HomeMy WebLinkAboutNCG550696_Lab Data_20220127ENCO Laboratories
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102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: 919.467.3090 FAX: 919.467.3515
Thursday, January 27, 2022
McFarland Septic (WA021)
Attn: Waylon McFarland
6801 Mt. Hermon Church Road
Durham, NC 27705
RE: Laboratory Results for
Project Number: 1609 US HWY 15 501 S., Project Name/Desc: Wastewater
ENCO Workorder(s): CF00345
Dear Waylon McFarland,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, January 10, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Amanda L. Gaines
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 1 of 11
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Effluent -1609 U5 HWY 15 501 S.
Lab ID: CF00345-01
Sampled: 01/10/22 11:00
Received: 01/10/22 11:52
Parameter
CALC
Colilert 18
SM 2540D-2011
SM 5210 8-2011
[CALC]
NO PREP
NO PREP
NO PREP
Hold Date/Time(s)
02/07.22
01/10122 18:55 01/11..22
01/17122
01/12/22 11:00
pren Data/Timefsl
01/20/22 08:57
12:17 01/10/22 14:13
01/13/22 18:06
01/12/22 08:34
Analysis Date/Timefal
01/21/22 12:37
01/11/22 11:15
01/13/22 18:06
01/12/22 08:34
Client ID: Effluent -1609 US HWY IS 501 5.
Lab ID: CF00345-01RE1
Sampled: 01/10/22 11:00
Received: 01/10/22 11:52
PSIOma=
EPA 351.2
EPA 353.2
EPA 365.4
Ementation
Same
NO PREP
Same
Hold Date/Timers)
02/07r22
02/07/22
02/07/22
preo Date/Time(s)
01/17/22
01/20/22
01/17/22
12:18
08:57
12:18
Analysis Datellimefs1
01/21/22 12:37
01/20/22 13:20
01/21/22 12:55
client ID: Effluent -1609 US HWY 15 501 5.
Lab ID: CF00345-01RE2
Sampled: 01/10/22 11:00
Received: 01/10/22 11:52
ParamESEr
EPA 350.1
EDaQa ration
NO PREP
Hold Date!Timefsl
02/07/22
Free Date/Timers)
01/18/22 14:29
p�vsis Date/Tlmefsl
01/19/22 14:36
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 2 of 11
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SAMPLE DETECTION SUMMARY
Client ID: Effluent -1609 US HWY 15 501 S.
Lab ID: CF00345-01
Ankle
Biochemical Oxygen Demand
Coliform, Fecal
Total Nitrogen - Total
Total Suspended Solids
Client ID: Effluent -1609 US HWY 15 501 S.
AnaMe
Phosphorus- Total
Total Kjeldahl Nitrogen
Client ID: Effluent -1609 US HWY 15 501 S.
Anal&
Ammonia as N
Keau1 EINt
>210
2.0
85 D
25
KmHa BEL
9.7 0
85 D
PaiNStif112
84 0
MQL
2.0
1.0
1.3
8.3
EQL
2.0
1.0
2.4
8.3
tab ID: CF00345-01RE1
Unita
mg/L
MPN/100 mL
mg/L
mg/L
Method
SM 5210 B-2011
Coble- t 18
CALC
SM 2540D-2011
Klan
B-02
MQl
0.25
1.3
YQL
1.0
2.4
Lab ID: CF00345-01RE2
MQl
4.0
EQL
9.0
Malta
mg/L
mg/L
Untta
mg/L
Naiad
EPA 365.4
EPA 351.2
MBA19d
EPA 350.1
Mtn
i* L
1
i inu This repot relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 3 of 11
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ANALYTICAL RESULTS
Description: Effluent -1609 US HWY 15 501 S.
Matrix: Waste Water
Project: Wastewater
Lab Sample ID:CF00345-01
Sampled:01/10/22 11:00
Sampled Sy:Brendan Towner
Received: 01/10/22 11:52
Work Order: CF00345
Classical Chemistry Parameters
^ - ENcn Cary cr,arfad a fj4e INC 591.1
Apalvte fCAs Numberl
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand"
Nitrate/Nitrite as NA
Phosphorus[7723-14-0]^
Total gjeldahl Nitrogen^
Total Nitrogen [17778-88-0]
Total Suspended Solids".
Multi Elsa UM* RE I1QL Mk Ikea Method Mai BY Matra
84 D mg/L 90 4.0 9.0 2A18023 EPA 350.1 01/19/22 14:36 )AH
>210 mg/L 1 2.0 2.0 2A12004 SM 5210 6-2011 01/12/22 08:34 JOC 13-02
< 0.041 mg/L 1 0.041 0.10 2A20013 EPA 353.2 01/20/22 13:20 )AH
9.7 D mg/L 10 0.25 1.0 2A14005 EPA 365.4 01/21/22 12:55 )AH
85 D mg/L 5 1.3 2.4 2A14004 EPA 351.2 01/21/22 12:37 JAH
85 D mg/L 5 1.3 2.4 [CALC] CALC 01/21/22 12:37 )AH
25 mg/1 3.33 8.3 8.3 2A13023 SM 2540D-2011 01/13/22 18:06 DM)
Microbiological Parameters
^ • EIPCO Cary certfedanr/y& (NC 5911
Analvte fCASNumb]
Conform, Focal"
RONlla Om 118118 QE MQL EQ. Bitch Method Anailaril $x Rao
2.0 MPN/100 1 1.0 2A13041 Colllert 18 01/11/22 11:15 MN
mL
F:H+� This report relates only to the sample as received by the laboratory. and may only be reproduced in full.
Page 4 of 11
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2412004 - NO PREP
Blank(2A12004-BLX1)
Prepared & Analyzed: 01/12/2022 08:34
.Anahrte
Biochemical Oxygen Demand
Resit Flan
2.0 U
P01. Unita
2.0 mg/L
Spike Source
Level NU=
%REC
%REC j.kajm
RPD
RPD Umit jydam-
LCS(2A12004-BS1)
Prepared & Analyzed: 01/12/2022 08:34
Analvte
Biochemical Oxygen Demand
Elea
210
MIL MIAs
2.0 mg/L
Spike Source
Level EMI
198
%REC
%REC jamjm
105
85-115
RPD
RPD ljmjt lis
_Duplicate (2A12004-DUPI)
Prepared & Analyzed: 01/12/2022 08:34
1
Source: CF0041B-01
AnaIvt
Biochemical Oxygen Demand
Saltali 2A13023 - NO PREP
Spike
Result Elan e01 Unite Level
4.0 2.0 mg/L
Source
4.0
%REC
%REC Lima
RPD
0.9
RPD
Limit Maui&
30
Blank (2A13023-BLK1)
Prepared & Analyzed: 01/13/2022 18:06
Ana an
Total Suspended Solids
Result Elsa
2.5 U
EEL
2.5
Units
mg/L
Spike Source
Level &EAR
%REC
%REC Lia
RPD
RPD Limit ROIL
LCS(2A13023-BS1)
Prepared &Analyzed: 01/13/2022 18:06
Total Suspended Solids
Resift Elsa
91
P01 5a61�
2.5 mg/L
Spike Source
Level Rezill
100
%REC
%REC 11mit2
91
80-120
RPD
RPD Limit
Duplicate (2A13023-DUP1)
Prepared & Analyzed:
01/13/2022 18:06
Source: CE16452-01
Anitllle
Total Suspended Solids
Spike
R4501t Elsa P01 Unita Level
510
42
mg/L
Source
500
%REC
%REC Limits
RPD
2
Duplicate (2A13023-DUP2)
Prepared & Analyzed: 01/13/2022 18:06
Source: CE19001-01
_Rankle
Total Suspended Solids
Saudi 2414004 - Same
Spike
Result Elan P0L finite Level
28
8.3 mg/L
Source
Rasa
30
%REC
%REC j
RPD
5
RPD
IAMB
20
RPD
111111
20
Nato_
Matt
atm
flutes
-Blank (2A14004-BLK1)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:00
Aoalrias
Total Kjeldahl Nitrogen
Result Elan
0.26 U
P01
0.48
Spike
!Units Level
mg/L
Source
and
%REC
%REC Lim1
RPD
RPD Limit
LCS (2A14004-BS1)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:02
Amble
Total Kjeldahl Nitrogen
Result Elan
11
P41.
0.48
Spike
Unita Level
mg/L 12.0
Source
MOB
%REC
92
%REC
Limlh
90-110
RPD
RPD Limit
FINAL
This report relates ony to the sample as received by the laboratory, and may only be rearod xac 9 rus
Page 5 of 11
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2A14004 - Same - Continued
Matrix Spike (1A14004-MS1)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:06
Source: CE18800-01
Total Kjeldahl Nitrogen
Result Flea
4.2
MIL
0.48
!!nits
mg/L
Spike
Level
4.80
Source
Rea&
0.26
%REC
88
%REC
Ltmilit
90-110
RPD
RPD Lim)! Rata-
QM-07
Matrix Spike (2A14004-MS2)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:11
Source: CE19000-01
_Aaalvte
Total Kjeldahl Nitrogen
Result Elea
7.5
P91
0.48
Quite
mg/L
Spike
Level
4.80
Source
Reid!
2.8
%REC
%REC limita
97
90-110
RPD
RPD Limit lam_
Matrix Spike Dup (2A14004-MSD1)
Prepared: 01/17/2022 12-18 Analyzed: 01/21/2022 10:08
Source: CE1B800-01
lambda
Total Kjeldahl Nitrogen
Batdt 2414005 - Same
Spike Source %REC RPD
Rebuilt ilea P0L !!nits Level Roma %REC LiBllte RPD Unit NptSE-
4.2 0.48 mg/L 4.80 0.26 88 90-110 0.6 10 QM-07
Blank (2A14005-BLKI)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:16
13nalvte
Phosphorus
Resit Hee
0.025 U
Spike Source %REC RPD
1101 !!nits Level gestll! %REC unite RPD Limit kotes
0.10 mg/L
LCS(2A14005-B81)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:18
lina1
Phosphorus
Remit flea
1.5
Spike Source
PDL Units Level Rlalt
0.10 mg/L
L.60
%REC
92
%REC
Limits
80-120
RPD
RPD Limit Rates_
Matrix Spike (2A14005-MSI)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:20
Source: CE18800-01
Phosphorus
Result Flan
0.65
PQL Quits
mg/L
0.10
Spike
Level
0.640
Source
Emma
0.025 U
%REG
%REC Limb
102
80-120
RPD
RPD Limit R.4
Matrix Spike Dup (2A14005-MSD1)
Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:22
Source: CE18800-01
_Anaheim
Phosphorus
Batch 2417023 - NO PREP
Spike Source %REC
Result Ha6 P0L Linite Level Result %REC limit!
0.64 0.10 mg/L 0.640 0.025 U 101 80-120
RPD
RPD Limit Retie_
1 25
[Blank (2A17023-BLK1)
Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:00
_Analyse
Nitrate/Nitrite as N
Resuu Has
0.041 U
Spike Source %REC RPD
Eft Unlit Level Result %REC Limb RPD Limit I
0.10
mg/L
LCS(2A17023-BSI.)
Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:05
.Amble
NitrahE N trite as N
Spike Source %REC
Reset Han P91 Units Level Result %REC Linda
1.3 0.10 mg/L 1.25 102 90-110
RPD
RPD Lim )yam.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 11
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2.417023 - NO PREP - Continued
Matrix Spike (2A17023-MS1)
Prepared: 01/1712022 12:09 Analyzed: 01/17/2022 14:09
Source: CE15918-01
Anita
Nitrate/Nitrite as N
Result Flan
1.0
Pill Units
mg/L
0.10
Spike Source
Level Ewalt
0.521
0.44
%REC
%REC Limits
111
90-L10
RPD
RPD Limit 1
QM-07
Matrix Spike (2A17023-MS2)
Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:14
Source: CE18800-01
.Analvte
Nitrate/Nitrite as N
[WWI Has
u.61
PQL Units
mg/L
0.10
Spike
Level
'.l 521
Source
Rand
0.058
%REC
%REC Limits
106
90-110
RPD
RPD Lit Notes
Matrix Spike Dup (2Ai7023-M5D1)
Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:11
Source: CE15918-01
MOM
Nitrate/Nitrite as N
Batch 2A18023 - NO PREP
Spike Source %REC RPD
Result Han P01. !!nits Level Haig %REC LUBA RPD Um(t Retlls-
1.1 0.10 mg/L 0 521 0.44 127 90-110 8 10 QM-07
Blank (2A18023-BLK1)
Prepared; 01l18/2022 14:29 Analyzed: 01/19/2022 10:51
Analvta
Ammonia as N
Remit Elan
0.045 L
Spike Source %REC RPD
P01. MSS Level Rash %REC Limila RPD ulna grates
D.10
mg/L
LCS(2A18023-BS1)
Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:53
Amide
Ammonia as N
Spike Source %REC RPD
Result Han E01 Units Level Raga %REC l,Oplta RPD Limit
1.0
0.10
mg/L
1.01
99 90-110
Matrix Spike (2A18023-MS1)
Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:56
Source: CE19976-01
InahLta
Ammonia as N
Result Has
0.51
P01. Units
mg/L
0.10
Spike Source %REC RPD
Level Adult %REC limits RPD Limit Notes
0.393 0.16
90 90-110
Matrix Spike (2A18023-M52)
Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 11:02
Source: CE19977-01
Ana
Ammonia as N
Result His
0.58
P91 Units
mg/L
0.10
Spike Source
Level Rusk
0.11
0.393
%REC
%REC Limits
119 90-110
RPD
RPD limit Il' 9tii.
QM-07
Matrix Spike Dup (2A18023-MSD1)
Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:58
Source: CE19976-01
Antra
Ammonia as N
Batdt 2420013 - NO PREP
Spike Source %REC RPD
Result Elas P01 1Lnita Level Ems %REC Limit RPD Limit Notes
0.49 0.10 mg/L 0.393 0.16 84 90-110 5 10 QM-07
Blank(2A20013-BLK1)
Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:38
Anahrlz
Nitrate/Nitrite as N
Spike Source %REC RPD
Result Flan PQl Units Level EMI %REC Limila RPD Limit Na
0.041 U 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be repradimn in hid
Page 7 of 11
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2A201013 - NO PREP - Continued
LCS (2A20013-BS1)
Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:40
Analids
Nitrate/Nitrite as N
Result East
1.4
PQL UOIU
mg/L
0.10
Spike Source
Level
1.25
%REC
%REC ),jmite RPD
108 90-110
RPD
Lmit N
Matrix Spike (2A20013-MS1)
Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:44
Source: CE19887-01
_
Anaktn
Nitrate/Nitrite as N
Ronal! Elsa
0.041 U
Spike
POL Vella Level
0.10
mg/L
0.521
Source
Mad
0.041 U
%REC
%REC iambi RPD
90-110
RPD
Lad TlBteE-
QM-07
Matrix Spike (2A20013-MS2)
Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:49
Source: CE19887-02
.ADalvta
NItrate/Nitrite as N
Result Elea
0.041 U
Spike
P0L Unita Level
0.10
mg/L
0.521
Source
Hasid[
0.041 U
%REC
%REC Llm(ta RPD
90-110
RPD
Umit Rotes
QM-07
Matrix Spike Dup (2A20013-MSD1)
Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:45
Source: CE19887-01
�Dshda
Nitrate/Nitrite as N
!tweak Rea
0.041 U
POL Units
mg/L
0.10
Spike
Level
0.521
Source
0.041 U
%REC
%REC UlI11.� RPD
90-110
RPD
Lmit
10
QM-07
Microbiological Parameters - Quality Control
Batch 2A13041 - NO PREP
Duplicate (2A13041-DUP1)
Prepared: 01/10/2022 14:13 Analyzed: 01/11/2022 11:15
1
Source: CF00343-01
.AneMO
CoIiform, Fecal
Rauh Elan
1.0 U
110.1 Units
1.0 MPN/100 mL
Spike
Level
Source
Read
1.0 U
%REC
%REC
RPD
RPD Limit Rates.
25
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 11
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-02 The sample dilutions set up for the analysis failed to meet the criteria of a residual dissolved oxygen of at
least 1 mg/I. Therefore the reported result is an estimated value only.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
F.N This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 9 of 11
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Page 10of11 '
Sample Preservation Verification
ENCO Cary
Work Order: CF00345
Client: McFarland Septic (WA021)
Logged In- 10-Jan-22 12:08
Preservation Check Performed By:
Project: Wastewater
Project #: 1609 US HWY 15 501 S.
Logged By: Samantha L yatt
Date/Time. i l Z t 7,2,C)
CE00345-01
ion
:•-Cantf
"_ P
Pi .(01)
R gutrienti .
pN Chec (621J
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Driefilme '
PHAl*itee ►rastio
/Reagent Ceed/C.cmiinQnts
C
250mLP+H2SO4
<2
Y N / NA
•
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pH Strip ID•
C IELMNT\Printlwko_PreservationCheck_rpt
Reagent Name
ID Reagent Narne
3
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ID
5
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Reagent Name ID
I Page 11 of 11
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1609 US Hwy 15-501 S, Chapel Hill, NC 27516
Ed Moore 2022
Effluent Ouality Standards
Parameter
NOT to Exceed (mg/L)
Results
BOD
<45 mg/L
> 210 mg/L
TSS
<45 mg/L
25 mg/L
Fecal Coliform
<400 (colonies/100 ml)
2.0 cfu/100 ml
Total Nitrogen
S5 mg/L
Total Phosphorus
9.7 mg/L
Ammonia
84 mg/ L
Comments: BOD was above the acceptable parameter.
• •
•
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