Blank (1607020-BLK1)
Prepared: 07/07/2021 15:41 Analyzed: 07/07/2021 17:15
Analvte
Nitrite as N
Result Elan P(L
Spike Source
Uolts Level lresulh %REC
0.017 U 0.10 mg/L
%REC
Limits
RPD
RPD Limit NGtei
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1G07020 - NO PREP - Continued
LCS(1807020-BS1)
Prepared: 07/07/2021 15:41 Analyzed: 07/07/2021 17:34
Analvte
Nitrite as N
ftsult Elan PAX Units
1.1
0.10
mg/L
Spike Source
Level ges� tii
1.00
%REC
%REC Lirni RPD
106
90-110
RPD
emit ROIL
Matrix Spike (1G07020-MS1)
Prepared: 07/07/2021 15:41 Analyzed: 07/07/2021 18:14
1
Source: CE08078-01
ADaltds
Nitrite as N
Result
2.3
Plan
D
POI Units
mg/L
0.50
Spike
Level
1.00
Source
Result
1,3
%REG
%REC Limit¢ RPD
105 90-110
RPD
"mi
Notes
Matrix Spike Dup (1607020-MSD1)
Prepared: 07/07/2021 15:41 Analyzed: 07/07/2021 18:15
1
Source: CE08078-01
Analvte
Nitrite as N
Batch 1G09007 - NO PREP
Result
2.3
Pt� p
D 0.50
Spike
Units Level
mg/L 1.00
Source
Result
1.3
%REC
%REC MBAs RPD
105 90-110 0.2 10
RPD
Notes
Blank (1G09007-BLK1)
Prepared & Analyzed: 07/13/2021 21:00
Analvte
Total Suspended Solids
Resmit El�q
Z.5 U
PQL Units
2.5 mg/L
Spike Source
Level Result
%REG
%REC Limits RPD
RPD
Limit
[LCS(1G09007-BS1)
Analvte
Total Suspended Solids
Prepared & Analyzed: 07/13/2021 21:00
Duplicate (1G09007-DUP1)
Source: CE08251-01
Analvte
Total Suspended Solids
Duplicate (1G09007-DUP2)
Result Flan
110
POI Units
2.5 mg/L
Result Flan PDL
2000
120
Units
mg/L
Spike
Level
100
Source
Result
%REG
%REC Limits RPD
112
80-120
Prepared & Analyzed: 07/13/2021 21:00
Spike
Level
Source
Result
740
%REC
%REC LLmitl RPD
Prepared & Analyzed: 07/13/2021 21:00
91
RPD
<Smit
RPD
Limit
20
ti
1
Notes
QM-12
Source: CE08266-01
-Analvte
Total Suspended Solids
Batch 1G09009 - NO PREP
Spike
Result fIM ED4 Units Level
20
5.8 mg/L
Source
)result
18
%REC
%REC Limits RPD
10
RPD
Unlit Lr4#BP
20
Blank (1G09009-BLK1)
Prepared: 07/09/2021 10:06 Analyzed: 07/09/2021 13:04
.Anahrte
Chemical Oxygen Demand
Result Nan PAX
10 U
10
Units
mg/L
Spike
Level
BOO
Source
%REC
WuREC Limits RPD
RPD
Limit
LCS (1809009-BS1)
Malvte
Chemical Oxygen Demand
Prepared: 07/09/2021 10:06 Analyzed: 07/09/2021 13:04
Result Flan PQl Units
510
10 mg/L
Spike
Level
500
Source
Emit
%REC
%REC Limits RPD
103 90-110
RPD
Limit Notes.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in fult.
Page 8 of 13

www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch.1G09009 - NO PREP - Continued
114atrlx Spike (1G09009-MSJ.)
Prepared: 07/09/2021 10:06 Analyzed: 07/09/2021 13:04
Source:CE0D737-01
Ambits
Chemical Oxygen Demand
Spike Source
Result Bag P01. Units Level Result
370
970
10
mg/L
S26
%REC RPD
%REC Limits RPD Lim+�t
113
90-110
Notes
QM-07
Matrix Spike Dup (1G09009-MSD1)
Prepared: 07/09/2021 10:06 Analyzed: 07/09/2021 13:04
Source: CE00737-01
na
Chemical Oxygen Demand
Batch 1G09018 - Same
Spike Source %REC RPD
Result Flan PAL Units Level Ballo %REC Limits RPD Limit Notes
900 10 mg/L 526 370 100 90-110 8 5 QM-11
[Black (1609018-BLK1)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 16:59
1
Analvte
Total Kjeldahl Nitrogen
LCS(1G09018-BS1)
Result
0.26
Elan
u
Spike
PQL Units Level
0.48
mg/L
Source
Result %REC RPD irri
%REC
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 17:01
RPD
Analvte
Total Kjeldahl Nitrogen
Spike
Result Elan PQL Una Level
12
0.48
mg/L
12.0
Source
Result
%REC
9/aREC Limits
103
90-110
RPD
RPD Limit l
[Matrix Spike (1G09018-M51)
Source:CE08078-01
Analvte
Total Kjeldahl Nitrogen
Result flas P0L
13
0.48
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 17:05
Spike
Units Level
mg/L
4.80
Source
Result
7.7
%REC
%REC Limits:
106
90-110
RPD
RPD Limit
1
Matrix Spike (1G09018-M52)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 17:10
Source:CE09273-01
Analvte
Total Kjeldahl Nitrogen
Result Flan PQL Units
7.7
0.48
mg/L
Spike
Level
4.80
Source
Rend
2.8
%REC
%REC Limps
102
90-110
RPD
RPD Ljn1t
Notes_
Matrix Spike Dup (1G09018-MSD1)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 17:06
1
Source: CE08078-01
Analvte
Total Kjeldahl Nitrogen
Batch 2G09020 - Same
Spike Source
Result flan PQL Units Level Result
12 0.48 mg/L 4.80 7.7
%REC
%REC Limits
94 90-110
RPD
RPD Limit MAL
5 10
Blank (1G09020-BLK1)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 18:15
1
.Amide
Phosphorus
$e tlC fee
0.025 U
Spike
PQL knits Level
0.10
mg/L
Source
EMIR
%REC
%REC Limits RPD
RPD
Unlit
LCS(1G09020-BS1)
Analvte
Phosphorus
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 18:17
Spike
Result Ban PQL Units Level
1.6 0.10 mg/L 1.60
Source
1395&
%REC RPD
%REC Limits RPD Ljplit i
100 80-120
FINAL This report relates only to the sample es received by the laboratory, and may only be reproduced in full.
Rage 9of13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1609020 - Same - Continued
',Matrix Spike (1G09020-M51)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 18:19
Source: CE08078-01
Analvte
Phosphorus
Result Flag
3.7 0
P-QL
0.50
Units
mg/L
Spike Source %REC RPD
Level Result %REC Limas RPD Limit
0.640 2.9
122
80-120
dote;
QM-07
Matrix Spike Dup (1609020-MSD1)
Prepared: 07/09/2021 11:55 Analyzed: 07/12/2021 18:21
Source: CE08078-01
Analvte
Phosphorus
Batch 1G09022 - NO PREP
Spike Source %REC RPD
Result Plan PAL. Units Level gum t %REC Limits RPD imp 1191$s
3.8 D 0,50 mg/L 0.640 2.9 129 80-120 1 25 QM-07
(Blank (1609022-BLK1)
Prepared: 07/09/2021 10:39 Analyzed: 07/09/2021 I3:43
1
Analy�
Nitrate/Nitrite as N
LCS (1G09022-BS1)
Analvte
Nitrate/Nitrite as N
Result Flan PQL
0.041 U
0.10
Spike Source
Units Level gar
mg/L
%REC RPD
%REC Limits RPD Limit Notes
Prepared: 07/09/2021 10:39 Analyzed: 07/09/2021 13:45
Spike Source %REC RPD
Result Flan P91 Units Level Emit %REC mmtk RPD Limit MIZE-
1.2
0.10
mg/L
1.25
94
90-110
Matrix Spike (1G09022-M51)
Prepared: 07/09/2021 10:39 Analyzed: 07/09/2021 13:48
1
Source: CE09592-01
Analvte
Nitrate/Nitrite as N
Result ERR P01. Units
1.7
0.10
mg/L
Spike
Level
0.521
Source
Result
1.3
%REC
%REC Limits
84
90-110
RPD
RPD Limit
QM-07
Matrix Spike (1G09022-MS2)
Prepared: 07/09/2021 10:39 Analyzed: 07/09/2021 14:20
1
Source: CE09594-01
Apah to
Nitrate/Nitrite as N
Spike Source %REC
Result Fin NIL Units Level Emit %REC Limits
65 5.0 mg/L 25.0 37 115 90-110
RPD
RPD Limit
Notes
QM-07
[ Matrix Spike Dup (1G09022-M5131)
Source: CE09592-01
Analvte
Nitrate/Nitrite as N
Batch 1G12013 - NO PREP
all
Prepared: 07/09/2021 10:39 Analyzed: 07/09/2021 13:50
1
Spike Source %REC RPD
Result Flag POI Units Level Ream %REC Limits RPD Unit Notes
1.9 0.10 mg/L 0.521 1,3 109 90-110 7 10
Blank (1G12013-BLK1)
Prepared: 07/12/2021 10:08 Analyzed: 07/12/2021 12:38
1
Analvte
Ammonia as N
Result Elan
u
0.045
Spike Source
P-QI. UJnita Level Result %REC 4lmits RPD
0.10
mg/L
%REC
RPD
Limit
Notes
LcS(1G12013-BS1)
Prepared: 07/12/2021 10:08 Analyzed: 07/12/2021 12:40
1
Analvte
Ammonia as N
Spike Source
Result Flag P_OL !bits Level Result
1.0 0.10 mg/L 1.01
%REC
%REC Limit
99 90-110
RPD
RPD Limit Notes_
FINAL This report relates only to the sampe as received by the laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
'Jessica! Chemistry Parameters - Quality Control
Batch 1G12Oi3 - NO PREP - Continued
Matrix Spike (1612013-MS1)
ti
Prepared: 07/12/2021 10:08 Analyzed: 07/12/2021 12:43
Source: CE09592-01
Analvte
Ammonia as N
Spike
Result Elan P01. Units Level
0.33
0.10
mg/L
0.393
Source
Result
0.045 U
%REC
84
%REC
61miS& RPD
90-110
RPD
Liea1S Notes
QM-07
[Matrix Spike OG12013-1452)
Source: CE09594-01
Analvte
Ammonia as N
Prepared: 07/12/2021 10:08 Analyzed: 07/12/2021 12:52
Result EBB
0.36
POL Units
mg/L
0.10
Spike
Level
0.393
Source
Resltlt
0.045 U
%REC
92
%REC
Li its RPD
90-110
RPD
3.imlt
f
Notes
[Matrix Spike Dup (1G12013-MSD1)
Source:C[09592-01
An Jyte
Ammonia as N
Batch 1G12046 - NO PREP
Prepared: 07/12/2021 10:08 Analyzed: 07/12/2021 12:45
1
Reams Hag P9.i
Source
Result
0.31 0.10 mg/L 0.393 0.045 U
Spike
nits Level
%REC
%REC Lirpits RPD
B0 90-110 6
RPD
Limit
10
QM-07
[Blank (1G12046-BLK1)
Prepared & Analyzed: 07/12/2021 18:30
Analvte
Total Solids
Result Elan
U
0.0050
Spike Source
POL Unita Level Result %REC Limits RPD
0.0050 % by Volume
%REC
RPD
Limit Notes
LCS(1G12046-6S1)
Prepared & Analyzed: 07/12/2021 18:30
Artakte
Total Solids
Result File
1100
ILQL
50
Spike
Units Level
mg/L
1100
Source
Result
%REC
%REC Limits RPD
100
90-110
RPD
Limit
Duplicate (1G12046-DUP1)
Prepared & Analyzed: 07/12/2021 18:30
Source: CE03416-01
Analvte
Total Solids
Result Flag
0.24
Spike
P41 Ulm Level
0.0050 % by Volume
Source
Result
0.24
%REG
%REC Limits
RPD
1
RPD
Limit Notes
5
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 Central Pon Or 4810 0xeculno Park Court, Suits, 111
Orlando. FL 32824 JarksonvMe.FL 32216.6009
{407)826-5314 19041225-3007 Fix190412984210
:Rent Name
Novozymee North America (N0008)
77 Perry Chapel Church Road
Promo! Number
[novel
Protect Name. oe1C
Monthly - week One- SBM
lay ST 2p
Frenkilnthn, NC 27525
PO a r B4kn9lnfo
3700044905
Tel
494-3000
Fax
Reporting
Cr eCh
Semp(erlai Name. A1(iRallan tPnnti Bea
^Contact
a tots Payable
Tokt Cc Ji 4 YeAc..'
Sampler S.gnatur S raLoralronlTime
F � krr;f417E:054
Item a
C:t9, 1
Sample ID Wield alenitlw 1l onl Collection Dale Tane C)mp / Desb
SBM ?—G?( 60:30 c„ Lb
Mains
(see tame)
Total a of
Containers
7
x x
102 A Woodwnndaindustrial CI
Cary. NC 27511
jB19►487.3090 Fax[phone]
Page — Of
Arse gee
BOD SM521OB
COD SM5220D
1
TSS SM2S40D
8
1
r-
i
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Prsaarvalivn 'See Codee)1Corndne ea necesaaryt
x
x
x
x
x
H814885180 iurnarouno
Times
Note Rush requ0SlS sublecl id
acceptance by the 1aCIi e
Standard
Expedited
Due,1
Lab Workorder
CE08079
Sample Comments
Sample Ka Prepared By
Cornmenta)Speclal Reportlnla Reg
r+irr�as
Dawnin.
(a PO EI
Rehnqurehed By
JC4".'
Re4 nqulshed By
<-- Total tt of Containers
Datsrl�me
?-G .7l oc,:c
Daleatme
Received 8y
Ae$nqurrhed By
Coder a-s 8 Temps on RecaIpl
Date+Tme
Received By
Matrix SW -Groundwater SO-SoilPW-Orinkm0 Water SE-Sedunent SW -Surface We1sr WW-Wasler,ater A•Asr O-Other tda4N In comments) Preservation. 1-Ice H41CI N-rllvcTa a n�su.
Note All samples submitted to ENCO Lacs .rro at eueordenCe with the reins and conditions lasted on the reverse of this burn. urgent 'Inca ashen agmemanls ens(
Da(errxne
7pee
7d'- 54)
Delerrlma
Dalsrrlms
Condition U ocelot
Acceptable Unacceptable
...,,,._. „ ... e.,..,ti.ri1i1

Sample Preservation Verification
ENCD Cary
Work Order CE08079
Client Novozymes North America (N0008)
Logged In 06-Jul-21 10:26
Preservation Check Performed By:
Project: Monthly - Week One - SBM
Protect #: [none]
Logged By: Samantha ~J
L yatt
Date/Time: 1 �j
�. [ 1030
CE08079-01
Cant
0
Type
250mLP+H2SO4
E 250mLP+HNO3
Pres (pH)
Requirement
<2
<2
pH Checked /
n Control
/ N / NA
Yi N / NA
pH Adjusted
Cme Reagent Used/Comments
Ad
Adjustusted
-�c2 Nzs -
Y1 N 7 Z t-3'JL)3
Y / N 1 NA � \ 21 lU3J
Rea en am t Name ID Reagent Name ID Reagent Name ID
1
2
pH Strip ID:
C ►�
Csss-
3 5
4 6
C:lelmnt\Printlwko_PreservationCheck. rpt
Page 1 of 1

rtiit ENCO Laboratories
A ccu ra tea Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX; 919.467.3515
Thursday, August 19, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE10686
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, August 3, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates enly to the sample as received by the laboratory, and may only be reproduced in fuF. Page 1 of 13

SAMPLE SUMMARY/ LABORATORY CHRONICLE
Client ID: SBM Lab ID: CE10686-01
www.encolabs.com
Sampled: 08/03/21 07:40 Received: 08/03/21 09:00 I
Parameter Preparation Hold Date!Time(s1 Prep Date/Time(s) Anelvsis Date/Timefs)
CSU Method EPA 3005A 04/28/24 08/05/21 09:18 08/09/21 16:04
EPA 350.1 NO PREP 08/31/21 08/06/21 09:03 08/06/21 11:04
EPA 351.2 Same 08/31/21 08/10/21 11:38 08/12/21 11:50
EPA 353.2 NO PREP 08/05/21 07:40 08/03/21 15:15 08/03/21 18:14
EPA 353.2 [CALCj 08/05/21 07:40 08/09/21 15:08 08/10/21 14:01
EPA 353.2 NO PREP 08/31/21 08/09/21 15:08 08/10/21 14:01
EPA 365.4 Same 08/31/21 08/10/21 11:38 08/18/21 14:51
EPA 6010D EPA 3005A 01/30/22 08/05/21 09:18 08/09/21 13:50
EPA 7470A EPA 245.1 08/31/21 08/11/21 07:13 08/12/21 15:50
SM 25408-2011 NO PREP 08/10/21 08/10/21 19:00 08/10/21 19:00
SM 2540D-2011 NO PREP 08/10/21 08/10/21 18:41 08/10/21 18:41
SM 5210 8-2011 NO PREP 08/05/21 07:40 08/04/21 09:35 08/04/21 09:35
SM 52200-2011 Same 08/31/21 08/03/21 14:41 08/03/21 17:20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 2 of 13

Client ID: SBM
Anal e
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Tota'
Chemical Oxygen Demand
Magnesium - Total
Molybdenum - Total
Nickel - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Phosphorus- Total
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
SAMPLE DETECTION SUMMARY
Lab ID: CE10686-01
FlaatE fkgM41
11.8 0.420
130 D 4.0
5300 2.0
2780 0.390
21000 800
11.2 0.290
0.0353 3 0.0250
0.0379 1 0.0220
11 0 2.0
11 D 2.0
0.53 0.017
180 D 2.5
576 1.50
353 4.00
1.83
860 D
2.6
5900
0.156
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rMA4 Method Notes
1.00 mg/L EPA 6010D
9.0 mg/L EPA 350.1
2.0 mg/L SM 5210 B-2011 B-07
1.00 mg/L EPA 6010D
800 mg/L SM 5220D-2011
1.00 mg/L EPA 6010D
0.100 mg/L EPA 6010D
0.100 mg/L EPA 6010D
4.8 mg/L EPA 353.2
4.8 mg/L EPA 353.2
0.10 rng/L EPA 353.2
10 mg/L EPA 365.4
5.00 mg/L EPA 60100
5.00 mg/L EPA 6010D
[blank] CSU Method
26 48 mg/L EPA 351,2
0.050 0.050 % by Volume SM 2540B-2011
250 250 mg/L SM 2540D-2011
0.0440 0.100 mg/L EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 3 of 13

-11
ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID:CE10686-01
Sampled:08/03/21 07:40
Sampled By:Adam Fauccette
www.encolabs.00m
Received: 08/03/21 09:00
Work Order: CE10686
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certrred anaryte INC 591]
jlnalyte [CAS Numberl
Mercury [7439-97-6r
Results Bag Units 2E M]2L EQL ]latch
0.000750 U mg/L
5 0.000750 0.00100 1H11002
M& had
EPA 7470A
Ana w& 0Y BORE
08/12/21 15:50 RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO CaryiwDfiad afl*1e /NC 591]
Analvte [CAS Numberl
Aluminum [7429-90-5]^
Arsenic[7440-38-2]^
Cadmium [7440-43-9]^
Calcium [7440-70-2]^
Copper[7440-50-8}^
Lead [7439-92-1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel [7440-02-0j^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-53^
Zinc [7440-66-6]^
Resul[5 Fps Units a MI NI Datch Method MAMMA�][
11.8 mg/L 10 0.420 1.00 1H05012 EPA 6010D 08/09/21 13:50 ]DH
0.0760 U mg/L 10 0.0760 0.100 1H05012 EPA 6010D 08/09/21 13:50 JDH
0.00360 U mg/L 10 0.00360 0.0100 1H05012 EPA 6010D 08/09/21 13:50 3DH
2780 mg/L 10 0.390 1.00 1H05012 EPA 6010D 08/09/21 13:50 3011
0.0160 U mg/L 10 0.0160 0.100 1H05012 EPA 6010D 08/09/21 13:50 JDH
0.0310 U mg/L 10 0.0310 0.100 1H05012 EPA 6010D 08/09/21 13:50 3DH
11.2 mg/L 10 0.290 1.00 1H05012 EPA 60100 08/09/21 13:50 3DH
0.0353 3 mg/L 10 0.0250 0.100 1H05012 EPA 60100 08/09/21 13:50 3DH
0.0379 3 mg/L 10 0.0220 0.100 1H05012 EPA 6010D 08/09/21 13:50 3DH
576 mg/L 10 1.50 5.00 1H05012 EPA6010D 08/09/2113:50 3DH
0.0620 U mg/L 10 0.0620 0.100 1H05012 EPA 6010D 08/09/21 13:50 3DH
353 mg/L 10 4.00 5.00 1H05012 EPA 6010D 08/09/21 13:50 3D11
0.156 mg/1 10 0.0440 0.100 1H05012 EPA 6010D 08/09/21 13:50 3DH
Classical Chemistry Parameters
- ENC° Cary certified anatyte INC 591 j
Anahrte [CAS Number
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand^
Chemical Oxygen Demand^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Total Suspended Solids^
gesult5 €igg lets E ]1Q]. EQI. MAIO Method Analyzed 83
130 0 mg/L 90 4.0 9.0 1H06007 EPA 350.1 08/06/21 11:04 JAH
5300 m9/L 1 2.0 2.0 1H04010 SM 5210 B-2011 08/04/21 09:35 30C 8-07
21000 mg/L 80 800 800 1H03026 SM 5220D-2011 08/03/21 17:20 JOC
11 D mg/L 48 2.0 4.8 [CALC} EPA 353.2 08/10/21 14:01 JAH
11 D mg/L 48 2,0 4.8 11109034 EPA 353.2 08/I0/21 14:01 3A11
0.53 mg/L 1 0.017 0.10 1H03037 EPA 353.2 08/03/21 18:14 JAH
180 D mg/L 100 2,5 10 1H10022 EPA 365.4 08/18/21 14:51 3A1-I
1.83 [blank] 1 1H05012 cSU Method 08/09/21 16:04 JDH
860 0 mg/L 100 26 48 1H10021 EPA 351.2 08/12/21 11:50 JAH
2.6 % by Volume 10 0.050 0.050 1H10046 514 25408-2011 08/10/21 19:00 DM)
5900 mg/L 100 250 250 1H06015 SM 25400-2011 08/10/21 18:41 DM3
Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
1
Metals by EPA 6000/7000 Series Methods - Quality Control
1
Batch 11111002 - EPA 245.1
[Blank (1H11002-BLK1)
Prepared: 08/11/2021 07:13 Analyzed: 08/12/2021 15:22
Analvte
Mercury
Result Flan P01.
0.000150 U 0.000200
Spike Source
Units Level Result
mg/L
%REC RPD
%REC Limits RPD Limit Notes
LCS (1H11002-BS1)
Prepared: 08/11/2021 07:13 Analyzed: 08/12/2021 15:24
Analvte
Mercury
Result Etas P_01. Units
0.00540 0.000200
mg/L
Spike Source %REC
Level Result %REC L;.B115s
0.00500
108
80-120
RPD
RPD Lfmlt
[Matrix Spike (1H11002-M51)
Source:CE10387-03
Analvte
Mercury
Prepared: 08/11/2021 07:13 Analyzed: 08/12/2021 15; 26
1
Result Bag
13.00520 0.000200
Units
mg/L
Spike Source
Level Result %REC
0.00500 0.00015011 104
%REG
Limits RPD Limit
75-125
RPD
Notes
Matrix Spike Dup (1H11002-MSD1)
Source: CE10387-03
Analvte
Mercury
Result Fiats PQL
0.00531 0.000200
Units
mg/L
Prepared: 08/11/2021 07:13 Analyzed: 08/12/2021 15:28
Spike
Level
0.00500
Source
Result
0.000150 U
%REC
%REC Limits
75-125
106
RPD
RPD mi
2
25
1
Notes
Post Spike (1H11002-PS1)
Source: CE10387-03
Analvte
Mercury
Result Elen
5.39
0.200
.E0L Units
ug/L
Prepared: 08/11/2021 07:13 Analyzed: 08/12/2021 15:30
Spike
Level
4.76
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 11105012 - EPA 3005A
Source
Result
-0.00267
1
%REC RPD
%REC Limits RPD VpA Notes
113
75-125
Blank (1H05012-BLK1)
Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 13:24
1
_ tnallde
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Rip ylt Flan P.41 Units Level
0.0420 11 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0,00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0,0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 11 0.0100 mg/L
%REC
Result %REC
RPD
RPD Limit
I LCS (1H05012-SS1) Prepared: 08/05/202109:18 Analyzed: 08/09/2021 13:29
Notes
1
Analvte
Aluminum
Arsenic
FINAL
Spike
Result Eau POI &Mils Level
2.17 0,100 mg/L 2.00
0.208 0.0100 mg/L 0.200
Source
Result
%REC
%REC Limits
109 80-120
104 80-120
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD l MA
Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1H05012 - EPA 3005A - Continued
LCS (11105012-B51) Continued
Analy�
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 13:29
Spike
Result Etas .EQL Units Level
0.0206 0.00100 mg/L 0.0200
2.27 0.100 mg/L 2.00
0.201 0.0100 mg/L 0.200
0.206 0.0100 mg/L 0.200
2.18 0.100 mg/L 2.00
0.202 0.0100 mg/L 0.200
0.213 0.0100 mg/L 0.200
10.7 0.500 mg/L 10.0
0.211 0.0100 mg/L 0.200
10.8 0.500 mg/L 10.0
0.213 0.0100 mg/L 0.200
Matrix Spike (1H05012-MS1)
Source: CE09197-01
ARAM?
Aluminum
Arsenic
Cadmium
Calcium
Copler
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Source
Result
%REC
%REC Limits
103 80-120
114
10i
103
109
101
107
107
105
108
107
80-120
80-120
80-120
80-120
80.120
80-120
80-120
80-120
80-120
80-120
RPD
RPD !Jmit Mkt.
Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 13:32
Spike
Result Flag P01 Units Level
2.21 0.100 mg/L 2.00
0.206 0.0100 mg/L 0.200
0.0209 0.00100 mg/L 0.0200
2.57 0.100 mg/L 2.00
0.221 0.0100 mg/L 0.200
0.211 0.0100 mg/L 0.200
2.35 0.100 mg/L 2.00
0.204 0.0100 mg/L 0.200
0.216 0.0100 mg/L 0.200
11.4 0.500 mg/L 10.0
0.209 0.0100 mg/L 0.200
16.8 0.500 mg/L 10.0
0.229 0.0100 mg/L 0.200
Source
Basalt
0.0862
0.00760 U
0.000360 U
0.0850
0.00160 U
0.00310 U
0.242
0.00250 U
0.00220 U
0.869
0.00620 U
6.33
0.00440 U
%REC
%REC L
106 75-125
103 75-125
104 75-125
124 75-125
111 75-125
106 75-125
105 75-125
102 75-125
108 75-125
105 75-125
104 75-125
105 75-125
115 75-125
RPD
RPD mi Notes
Matrix Spike Dup (1H05012-MSD1) Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 13:40
Source: CE09197-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Z.nt
Spike Source %REC RPD
Result flag P91 Units Level Result %REC Limits RPD U7mit l
2.26 0.100 mg/L 2.00 0.0862 109 75-125 2 20
0.199 0.0100 mg/L 0,200 0.00760 U 100 75-125 4 20
0.0202 0.00100 mg/L 0.0200 0.000360 U 101 75-125 3 20
2,32 0.100 mg/L 2.00 0,0850 112 75-125 10 20
0.202 0,0100 mg/L 0.200 0.00160 U 101 75-125 9 20
0.201 0.0100 mg/L 0.200 0.003I0 U 100 75-125 5 20
2.39 0.100 mg/L 2.00 0,242 107 75-125 2 20
0.196 0,0100 mg/L 0.200 0.00250 U 98 75-125 4 20
0.209 0.0100 mg/L 0.200 0.00220 U 104 75-125 3 20
11.4 0.500 mg/L 10.0 0.869 105 75-125 0.1 20
0.201 0.0100 mg/L 0.200 0.00620 U 101 75-125 4 20
15.8 0.500 mg/L 10.0 6.33 104 75-125 0.3 20
0.206 0.0100 mg/L 0.200 0.00440 U 103 75-125 11 20
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1H05011- EPA 3005A - Continued
[Post Spike (1H05012-PS1)
Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 13:43
1
Source: CE09197-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copier
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Rew t
2.19
0.209
0.0209
2.29
0.202
0.207
2.35
0.203
0.216
11.6
0.211
17.0
0.217
Han P_41.
0.100
0.0100
0.110100
0.100
0.0100
0.0100
0.100
0.0100
0.0100
0,500
0.0100
0,500
0.0100
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0,200
0.0200
2.00
0.200
0.200
2.00
0,200
0.200
10.0
0.200
10.0
0,200
Source
Result
0.0862
0.00270
-1.15E-5
0.0850
-8.86E-5
-0.00212
0.242
5.82E-5
0.000238
0.869
0,0009132
6.33
0.000293
%REC
%REC limits RPD
105 80-120
103 80-120
104 80-120
110 80-120
101 80-120
103 80-120
105 80-120
101 B0-120
108 80-120
107 80-120
105 80-120
107 80-120
108 80-120
RPD
Limit
Notes
Classical Chemistry Parameters - Quality Control
Batch 11103026 - Same
1
Blank (1H03026-BLK1)
Prepared: 08/03/2021 14:41 Analyzed: 08/03/2021 17:20
1
Anal
Chemical Oxygen Demand
Result Flan
10
POL Units
10 mg/L
Spike Source
Level Rua
%REC
%REC Limas RPD
RPD
Limit
Notes
LCS(1H03026-BS1)
Prepared: 08/03/2021 14:41 Analyzed: 08/03/2021 17:20
-AnaIvte
Chemical Oxygen Demand
Result Elan PQL
500
10
Spike
!Data Level
mg/L 500
Source
13€ tit
%REC
%REC Limits RPD
99
90-110
RPD
Limit
Notes
Matrix Spike (1H03026-MS1)
Source: CE09808-01
Chemical Oxygen Demand
Prepared: 0B/03/2021
Spike
Result Elan PQL Units Level
620
10 mg/L
Source
BMA
526 140
14:41 Analyzed: 08/03/2021 17:20
%REC
alaREC Limits RPD
91 90-110
RPD
Limit
Matrix Spike Dup (1H03026-MSD1)
Source: CE09808-01
AMMO
Chemical Oxygen Demand
Batch 11103037 - NO PREP
Result Elsa
630
Prepared: 08/03/2021 14:41 Analyzed: 08/03/2021 17:20
m m M =
P_Q.L Units
10 mg/L
Spike Source
Level Result
526 140
%REC
93
%REC
limits RPD
90-110 2
RPD
limit lY2igL
5
[Blank (1H03037-BLIC1)
Prepared: 08/03/2021 15:15 Analyzed: 08/03/2021 17:58
Anahrte
Nitrite as N
Result Elan
0.017 U
P9l Units
mg/L
0.10
Spike Source
Level gesult
%REC
%REC Limits RPD
RPD
LLmI+ Notes
ILCS(1H03037-BS1)
Prepared: 08/03/2021 15:15 Analyzed: 08/03/2021 18:34
Spike Source
Result Dan EQL !BILLS Level Result
%REC
%REC Limits RPD
RPD
Limit Notes.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 11103037 - NO PREP - Continued
LCS (11103037-BS1) Continued
Prepared: 08/03/2021 15:15 Analyzed: 0B/03/2021 18:34
Y
Analvte
Nitrite as N
Result Flan
1.0
POL Un�s
mg/L
0.10
Spike
Level
1.00
Source
Result
%REC
%REC Limits RPD i i Notes
105
90-110
RPD
Matrix Spike (11103037-MS1)
Prepared: 08/03/2021 15:15 Analyzed: 08/03/2021 18:02
Source:CE09197-01
Anah to
Nitrite as N
Result !IPA
0.98
POL Units
mg/L
0.10
Spike
Level
1,00
Source
Result
0.017 U
%REC
%REC Umits RPD
98
90-110
RPD
Notes
[Matrix Spike (1H03037-M52)
Source: CE09197-02
Analvte
Nitrite as N
Prepared: 08/03/2021 15:15 Analyzed: 08/03/2021 18:05
■
Result Flan PAL
0.86
0.10
nits
mg/L
Spike Source
Level gegg&
0.017 U
1.00
%REC RPD
%REC Limits RPD Limit NQLSS.,
86
90-110
QM-07
Matrix Spike Dup (1H03037-MSD1)
Prepared: 08/03/2021 15:15 Analyzed: 08/03/2021 18:03
■
Source: CE09197-01
Analvte
Nitrite as N
Batch 11104010 - NO PREP
Spike Source
Result Elan P0L Units Level Result
0.99 0.10 mg/L 1.00 0.017 U
%REC
%REC Limits RPD
RPD
rit Now
99 90-110 0.3 10
Blank (1H04010-BLK1)
Prepared S. Analyzed: 08/04/2021 09:35
Analvte
Biochemica! Oxygen Demand
Result Ban P41
2.0
U
2.0
Units
mg/L
Spike
Level
Source
Result
%REC
%REC Limits
RPD
RPD Limit 1'[' nnCs
LCS(11104010-BS1)
Prepared & Analyzed: 08/04/2021 09:35
.Analvte
Biochemical Oxygen Demand
Result Hag
150
Spike Source
P_Q.L Units Level Result
2.0 mg/L
198
%REG
78
%REC RPD
Limits RPD Limit
85-115
Notes
B-07
Duplicate (1H04010-DUP1)
Prepared & Analyzed: OB/04/2021 09:35
Source: CE06408-01
AnaMe
Biochemical Oxygen Demand
Batch 1H05012 - EPA 3005A
Spike Source
Result Elan PM- Units Level Result
2.0 U 2.0 mg/L 2.0 U
%REC RPD
%REC Limits RPD Limit Noses.,
30 8-07
Blank (1H05012-BLK1)
Prepared: 08/05/2021 09:18 Analyzed: 08/09/2021 16:08
Analvtr
Sodium Adsorption Ratio
Batch 11106007 - NO PREP
Result Elms Pot. Units
0.00 U [blank]
Spike Source
Level Rs M1t
%REC RPD
%REC Limits RPD Llnlit .
[Blank (1H06007-BLK1)
Prepared: 08/06/2021 09:03 Analyzed: 08/06/2021 10:49
Analvte
Ammonia as N
Spike Source
Result Plan P_0.L Units Level Rest ltt %REC Limitp RPD Limit Notes
0.045 U 0.10 mg/L
%REC
RPD
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In lull.
Page 8ef13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 11106007 - NO PREP - Continued
1.CS(1H06007-BS1)
Prepared: 08/06/2021 09:03 Analyzed: 08/06/2021 10:50
Analvte
Ammonia as N
Result
1.0
Spike Source
Flan PQL Units Level Result
1.01
0.10
mg/L
%REC
%REC Limns
103
90-110
RPD
RPD I €mit Natal_
Matrix Spike (1H06007-MS1)
Prepared: 08/06/2021 09:03 Analyzed: 08/06/2021 10:54
1
Source: CE11030-01
Analvte
Ammonia as N
Matrix Spike (11106007-MS2)
Source: CE11032-01
Analvte
Ammonia as N
Result flag
0.90
P_Q.L Units
mg/L
0.10
Spike
Level
0.393
Source
Result
0.058
%REC
86
%REC
limits
90-110
RPD
RPD tit
Prepared: 08/06/2021 09:03 Analyzed: 08/06/2021 10:59
Spike
Result .Flag PS)L Units Level
0.36
0.10
mg/L
0.393
Source
Result
0.045 U
%REC
91
%REC RPD
Limits RPD Limit
90-110
Hates
QM-07
Matrix Spike Dup (1H06007-MSD1)
Prepared: 08/06/2021 09:03 Analyzed: 08/06/2021 10:56
Source: CE11030-01
AnahaP
Ammonia as N
Batch 1H06015 - NO PREP
Spike Source %REC RPD
Result Flan PQL Units Level Result %REC Limits RPD Limit 1
0.39 0,10 mg/L 0.393 0.058 84 90-110 3 10 QM-07
[Blank (1H06015-BLK1)
Prepared &Analyzed: 08/10/2021 18:41
Amble
Total Suspended Solids
Raw& flag
2.5 U
Spike
PQL Units Level
2.5
mg/L
Source
Result
%REC RPD
%REC Limits RPD Limit Notes
I.LCS(1H06015-851)
A__nahse
Tolal Suspended Solids
Result Elan
100
2.5
Units
mg/L
Prepared & Analyzed: 08/10/2021 1B:41
Spike
Level
100
Source
%REC RPD
%REC Umits RPD Limit Mu_
103
80-120
Duplicate (1H06015-DUP1)
Prepared & Analyzed: 08/10/2021 18:91
Source: CE06253-01
Analvte
Total Suspended Solids
Spike
Result Elan EQL Units Level
540
100
mg/L
Source
670
%REC
%REC Limits
RPD
RPD Limit Notes
20 20
Duplicate (11106015-DUP2)
Prepared & Analyzed: 0B/10/2021 18:41
Source: CE10900-01
.Anal
Total Suspended Solids
Batch 1H09034 - NO PREP
Spike Source
Result Elae PQL Vnita Level Result
29 12 mg/L 34
%REC
RPD
%REC Limli RPD Limit
14
20
Blank (1H09034-BLK1)
Prepared: 08/09/2021 15:08 Analyzed: 08/10/2021 13:32
1
nalvte
Nitrate/Nitrite as N
Spike Source
Result Flag P9.L Units Level Remit %REC Limits RPD Limit
0.041 U 0.10 mg/L
%REC
RPD
Nam
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch .H09034 - NO PREP - Continued
LCS (1H09034-BS1)
Analvte
Nitrate/Nitrite as N
Matrix Spike (1H09034-MS1)
Source: CE10192-01
Analvte
Nitrate/Nitrite as N
Matrix Spike (1H09034-MS2)
Source: CE10192-02
Ana
Nitrate/Nitrite as N
Matrix Spike Dup (1H09034-MSD1)
Source: CE10192-01
Analvte
Nitrate/Nitrite as N
Batch 1H10021 - Same
Prepared: 08/09/2021 15:08 Analyzed: 08/10/2021 13:33
Result Elan POL Units
1.3
0.10
mg/L
Result Flan PQL Units
1.5
Result Flag
7.2
Result
1.9
0.10
0.50
Spike Source
Level gg# ft
1.25
%REC
%REC Limits
105
90-110
RPD
RPD Limit l
Prepared: 08/09/2021 15:08 Analyzed: 08/10/2021 13:37
Spike
Level
mg/L 0.521
Source
Bead
0.83
%REC
%REC Llgak
129
90-110
RPD
Prepared: 08/09/2021 15:08 Analyzed: 08/10/2021 13:42
Spike
nits Level
mg/L
Has POL Units
0.10 mg/L
2.50
Source
Result
4,8
%REG
%REC lainjtg RPD
95
90-110
Prepared: 08/09/2021 15:08 Analyzed: 08/10/2021 13:39
Spike
Level
Source
Result
0,521 0.83
%REC
%REC Limits RPD
108 90-110 7
RPD
Unlit
RPD
Limit
RPD
Lim
10
QM-07
1
HEIM
Blank (1H10021-BLK1)
Prepared: 08/10/2021 11:38 Analyzed: 08/12/2021 11:27
1
Analvte
Total Kjeldahl Nitrogen
LCS(1H10021-BS1)
6nAhtte
Total Kjeldahl Nitrogen
I. Matrix Spike (1H10021-MS1)
Source: CE11040-01
Analvte
Total Kjeldahl Nitrogen
LMatxix Spike (1H10021-MS2)
Source: CE11039-01
•Aaahv
Total Kjeldahl Nitrogen
Matrix Spike Dup (1H10021-MSD1)
Source:CE11040-01
AI
Total Kjeldahl Nitrogen
Batch 1H10022 - Same
Result fieS
0.26 U
PQL Units
mg/L
0.48
Result lice QL
13
Result
5.5
0.48
Spike Source
Level Result
%REC
%REC Limas
RPD
RPD Lil1Lt
Prepared: 08/10/2021 11:38 Analyzed: 08/12/2021 11:29
Spike Source
Level Result
mg/L 12.0
%REC
%REC Limits
107
90-110
RPD
RPD grak i
Prepared: 08/10/2021 11:38 Analyzed: 08/12/2021 11:32
Spike
Han PQL knits Level
Result Elan
5.8
Resat flag
4.0
0.48
mg/L
Poi. Units
0.48 mg/L
POL v iln
0.48 mg/L
4.80
Source
BOMA
1.0
%REC
%REC Limits RPD
92
90-110
Prepared: 08/10/2021 11:38 Analyzed: 08/12/2021 11:38
Spike
Level
4.80
Source
Result
0.26 U
e/oREC
%REC Limits RPD
120
90-110
Prepared: 08/10/2021 11:38 Analyzed: 08/12/2021 11:34
Spike
Level
4.80
Source
Result
1.0
%REC
62
%REC
Limits RPD
90-110 30
RPD
Limit
1
Notes
RPD
Limit !-
QM-07
RPD
i milt
10
1
QM-07,
QM-11
FINAL
This report relates only to the sample as recelved by the laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
r
Batch 11110022 - Same - Continued
Blank (11.110022-BLK1)
Prepared: 08/10/2021 11:38 Analyzed: 08/18/2021 14:32
1
Atlal�s
Phosphorus
[LCS(1H10022_BS1)
Arayle
Phosphorus
Result flag
0.025 U
Spike Source
P01- Units Level Result %REC IimRs RPD
0.10 mg/L
Result Egg PQL
1.5
0.10
Units
mg/L
%REC
Prepared: 08/10/202111:38 Analyzed: 08/18/202114:34
Spike Source
Level Result
1.60
RPD
Limit
%REC RPD
%REC Limits RPD Mott
97
80-120
Matrix Spike (1H10022-MS1)
Prepared: 08/10/2021 11:38 Analyzed: 08/18/2021 14:39
Source: CE11040-01
Analvte
Phosphorus
Matrix Spike Dup (1H10022-MSD1)
Source:CEt1040-01
Analvte
Phosphorus
Batch 1H10046 - NO PREP
Result F_ laa l�l
0.59
0.10
Units
mg/L
Spike
Level
0.640
Source
Result
0.025 U
%REC
92
%REC RPD
Limits RPD Llnat
80-120
Prepared: 08/10/2021 11:38 Analyzed: 08/18/2021 14:40
Spike Source
Result flan POI Units Level Result
0.55 0.10 mg/L 0.640 0.025 U
%REC
%REC Limits RPD Limit
85 80-120 8 25
RPD
Blank (1H10046-BLK1)
Prepared & Analyzed: 08/10/2021 19:00
1
Analvte
Total Solids
[LCS (1H10046-BS1)
not
Total Solids
Duplicate (1H10046-DUP1)
Source: CE10685-01
Analvte
Total Solids
Spike Source
Result Elae E QL !!sits Level Result %REC Limits RPD lrmit totes
0.0050 U 0.0050 % by Volume
%REC
Prepared &Analyzed: 08/10/2021 19:00
Spike Source
Result Flag POI llniti Level Result
1100 50 mg/L 1100
Bes_ull flag
0.22
%REC
%REC timits RPD
99
90-110
Prepared & Analyzed: 08/10/2021 19:00
Spike
P01. Units Level
0.0050 % by Volume
Source
Rona
0.22
RPD
RPD
Um
%REC RPD
%REC kuntE RPD Limit Notes
0.4 5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
3 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
lE The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitatlon Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification'.
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALL] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-07 LCS exceeded control limits for this test. The test can not be repeated due to method constraints. The
result should be considered an estimated value.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 12of13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
ions Central Port Dr 4810 Executwe Path Court Surte 111
Organdy) FL 32624 Jacksortvgle. FL 32214.8089
14071828-5314 0)04)296.3007 F4x[904)296-8210
102•A Woodwinds rnduatnar Cr
Cary NC 27511
19191487.3090 Fixi319)467.3515
www.encolabs.com
Page _ of
Owl Name
Novtozymes North America (N0008)
?Roc( Number
[Mane]1
Requested Analyses
Requested Turnaround
Times
Note Rush requests subject [n
acceptance the fealty
_Standard
_ Expedited
a
Due-_���_
I
U
_
§
A01
BOD SM5210B
COD SM5220D
a
8
Nitrite a5 N 3532.TS S M2540H
TSS SM254OD
Address
77' Perry Chapel Church Road
Pineal NameDeec
Monthly - Week One - SBM
C4y75TZrp
Frankllntan, NC 27525
PO e l B 11.nq Info
3700044905i
Tel
[phone]
Fes
Reporting Canted
Scott Creech
Samplerls) Name. A .Icon (Knot)
i DA,- Ge
*
1341i Contact
CCo�u1Is Payable
Lab Workorder
CE 1 0686
Sarrrpfer -,
41 _
Site Location I Time Zone
MUD
Zl
T
pr..f5ee j IGomhrne as necessary)
-
Ism a
Sample ID (Freed Idenhfrcaiim)
I Collectron
Collection Dale ilme
Camp Grab
Meulx
Isee cycles)
Total II of
Containers
Sample Comments
S
SBM
3-L I.
O1"1)
8L
7
X
X
X
X
X
X
X
•
a
_
<-- Total if of Containers
Sample K4 Prepared By
Dere/Time
Retina
By
Dalefrnne
Recervad Byd
Dela/Tone
Comments Special Reporting Regtut enenfs
Rea unshed By
oratehrome
Received By
Dat6,Trms
Relinquished By
DstelTlme
ReceivedByOat.Time
Cooler N s 5 Tampa on Receipt. l `1 O
lJ
Condition upon ipt
_ cceptable Unacceptable
Matrix GW-Groundwater SD -San DWDrinkeng Water SE -sediment SW -Surface Wafer WW-Wasterreter A-Atr 0-01her (detail in comments) Preservatton: I.1ce H-NCI N-tiNO3 ts-Fi2SOa NQ•NaUH v-wrer
Note :All aamp[sa aubmiued to ENCO Labs are In accordance with Me terns and conditions holed on the (scene of this form• unless mar written egreemente exist

Sample Preservation Verification
ENCO Cary
Work Order CE10686 Project: Monthly - Week One - SBM
Client: Novozymes North America N0008) Project # [none]
Logged In 03-Aug-21 11:28 Logged By: Samantha L Hatt �r� f
t
Preservation Check Performed By. 1 ., Date/Time: 9 G.
CE10686-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
n Control
pH Adjusted Date/Time
+r.‘ Adjusted
Used/Comments
0
250mLP+H2SO4
<2
N / NA Yf N / NA
)i
I
1 tt t-)
.\ 1r�
1-{ V S 0
L/
E
250mLP+HNO3
<2
Y N 1 NA Y '! N / NA
* 7-Inn ( _
V `
1
2
Reagent Name
ID Reagent Name
pH Strip 10.
Coy
3
4
ID
5
6
Reagent Name ID
C:1ELM NTIP rintlwko_P reservationCh eck. rpt
Page 1 of

ENCO Laboratorws
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, September 30, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: (none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE11550
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, September 7, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as recemed by the laboratory, and may only be reproduced In full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CE11550-01
Sampled: 09/07/21 02:30 Received: 09/07/21 08:30
Parameter
CSO Method
EPA 350.1
EPA 351.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 7470A
SM 2540E-2011
SM 2540D-2011
SM 5210 B-2011
SM 5220D-2011
Preparation
EPA 3005A
NO PREP
Same
NO PREP
[CALC1
NO PREP
EPA 3005A
EPA 245.1
NO PREP
NO PREP
NO PREP
Same
Hold Date/Time(sl
06/02/24
10/05/21
10/05/21
09/09/21 02:30
09/09/21 02:30
10/05/21
03/06/22
10/05/21
09/14/21
09/14/21
09/09/21 02:30
10/05/21
Client ID: SBM Lab ID: CE11550-01RE1
parameter
EPA 365.4
Preparation
Same
Hold Date!Time(s1
10/05/21
prep Date/Time(s1 Analysis DatelTime(sl
09/08/21 12:49
09/13/21 16:00
09/16/21 12:23
09/08/21 14:56
09/13/21 09:04
09/13/21 09:04
09/08/21 12:49
09/14/21 07:37
09/14/21 16:32
09/10/21 09:52
09/08/21 12:06
09/10/21 08:50
09/09/21 13:08
09/14/21 10:27
09/27/21 15:59
09/08/21 17:28
09/13/21 12:37
09/13/21 12:37
09/09/21 11:16
09/15/21 11:03
09/14/21 16:32
09/10/21 09:52
09/08/21 12:06
09/10/21 11:40
Sampled: 09/07/21 02:30 Received: 09/07/21 08:30
Prep Date/Time(s) Analysis DatelTime(s)
09/21/21 12:57 09/30/21 11:43
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 2 of 14

Client ID: SBM
Analvte
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Copper - Total
Magnesium - Total
Molybdenum - Total
Nickel - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
SAMPLE DETECTION SUMMARY
1
Lab ID: CE11550-01
Result Flau MDL
417 0.420
93 D 4.0
7300 2.0
3860 0.390
22000 800
0.366 0.0160
73.5 0.290
0.0396 .1 0.0250
0.0812 ] 0.0220
6.5 D 0.41
6.6 D 0.41
0.11 0.017
381 B 1.50
237 4.00
1.03
950 0
4.3
20000
1.51
QL Units
1.00 mg/L
9.0 mg/L
2.0 mg/l.
1.00 mg!L
800 mg/L
0.100 mg/L
1.00 mg/L
0.100 mg/L
0.100 mg/L
1.0 mg/L
1.0 mg/L
0.10 mg/L
5.00 mg/L
5.00 mg/L
[blank]
26 48 mg/L
0.12 0.12 % by Volume
500 500 mg/L
0.0440 0.100 mg/L
www.encolabs.com
Method Notes
EPA 6010D
EPA 350.1
SM 5210 B-2011
EPA 6010D
5M 5220D-2011
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 353.2
EPA 353.2
EPA 353.2
EPA 60100
EPA 6010D
CSU Method
EPA 351.2
SM 2540B-2011
SM 2540D-2011
EPA 6010D
LL Client ID: SBM
& iyte .RDAJAI Flag MDL I IL 1la% Notes
Phosphorus - Total 370 D 12 50 mg/L
Lab ID: CE11550-01RE1
EPA 365.4
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Metals by EPA 6000/7000 Series Methods
Lab Sample ID:CE11550-01
Sampled: 09/07/21 02:30
Sampled By:Elvin C Williamson
Received: 09/07/21 08:30
Work Order: CE11550
i
^ - ENCO farycertfed analyte[NC 591]
Analvte ICAS Numberl
Mercury [7439-97-6]^
Jtesults Flaq
0.000750 U
Units
mg/L
DI fltPL PAL Batch
5 0.000750 0.00100 1114003
Metals (total recoverable) by EPA 6000/7000 Series Methods
�• - ENCO Cary Lea Nf f,w alyffi [NC 591]
Analvte ICAS Numberl
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440.43-9]^
Cadmum [7440-70-2]^
Copper[7440-50-8]^
Lead [7439-92.1}^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel[7440-02-0]^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc[7440-66-6]^
LessidtE
417
0.0760
0.00360
3860
0.366
0.0310
73.5
0.0396
0.0812
381
0.0620
237
1.51
Elan
units
mg/L
U mg/L
U mg/L
rng/L
mg/L
U mg/L
mg/L
3 mg/L
3 mg/L
B mg/L
U mg/L
mg/L
mg/L
Classical Chemistry Parameters
- ENCO avry certffed analyle INC 591]
Anaitl:g [CAS Number]
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand^
Chemical Oxygen Demand^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N"
Nitrite as N [14797-65-0]^
Phosphorus[7723.14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen"
Total Solids^
Total Suspended Solids^
-w
Method A0811t78d BY Notes
EPA 7470A 09/15/21 11:03 CPH
E !QL EQL
10 0.420 1.00
10 0.0760 0.140
10 0.00360 0.0100
10 0.390 1.00
10 0.0160 0.100
10 0.0310 0.100
10 0.290 1.00
10 0.0250 0.100
10 0.0220 0.100
10 1.50 5.00
10 0.0620 0.100
10 4.00 5.00
10 0.0440 0.100
Bata
1108016
1I08016
1108016
1108016
1108016
1I080I6
1I08016
1I08016
1I08016
1108016
1I08016
1108016
1108016
Method
EPA 6010D
EPA 6010D
EPA 6010D
EPA 60100
EPA 6010D
EPA 60101)
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
ADal12ed OX
09/09/21 11:16 3DH
09/09/21 11:16 3DH
09/09/2111.16 3DH
09/09/21 11:16 JDH
09/09/21 11:16 JDH
09/09/21 11:16 3DH
09/09/21 11:16 3DH
09/09/21 11:16 3DH
09/09/21 11:16 JDH
09/09/21 11:16 3DH
09/09/21 1I:16 3DH
09/09/21 11:16 JDH
09/09/21 11:16 3DH
Results Flaq units 2F lypl f L ]latch Method Allalvzed Ay Notes
93 D mg/L 90 4.0 9.0 1I13018 EPA 350.1 09/14/21 10:27 JAH
7300 mg/L 1 2.0 2.0 1108006 SM 5210 8-2011 09/08/21 12:06 JOC
22000 mg/L 80 800 800 1110003 SM 52200-2011 09/10/21 11:40 30C
6.5 0 mg/L 10 0.41 1.0 [CALC] EPA 353.2 09/13/21 12:37 JAH
6.6 0 mg/L 10 0,41 1.0 1113006 EPA 353.2 09/13/21 12:37 JAH
0.11 mg/L 1 0.017 0.10 1108022 EPA 353.2 09/08/21 17:28 JAH
370 D mg/L 500 12 50 1I21018 EPA 365.4 09/30/21 11:43 JAH
1.03 [blank] 1 1108016 CSU Method 09/09/21 13:08 JDH
950 0 mg/L 100 26 98 1I15013 EPA 351.2 09/27/21 15:59 JAH
4.3 % by Volume 25 0.12 0.12 1114015 5M 25408-2011 09/14/21 16:32 DM3
20000 mg/L 200 500 500 1109012 SM 25400-2011 09/10/21 09:52 ZGW
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

www.encolabs.com
QUALITY CONTROL DATA
(Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1114003 - EPA 245,1
Blank(1114003-BLK1)
Prepared: 09/14/2021 07:37 Analyzed: 09/15/2021 10:37
Analvte
Mercury
Result Rae PAL
0.000150 U 0.000200
Spike Source
Units Level AMR
mg/L
%REC RPD
%REC Limits RPD pit [dotes
[LCS (1I14003-851)
Anande
Mercury
Prepared: 09/14/2021 07:37 Analyzed: 09/15/2021 10:40
Result flag A4.L Units
0.00495 0.000200
mg/L
Spike
Level
0.00500
Source
jtesult
%REC RPD
%REC Limits RPD Mud Nptes
99
80-120
Matrix Spike (1I14003-MS1)
Prepared: 09/14/2021 07:37 Analyzed: 09/15/2021 10:42
1
Source: CE12846-01
Analvte
Mercury
Result
0.00515
F q PAS
0.000200
Units
mg/L
Spike Source
Level Result %REC
0.00500 0.000150 U 103
%REC
Limits
75-125
RPD
RPD Limit ROM_
Matrix Spike pup (1I14003-MSD1)
Prepared: 09/14/2021 07:37 Analyzed: 09/15/2021 10:44
■
Source: CE12846-01
Anelvte
Mercury
Result Ilan P01 Units
0.00490 0.000200
mg/L
Spike
Level
0.00500
Post Spike (1I14003-PS1)
Source: CE12846-01
Analvte
Mercury
Result flag
5.13
Source
Result %REC
0.000150 U 98
%REC RPD
Limits RPD Ulna Notes.
75-125 5 25
Prepared: 09/14/2021 07:37 Analyzed: 09/15/2021 10:46
Spike
P01 Units Level
0.200
ug/L
5.00
Source
Result
-0.0113
%REC RPD
%REC Limits RPD mil Noter�
103 75-125
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1108016 - EPA 3005A
Blank (1108016-BLK1)
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:22
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Rend flan Pot Units Level
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0,400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
RPD
Result %REC Lin1itS RPD Limit Notes
[Blank (1I08016-BtK2) Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:28
Aluminum
Arsenic
FINAL
Spike Source
Result Ban P01. Units Level Result %REC Limits
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
%REC
1
RPD
RPD Limit Balm
Page 5 of 14

www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1108016 - EPA 3005A - Continued
Blank (1108016-BLI[R) Continued
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:28
Anablle
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result Flag P01. Units Level lam
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.183 3 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%RFC
%REC Limits
RPD
RPD imi Notes
I LCS(1I08016-851)
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:39
Anatvbe
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result flags P01, !hub Level Result %REC Limits
2.03 0.100 mg/L 2.00 101 80-120
0.197 0.0100 mg/L 0.200
0.0200 0.00100 mg/L 0.0200
2.13 0.100 mg/L 2.00
0.197 0.0100 mg/L 0.200
0.198 0.0100 mg/L 0.200
2.02 0.100 mg/L 2.00
0.199 0.0100 mg/L 0.200
0.203 0.0100 mg/L 0.200
10.5 B 0.500 mg/L 10.0
0.199 0.0100 mg/L 0.200
10.3 0,500 mg/L 10.0
0.205 0.0100 m9/L 0.200
98
100
107
98
99
101
99
101
105
99
103
102
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
RPD
RPD Um!
Matrix Spike (1108016-MSI) Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:42
1
Source: CE11396-01
Anable
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Elan P01. Units Level Rao %REC Limits RPD Limit Nato_
2.05 0.100 mg/L 2.00 0.103 97 75-125
0.150 0.0100 mg/L 0.200 0.00760 U 75 75-125
0.0144 0.00100 mg/L 0.0200 0.000360 U 72 75-125
565 0.100 mg/L 2.00 567 NR 75-125
0.201 0.0100 mg/L 0.200 0.00160 U 101 75-125
0.184 0.0100 mg/L 0.200 0.00310 U 92 75-125
31.0 0.100 mg/L 2.00 29.3 86 75-125
0.203 0.0100 mg/L 0.200 0.00974 96 75-125
0.214 0.0100 mg/L 0.200 0.0210 97 75-125
40.2 8 0.500 mg/L 10.0 29.9 103 75-125
0.159 0.0100 mg/L 0.200 0.00620 U 80 75-125
147 0.500 mg/L 10.0 138 88 75-125
0.201 0.0100 m5/L 0.200 0.00940 96 75-125
QM-07
QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 14

www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1108016 - EPA 3005A - Continued
[Matrix Spike Dup (1I08016-MSD1)
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 10:45
Source: CE11396-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Mickel
Potassium
Selenium
Sodium
Zinc
Result
2.07
0.151
0.0142
573
0.200
0.185
31.5
0.202
0.212
40.2
0.158
149
0.201
Ilan LOL
0.100
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.010C
0.0100
B 0.500
0.0100
0.500
0.0100
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0,200
0.0200
2.00
0.200
0.200
2.00
0.200
0,200
10.0
0.200
10.0
0.200
Source
Result
0.103
0.00760 U
0.000360 U
567
0.00160 U
0.00310 U
29.3
0.00974
0.0210
29.9
0.00620 U
138
0.00990
%REC RPD
%REC Limi RPD imi Notes
98 75-125 1
75 75-125 0.5
71 75-125 1
277 75-125 1
100 75-125 0.4
92 75-125 0.4
111 75-125 2
96 75-125 0.5
96 75-125 0.9
103 75-125 0.2
79 75-125 0.9
111 75-125 2
96 75-125 0.09
20
2C
20 QM-07
20 QM-07
20
20
20
20
20
20
20
20
20
[Post Spike (1I08016-PS1) Prepared: 09/08/2021 12:99 Analyzed: 09/09/2021 10:48
1
Source: CE11396-01
Analvte
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
R,eNult Bag P_01 Units Level Egad %REC Limits
2.12 0.100 mg/L 2.00 0.103 101 80-120
0.157 0.0100 m9/L 0.200 -0.0508 78 80-120
0.0155 0.00100 mg/L 0.0200 -0.00455 77 80-120
555 0.100 mg/L 2.00 567 NR 80-120
0.211 0.0100 mg/L 0.200 0.000202 105 80-120
0.193 0.0100 mg/L 0,200 -0.00496 97 80-120
30.5 0.100 mg/L 2.00 29.3 61 80-120
0.212 0.0100 mg/L 0.200 0.00974 101 80-120
0.222 0.0100 mg/L 0.200 0.0210 100 80-120
40.0 B 0.500 mg/L 10.0 29.9 101 80-120
0.186 0.0100 mg/L 0.200-0.0398 93 80-120
145 0.500 mg/L 10.0 138 72 80-120
0.211 0.0100 mg/L 0.200 0.00990 101 80-120
Classical Chemistry Parameters - Quality Control
RPD
RPD limit
QM-08
QM-08
QM-08
QM-08
QM-08
1
Batch 1108006 - NO PREP
l Blank (1I08006-BLK1)
Prepared & Analyzed: 09/08/2021 12:06
Analvte
Biochemical Oxygen Demand
Result i
2.0 U
Spike Source
POL Units Level Result %REC limits RPD Unlit Not.
2.0 mg/L
%REC
RPD
LCS(1I08006-B51)
Prepared & Analyzed: 09/08/2021 12:06
Analvte
Biochemical Oxygen Demand
Result Elan P91 Units
170
2.0
mg/L
Spike
Level
198
Source
Result
%REC RPD
%REC Limrt£ RPD limit Notes
88
85-115
(Duplicate (1108006-DUP1)
Source: CE09680-01
FINAL
Prepared & Analyzed: 09/08/2021 12:06
Spike Source
Result Elan P01 Unita Level await %REG Limits RPD
%REC
This report relates only to the sample as received by the laboratory, and may only be reproduced In his.
RPD
Limn
Notes
Page 7 of 14

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QUALITY CONTROL DMA
Classical Chemistry Parameters - Quality Control
1
Hatch 1108006 - NO PREP - Continued
Duplicate (1I08006-DUP1) Continued
Prepared & Analyzed: 09/08/2621 12:06
Source: CEO96130-01
Ana vte
Biochemical Oxygen Demand
Batch 1108016 - EPA 3005A
Spike Source
Result Elas POI Units Level Result
4.0 2.0 mg/L 4.0
%REC RPD
%REC Limits RPD Limit
0.7 30
N
[Blank (1I08016-BLK1)
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 13:08
Analvte
Sodium Adsorption Ratio
Result Elan P 1.
0.00 U
Units
[blank]
Spike
Level
Source
Result
%REC
%REC Ltmlts
RPD
RPD Limit Notes
Blank(1I08016-BLK2)
Prepared: 09/08/2021 12:49 Analyzed: 09/09/2021 13:08
Amite
Sodium Adsorption Ratio
Batch 1108022 - NO PREP
Result Flag P0L Units
0.00 U [blank]
Spike Source
Level kncrd} %REC Limits RPD Limi Notes
%REC
RPD
Blank (1I08022-BLK1)
Prepared: 09/08/2021 14:56 Analyzed: 09/08/2021 17:20
Analvte
Nitrite as N
Result Elae P 1.
0.017 U
0,10
Spike Source
Wilts Level Ewalt
mg/L
%REC
%REC Limit;
RPD
RPD Limit
LCS(1I08022-BS1)
Prepared: 09/08/2021 14:56 Analyzed: 09/08/2021 17:19
Analvte
Nitrite as N
R It Flan POI.
1.0
0.10
nits
mg/l.
Spike Source
Level Result
1.00
%REC RPD
%REC Chits RPD Ling Notes
103
90-110
Matrix Spike (11013022-MS1)
Prepared: 09/08/2021 14:56 Analyzed: 09/08/2021 17:22
i
Source: CE13743-01
Analvte
Nitrite as N
Result Elao
1.0
PQL units
mg/L
0.10
Spike
Level
1.00
Source
Result
0.019
%REC
98
%REC
LilllEti
90-110
RPD
RPD Lunt'
Matrix Spike (1I08022-MS2)
Prepared: 09/08/2021 14:56 Analyzed: 09/08/2021 17:25
Source: CE13743-03
Anahrle
Nitrite as N
Spike Source
AM& Etas PM Units Level Result
0.017 U
0.97
0.10
mg/L
1.00
%REC RPD
%REC n1_1,0 RPD Limit
97
90-110
Matrix Spike Dup (1I08022-MSD1)
Prepared: 09/08/2021 14:56 Analyzed: 09/08/2021 17:23
Source: CE13743-01
.Ankle
Nitrite as N
Batch 1109012 - NO PREP
Spike Source
Result )]as PCl_L Units Level Result
1.0 0.10 mg/L 1.00 0.019
Blank (1I09012-BLK1)
%REC RPD
%REC Lrmlls RPD Limit
98 90-110 0.06 10
Prepared & Analyzed: 09/10/2021 99:52
Spike
Analvte Result Elee P41. Units Level
Total Suspended Solids 2.5 U 2.5 mg/L
Source
Result
%REC RPD
%REC }imits RPD Limit Not
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1109012 - NO PREP - Continued
LCS (1I09012-BS1)
Prepared & Analyzed: 09/10/2021 09:52
1
Analvte
Total Suspended Solids
Read Han
100
P91 Units'
2.5 mg/L
Spike Source
Level Result
100
%REC
%REC Limits
101
80-120
RPD
RPD Limit Notes
Duplicate (iI09012-DUP1)
Prepared & Analyzed: 09/10/2021 09:52
1
Source: CE11426-01
Analvte
Total Suspended Solids
Spike Source
Result Ban EQL Units Level Result
2200
2500
250
mg/L
%REC
%REC Limits RPD
1I
RPD
LIMA
20
Duplicate (1109012-DUP2)
Prepared &Analyzed: 09/10/2021 09:52
1
Source: CE11550-01
Analvte
Total Suspended Solids
Batch 1110003 - Same
Result Elan PQL
19000
Spike
nits Level
0.01 mg/L
Source
Result
20000
%REC RPD
%REC Limits RPD Limit
2 20
Blank (1I10003-BLK1)
Prepared: 09/10/202108:50 Analyzed: 09/10/2021 11:40
Analvte
Chemical Oxygen Demand
Spike Source
Result Elan P.01 knits Level R UR
10 U 10 mg/L
%REC
%REC Limits
RPD
RPD Limit Nato_
LCS(1110003-BS1)
Prepared: 09/10/2021 08:50 Analyzed: 09/10/2021 11:40
Anal
Chemical Oxygen Demand
Spike Source %REC RPD
Result flan EQL !!nits Level Result %REC Um& RPD Limit News
510
10
mg/L
500
103
90-110
Matrix Spike (1110003-MS1)
Prepared: 09/10/2021 08:50 Analyzed: 09/10/2021 11:40
1
Source: CEI0018-01
Analvte
Chemical Oxygen Demand
Spike Source %REC RPD
Rftnilt Ban P_Q.L Units Level Result %REC Limit RPD Ijmn
590 10 mg/L 526 49 103 90-110 LL
LMatsix Spike Dup (1I10003-MSD1) Prepared: 09/10/2021 08:50 Analyzed: 09/10/2021 11:40
• w ffff�
Source:CE10916-01
Analvte
Chemical Oxygen Demand
Batch 1113006 - NO PREP
Spike Source %REC RPD
Result Elan EQL Units Level Result %REC Limits RPD Limit Notes_
580 10 mg/L 526 49 100 90-110 2 5
Blank (1I13006-BLK1)
Prepared: 09/13/2021 09:09 Analyzed: 09/13/2021 12:21
Amebas!
Nitrate/Nitrite as N
Result Elan
u
0.041
Spike Source
POL Units Level uomft %REC Limits RPD Limit Noies-
0.10 rng/L
%REC
RPD
LCS (1113006-BS1)
Prepared: 09/13/2021 09:04 Analyzed: 09/13/2021 12:23
Analvte
Nitrate/Nitrite as N
Spike
Result Eau PQ Units Level
1.3 0.10 mg/L 1.25
Source
Result
%REC
%REC WAN
102 90-110
RPD
RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 9 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Hatch 1113006 - NO PREP - Continued
Matrix Spike (1I13006-MS1)
Prepared: 09/13/2021 09:04 Analyzed: 09/13/2021 12:27
Source: CE11369-01
Analvte
Nitrate/Nitrite as N
Result Elan
0.90
PQI. Units
mg/L
0.10
Spike
Level
0.521
Source
Result
0.33
%REC
111
%REC
Limit
90-110
RPD
RPD
Motes
QM-07
[Matrix Spike (1I13006-MS2)
Source:CE11370-01
Analvte
Nitrate/Nitrite as N
Prepared: 09/13/2021 09:04 Analyzed: 09/13/2021 12:32
Result Flag PQL
0.71
0.10
Units
mg/L
Spike Source
Level Result
0.521
0.13
%REC RPD
%REC Limits RPD mit
112
90-110
Notes
QM-07
Matrix Spike Dup (1113006-MSD1)
Source:CE11369-01
Analvte
Nitrate/Nitrite as N
Batch 1113010 - NO PREP
Prepared: 09/13/2021 09:04 Analyzed: 09/13/2021 12:28
Spike Source %REC RPD
Result Flag PQL Units Level Resul>i %REC Li111112 RPD Limit
0.95 0.10 mg/L 0.521 0.33 119 90-110 5 10 QM-07
[Blank (1113018-8LK1)
Prepared: 09/13/2021 16:00 Analyzed: 09/14/2021 10:04
Y
.Anehrte
Ammonia as N
Result Eine
0.095 U
Spike Source
EDI. Units Level Result
0.10 mg/L
%REC
RPD
%REC r units RPD Limit Notes
LCS(1I13018-851)
Prepared: 09/13/2021 16:00 Analyzed: 09/14/2021 10:06
Analvte
Ammonia as N
Result Flag
1.1
PQL Units
mg/L
0.10
Spike Source %REC
Level Result %REC Limn
1.01
107
90-110
RPD
RPD unfit
Notes
Matrix Spike (1113018-MS1)
Prepared: 09/13/2021 16:00 Analyzed: 09/14/2021 10:10
Source: CE11435-01
Ana
Ammonia as N
Matrix Spike (1I13018-MS2)
Source: CE11440-01
Analvte
Ammonia as N
Result Elsa E.91
0.54
Result Flan
0.38
0.10
Units
mg/L
PQL !!lilts
mg/L
0.10
Spike Source
Level Result
0.393
0.20
%REC RPD
%REC im RPD LUlit
85
90-110
Prepared: 09/13/2021 16:00 Analyzed: 09/14/2021 10:15
Spike Source
Level Result
0.045 U
0.393
Notes_
QM-07
1
%REC RPD
%REC Limits RPD Limit Notes
97
90-110
Matrix Spike Dup (1I13018-MSD1)
Prepared: 09/13/2021 16:00 Analyzed: 09/14/2021 10:11
Source:CE11435-01
Analvte
Ammonia as N
Hatch 1114015 - NO PREP
Result Etas PQL Units
0.54
Spike Source
Level giMRt
0.10 mg/L 0.393 0.20
%REC RPD
%REC Limits RPD Lilt
86 90-110 0.8 10 QM-07
[Blank (1I14015-BLK1)
Prepared &Analyzed: 09/14/2021 16:32
1
Analvte
Total Solids
Spike Source
Result Ejag PQL tlnat5 Level BMA %REC Limig RPD
0.0050 U 0.0050 % by Volume
%REC
RPD
Umt
BOIL
FINAL This report relates only to the sample as received ay the laboratory, and may only be reproduced In full.
Page 10 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1114015 - NO PREP - Continued
LCS(1I1.4015-BS1)
Prepared & Analyzed: 09/14/2021 16:32
Analvte
Total Solids
Result Flag POI Units
1100
50
mg/L
Spike Source
Level BOO
ii
1100
%REC RPD
%REC Limits RPD Limit t
100
90-110
i
Duplicate (1114015-DUP1)
Prepared &Analyzed: 09/14/2021 16:32
Source: CE11549-01
Anaivte
To Solids
Batch 1115013 - Same
Spike Source
Result Elan EQ.4 Units Level Result
0.23
0.23 0.0050 % by Volume
RPD
%REC Limits RPD L!l111t dots
z 5
Y
%REC
Blank (1I15013-BLK1)
Prepared: 09/16/2021 12:23 Analyzed: 09/27/2021 15:19
Analvte
Total Kjeldahl Nitrogen
LCS (1I15013-B51)
Anakte
Total Kjeldahl Nitrogen
Result Elan
0.26
Spike
i'_QL Units Level
0.48
mg/L
Result Elan POI Units
13
0.48
mg/L
Source
Result;
%REC
%REC Limits
RPD
RPD Unlit
Prepared: 09/16/2021 12:23 Analyzed: 09/27/2021 15:40
Spike Source %REC
Level Rama %REC Limits
12.0
108
90-110
■
RPD
RPD Limit NOW_
[Matrix Spike (1I15013-MS1)
Source: CE11549-01
Analvte
Total Kjeldahl Nitrogen
Prepared: 09/26/2021 12:23 Analyzed: 09/27/2021 15:44
1
Result Elan
17
PAL units
rrg/L
0.48
Spike Source
Level Result
17
4.80
%REC
%REC Limits RPD
NR
90-110
RPD
Limit
jY_q�a
QM-07
Matrix Spike (1I15013-MS2)
Source: CE13234-01
Analvte
Total Kjeldahl Nitrogen
Prepared: 09/16/2021 12:23 Analyzed: 09/27/2021 15:49
Spike
Result Plan P-QL Units Level
1.5
0.48
mg/L
4.80
Source
Result
1.1
%REC
7
%REC
Limits
90-110
RPD
RPD
Limit
Notes
QM-07
Matrix Spike Dup (1115013-MSD1)
Source:CE11549-01
Anallde
Total Kjeldahl Nitrogen
Batch 1115015 - Same
Prepared: 09/16/2021 12:23 Analyzed: 09/27/2021 15:45
Spike Source %REC RPD
Result than PQL Units Level Result %REC 1 n RPD Unlit ices_
16 0.48 mg/L 4.80 17 NR 90-110 7 10 QM-07
Blank(1I15015-BLK1)
Prepared: 09/16/2021 12:23 Analyzed: 09/28/2021 13:18
Anallte
Phosphorus
Result Elan
0.025 U
Spike
P_QL Units Level
0.10
mg/L
Source
Res= %REC Limits RPD limit
%REC
RPD
I LCS (1I15015-BS1)
Prepared: 09/16/2021 12:23 Analyzed: 09/28/2021 13:19
Anaki&
Phosphorus
Spike Source
Result EIS P-QL Units Level Result
1.6 0.10 mg/L 1.60
%REC
%REC Lim&
98 80-120
RPD
RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11of14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1115015 - Same - Continued
[Matrix Spike (1I15015-MS1)
Prepared: 09/16/2021 12:23 Analyzed: 09/28/2021 13:22
Source: CE11549-01
Analvte
Phosphorus
Result
13
Elan EDI
E
0.10
Units
mg/L
Spike
Level
Source
13
%REG
%REC Limits RPD
80-120
RPD
Limit
Notes
QM-07
Matrix Spike Dup (1I15015-MSD1)
Prepared: 09/16/2021 12:23 Analyzed: 09/28/2021 13:23
1
Source: CE11549-01
An;llyte
Phosphorus
Batch 2121018 - Same
Result E189
13 E
Spike
PQL MBAs Level
0.10 mg/L
Source
Result
13
%REC
%REC Limits RPD
80-120 0.1
RPD
Limit
25
QM-07
[Blank (1I21018-BLK1)
Prepared: 09/21/2021 12:57 Analyzed: 09/30/202I 11:04
AnaktO
Phosphorus
Result EMI
0.025 U
Spike Source
POI. Units Level Result %REG limits RPD
0.10 mg/L
%REC
RPD
Limit !is_
[LCS(1U21018-BS1)
Prepared: 09/21/2021 12:57 Analyzed: 09/30/2021 11:05
Anabtte
Phosphorus
Result Hag
1.5
Spike
PQL Units Level
0.10
mg/L
1.60
Source
Result
%REC
%REC Limits RPD
97
80-120
RPD
Limn
Matrix Spike (4I21018-MS1)
Prepared: 09/21/2021 12:57 Analyzed: 09/30/2021 11:08
Source: CE11835-01
Analvte
Phosphorus
Result 11as P9l
0.89
0.10
Units
mg/L
Spike
Level
0.690
Source
&Ed
0.80
%REC
%REC Limits RPD
14
80-120
RPD
Unlit
NoteE..
QM-07
[Matrix Spike Dup (1I21018-MSD1)
Source: CE11835-01
Anoints
Phosphorus
Prepared: 09/21/2021 12:57 Analyzed: 09/30/2021 11:09
Result lv
1.5
PQL Units
0.10 mg/L
Spike Source
Level Resin
0.640 0,80
%REC
RfaREC Uinta RPD
113 80-120 53
RPD
Limit
25
FINAL This report relates only to the sample as received by the laboratory, and may only 6e reproduced In full.
Page 12 el 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
3 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
{CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 14

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
10775 Central Port Dr 4510 Executive Perk Court Suite 111
Orlando. FL 32624 .tarkemovlle FI. 322186069
0071028.5314 (9041290.300'7 Fee [phone]
102•A Woodwinds Industnel G
Cary, NC 27511
10191487.3090 Fak(9191487-3515
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Page _ of
Chen! Name
Novozymes North America (N0008)
P ecl Number
[none]
Requested Analyses
Requested Turnaround
N.
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acceptance by the facility
_ Standard
Expedited
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Due _l_l__
Address
77 Perry Chapel Church Road
Pra,� 1NamNDesc
Monthly - Week One - SBM
C4 /STIZe
Frankinton, NC 27525
PO M 15 Hr kilo
3700044905 —
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Reporting ��
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Condition Upon Receipt
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MatrixGW-Gtoundweter SO.Sorl DW-prinking Water SE -Sediment SW -Surface Water WW-Weslaweter A -Air 0-0lher (dabs in cornmeal') Preservation:1-tos H-HC1 N-HNO3 S-H2SO4 NO-NaOH 0-Other piled in comments)
Note AA samples submitted to ENCO Labe are in accordance welt Me time and conditions bated on the mimeo of the lone union F+ror written agreements um

Sample Preservation Verification
ENCO Cary
Work Order CE11550
Client: Novozymes North America (N0008)
Logged In 07-Sep-21 11 25
Preservation Check Performed By:
Project Monthly - Week One - SBM
Project #: [none]
Logged By. Rachel Ann Yo is
Date/Time: ct 1 Z-L b z-0
1550.01
Cont
Type
Pres (pH)
pH Checked /
In Control
pH Adjusted Date/Trne
Adiu_ted
Reagent Used/Comments
D
25DmLP�H2SO4
<2
iti'''? N / NAB
v N / NA�ji7ltI ILA,
%% ` �
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250mLP+HNO3
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Reagent Name ID
1 k125-I
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pH Strip ID:
PH Strips OOI"0555
C lelmnt\Printawko_PreservationCheck.rpt
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Reagent Name ID Reagent Name ID
5
6
Page 1 of 1

ENCO Laboratorks
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, October 21, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE13955
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, October 5, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Parameter Preparation
CSU Method EPA 3005A
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 [CALC]
EPA 353.2 NO PREP
EPA 365.4 Same
EPA 6010D EPA 3005A
EPA 7470A EPA 295.1
SM 25408-2011 NO PREP
SM 2540D-2011 NO PREP
SM 5210 8-2011 NO PREP
SM 5220D-2011 Same
Lab ID: CE13955-01
Sampled: 10/05/21 01:25 Received: 10/05/21 08:30
Hold Date/Time(s1
06/30/24
11/02/21
11/02/21
10/07/21 01:25
10/07/21 01:25
11/02/21
11/02/21
04/03/22
11/02/21
10/12/21
10/12/21
10/07/21 01:25
11/02/21
Preis Date/Time(s).
10/06/21 09:41
10/08/21 09:05
10/14/21 12:00
10/05/21 15:39
10/14/21 09:47
10/14/21 09:47
10/14/21 12:00
10/06/21 09:41
10/07/21 08:12
10/12/21 18:22
10/11/21 16:52
10/06/21 10:51
10/12/21 11:23
Analysis Date/Time(?l
10/07/21 15:28
10/08/21 12:14
10/19/21 11:41
10/05/21 17:03
10/14/21 14:12
10/14/21 14:12
10/19/21 12:47
10/07/21 12:47
10/08/21 09:27
10/12/21 18:22
10/11/21 16:52
10/06/21 10:51
10/12/21 13:59
Client ID: SBM Lab ID: CE13955-01RE1
Sampled: 10/05/21 01:25 Received: 10/05/21 08:30
Parameter Preparation
SM 4500CI E-2011 NO PREP
Hold Date/Timels1
11/02/21
prep_Date/Tlme(s1
10/18/21 09:31
Analysis Date/Times}
10/18/21 13:18
FINAL
ibis report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 of 14

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Af, alvth
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Magnesium - Total
Nitrate as N
Nitrate/Nilrite as N
Nitrite as N
Phosphorus - Total
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
Lab ID: CE13955-01
1
Results fljg E1121 POL Units Me__
55.0 0.420 1.00 mg/L EPA 6010D
120 D 4.0 9.0 mg/L EPA 350.1
14000 2.0 2.0 mg/L SM 5210 6-2011
233o 0.390 1.00 mg/L EPA 6010D
30000 800 800 mg/L SM 5220D-2011
1.74 0.290 1.00 mg/L EPA 6010D
8.6 D 0.41 1.0 mg/L EPA 353.2
8.9 0 0.41 1.0 mg/L EPA 353.2
0.31 0.017 0.10 mg/L EPA 353.2
320 D 12 50 mg/L EPA 365.4
463 1.50 5.00 mg/L EPA 6010D
353 4.00 5.00 mg/L EPA 6010D
1.56 [blank] CSU Method
1200 D 26 48 mg/L EPA 351.2
4,6 0.12 0.12 % by Volume SM 2540B-2011
22000 250 250 mg/L SM 25400-2011
0.0917 2 0.0440 0.100 mg/L EPA 6010D
Client ID: SBM Lab ID: CE13955-01RE1
Anahrte
Chloride
Notes
Results flas MOL EQL TyAtE actin! Notes
580 D 19 50 mg/L SM 45000 E-2011
1
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CE13955 01 Received: 10/05/21 08:30
Matrix: Sludge Sampled:10/05/21 01:25 Work Order: CE13955
Project: Monthly Week One SBM Sampled By:Elvin C Williamson
Metals by EPA 6000/7000 Series Methods
^ - ENLW Cary certified analyte INC 591]
Analvte ICAS Number]
Mercury [7439-97-6I^
Results Elea ni a rm.L Pi. Batch Method &DIEM Dv: Meta
0,000750 U mg/L 5 0.000750 0.00100 1307007 EPA 7470A 10/08/21 09:27 CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
1
A - ENCO Cary cerliEed analyte [NC 591j
Analvte [CAS Number] Results flats nr QE N L P9& litthsai Analiard Ikt nolo
Aluminum [7429-90-5]^ 55.0 mg/1. 10 0.420 1.00 1306014 EPA 6010D 10/07/21 12:47 3DH
Arsenic[7440-38-2]^ 0.0760 U mg/L 10 0.0760 0.100 1106014 EPA 6010D 10/07/21 12:47 3DH
Cadmium [7440-43-9]^ 0.00360 U mg/L 10 0.00360 0.0100 1306014 EPA 6010D 10/07/21 12:47 3DH
Calcium [7440-70-2]^ 2330 mg/L 10 0.390 1.00 1306014 EPA 6010D 10/07/2I 12:47 3DH
Copper[7440-50-8]^ 0.0160 U mg/L 10 0.0160 0.100 1306014 EPA 6010D 10/07/21 12:47 3DH
Lead 17439-92.11" 0.0310 U mg/L 10 0.0310 0.100 1)06014 EPA 6010D 10/07/21 12:47 3131-1
Magnesium [7439-95-4]^ 1.79 mg/L 10 0.290 1.00 1306014 EPA 6010D 10/07/21 12:47 3DH
Molybdenum [7439-98-7]^ 0.0250 U mg/L 10 0.0250 0.100 1306014 EPA 6010D 10/07/21 12:47 3DH
Nickel [7440-02-0]^ 0.0220 U mg/L 10 0.0220 0.100 1306014 EPA 6010D 10/07/21 12:47 3DH
Potassium [7440-09-7]^ 463 mg/L 10 1.50 5.00 1306014 EPA 6010D 10/07/21 12:47 3DH
Selenium 17782-49-4^ 0,0620 U mg/L 10 0.0620 0.100 1306014 EPA 6010D 10/07/21 12:47 JDH
Sodium [7440-23-5]^ 353 mg/L 10 4.00 5.00 1306014 EPA 6010D 10/07/21 12:47 3DH
Zinc[7440-66-6]^ 0.0917 1 mg/L 10 0.0440 0.100 1306014 EPA 6010D 10/07/21 12:47 3DH
Classical Chemistry Parameters
^ - EN[, Cary certified anaIyt INC 591]
Analvte [CS Number] lieldM Flag Volta l2f %I Mk Batch =bad A Anal @x Mates
Ammonia as N [7664-41-71" 120 D mg/L 90 4.0 9.0 1308018 EPA 350.1 10/08/21 12:14 JAH
Biochemical Oxygen Demand" 14000 rng/L 1 2.0 2.0 1306001 SM 5210 B-2011 10/06/21 10:51 JOC
Chemical Oxygen Demand^ 30000 mg/L 80 800 800 1312010 SM 5220D-2011 10/12/21 13:59 JOC
Chloride [16887-00-6]^ 580 D mg/L 10 19 50 1318016 SM 4500CI E-2011 10/18/21 13:18 3AH
Nitrate as N [14797-55-8] 8.6 D mg/L 10 0.41 1.0 [CALCI EPA 353.2 10/14/21 14:12 3AH
Nitrate/Nitrite as N^ 8.9 D rng/L 10 0.91 1.0 1314016 EPA 353,2 10/14/21 14:12 3AH
Nitrite as N [14797-65-0]^ 0.31 rng/L 1 0.017 0.10 1J05027 EPA 353.2 10/05/21 17:03 JAH
Phosphorus(7723-14-0]^ 320 D mg/L 500 12 50 1314019 EPA 365.4 10/19/21 12:47 JAH
Sodium Adsorption Ratio 1.56 [blank] 1 1306014 CSU Method 10/07/21 15:28 JDH
Total Kjeldahl Nitrogen^ 1200 D mg/L 100 26 48 1314018 EPA 351.2 10/19/21 11:41 341
Total Solids^ 4.6 % by Volume 25 0.12 0.12 1312029 SM 2540B-2011 10/12/21 18:22 DM/
Total Suspended Solids^ 22000 mg/L 100 250 250 1111027 SM 2540D-2011 10/11/21 16:52 Dal
FINAL
This report relates only to tfie sample as received by the laboratory, and may only be reproduced In full. Page 4 of 14

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1707007 - EPA 245.1
Blank (1307007-BLK1)
Prepared: 10/07/2021 OB:12 Analyzed: 10/08/2021 09:07
Analvte
Mercury
Spike
RBIult flag P01. Units Level
0.000150 U 0.000200
mg/L
Source
EMIR
%REC
RPD
%REC Limits RPD LiL•llt Notes
LLCS(1307007-BS1)
Prepared: 10/07/2021 08:12 Analyzed: 10/08/2021 09:19
_MAAR
Mercury
Result flag P0L Units
0.00523 0.000200
mg/L
Spike Source %REC
Level Result %REC LjmjkE
0.00500
105
80-120
RPD
RPD Limit Nobel
Matrix Spike (1307007-M51)
Prepared: 10/07/2021 08:12 Analyzed: 10/08/2021 09:16
Source: CE14121-01
Analvte
Mercury
R sui Nan OLL
0.00542 0.000200
Spike Source
Units Level Result
mg/L
0.00500 0.000150 U
%REC RPD
%REC Limits RPD Limit
108
75-125
Matrix Spike Dup (1307007-MSD1)
Prepared: 10/07/2021 08:12 Analyzed: 10/08/2021 09:18
1
Source: CE14121-01
Analvte
Mercury
Result Flan P0.
0.00526 0.000200
Units
mg/L
Spike
Level
0.00500
Source
Result
0.000150 U
%REC
%REC vienu
105
75-125
RPD
3
RPD
mi
25
Post Spike (1307007-PS1)
Prepared: 10/07/2021 08:12 Analyzed: 10/08/2021 09;20
1
Source: CE14121-01
Analvte
Mercury
Spike Source %REC RPD
Result flea P01. Units Level Bela %REC 'rafts RPD limit N^ tes
5.76 0.200 ug/L 4.76-0.00705 121 75-125
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
1
Batch IJ06014 - EPA 3005A
Blank(1J06014-BLK1)
Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 11:23
1
Analvte
Aluminum
Arsenic
Cadmium
Calaum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Elea P01, !.nits
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
Spike Source
Level
%REC
Result %REC LjipjjA
RPD
RPD Limit
[LCS (1306014-B51) Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 11:33
r
Analvte
Aluminum
Arsenic
Spike Source
Result Flag PSIL Units Level Resit
1.99 0.100 mg/L 2.00
0.184 0.0100 mg/L 0.200
%REC
%REC Lim 1
100 80-120
92 80-120
RPD
RPD LIONS Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 5of14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/ 7000 Series Methods - Quality Control
Batch 1305014 - EPA 3005A - Continued
LCS (1706014-BS1) Continued
Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 11:33
A. 4allte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Flaa LQL Units Level
0.0199 0.00100 mg/1 0.0200
2.08 0.100 mg/L 2.00
0.189 0.0100 mg/L 0.200
0.192 0.0100 mg/L 0.200
1.98 0.100 mg/L 2.00
0.189 0.0100 mg/L 0,200
0.201 0.0100 mg/L 0.200
10.1 0.500 mg/L 10.0
0.189 0.0100 mg/L 0.200
9.99 0.500 mg/L 10.0
0.197 0,0100 mg/L 0.200
Matrix Spike (1]06014-MS1)
Source: CE14487-03
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
14.1
0.183
0.0206
7.91
0.212
0.200
5.79
0.192
0.224
10.7
0.180
38.8
0.239
Source
Result
%REC
%REC Limits RPD
99 80-120
104 80-120
95 80-120
96 80-120
99 80-120
94 80-120
100 80-120
101 80-120
95 80-120
100 80-120
98 80-120
Prepared: 10/06/2021 09:4, Pridryceu: 10/07/202.....16
RPD
Limit
Notes
Spike Source %REC RPD
Flag P44 Units Level Jtesult %REC Ljmlt& RPD Limit NQts&
0.100 mg/L 2.00 12.3 92 75-125
0.0100 mg/L 0.200 0.00760 U 92 75-125
0.00100 mg/L 0,0200 0.000360 U 103 75-125
0.100 mg/L 2,00 6.26 83 75-125
0.0100 mg/L 0.200 0.0191 96 75-125
0.0100 mg/L 0.200 0.00310 U 100 75-125
0.100 mg/L 2.00 3.84 97 75-125
0.0100 m9/1- 0.200 0.00250 U 96 75-125
0.0100 mg/L 0.200 0.0158 104 75-125
0.500 mg/L 10.0 0.641 100 75-125
0.0100 mg/L 0.200 0.00620 U 90 75-125
0.500 mg/L 10.0 29.4 94 75-125
0.0100 mg/L 0.200 0.0300 104 75-125
I Matrix Spike Dup (1306014-MSD1) Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 11:39
1
Source: CE14487-03
Analy e
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Dag PQj. Units Level Result %REC Limits RPD URA Notes
13.6 0.100 mg/L 2.00 12.3 69 75-125 4 20 QM-07
0.182 0.0100 m9/1- 0,200 0.09760 U 91 75-125 0.5 20
0.0208 0.00100 mg/L 0.0200 0.000360 U 104 75-125 0.9 20
7.84 0.100 mg/L 2.00 6.26 79 75-125 0.9 20
0.212 0.0100 mg/L 0.200 0.0191 96 75-125 0.05 20
0.201 0.0100 mg/L 0.200 0.00310 U 101 75-125 0.6 20
5.64 0.100 mg/L 2.00 3.84 90 75-125 3 20
0.194 0.0100 mg/L 0.200 0.00250 U 97 75-125 0.8 20
0.222 0.0100 mg/L 0.200 0.0158 103 75-125 1 20
10.8 0.500 mg/L 10.0 0.641 102 75-125 1 20
0.181 0.0100 mg/L 0.200 0.00620 U 91 75-125 0.6 20
38.7 0.500 mg/L 10.0 29.4 93 75-125 0.2 20
0.241 0.0100 mg/L 0.200 0.0300 106 75-125 1 20
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In fuH. Page 6 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1.705014 - EPA 3005A - Continued
[Post Spike (1306014-PS1)
Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 11:41
Source:CE14487-03
Analvte
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
13.9
0.188
0.0709
7.75
0.212
0.202
5.69
0.195
0.227
10.6
0.179
37.9
0.242
Flan Mk
0.I00
0.0100
0.00100
0.100
0.0100
0.0100
0.100
0.0100
0.0I00
0.500
0.0100
0.500
0.0100
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Source
Jtesult
12.3
-0.0120
9.32E-5
6.26
0.0191
0.00153
3.84
-0.00235
0.0158
0,641
-0.0183
29.4
0.0300
%REC
%REC Limits RPD
78 80-120
94 80-120
104 80-120
74 80-120
97 80-120
100 80-120
92 80-120
97 e0-120
106 80-120
100 80-120
89 80-120
85 80.120
106 80-120
RPD
Limit
Notes
QM-08
QM-08
Classical Chemistry Parameters - Quality Control
Batch 1305027 - NO PREP
1
[Blank (1)05027-BLK1)
Prepared: 10/05/2021 15:39 Analyzed: 10/05/2021 16:59
1
_AMMO
Nitrite as N
Result Flag
u
0.017
POL Units
mg/L
0,10
Spike Source
Level BALUA
%REC
%REC Limits
RPD
RPD Limit Notes
LCS(1305027-B51)
Prepared: 10/05/2021 15:39 Analyzed: 10/05/2021 17:10
Analvte
Nitrite as N
Result Hag POL
0.99
0.10
Units
mg/L
Spike Source
Level Rand}
1.00
%REC
%REC Limits RPD
99
90-110
RPD
Limit
[Matrix Spike (1705027-MS1)
Prepared: 10/05/2021 15:39 Analyzed: 10/05/2021 17:56
1
Source: CE13954-01
Anahrte
Nitrite as N
Spike
Result BRA P24 Units Level
2.3 0
0.50
mg/L
1.00
Source
Result
2.3
%REC
%REC Limits RPD
NR
90-110
RPD
Umit
WO_
QM-07
Matrix Spike Dup (1705027-MSD1)
Prepared: 10/05/2021 15:39 Analyzed: 10/05/2021 17:57
Y
Source: CE13954-01
Analvte
Nitrite as N
Batch 1306001- NO PREP
Spike
Result Flag POI units Level
2.3 D 0.50 mg/L 1.00
Source
Jtesuit %REC
2.3 NR
%REC
Limits RPD
90-110 0
RPD
Limit
10
Nate
QM-07
[Blank (L106001-13LKI)
Prepared & Analyzed: 10/06/2021 10:51
Anavim
Biochemical Oxygen Demand
Result
2.0
Spike Source
Elie PQL Units Level Result %REC Units RPD
U 2.0 mg/L
%REC
RPD
Us*
Notes_
1LCS(1]06001-est)
na
Prepared &Analyzed: 10/06/2021 10:51
Spike
Result flan in. Units Level
Source
Rend
%REC
%REC Liirnits RPD
RPD
Limit
N
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1.706001 - NO PREP - Continued
LCS(1306001-BS1)Continued
Analvte
Biochemical Oxygen Demand
1
Prepared & Analyzed: 10/06/2021 10:51
Result llae
200
POL Units
2.0 mg/L
Spike
Level
198
Source
Brauft
%REC
100
%REC
Limits
85-115
RPD
RPD Limit NQtgg
[Duplicate (1706001-DUP1)
Prepared & Analyzed: 10/06/2021 10:51
Source:CE12868-01
Analvte
Biochemical Oxygen Demand
Batch 1706014 - EPA 3005A
Spike Source %REC RPD
Result flan PM. Wiiif Level Result %REC Limits RPD rni
5.5 2.0 mg/L 5,5 0,5 30
r
Blank(1306014-BLK1)
Prepared: 10/06/2021 09:41 Analyzed: 10/07/2021 15:29
Analvte
Sodium Adsorption Ratio
Batch 1708018 - NO PREP
Result Elan
0.00 U
Spike Source
PQl. Units Level Result
[blank]
%REC RPD
%REC linhits RPD Unlit Notes
Blank (1308018-BLK1)
Prepared: 10/08/2021 09:05 Analyzed: 10/08/2021 11:51
1
Anahfte
Ammonia as N
Result flee
0.095 U
Spike Source
IPQL Units Level l3latiliit
0.10 mg/L
%REC RPD
%REC Limits RPD Limit Notes.
LCS(1]08018-851)
Prepared: 10/08/2021 09:05 Analyzed: I0/08/2021 11:53
1
Analvte
Ammonia as N
Result Flaci
1.1
Spike Source %REC
iPQQL Uni Level Result %REC Limns
0.10
mg/L
1.01
106
90-110
RPD
RPD Limit N9.IS
[Matrix Spike (1308018-MS1)
Source: CE12868-01
Analvte
Ammonia as N
Prepared: 10/08/2021 09:05 Analyzed: 10/08/2021 11:57
Remit Elan
0.38
POL 1lni.
mg/L
0.10
Spike Source
Level Rays
0.393
0.045
%REC
98
%REC
Lim
90-110
RPD
RPD Limit BIWA.
Matrix Spike (1308018-M52)
Prepared: 10/08/2021 09:05 Analyzed: 10/08/2021 12:05
Source: C813346-01
Analvte
Ammonia as N
Spike
Result Bali PQL Units Level
0,393
0.37
0.10
mg/L
Source
ROlR
0.045 U
%REC RPD
%REC Limi RPD Limi Notes
95
90-110
Matrix Spike Dup (1308018-MS131)
Prepared: 10/08/2021 09:05 Analyzed: 10/08/2021 11:58
Source: CE12868-01
Analvte
Ammonia as N
Batch 1711027 - NO PREP
Spike Source
Result Elea PQL Units Level ROAR
0.39 0.10 mg/L 0.393 0.045
%REC RPD
%REC Limits RPD Limit
98 90-110 0.7 10
1'l2t8.a
Blank(1711027-BLK1)
Prepared & Analyzed: 10/11/2021 16:52
1
Total Suspended Solids
Spike Source
Result Elan PQL Units Level Lead
2.5 U 2.5 mg/L
%REC
RPD
%REC Limits RPD mil
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 14

c
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
QO
www.encolabs.com
1
Batch 1'11027 - NO PREP - Continued
LCS(1)11027-BS1)
Prepared &Analyzed: 10/11/2021 16:52
1
naivte
Total Suspended Solids
Result flag
100
LOL
2.5
Units
mg/L
Spike
Level
100
Source
Result
%REC RPD
%REC Lid/2 RPD m€
100
80-120
litter
L
Duplicate (1311027-DUP1)
Prepared & Analyzed: 10/11/2021 16:52
J
Source: CE13394-01
Analvte
Total Suspended Solids
Batch 1.712010 - Same
Spike Source %REC RPD
Besuli Eau ES21. Units Level Result %REC Limits RPD 'mit Notes
460 120 mg/L 540 16 20
Blank (1312010-BLK1)
Prepared: 10/12/2021 11:23 Analyzed: 10/12/2021 13:59
Analvte
Chemical Oxygen Demand
Spike Source %REC RPD
Result Bag E41 Units Level Result %REC Limits RPD "mi Note_
10
U
10
mg/L
LCS(1312010-BS1)
Prepared: 10/12/2021 11:23 Analyzed: 10/12/2021 13:59
1
Analvte
Chemical Oxygen Demand
Result Elag E01. 11011s
520
10
mg/L
Spike Source
Level
500
%REC RPD
%REC i i RPD Limit
103
90-110
Matrix Spike (1312010-MS1)
Prepared: 10/12/2021 11:23 Analyzed: 10/12/2021 13:59
Source: CE12121-01
Analvte
Chemical Oxygen Demand
Result flag P32L Units
590
10
mg/L
Spike
Level
526
Source
)tesult
42
%REC RPD
%REC Limits RPD Limit
105
90-110
[Matrix Spike Dup (1312010-MSD1)
Prepared: 10/12/2021 11:23 Analyzed: 10/12/2021 13:59
Source: CE12121-01
Ano de
Chemical Oxygen Demand
Batch 1.712020 - NO PREP
Spike Source %REC RPD
Result Elaa P0l. Units Level Rem %REC Limits RPD irme ROIL
580 10 mg/L 526 42 103 90-110 2 5
Blank (1312029-BLK1)
Prepared & Analyzed: 10/12/2021 18:22
Analvte
Total Solids
Result Flan
0.0050 U
P44
Spike
Units Level
0.0050 % by Volume
Source
Result
%REC
RPD
%REC Limits RPD t Notes
L_CS(1312029-B51)
Prepared & Analyzed: 10/12/2021 18:22
1
Analvte
Total Solids
RSS111t flag
1100
EDI
50
Spike Source
Level Result
1100
%REC RPD
%REC Liimlts RPD LiS1Jt
101
90-110
Duplicate (1.312029-DUP1)
Prepared &Analyzed : 10/12/2021 18:22
Source:CE13954-01
Analvte
Total Solids
Batch 1J14016 - NO PREP
Rata
Spike Source %REG RPD
Result flag ROL Units Level Emit %REC 'Limits RPD Limit 'i�.tils
0.23 0.0050 % by Volume 0.23 2 5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1J14016 - NO PREP - Continued
Blank(1114016-B1.K1)
Prepared: 10/14/2021 09:47 Analyzed: 10/14/2021 13:47
.Analyte
Nitrate/Nitrite as N
Result Elan
0.041 U
Spike
PS& Units Level
0.10
mg/L
Source
Bala
%REC RPD
%REC Limits RPD Limit NeteF_
LCS (1314016-BS1)
Prepared: 10/14/2021 09:47 Analyzed: 10/14/2021 13:48
Analvte
Nitrate/Nitrite as N
Spike
Result flan E9.1- Units Level
1.2
0.10
mg/L
1.25
Source
Result
%REC
95
%REC
Linr[ts RPD Limit
90-110
RPD
Matrix Spike (1314016-MS1)
Prepared: 10/14/2021 09:47 Analyzed: 10/14/2021 13:52
Source:CE14489-01
Anahrte
Nitrate/Nitrite as N
Res Flag
0.56
PS&
0.10
Spike
Units Level
mg/L
0.521
Source
Result
0.041 U
%REC RPD
%REC -rmi RFD D 5L
107
90-110
Matrix Spike (1314016-MS2)
Prepared: 10/14/2021 09:47 Analyzed: 10/14/2021 13:57
Source: CE14489-02
Anahrte
Nitrate/Nitrite as N
Spike
Result Etas PQL !!nits Level
0.55
0.10
mg/L
0.521
Source
Result
0.041 U
%REC RPD
%REC Limits RPD Limit MARL
106
90-110
Matrix Spike Dup (1314016-MSD1)
Prepared: 10/14/2021 09:47 Analyzed: 10/14/2021 13:54
Source: CE14489-01
Analvte
Nitrate/Nitrite as N
Batch 1114018 - Same
Spike Source
Result flea PS& Unita Level Result
0.55 0.10 mg/L 0.521 0.041 U
%REC RPD
%REC Limits RPD Limit Nowt g
106 90-110 0.7 10
[Blank (L714018-BLK1)
Analvte
Total Kjeldahl Nitrogen
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 10:55
Spike Source %REC RPD
Result Sae PQL Units Level Result %REC Limits RPD Limit Notes
0.26 U 0.48 mg/L
LCS (1314018-051)
Analvte
Total Kjeldahl Nitrogen
Result Elan l201. ![nits
13
0.48
mg/L
Prepared: 10/14/202. 12:00 Analyzed: 10/19/2021 11:20
Spike Source
Level BOA
12.0
%REC RPD
%REC Limits RPD Lkna
107
90-110
EMIL
Matrix Spike (1314018-MS1)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 11:24
Source: CE14857-01
ABabrte
Total Kjeldahl Nitrogen
Result Flan
4.4
POL
0.48
Units
mg/L
Spike Source
Level Rsssdft
0.42
4.80
%REC
82
%REC RPD
Limits RPD limit Notes
90-110
QM-07
Matrix Spike (1214018-MS2)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 11:29
Source: CE14843-01
Analvte
Total Kjeldahl Nitrogen
Spike Source
Hawk Flags PQL Units Level Result
4.9 0.48 mg/L 4.80 1.2 76 90-110
%REC
%REC Lints
RPD
RPD Limit
i
Notes
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 10 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1714018 - Same - Continued
[Matrix Spike Dup (1314018-MSD1)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 11:25
Source: CE14657-01
Analvte
Total Kjeldahl Nitrogen
Batch 1.714019 - Same
Spike Source %REC
Result Bail PQL Units Level %REC L€mPts RPD
3.1 0.48 mg/L 9.80 0.42 56 90-110
RPD
Notes
33 10 QM-07,
QM-11
[Blank(1314019-BLK1)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 12:38
r
A aAgg
Phosphorus
Result flag
0.025 U
Spike
PQL Unib Level
0.10
mg/L
Source
Result
%REC
%REC Limits RPD
RPD
Lie& Notes
LCS(1314019-BS1)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 12:39
1
Analvte
Phosphorus
Result
1.7
Spike
Flan PQL Units Level
0.10
mg/L
1.60
Source
Result
%REC RPD
%REC Limits RPD Limit
103
80-120
Notes
Matrix Spike (1314019-MS1)
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 12:42
Source: CE14857-01
Analvte
Phosphorus
Matrix Spike Dup (1314019-MSD1)
Result Flan
7.2 0
PQL Units
mg/L
0.50
Spike
Level
0.640
Source
Resuit
6.7
%REC
%REC Limits RPD
71
80-120
Prepared: 10/14/2021 12:00 Analyzed: 10/19/2021 12:43
RPD
L€m€t
Notes
QM-07
Source: CE14857-01
Analvte
Phosphorus
Batch 1J18016 - NO PREP
Spike Source %REC RPD
Result Fine P41 Lints Level Emit %REC Limits RPD Limit Bolas_
7.1 D 0.50 mg/L 0.640 6.7 64 80-120 0.6 25 QM-07
Blank(1318016-BLK1)
Prepared: 10/18/2021 09:31 Analyzed: 10/18/2021 12:20
Analvte
Chloride
Result BM
1.9 U
Spike Source
PQL Units Level Result %REC Limits RPD
5.0 mg/L
%REC
RPD
Limit
1
LCS(1318016-8S1)
Prepared: 10/18/2021 09:31 Analyzed: 10/18/702I 12:20
llndhrim
Chloride
Result Flag
99
POL Units
5.0 mg/L
Spike Source
Level Result
100
%REC
%REC Limits RPD
99
80-120
RPD
Limit
Duplicate (1318016-DUP1)
Prepared: 10/18/2021 09:31 Analyzed: 10/18/2021 12:23
Source: CE13349-01
1
Anaivte
Chloride
Result Etas
D
520
POL
50
Spike
MILLS Level
mg/L
Source
Result
530
%REC
RPD
%REC Limits RPD Limit H
2 10
Matrix spike (L118016-M51)
Prepared: 10/18/2021 09:31 Analyzed: 10/18/2021 12:22
1
Source: CE13349-01
Ana
Chloride
Spike Source %REC RPD
i t Flag PQL MB& Level Resuit %REC Minks RPD Limit BMW_
930 50 mg/L 400 530 99 80-120
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 14

www.encalabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1J18016 - NO PREP - Continued
[Matrix Spike Dup (1318016-MSD1)
Prepared: 10/18/2021 09:31 Analyzed: 10/18/2021 12:22
Source: CE13349-01
Analvte
Chloride
Spike Source %REC
Result Flag PQL lints Level RANK %REC Limps
930 50 mg/L 400 530 99 80-120
RPD
RPD Limit Notes
0.1 25
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
8 The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LC5 recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In fuii. Page 131114

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 Central Pori Dr
Orlando. FL 32624
1407) 626-5314
4610 E.xeaHrve Parr Court Suds 111
Jacksotrn9e, FL 32216-6069
49041 296-3007 Fax t9041296-6210
102-A Woodwinds Industrial CI
Cary, NC 27511
949) 467.3000 Fax [phone]
Page of
Chant Name
Novozyrnes North America (N0008)
Addr.s.
77 Perry Chapel Church Road
Protect Number
[none]
Prowl Nema'Desc
Monthly - Week One - SBM
Requested Analyses
CnyiSTr2ip
Frenkllnton, NC 27525
PDX 1 Into
3700 05
Tal 494.3000
Fax
Reporting Confect
Scoit Creech
Srlmplerls) Name Alhpaaon (Prom
61w,, ,SiA)
Sampler's) Si9neitrre
tillry L 4J- rakr*1 �
Item s
Sample ID Wield ldentdlrationl
SBM
Collection Date
Vocc?olidnis Payable
Site La®[gn +Tune Zone
Collection
Trine
Comp l Grab
Mete
(See coolest
Total X al
Cama:nar%
BOD SM5210B
Prase
0
0
COD SM5220D
TSS SM2540D
Requested Turnaround
Times
Note Rush ,',VS.'. S.. subtacl. to
rr r, by the lacsdy
Standard
_ Expedited
Due / e_1
rvation [See Codes) ICam1Xte as n.ce.s.ryl
lv-s_ rV
et. x5
G
SL
7
x x x
Lab Workorder
CE 13955
Sample Comments
Rolrnqurehed By
I JO
Relinquished By
Relinquished By
Cooler as & Temps an Receipt
<-- Total A of Containers
DawTime
/a-.5-; A
DaleiTXne
DetsTtm.
Recorved By
2 U pL
Conditton•Upon Receipt
'Acceptable
Matrix OW -Groundwater SO -Sod DWDdntrrn9 Water SE•Sed maid SWSurfece Water W W-Wastewater A•Air 0-Other (detail in comments) Preservation: I -Ice tf-HCI N44NO3 S-H2SO4 NO-NaOH 0.09ter idyls& m oommanls)
Note . Aft samples submitted to ENCO Labs are in accordance with the farms and conditions listed on the reverse of this form. unless pr.or written agreements axial
D.IaOrwne
it- s-x, 0.5:iJ
DeffiFrma
Daterrlme
Unacceptable

Sample Preservation Verification
ENCO Cary
Work Order. CE13955
Client Novozymes North America (N0008)
Logged In 05-Oct-21 13 15
Preservation Check Performed By:
Project Monthly - Week One - SBM
Project # [none]
Logged By Rachel An � Ya�i� t D�
Date/Time.O]
1
Cont
Type
Pres (pH)
pH Checked /
In ControlAdiusted
pH Adjusted Date/Time
Reagent Used/Comments
D
250mLP+H2504
<2 y
' / N / NA
Y
! NA
E
250mLP+HNO3
<2
j N / NA
Y / N
NA
1
2
Reagent Name
ID
pH Strip ID.
PH Strips C0F0555
C:\elmnt\Prii•Lvrnv,_. ,GOCITaUVI141IGL.n.IPt
Reagent Name ID
3
5
6
Reagent Name ID
Page 1 of '

NCO Laboratorws
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, November 16, 2021
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE16415
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 2, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 1 al 14

SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CE16415-01
Sampled: 11/02/21 02:40
Parameter Preparation
CSU Method EPA 3005A
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 [CALC]
EPA 353.2 NO PREP
EPA 365.4 Same
EPA 6010D EPA 3005A
EPA 7470A EPA 245.1
SM 2540B-2011 NO PREP
SM 2540D-2011 NO PREP
SM 4500CI E-2011 NO PREP
SM 5210 B-2011 NO PREP
SM 5220D-2011 Same
Hold Date/Timefsl
07/28/24
11/30/21
11/30/21
11/04/21 02:40
11/04/21 02:40
11/30/21
11/30/21
05/01/22
11/30/21
11/09/21
11/09/21
11/30/21
11/04/21 02:40
11/30/21
www.encoiabs.com
Received: 11/02/21 OB:00
Prep Date/Timefsl Analysis Date/Timefsl
11/05/21 10:56 11/09/21 15:56
11/04/21 09:43 11/04/21 13:30
11/09/21 12:54 11/11/21 14:01
11/02/21 15:52 11/02/21 17:30
11/05/21 10:56 11/05/21 13:52
11/05/21 10:56 11/05/21 13:52
11/09/21 15:00 11/15/21 16:33
11/05/21 10:56 11/09/21 12:53
11/05/21 13:13 11/09/21 09:17
11/05/21 19:00 11/05/21 19:00
11/08/21 14:23 11/08/21 18:00
11/08/21 08:59 11/08/21 10:51
11/03/21 13:41 11/03/21 13:41
11/08/21 13:34 11/08/21 16:15
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 2 of 14

Client ID: SBM
Anal e
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Chloride
Magnesium - Total
Nickel - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Phosphorus - Total
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Zinc - Total
www.encolabs.com
SAMPLE DETECTION SUMMARY
Lab ID: CE 16415-01
Results 1,31g MDL ni Ilsnld
2.85 0.420 1.00 mglL EPA 6010D
180 D 4.0 9.0 mg/L EPA 350.1
10000 2.0 2.0 mglL SM 5210 8-2011
1670 0.390 1.00 mg/L EPA 6010D
32000 800 800 mg/L SM 5220D-2011
580 D 19 50 mg/L SM 4500CI E-2011
15.6 0.290 1.00 mg/L EPA 6010D
0.0226 1 0.0220 0.100 mg/L EPA 6010D
5.4 D 0.41 1.0 mglL EPA 353.2
5.6 0 0.41 1.0 mg/L EPA 353.2
0.13 0.017 0.10 mg/L EPA 353.2
530 D 12 50 mg/L EPA 365.4
393 1.50 5.00 mg/L EPA 6010D
193 4.00 5.00 mg/L EPA 6010D
1.29 {blank] CSU Method
480 D 26 48 mg/L EPA 351.2
4.0 0.12 0.12 % by Volume SM 25408-2011
28000 500 500 mg/L SM 25400-2011
0.148 0.0440 0.100 m9/L EPA 6010D
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 3 of 14

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ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project Monthly - Week One - SBM
Lab Sample ID:CE16415-01
Sampled:11/02/21 02:40
Sampled By:Elvin C Williamson
Received: 11/02/21 08:00
Work Order: CE16415
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certrrred anaryte[NC 591j
Apalvte TCAS Number"'
Mercury [7439-97-6]^
Results flag
0.000750 U
ni
mg/L
DE MI6 44 1=11 Method Analysed gill: NOas
5 0.000750 0.00100 1K05031 EPA 7470A 11/09/21 09:17 CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary ceralred anaryte INC 591]
Analvte [CAS Number"'
Aluminum [7429-90-5]^
Arsenic [7440-38-2]^
Cadmium [7440-43-9]^
Calcium [7440-70-2]^
Copper[7440-50.8]^
Lead [7439-92.1]^
Magnesium [7439-95-4]^
Molybdenum [7439-98-7]^
Nickel [7440-02-0]^
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc [7440-66-6]^
Results
2.85
0.0760
0.00360
1670
0.0160
0.0310
15.6
0.0250
0.0226
393
0.0620
193
0.148
Classical Chemistry Parameters
^ - ENCO Cary certhWanatyte INC 591]
Apalvte [CAS Numbed
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand^
Chemical Oxygen Demand^
Chloride [16887-00-6]^
Nitrate as N [14797-55-8]
Nitrate/Nitrite as N^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen^
Total Solids^
Total Suspended Solids^
] 189 11 P44 Balch Method
m9/L 10 0.420 1.00 1K05013 EPA 6010D
U mg/L 10 0.0760 0.100 1K05013 EPA 6010D
U mg/L 10 0.00360 0.0100 1K05013 EPA 6010D
mg/L 10 0,390 1.00 1K05013 EPA 6010D
U mg/1. 10 0.0160 0.100 1K05013 EPA 6010D
lJ mg/L 10 0.0310 0.100 1K05013 EPA 6010D
mg/L 10 0.290 1.00 1K05013 EPA 6010D
U mg/L 10 0.0250 0.100 1K05013 EPA 60100
J mg/L 10 0.0220 0.100 1K05013 EPA 60100
mg/L 10 1.50 5.00 1K05013 EPA 6010D
U mg/L 10 0.0620 0.100 1K05013 EPA 6010D
mg/L 10 4.00 5.00 1K05013 EPA 6010D
mg/L 10 0.0440 0.100 1K05013 EPA 6010D
iamined
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
11/09/21 12:53
NI Notes
JDH
]DE-1
JDH
JDH
]DH
JDH
JDH
JDH
JDH
JDH
3DH
JDH
JDH
Results Flag Units N. MU EDI Batch Method laduzi 6Y Notes
180 D mg/L 90 4.0 9.0 1K04020 EPA 350.1 11/04/21 13:30 JAH
10000 m9/1 1 2.0 2.0 11(03014 SM 5210 B-2011 11/03/21 13:41 JOC
32000 mg/L 80 800 800 1K08021 SM 5220D-2011 11/08/21 16:15 JOC
580 D mg/L 10 19 50 1K08008 SM 450001E-2011 11/08/21 10:51 JAH
5.4 D mg/L 10 0.41 1.0 [CALC] EPA 353.2 11/05/21 13:52 .JAH
5.6 D mg/L 10 0,41 1.0 1K05011 EPA 353.2 11/05/21 13:52 JAM
0.13 mg/L 1 0.017 0.10 1K02029 EPA 353.2 11/02/21 17:30 JAH
530 D mg/L 500 12 50 1K09024 EPA 365.4 11/15/21 16:33 JAH
1.29 [blank] 1 1K05013 CSU Method 11/09/21 15:56 JDH
480 D mg/L 100 26 48 1K09020 EPA 351.2 11/11/21 14:01 JAH
4.0 % by Volume 25 0.12 0.12 1K05040 SM 25408-2011 11/05/21 19:00 DMJ
28000 rng/L 200 500 500 1K08028 SM 2540D-2011 11/08/21 18:00 DMJ
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
1
Batch 1K05031 - EPA 245.1
Blank (1K05031-BLKL)
Prepared: 11/05/2021 13:13 Analyzed: 11/09/2021 08:23
Analvte
Mercury
LCS(1K05031-B51)
Analvte
Mercury
0.000150 U 0.000200
Spike Source
Result Flag e06 il*i Level Result %REC limits RPD Limit tl2leL
mg/L
%REC
Prepared: 11/05/2021 13:13 Analyzed: 11/09/2021 08:27
Spike
Result Elan EQl. Units Level
0.00516 0.000200 mg/L 0.00500
Source
Result
%REC
RPD
RPD
%REC Limits RPD i [
103
80-120
1
Matrix Spike (1K05031-MS1)
Source:CE16371-01
Analvte
Mercury
Matrix Spike Dup (1K05031-MSD1)
Source: CE16371-01
Analy
Mercury
[Post Spike (1K05031-PS1)
Source: CE16371-01
"Anellde
Mercury
Result Flag P91. Units
0.00540 0.000200
Result Eau EQL
mg/L
Units
0.00543 0.000200 mg/L
Result Elam
5.27
Prepared: 11/05/2021 13:13 Analyzed: 11/09/2021 08:32
Spike
Level
0.00500
Source
Result
0.000150 U
%REC RPD
%REC Limits RPD limit Meg_
108
75-125
Prepared: 11/05/2021 13:13 Analyzed: 11/09/2021 08:34
Spike
Level
0.00500
Source
Result %REC
0.000150 U 109
1
%REC RPD
J j RPD Limit Rotes
25
75-125
0.5
Prepared: 11/05/2021 13:13 Analyzed: 11/09/2021 08:36
Spike
P Units Level
0.200
ug/L 4.76
Source
Result %REC
0.0387
110
%REC
Limits
75-125
RPD
RPD Limi
1
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1K05013 - EPA 3005A
1
Blank (1K05013-BLK1)
Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:21
Analvte
Aluminum
Arsenic
Cadmium
Callum
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source
Result ELM Pot units Level Result %REC Limits RPD Limit Notei
0.0420 U 0.100 mg/L
0.00760 11 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0.0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
LCS (1K05013-BS1) Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:28
RPD
Y
Analvte
Aluminum
Arsenic
FINAL
Spike Source
Result MS E0L Units Level Result
2.02 0.100 mg/L 2.00
0.199 0.0100 mg/L 0.200
%REC
%REC irn'
101 80-120
99 80-120
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit bates
Page 5 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1K05013 - EPA 3005A - Continued
LCS(1K05013-BSI) Continued
Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:28
Analvte
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Remit Ma EQL Units Level
0.0202 0.00100 mg/L 0.0200
2.08 0.100 mg/L 2.00
0.198 0.0100 mg/L 0.200
0.201 0.0100 mg/L 0.200
2.02 0.100 rng/L 2.00
0.200 0.0100 mg/L 0.200
0.199 0.0I00 mg/L 0.200
10.1 0.500 mg/L 10.0
0.208 0.0100 mg/L 0.200
10.2 0.500 mg/L 10.0
0.206 0.0100 mg/L 0.200
Source
Result
%REC
%REC Limits RPD
101 80-120
104 80-120
99 80-120
100 80-120
101 80-120
100 80-120
100 80-120
101 80-120
104 80-120
102 80-120
103 80-120
RPD
Limit
Notes
Matrix Spike (1K05013-MS1) Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:31
Source: CE16371-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Fan POI Units Level
2.01 0.100 mg/L 2.00
0.183
0.0194
47.g
0.191
0.197
17.8
0.198
0.196
16.2
0.195
50.9
0.207
0.0100 mg/L 0.200
0.00100 mg/L 0.0200
0.100 mg/L 2.00
0.0100 mg/L 0.200
0,0100 mg/L 0.200
0.100 mg/L 2.00
0.0I00 mg/L 0.200
0.0100 mg/L 0.200
0.500 mg/L 10.0
0.0100 mg/L 0.200
0.500 mg/L 10.0
0.0100 mg/L 0.200
Source
Result
0.0420 U
0.00760 U
0.000360 U
49.5
0.00160 U
0.00310 U
16.9
0.00250 U
0.00242
6.64
0.00620 U
43.7
0.00546
%REC
100
91
97
NR
95
98
47
99
97
96
98
72
101
%REC
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
RPD
RPD Unit Notea.
QM-07
QM-07
QM-07
Matrix Spike Dup (1K05013-MSD1)
Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:38
■
Source:CE16371-01
Analvte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC RPD
Result Flan PQL MAU Level Reza %REC Umit& RPD ilmk !
2,12 0.I00 m9/L 2.00 0.0420 U 106 75-125 6 20
0.190 0.0100 mg/L 0.200 0.00760 U 95 75-125 4 20
0.0198 0.00100 mg/L 0.0200 0.000360 U 99 75-125 2 20
50.2 0.100 mg/L 2.00 49.5 37 75-125 5 20 QM-07
0.195 0.0100 m9/L 0.200 0.00160 U 98 75-125 2 20
0.198 0.0100 mg/L 0.200 0.00310 U 99 75-125 0.5 20
18.9 0.100 mg/L 2.00 16.9 99 75-125 6 20
0.202 0,0100 mg/L 0.200 0.00250 U 101 75-125 2 20
0.199 0.0100 mg/L 0.200 0.00242 98 75-125 2 20
16.6 0.500 mg/L 10.0 6.64 99 75-125 2 20
0.201 0.0100 mg/L 0.200 0.00620 U 101 75-125 3 20
52.7 0.500 mg/L 10.0 43.7 90 75-125 3 20
0.211 0.0100 mg/L 0.200 0.00546 103 75-125 2 20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 14

www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1K05013 - EPA 3005A - Continued
Post Spike (1K05013-PS1)
Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 11:41
1
Source: CE16371-01
_MAMA
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Flan EU Units
2.23 0.100 mg/L
0.208 0.0100 mg/L
0.0212 0.00100 mg/L
51.0 0.100 mg/L
0.209 0.0100 mg/L
0.213 0.0100 mg/L
18.8 0.100 mg/L
0.217 0.0100 mg/L
0.215 0.0100 mg/L
17.5 0.500 mg/L
0.214 0.0100 mg/L
54.1 0.500 mg/L
0.228 0.0100 mg/L
Spike Source %REC
Level Hasa %REG Limits RPD
2.00 0.0122 111 80-120
0,200 -0.0114 104 80-120
0.0200-0.000468 106 80-120
2.00 49.5 75 80-120
0.200 -0.00197 104 80-120
0.200 -0.00254 105 80-120
2.00 16.9 93 80-120
0.200 0.000834 108 80-120
0.200 0.00242 106 80-120
10.0 6.64 109 80-120
0.200 -0.00585 107 80-120
10.0 43.7 104 80-120
0.200 0.00546 111 80-120
RPD
Limit
Nam
QM-08
IassicaI Chemistry Parameters - Quality Control
1
Batch 1K02029 - NO PREP
Blank (1K02029-BLK1)
Prepared: 11/02/2021 15:52 Analyzed: 11/02/2021 17:17
Analvte
Nitrite as N
ILCS(1K02029-BS1)
Analvte
Nitrite as N
Matrix Spike (1K02029-MS1)
Source: CE15893-01
Analtde
Nitrite as N
Matrix Spike (1K02029-MS2)
Source: CE15896-01
Analvte
Nitrite as N
Spike Source
Result I9ao P9L UD1 Level Result %REC Limits
0.017 U 0.10 mg/L
%REC
RPD
Prepared: 11/02/2021 15:52 Analyzed: 11/02/2021 17:40
Spike
Result Elea E01. Units Level
1.0 0.10 mg/L 1.00
Source
Result
RPD
Limit
rInteL
%REC RPD
%REC Lirnits RPD Limit RQtGE
101
90-110
Prepared: 11/02/2021 15:52 Analyzed: 11/02/2021 17:19
Spike Source
ResultFlan P_QL Unila Level Revd%
1.0 0.10 rng/L 1.00 0.048
Result Flan P9L units
1.3
0.10
mg/L
Matrix Spike Dup (1K02029-MSD1)
Source: CE15893-01
Anatvte
Nitrite as N
Batch 1K03014 - NO PREP
%REC
%REC Limlta
95
90-110
RPD
RPD Qimit
Prepared: 11/02/2021 15:52 Analyzed: 11/02/2021 17:22
Spike Source
Level Result
1.00 0.38 96 90-110
%REC
%REC Limits
1
RPD
RPD Limit (rotes
Prepared: 11/02/2021 15:52 Analyzed: 11/02/2021 17:20
Spike Source %REC RPD
Result ERR PILL LlnI Level Result %REC Limits RPD Mmit NQt52-
1.0 0.10 mg/L 1.00 0.048 95 90-110 0.1 10
Blank(1K03014-BLK1)
Prepared &Analyzed: 11/03/2021 13:41
.ARabfig
Resufl Elan P94
Units
Spike Source
Level Result
%REC
%REC Lirnita
RPD
RPD Limit
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 7 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1KO3O14 - NO PREP - Continued
Blank (1K03014-BLK1) Continued
Prepared & Analyzed: 11/03/2021 13:41
&sonde
Biochemical Oxygen Demand
LCS (1K03014-13S1)
Spike Source %REC RPD
Result Flag EQL Units Level Result %REC L zn!ls RPD Limit Notes
2.0 U 2.0 mg/L
Prepared & Analyzed: 11/03/2021 13:41
1
Analvte
Biochemical Oxygen Demand
[Duplicate (1K03014-DUP1)
Source: CE15153-01
Analvte
Biochemical Oxygen Demand
Batch 1KO4O2O - NO PREP
Spike Source
Result Flaq MK. Units Level Rena
180 2.0 mg/L 198
%REC
89
%REC RPD
Limits RPD Limit Notes
85-115
Prepared & Analyzed: 11/03/2021 13:41
Spike Source %REC RPD
Result ElEr P_01. Units Level Result %REC Limits RPD Lia+it
7.3 2.0 mg/L 7.5 2 30
1
Notes
Blank (1K04020-81_K1)
Prepared: 11/04/2021 09:43 Analyzed: 11/04/2021 12:53
Analvte
Ammonia as N
[LCS(1K04020-BS1)
Analvte
Ammonia as N
Matrix Spike (1K04020-MS1)
Source: CE11436-01
_Analvte
Ammonia as N
Matrix Spike (1K04020-MS2)
Source:CE11436-01
Ammonia as N
Matrix Spike Pup (1K04020-MSD1)
ti
Source: CE11436-01
Analvte
Ammonia as N
Batch 1K05011 - NO PREP
Result Flan P41
0.045 U
0.10
Result ELM MI
1.0
0.I0
Result Mau POI
0.52
Result flag
0.41
Spike Source %REC
Units Level Result %REC Limits
mg/L
RPD
RPD Limit !kolas_
Prepared: 11/04/2021 09:43 Analyzed: 11/04/2021 12:55
Spike Source
units Level Result
mg/L 1.01
%REC RPD
%REC Limit& RPD
103
90-110
Prepared: 11/04/2021 09:43 Analyzed: 11/04/2021 12:58
Spike Source
Units Level Butt
0.10 mg/L 0,393 0.17
0.10
Result Flan P01=
0.52
%REC RPD
%REC Limits RPD Lint
91
90-110
Prepared: 11/04/2021 09:43 Analyzed: 11/04/2021 13:07
Spike
Units Level
mg/L
0.393
Source
i;ngult
0.066
%REC
%REC Limits RPD
89
90-110
Prepared: 11/04/2021 09:43 Analyzed: 11/04/2021 13:00
Spike Source
units Level BURR
0.10 mg/L 0.393 0.17
%REC
%REC Llnllt4
89 90-110
RPD
LLmit
i
Kota_
Now£
QM-07
RPD
RPD Limn N.
1 10 QM-07
sank(1K05011-BLK1)
Prepared: 11/05/2021 10:56 Analyzed: 11/05/2021 13:17
Analvte
Nitrate/Nitrite as N
Spike
Result Ftan PQL Units Levet
0.041 U 0.10 mg/L
Source
Emit
%REC
%REC Limita RPD
RPD
LdmSt
IYI
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 14

www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1K05011 - NO PREP - Continued
LCS (1KO5011-B51)
Prepared: 11/05/2021 10:56 Analyzed: 11/05/2021 13:19
1
Analvte
Nitrate/Nitrite as N
Matrix Spike (1K05011-MS1)
Source: CE11319-01
Analvte
Nibate/Nitrite as N
[Matrix Spike (1K05011-M52)
Source: CE15048-01
Analvte
Nitrate/Nitrite as N
[Matrix Matrix Spike Dup (1K05011-MSD1)
Source: CE11319-01
Analvte
Nitrate/Nitrite as N
Batch 1K05013 - EPA 3005A
Spike Source
Result Flan POI Units Level Result
1.2 0.10 mg/L
Result Flan
23
Result Bee
0.55
1.25
%REC
97
%REC
Limits
90-110
RPD
RPD Limit l
Prepared: 11/05/2021 10:56 Analyzed: 11/05/2021 13:22
Spike Source
PA& Uftita Level Result
1.0 mg/L 5,00 18
P
0.10
%REC
%REC Limits
106
90-110
RPD
RPD Limit
Prepared: 11/05/2021 10:56 Analyzed: 11/05/2021 13:28
Spike
tabu Level
mg/L 0.521
Source
RRee,,sult
0.041 U
%REC
%REC Limits
106
90-110
1
RPD
RPD Limit NAM
-
Prepared: 11/05/2021 10:56 Analyzed: 11/05/2021 13:24
Spike Source
Result Flag P01. Units Level Result
23 1.0 mg/L 5.00 18
%REC
%REC Limits
106 90-110
i
RPD
RPD LIBilt Rek.s
0.1 10
Blank (1K05013-BLK1)
Prepared: 11/05/2021 10:56 Analyzed: 11/09/2021 15:56
Acolyte
Sodium Adsorption Ratio
Batch 1K05040 - NO PREP
Result Bag PAL Units
0.00 U [blank]
Spike Source %REC RPD
Level Result %REC Limits RPD LLmiE
N4US-
[Blank (1K05040-BLK1)
Prepared & Analyzed: 11/05/2021 19:00
Anahrte
Total Solids
Spike
Resoit Han P01. Units Level
0.0050 U 0.0050 % by Volume
Source
MEd
%REC RPD
%REC Li►A RPD Limit Nos
[LCS(1K05040-BS1)
.Anand4
Total Solids
Prepared & Analyzed: 11/05/2021 19:00
Spike Source
Result Flag PSOL U.flits Level Result
1100 50 mg/L 1100
%REC RPD
%REC girgta RPD Limit NoteS
104 90-110
Duplicate (1K05040-DUP1)
Prepared & Analyzed: 11/05/2021 19:00
Source: CE16414-01
Anal tie
Total Solids
Batch 11C08008 - NO PREP
NI •
t
Spike Source %REC RPD
Result Flan P_QL units Level MAUR %REC Limits RPD Llnit Notes
0.24 0.0050 % by Volume 0.24 0.8 5
liinimBlank (1K08008-BLK1)
mom
Prepared: 11/08/2021 08:59 Analyzed: 11/08/2021 10:40
.Anand&
Chloride
Spike Source
Result Mao P0L Units Level Beradt %REC Limits RPD Li i Notr
1.9 U 5.0 mg/1-
%REC
RPD
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 14

www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1K08008 - NO PREP - Continued
[LCS(1K08008-BS1)
Prepared: 11/08/2021 08:59 Analyzed: 11/08/2021 10:41
Analxts
Chloride
Result Fla E0.L Units
100
5.0
mg/L
Spike
Level
100
Source
Result
%REC RPD
%REC Li1711 RPD Unlit Reiss_
100
80-120
Duplicate (1K08008-DUPL)
Prepared: 11/08/2021 08:59 Analyzed: 11/08/2021 10:44
Source: CE15686-02
Analvte
Chloride
Result Flan EQ.L
2.9 3
5.0
Spike
Units Level
mg/L
Source
Result
2.6
%REC
RPD
%REC Limits RPD Mad Notes
13 10 OM-12
Matrix Spike (1K06008-MS1)
Prepared: 11/08/2021 08:59 Analyzed: 11/08/2021 10:42
Source: CE15686-01
Analvte
Chloride
Spike
Result Flan P 1. Units Level
48 5.0 mg/L 37.5
Source
Re&u�t
6.8
%REC RPD
%REC Limits RPD Link
111
80-120
L
Matrix Spike Dup (1K0800S-MSD1)
Prepared: 11/08/2021 08:59 Analyzed: 11/08/2021 10:43
Source: CE15686-01
Analvte
Chloride
Batch 11(08021 - Same
Spike Source %REC
Result Etch 201 Units Level Egad %REC Limits
49 5.0 m9/L 37.5 6.8 112 80-120
RPD
RPD unit Lr4t
25
[Blank (1K08021-BLK1)
Prepared: 11/08/2021 13:34 Analyzed: 11/08/2021 16:15
Analvte
Chemical Oxygen Demand
Beeklt alas
10 U
Spike Source
EQL Ut1i Level Result %REC Limits RPD Umst Notes
10 mg/L
%REC
RPD
LCS (1K08021-BS1)
Analvte
Chemical Oxygen Demand
RgrFylt Elan
510
Prepared: 11/08/2021 13:34 Analyzed: 11/08/2021 16:15
Spike Source
EQL Units Level Emit
10
mg/L
500
%REC
102
%REC
Limits
90-110
RPD
RPD Limit Notes
[Matrix Spike (1K08021-MS1)
Source: CE08091-01
Analvte
Chemical Oxygen Demand
Prepared: 11/0B/2021 13:34 Analyzed: 11/08/2021 16:15
Result flag
8300
Spike Source
Unit Level Eesult
mg/L 5000 3600
%REC RPD
%REC RPD Lind Miss_
95
90-110
Matrix Spike Dup (1K08021-MSD1)
Source: CE08091-01
Analvte
Chemical Oxygen Demand
Batch 1K08028 - NO PREP
Prepared: 11/08/2021 13:34 Analyzed: 11/08/2021 16:15
Spike Source
Result Flan E_41 Units Level Result
8100 100 mg/L 5000 3600
%REC
%REC LlmiLt
91 90-110
RPD
RPD Limit Notes
2 5
[Blank (1K08028-BLK1)
Prepared: 11/08/2021 14:23 Analyzed: 11/08/2021 18:00
1
Analvte
Total Suspended Solids
Spike Source
Result Fla 1?01 Un(18 Level Result %REC Limits RPD
2.5 U 2.5 mg/L
%REC
RPD
L+i
RIVAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 10 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1K08028 - NO PREP - Continued
LCS (1K08028-B51)
Prepared: 11/08/2021 14:23 Analyzed: 11/08/2021 18:00
Analvte
Total Suspended Solids
Duplicate (1K08028-DUP1)
Source: CE16569-01
Analvte
Total Suspended Solids
Batch 1K09020 - Same
Result Eau
82
EDI Units
2.5 mg/L
Spike Source
Level Result
100
%REC
82
%REC
Limits
80-120
RPD
RPD mJ
Prepared 11/08/2021 14:23 Analyzed: 11/08/2021 18:00
Spike Source
Result )fig PQ.L Pnits Level Result
1000 62 mg/L 1100
%REC
RPD
%REC j imits RPD Mai
Notes
5 20
Blank (1K09020-BLK1)
Prepared: 11/09/2021 12:54 Analyzed: 11/11/2021 12:13
AR:IMO
Total Kjeldahl Nitrogen
Spike Source %REC RPD
Result Flag PQL Units Level Result %REC Limits RPD Umit .
0.26
u
0.48
mg/L
I,iCS(1K09020-BS1)
Analvte
Toal Kjeldahl Nitrogen
Matrix Spike (1K09020-MS1)
Source: CE15893-01
Analyte
Total Kjeldahl Nitrogen
Matrix Spike (1K09020-MS2)
Prepared: 11/09/2021 12:54 Analyzed: 11/11/2021 12:15
Spike
Result flan R_4.L ilnitE Level
13 0.48 mg/L 12.0
Source
Result
%REC RPD
%REC Lin_tits RPD L!lnit N4tSi
107
90-110
Prepared: 11/09/2021 12:54 Analyzed: 11/11/2021 12:18
Spike
R _suit flag P.OL Units Level
14 0 0.96 mg/L 4.80
Source
cult
9.0
%REC
%REC n It6
105
90-110
RPD
RPD Malt Nell
Prepared: 11/09/2021 12:54 Analyzed: 11/11/2021 12:24
1
Source: CE15898-01
Analvte
Total Kjeldahl Nitrogen
Matrix Spike Dup (1K09020-MSD1)
Source: CE15893-01
Analvte
Total Kjeldahl Nitrogen
Batch 1K09024 - Same
Spike
Rujt Flag POI Units Level
13 0.48 mg/L 4,80
Source
5.4
%REC RPD
%REC Limits RPD Lim!t
151
90-110
Prepared: 11/09/2021 12:54 Analyzed: 11/11/2021 12:20
Spike Source
Result floe PQL goats Level $ego
13 0 0.96 mg/L 4.80 9.0
%REC
%REC Maurits
81 90-110
RPD
RPD Lhulf
8 10
N
QM-07
NAIL
QM-07
Blank (11109024-BLK1)
Prepared: 11/09/2021 15:00 Analyzed: 11/15/2021 14:22
-I
linsibrtle
Phosphorus
1,LCS(1K09024-BS1)
.Anaiidre
Phosphorus
Spike Source
Result Elan PQL Units Level Result
0.025 U 0.10 mg/L
%REC
%REC Limits
RPD
RPD Limit N412:1.
Prepared: 11/09/2021 15:00 Analyzed: 11/15/2021 14:23
Spike Source %REC
Result flag PQL Units Level Roll %REC Limits
1.5 0.10 mg/L 1.60 93 80-120
RPD
RPD Limit iiQtos_
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1K09024 - Same - Continued
Matrix Spike (1K09024-MS1)
Prepared: 11/09/2021 15:00 Analyzed: 11/15/2021 14:26
Source:CE15893-01
Analvte
Phosphorus
Result flag POL
9.8 0
1.0
Units
mg/L
Spike Source
Level Result
0.640
9.0
%REC RPD
%REC Limas RPD 'mit Nate.
118
80-120
Matrix Spike Dup (1K09024-MSD1)
Source: CE15893-01
Analvte
Phosphorus
Prepared: 11/09/2021 15:00 Analyzed: 11/15/2021 14:27
Spike Source
Result Han MI ilnila Level Result
9.0 0 1.0 mg/L 0.640 9.0
1
%REC RPD
%REC imf RPD Limit NOD_
0.6 80-120 8 25 QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
s The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
• The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL; Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALL] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory. and may only be reproduced in full. Page 13 of 34

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
10775 Centel Pon Dr 4810 Executive Perk Court, Suit, 111
Orlando FL 32624 Jecksronveia FL 32210-6069
(407t 626.5314 •
(9041 24630b7 Fax [phone],8210
102-A WoOdwmda Industrial CI
Gary NC 27511
(919t4673090 Fax [phone]
CI t ame
cn+ozymes North America (N0008)
ProfnNu
on
Adtllri Perry Chapel Church Road
Pa Irithii - Week One - SBM
TrsnMinton, NC 27525
Po ell 49D5
Requested Analyses
Tel [phone]
Fax
5ampat(si Name Affklabas (Pmq
E/ki 4 44(/; "7fvr✓
Semp*1I) St9rwture
t
Item s
Sample ID (Fast Idenbrtcallxt
m
BIL "wets Payable
Site Location 1 Time Zone
BOD SM5210B
z
i
t.,
COD SM5220D
TSS SM2540D
Collection Date
CtNeclwn
Time
Comp f Grab
Matrix Total 8 of
+see cods Contatners
Prase
rvatlon ISee Coded ICArbr
no as Waco
SSalyI
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Page of
Requested Turnaround
Times
Note Rush requests subject to
acceptance by the facility
Standard
Expedited
Due / /
Lab Workorder
CE115
Sample Comments
Ili
iv: 90
6-
SL 7
Sample K+1 Prepared By Osto.Tme
ZD (
Comments/SpecialRsquhemants
iiehnquWwtl By
Relancsiated By
Relinquished By
Coder s'e & Temps on Receipt
<•- Total # at Containers
Dale/Time
Jl 2 -.2/ )
Det&Tene
Datalrims
Recea.d By� fIL
R By
Awaked By
CgLWllsyrs Upon Receipt
Acceptable
Matrix. GW-Groundwater 90-Sod DW.Drinkmg Water SE-Sedlmant SW -Surface Water WW-Wastewater A -Air 0.Other Idetad rn comments) Preservetfon: I -Ice H-HCI N-1-1NO3 5 H2SO4 NO-NiOH 401her fdetal in comments)
Note AN samples submitted m ENCO Labs ere in accordance with the terms and conditions listed on the reverse of this form, unless Pnor written agreements exist
Ieo0
Dols/rim.
!r -� 7/
Daalrrrna
•
Det&rsns
Unacceptable

Sample Preservation Verification
ENCO Cary
Work Order CE16415
Client Novozymes North America (N0006)
Logged In 02-Nov-21 10.57
Preservation Check Performed By*
r
Project.
Project #:
Logged By
Monthly - Week One - StIM
[none]
Samantha L Hyatt j�j�
Date/Time* 1 1
CE16415-01
Cant
D
Type
250mLP+H2504
E 250mLP+HNO3
Pres (pH}
Requirement
<2
<2
pH Checked /
In Control
N/N
YiN/N
pH Adjusted
Y N / NAitizi [ L((L
A
Y N / NA
Date/Time
Adiusted
Reagent Used/Comments
1 32
Reagent Name
2
ID Reagent Name
pH Strip ID' /0
C•IELMNTIPrintlwko_PreservationCheck.rpt
3
4
ID
5
6
Reagent Name iD
Page " of

ENCO Laboratorks
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, December 29, 2021
Novozymes North America (N000S)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CE18640
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, December 8, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted,
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
if you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
/Lef, eost_teh
Bill Scott For Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the I boratc-y, and may only be reproduced In full.
I Page 1 of 15 1

SAMPLE SUMMARY/LABORATORY CHRONICLE
1
Client ID: SBM
Parameter prenaratlon
CSU Method EPA 3005A
EPA 350.1 NO PREP
EPA 351.2 Same
EPA 353.2 NO PREP
EPA 353.2 [CALL]
EPA 353.2 NO PREP
EPA 6010D EPA 3005A
EPA 7470A EPA 245.1
SM 25408-2011 NO PREP
SM 2540D-2011 NO PREP
SM 45000 E-2011 NO PREP
SM 5210 B-2011 NO PREP
SM 5220D-2011 Same
Lab ID: CE18640-01
Hold Date/Timefs)
09/02/24
01/05/22
01/05/22
12/10/21 07:50
12/10/21 07:50
01/05/22
06/06/22
01/05/22
12/15/21
12/15/21
01/05/22
12/10/21 07:50
01/05/22
www.encolabs.com
Sampled: 12/08/21 07:50 Received: 12/08/21 09:00
Prep Date/Time(s)
12/09/21 06:53
12/16/21 06:38
12/20/21 13:10
12/08/21 15:51
12/20/21 10:21
12/20/21
12/09/21
12/14/21
12/14/21
12/14/21
12/08/21
12/09/21
12/09/21
10:21
06:53
07:57
17:00
18:42
13:34
14:02
12:05
Analysis Date/Times)
12/10/21 16:35
12/16/21 09:36
12/21/21 13:08
12/08/21 17:06
12/20/21 17:31
12/20/21 17:31
12/10/21 15:11
12/15/21 09:54
12/14/21 17:00
12/14/21 18:42
12/08/21 15:10
12/09/21 14:02
12/10/21 12:05
Client ID: SBM Lab ID: CE18640-01RE1
Parameter Preparation Mold Date/Time(S1
EPA 365.4 Same 01/05/22
Sampled: 12/08/21 07:50 Received: 12/08/21 09:00
PreD Date/Time(s) Analysis Date/Times)
12/20/21 13:21 12/27/21 17:14
FINAL This report relates only to the sample as received by the laboratory. and may only be reproduced in full.
Page2of15 I

&What
Phosphorus - Total
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: SBM
Analvte
Aluminum - Total
Ammonia as N
Biochemical Oxygen Demand
Calcium - Total
Chemical Oxygen Demand
Chloride
Magnesium - Total
Nitrate as N
Nitrate/Nitrite as N
Nitrite as N
Potassium - Total
Sodium - Total
Sodium Adsorption Ratio
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Lab ID: CE38640-01
Results Egg
6.34
75
4300
2210
23000
430
1.39
8.6
8.7
0.058
394
265
1.55
330
4.1
14000
MDL
0.420
❑ 4.0
2.0
0.390
B00
D 9.5
0.290
❑ 0.41
❑ 0.41
] 0.017
1,50
4.00
FLQL
nits
1.00 mg/L
9.0 mg/L
2.0 mg/L
1.00 mg/L
800 mg/L
25 mg/L
1.00 mg/L
1.0 mg/L
1.0 mg/L
0.10 mg/L
5.00 mg/L
5.00 rng/L
[blank]
D 26 48 mg/L
0.12 0.12 % by Volume
500 500 mg/L
Client ID: SBM Lab ID: CE18640-01REE
Results Elsa !"19b 114.L. Units Method Notes
260 D 25 100 mg/L EPA 365.4
Method
EPA 6010D
EPA 350.1
SM 5210 B-2011
EPA 6010D
SM 5220D-2011
SM 4500CI E-2011
EPA 6010D
EPA 353.2
EPA 353.2
EPA 353.2
EPA 6010D
EPA 6010D
CSU Method
EPA 351.2
SM 2540B-2011
SM 25400-2011
Notes
FINAL This report relates only to the sample as received by the laboratory, and may c r'::r: rep•odu: 1 in Full.
I Page3of15

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM
Matrix: Sludge
Project: Monthly - Week One - SBM
Lab Sample ID:CE18640-01
Sampled:12/08/2 1 07:50
Sampled By: Elbert Alston
Received: 12/0B/21 09:00
Work Order CE18640
Metals by EPA 6000/7000 Series Methods
- ENCO Cary centered analyte [MC 591]
Analvte ',CAS Numberl
Mercury [7439-97-6]^
Results Flag
0.000150 U
YAM
mg/L
W. M L P_Qb 68trh
1 0.000150 0.000200 1L14003
Method
EPA 7970A
Analyzed Bx Mtn
12/15/21 09:54 CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte INC 591]
Analvte ',CASNumberl Results En SJDi PE ROL M. [fetch Meting Malaticed
Aluminum [7429-90-5]^ 6.34 mg/L 10 0.420 1.00 1L09001 EPA 6010D 12/10/21 15:11
Arsenic[7440.38-2]^ 0,0760 U mg/L 10 0.0760 0.100 1L09001 EPA 6010D 12/10/21 15:11
Cadmium [7490-43-9]^ 0.00360 U mg/L 10 0.00360 0.0100 1L09001 EPA 6010D 12/10/21 15:11
Calcium [7440-70-2]^ 2210 mg/1 10 0.390 1.00 1L09001 EPA 6010D 12/10/21 15:11
Copper[7440.50.81^ 0.0160 U mg/L 10 0.0160 0.100 1L09001 EPA 6010D 12/10/21 15:11
Lead [7439-92.1]^ 0.0310 U mg/L 10 0.0310 0.100 1109001 EPA 60101) 12/10/21 15:11
Magnesium [7439-95-4]" 1.39 mg/L 10 0.290 1.00 1L09001 EPA 60100 12/10/21 15:11
Molybdenum [7439-98-7]^ 0.0250 U mg/L 10 0.0250 0.100 1L09001 EPA 6010D 12/10/21 15:11
Nickel[7440.02-0]^ 0.0220 U m9/L 10 0.0220 0.100 1L09001 EPA 6010D 12/10/21 15:11
Potassium [7440-09-7]^ 394 mg/L 10 1.50 5.00 1L09001 EPA 6010D 12/10/21 15:11
Selenium [7782-49-2]^ 0.0620 U mg/L 10 0.0620 0.100 1L09001 EPA 6010D 12/10/21 15:11
Sodium [7440-23-5]^ 265 mg/L 10 4.00 5.00 1L09001 EPA 6010D 12/10/21 15:11
Zinc [7940-66-61^ 0.0440 U mg/L 10 0.0440 0.100 1L09001 EPA 6010D 12/10/21 15:11
Classical Chemistry Parameters _ .1
. . _______
MY Notes
]DH
]DH
JDH
JDH
JDH
JDH
JDH
JDH
JDH
JDH
]DH
JDH
JDH
^ - ENCO Cary certified analyte[NC 591]
Analvte [CAS Numberl gesults nag Mgit2 PE BPI POL Bash =bed Baelned la =ea
Ammonia as N [7664-41-71^ 75 D mg/L 90 4.0 9.0 1L16004 EPA 350.1 12/16/21 09:36 JAH
Biochemical Oxygen Demand^ 4300 mg/L 1 2.0 2.0 1L09024 SM 5210 13-2011 12/09/21 14:02 JOC
Chemical Oxygen Demand^ 23000 mg/L 80 800 B00 1L09035 SM 5220D-2011 12/10/21 12:05 JOC
Chloride [16887-00-6]^ 430 D mg/L 5 9.5 25 IL08031 SM 4500CI E-2011 12/08/21 15:10 JAH
Nitrate as N [14797-55-8] 8.6 D mg/L 10 0.41 1.0 [CALC] EPA 353.2 12/20/21 17:31 JAH
Nitrate/Nitrite as N" 8.7 D mg/L 10 0.41 1.0 1L20014 EPA 353.2 12/20/21 17:31 ]AH
Nitrite as N [14797-65-0]^ 0.058 ] mg/L I 0.017 0.10 1L08037 EPA 353.2 12/08/21 17:06 IAH
Phosphorus[7723-14-01^ 260 D mg/L 1000 25 100 1L20029 EPA 365.4 12/27/21 17:14 JAH
Sodium Adsorption Ratio 1.55 [blank] 1 1L09001 CSU Method 12/10/21 16:35 3DH
Total Kjeldahl Nitrogen" 33D D mg/L 100 26 48 1L20028 EPA 351.2 12/21/21 13:08 JAH
Total Solids^ 4.1 % by Volume 25 0.12 0.12 1L14011 SM 2540B-2011 12/14/21 17:00 DM]
Total Suspended Solids^ 14000 mg/L 200 500 500 1L14010 SM 2540D-2011 12/14/21 18:42 DM]
FINAL This report relates only to the sample as rep _ by the laboratory, and may only be reproduced In full.
Page 4 of 15

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1L14003 - EPA 243.1
Blank(1114003-BLK1)
Prepared: 12/14/2021 07:57 Analyzed: 12/15/2021 08:41
Y
Analvte
Mercury
LCS (1L14003-BS1)
.Analvte
Mercury
Spike Source
Result pSao P01. Units Level Result %REC Limits RPD Mad Notes
0.000150 U 0.000200 mg/L
Result Bag POL.
0.00530 0.000200
Units
mg/L
%REG
Prepared: 12/14/2021 07:57 Analyzed: 12/15/2021 08:45
Spike Source %REC
Level Result %REC Limits
0.00500
106
80-120
RPD
RPD
RPD 'mit
Matrix Spike (1L14003-MS1)
Prepared: 12/14/2021 07:57 Analyzed: 12/15/2021 08:47
Source: CE18272-05
Analvte
Mercury
Spike Source %REC
Fjm P0L Units Level Result %REC Limits RPD
0.00515 0.000200 mg/L 0.00500 0.000150 U 103
75-125
RPD
Limit
Matrix Spike Dup (1L14003-MS131)
Source: CE18272-05
Anafvee
Mercury
Post Spike (1L14003-P51)
Source: CE18272-05
Analvte
Mercury
Result flan P.M. Units
0.00532 0.000200 mg/L
Prepared: 12/14/2021 07:57 Analyzed: 12/15/2021 08:49
Spike Source
Result %REC Limits
Level
0.00500 0.000150 U 106
%REC
75-125
RPD
3
Prepared: 12/14/2021 07:57 Analyzed: 12/15/2021 08:52
Spike
ftsult BBB E01. Units Level
5.48 0.200 ug/L
4.76
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1L09001 - EPA 3005A
Source
Result
0.00581
%REC
%REC Limits
115
75-125
RPD
Limit
25
RPD
RPD Limit
1
Notes
1
Blank (1L09001-BLK1)
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:37
Anatito
Aluminum
Arsenic
Cadmium
Calcium
Capper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Znc
Spike Source
Re tit Else PQ1 Units Level Result %REC Limits RPD ljmit 1
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00286 3 0.0100 mg/L
0.00310 U 0,0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 mg/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
%REC
RPD
l
Blank (1L09001-8LK2) Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:42
•
1
Analvte
Aluminum
Arsenic
FINAL
Spike Source
Result Tian P.M WILE Level Result %REC Liml s
0.0420 U 0.100 mg/L
0.00760 U 0.0100 mg/L
This report relates only to the sample es received by the laboratory, and may only be reproduced In full.
%REC
RPD
RPD limit Notes
Page 5 of 15

Luc
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1L09001- EPA 3005A - Continued
Blank (1L09001-B1.K2) Continued
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:92
Made
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result Flan P.M. Units
0.000360 U 0.00100 mg/L
0.0390 U 0.100 mg/L
0.00160 U 0.0100 mg/L
0.00310 U 0,0100 mg/L
0.0290 U 0.100 mg/L
0.00250 U 0.0100 m9/L
0.00220 U 0.0100 mg/L
0.150 U 0.500 mg/L
0.00620 U 0.0100 mg/L
0.400 U 0.500 mg/L
0.00440 U 0.0100 mg/L
Spike Source
Level Result %REC Limits RPD Limit Mira
REC
RPD
[LCS(1L09001-BS1)
Anaivte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:47
Result Flag £LL Units
1.90 0.100 mg/L
0.190 0.0100 mg/L
0.0199 0.00100 mg/L
2.07 0100 mg/L
0.189 B 0.0100 mg/L
0.194 0.0100 mg/L
1.93 0.100 mg/L
0.191 0.0100 mg/L
0.198 0.0100 mg/L
10.0 0.500 mg/L
0.209 0.0I00 mg/L
9.98 0.500 mg/L
0.202 0,0100 mg/L
Spike
Level
2.00
0.200
0.0200
2.00
0.200
0.200
2.00
0.200
0.200
10.0
0.200
10.0
0.200
Source
Head
%REC
95
95
99
104
95
97
97
95
99
100
105
100
141
%REC
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
RPD
RPD Limit
Notes
Matrix Spike (1L09001-MSI) Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:49
1
Source: CE19014-01
6RaMe
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REC
Result Flan PI1 Units Level Result %REC Limits
3.48 0.100 mg/L 2.00 1.23 112 75-125
0.193 0,0100 mg/L 0.200 0.00760 U 96 75-125
0.0192 0.00100 mg/L 0.0200 0.000407 94 75-125
7.11 0.100 mg/L 2.00 5.31 90 75-125
0.189 B 0.0100 mg/L 0.200 0.00293 93 75-125
0.202 0,0100 mg/L 0.200 0.00601 98 75-125
3.13 0.100 mg/L 2.00 1.25 94 75-125
0.195 0.0100 mg/L 0.200 0.00250 U 97 75-125
0.197 0.0100 mg/L 0.200 0.00473 96 75-125
12.8 0.500 mg/L 10.0 2.98 98 75-125
0.196 0.0100 mg/L 0.200 0.00620 U 98 75-125
13.6 0.500 mg/L 10.0 3.85 97 75-125
0.203 0.0100 mg/L 0.200 0.0102 97 75-125
RPD
RPD Limit MARL
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in NIL
Page 6 of 15

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QUALTTY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1L09001 - EPA 3005A - Continued
Matrix Spike (11.09001-MS2)
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 14:29
Source:CE19014-02
Analute
Aluminum
Arsenic
Cadmium
Calcium
CoPPer
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Result
8.21
0.186
0.0184
7.17
0.190
0.190
4.78
0.174
0.203
12.5
0.181
18.2
0.238
Spike
Elan P0L Units Level
0.100 mg/L 2.00
0.0100 mg/L 0,200
0,00100 mg/L 0.0200
0.100 mg/L 2.00
B 0.0100 mg/L 0.200
0.0100 mg/L 0,200
0.100 mg/L 2.00
0.0100 mg/L 0.200
0.0100 mg/L 0.200
0.500 mg/L 10.0
0.0100 mg/L 0.200
0.500 mg/L 10.0
0.0100 mg/L 0.200
Source %REC
Result %REC Limits RPD
6.30 96 75-125
0.0127 87 75-125
0.000689 89 75-125
5,55 81 75-125
0.0216 84 75-125
0.0117 89 75-125
3.16 81 75-125
0.00250 U 87 75-125
0.0193 92 75-125
4.08 85 75-125
0.00620 U 91 75-125
9.73 85 75-125
0.0568 90 75.125
Matrix Spike Dup (1L09001-MSD1) Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:52
Source: CE19014-01
Anaildte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike
Result Fise PQL Units Level
3.71 0.100 mg/L 2.00
0.192 0.0100 mg/L 0.200
0.0196 0.00100 mg/L 0.0200
7.05 0.100 mg/L 2.00
0.187 B 0.0100 mg/L 0.200
0.198 0.0100 m9/L 0.200
3.16 0.100 mg/L 2.00
0.188 0.0100 mg/L 0.200
0.202 0.0100 mg/L 0.200
12.6 0.500 mg/L 10.0
0.192 0.0100 mg/L 0,200
13.3 0.500 mg/L 10.0
0.209 0.0100 mg/L 0.200
Source
Beta
1.23
0.00760 U
0.000407
5.31
0.00293
0,00601
1.25
0.00250 U
0.00473
2.98
0.00620 U
3.85
0.0102
%REC
124
96
96
87
92
96
95
94
99
96
96
95
100
%REG
Lim&
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75.125
RPD
Limit
RPD
RPD ini
6 20
0.5
2
0.8
1
2
0.8
3
2
1
2
2
3
20
20
20
20
20
20
20
20
20
20
20
20
ojidutL
Post Spike (1L09001-PS1) Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 13:54
Source: CE19014-01
Analyte
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Spike Source %REG
Result Flag PRL Units Level Result %REC Clang
3.23 0.100 mg/L 2.00 1.23 100 80-120
0.205 0.0100 m9/L 0,200 -0.000636 102 80-120
0.0209 0.00100 mg/L 0.0200 0.000407 103 80-120
7.43 0.100 mg/L 2.00 5.31 106 80.120
0.198 B 0.0100 mg/L 0.200 0.00293 97 80-120
0.210 0.0100 mg/L 0.200 0.00601 102 80-120
3.28 0.100 mg/L 2.00 1.25 101 80-120
0.200 0.0100 mg/L 0.200 0.000435 100 80-120
0.217 0.0100 mg/L 0.200 0.00473 106 80-120
13.3 0.500 mg/L 10.0 2.98 103 80-120
0.206 0.0100 mg/L 0.200-0.000338 103 80-120
14.1 0.500 mg/L 10.0 3.85 102 80-120
0.223 0.0100 mg/L 0,200 0.0102 107 80-120
RPD
RPD I.Lt
Classical Chemistry Parameters - Quality Control
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
71 age 7 of 15

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QUALITY CONTROL DATA
!Classical Chemistry Parameters - Quality Cont''^
Batch 1L08031 - NO PREP
Blank (1L08031-BLK1)
Analvte
Chloride
Result
1.9
1
Prepared: 12/08/2021 13:34 Analyzed: 12/08/2021 15:02
Spike Source %REC RPD
P01 MI Level Result %REC Limits RPD Limit
5.0
mg/L
ILCS(1L08031-BS1)
Prepared: 12/08/2021 13:34 Analyzed: 12/08/2021 15:03
_Ma d&
Chloride
Result BAR
100
EDI
5.0
Ul>ll
mg/L
Spike
Level
100
Source
Result
%REC
%REC Limits
105
80-120
RPD
RPD Limit Notes_
[Duplicate (1L08031-DUP1)
Prepared: I2/08/2021 13:34 Analyzed: 12/08/2021 15:06
Source: CE16609-02
Analvte
Chloride
Result Flan
15
Spike Source
P9L Units Level $g rllt
5.0 mg/L
15
%REC
%REC Limits RPD
6
Matrix Spike (1L08031-MS1)
Prepared: 12/08/2021 13:34 Analyzed: 12/08/2021 15:05
Source: CE16609-01
_Analvte
Chloride
Result Elan
72
P01 Units
5.0 mg/L
Spike
Level
37.5
Source
Result
29
%REC
%REC LJm1ts RPD
113
80-120
RPD
Limit
10
RPD
Unlit
gates
[Matrix Spike Dup (1L08031-MSD1)
Prepared: 12/08/2021 13:34 Analyzed: 12/08/2021 15:05
Source:CE16609-01
Analvte
Chloride
Batch 1L08037 - NO PREP
Spike Source %REC
Resu flag P01. Units Level Result %REC Limhe
73 5.0 mg/L 37.5 29 115 80-120
RPD
RPD Limit
25
Blank (1L08037-BLK1)
Prepared: 12/08/2021 15:51 Analyzed: 12/08/2021 16:59
_Analvte
Nitrite as N
Result MAO
U
0.017
Spike Source
PDI. Units Level Result
0.10 mg/L
%REC
RPD
%REC Limits RPD Limit Notes
LCS(1L08037-651)
Prepared: 12/08/2021 15:51 Analyzed: 12/08/2021 17:11
Analvte
Nitrite as N
Result
0.97
Spike Source
Flag EOL DOA Level Re@ult
0.10 mg/L
1.00
%REC
97
%REC RPD
Limits RPD Limit Notes
90-110
(Matrix Spike (1L08037-MS1)
Source: CE18635-04
_Malady
Nitrite as N
Prepared: 12/08/2021 15:51 Analyzed: 12/08/2021 17:01
Spike
Result Flag POL Units Level
1.0 0.10 mg/L
1.00
Source
Result
0,029
%REC RPD
%REC Limits RPD limit MIL
97
90-110
Matrix Spike Dup (1L08037-MSDL)
Prepared: 12/08/2021 15:51 Analyzed: 12/08/2021 17:02
Source: CE18635-04
Nitrite as N
Batch 1L09001 - EPA 3005A
Spike Source %REC RPD
!result Flag EQ4 U0its Level Rem& %REC Limits RPD Lima IY4
1.0 0.10 mg/L 1.00 0.029 99 90-110 2 10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 15

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QUALITY CONTROL DATA
[Classical Chemistry Parameters - Quality Control
Y
Batch 1L09001 - EPA 3005A - Continued
[Blank(1L09001-BLK1)
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 16:35
Analvte
Sodium Adsorption Ratio
Result Etas
0.00 U
PQL
MIMS
[blank]
Spike Source
Level Result
%REC
%REC (:hilts
RPD
RPD
t Motes
Blank (1L09001-BLK2)
Prepared: 12/09/2021 06:53 Analyzed: 12/10/2021 16:35
Analvte
Sodium Adsorption Ratio
Batch 1L09024 - NO PREP
Result Flag
0.00 U
P94 Units
[blank)
Spike Source
Level Result
%REC
%REC Limits
RPD
RPD
MBA dotes
Blank (1L09024-BLK1)
Prepared & Analyzed: 12/09/2021 14:02
Analvte
Biochemical Oxygen Demand
Result Flax POI
2.0 U
units
2.0 mg/L
Spike Source
Result %REC
Lave!
%REC
ittL_fit2 RPD
RPD
llll]]L Mat
ILCS(1109024-BS1)
Prepared & Analyzed: 12/09/2021 14:02
Analvte
Biochemical Oxygen Demand
moult Flag
210
Spike
P41 units Level
2.0
mg/L
198
Source
AMR
%REC
%REC Limits RPD
105
85-115
Duplicate (1L09024-DUP1)
Prepared & Analyzed: 12/09/2021 19:02
Source: CE18341-01
Analyte
Biochemical Oxygen Demand
Batch 1L09035 - Same
Result f g
4.8
Spike
P41. Smile Level
2.0 mg/L
Source
Result
5.3
%REC
%REC Limits
RPD
Mai Nam
RPD
RPD Limit
10 30
L
Blank (1L09035-BLK1)
Prepared: 12/09/2021 12:05 Analyzed: 12/10/2021 12:05
Analvte
Chemita1 Oxygen Demand
Result flae
10 U
10
Units
mg/L
Spike Source
Level Result
%REC
%REC Limits RPD
RPD
Unit
Motes
LCS(1L09035-B51)
Prepared: 12/09/2021 12:05 Analyzed: 12/10/2021 12:05
Analvte
Chemical Oxygen Demand
Result Flag
510
Spike
PQL Units Level
10
mg/L
500
Source
%REC
%REG Limits RPD
102
90.110
l
Matrix Splice (1109035-MS1)
Prepared: 12/09/2021 12:05 Analyzed: 12/10/2021 12:05
Source: CE12272-01
Analvte
Chemical Oxygen Demand
Result lea
820
Spike
PQL !!oils Level
10
mg/L
526
Source
RIAERR
290
%REC
%REC Lin3it£ RPD
101
90-110
RPD
Limit
RPD
Limit
MIL
Rai
1.
Matrix Spike Dup (iL09035-MSD1)
Prepared: 12/09/2021 12:05 Analyzed: 12/10/2021 12:05
Source: CE12272-01
_AMMO
Chemical Oxygen Demand
Batch 1L14010 - NO PREP
Result Flag
820
Spike
PQL that; Level
10 mg/L
Source
Result
526 290
%REC
%REC limits RPD
101 90.110 0
RPD
5
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in fun.
Page 9 Of 15

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
1
Batch 1114010 - NO PREP - Continued
Blank(1L14010-BLK1)
Prepared & Analyzed: 12/14/2021 18:42
1
Analvte
Total Suspended Solids
Result Flag
2.5 U
Spike Source
POL Units Level EntilLt %REC Limits RPD Limit Notes
2.5 mg/L
%REC
RPD
LCS (1L14010-BS1)
Analvte
Total Suspended Solids
Result Elan £QL
93
2.5
Units
mg/L
Prepared & Analyzed: 12/14/2021 18:42
Spike
Level
100
Source
Result
%REC
93
1
%REC RPD
Limits RPD -mi NQF -
80-120
Duplicate (1L14010-DUP1)
Prepared &Analyzed: 12/14/2021 18:42
Source: CE16675-01
Analvte
Total Suspended Solids
Result Elan PQL
790
120
rUA.s
mg/L
Spike Source
Level Result
2100
%REG
%REC Limits RPD
90
RPD
20
NoteI,
QM-12
Duplicate (1L14010-DUP2)
Prepared & Analyzed: 12/14/2021 18:42
■
Source: CE14715-02
Analvte
Total Suspended Solids
Batch 1L14011 - NO PREP
Spike Source
Result Elan P_9I. Units Level Result
82 25 mg/L 79
%REC RPD
%REC Limits RPD Limit Natal.
4 20
l Blank (1L14011-BLK1)
Prepared &Analyzed: 12/14/2021 17:00
1
Analvte
Total Solids
Spike Source
Result flan PAL Units Level Result %REC Limits RPD
0.0050
U 0.0050 % by Volume
%REC
RPD
Limit Notes
LCS (1L14011-BS1)
Anable
Total Solids
Prepared & Analyzed: 12/14/2021 17:00
Result
1000
Spike
Elasi PQL Units Level
50
mg/L
1100
Source
Result
%REC RPD
%REC Limits RPD Unlit WAAL
94
90-110
Duplicate (1L14011-DUP1)
Prepared & Analyzed: 12/14/2021 17:00
1
Source: CE15936-01
Ana M
Total solids
Batch 1L16004 - NO PREP
Result Elan
0.29
Spike
PQL Units Level
0.0050 46 by Volume
Source
Rne..A
0.28
%REC
RPD
%REC Limits RPD Limit NOte3
1
5
Blank (1L16004-BLK1)
Prepared: 12/16/2021 06:38 Analyzed: 12/16/2021 08:54
1
Analvte
Ammonia as N
Result Elea
0.045 U
ROL
0.10
Units
mg/L
Spike Source %REC
Result %REC Limits
Level
RPD
RPD Limit
Notes.
LCS (1L16004-BS1)
Analvte
Ammonia as N
Prepared: 12/16/2021 06:38 Analyzed: 12/16/2021 08:56
Spike
Result Elan PQL Units Level
0.99 0.10 mg/L 1.01
Source
MEd
%REC
%REC Limits RPD
98 90-110
1
RPD
L At ROLM.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fWi.
Page 10 of 15

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 1L16004 - NO PREP - Continued
Matrix Spike (1L16004-MS1)
Prepared: 12/16/2021 06:38 Analyzed: 12/16/2021 08:59
1
Source: CE18340-01
iulakte
Ammonia as N
Result Elm;
0.56
PL
0.10
Molts
mg/L
Spike
Level
0.393
Source
Result
0.22
%REC RPD
%REC Limits RPD Limit Notes
86
90-110
QM-07
[Matrix Spike (1116004-MS2)
Source: CE18343-01
na
Ammonia as N
Prepared: 12/16/2021 06:38 Analyzed: 12/16/2021 09:04
Result Bea EDI
0.33
0.10
VMS
mg/L
Spike Source
Level Result
0.393
0.04511
%REC
84
%REC
Limits
90-110
RPD
RPD im'
QM-07
Matrix Spike Dup (1L16004-MSD1)
Prepared: 12/16/2021 06:38 Analyzed: 12/16/2021 09:01
Source: CE18340-01
Analvte
Ammonia as N
Batch 1L20014 - NO PREP
Spike Source %REC RPD
Result Sag P_QI- 1U_fiU Level Result WaR£C !jag RPD t
0.57 0.10 mg/L 0.393 0.22 90 90-110 3 10
Blank (1120014-BLK1)
Prepared: 12/20/2021 10:21 Analyzed: 12/20/2021 16:50
1
Analvte
Nitrate/Nitrite as N
Result
0.041
Flan
u
Spike
?QL Units Level
0.10
mg/L
Source
Result
%REC
%REC Limits RPD
RPD
Limit Rates
[LCS (1L20014-BS1)
Analvte
Nitrate/Nitrite as N
Prepared: 12/20/2021 10:21 Analyzed: 12/20/2021 16:52
Y
Result fl q
1.4
EQL Units
mg/L
0.10
Spike Source
Level Rn811t
1.25
%REC
110
%REC
MBAS
90-110
RPD
RPD Qat
Matrix Spike (1120014-MS1)
Source: CE16854-02RE2
Analvte
Nitrate/Nitrite as N
Result Elan P41
19
0.10
Linits
mg/L
1
Matrix Spike (1L20014-MS2)
Source: CE16862-01
Anahrte
Nitrate/Nitrite as N
Prepared: 12/20/2021 10:21 Analyzed: 12/20/2021 16:55
Spike Source
Level Result
0,521
19
%REC RPD
%REC Unite RPD Limit
46
90-110
1
Ram
QM-07
Prepared: 12/20/2021 10:21 Analyzed: 12/20/2021 17:01
room
Spike
Result Elan PQL units Level
1.2
0.10
mg/L
0,521
Source
Result
0.72
%REC
%REC Limits
94
90-110
RPD
RPD Limit
1
[Matrix Spike Dup (1L20014-MSD1)
Source: CE16854-02RE2
Ana6de
Nitrate/Nitrite as N
Hatch 1L20028 - Same
Prepared: 12/20/2021 10:21 Analyzed: 12/20/2021 16:57
Spike Source %REC
Result Flea Pot. Units Level Result %REC Limits
19 0.10 m9/L 0.521 19 29 90-110 0.5 10
RPD
RPD Limit
1
QM-07
Blank (1120028-B1.K1)
Prepared: 12/20/2021 13:10 Analyzed: 12/21/2021 12:21
1
Anitty
Total Kjeldahl Nitrogen
Spike
Result 17;1St EQL Units Level
0.26 U 0.48 mg/L
Source
%REC
RPD
%REC Limits RPD Limit Note
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 15 I

www.encolabs.Com
QUALITY CONTROL DATA
(Classical Chemistry Parameters - Quality Cor"nl
Batch 1L20028 - Same - Continued
LCS (1120028-BS1)
Prepared: 12/20/2021 13:10 Analyzed: 12/21/2021 12:23
Analvte
Total Kjeldahl Nitrogen
Matrix Spike (1L20028-MS1)
Source: CE14845-01
Analvte
Tobi Kjeldahl Nitrogen
[Matrix Spike (1L20028-MS2)
Source: CE16692-01
Analvte
Total Kjeldahl Nitrogen
Matrix Spike Dup (1120028-MSD1)
Source:CE14845-01
Analvte
Total Kjeldahl Nitrogen
Batch 1L20029 - Same
Blank(1120029-BLR2)
Result Elora
11
PQL Unit/
mg/L
0.48
Spike
Level
12.0
Source
Bela
%REC
%REC im RPD
90
90-110
Prepared: 12/20/2021 13:10 Analyzed: 12/21/2021 12:27
Spike
Result flee PQL Marts Level
4.6
0.48
Result Pla_o POL
8.1
0.48
mg/L
Units
4.80
Source
Result
1.1
%REC
%REC ljnits RPD
74
90.110
Prepared: 12/20/2021 13:10 Analyzed: 12/21/2021 12:32
Spike
Level
mg/L 4,80
Result Etas P_OL Units
4.7 0.48 mg/L
Source
Result
4.0
%REC
%REC Limits RPD
85
90-110
Prepared: 12/20/2021 13:10 Analyzed: 12/21/2021 12:28
Spike
Level
4,80
Source
Result
1.1
%REC
%REC Limits RPD
74 90-110 0.8
Prepared: 12/20/2021 13:21 Analyzed: 12/27/2021 16:48
RPD
Unlit
1
RPD
Limit Notes_
QM-07
1
RPD
QM-07
RPD
Limit
10
Notes_
QM-07
1
Analvte
Phosphorus
LCS (1L20029-BS2)
Analvte
Phosphorus
Matrix Spike (1120029-MS2)
Source: CE14845-01RE1
Analvte
Phosphorus
Result Nag PQL
0.025 U
0.10
Spike Source
Units Level Result %REC Ljmits RPD
mg/L
%REC
Prepared: 12/20/2021 13:21 Analyzed: 12/27/2021 16:49
Spike
Result Flan P_O1. Units Level
1.5
Rye ult flan
2.6 D
0.10
0.50
mg/L
Units
mg/L
1.60
Source
Result
%REC
%REC Limits RPD
95
80-120
Prepared: 12/20/2021 13:21 Analyzed: 12/27/2021 16:52
Spike
Level
0.640
Source
Result
1.6
%REC
%REC Limits RPD
155
80-120
RPD
Limit
RPD
Limit
RPD
Limit
l
Note
QM-07
Matrix Spike Dup (1L20029-M5D2)
Prepared: 12/20/2021 13:21 Analyzed: 12/27/2021 16:53
Source: CE14845-01RE1
Analvte
Phosphorus
Result Etas
2.8 D
P12!< Units
0.50 mg/L
Spike Source
Level Result
0.640 1.6
%REC
%REC Limits RPD
189 80-120 8
RPD
_limit
25
Notes..
QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 12 of 15

www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC1 Calculated analyte - MDL./MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 13 of 15

10775 Central Port or 4510 ExecuIhae Park Court, Suite 111
Orlando FL 32524 Jacksonville. FL 32216.5069
[phone] (904) 296.30d7 Fax [phone]
Ghent Name
Novozyrnes North America (NOt 0B)
Pralecl Number
[none]
AIrPerry Chapel Church Road
Gd rSZip
rTAIdinton, NC 27525
Tel
494-3000
l cNrt lu Week One- SBM
Fax
Bemplerie) NeIfIIm Mimi)
kprne.htj1-I \
Snrnptersa silpretnre
I,�J
an+
Sam* ID 1FielA IrlenAtaeonr
Collection Dela
SBM
121
ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
1024 Woodwinds Industrial CI
Cary NC 27511
01191467-3090 Fax Mg) 487.3515
Requested Anetyw
PO a 1 BH1mg Into
37000449435
Repo! In.; C,,nl.t.t
Scott Creech
BJkn Contactnal Payable
Site Locatk 1 Time Zone
Collection
Trine
V
Comp / Grab
Mabix
ISee coded
Total Y of
[gHamere
P sisrv.Uen ISee Ccdeei [Combine as necessary)
www.encolabs.com
Page of
Requested Turnaround
Times
Nola Rush requests aublect to
acceptance by the lacy +.
Standard
— Expedited
Due —/ /
Lab Workarder
tE l8640
Sample Comments
X
X
X
X
Semple Kit Prepared By
Datellrme
Heiki., . tied • y
mro oti/Spectel Reporting Requirements
Re'rngteshed By
<— Total * of Containers
/Owe/Time Received By
1214241/3e01)
Date/Tirme RacerveKI b
Daterfine
le-9ii*/W !A
Dale.Trme
SD Retina:w hed By Dawflme
Received By
CQ
(D
1 dIt Cooler It's IL Tempe on Receipt L
/6
a
A1GW-Groundwater SO. Soilrev DW-Dnnkmg Water 5E-enant SW -Surface Weer WW-Wastemler A -Ali 0-Other (dated in comments) Preservation: 1-1p H-RCt N IiNp3 S-H2SO4 NO-NaOH 04.1.ther 4
Note Al sarnpkt sr,bm chit t,r ENCO Labs are in accordance with the terms and conttians hated on the reverse of thin Corm. unless poor wrtllen agreements exist
Det.TTlme
C Bo pon Recetpl
Acceptable - Unacceptable
lad m rrmments)

Sample Preservation Verification
ENCO Cary
Work Order
Client
Logged In
•
CE18640
Novozymes North America (NO008)
08-Dec-21 10:49
Preservation Check Performed By
CE18640-01
Project:
Project #
Logged By
Monthly - Week One - SBM
[none]
Samantha L Hyatt 2
Date/Ttme laci74( [130
Cont Type
1
2
25OmLP+H2SO4
250mLP+HNO3
Reagent Name
1- .SdL
pH Strip ID
Pres (pH)
Requirement
<2
<2
ID
0141655
C r1D 491
C' ,_S
3
4
pH Checked /
Control
pH Adjusted
Y / N / NA(! N 1 NA17
Y)N/NA
7)N/NA
Reagent Name ID
Date.rme
Adjusted
5
6
Reagent Used/Comments
4.2rwL. LK50(.1 ✓�
4aIl.. 1-tNtz3 r
Reagent Name ID
t \ELMNT\Printlwko�,
PreservationCheck. rpt
f Page 15of15