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HomeMy WebLinkAboutNCG550696_Lab Data_20220127ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, January 27, 2022 McFarland Septic (WA021) Attn: Waylon McFarland 6801 Mt. Hermon Church Road Durham, NC 27705 RE: Laboratory Results for Project Number: 1609 US HWY 15 501 S., Project Name/Desc: Wastewater ENCO Workorder(s): CF00345 Dear Waylon McFarland, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, January 10, 2022. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Amanda L. Gaines Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 11 www.entaolabs.00m SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Effluent -1609 U5 HWY 15 501 S. Lab ID: CF00345-01 Sampled: 01/10/22 11:00 Received: 01/10/22 11:52 Parameter CALC Colilert 18 SM 2540D-2011 SM 5210 8-2011 [CALC] NO PREP NO PREP NO PREP Hold Date/Time(s) 02/07.22 01/10122 18:55 01/11..22 01/17122 01/12/22 11:00 pren Data/Timefsl 01/20/22 08:57 12:17 01/10/22 14:13 01/13/22 18:06 01/12/22 08:34 Analysis Date/Timefal 01/21/22 12:37 01/11/22 11:15 01/13/22 18:06 01/12/22 08:34 Client ID: Effluent -1609 US HWY IS 501 5. Lab ID: CF00345-01RE1 Sampled: 01/10/22 11:00 Received: 01/10/22 11:52 PSIOma= EPA 351.2 EPA 353.2 EPA 365.4 Ementation Same NO PREP Same Hold Date/Timers) 02/07r22 02/07/22 02/07/22 preo Date/Time(s) 01/17/22 01/20/22 01/17/22 12:18 08:57 12:18 Analysis Datellimefs1 01/21/22 12:37 01/20/22 13:20 01/21/22 12:55 client ID: Effluent -1609 US HWY 15 501 5. Lab ID: CF00345-01RE2 Sampled: 01/10/22 11:00 Received: 01/10/22 11:52 ParamESEr EPA 350.1 EDaQa ration NO PREP Hold Date!Timefsl 02/07/22 Free Date/Timers) 01/18/22 14:29 p�vsis Date/Tlmefsl 01/19/22 14:36 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 11 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Effluent -1609 US HWY 15 501 S. Lab ID: CF00345-01 Ankle Biochemical Oxygen Demand Coliform, Fecal Total Nitrogen - Total Total Suspended Solids Client ID: Effluent -1609 US HWY 15 501 S. AnaMe Phosphorus- Total Total Kjeldahl Nitrogen Client ID: Effluent -1609 US HWY 15 501 S. Anal& Ammonia as N Keau1 EINt >210 2.0 85 D 25 KmHa BEL 9.7 0 85 D PaiNStif112 84 0 MQL 2.0 1.0 1.3 8.3 EQL 2.0 1.0 2.4 8.3 tab ID: CF00345-01RE1 Unita mg/L MPN/100 mL mg/L mg/L Method SM 5210 B-2011 Coble- t 18 CALC SM 2540D-2011 Klan B-02 MQl 0.25 1.3 YQL 1.0 2.4 Lab ID: CF00345-01RE2 MQl 4.0 EQL 9.0 Malta mg/L mg/L Untta mg/L Naiad EPA 365.4 EPA 351.2 MBA19d EPA 350.1 Mtn i* L 1 i inu This repot relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 11 www.encolabs.com ANALYTICAL RESULTS Description: Effluent -1609 US HWY 15 501 S. Matrix: Waste Water Project: Wastewater Lab Sample ID:CF00345-01 Sampled:01/10/22 11:00 Sampled Sy:Brendan Towner Received: 01/10/22 11:52 Work Order: CF00345 Classical Chemistry Parameters ^ - ENcn Cary cr,arfad a fj4e INC 591.1 Apalvte fCAs Numberl Ammonia as N [7664-41-7]^ Biochemical Oxygen Demand" Nitrate/Nitrite as NA Phosphorus[7723-14-0]^ Total gjeldahl Nitrogen^ Total Nitrogen [17778-88-0] Total Suspended Solids". Multi Elsa UM* RE I1QL Mk Ikea Method Mai BY Matra 84 D mg/L 90 4.0 9.0 2A18023 EPA 350.1 01/19/22 14:36 )AH >210 mg/L 1 2.0 2.0 2A12004 SM 5210 6-2011 01/12/22 08:34 JOC 13-02 < 0.041 mg/L 1 0.041 0.10 2A20013 EPA 353.2 01/20/22 13:20 )AH 9.7 D mg/L 10 0.25 1.0 2A14005 EPA 365.4 01/21/22 12:55 )AH 85 D mg/L 5 1.3 2.4 2A14004 EPA 351.2 01/21/22 12:37 JAH 85 D mg/L 5 1.3 2.4 [CALC] CALC 01/21/22 12:37 )AH 25 mg/1 3.33 8.3 8.3 2A13023 SM 2540D-2011 01/13/22 18:06 DM) Microbiological Parameters ^ • EIPCO Cary certfedanr/y& (NC 5911 Analvte fCASNumb] Conform, Focal" RONlla Om 118118 QE MQL EQ. Bitch Method Anailaril $x Rao 2.0 MPN/100 1 1.0 2A13041 Colllert 18 01/11/22 11:15 MN mL F:H+� This report relates only to the sample as received by the laboratory. and may only be reproduced in full. Page 4 of 11 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 2412004 - NO PREP Blank(2A12004-BLX1) Prepared & Analyzed: 01/12/2022 08:34 .Anahrte Biochemical Oxygen Demand Resit Flan 2.0 U P01. Unita 2.0 mg/L Spike Source Level NU= %REC %REC j.kajm RPD RPD Umit jydam- LCS(2A12004-BS1) Prepared & Analyzed: 01/12/2022 08:34 Analvte Biochemical Oxygen Demand Elea 210 MIL MIAs 2.0 mg/L Spike Source Level EMI 198 %REC %REC jamjm 105 85-115 RPD RPD ljmjt lis _Duplicate (2A12004-DUPI) Prepared & Analyzed: 01/12/2022 08:34 1 Source: CF0041B-01 AnaIvt Biochemical Oxygen Demand Saltali 2A13023 - NO PREP Spike Result Elan e01 Unite Level 4.0 2.0 mg/L Source 4.0 %REC %REC Lima RPD 0.9 RPD Limit Maui& 30 Blank (2A13023-BLK1) Prepared & Analyzed: 01/13/2022 18:06 Ana an Total Suspended Solids Result Elsa 2.5 U EEL 2.5 Units mg/L Spike Source Level &EAR %REC %REC Lia RPD RPD Limit ROIL LCS(2A13023-BS1) Prepared &Analyzed: 01/13/2022 18:06 Total Suspended Solids Resift Elsa 91 P01 5a61� 2.5 mg/L Spike Source Level Rezill 100 %REC %REC 11mit2 91 80-120 RPD RPD Limit Duplicate (2A13023-DUP1) Prepared & Analyzed: 01/13/2022 18:06 Source: CE16452-01 Anitllle Total Suspended Solids Spike R4501t Elsa P01 Unita Level 510 42 mg/L Source 500 %REC %REC Limits RPD 2 Duplicate (2A13023-DUP2) Prepared & Analyzed: 01/13/2022 18:06 Source: CE19001-01 _Rankle Total Suspended Solids Saudi 2414004 - Same Spike Result Elan P0L finite Level 28 8.3 mg/L Source Rasa 30 %REC %REC j RPD 5 RPD IAMB 20 RPD 111111 20 Nato_ Matt atm flutes -Blank (2A14004-BLK1) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:00 Aoalrias Total Kjeldahl Nitrogen Result Elan 0.26 U P01 0.48 Spike !Units Level mg/L Source and %REC %REC Lim1 RPD RPD Limit LCS (2A14004-BS1) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:02 Amble Total Kjeldahl Nitrogen Result Elan 11 P41. 0.48 Spike Unita Level mg/L 12.0 Source MOB %REC 92 %REC Limlh 90-110 RPD RPD Limit FINAL This report relates ony to the sample as received by the laboratory, and may only be rearod xac 9 rus Page 5 of 11 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 2A14004 - Same - Continued Matrix Spike (1A14004-MS1) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:06 Source: CE18800-01 Total Kjeldahl Nitrogen Result Flea 4.2 MIL 0.48 !!nits mg/L Spike Level 4.80 Source Rea& 0.26 %REC 88 %REC Ltmilit 90-110 RPD RPD Lim)! Rata- QM-07 Matrix Spike (2A14004-MS2) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 10:11 Source: CE19000-01 _Aaalvte Total Kjeldahl Nitrogen Result Elea 7.5 P91 0.48 Quite mg/L Spike Level 4.80 Source Reid! 2.8 %REC %REC limita 97 90-110 RPD RPD Limit lam_ Matrix Spike Dup (2A14004-MSD1) Prepared: 01/17/2022 12-18 Analyzed: 01/21/2022 10:08 Source: CE1B800-01 lambda Total Kjeldahl Nitrogen Batdt 2414005 - Same Spike Source %REC RPD Rebuilt ilea P0L !!nits Level Roma %REC LiBllte RPD Unit NptSE- 4.2 0.48 mg/L 4.80 0.26 88 90-110 0.6 10 QM-07 Blank (2A14005-BLKI) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:16 13nalvte Phosphorus Resit Hee 0.025 U Spike Source %REC RPD 1101 !!nits Level gestll! %REC unite RPD Limit kotes 0.10 mg/L LCS(2A14005-B81) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:18 lina1 Phosphorus Remit flea 1.5 Spike Source PDL Units Level Rlalt 0.10 mg/L L.60 %REC 92 %REC Limits 80-120 RPD RPD Limit Rates_ Matrix Spike (2A14005-MSI) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:20 Source: CE18800-01 Phosphorus Result Flan 0.65 PQL Quits mg/L 0.10 Spike Level 0.640 Source Emma 0.025 U %REG %REC Limb 102 80-120 RPD RPD Limit R.4 Matrix Spike Dup (2A14005-MSD1) Prepared: 01/17/2022 12:18 Analyzed: 01/21/2022 11:22 Source: CE18800-01 _Anaheim Phosphorus Batch 2417023 - NO PREP Spike Source %REC Result Ha6 P0L Linite Level Result %REC limit! 0.64 0.10 mg/L 0.640 0.025 U 101 80-120 RPD RPD Limit Retie_ 1 25 [Blank (2A17023-BLK1) Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:00 _Analyse Nitrate/Nitrite as N Resuu Has 0.041 U Spike Source %REC RPD Eft Unlit Level Result %REC Limb RPD Limit I 0.10 mg/L LCS(2A17023-BSI.) Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:05 .Amble NitrahE N trite as N Spike Source %REC Reset Han P91 Units Level Result %REC Linda 1.3 0.10 mg/L 1.25 102 90-110 RPD RPD Lim )yam. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 11 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 2.417023 - NO PREP - Continued Matrix Spike (2A17023-MS1) Prepared: 01/1712022 12:09 Analyzed: 01/17/2022 14:09 Source: CE15918-01 Anita Nitrate/Nitrite as N Result Flan 1.0 Pill Units mg/L 0.10 Spike Source Level Ewalt 0.521 0.44 %REC %REC Limits 111 90-L10 RPD RPD Limit 1 QM-07 Matrix Spike (2A17023-MS2) Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:14 Source: CE18800-01 .Analvte Nitrate/Nitrite as N [WWI Has u.61 PQL Units mg/L 0.10 Spike Level '.l 521 Source Rand 0.058 %REC %REC Limits 106 90-110 RPD RPD Lit Notes Matrix Spike Dup (2Ai7023-M5D1) Prepared: 01/17/2022 12:09 Analyzed: 01/17/2022 14:11 Source: CE15918-01 MOM Nitrate/Nitrite as N Batch 2A18023 - NO PREP Spike Source %REC RPD Result Han P01. !!nits Level Haig %REC LUBA RPD Um(t Retlls- 1.1 0.10 mg/L 0 521 0.44 127 90-110 8 10 QM-07 Blank (2A18023-BLK1) Prepared; 01l18/2022 14:29 Analyzed: 01/19/2022 10:51 Analvta Ammonia as N Remit Elan 0.045 L Spike Source %REC RPD P01. MSS Level Rash %REC Limila RPD ulna grates D.10 mg/L LCS(2A18023-BS1) Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:53 Amide Ammonia as N Spike Source %REC RPD Result Han E01 Units Level Raga %REC l,Oplta RPD Limit 1.0 0.10 mg/L 1.01 99 90-110 Matrix Spike (2A18023-MS1) Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:56 Source: CE19976-01 InahLta Ammonia as N Result Has 0.51 P01. Units mg/L 0.10 Spike Source %REC RPD Level Adult %REC limits RPD Limit Notes 0.393 0.16 90 90-110 Matrix Spike (2A18023-M52) Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 11:02 Source: CE19977-01 Ana Ammonia as N Result His 0.58 P91 Units mg/L 0.10 Spike Source Level Rusk 0.11 0.393 %REC %REC Limits 119 90-110 RPD RPD limit Il' 9tii. QM-07 Matrix Spike Dup (2A18023-MSD1) Prepared: 01/18/2022 14:29 Analyzed: 01/19/2022 10:58 Source: CE19976-01 Antra Ammonia as N Batdt 2420013 - NO PREP Spike Source %REC RPD Result Elas P01 1Lnita Level Ems %REC Limit RPD Limit Notes 0.49 0.10 mg/L 0.393 0.16 84 90-110 5 10 QM-07 Blank(2A20013-BLK1) Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:38 Anahrlz Nitrate/Nitrite as N Spike Source %REC RPD Result Flan PQl Units Level EMI %REC Limila RPD Limit Na 0.041 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be repradimn in hid Page 7 of 11 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 2A201013 - NO PREP - Continued LCS (2A20013-BS1) Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:40 Analids Nitrate/Nitrite as N Result East 1.4 PQL UOIU mg/L 0.10 Spike Source Level 1.25 %REC %REC ),jmite RPD 108 90-110 RPD Lmit N Matrix Spike (2A20013-MS1) Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:44 Source: CE19887-01 _ Anaktn Nitrate/Nitrite as N Ronal! Elsa 0.041 U Spike POL Vella Level 0.10 mg/L 0.521 Source Mad 0.041 U %REC %REC iambi RPD 90-110 RPD Lad TlBteE- QM-07 Matrix Spike (2A20013-MS2) Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:49 Source: CE19887-02 .ADalvta NItrate/Nitrite as N Result Elea 0.041 U Spike P0L Unita Level 0.10 mg/L 0.521 Source Hasid[ 0.041 U %REC %REC Llm(ta RPD 90-110 RPD Umit Rotes QM-07 Matrix Spike Dup (2A20013-MSD1) Prepared: 01/20/2022 08:57 Analyzed: 01/20/2022 12:45 Source: CE19887-01 �Dshda Nitrate/Nitrite as N !tweak Rea 0.041 U POL Units mg/L 0.10 Spike Level 0.521 Source 0.041 U %REC %REC UlI11.� RPD 90-110 RPD Lmit 10 QM-07 Microbiological Parameters - Quality Control Batch 2A13041 - NO PREP Duplicate (2A13041-DUP1) Prepared: 01/10/2022 14:13 Analyzed: 01/11/2022 11:15 1 Source: CF00343-01 .AneMO CoIiform, Fecal Rauh Elan 1.0 U 110.1 Units 1.0 MPN/100 mL Spike Level Source Read 1.0 U %REC %REC RPD RPD Limit Rates. 25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 11 www.encolabs.coni FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. B-02 The sample dilutions set up for the analysis failed to meet the criteria of a residual dissolved oxygen of at least 1 mg/I. Therefore the reported result is an estimated value only. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. F.N This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 9 of 11 a ce N oW d cI a 1 Elil La a Ifi d if 3 1 m ' i ¶ji blj m epeseun — $pg� C_ ~ - i i di. { 1 a I 1 a-Ct y„. 4 9 1 -Z I j. .; NI 1 � [ li k C;7 i? i , tD, o FkiL � �, trkliilIclizr-i• 11 ME Page 10of11 ' Sample Preservation Verification ENCO Cary Work Order: CF00345 Client: McFarland Septic (WA021) Logged In- 10-Jan-22 12:08 Preservation Check Performed By: Project: Wastewater Project #: 1609 US HWY 15 501 S. Logged By: Samantha L yatt Date/Time. i l Z t 7,2,C) CE00345-01 ion :•-Cantf "_ P Pi .(01) R gutrienti . pN Chec (621J 7Coribvi. Driefilme ' PHAl*itee ►rastio /Reagent Ceed/C.cmiinQnts C 250mLP+H2SO4 <2 Y N / NA • Y N NA 1 2 pH Strip ID• C IELMNT\Printlwko_PreservationCheck_rpt Reagent Name ID Reagent Narne 3 4 ID 5 6 Reagent Name ID I Page 11 of 11 ■ ■ 7 ▪ JI II 11 I ■ ■ 7 ■ ■ ■ ■ 1 ■ 142. • - ■ - ■- ■ ■■ - ■ ■ -I I • 1- VI? ' AlA - • %rim ■ ■ -■ ■ ti ■ •. ■ -■ • • • ti • • .19 ✓ ■ • - J 7- - • • • • m. : 1609 US Hwy 15-501 S, Chapel Hill, NC 27516 Ed Moore 2022 Effluent Ouality Standards Parameter NOT to Exceed (mg/L) Results BOD <45 mg/L > 210 mg/L TSS <45 mg/L 25 mg/L Fecal Coliform <400 (colonies/100 ml) 2.0 cfu/100 ml Total Nitrogen S5 mg/L Total Phosphorus 9.7 mg/L Ammonia 84 mg/ L Comments: BOD was above the acceptable parameter. • • • 1 1 • • • •• • • r • %. •