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HomeMy WebLinkAboutWQ0005809_Monitoring - 07-2021_20211221 DWR - NonDischarge Monitoring Report Submittal •4 .. NORTH CAROLINA Enrlranmenlel QHaflly Monitoring Report Submittal .............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. Permit Number#* WQ0005809 Name of Facility:* Colonial Pipeline Greensboro Junction Month:* July Year:* 2021 Report Information Type* Upload Document* Revised-GW-59 GW 59 Submittal July 11.87MB 2021.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2,NDMLR,GW-59). Confirmation Email Address:* MHughes@colpipe.corn Name of Submitter:* Maribeth Hughes Signature: Date of submittal: 12/21/2021 This will be filled in automatically Initial Review ................... Reviewer: Mokashi, Poorva Is the project number correct?* WQ0005809 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Accepted Date: 2/4/2022 GW-59A COMPLIANCE REPORT FORM Permit# W00005809 (Submit one each monitoring period with GW-59 forms.) ] Enter date monitoring results were due.(AUGUST 31,2021)Will this monitoring report(GW-59 and GW-59A) YES NO be submitted after the established due date? .. 2 Was any required information missing on the GW-59 report forms? YES( NO IF the answer to question 1 or 2 is"YES",list in the space provided below the well identification number(s)and explain the \\problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing identificat n YES NO plate,area overgrown,etc.)?If the answer is"Yes",contact the Regional Office,for guidance. Some wells need locks and protective casings. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is"NO",skip to section 8. If the answer to question 4 is"YES"list the affected wells individually with constituent(s)and concentration(s) exceeding standards in the space provided below: pH for all monitor wells sampled was below the range of 6.5-8.5 SU. 5 For the constituents identified in question 4 above,have standards been exceeded previously for the same ( YES ) NO constituent(s)in the same well(s)in the last two years? ` / If the answer to question 5 is"NO",skip to section 8. If the answer to question 5 is"YES",list in the space provided below,each well with constituent(s)exceeding standards,concentration(s)reported,and sample collection date for each occurrence(for the last two years). All MW's had a pH less than 6.5 SU in previous sampling events. 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES( NO If the answer is"YES",a groundwater quality problem maybe occurring.CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is"NO",monitoring wells may be improperly located;contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YE NO quality problem? If the answer to question 7 is"YES",describe those actions in the space provided below. If the answer to question 7 is"NO';contact the Regional Office within 90 days;an evaluation maybe required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility.Failure to do so may subject the permittee to a Notice of Violation, fines,and/or penalties. 8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (ComplianceR GW-59A)is true and com a to the best of my knowledge. ' )�(2' Signature of Permittee(or Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 ulc Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 county Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (Zip) ❑ Spray Field ❑Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Upgradient Of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-1 Date sample collected: 7/30/2021 FIELD ANALYSES: WAS Well Depth: 21.9 ft. Well Diameter: 2 in. pH 00400: 5.7 units Temp. 00010: 17.6 °c DRY at Depth to Water Level 82546: 11.61 ft.below measuring point Screened Interval: ft. to ft. Spec.Cond.00094: 0.0373 µMhos time of sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5 gallons Appearance Clear here: Samples for metals were collected unfiltered: El YES ❑ NO and field acidified: 0 YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 1.4 mg/L Zn-Zinc 01092 <0.01 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 269 mg/L Al-Aluminum o1105 mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 <5.0 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? 0 Yes(1) ❑ No(0) Specific Conductance 00095 Mhos K-Potassium 00937 mg/L VOC 7873 method# 8260D Total Ammonia o0610 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen:NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DW R-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Brian Smith ---1----3- of. 1/ (//21 Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY Mail Original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1817 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 ulC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 County Guilford ❑ Lagoon ❑Remediation: Infiltration Gallery (City) (State) (Zip) ❑ Spray Field lEl Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Upgradient of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-2 Date sample collected: 7/30/2021 FIELD ANALYSES: WAS Well Depth: 25.5 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp.00o10: 17.5 °C DRY at time of Depth to Water Level 82546:8.28 ft.below measuring point Screened Interval: 18 ft. to 23 ft. Spec.Cond.00094: 0.0211 µMhos sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 3.5 gallons Appearance Clear here:Li Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: ❑■ YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead o1051 <5.0 ug/L Coliform:MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 3.5 mg/L Zn-Zinc 01092 <0.01 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P o0665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 - mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 177 mg/L Al-Aluminum 01105 mg/L Total Xylene - <1.0 ug/L pH (Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00916 <1.0 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <5.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? lI Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DW R-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Brian Smith ( ) /(- -- 11 /fit l/21 Permittee(or Authorized Agent)Name and Title-Please print or type Signature of 1$ermittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and`1 copy to: 1617 MAI SERVICE CENTER,RALEIGH,NC 37899-1 6 9 7 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 uic Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (street) NC 27409 county Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (Zip) ❑ Spray Field ❑ Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name:Upgradient Of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-3 Date sample collected: 7/30/2021 FIELD ANALYSES: WAS Well Depth: 40.30 ft. Well Diameter: 2 in. pH o0400: 5.9 units Temp.00o1o: 1 8.3 °C DRY at Depth to Water Level 82546:15.62 ft. below measuring point Screened Interval: ft. to ft. Spec.Cond.00094: 0.0060 µMhos time of sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 8 gallons Appearance Clear here:n Samples for metals were collected unfiltered: ❑■ YES El NO and field acidified: •YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 0062o 0.45 mg/L Zn-Zinc 01092 <0.01 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 363 mg/L AI-Aluminum o1105 mg/L pH(Lab)00403 units Ba-Barium 01007 ug/L Total Xylene - <1.0 ug/L TOC 00680 mg/L Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug!L Arsenic 01002 ug/L Chromium:Total 01034 <5.0 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑l Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L method# (Ammonia Nitrogen;NH3as N,Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. f Brian Smith 1 _ t 1 ql/ z f Permittee(or Authorized Agent)Name and Title-Please print or type Sign ermittee(or uthorized Agen (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and Copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non Discharge WQ0005809 uIC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (street) NC 27409 County Guilford 0 Lagoon ❑Remediation: Infiltration Gallery (City) (State) (Zip) ❑ Spray Field 0 Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor lII Land Application of Sludge Well Location/Site Name:Downgradient of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-4 (MW-135) Date sample collected: 7/30/2021 FIELD ANALYSES: WAS Well Depth: 29.9 ft. Well Diameter: 2 in. pH 00400: 5.7 units Temp.00010: 1 5.7 °C DRY at Depth to Water Level 82546:19.89 ft.below measuring point Screened Interval: ft. to ft. Spec.Cond.00094: 0.0054 µMhos time of sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: Samples for metals were collected unfiltered: ❑I• YES ❑ NO and field acidified: LI YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 <0.040 mg/L Zn-Zinc 01092 0.0139 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 83.0 mg/L Al-Aluminum 01105 mg/L Total Xylene - <1.0 ug/L pH (Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00916 <1.0 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <5.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? 0 Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Brian Smith I 119 (Z1 Permittee(or Authorized Agent)Name and Title-Please print or type Sig e.iCof Permittee(or Authorized Agent) _ (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 UIC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 county Guilford ID Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (Zip) ❑ Spray Field ❑Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 El Rotary Distributor 0 Land Application of Sludge Well Location/Site Name:Downgradient of Field No.of wells to be sampled: 6 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): 6 Date sample collected: 7/30/2021 FIELD ANALYSES: WAS Well Depth: 21.1 ft. Well Diameter: 2 in. pH 00400: 6.0 units Temp.00o10: 16.9 °C DRY at Depth to Water Level 82546:7.0 ft.below measuring point Screened Interval: 4 ft. to 17 ft. Spec. Cond.00094: 0.0515 µMhos time of sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 7 gallons Appearance Clear here:—] Samples for metals were collected unfiltered: •YES ❑ NO and field acidified: ❑■ YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N ooe2o <0.040 mg/L Zn-Zinc 01092 <0.010 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 83.0 mg/L Al-Aluminum 01105 mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units - Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium 00916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug/L Arsenic 01002 ug/L Chromium:Total 01034 <5.0 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate o0945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑■ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L method# (Ammonia Nitrogen,NH3 asN;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for!;Wowing violations. Brian Smith V !( 1 ctli Permittee(or Authorized Agent)Name and Title-Please print or type T. ire of Permittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and Copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 6/30/2022 Facility Name: Colonial Pipeline Company Greensboro Junction WWTF Non-Discharge WQ0005809 uIC Permit Name(if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro (Street) NC 27409 county Guilford ❑ Lagoon El Remediation: Infiltration Gallery (City] (State) (Zip) ❑ Spray Field ❑ Remediation: Contact Person: Brian Smith Telephone#: 336-931-6027 ❑ Rotary Distributor 0 Land Application of Sludge Well Location/Site Name:Upgradient of Field No.of wells to be sampled: 6 El Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): 183 Date sample collected: 8/2/2021 FIELD ANALYSES: WAS Well Depth: 25.2 ft. Well Diameter: 2 in. pH 00400: 5.6 units Temp.00010: 1 8.9 °C DRY at Depth to Water Level 82546:8.78 ft.below measuring point Screened Interval: ft. to ft. Spec.Cond.00094:0.0129 µMhos time of sampling, Measuring Point is ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 8 gallons Appearance Clear here: Samples for metals were collected unfiltered: I]YES ❑ NO and field acidified: Li YES ❑NO LABORATORY INFORMATION Date sample analyzed:8/6/2021 Laboratory Name: Pace Laboratory Certification No. 12 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead o1051 <5.0 ug/L Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 0.19 mg/L Zn-Zinc 01092 <0.01 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 75.0 mg/L Al-Aluminum 01105 mg/L Total Xylene - <1.0 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L TOC 00680 mg/L Ca-Calcium o0916 mg/L Chloride 00940 mg/L Cd-Cadmium 01027 <1.0 ug/L Arsenic o1002 ug/L Chromium:Total 01034 <5.0 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? Ia Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# 8260D Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen,NH3 asN;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Brian Smith �� � /( (7124 Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date) GW-59 Rev.06-07-2018 Pace Analytical Services,LLC aceAnal tica 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 August 06, 2021 Michael Pfeifer S&M E 3201 Spring Forest Road Raleigh, NC 27616 RE: Project: CPC Greensboro 216623 Pace Project No.: 92552615 Dear Michael Pfeifer: Enclosed are the analytical results for sample(s)received by the laboratory on July 30, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte • Pace Analytical Services-Raleigh If you have any questions concerning this report, please feel free to contact me. Sincerely, a ` \(1' '`?'a-.ar,C Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/' Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 CERTIFICATIONS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Pace Analytical Services Raleigh 4915 Waters Edge Dr.#120, Raleigh, NC 27606 North Carolina Drinking Water Certification#: 37731 North Carolina Wastewater Certification#:67 Pace Analytical Services Charlotte 9800 Kincey Ave.Ste 100, Huntersville, NC 28078 South Carolina Certification#: 99006001 Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#: E87627 North Carolina Drinking Water Certification#: 37706 Kentucky UST Certification#: 84 North Carolina Field Services Certification#: 5342 Virginia/VELAP Certification#:460221 North Carolina Wastewater Certification#: 12 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville, NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#: E87648 South Carolina Certification#: 99030001 North Carolina Drinking Water Certification#: 37712 Virginia/VELAP Certification#:460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 43 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 SAMPLE ANALYTE COUNT Project: CPC Greensboro 216623 Pace Project No.: 92552615 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92552615001 MW-1 EPA 200.7 Rev 4.4 1994 DS 4 PASI-A EPA 8260D NSCQ 63 PASI-C SM 9222D-2006 WT 1 PASI-R SM 2540C-2011 ZMC 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 2 PASI-A EPA 365.1 Rev 2.0 1993 DMN 1 PASI-A SM 4500-CI-E-2011 HMH 1 PASI-A 92552615002 MW-2 EPA 200.7 Rev 4.4 1994 DS 4 PASI-A EPA 8260D NSCQ 63 PASI-C SM 9222D-2006 WT 1 PASI-R SM 2540C-2011 MJP 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 2 PASI-A EPA 365.1 Rev 2.0 1993 DMN 1 PASI-A SM 4500-CI-E-2011 HMH 1 PASI-A 92552615003 MW-6 EPA 200.7 Rev 4.4 1994 DS 4 PASI-A EPA 8260D NSCQ 63 PASI-C SM 9222D-2006 WT 1 PASI-R SM 2540C-2011 MJP 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 2 PASI-A EPA 365.1 Rev 2.0 1993 DMN 1 PASI-A SM 4500-CI-E-2011 HMH 1 PASI-A 92552615004 MW-3 EPA 200.7 Rev 4.4 1994 DS 4 PASI-A EPA 8260D NSCQ 63 PASI-C SM 2540C-2011 MJP 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 2 PASI-A 92552615005 MW-4(MW-135) EPA 200.7 Rev 4.4 1994 DS 4 PASI-A EPA 8260D NSCQ 63 PASI-C SM 2540C-2011 MJP 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 2 PASI-A - 1 - 1• 1• 1 - REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/' Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 SAMPLE ANALYTE COUNT Project: CPC Greensboro 216623 Pace Project No.: 92552615 Analytes Lab ID Sample ID Method Analysts Reported Laboratory PASI-A= Pace Analytical Services-Asheville PASI-C= Pace Analytical Services-Charlotte PASI-R= Pace Analytical Services-Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 4 of 43 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-1 Lab ID: 92552615001 Collected: 07/30/21 09:10 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:02 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:02 7440-47-3 Lead <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:02 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:02 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/06/21 01:26 67-64-1 Benzene <1.0 ug/L 1.0 1 08/06/21 01:26 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/06/21 01:26 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/06/21 01:26 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/06/21 01:26 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/06/21 01:26 74-83-9 v2 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/06/21 01:26 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/06/21 01:26 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 75-00-3 IK Chloroform <1.0 ug/L 1.0 1 08/06/21 01:26 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/06/21 01:26 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 01:26 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 01:26 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/06/21 01:26 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/06/21 01:26 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/06/21 01:26 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/06/21 01:26 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/06/21 01:26 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:26 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:26 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:26 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:26 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:26 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:26 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:26 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:26 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:26 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 08/06/21 01:26 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/06/21 01:26 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/06/21 01:26 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 08/06/21 01:26 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/06/21 01:26 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 43 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-1 Lab ID: 92552615001 Collected: 07/30/21 09:10 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 01:26 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/06/21 01:26 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 01:26 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 01:26 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 01:26 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 01:26 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 01:26 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:26 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 01:26 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/06/21 01:26 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 01:26 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 01:26 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 01:26 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 01:26 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 01:26 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 01:26 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 01:26 95-47-6 Surrogates 4-Bromofluorobenzene(S) 101 % 70-130 1 08/06/21 01:26 460-00-4 1,2-Dichloroethane-d4(S) 101 % 70-130 1 08/06/21 01:26 17060-07-0 Toluene-d8(S) 99 % 70-130 1 08/06/21 01:26 2037-26-5 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 269 mg/L 25.0 1 08/03/21 18:53 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate 1.4 mg/L 0.040 1 07/31/21 13:44 14797-55-8 Nitrogen, Nitrite <0.040 mg/L 0.040 1 07/31/21 13:44 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-2 Lab ID: 92552615002 Collected: 07/30/21 09:30 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:12 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:12 7440-47-3 Lead <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:12 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:12 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/06/21 01:45 67-64-1 Benzene <1.0 ug/L 1.0 1 08/06/21 01:45 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/06/21 01:45 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/06/21 01:45 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/06/21 01:45 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/06/21 01:45 74-83-9 v2 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/06/21 01:45 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/06/21 01:45 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 75-00-3 IK Chloroform <1.0 ug/L 1.0 1 08/06/21 01:45 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/06/21 01:45 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 01:45 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 01:45 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/06/21 01:45 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/06/21 01:45 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/06/21 01:45 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/06/21 01:45 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/06/21 01:45 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:45 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:45 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 01:45 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:45 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:45 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 01:45 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:45 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:45 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 01:45 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 08/06/21 01:45 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/06/21 01:45 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/06/21 01:45 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 08/06/21 01:45 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/06/21 01:45 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-2 Lab ID: 92552615002 Collected: 07/30/21 09:30 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 01:45 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/06/21 01:45 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 01:45 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 01:45 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 01:45 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 01:45 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 01:45 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 01:45 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 01:45 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/06/21 01:45 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 01:45 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 01:45 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 01:45 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 01:45 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 01:45 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 01:45 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 01:45 95-47-6 Surrogates 4-Bromofluorobenzene(S) 101 % 70-130 1 08/06/21 01:45 460-00-4 1,2-Dichloroethane-d4(S) 100 % 70-130 1 08/06/21 01:45 17060-07-0 Toluene-d8(S) 100 % 70-130 1 08/06/21 01:45 2037-26-5 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 177 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate 3.5 mg/L 0.040 1 07/31/21 13:45 14797-55-8 Nitrogen, Nitrite <0.040 mg/L 0.040 1 07/31/21 13:45 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-6 Lab ID: 92552615003 Collected: 07/30/21 08:50 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:15 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:15 7440-47-3 Lead <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:15 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:15 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/06/21 02:03 67-64-1 Benzene <1.0 ug/L 1.0 1 08/06/21 02:03 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:03 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/06/21 02:03 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/06/21 02:03 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/06/21 02:03 74-83-9 v2 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/06/21 02:03 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/06/21 02:03 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 75-00-3 IK Chloroform <1.0 ug/L 1.0 1 08/06/21 02:03 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/06/21 02:03 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:03 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:03 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/06/21 02:03 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:03 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/06/21 02:03 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/06/21 02:03 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/06/21 02:03 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:03 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:03 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:03 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:03 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:03 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:03 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:03 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:03 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:03 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 08/06/21 02:03 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/06/21 02:03 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/06/21 02:03 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 08/06/21 02:03 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/06/21 02:03 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-6 Lab ID: 92552615003 Collected: 07/30/21 08:50 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 02:03 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/06/21 02:03 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 02:03 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 02:03 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 02:03 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 02:03 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 02:03 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:03 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:03 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/06/21 02:03 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 02:03 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 02:03 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 02:03 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 02:03 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 02:03 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 02:03 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 02:03 95-47-6 Surrogates 4-Bromofluorobenzene(S) 101 % 70-130 1 08/06/21 02:03 460-00-4 1,2-Dichloroethane-d4(S) 102 % 70-130 1 08/06/21 02:03 17060-07-0 Toluene-d8(S) 99 % 70-130 1 08/06/21 02:03 2037-26-5 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 83.0 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate <0.040 mg/L 0.040 1 07/31/21 13:43 14797-55-8 Nitrogen, Nitrite <0.040 mg/L 0.040 1 07/31/21 13:43 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-3 Lab ID: 92552615004 Collected: 07/30/21 10:20 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:25 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:25 7440-47-3 Lead <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:25 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:25 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/06/21 02:21 67-64-1 Benzene <1.0 ug/L 1.0 1 08/06/21 02:21 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:21 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/06/21 02:21 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/06/21 02:21 74-83-9 v2 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/06/21 02:21 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/06/21 02:21 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-00-3 IK Chloroform <1.0 ug/L 1.0 1 08/06/21 02:21 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/06/21 02:21 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:21 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:21 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/06/21 02:21 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:21 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/06/21 02:21 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/06/21 02:21 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:21 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:21 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:21 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:21 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:21 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:21 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 08/06/21 02:21 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/06/21 02:21 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/06/21 02:21 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 08/06/21 02:21 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/06/21 02:21 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-3 Lab ID: 92552615004 Collected: 07/30/21 10:20 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 02:21 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/06/21 02:21 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 02:21 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 02:21 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 02:21 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 02:21 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:21 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:21 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/06/21 02:21 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 02:21 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 02:21 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 02:21 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 02:21 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 02:21 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 02:21 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 02:21 95-47-6 Surrogates 4-Bromofluorobenzene(S) 100 % 70-130 1 08/06/21 02:21 460-00-4 1,2-Dichloroethane-d4(S) 98 % 70-130 1 08/06/21 02:21 17060-07-0 Toluene-d8(S) 99 % 70-130 1 08/06/21 02:21 2037-26-5 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 363 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate 0.45 mg/L 0.040 1 07/31/21 13:50 14797-55-8 Nitrogen, Nitrite <0.040 mg/L 0.040 1 07/31/21 13:50 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-4(MW-135) Lab ID: 92552615005 Collected: 07/30/21 10:00 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/04/21 02:00 08/04/21 18:28 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:28 7440-47-3 Lead <5.0 ug/L 5.0 1 08/04/21 02:00 08/04/21 18:28 7439-92-1 Zinc 13.9 ug/L 10.0 1 08/04/21 02:00 08/04/21 18:28 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/06/21 02:39 67-64-1 Benzene <1.0 ug/L 1.0 1 08/06/21 02:39 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:39 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/06/21 02:39 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/06/21 02:39 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/06/21 02:39 74-83-9 v2 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/06/21 02:39 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/06/21 02:39 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 75-00-3 IK Chloroform <1.0 ug/L 1.0 1 08/06/21 02:39 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/06/21 02:39 74-87-3 2-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:39 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/06/21 02:39 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/06/21 02:39 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/06/21 02:39 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/06/21 02:39 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/06/21 02:39 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/06/21 02:39 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:39 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:39 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/06/21 02:39 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:39 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:39 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/06/21 02:39 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:39 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:39 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/06/21 02:39 10061-02-6 Diisopropyl ether <1.0 ug/L 1.0 1 08/06/21 02:39 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/06/21 02:39 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/06/21 02:39 87-68-3 2-Hexanone <5.0 ug/L 5.0 1 08/06/21 02:39 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/06/21 02:39 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC Greensboro 216623 Pace Project No.: 92552615 Sample: MW-4(MW-135) Lab ID: 92552615005 Collected: 07/30/21 10:00 Received: 07/30/21 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Methylene Chloride <5.0 ug/L 5.0 1 08/06/21 02:39 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/06/21 02:39 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/06/21 02:39 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/06/21 02:39 91-20-3 Styrene <1.0 ug/L 1.0 1 08/06/21 02:39 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/06/21 02:39 127-18-4 Toluene <1.0 ug/L 1.0 1 08/06/21 02:39 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/06/21 02:39 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/06/21 02:39 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/06/21 02:39 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/06/21 02:39 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/06/21 02:39 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/06/21 02:39 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/06/21 02:39 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/06/21 02:39 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/06/21 02:39 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/06/21 02:39 95-47-6 Surrogates 4-Bromofluorobenzene(S) 101 % 70-130 1 08/06/21 02:39 460-00-4 1,2-Dichloroethane-d4(S) 100 % 70-130 1 08/06/21 02:39 17060-07-0 Toluene-d8(S) 100 % 70-130 1 08/06/21 02:39 2037-26-5 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Asheville Total Dissolved Solids 83.0 mg/L 25.0 1 08/04/21 11:26 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate <0.040 mg/L 0.040 1 07/31/21 13:46 14797-55-8 Nitrogen, Nitrite 0.056 mg/L 0.040 1 07/31/21 13:46 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637851 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005 METHOD BLANK: 3348752 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L <1.0 1.0 08/04/21 17:17 Chromium ug/L <5.0 5.0 08/04/21 17:17 Lead ug/L <5.0 5.0 08/04/21 17:17 Zinc ug/L <10.0 10.0 08/04/21 17:17 LABORATORY CONTROL SAMPLE: 3348753 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 529 106 85-115 Chromium ug/L 500 543 109 85-115 Lead ug/L 500 543 109 85-115 Zinc ug/L 500 528 106 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3348754 3348755 MS MSD 92552572001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 512 526 102 105 70-130 3 Chromium ug/L ND 500 500 495 512 99 102 70-130 3 Lead ug/L 0.93 500 500 1390 1390 92 92 70-130 0 mg/L Zinc ug/L ND 500 500 506 510 101 102 70-130 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3348756 3348757 MS MSD 92552615003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L <1.0 500 500 521 506 104 101 70-130 3 Chromium ug/L <5.0 500 500 519 499 103 100 70-130 4 Lead ug/L <5.0 500 500 513 498 102 99 70-130 3 Zinc ug/L <10.0 500 500 505 490 100 97 70-130 3 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 24 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637684 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005, 92552615006,92552615007, 92552615008 METHOD BLANK: 3347642 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005, 92552615006,92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L <1.0 1.0 08/05/21 18:11 1,1,1-Trichloroethane ug/L <1.0 1.0 08/05/21 18:11 1,1,2,2-Tetrachloroethane ug/L <1.0 1.0 08/05/21 18:11 1,1,2-Trichloroethane ug/L <1.0 1.0 08/05/21 18:11 1,1-Dichloroethane ug/L <1.0 1.0 08/05/21 18:11 1,1-Dichloroethene ug/L <1.0 1.0 08/05/21 18:11 1,1-Dichloropropene ug/L <1.0 1.0 08/05/21 18:11 1,2,3-Trichlorobenzene ug/L <1.0 1.0 08/05/21 18:11 1,2,3-Trichloropropane ug/L <1.0 1.0 08/05/21 18:11 1,2,4-Trichlorobenzene ug/L <1.0 1.0 08/05/21 18:11 1,2-Dibromo-3-chloropropane ug/L <2.0 2.0 08/05/21 18:11 1,2-Dibromoethane(EDB) ug/L <1.0 1.0 08/05/21 18:11 1,2-Dichlorobenzene ug/L <1.0 1.0 08/05/21 18:11 1,2-Dichloroethane ug/L <1.0 1.0 08/05/21 18:11 1,2-Dichloropropane ug/L <1.0 1.0 08/05/21 18:11 1,3-Dichlorobenzene ug/L <1.0 1.0 08/05/21 18:11 1,3-Dichloropropane ug/L <1.0 1.0 08/05/21 18:11 1,4-Dichlorobenzene ug/L <1.0 1.0 08/05/21 18:11 2,2-Dichloropropane ug/L <1.0 1.0 08/05/21 18:11 2-Butanone(MEK) ug/L <5.0 5.0 08/05/21 18:11 2-Chlorotoluene ug/L <1.0 1.0 08/05/21 18:11 2-Hexanone ug/L <5.0 5.0 08/05/21 18:11 4-Chlorotoluene ug/L <1.0 1.0 08/05/21 18:11 4-Methyl-2-pentanone(MIBK) ug/L <5.0 5.0 08/05/21 18:11 Acetone ug/L <25.0 25.0 08/05/21 18:11 Benzene ug/L <1.0 1.0 08/05/21 18:11 Bromobenzene ug/L <1.0 1.0 08/05/21 18:11 Bromochloromethane ug/L <1.0 1.0 08/05/21 18:11 Bromodichloromethane ug/L <1.0 1.0 08/05/21 18:11 Bromoform ug/L <1.0 1.0 08/05/21 18:11 Bromomethane ug/L <2.0 2.0 08/05/21 18:11 v2 Carbon tetrachloride ug/L <1.0 1.0 08/05/21 18:11 Chlorobenzene ug/L <1.0 1.0 08/05/21 18:11 Chloroethane ug/L <1.0 1.0 08/05/21 18:11 IK Chloroform ug/L <1.0 1.0 08/05/21 18:11 Chloromethane ug/L <1.0 1.0 08/05/21 18:11 cis-1,2-Dichloroethene ug/L <1.0 1.0 08/05/21 18:11 cis-1,3-Dichloropropene ug/L <1.0 1.0 08/05/21 18:11 Dibromochloromethane ug/L <1.0 1.0 08/05/21 18:11 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 METHOD BLANK: 3347642 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005, 92552615006,92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L <1.0 1.0 08/05/21 18:11 Dichlorodifluoromethane ug/L <1.0 1.0 08/05/21 18:11 Diisopropyl ether ug/L <1.0 1.0 08/05/21 18:11 Ethylbenzene ug/L <1.0 1.0 08/05/21 18:11 Hexachloro-1,3-butadiene ug/L <2.0 2.0 08/05/21 18:11 m&p-Xylene ug/L <2.0 2.0 08/05/21 18:11 Methyl-tert-butyl ether ug/L <1.0 1.0 08/05/21 18:11 Methylene Chloride ug/L <5.0 5.0 08/05/21 18:11 Naphthalene ug/L <1.0 1.0 08/05/21 18:11 o-Xylene ug/L <1.0 1.0 08/05/21 18:11 p-lsopropyltoluene ug/L <1.0 1.0 08/05/21 18:11 Styrene ug/L <1.0 1.0 08/05/21 18:11 Tetrachloroethene ug/L <1.0 1.0 08/05/21 18:11 Toluene ug/L <1.0 1.0 08/05/21 18:11 trans-1,2-Dichloroethene ug/L <1.0 1.0 08/05/21 18:11 trans-1,3-Dichloropropene ug/L <1.0 1.0 08/05/21 18:11 Trichloroethene ug/L <1.0 1.0 08/05/21 18:11 Trichlorofluoromethane ug/L <1.0 1.0 08/05/21 18:11 Vinyl acetate ug/L <2.0 2.0 08/05/21 18:11 Vinyl chloride ug/L <1.0 1.0 08/05/21 18:11 Xylene(Total) ug/L <1.0 1.0 08/05/21 18:11 1,2-Dichloroethane-d4(S) % 100 70-130 08/05/21 18:11 4-Bromofluorobenzene(S) % 103 70-130 08/05/21 18:11 Toluene-d8(S) % 100 70-130 08/05/21 18:11 LABORATORY CONTROL SAMPLE: 3347643 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.4 111 70-130 1,1,1-Trichloroethane ug/L 50 55.1 110 70-130 1,1,2,2-Tetrachloroethane ug/L 50 56.3 113 70-130 1,1,2-Trichloroethane ug/L 50 55.1 110 70-130 1,1-Dichloroethane ug/L 50 55.7 111 70-130 1,1-Dichloroethene ug/L 50 58.5 117 70-132 1,1-Dichloropropene ug/L 50 56.0 112 70-131 1,2,3-Trichlorobenzene ug/L 50 55.6 111 70-134 1,2,3-Trichloropropane ug/L 50 53.2 106 70-130 1,2,4-Trichlorobenzene ug/L 50 56.4 113 70-130 1,2-Dibromo-3-chloropropane ug/L 50 52.9 106 70-132 1,2-Dibromoethane(EDB) ug/L 50 54.6 109 70-130 1,2-Dichlorobenzene ug/L 50 54.4 109 70-130 1,2-Dichloroethane ug/L 50 53.6 107 70-130 1,2-Dichloropropane ug/L 50 58.3 117 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 26 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 LABORATORY CONTROL SAMPLE: 3347643 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,3-Dichlorobenzene ug/L 50 55.2 110 70-130 1,3-Dichloropropane ug/L 50 54.1 108 70-130 1,4-Dichlorobenzene ug/L 50 55.6 111 70-130 2,2-Dichloropropane ug/L 50 59.3 119 70-130 2-Butanone(MEK) ug/L 100 111 111 70-133 2-Chlorotoluene ug/L 50 57.9 116 70-130 2-Hexanone ug/L 100 117 117 70-130 4-Chlorotoluene ug/L 50 55.1 110 70-130 4-Methyl-2-pentanone(MIBK) ug/L 100 115 115 70-130 Acetone ug/L 100 106 106 70-144 Benzene ug/L 50 57.1 114 70-130 Bromobenzene ug/L 50 55.8 112 70-130 Bromochloromethane ug/L 50 53.7 107 70-130 Bromodichloromethane ug/L 50 56.3 113 70-130 Bromoform ug/L 50 53.0 106 70-131 Bromomethane ug/L 50 41.9 84 30-177 v2 Carbon tetrachloride ug/L 50 57.0 114 70-130 Chlorobenzene ug/L 50 55.3 111 70-130 Chloroethane ug/L 50 44.9 90 46-131 IK Chloroform ug/L 50 53.3 107 70-130 Chloromethane ug/L 50 53.8 108 49-130 cis-1,2-Dichloroethene ug/L 50 56.3 113 70-130 cis-1,3-Dichloropropene ug/L 50 57.3 115 70-130 Dibromochloromethane ug/L 50 55.5 111 70-130 Dibromomethane ug/L 50 53.8 108 70-130 Dichlorodifluoromethane ug/L 50 52.0 104 52-134 Diisopropyl ether ug/L 50 54.9 110 70-131 Ethylbenzene ug/L 50 56.0 112 70-130 Hexachloro-1,3-butadiene ug/L 50 57.8 116 70-131 m&p-Xylene ug/L 100 112 112 70-130 Methyl-tert-butyl ether ug/L 50 51.9 104 70-130 Methylene Chloride ug/L 50 55.9 112 68-130 Naphthalene ug/L 50 55.8 112 70-133 o-Xylene ug/L 50 54.2 108 70-130 p-lsopropyltoluene ug/L 50 56.8 114 70-130 Styrene ug/L 50 56.0 112 70-130 Tetrachloroethene ug/L 50 55.1 110 70-130 Toluene ug/L 50 56.6 113 70-130 trans-1,2-Dichloroethene ug/L 50 58.5 117 70-130 trans-1,3-Dichloropropene ug/L 50 57.0 114 70-130 Trichloroethene ug/L 50 55.8 112 70-130 Trichlorofluoromethane ug/L 50 49.1 98 61-130 Vinyl acetate ug/L 100 120 120 70-140 Vinyl chloride ug/L 50 54.0 108 59-142 Xylene(Total) ug/L 150 166 111 70-130 1,2-Dichloroethane-d4(S) % 94 70-130 4-Bromofluorobenzene(S) % 100 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 LABORATORY CONTROL SAMPLE: 3347643 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Toluene-d8(S) % 100 70-130 MATRIX SPIKE SAMPLE: 3352190 92552615006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L <1.0 20 23.3 117 70-135 1,1,1-Trichloroethane ug/L <1.0 20 23.2 116 70-148 1,1,2,2-Tetrachloroethane ug/L <1.0 20 23.3 116 70-131 1,1,2-Trichloroethane ug/L <1.0 20 21.4 107 70-136 1,1-Dichloroethane ug/L <1.0 20 23.6 118 70-147 1,1-Dichloroethene ug/L <1.0 20 25.0 125 70-158 1,1-Dichloropropene ug/L <1.0 20 23.9 119 70-149 1,2,3-Trichlorobenzene ug/L <1.0 20 22.8 114 68-140 1,2,3-Trichloropropane ug/L <1.0 20 23.0 115 67-137 1,2,4-Trichlorobenzene ug/L <1.0 20 22.9 115 70-139 1,2-Dibromo-3-chloropropane ug/L <2.0 20 21.9 109 69-136 1,2-Dibromoethane(EDB) ug/L <1.0 20 22.8 114 70-137 1,2-Dichlorobenzene ug/L <1.0 20 23.2 116 70-133 1,2-Dichloroethane ug/L <1.0 20 21.9 110 67-138 1,2-Dichloropropane ug/L <1.0 20 23.8 119 70-138 1,3-Dichlorobenzene ug/L <1.0 20 24.1 121 70-133 1,3-Dichloropropane ug/L <1.0 20 22.9 115 70-136 1,4-Dichlorobenzene ug/L <1.0 20 24.2 121 70-133 2,2-Dichloropropane ug/L <1.0 20 25.0 125 52-155 2-Butanone(MEK) ug/L <5.0 40 43.4 108 61-147 2-Chlorotoluene ug/L <1.0 20 25.2 126 70-141 2-Hexanone ug/L <5.0 40 49.7 124 67-139 4-Chlorotoluene ug/L <1.0 20 24.5 123 70-135 4-Methyl-2-pentanone(MIBK) ug/L <5.0 40 45.3 113 67-136 Acetone ug/L <25.0 40 41.8 104 55-159 Benzene ug/L <1.0 20 23.6 118 67-150 Bromobenzene ug/L <1.0 20 23.9 119 70-134 Bromochloromethane ug/L <1.0 20 22.2 111 70-146 Bromodichloromethane ug/L <1.0 20 22.5 112 70-138 Bromoform ug/L <1.0 20 20.1 100 57-138 Bromomethane ug/L <2.0 20 18.1 91 10-200 v2 Carbon tetrachloride ug/L <1.0 20 23.8 119 70-147 Chlorobenzene ug/L <1.0 20 23.9 119 70-137 Chloroethane ug/L <1.0 20 26.9 134 51-166 IK Chloroform ug/L <1.0 20 22.3 112 70-144 Chloromethane ug/L <1.0 20 21.9 110 24-161 cis-1,2-Dichloroethene ug/L <1.0 20 23.4 117 67-148 cis-1,3-Dichloropropene ug/L <1.0 20 22.1 110 70-142 Dibromochloromethane ug/L <1.0 20 22.5 112 68-138 Dibromomethane ug/L <1.0 20 21.3 106 70-134 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 28 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 MATRIX SPIKE SAMPLE: 3352190 92552615006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Dichlorodifluoromethane ug/L <1.0 20 24.0 120 43-155 Diisopropyl ether ug/L <1.0 20 21.8 109 65-146 Ethylbenzene ug/L <1.0 20 24.6 123 68-143 Hexachloro-1,3-butadiene ug/L <2.0 20 24.2 121 62-151 m&p-Xylene ug/L <2.0 40 49.5 124 53-157 Methyl-tert-butyl ether ug/L <1.0 20 20.3 102 59-156 Methylene Chloride ug/L <5.0 20 23.4 117 64-148 Naphthalene ug/L <1.0 20 22.3 111 57-150 o-Xylene ug/L <1.0 20 23.9 119 68-143 p-lsopropyltoluene ug/L <1.0 20 25.1 125 70-141 Styrene ug/L <1.0 20 24.5 122 70-136 Tetrachloroethene ug/L <1.0 20 23.9 120 70-139 Toluene ug/L <1.0 20 23.2 116 47-157 trans-1,2-Dichloroethene ug/L <1.0 20 24.1 121 70-149 trans-1,3-Dichloropropene ug/L <1.0 20 22.1 110 70-138 Trichloroethene ug/L <1.0 20 23.0 115 70-149 Trichlorofluoromethane ug/L <1.0 20 21.6 108 61-154 Vinyl acetate ug/L <2.0 40 47.9 120 48-156 Vinyl chloride ug/L <1.0 20 22.6 113 55-172 Xylene(Total) ug/L <1.0 60 73.4 122 66-145 1,2-Dichloroethane-d4(S) % 101 70-130 4-Bromofluorobenzene(S) % 100 70-130 Toluene-d8(S) % 99 70-130 SAMPLE DUPLICATE: 3352189 92552615005 Dup Parameter Units Result Result RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L <1.0 <1.0 1,1,1-Trichloroethane ug/L <1.0 <1.0 1,1,2,2-Tetrachloroethane ug/L <1.0 <1.0 1,1,2-Trichloroethane ug/L <1.0 <1.0 1,1-Dichloroethane ug/L <1.0 <1.0 1,1-Dichloroethene ug/L <1.0 <1.0 1,1-Dichloropropene ug/L <1.0 <1.0 1,2,3-Trichlorobenzene ug/L <1.0 <1.0 1,2,3-Trichloropropane ug/L <1.0 <1.0 1,2,4-Trichlorobenzene ug/L <1.0 <1.0 1,2-Dibromo-3-chloropropane ug/L <2.0 <2.0 1,2-Dibromoethane(EDB) ug/L <1.0 <1.0 1,2-Dichlorobenzene ug/L <1.0 <1.0 1,2-Dichloroethane ug/L <1.0 <1.0 1,2-Dichloropropane ug/L <1.0 <1.0 1,3-Dichlorobenzene ug/L <1.0 <1.0 1,3-Dichloropropane ug/L <1.0 <1.0 1,4-Dichlorobenzene ug/L <1.0 <1.0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 29 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 SAMPLE DUPLICATE: 3352189 92552615005 Dup Parameter Units Result Result RPD Qualifiers 2,2-Dichloropropane ug/L <1.0 <1.0 2-Butanone(MEK) ug/L <5.0 <5.0 2-Chlorotoluene ug/L <1.0 <1.0 2-Hexanone ug/L <5.0 <5.0 4-Chlorotoluene ug/L <1.0 <1.0 4-Methyl-2-pentanone(MIBK) ug/L <5.0 <5.0 Acetone ug/L <25.0 <25.0 Benzene ug/L <1.0 <1.0 Bromobenzene ug/L <1.0 <1.0 Bromochloromethane ug/L <1.0 <1.0 Bromodichloromethane ug/L <1.0 <1.0 Bromoform ug/L <1.0 <1.0 Bromomethane ug/L <2.0 <2.0 v2 Carbon tetrachloride ug/L <1.0 <1.0 Chlorobenzene ug/L <1.0 <1.0 Chloroethane ug/L <1.0 <1.0 IK Chloroform ug/L <1.0 <1.0 Chloromethane ug/L <1.0 <1.0 cis-1,2-Dichloroethene ug/L <1.0 <1.0 cis-1,3-Dichloropropene ug/L <1.0 <1.0 Dibromochloromethane ug/L <1.0 <1.0 Dibromomethane ug/L <1.0 <1.0 Dichlorodifluoromethane ug/L <1.0 <1.0 Diisopropyl ether ug/L <1.0 <1.0 Ethylbenzene ug/L <1.0 <1.0 Hexachloro-1,3-butadiene ug/L <2.0 <2.0 m&p-Xylene ug/L <2.0 <2.0 Methyl-tert-butyl ether ug/L <1.0 <1.0 Methylene Chloride ug/L <5.0 <5.0 Naphthalene ug/L <1.0 <1.0 o-Xylene ug/L <1.0 <1.0 p-lsopropyltoluene ug/L <1.0 <1.0 Styrene ug/L <1.0 <1.0 Tetrachloroethene ug/L <1.0 <1.0 Toluene ug/L <1.0 <1.0 trans-1,2-Dichloroethene ug/L <1.0 <1.0 trans-1,3-Dichloropropene ug/L <1.0 <1.0 Trichloroethene ug/L <1.0 <1.0 Trichlorofluoromethane ug/L <1.0 <1.0 Vinyl acetate ug/L <2.0 <2.0 Vinyl chloride ug/L <1.0 <1.0 Xylene(Total) ug/L <1.0 <1.0 1,2-Dichloroethane-d4(S) % 100 103 4-Bromofluorobenzene(S) % 101 99 Toluene-d8(S) % 100 100 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 30 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637421 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF)-RAL Laboratory: Pace Analytical Services-Raleigh Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 METHOD BLANK: 3346246 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/31/21 12:28 SAMPLE DUPLICATE: 3346247 92552615007 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 31 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637732 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001 METHOD BLANK: 3348012 Matrix: Water Associated Lab Samples: 92552615001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L <25.0 25.0 08/03/21 18:51 LABORATORY CONTROL SAMPLE: 3348013 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 3348014 92552532010 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 460 461 0 SAMPLE DUPLICATE: 3348015 92552533015 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 41.0 36.0 13 Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 32 of 43 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637924 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615002,92552615003, 92552615004,92552615005, 92552615006, 92552615007,92552615008 METHOD BLANK: 3348901 Matrix: Water Associated Lab Samples: 92552615002,92552615003, 92552615004,92552615005, 92552615006, 92552615007,92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L <25.0 25.0 08/04/21 11:26 LABORATORY CONTROL SAMPLE: 3348902 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 3348903 92552615002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 177 177 0 SAMPLE DUPLICATE: 3348904 92552687004 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 1730 1740 1 Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 33 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 638189 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 METHOD BLANK: 3350522 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Ammonia mg/L <0.10 0.10 08/05/21 11:36 LABORATORY CONTROL SAMPLE: 3350523 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen,Ammonia mg/L 5 4.9 97 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3350524 3350525 MS MSD 92552050005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen,Ammonia mg/L 20.4 5 5 25.3 25.2 99 96 90-110 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3350526 3350527 MS MSD 92552050006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen,Ammonia mg/L 20.7 5 5 25.5 26.9 95 123 90-110 5 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 34 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637271 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite, Unpres. Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005, 92552615006,92552615007, 92552615008 METHOD BLANK: 3345722 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615004, 92552615005, 92552615006,92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L <0.040 0.040 07/31/21 13:35 Nitrogen, Nitrite mg/L <0.040 0.040 07/31/21 13:35 LABORATORY CONTROL SAMPLE: 3345723 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.6 103 90-110 Nitrogen, Nitrite mg/L 1 1.0 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3345724 3345725 MS MSD 92552615007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.45 1.5 1.5 2.0 2.0 103 103 90-110 0 Nitrogen, Nitrite mg/L <0.040 1 1 1.0 1.0 100 101 90-110 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 35 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637811 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 METHOD BLANK: 3348633 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L <0.050 0.050 08/04/21 12:16 LABORATORY CONTROL SAMPLE: 3348634 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 103 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3348635 3348636 MS MSD 92551429001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.9 2.5 2.5 4.4 4.5 99 102 90-110 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3348637 3348638 MS MSD 92552687004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 104 103 90-110 1 Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 36 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC Greensboro 216623 Pace Project No.: 92552615 QC Batch: 637697 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 METHOD BLANK: 3347783 Matrix: Water Associated Lab Samples: 92552615001,92552615002, 92552615003,92552615006, 92552615007, 92552615008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L <1.0 1.0 08/03/21 16:06 LABORATORY CONTROL SAMPLE: 3347784 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 20.3 102 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3347785 3347786 MS MSD 92552252011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 39.6 10 10 44.9 47.2 53 76 90-110 5 M1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3347787 3347788 MS MSD 92552353005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 116 10 10 119 135 30 183 90-110 12 M1,R1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 37 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 QUALIFIERS Project: CPC Greensboro 216623 Pace Project No.: 92552615 DEFINITIONS DF-Dilution Factor, if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s)did not meet method acceptance criteria;this result should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. R1 RPD value was outside control limits. v2 The continuing calibration verification was below the method acceptance limit.The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 38 of 43 Pace Analytical Services,LLC aceAnal tical 9800 ncey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CPC Greensboro 216623 Pace Project No.: 92552615 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92552615001 MW-1 EPA 200.7 Rev 4.4 1994 637851 EPA 200.7 Rev 4.4 1994 637868 92552615002 MW-2 EPA 200.7 Rev 4.4 1994 637851 EPA 200.7 Rev 4.4 1994 637868 92552615003 MW-6 EPA 200.7 Rev 4.4 1994 637851 EPA 200.7 Rev 4.4 1994 637868 92552615004 MW-3 EPA 200.7 Rev 4.4 1994 637851 EPA 200.7 Rev 4.4 1994 637868 92552615005 MW-4(MW-135) EPA 200.7 Rev 4.4 1994 637851 EPA 200.7 Rev 4.4 1994 637868 92552615001 MW-1 EPA 8260D 637684 92552615002 MW-2 EPA 8260D 637684 92552615003 MW-6 EPA 8260D 637684 92552615004 MW-3 EPA 8260D 637684 92552615005 MW-4(MW-135) EPA 8260D 637684 92552615006 MW-5 EPA 8260D 637684 92552615007 MW-7 EPA 8260D 637684 92552615008 MW-9 EPA 8260D 637684 92552615001 MW-1 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615002 MW-2 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615003 MW-6 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615006 MW-5 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615007 MW-7 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615008 MW-9 SM 9222D-2006 637421 SM 9222D-2006 637423 92552615001 MW-1 SM 2540C-2011 637732 92552615002 MW-2 SM 2540C-2011 637924 92552615003 MW-6 SM 2540C-2011 637924 92552615004 MW-3 SM 2540C-2011 637924 92552615005 MW-4(MW-135) SM 2540C-2011 637924 92552615006 MW-5 SM 2540C-2011 637924 92552615007 MW-7 SM 2540C-2011 637924 92552615008 MW-9 SM 2540C-2011 637924 92552615001 MW-1 EPA 350.1 Rev 2.0 1993 638189 92552615002 MW-2 EPA 350.1 Rev 2.0 1993 638189 92552615003 MW-6 EPA 350.1 Rev 2.0 1993 638189 92552615006 MW-5 EPA 350.1 Rev 2.0 1993 638189 92552615007 MW-7 EPA 350.1 Rev 2.0 1993 638189 92552615008 MW-9 EPA 350.1 Rev 2.0 1993 638189 92552615001 MW-1 EPA 353.2 Rev 2.0 1993 637271 92552615002 MW-2 EPA 353.2 Rev 2.0 1993 637271 92552615003 MW-6 EPA 353.2 Rev 2.0 1993 637271 92552615004 MW-3 EPA 353.2 Rev 2.0 1993 637271 92552615005 MW-4(MW-135) EPA 353.2 Rev 2.0 1993 637271 92552615006 MW-5 EPA 353.2 Rev 2.0 1993 637271 92552615007 MW-7 EPA 353.2 Rev 2.0 1993 637271 92552615008 MW-9 EPA 353.2 Rev 2.0 1993 637271 92552615001 MW-1 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 92552615002 MW-2 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 92552615003 MW-6 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 92552615006 MW-5 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 39 of 43 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CPC Greensboro 216623 Pace Project No.: 92552615 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92552615007 MW-7 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 92552615008 MW-9 EPA 365.1 Rev 2.0 1993 637811 EPA 365.1 Rev 2.0 1993 637882 92552615001 MW-1 SM 4500-CI-E-2011 637697 92552615002 MW-2 SM 4500-CI-E-2011 637697 92552615003 MW-6 SM 4500-CI-E-2011 637697 92552615006 MW-5 SM 4500-CI-E-2011 637697 92552615007 MW-7 SM 4500-CI-E-2011 637697 92552615008 MW-9 SM 4500-CI-E-2011 637697 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/06/2021 03:53 PM without the written consent of Pace Analytical Services,LLC. Page 40 of 43 ' • • .. Ma441Cat a _sample CeeditDolfoemeont:::meRaceiptiscuit: 1 Document Revisedpap i Octoof 2 ber213,,207.0 Document No.: ' Issuing Authortty: 1. F.CAR-C3-033-Rev.01 Pece Carolinas Duet,Office Laboratory receiving samples: Asheville El EdenD Greenwood 0 Huntersvlite[] RaleightaelcsvIlleCi AtlantaD Kernersvilie0 W 0 it : 92552615 i 1110')a I'i,^.. IOU f.' ProjeCt 111 )10U •,_, III 11 1E11E1 1 1 ii Coiukr: [Fed Ex. -CUPS Dill USPS OCilent 0 Commercial E-Perr"--- DOther: • 92552E115 Custody Seal Present? Oyes Eirtra Seals Intact? Oyes Dateflardals Femurs&mining Contents -1/ 0 feq ( Packing Materlah OBubbfe Wrap Qeze 4..gs ['None G Other BlologlealTlssuoke? . Thermometer .[Des ONo ROA 0 rit Gm 10: q 1--roc_75- Twe of Ice: et DElue tpeona Correction Factor. . Cooler Temp: 'LP Add/Subtract(T) (...,„ () Temp should be ibove freezing to 6'C pargies out of temp criteria.Samples on ke,coorIng process Cooler Temp Corrected CC): , , (4 Iras begun USDA Regulated Soil{arvcvater sample) v are theinne edthln thelni a : rSC(check maps)? Did simples ornate from eforelen source(internationally, Yes UNO • 'iriciirdlit FWirrind-PF.ierto Rico]r Ows—EINts--- ----- ."-' -'-'- • — Comments/Discrepancyt ! , - Chain of Custody Present? CiTtg----ONo ON/A 1- • , Samples Arrived within Hold Time? arel'el_gli No Orq/A 2 Short Hold Time Analysis{.72 hr.)? ilar..."bN0 ON/A 3. Rush Turn Around lime Requested? OYes ®Na ijNr.e 4. I . i Sufficient Volume? EDOND ON/A S. Correct Containers Usec17 Elii< -Ejtio ON/A 6. -Pace Containers Used? DAC rjNo oNi,e, Containers intact?" E9Yur---E:INo IlliN „7. — Dissolved analysis:Samples Field Filtered? Des ONo ON< B. . Sample Labels Match COC? {Dee' No ON/A 9. • ' „ -Includes Date/The/ID/Analysis Matrix ___ Headspace in VOA Vials(>5-6rnm)? rgrirlo ziN/A___, 10. Trip Blank Present? . OYes ONo OMIT 11. . . i Trip Blank Cu stoci,Seals Present? . Yes No A , COMMENTS/SAMPLE DISCREPANCY , Field Data Required? °Yes EINo 10 V\I Lk t1\Y) -ci. c . -(..) )(14-_,el -'S .7)(.:i, , y-0. (%p)\iT( Cl_, '',,c''' 'kit-0, t, )e,-- - ) ),),y-)..--.2),() v) e 4,),)16' (T..:"zA.,c(),) r,• 2.--)4)(,)() ') Lot ID.of spilt containers: . , • CLIENT NOTIFICATION/RESOLUT1ON 1 I , , f ; I ' . ' .., Person contacted: • Date/Time: ..,. --------- - .--- ..-- ---..--"' ATI'r----------------D47-- 3"1:)-:`"?.:..","r--"`'—`------ , I Project Manager SCURF Review: . .- _ Project Manager SRF Review: \,4, 2/14 1 .{ ,t. Oat,: 7 /30/ZI Page 41 of 4.3 Document Name: 1 Z12 7-1 Sample Unditifee Upon NgtalASCLIV C*cument ReA ii4tdPa '1"4;tQof 2 ber Document No.t Issuing Authority F-CAR-C$41133Itsv.07 Face CatuffnaeQUel MI *Check mark top half of box if pH and/or dechlorination is Project. WO* : 92552615 verified and with, the acceptance range for preservation samples. ' PM: AMB Due Date: 08/06/21 ExcePtfant VOA Coliform MC,on and Grease,EiR0/8013 lwater)DOC,LLHg CLIENT: 92—S&ME RAL "Bottom half of box Is to list number of bottles 1 , 9 7. — 0 ::: 475: re — S n.. — ... 27.-1g $, 'i." ‘c , Cr* 1 i , ;,71 ''•''' Z . 0 rg s i —,,,, 7',/,,, .9 7 ft 2 A -',i. lt," e VI — v c c c ?Long _ ire" m =1 — g1 iti ? g, g !, 1 ). z n 4 iicf,. ...b, 4 44:fit 4A blez z 2 1 i. a B 11. 011111 -2ill .q. 142, 8, 8ggliAg 14gi - 4- 1-1i - -J.--4-1 'IT1-, 1 -6 1- 1 - -4 4 g1 I ! se IM 'l 9 q' .1 flAfr' e, 2 #H2 ,2115i4i44Eiggg ,g15: 4, ' g, g, ... . a I._ t_.....eni_ ._ 1 -1 1111 . i i hik , 1111 Ril 1 1 1 I 111 . ill, 1 I OVI 10;7.,ih 11111L ALL 111ki : lstimmiligimm 1 3 , 1 Ili, 7 .'1 - I I IIIIN 1 8 1 iji‘ 1 11 1111 343. . Ills 1 I I 1 i , 1101 i a 1 i I i 0 Iliti I I j„1 lig Ili, ' 11111Lik 1 141141141 pH Adjustment Log for Preserved Samples Sample ID Type et Preservative pH upon receipt ' Date preservation adjusted Time preservation Amount of Preservative Lot# adjusted added 1 — — Note: Whenever there is a discrepancy affecting Nontheacolina compliance samples,a copy of this form Will be sent to the North Carolina OEHNR Certrfication Office ll,a. r 1 ' 1 Out of hold,incorrect preservetsue,cut of temp.incorrect containers. A .... _ -..% Page 42 of 41 17,to et abed N.'` cc, el cs sin NO ,..., ITEM Al ,... 1 , • 0 p 4 , I F t. 1 2 a in a I ' 1 01 0 0 g 2 c N 1 it i 1 i c g▪ 0 i 0 02 pi I k g I g g .. 34* 3, 8 › i i -,'en V93t1P141% 101 1 2. 1r e Igor t ' M a g'z z gio MATRIX CODE aros solid cadoe fo 164) 1" 0.. i / I 0 SAMPLE TYPE (GeGRAS CPCOMP) 13 1 1 ' 831.2 i It. ? M I , . .., 4 I' . , , r 0 6 ' ` A 1 , g 0 1 A --i 1 I I ',. ' 1'' 9. 9 9 9 ero , P ' I 5 i I i A I I 1 Eli SAMPLE TEMP AT COLLECTION on C "oS. a #OF COhlTAINERo . P. (fill 1. 1 11. / R (1) Unpreserved 1 7• 1 i g 's N g It▪ 0 I e 4c1 g 0 § HaSO4 or . 9 'I , HNO3 E' .e. :T, 5 ,11, , ificgi II 110111 1 NaOH I v gu k ... Na2S203 i'll\!\114. ,1.1'1.1 III g°‘6.'cl. , .,,. '''',,' r II ___L _Methanol 1 ig 1 I Other ' 'i ' '' ' ' -- 1 ..,',., x x 208.7 metals-Cd,Cr,(3b,Zo .r4,,`, X X 1 x Nitrate(48 hrs) 1 1 1 1 1 Ef to• .* limn . ri 3 31131:11 x Total Dissolved Solids - ' ' - " .: 3 .. 1 x 62003 VOCs 1 0 , i •••ill. ' "l -"""""1 ] x Chloride Wirr,ii i --Cl 0 .R, C x Fecal Collforrn(8 hrs) : .1.,.2,-, c 2 ., m 3 Amrrionle,phosphorus f' a I x 8260 VOC rADI c 19n '- 1 : .,......-, T III p .m in*0 . ,... 1 II 1111.11111 'Residual Chlorine(YIN) it.19. Pereised cm .. C,7,n) , :° .;7',,::.• ' l' ice com t 1 lg. 4 1 Censtoes , :1 C)C)m, „ I sealed copier , . u rt7N) I ) ) 0 C) (3 0 _ 1 i Simples Intact 1 I 1 I 1 _ 1 , Pace Analytical Services,LLC yical 9800 Kincey Ave. Suite 100 aceAnalJq/� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 August 10, 2021 Michael Pfeifer S&M E 3201 Spring Forest Road Raleigh, NC 27616 RE: Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Dear Michael Pfeifer: Enclosed are the analytical results for sample(s)received by the laboratory on August 02, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte • Pace Analytical Services-Eden • Pace Analytical Services-Raleigh If you have any questions concerning this report, please feel free to contact me. Sincerely, a, 4.)altartj Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures Ito uA'ga REPORT OF LABORATORY ANALYSIS ° AI This report shall not be reproduced,except in full, ,,,,11111111111 without the written consent of Pace Analytical Services,LLC. Page 1 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/' Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 CERTIFICATIONS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Pace Analytical Services Raleigh 4915 Waters Edge Dr.#120, Raleigh, NC 27606 North Carolina Drinking Water Certification#: 37731 North Carolina Wastewater Certification#:67 Pace Analytical Services Charlotte 9800 Kincey Ave.Ste 100, Huntersville, NC 28078 South Carolina Certification#: 99006001 Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#: E87627 North Carolina Drinking Water Certification#: 37706 Kentucky UST Certification#: 84 North Carolina Field Services Certification#: 5342 Virginia/VELAP Certification#:460221 North Carolina Wastewater Certification#: 12 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville, NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#: E87648 South Carolina Certification#: 99030001 North Carolina Drinking Water Certification#: 37712 Virginia/VELAP Certification#:460222 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification#:633 North Carolina Drinking Water Certification#: 37738 Virginia/VELAP Certification#:460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.caim (704)875-9092 SAMPLE ANALYTE COUNT Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92552838001 MW-183 SM 2540C-2011 LRB 1 PASI-E EPA200.7 Rev 4.4 1994 SH1 4 PASI-A EPA 8260D PM1 63 PASI-C SM 9222D-2006 WT 1 PASI-R EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 4500-CI-E-2011 DMN 1 PASI-A PASI-A= Pace Analytical Services-Asheville PASI-C= Pace Analytical Services-Charlotte PASI-E= Pace Analytical Services-Eden PASI-R= Pace Analytical Services-Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 23 Pace Analytical Services,LLC o aceAnalytical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08/02/21 10:30 Received: 08/02/21 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services-Eden Total Dissolved Solids 75.0 mg/L 25.0 1 08/04/21 17:51 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Cadmium <1.0 ug/L 1.0 1 08/05/21 13:40 08/06/21 01:23 7440-43-9 Chromium <5.0 ug/L 5.0 1 08/05/21 13:40 08/06/21 01:23 7440-47-3 Lead <5.0 ug/L 5.0 1 08/05/21 13:40 08/06/21 01:23 7439-92-1 Zinc <10.0 ug/L 10.0 1 08/05/21 13:40 08/06/21 01:23 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone <25.0 ug/L 25.0 1 08/10/21 11:40 67-64-1 Benzene <1.0 ug/L 1.0 1 08/10/21 11:40 71-43-2 Bromobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 108-86-1 Bromochloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 74-97-5 Bromodichloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-27-4 Bromoform <1.0 ug/L 1.0 1 08/10/21 11:40 75-25-2 Bromomethane <2.0 ug/L 2.0 1 08/10/21 11:40 74-83-9 2-Butanone(MEK) <5.0 ug/L 5.0 1 08/10/21 11:40 78-93-3 Carbon tetrachloride <1.0 ug/L 1.0 1 08/10/21 11:40 56-23-5 Chlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 108-90-7 Chloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-00-3 Chloroform <1.0 ug/L 1.0 1 08/10/21 11:40 67-66-3 Chloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 74-87-3 v2 2-Chlorotoluene <1.0 ug/L 1.0 1 08/10/21 11:40 95-49-8 4-Chlorotoluene <1.0 ug/L 1.0 1 08/10/21 11:40 106-43-4 1,2-Dibromo-3-chloropropane <2.0 ug/L 2.0 1 08/10/21 11:40 96-12-8 Dibromochloromethane <1.0 ug/L 1.0 1 08/10/21 11:40 124-48-1 1,2-Dibromoethane(EDB) <1.0 ug/L 1.0 1 08/10/21 11:40 106-93-4 Dibromomethane <1.0 ug/L 1.0 1 08/10/21 11:40 74-95-3 1,2-Dichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 95-50-1 1,3-Dichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 541-73-1 1,4-Dichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 106-46-7 Dichlorodifluoromethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-71-8 1,1-Dichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-34-3 1,2-Dichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 107-06-2 1,1-Dichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 75-35-4 cis-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 156-59-2 trans-1,2-Dichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 156-60-5 1,2-Dichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 78-87-5 1,3-Dichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 142-28-9 2,2-Dichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 594-20-7 1,1-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 563-58-6 cis-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 10061-01-5 trans-1,3-Dichloropropene <1.0 ug/L 1.0 1 08/10/21 11:40 10061-02-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 23 Pace Analytical Services,LLC o aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08/02/21 10:30 Received: 08/02/21 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Diisopropyl ether <1.0 ug/L 1.0 1 08/10/21 11:40 108-20-3 Ethylbenzene <1.0 ug/L 1.0 1 08/10/21 11:40 100-41-4 Hexachloro-1,3-butadiene <2.0 ug/L 2.0 1 08/10/21 11:40 87-68-3 IK 2-Hexanone <5.0 ug/L 5.0 1 08/10/21 11:40 591-78-6 p-lsopropyltoluene <1.0 ug/L 1.0 1 08/10/21 11:40 99-87-6 Methylene Chloride <5.0 ug/L 5.0 1 08/10/21 11:40 75-09-2 4-Methyl-2-pentanone(MIBK) <5.0 ug/L 5.0 1 08/10/21 11:40 108-10-1 Methyl-tert-butyl ether <1.0 ug/L 1.0 1 08/10/21 11:40 1634-04-4 Naphthalene <1.0 ug/L 1.0 1 08/10/21 11:40 91-20-3 Styrene <1.0 ug/L 1.0 1 08/10/21 11:40 100-42-5 1,1,1,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 630-20-6 1,1,2,2-Tetrachloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 79-34-5 Tetrachloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 127-18-4 Toluene <1.0 ug/L 1.0 1 08/10/21 11:40 108-88-3 1,2,3-Trichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 87-61-6 1,2,4-Trichlorobenzene <1.0 ug/L 1.0 1 08/10/21 11:40 120-82-1 1,1,1-Trichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 71-55-6 1,1,2-Trichloroethane <1.0 ug/L 1.0 1 08/10/21 11:40 79-00-5 Trichloroethene <1.0 ug/L 1.0 1 08/10/21 11:40 79-01-6 Trichlorofluoromethane <1.0 ug/L 1.0 1 08/10/21 11:40 75-69-4 1,2,3-Trichloropropane <1.0 ug/L 1.0 1 08/10/21 11:40 96-18-4 Vinyl acetate <2.0 ug/L 2.0 1 08/10/21 11:40 108-05-4 Vinyl chloride <1.0 ug/L 1.0 1 08/10/21 11:40 75-01-4 Xylene(Total) <1.0 ug/L 1.0 1 08/10/21 11:40 1330-20-7 m&p-Xylene <2.0 ug/L 2.0 1 08/10/21 11:40 179601-23-1 o-Xylene <1.0 ug/L 1.0 1 08/10/21 11:40 95-47-6 Surrogates 4-Bromofluorobenzene(S) 102 % 70-130 1 08/10/21 11:40 460-00-4 1,2-Dichloroethane-d4(S) 106 % 70-130 1 08/10/21 11:40 17060-07-0 Toluene-d8(S) 97 % 70-130 1 08/10/21 11:40 2037-26-5 MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method:SM 9222D-2006 Pace Analytical Services-Raleigh Fecal Coliforms ND CFU/100 mL 1.0 1 08/02/21 14:48 08/03/21 15:41 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia <0.10 mg/L 0.10 1 08/06/21 11:55 7664-41-7 353.2 Nitrogen,NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen, Nitrate 0.19 mg/L 0.040 1 08/04/21 01:41 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 ANALYTICAL RESULTS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Sample: MW-183 Lab ID: 92552838001 Collected: 08/02/21 10:30 Received: 08/02/21 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus <0.050 mg/L 0.050 1 08/04/21 18:46 08/04/21 23:01 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 15.3 mg/L 1.0 1 08/09/21 09:54 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 638125 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92552838001 METHOD BLANK: 3350306 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L <25.0 25.0 08/04/21 17:51 LABORATORY CONTROL SAMPLE: 3350307 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 256 102 90-110 SAMPLE DUPLICATE: 3350308 92552838001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 75.0 73.0 3 Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 638267 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552838001 METHOD BLANK: 3350753 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L <1.0 1.0 08/05/21 23:35 Chromium ug/L <5.0 5.0 08/05/21 23:35 Lead ug/L <5.0 5.0 08/05/21 23:35 Zinc ug/L <10.0 10.0 08/05/21 23:35 LABORATORY CONTROL SAMPLE: 3350754 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 523 105 85-115 Chromium ug/L 500 527 105 85-115 Lead ug/L 500 533 107 85-115 Zinc ug/L 500 502 100 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3350755 3350756 MS MSD 92551262001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 499 500 100 100 70-130 0 Chromium ug/L ND 500 500 484 488 97 98 70-130 1 Lead ug/L ND 500 500 488 486 97 97 70-130 0 Zinc ug/L 71.5 500 500 547 546 95 95 70-130 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3350757 3350758 MS MSD 92552445001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 495 494 99 99 70-130 0 Chromium ug/L ND 500 500 483 483 97 97 70-130 0 Lead ug/L ND 500 500 489 484 98 97 70-130 1 Zinc ug/L ND 500 500 476 476 94 94 70-130 0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 639115 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92552838001 METHOD BLANK: 3355094 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L <1.0 1.0 08/10/21 10:29 1,1,1-Trichloroethane ug/L <1.0 1.0 08/10/21 10:29 1,1,2,2-Tetrachloroethane ug/L <1.0 1.0 08/10/21 10:29 1,1,2-Trichloroethane ug/L <1.0 1.0 08/10/21 10:29 1,1-Dichloroethane ug/L <1.0 1.0 08/10/21 10:29 1,1-Dichloroethene ug/L <1.0 1.0 08/10/21 10:29 1,1-Dichloropropene ug/L <1.0 1.0 08/10/21 10:29 1,2,3-Trichlorobenzene ug/L <1.0 1.0 08/10/21 10:29 1,2,3-Trichloropropane ug/L <1.0 1.0 08/10/21 10:29 1,2,4-Trichlorobenzene ug/L <1.0 1.0 08/10/21 10:29 1,2-Dibromo-3-chloropropane ug/L <2.0 2.0 08/10/21 10:29 1,2-Dibromoethane(EDB) ug/L <1.0 1.0 08/10/21 10:29 1,2-Dichlorobenzene ug/L <1.0 1.0 08/10/21 10:29 1,2-Dichloroethane ug/L <1.0 1.0 08/10/21 10:29 1,2-Dichloropropane ug/L <1.0 1.0 08/10/21 10:29 1,3-Dichlorobenzene ug/L <1.0 1.0 08/10/21 10:29 1,3-Dichloropropane ug/L <1.0 1.0 08/10/21 10:29 1,4-Dichlorobenzene ug/L <1.0 1.0 08/10/21 10:29 2,2-Dichloropropane ug/L <1.0 1.0 08/10/21 10:29 2-Butanone(MEK) ug/L <5.0 5.0 08/10/21 10:29 2-Chlorotoluene ug/L <1.0 1.0 08/10/21 10:29 2-Hexanone ug/L <5.0 5.0 08/10/21 10:29 4-Chlorotoluene ug/L <1.0 1.0 08/10/21 10:29 4-Methyl-2-pentanone(MIBK) ug/L <5.0 5.0 08/10/21 10:29 Acetone ug/L <25.0 25.0 08/10/21 10:29 Benzene ug/L <1.0 1.0 08/10/21 10:29 Bromobenzene ug/L <1.0 1.0 08/10/21 10:29 Bromochloromethane ug/L <1.0 1.0 08/10/21 10:29 Bromodichloromethane ug/L <1.0 1.0 08/10/21 10:29 Bromoform ug/L <1.0 1.0 08/10/21 10:29 Bromomethane ug/L <2.0 2.0 08/10/21 10:29 Carbon tetrachloride ug/L <1.0 1.0 08/10/21 10:29 Chlorobenzene ug/L <1.0 1.0 08/10/21 10:29 Chloroethane ug/L <1.0 1.0 08/10/21 10:29 Chloroform ug/L <1.0 1.0 08/10/21 10:29 Chloromethane ug/L <1.0 1.0 08/10/21 10:29 v2 cis-1,2-Dichloroethene ug/L <1.0 1.0 08/10/21 10:29 cis-1,3-Dichloropropene ug/L <1.0 1.0 08/10/21 10:29 Dibromochloromethane ug/L <1.0 1.0 08/10/21 10:29 Dibromomethane ug/L <1.0 1.0 08/10/21 10:29 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 METHOD BLANK: 3355094 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dichlorodifluoromethane ug/L <1.0 1.0 08/10/21 10:29 Diisopropyl ether ug/L <1.0 1.0 08/10/21 10:29 Ethylbenzene ug/L <1.0 1.0 08/10/21 10:29 Hexachloro-1,3-butadiene ug/L <2.0 2.0 08/10/21 10:29 IK m&p-Xylene ug/L <2.0 2.0 08/10/21 10:29 Methyl-tert-butyl ether ug/L <1.0 1.0 08/10/21 10:29 Methylene Chloride ug/L <5.0 5.0 08/10/21 10:29 Naphthalene ug/L <1.0 1.0 08/10/21 10:29 o-Xylene ug/L <1.0 1.0 08/10/21 10:29 p-lsopropyltoluene ug/L <1.0 1.0 08/10/21 10:29 Styrene ug/L <1.0 1.0 08/10/21 10:29 Tetrachloroethene ug/L <1.0 1.0 08/10/21 10:29 Toluene ug/L <1.0 1.0 08/10/21 10:29 trans-1,2-Dichloroethene ug/L <1.0 1.0 08/10/21 10:29 trans-1,3-Dichloropropene ug/L <1.0 1.0 08/10/21 10:29 Trichloroethene ug/L <1.0 1.0 08/10/21 10:29 Trichlorofluoromethane ug/L <1.0 1.0 08/10/21 10:29 Vinyl acetate ug/L <2.0 2.0 08/10/21 10:29 Vinyl chloride ug/L <1.0 1.0 08/10/21 10:29 Xylene(Total) ug/L <1.0 1.0 08/10/21 10:29 1,2-Dichloroethane-d4(S) % 105 70-130 08/10/21 10:29 4-Bromofluorobenzene(S) % 104 70-130 08/10/21 10:29 Toluene-d8(S) % 98 70-130 08/10/21 10:29 LABORATORY CONTROL SAMPLE: 3355095 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.5 105 70-130 1,1,1-Trichloroethane ug/L 50 50.3 101 70-130 1,1,2,2-Tetrachloroethane ug/L 50 50.9 102 70-130 1,1,2-Trichloroethane ug/L 50 48.7 97 70-130 1,1-Dichloroethane ug/L 50 49.0 98 70-130 1,1-Dichloroethene ug/L 50 49.9 100 70-132 1,1-Dichloropropene ug/L 50 49.9 100 70-131 1,2,3-Trichlorobenzene ug/L 50 56.2 112 70-134 1,2,3-Trichloropropane ug/L 50 52.2 104 70-130 1,2,4-Trichlorobenzene ug/L 50 56.0 112 70-130 1,2-Dibromo-3-chloropropane ug/L 50 52.7 105 70-132 1,2-Dibromoethane(EDB) ug/L 50 52.3 105 70-130 1,2-Dichlorobenzene ug/L 50 53.7 107 70-130 1,2-Dichloroethane ug/L 50 49.2 98 70-130 1,2-Dichloropropane ug/L 50 48.3 97 70-130 1,3-Dichlorobenzene ug/L 50 53.9 108 70-130 1,3-Dichloropropane ug/L 50 52.8 106 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 LABORATORY CONTROL SAMPLE: 3355095 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 54.5 109 70-130 2,2-Dichloropropane ug/L 50 50.4 101 70-130 2-Butanone(MEK) ug/L 100 95.5 96 70-133 2-Chlorotoluene ug/L 50 54.6 109 70-130 2-Hexanone ug/L 100 98.9 99 70-130 4-Chlorotoluene ug/L 50 52.3 105 70-130 4-Methyl-2-pentanone(MIBK) ug/L 100 93.7 94 70-130 Acetone ug/L 100 97.4 97 70-144 Benzene ug/L 50 49.3 99 70-130 Bromobenzene ug/L 50 53.0 106 70-130 Bromochloromethane ug/L 50 47.2 94 70-130 Bromodichloromethane ug/L 50 48.2 96 70-130 Bromoform ug/L 50 49.2 98 70-131 Bromomethane ug/L 50 44.4 89 30-177 Carbon tetrachloride ug/L 50 52.9 106 70-130 Chlorobenzene ug/L 50 53.2 106 70-130 Chloroethane ug/L 50 40.1 80 46-131 Chloroform ug/L 50 48.1 96 70-130 Chloromethane ug/L 50 35.7 71 49-130 v3 cis-1,2-Dichloroethene ug/L 50 47.9 96 70-130 cis-1,3-Dichloropropene ug/L 50 48.9 98 70-130 Dibromochloromethane ug/L 50 52.5 105 70-130 Dibromomethane ug/L 50 47.3 95 70-130 Dichlorodifluoromethane ug/L 50 50.1 100 52-134 Diisopropyl ether ug/L 50 45.0 90 70-131 Ethylbenzene ug/L 50 53.0 106 70-130 Hexachloro-1,3-butadiene ug/L 50 51.5 103 70-131 IK m&p-Xylene ug/L 100 106 106 70-130 Methyl-tert-butyl ether ug/L 50 48.3 97 70-130 Methylene Chloride ug/L 50 46.6 93 68-130 Naphthalene ug/L 50 53.5 107 70-133 o-Xylene ug/L 50 52.3 105 70-130 p-lsopropyltoluene ug/L 50 56.2 112 70-130 Styrene ug/L 50 52.4 105 70-130 Tetrachloroethene ug/L 50 52.8 106 70-130 Toluene ug/L 50 48.6 97 70-130 trans-1,2-Dichloroethene ug/L 50 49.4 99 70-130 trans-1,3-Dichloropropene ug/L 50 47.7 95 70-130 Trichloroethene ug/L 50 49.9 100 70-130 Trichlorofluoromethane ug/L 50 47.2 94 61-130 Vinyl acetate ug/L 100 106 106 70-140 Vinyl chloride ug/L 50 45.8 92 59-142 Xylene(Total) ug/L 150 159 106 70-130 1,2-Dichloroethane-d4(S) % 102 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 96 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/ Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3355096 3355097 MS MSD 92553998011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 200 200 270 267 135 133 70-135 1 1,1,1-Trichloroethane ug/L ND 200 200 300 270 150 135 70-148 10 M1 1,1,2,2-Tetrachloroethane ug/L ND 200 200 235 260 118 130 70-131 10 1,1,2-Trichloroethane ug/L ND 200 200 278 250 139 125 70-136 11 M1 1,1-Dichloroethane ug/L ND 200 200 294 256 147 128 70-147 14 1,1-Dichloroethene ug/L ND 200 200 313 272 156 136 70-158 14 1,1-Dichloropropene ug/L ND 200 200 291 266 145 133 70-149 9 1,2,3-Trichlorobenzene ug/L ND 200 200 182 275 91 138 68-140 41 R1 1,2,3-Trichloropropane ug/L ND 200 200 247 259 123 129 67-137 5 1,2,4-Trichlorobenzene ug/L ND 200 200 173 265 87 132 70-139 42 R1 1,2-Dibromo-3-chloropropane ug/L ND 200 200 175 265 88 132 69-136 41 R1 1,2-Dibromoethane(EDB) ug/L ND 200 200 264 259 132 130 70-137 2 1,2-Dichlorobenzene ug/L ND 200 200 238 269 119 134 70-133 12 M1 1,2-Dichloroethane ug/L ND 200 200 293 253 146 126 67-138 15 M1 1,2-Dichloropropane ug/L ND 200 200 279 251 140 125 70-138 11 M1 1,3-Dichlorobenzene ug/L ND 200 200 275 271 138 136 70-133 1 M1 1,3-Dichloropropane ug/L ND 200 200 263 267 131 133 70-136 2 1,4-Dichlorobenzene ug/L ND 200 200 267 271 134 135 70-133 1 M1 2,2-Dichloropropane ug/L ND 200 200 297 265 149 132 52-155 12 2-Butanone(MEK) ug/L ND 400 400 523 492 131 123 61-147 6 2-Chlorotoluene ug/L ND 200 200 349 283 175 142 70-141 21 M1 2-Hexanone ug/L ND 400 400 455 519 114 130 67-139 13 4-Chlorotoluene ug/L ND 200 200 327 269 164 134 70-135 20 M1 4-Methyl-2-pentanone(MIBK) ug/L ND 400 400 499 492 125 123 67-136 1 Acetone ug/L ND 400 400 553 472 138 118 55-159 16 Benzene ug/L ND 200 200 284 264 142 132 67-150 7 Bromobenzene ug/L ND 200 200 342 271 171 136 70-134 23 M1 Bromochloromethane ug/L ND 200 200 292 241 146 120 70-146 19 Bromodichloromethane ug/L ND 200 200 288 250 144 125 70-138 14 M1 Bromoform ug/L ND 200 200 236 239 118 119 57-138 1 Bromomethane ug/L ND 200 200 429 324 211 159 10-200 28 M1 Carbon tetrachloride ug/L ND 200 200 321 294 160 147 70-147 9 M1 Chlorobenzene ug/L ND 200 200 282 271 141 135 70-137 4 M1 Chloroethane ug/L ND 200 200 319 256 160 128 51-166 22 Chloroform ug/L 26.3 200 200 316 273 145 123 70-144 15 M1 Chloromethane ug/L ND 200 200 225 231 112 115 24-161 2 v3 cis-1,2-Dichloroethene ug/L 120 200 200 423 370 152 125 67-148 13 M1 cis-1,3-Dichloropropene ug/L ND 200 200 276 251 138 126 70-142 9 Dibromochloromethane ug/L ND 200 200 272 259 136 130 68-138 5 Dibromomethane ug/L ND 200 200 281 242 140 121 70-134 15 M1 Dichlorodifluoromethane ug/L ND 200 200 306 269 153 135 43-155 13 Diisopropyl ether ug/L ND 200 200 241 232 120 116 65-146 4 Ethylbenzene ug/L ND 200 200 286 275 143 138 68-143 4 Hexachloro-1,3-butadiene ug/L ND 200 200 173 264 86 132 62-151 42 IK,R1 m&p-Xylene ug/L ND 400 400 582 549 145 137 53-157 6 Methyl-tert-butyl ether ug/L ND 200 200 262 245 131 122 59-156 7 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3355096 3355097 MS MSD 92553998011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Methylene Chloride ug/L ND 200 200 293 248 146 124 64-148 17 Naphthalene ug/L ND 200 200 174 260 87 130 57-150 40 R1 o-Xylene ug/L ND 200 200 280 265 140 133 68-143 5 p-lsopropyltoluene ug/L ND 200 200 288 285 144 143 70-141 1 M1 Styrene ug/L ND 200 200 281 265 140 133 70-136 6 M1 Tetrachloroethene ug/L ND 200 200 272 276 136 138 70-139 2 Toluene ug/L ND 200 200 287 258 144 129 47-157 11 trans-1,2-Dichloroethene ug/L ND 200 200 301 262 150 131 70-149 14 M1 trans-1,3-Dichloropropene ug/L ND 200 200 272 245 136 122 70-138 10 Trichloroethene ug/L 903 200 200 1230 1180 162 141 70-149 4 M1 Trichlorofluoromethane ug/L ND 200 200 304 265 152 132 61-154 14 Vinyl acetate ug/L ND 400 400 575 543 144 136 48-156 6 Vinyl chloride ug/L ND 200 200 304 248 152 124 55-172 20 Xylene(Total) ug/L ND 600 600 862 814 144 136 66-145 6 1,2-Dichloroethane-d4(S) % 111 99 70-130 4-Bromofluorobenzene(S) % 99 100 70-130 Toluene-d8(S) % 103 98 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 637955 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF)-RAL Laboratory: Pace Analytical Services-Raleigh Associated Lab Samples: 92552838001 METHOD BLANK: 3349054 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 08/03/21 15:41 SAMPLE DUPLICATE: 3349055 92552832001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 20000 18000 11 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 638335 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552838001 METHOD BLANK: 3351143 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Ammonia mg/L <0.10 0.10 08/06/21 11:35 LABORATORY CONTROL SAMPLE: 3351144 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen,Ammonia mg/L 5 4.9 97 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3351145 3351146 MS MSD 92552488007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen,Ammonia mg/L ND 5 5 5.2 5.2 104 104 90-110 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3351147 3351148 MS MSD 92552488008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen,Ammonia mg/L ND 5 5 5.2 5.2 104 104 90-110 0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 637831 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite, Unpres. Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552838001 METHOD BLANK: 3348686 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L <0.040 0.040 08/04/21 01:30 LABORATORY CONTROL SAMPLE: 3348687 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.6 105 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3348688 3348689 MS MSD 92552784001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 8.4 1.5 1.5 9.3 9.5 63 78 90-110 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 638076 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552838001 METHOD BLANK: 3349910 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L <0.050 0.050 08/04/21 21:59 LABORATORY CONTROL SAMPLE: 3349911 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.3 91 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3349912 3349913 MS MSD 92551679001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 2.8 2.5 2.5 5.6 5.5 111 109 90-110 1 M1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3349914 3349915 MS MSD 92551748001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.7 2.6 106 106 90-110 1 Results presented on this page are in the units indicated by the"Units'.column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/� Huntersville,NC 28078 www.pacellabs.caim (704)875-9092 QUALITY CONTROL DATA Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 QC Batch: 638833 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92552838001 METHOD BLANK: 3353907 Matrix: Water Associated Lab Samples: 92552838001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L <1.0 1.0 08/09/21 09:40 LABORATORY CONTROL SAMPLE: 3353908 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 20.9 105 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3353909 3353910 MS MSD 92552488002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 416 10 10 433 413 173 -29 90-110 5 M1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3353911 3353912 MS MSD 92552488003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 362 10 10 353 362 -83 6 90-110 3 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 QUALIFIERS Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 DEFINITIONS DF-Dilution Factor, if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s)did not meet method acceptance criteria;this result should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. R1 RPD value was outside control limits. v2 The continuing calibration verification was below the method acceptance limit.The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit.Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 23 Pace Analytical Services,LLC aceAnal tical 9800 Kincey Ave. Suite 100 Jq/'� Huntersville,NC 28078 www.pacallabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CPC-Guilford County-Orphan Pace Project No.: 92552838 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92552838001 MW-183 SM 2540C-2011 638125 92552838001 MW-183 EPA 200.7 Rev 4.4 1994 638267 EPA 200.7 Rev 4.4 1994 638432 92552838001 MW-183 EPA 8260D 639115 92552838001 MW-183 SM 9222D-2006 637955 SM 9222D-2006 637957 92552838001 MW-183 EPA 350.1 Rev 2.0 1993 638335 92552838001 MW-183 EPA 353.2 Rev 2.0 1993 637831 92552838001 MW-183 EPA 365.1 Rev 2.0 1993 638076 EPA 365.1 Rev 2.0 1993 638146 92552838001 MW-183 SM 4500-CI-E-2011 638833 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 08/10/2021 03:48 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 23 ' . Document Name: Documnient Revised:October 23,,2020 , 21,A124ttai. Saelpie Condition Upon itecelptiSaNt) Pala 1.of 2 Document No.: Issuirre Authority: . IFCAit-C143134tev.07 Pace Quell/Office Laboratory recelltIng samples: 1 Asheville E] EdanC] Greenwood 0 lfuntersvfile 0 RalelghV Medmalcsville0 Atlanta° KemartvilinCI , , ,(, i;_,• Client Narita: i„., i Proiect WO* . 92552838 Carder: Fed Ex °UPS [j S °Client 111111 II 11 ll I I 1111 III D Comtherclal K..Pace 00ther: 92552838 Custody See)Present? 0Yes Zgo Seals Intact? 0Yes L1No Derellaitiali Person Exendelne Contents:n r I/ Packing Material: 0Bubbie Wrap ` greubble Bags 0None 0 Other Blologial Tissue Frozen? Therrnometer: [Yes 0110 471N/A Kiwet Owe ONone 11-1-0 ec Type at lom . Correction Factor: an Add/Subtract rc) 0! V Cooler Temp: Temp should be ibeve Freezing to 6•C . °Semple'autoftemp criteria.Simples on ke,cuoling pass Cooler Temp Corrected('C).; has began USDA Regulated Soil(pa N/A,water sample) .7.Dl. ...... . . ?. ... ..-. .-tone within the United Staten CA,NY,or SC(check maps)? Did sarnplesoriglnatefrom rforeign source(Mternatknally, .112.4 r40 - Tiidir-dlii RiviiTirtiffitrrfalUtWrjrae—UNtr-- ---- --• Comments/Orscrepancy: Chain of C -,.. Present? (des No III WA 1. Sa .les Arrived within Hold lime? Yes °No ON/A 2. Short Hold Time Analysts(<72 hr.)? gYrs ONO EIN/A 3. . I Rush Turn Around Time Requested? °Yes (!io ON/A 4. Sufficient Volume? Cirks _ON* ON/A 5. 1 I Correct Containers Used? Zee ONo ON/A 6. • -Pace Containers Used? flYes 111 No M N/A , Containers Intact? XrYes IN© •N/A 7. - i Dissolved - fs:Sam•les Reid Filtered? Yes 111Na ti A R. , , Sample Labels Match COC? pafes °No ON/A 9. -Includes Dateirane 0 Anal is Matrix: Hea• •,ce In VOA Vials(>5-6mm 7 ply" 1 g rio ON A 10. . Trip Blank Present? , Oyes °No DNA 11. Trip Blank Custody Seals Present? illYes RHO [ N/A CCM hitENTS/SAMPLE DISCREPANCY Field Data Required? °Yes °Nu Lot 10 of split containers; — CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/lime: Prefect Manager SCURF Review: Date; _ Prnfort Manager SRF Review: ° Date: Page 21 of 23 Docurnarrt Mamas DOCteneilt Eten45114:Octobat 28,2020 altil*tti I , .le Candwon U.., .— - . 2 of 2 Dm:insert Mo.: Issuing&Oddly: F-C4:143433.41ev.07 Pk*Carolinas Magee Cake *Check mark topbalf of bOx If pH and/or dechlorfnatIon Is Pfillec W 0# ' 92552838 verlfled and*At*the acceptance range for preservation m PM IAMB Due Date: 08/09/21 ilks. • imptteas:VOA,CoNform,TOC,Oa and&MEI,OR0/241,5(wear)DOC.LL.Hig CLIENT: 92-UNE RAL "%nom half of box Is to list number of bottles I 1 •r4 1 1 I i 1 I..., 1 -e i 1 111111 3 I I • 11111 1111 111/111 ' ' . i 1 illvdMillitallitelnelleffillaWINKINIIIIIII 1111111111111k1IN11111111E11111111111111E11111111 , 11111.1111111NOMMINIVIIIIIIIIIIIIIM,111111 1 4 11111111111111111111111111111111111111111111111111111 insimnrommummimommummortmo imorminesimminemomomminamm 1 7 11111111111111L11111111111111111111111111 I 11111b1011111 . 111111111111111111111111111E211111111111 111111E1111111 11111111111111111111111111111111111111111111111111111111 11111111111111111116,11N111111111 111111E1M 1111 immonemem 11111111111111111111111E111111111 111611111111111111111111111.11111111111111111111111 II . pH Adjustment Log for Preserved Samples Sample ro Type of Preservative pH upon receipt Date preservation adjusted Time prase/Um Amount of Preservative lot$ adjusted added Note; Whenever there Is a discrepancy affecting North Caroline compliance samples,a copy of this form will he sent la theNarth Carolloy gEHNe c4ru1Tation me ri,e. Out of hod,Incorrect preservative,out of temp,incorrect containers . ..,. .. . . . . Page 22 of 23 CZ;C)CZ abed -,,,I. 7e 4„,..,, ,,,r5..;`,7,-nt,'7AMPII!llt TE,,M1 4 7 ')l ,,.•0., T.11,°g,',,:`,t. -'r, 1,,i' ,,, I iiliff [ ... ,,=. 1,41:1,011:,t41.1?';'-‘1413,1kr,'-it„' . . pliy,?,41,,4 Mil 1,10, _ a 12.- 1' - W . •:„.' -1 I 11'1 f I •;„"'Z"..4, . 1 2 pi:3 ,,,,•,' 1 i : ;12 l• ...--.. 31 9,$ tr 0 t 1 § 1, )- . li,',0 li kl 50 rs' 5 R. 1 1 v Y. ? i011 a • 1 ' 0 ' 1 4 ,r- ,„„„„,,,,_ — ft PA . I-- 1 1 1 1 lMATRIX COM (sea vald codes to lern a SAMPLE TYPE pll6GRAS C.CONIP) ' k I ?le A e 11 O. A 4 IN g a 0 4 0 — ''i .,,..A._ A. 9 I a, .......6 4 C 2 I .-• , 0 ,0 , Or d . • ip SAMPLEIEMP AT COLLECT „„„ION 2, on (1) -a.OF CONTAINERS __ - g,'- 1 iii9111 wo) .. ,......._ __ c _ N - 5 Unpresemt 1 711 y g $ g th. "4 , r ?o • [ 1 g ° 0 \l•., NA Nli— 1 . -4 0 .. - 4, -r- , _ N HOI 1 IS ,g H. CI "*"* g P 8 la` c = 0 E ID Ltii,.... 1044,,I ' "4 '' Air ,,,,,,,- ,4k,.., ko"ri. ( i , -- 1-- — ' — I NeOH Na28203 Methan _ re or Zr' a 2 ,)-.1 ' a% m 0 toe'A'..... :A g °- i .2 ,. . , I Other 4.1 SI iii, ,01,4 a nd 0 - J 19 V914 j •ffin **I:5 e 7,i ('' Chloride - 1"?, , . - -, o , .......... Fethe Calearm(8 to ! On g I i.. - —— - _ _ - ?c Athreerne,003045rus 4 1:7 F. Narrow 08 Pr) ,.. , g c -RR T8:01 vOarescated Solids ..., = 1 1 -C'.. r, , 1 , ' . ............ EL .4. us( - (.. _ . ifil lli 'lli . 10 ......, 1„......L.: . TEMP In C Residual Chlorine(WM t ',,,,tr, I -,c eceived , •"""'"'"1 . R on 4,4 I ) c' r,„..,, ':,.,"1,, ., "3 CY cy) ;:,' , . , . , Gusto* Sealed ',IT Cooler Samples 1/4..k,) ',,*.? 01 l'• O'' 'lt lli7,1