NC0024911_Groundwater Monitoring Report October 2021_20211104

��/ G W-59A COMPLIANCE REPORT FORM Permit # NCO024911
X" (Sub ndl ogre each maniloring period with GIV-59 jorrns.)
1 Enter date monitoring results were due. I ''I1, 2021_) Will this monitoring report (GW-59 and GW-59A) YES
be submitted after the established due date?
2 Was any required information missing on the GW-59 report farms?
IF the answer to question f or 2 is "YES" list in the space provided below the well
explain the problems en ����4 K'rke required information.
Nov 0 9 2021
3 Are any 7thenitor wells in need of re air or maintenance (damaged asingunlocked ormissing cap,
identifica, area overgrmft,SE&J the answer is "Yes", contact the Regional Ogice far guidance.
INFf1RMAT1(1N PRO r. SING ONii
4 Are any
to or above the
If the answer to question 4 is "NO'; skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
MIN-05 MW-06R Myy_07
pli-5:5 P 5.2 MW-08R
pH 5.8
Mn 6,690 ug/L Mn 740 ug/L Mn 11,000 ug/L
Fe 1,080 ug/L Fe 37,600 ug/L
$ For the constituents identified in question 4 above, have standards been exceeded previously for the
same constituent(s) in the same weil(s) in the last two years?
If the answer to question 5 is "No" skip to section 8.
L
e answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards,
entrations) reported, and sample collection date for each occurrence (for the last two years).
5 pH Mn Fe MW-O6R pH Mn Fe9 5.8 482 ugIL MW-07 pH Mn Fe MW-08R PH Mn Fe
9 5.7 302 ug/L 10/2/19 6.1 12700ug/L 50,800ug/L
5.9 533 up/L 624 u9/L 1/2/20 6.3 1Q000 ugA 43,000,g/L 1/2/20 6.2 125ug/L 627 ugh ��y2p 6.3 10,40D uga 2,860 ug/L
56 Na/20 5.5 7,860 ugiL 1,820 ug/L BIB/20 59 308uB/L 447ugIL 8/8/20 11,700ugIL78,800ug4
0 56 10/23/20 5.2 9,330 ug/L 5,410 ug/L 10/23/20 5.9 19.700 u91L 70.700 uglL
5.4 1118/21 5.3 8,510 ugIL 1,2W ug/L 1/15/21 6.0 831 ug/L 10/23/2074,800 ug/L 61,600 ugIL
5.4 6124121 5.4 9,980 uglL 5360 u/I e/24/176 ug L 6/2A 27 15,000 ug 50,700 u�g/Lthe monitoring wells Listed in section 5 located at or beyond the review boundary-1
answer is "YES", a groundwater
OFFI qualify problem may be occurring. CONTACT THE REGIONAL
OFFCE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be Improperly
located; contact the Regional Office.
7 I Is the perm1 implementing previously approved actions required by
groundwater ouality orohlom?
it the answer to question 7 is "YES , descnbe those actions in the space
If the answer to question 7 is "NO", contact th_e Regional nrrI ,.ne
$ The person completing this portion (GW--59A) of the monitoring report should sign below and submit ti
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
Lhereby wledge that the above information was evaluated and the information submitted in this
ance Report GW-59A) is true and complete to the best of my knowledge.
ermittee (orAuthorized Age 't)i -g 1 , xy Oy LOL
I,,J,I �'" Dat
NOV
C 2021
GW-59A 12/8/2003 O 16
Water Quality Regional Operatior
/ .. , ,"In L" .,7 nu..,..
YES
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Pace Analytical Services, LLC
/ �r-aeeAnalVtical�` 2225 Riverside Dr.
/ www.pacelabs.cpm Asheville, NC 28804
October 25, 2021
Mr. Roger Edwards
Metropolitan Sewerage District
2028 Riverside Drive
Asheville, NC 28804
RE: Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Dear Mr. Edwards:
Enclosed are the analytical results for sample(s) received by the laboratory on October 01, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Ms. Shannon Bergeron, Metropolitan Sewerage District
Mr, John Gosnell, Metropolitan Sewerage District
Mr. Chad Ledford, Metropolitan Sewerage District
Mr. Dwayne Martin, Metropolitan Sewerage District
Ms. Cassandra McKnight, MSD of Buncombe County
Patrick Smith, MSD of Buncombe County, NC
Mr. Alan Taylor, Metropolitan Sewerage District
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, I.E.C.
[phone]
77
J Nuv i 6 ZUZI
UU""Y Operations
/,sheville Regional Office

aceAnalytical
Ww Pace]abs.com
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Pace Analytical Services Charlotte
9800 Kinceygve. Ste 100, Huntersville, NO 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification M 460221
North Carolina Wastewater Certification M 40
Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]

?��aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Lab ID Sample ID
92564509001 MW-05
92564509002 MW-06R
92564509003 MW-07
92564509004 MW-08R
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 200.7 Rev 4.4 1994
DS
10
PASI-A
EPA 245.1 Rev 3.01994
DBB1
1
PASI-A
SM 6200B
PM1
63
PASI-C
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
-EPA 350.1- Rev -2,0-1993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
EPA 200.7 Rev 4.4 1994
DS
10
PASI-A
EPA 245.1 Rev 3.01994
DB81
1
PASI-A
SM 62008
PM1
63
PASI-C
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2A 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.0 1993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
EPA 200.7 Rev 4.4 1994
DS
10
PASI-A
EPA 245.1 Rev 3.01994
DBBi
i
PASI-A
SM 6200B
PM1
63
PASI-C
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-0I-E-2011
MDW
1
PASI-A
SM 531OB-2011
MEMi
1
PASI-A
EPA 200.7 Rev 4A 1994
DS
10
PASI-A
EPA 245.1 Rev 3.01994
DB61
1
PASI-A
SM 6200B
PM1
63
PASI-C
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.

�AceAnalytical'
W W.Pacslabs.cam
race Analyucal services, uc
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Lab ID Sample ID
PAST -A = Pace Analytical Services -Asheville
PAST-C = Pace Analytical Services - Charlotte
SAMPLE ANALYTE COUNT
Method
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytes
Analysts Reported Laboratory

�tqceAnalj4ical-
www.paceiabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-OS
Lab ID: 92564509007 Collected: 10/01/21 16:10 Received: 10/01/21 17:05 Matrix: Water
Parameters
Results Units Report Limit OF
Prepared P Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
Collected By
Danielle
1
10/18/21 16:34
Schuler
1
10/18/21 16:34
Collected Date
10/1/21
Collected Time
15:62
1
10/18/21 16:34
pH
5Std. Units
1
10/18/21 16:34
Temperature
16.4
6.4 deg C
1
10/18/21 16:34
Static Water Level
18.23 feet
1
10/18/21 16:34
Specific Conductance
32.0 umhos/cm
1
10/18/21 16:34
Odor
None
1
10/18/21 16:34
Appearance
Clear
1
10/18/21 16:34
1
10/18/21 16:34
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
Barium
NO ug/L
10.0 1
10/12/21 03:38 10/12/21 18:25 7440-38-2
Cadmium
1ug/L
ND
ND
5.0 1
10/12/21 03:38 10/12/21 18:25 7440-39-3
Chromium
ug/L
1.0 1
10/12/21 03:38 10/12/21 18:25 7440-43.9
Iron
ND ug/L
5.0 1
10/12/21 03:38 10/12/21 18:25 7440-47-3
Lead
66.2 ug/L
50.0 1
10/12/21 03:38 10/12/21 18:25 7439-89-6
Manganese
NO ug/L
5.0 1
10/12/21 03:38 10/12/21 18:25 7439-92.1
Selenium
38.1 ug/L
5.0 1
10/12/21 03:38 10/12/21 18:25 7439-96.5
Silver
NO ug/L
10.0 1
10/12/21 03:38 10/12/21 18:25 7782-49.2
Sodium
NO ug/L
5.0 1
10/12/21 03:38 10/12/21 18:25 7440.22.4
NO ug/L
5000 1
10/12/21 03:38 10/12/21 18:25 7440.23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO u9/L
0.20 1
10/06/21 11:30 10/07/21 13:42 7439-97-6
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
Bromobenzene
NO ug/L
NO
0.50 1
10/06/21 21:15 71.43.2
Bromochloromethane
ug/L
ND
0.50 1
10/06/2121:15 108-86.1
Bromodichloromethane
ug/L
N
0.50 1
10/06/21 21:15 74.97-5
Bromoform
ug/L
NDO
0.50 1
10/06/21 21:15 75-27-4
Bromomethane
ug/L
NO
0.50 1
10/06/21 21:15 75-25-2
n-Butylbenzene
ug/L
Nug/L
5.0 1
10/06/21 21:15 74-83.9
sec-Butylbenzene
NO ug/L
0.50 1
10/06/21 21:15 104-51-8
tert-Butylbenzene
NO ug/L
0.50 1
10/O6/2121:15 135-98-8
135-9
Carbon tetrachloride
NO
0.50 1
10/06/21 21:15 6
Chlorobenzene
ug/L
NO
0.50 1
10/06/21 21:15 56-06.6
56-23..7
Chloroethane
ug/L
NO
0.50 1
10/06/21 21:15 108-9
Chloroform
ug/L
NO
1.0 1
10/06/21 21:15 3
75-00-3
Chloromethane
ug/L
NO
0.50 1
10/06/21 21:15
2-Chlorotoluene
ug/L
ND
1.0 1
10/06/21 21:15 74.87-3
ug/L
0.50 1
10/06/21 21:15 95.49-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

aceAnalytical
.w .pacelabe.cam
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-05
Lab ID: 92564609001 Collected:
10/01/21 16:10
Received: 10/01/21 17:05 Matrix: Water
Parameters
Results
Units Report Limit
OF
Prepared Analyzed CAS No, Qual
8200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
4-Chlorotoluene
ND
ug/L
0.50
1
10/06/21 21:15 106-43-4
1,2-Dibrom0-3-chloropropane
NO
ug/L
1.0
1
10/06/21 21:15 96.12-8
Dibromochloromethene
NO
ug/L
0.50
1
10106/2121:15 124-48-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
10/06/21 21:15 106-93-4
Dibromomethane
NO
ug/L
0.50
1
10/06/21 21:15 74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
10/06/21 21:15 95.50.1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10/06/21 21:15 541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
10/06/21 21:15 106-46.7
Dichlorodi8uoromethane
NO
ug/L
0.50
1
10/06/21 21:15 75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/06/21 21:15 75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
1
10/06/21 21:15 107-06-2
11-Dichloroethene
ND
ug/L
0.50
1
10/06/21 21:15 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
10/06/21 21:15 156.59.2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
10/06/21 21:15 156-60-5
1,2-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:15 78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:15 142-28-9
2,2-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:15 594.20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
10/06/21 21:15 563.58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
10/0612121:15 10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
10/06/21 21:15 10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
10/06/21 21:15 108-20-3
Ethylbenzene
NO
ug/L
0.50
1
10/06/21 21:15 100-41-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1
10/06/21 21:15 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10/06/21 21:15 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/06/21 21:15 75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
10/06/21 21:15 1634.04-4
Naphthalene
ND
ug/L
2.0
1
10/06/21 21:15 91-20-3
n-Propylbenzene
NO
ug/L
0.50
1
10/06/21 21:15 103.65.1
Styrene
NO
ug/L
0.50
1
10/06/21 21:15 100.42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 21:15 630.20.6
1,1,2,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 21:15 79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
10/08/21 21:15 127-18-4
Toluene
ND
ug/L
0.50
1
10/06/2121:15 108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
10106/2121:15 87-61-6
1,2,4-Trichlorobenzene
NO
ug/L
2.0
1
10/06/21 21:15 120-82-1
1,1,1-Trichloroethane
NO
ug/L
0.50
1
10/06/21 21:15 71-55-6
1,1,2-Trichloroethane
NO
ug/L
0.50
1
10/06/21 21:15 79.00.5
Trichloroethene
ND
ug/L
0.50
1
10/06/21 21:15 79-01-6
Trichloro8uoromethane
ND
ug/L
1.0
1
10/06/21 21:15 75-69-4
1,2,3-Trichloropropane
NO
ug/L
0.50
1
10/06/21 21:15 96-18-4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
1
10/06/21 21:15 95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
1
10/06/21 21:15 108-67-8
Vinyl chloride
NO
ug/L
1.0
1
10/06/21 21:15 75-01-4
m&p-Xylene
NO
ug/L
1.0
1
10/06/21 21:15 179601-23-1
o-Xylene
ND
ug/L
0.50
1
10/06/21 21:15 95-47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical
www.pacelabs.cam
Pace Analytical Services, LLC
2226 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
mrr-uo
Parameters
6200E MSV
Surrogates
1,2-Dichloroethane-d4 (S)
4-BromoOuorobenzene (S)
Toluene-0 (S)
2640C Total Dissolved Solids
Total Dissolved Solids
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
Date: 10/25/2021 09:52 AM
ANALYTICAL RESULTS
Lab ID: 92564509001 Collected: 10/01/21 WAD Received: 10/01/21 17:05 Matrix: Water
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
92 % 70.130 1
98 %
10/06/2121:15 17060-07-0
70-130 1
100 % 70-130 1
10/06/21 21:15 460-00-4
10/06/21 21:16 2037.26-5
Analytical Method: SM 2540C-2011
Pace Analytical Services -Asheville
34.0 mg/L 25.0 1
10/05/21 17:41
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
3.8 mg/L 1.0 1
10/02/21 22:50 14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
NO mg/L 0.10 1
10/16/21 13:03 7664-41-7
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.040 1
10/02/2100:50 14797-55.8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
1.4 mg/L 1.0 i
10/05/21 18:48 16887-00-6
Analytical Method: SM 5310B-2011
Pace Analytical Services -Asheville
ND mg/L 1.0 1
10/07/21 17:09 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.paaelabs.cam
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-06R Lab ID: 92664509002 Collected: 10/01/21 10:50 Received: 10/01/21 17:05 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
10/18/21 16:42
Collected By
Danielle
1
10/18/21 16:42
Schuler
Collected Date
1011121
1
10/18/21 16:42
Collected Time
10:28
1
10/18/21 16:42
pH
5.17 Std.-Units
1
10/18/21 16:42
Temperature
21.3 deg C
1
10/18/21 16:42
Static Water Level
10.49 feet
1
10/18/21 16:42
Specific Conductance
207.2 umhos/cm
1
10/18/21 16:42
Odor
None
1
10/18/21 16:42
Appearance
Clear
1
10/18/21 16:42
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
NO ug/L
10.0
1
10/12/21 03:38 10/12/21 18:28 7440-38-2
Barium
67.8 ug/L
5.0
1
10/12/21 03:38 10/12/21 18:28 7440-39-3
Cadmium
NO ug/L
1.0
1
10/12/21 03:38 10/12/21 18:28 7440.43.9
Chromium
NO ug/L
5.0
1
10/12/21 03:38 10/12/21 18:28 7440-47-3
Iron
1080 ug/L
50.0
1
10/12/21 03:38 10/12/21 18:28 7439-89-6
Lead
ND ug/L
5.0
1
10/12/21 03:38 10/12/21 18:28 7439-92-1
Manganese
6690 ug/L
5.0
1
10/12/21 03:38 10/12/21 18:28 7439-96-5
Selenium
NO ug/L
10.0
1
10/12/21 03:38 10/12/21 18:28 7782-49-2
Silver
NO ug/L
5.0
1
10/12/21 03:38 10/12/21 18:28 7440-22-4
Sodium
18400 ug/L
5000
1
10/12/21 03:38 10/12/21 18:28 7440-23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO ug/L
0.20
1
10/06/21 11:30 10/07/21 13:44 7439-97-6
6200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
NO ug/L
0.50
1
10/06/21 21:33 71-43-2
Bromobenzene
NO ug/L
0.50
1
10/06/21 21:33 108-86-1
Bromochloromelhane
NO ug/L
0.50
1
10/06/21 21:33 74-97-5
Bromodichloromethane
NO ug/L
0.50
1
10/06/21 21:33 75.27-4
Bromoform
ND ug/L
0.50
1
10/06/21 21:33 75.25.2
Bromomelhane
ND ug/L
5.0
1
10/06/21 21:33 74-83-9
n-Butylbenzene
ND ug/L
0.50
1
10/06/21 21:33 104-51-8
sec-Butylbenzene
ND ug/L
0.50
1
10/06/21 21:33 135-98-8
tert-Butylbenzene
ND ug/L
0.50
1
10/06/21 21:33 98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
10/06/21 21:33 56-23-5
Chlorobenzene
NO ug/L
0.50
1
10/06/21 21:33 108.90-7
Chloroethane
NO ug/L
1.0
1
10/06/21 21:33 75.00.3
Chloroform
NO ug/L
0.50
1
10/06/21 21:33 67-66-3
Chloromethane
NO ug/L
1.0
1
10/06/21 21:33 74-87-3
2-Chlorotoluene
NO ug/L
0.50
1
10/06/21 21:33 95-49-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

Pace Analytical services, LLD
/ ® 2225 Riverside Dr.
AnalyticalAsheville, NC 28804
www.pacelabsxom [phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-06R Lab ID: 92564509002 Collected: 10/01/21 10:50 Received: 10/01/21 17:05 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
4-Chlorololuene
NO
ug/L
0.50
1
10/06/2121:33 106.43.4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/06/21 21:33 96-12.8
Dibromochloromethane
NO
ug/L
0.50
1
10/06/21 21:33 124.48.1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
10/06/21 21:33 106-93-4
Dibromomethane
NO
ug/L
0.50
1
10/06/21 21:33 74-953
1,2-Dichlorobenzene
NO
ug/L
0.50
1
10/06/21 21:33 95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10/06/21 21:33 541-73-1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
10/06/21 21:33 106.46-7
Dichlorodifluoromethane
NO
ug/L
0.50
1
10/06/21 21:33 75.71.8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/06/21 21:33 75.34.3
1,2-Dichloroethane
NO
ug/L
0.50
1
10/06/21 21:33 107-06-2
1,1-Dichloroethane
NO
ug/L
0.50
1
10/06/21 21:33 75-35.4
cis-1,2-Dichloroethene
NO
ug/L
0.50
1
10/06/21 21:33 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
10/06/21 21:33 156-60-5
1,2-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:33 78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:33 142-28-9
2,2-Dichloropropane
NO
ug/L
0.50
1
10/06/21 21:33 594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
10/06/21 21:33 563-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
10/06/21 21:33 10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
0.50
1
10/0612121:33 10061-02-6
Diisopropyl ether
NO
ug/L
0.50
1
10/06/21 21:33 108.20-3
Ethylbenzene
NO
ug/L
0.50
1
10/06/21 21:33 100.41-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1
10/06/21 21:33 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10/06/21 21:33 98-82-8
Methylene Chloride
NO
ug/L
2.0
1
10/06/21 21:33 75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
1
10/06/21 21:33 1634-04-4
Naphthalene
NO
ug/L
2.0
1
10/06/21 21:33 91-20-3
n-Propylbenzene
NO
ug/L
0.50
1
10/06/21 21:33 103-65.1
Styrene
NO
ug/L
0.50
1
10/06/21 21:33 100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 21:33 630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 21:33 79-34-5
Tetrachloroethene
NO
ug/L
0.50
1
10/06/21 21:33 127-18-4
Toluene
NO
ug/L
0.50
1
10/06/21 21:33 108-88-3
1,2,3-Trichlorobenzene
NO
ug/L
2.0
1
10/06/21 21:33 87-61-6
1,2,4-Trichlorobenzene
NO
ug/L
2.0
1
10/06/21 21:33 120-82.1
1,1,1-Trichloroethane
NO
ug/L
0.50
1
10/06/21 21:33 71-55-6
1,1,2-Trichloroethane
NO
ug/L
0.50
1
10/06/21 21:33 79-00-5
Trichloroethene
NO
ug/L
0.50
1
10/06/21 21:33 79.01-6
Trichlorofluoromethane
NO
ug/L
1.0
1
10/06/21 21:33 75.69-4
1,2,3-Trichloropropane
NO
ug/L
0.50
1
10/06/21 21:33 96-18.4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
1
10/06/21 21:33 95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
1
10/06/21 21:33 108-67-8
Vinyl chloride
NO
ug/L
1.0
1
10/06/21 21:33 75.01-4
m&p-Xylene
NO
ug/L
1.0
1
10106/2121:33 179601-23-1
o-Xylene
NO
ug/L
0.50
1
10/06/21 21:33 95.47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

Pace Analytical Services, LLC
aceAnalytical - 2225 Riverside Dr.
www.pacelebs.cam Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-06R Lab ID: 92564509002 Collected: 10/01/21 10:50 Received: 10/01/21 17:05 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
92 %
4-Bromofluorobenzene (S)
70-130
94 %
1
10/06/21 21:33 17060-07.0
Toluene-d8 (S)
98 o/a 70-130
1
10/06/21 21:33 460-00-4
70-130
1
10/06/21 21:33 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
149 mg/L 25.0
1
10/05/21 17:41
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
69.1 mg/L 1.0
1
10/02/21 23:08 14808-79-8
360.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.15 mg/L 0.10
1
10/16/2113:05 7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.10 mg/L 0.040
1
10/02/21 00:42 14797-55-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
8.6 mg/L 1.0
1
10/05/21 18:49 16887-00-6
5310E TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
1.3 mg/L 1.0
1
10/07/21 17:29 7440-44-0
Date: 10/25/2021 09:52 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacslabsxom
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-07
Lab ID: 92564509003 Collected:
10/01/21 12:30
Received: 10/01/21 17:05 Matrix: Water
Parameters
Results Units Report Limit
OF
Prepared Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
10/18/21 16:43
Collected By
Danielle
1
10/18/21 16:43
Schuler
Collected Date
1011121
1
10/18/21 16:43
Collected Time
12:12
1
10/18/21 16:43
pH
6.81 Sid. Units
1
10/18/21 16:43
Temperature
22.5 deg C
1
10/18/21 16:43
Static Water Level
11.26 feet
1
10/18/21 16:43
Specific Conductance
330.0 umhos/cm
1
10/18/21 16:43
Odor
None
1
10/18/21 16:43
Appearance
Clear
1
10/18/21 16:43
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.41994
Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
NO ug/L
10.0
1
10/12/2103:38 10/1212118:31
7440.38-2
Barium
46.3 ug/L
5.0
1
10/12/2103:38 10/12/2118:31
7440-39-3
Cadmium
NO ug/L
1.0
1
10/1212103:38 10/12/2118:31
7440-43-9
Chromium
NO ug/L
5.0
1
10/12/2103:38 10/12/2118:31
7440-47-3
Iron
NO ug/L
50.0
1
10/1212103:38 10/12/2118:31
7439-89-6
Lead
NO ug/L
5.0
1
10112/2103:38 10/12/2118:31
7439-92-1
Manganese
740 ug/L
5.0
1
10/12/2103:38 10/12/2118:31
7439-96-5
Selenium
NO ug/L
10.0
1
10/12/2103:38 10/12/2118:31
7782-49-2
Silver
NO ug/L
5.0
1
10/12/2103:38 10112/2118:31
7440-22-4
Sodium
13200 ug/L
5000
1
10/12/2103:38 10/12/2118:31
7440-23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO ug/L
0.20
1
10/06/21 11:30 10/07/21 13:46
7439-97-6
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
NO ug/L
0.50
1
10/0612121:61
71.43-2
Bromobenzene
NO ug/L
0.50
1
10/06/2121:51
108.86.1
Bromochloromelhane
NO ug/L
0.50
1
10/06/2121:51
74.97.5
Bromodichloromethane
NO ug/L
0.50
1
10/06/2121:51
75.27.4
Bromoform
NO ug/L
0.50
1
10/06/2121:51
75-25-2
Bromomethane
NO ug/L
5.0
1
10/0612121:51
74-83-9
n-Butylbenzene
NO ug/L
0.50
1
10/06/2121:51
104-51-8
sec-Butylbenzene
NO ug/L
0.50
1
10/06/2121:51
135.98.8
tert-Butylbenzene
ND ug/L
0.50
1
10/06/2121:51
98-06-6
Carbon tetrachloride
NO ug/L
0.50
1
10/06/21 21:51
56-23-5
Chlorobenzene
NO ug/L
0.50
1
10/06/2121:51
108-90.7
Chloroethane
NO ug/L
1.0
1
10/06/2121:51
75-00-3
Chloroform
NO ug/L
0.50
1
10/06/2121:51
67-66-3
Chloromethane
NO ug/L
1.0
1
10/06/2121:51
74-87-3
2-Chlorotoluene
NO ug/L
0.50
1
10/06/2121:51
95-49-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC
�aceAnalytical 2225 Riverside Dr.
Asheville, NC 28804
www.0+celaba.com [phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-07 Lab ID: 92664609003 Collected: 10/01/21 12:30 Received: 10/01/21 17:05 Matrix: Water
Parameters Results Units Report Limit OF
8200E MSV
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromoch loromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dlchlorobenzene
1,3-Dlchlorobenzene
1,4-Dichlorobenzene
D i ch to rod i n u o ro m eth a n e
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlo ro9 uoromethane
1,2,3-Trichloropropene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Date: 10/25/2021 09:52 AM
Analytical Method: SM 62006
Pace Analytical Services - Charlotte
Prepared Analyzed CAS No. Qual
NO
ug/L
0.50
1
10/06/2121:51 106-43-4
NO
ug/L
1.0
1
10/06/2121:51 96-12.8
NO
ug/L
0.50
1
10/06/2121:51 124-48-1
NO
ug/L
0.60
1
10/06/2121:51 106-93.4
NO
ug/L
0.50
1
10/06/2121:51 74.95-3
NO
ug/L
0.50
1
10/06/2121:51 95.50-1
NO
ug/L
0.50
1
10/06/2121:51 541-73.1
NO
ug/L
0.50
1
10/06/2121:51 106-46-7
NO
ug/L
0.50
1
10/06/2121:51 75-71-8
NO
ug/L
0.50
1
10/06/2121:51 75.34-3
NO
ug/L
0.50
1
10/0612121:51 107-06-2
NO
ug/L
0.50
1
10/06/2121:51 75-35-4
ND
ug/L
0.50
1
10/06/2121:51 156-59-2
NO
ug/L
0.50
1
10/06/2121:51 156-60-5
NO
ug/L
0.50
1
10/06/2121:51 78-87-5
NO
ug/L
0.50
1
10/06/2121:51 142-28.9
NO
ug/L
0.50
1
10/0612121:51 594-20-7
ND
ug/L
0.50
1
10/0612121:51 563-58.6
NO
ug/L
0.50
1
10/06/2121:51 10061.01-5
NO
ug/L
0.50
1
10/06/2121:51 10061.02-6
NO
ug/L
0.50
1
10/06/2121:51 108-20-3
NO
ug/L
0.50
1
10/06/2121:51 100-41-4
NO
ug/L
2.0
1
10/06/2121:51 87-68-3
NO
ug/L
0.50
1
10/06/2121:51 98-82.8
NO
ug/L
2.0
1
10/06/2121:51 75.09-2
NO
ug/L
0.50
1
10/0612121:51 1634-04-4
NO
ug/L
2.0
1
10/06/2121:51 91-20-3
NO
ug/L
0.50
1
10/06/2121:51 103.65-1
NO
ug/L
0.50
1
10106/2121:51 100.42-5
NO
ug/L
0.50
1
10/06/2121:51 630-20-6
NO
ug/L
0.50
1
10/06/2121:51 79-34-5
NO
ug/L
0.50
1
10/06/2121:51 127-18-4
NO
ug/L
0.50
1
10/06/2121:51 108-88-3
NO
ug/L
2.0
1
10/06/2121:51 87.61-6
NO
ug/L
2.0
1
10/06/2121:51 120-82-1
NO
ug/L
0.50
1
10/06/2121:51 71.55-6
NO
ug/L
0.50
1
10/06/2121:51 79-00-5
NO
u9/L
0.50
1
10/06/2121:51 79.01-6
NO
ug/L
1.0
1
10/06/2121:51 75-69.4
NO
ug/L
0.50
1
10106/2121:51 96-18.4
NO
ug/L
0.50
1
10/06/2121:51 95-63-6
NO
ug/L
0.50
1
10/06/2121:51 108-67.8
NO
ug/L
1.0
1
10/06/2121:51 75-01.4
NO
ug/L
1.0
1
10/06/2121:51 179601-23.1
NO
ug/L
0.50
1
10/06/2121:51 95-47.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

�aceAnalytical*
wantpacrib.cam
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-07 Lab ID: 92664609003 Collected: 10/01/21 12:30 Received: 10/01/21 17:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
94 % 70-130
1
10/06/21 21:51 17060-07-0
4-Bromofluorobenzene (S)
96 % 70-130
1
10/06/21 21:51 460-00-4
Toluene-d8 (S)
99 % 70.130
1
10/06/21 21:51 2037-26.5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
225 mg/L 25.0
1
10/05/21 17:41
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
90.0 mg/L 2.0
2
10/03/2101:13 14808-79.8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
10/16/21 13:06 7664-41-7
363.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.39 mg/L 0.040
1
10/02/21 00:44 14797-55-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
6.3 mg/L 1.0
1
10/05/2118:50 16887-00-6
5310B TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
6.8 mg/L 1.0
1
10/20/21 03:13 7440-44-0
Date: 10/25/2021 09:52 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.

Pace Analytical Services, LLC
A �} °' 2225 Riverside Dr.
ace~nal ica/ Asheville, NO 28804
Ww .pacelaba.cam [phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-08R Lab ID: 92564609004 Collected: 10/01/21 14:15 Received: 10/01/21 17:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
10/18/21 16:44
Collected By
Danielle
1
10/18/21 16:44
Schuler
Collected Date
10/1/21
1
10/18/21 16:44
Collected Time
13:56
1
10/18/21 16:44
pH
6.77 Std. Units
1
10/18/21 16:44
Temperature
21.3 deg C
1
10/18/21 16:44
Static Water Level
10.79 feet
1
10/18/21 16:44
Specific Conductance
429.9 umhos/cm
1
10/18/21 16:44
Odor
None
1
10/18/21 16:44
Appearance
Reddishloil
1
10/18/21 16:44
y
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND ug/L
10.0
1
10/12/2103:38 10112/2118:41 7440.38-2
Barium
41.5 ug/L
5.0
1
10/12/2103:38 10/12/2118:41 7440-39-3
Cadmium
ND ug/L
1.0
1
10/12/2103:38 10/12/2118:41 7440.43-9
Chromium
ND ug/L
5.0
1
10/12/2103:38 10/12/2118:41 7440.47-3
Iron
37600 ug/L
50.0
1
10/12/2103:38 10/12/2118:41 7439.89-6
Lead
ND ug/L
5.0
1
10/1212103:38 10/12/2118:41 7439-92-1
Manganese
11000 ug/L
25.0
5
10/12/21 03:38 10/13/21 18:33 7439-96-5
Selenium
ND ug/L
10.0
1
10/12/2103:38 10/12/2118:41 7782-49-2
Silver
ND ug/L
5.0
1
10/12/2103:38 10112/2118:41 7440-22-4
Sodium
26700 ug/L
5000
1
10/12/2103:38 10/12/2118:41 7440-23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
10/06/21 11:30 10/07/21 13:53 7439-97-6
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
ND ug/L
0.50
1
10/06/21 22:09 71-43-2
Bromobenzene
ND ug/L
0.50
1
10/06/21 22:09 108-86-1
Bromochloromethane
ND ug/L
0.50
1
10/06/21 22:09 74-97-5
Bromodichloromethane
NO ug/L
0.50
1
10/06/21 22:09 75.27-4
Bromoform
ND ug/L
0.50
1
10/06/21 22:09 75-25-2
Bromomethane
ND ug/L
5.0
1
10/06/21 22:09 74-83-9
n-Butylbenzene
NO ug/L
0.50
1
10/06/21 22:09 104-51-8
sec-Butylbenzene
ND ug/L
0.50
1
10/06/21 22:09 135-98-8
tart-Butylbenzene
ND ug/L
0.50
1
10/06/21 22:09 98-06-6
Carbon tetrachloride
NO ug/L
0.50
1
10/06/21 22:09 56-23-5
Chlorobenzene
ND ug/L
0.50
1
10/06/21 22:09 108-90-7
Chloroethane
ND ug/L
1.0
1
10/06/21 22:09 75-00.3
Chloroform
NO ug/L
0.50
1
10/06/21 22:09 67-66.3
Chloromethane
ND ug/L
1.0
1
10/06/21 22:09 74-87-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

Pace Analytical Services, LLC
ceAnalytical � 2225 Riverside Asheville, NC 2880404
www.vacela6s.cam [phone]
ANALYTICAL RESULTS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Sample: MW-0811 Lab ID: 92564609004 Collected: 10/01/21 14:15 Received: 10/01/21 17:05 Matrix: Water
Parameters
Results
Units Report Limit
OF
Prepared Analyzed CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
2-Chlorotoluene
NO
ug/L
0.60
1
10/06/21 22:09 95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
10/06/2122:09 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/06/21 22:09 96-12-8
Dibromochloromethane
NO
ug/L
0.50
1
10/06/2122:09 12448-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
10/06/21 22:09 106.93-4
Dibromomethane
NO
ug/L
0.50
1
10/06/21 22:09 74.95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
10/06/21 22:09 95-50.1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10/06/21 22:09 541-73.1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
10/06/2122:09 106-46-7
Dichlorodi8uoromethane
NO
ug/L
0.50
1
10/06/21 22:09 75.71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/06/21 22:09 75-34.3
1,2-Dichloroethane
NO
ug/L
0.50
1
10/06/2122:09 107-06.2
1,1-Dichloroethene
NO
ug/L
0.50
1
10/06/21 22:09 75-35.4
cis-1,2-Dichloroethene
NO
ug/L
0.50
1
10/06/2122:09 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
10/06/2122:09 156.60-5
1,2-Dichloropropane
NO
ug/L
0.50
1
10/06/2122:09 78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
1
10/06/2122:09 142-28.9
2,2-Dichloropropane
NO
ug/L
0.50
1
10/06/21 22:09 594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
10/06/21 22:09 563-58.6
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
10/06/2122:09 10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
0.50
1
10/06/2122:09 10061-02-6
Diisopropyl ether
NO
ug/L
0.50
1
10/06/21 22:09 108.20-3
Ethylbenzene
NO
ug/L
0.50
1
10/06/2122:09 100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
10/06/21 22:09 87-68.3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10/06/21 22:09 98-82-8
Methylene Chloride
NO
ug/L
2.0
1
10/06/21 22:09 75-09-2
Methyl -tart -butyl ether
NO
ug/L
0.50
1
10/06/21 22:09 1634-04.4
Naphthalene
NO
ug/L
2.0
1
10/06/21 22:09 91-20-3
n-Propylbenzene
NO
ug/L
0.50
1
10106/2122:09 103-65-1
Styrene
NO
ug/L
0.50
1
10/06/2122:09 100-42.5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 22:09 630-20.6
1,1,2,2-Tetrachloroethane
NO
ug/L
0.50
1
10/06/21 22:09 79-34.5
Tetrachloroethene
NO
ug/L
0.50
1
10/06/21 22:09 127-18.4
Toluene
NO
ug/L
0.50
1
10/06/2122:09 108-88-3
1,2,3-Trichlorobenzene
NO
ug/L
2.0
1
10/06/21 22:09 87-61-6
1,2,4-Trichlorobenzene
NO
ug/L
2.0
1
10/06/2122:09 120-82-1
1,1,1-Trichloroethane
NO
ug/L
0.50
1
10/06/21 22:09 71-55-6
1,1,2-Trichloroethane
NO
ug/L
0.50
1
10/06/21 22:09 79-00.5
Trichloroethene
NO
ug/L
0.50
1
10/06/21 22:09 79.01-6
Trichloro8uoromethane
NO
ug/L
1.0
1
10/06/21 22:09 75.69-4
1,2,3-Trichloropropane
NO
ug/L
0.50
1
10/06/21 22:09 96.18-4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
1
10/06/21 22:09 95.63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
1
10/06/2122:09 108-67-8
Vinyl chloride
NO
ug/L
1.0
1
10/06/21 22:09 75-01-4
m&p-Xylene
NO
ug/L
1.0
1
10/06/2122:09 179601-23-1
o-Xylene
NO
ug/L
0.50
1
10/06/21 22:09 95-47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical
www.pacelabsxom
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Oct2021 MW 1011
Pace Project No.: 92564509
Sample: MW-08R Lab ID: 92564509004 Collected: 10/01/21 14:15 Received: 10/01/21 17:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
93 % 70-130
1
10/06/21 22:09 17060.07.0
4-Bromofluorobenzene (S)
97 % 70-130
1
10/06/21 22:09 460-00-4
Toluene-d8 (S)
98 % 70-130
1
10/06/21 22:09 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
194 mg/L 25.0
1
10/05/21 17:41
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
39.3 mg/L 1.0
1
10/02/2123:38 14808-79-8
360.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.42 mg/L 0.10
1
10/16/2113:08 7664.41.7
363.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.20
5
10/02/21 01:12 14797-55-8
4600 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
21.6 mg/L 1.0
1
10/05/2118:51 16887-00-6
5310B TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
2.1 mg/L 1.0
1
10/07/21 17:46 7440-44.0
Date: 10/25/2021 09:52 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2228 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 652167 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3420054 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Arsenic
ug/L
NO
- 10.0
10/12/2118:00
Barium
ug/L
NO
5.0
10/12/2118:00
Cadmium
ug/L
ND
1.0
10/12/2118:00
Chromium
ug/L
ND
5.0
10/12/2118:00
Iron
ug/L
ND
50.0
10/12/2118:00
Lead
ug/L
ND
5.0
10/12/2118:00
Manganese
ug/L
ND
5.0
10/12/2118:00
Selenium
ug/L
ND
10.0
10/12/2118:00
Silver
ug/L
ND
5.0
10/12/2118:00
Sodium
ug/L
ND
5000
10/12/2118:00
LABORATORY CONTROL SAMPLE:
Parameter
3420055
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
ug/L
500
488
98
85-115
Barium
ug/L
500
516
103
85-115
Cadmium
ug/L
Soo
504
101
85-115
Chromium
ug/L
500
509
102
85-115
Iron
ug/L
5000
5180
104
85-115
Lead
ug/L
500
508
102
85-116
Manganese
ug/L
500
504
101
85-115
Selenium
ug/L
500
478
96
85-115
Silver
ug/L
250
255
102
85-115
Sodium
ug/L
5000
5220
104
85-115
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
3420056
3420057
MS
MSD
92564407010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
ug/L
26.6
500
500
552
533
105
101
70.130
3
Barium
ug/L
1360
500
500
1910
1860
110
99
70.130
3
Cadmium
ug/L
9.8
500
500
566
547
111
107
70.130
3
Chromium
ug/L
7.4
500
500
455
442
90
87
70-130
3
Iron
ug/L
182
5000
5000
4880
4640
94
89
70-130
5
Lead
ug/L
ND
500
500
437
419
87
84
70-130
4
Manganese
ug/L
57600
500
500
57200
56300
-88
-254
70-130
1 E
Selenium
ug/L
141
500
500
212
200
14
12
70-130
6 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

aceAnalydcal
www.pacelabsxc n
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3420056 3420057
MS MSD
92564407010 Spike Spike MS MSD MS MSD % Rae
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Silver ug/L 46.7 250 250 273 260 91 85 70-130 5
Sodium ug/L 105000 5000 5000 1010000 970000 -780 -1650 70-130 4 E
0
MATRIX SPIKE & MATRIX
Parameter
SPIKE DUPLICATE: 3420058
MS
92564991002 Spike
Units Result Cone.
MSD
Spike
Cone.
3420059
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD Qual
Arsenic
ug/L
NO
500
500
491
490
98
98
70-130
0
Barium
ug/L
NO
500
500
520
622
103
104
70-130
0
Cadmium
ug/L
NO
500
500
503
505
101
101
70-130
0
Chromium
ug/L
ND
500
500
489
491
98
98
70-130
0
Iron
ug/L
82.7
5000
5000
5060
5070
100
100
70-130
0
Lead
ug/L
ND
500
500
500
600
100
100
70-130
0
Manganese
ug/L
6.5
500
500
495
497
98
98
70-130
0
Selenium
ug/L
ND
500
500
512
509
102
102
70-130
1
Silver
ug/L
ND
250
250
249
248
100
99
70-130
0
Sodium
ug/L
ND
5000
5000
5580
5580
105
105
- 70.130
0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

aceAnaljftal
www.pacelabs.cem
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 661254 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3415467 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2•Tetrachloroethane
ug/L
NO
0.50
10/06/21 15:17
1,1,1-Trichloroethane
ug/L
ND
0.50
10/06/21 15:17
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
10/06/21 15:17
1,1,2-Trichloroethane
ug/L
ND
0.50
10/06/21 15:17
1,1-Dichloroelhane
ug/L
ND
0.50
10/06/21 15:17
1,1-Dichloroethene
ug/L
ND
0.50
10/06/21 15:17
1,1-Dichloropropene
ug/L
ND
0.50
10/06/21 15:17
1,2,3-Trichlorobenzene
ug/L
ND
2.0
10/06/21 15:17
1,2,3-Trcchloropropane
ug/L
NO
0.50
10/06/21 15:17
1,2,4-Trichlorobenzene
ug/L
NO
2.0
10/06/21 15:17
1,2,4-Trimethylbenzene
ug/L
NO
0.50
10/06/21 15:17
1,2-Dibromo-3-chloropropane
ug/L
NO
1.0
10/06/21 15:17
1,2-Dibromoethane (EDB)
ug/L
NO
0.50
10/06/21 15:17
1,2-Dichlorobenzene
ug/L
ND
0.50
10/06/21 15:17
1,2-Dichloroethane
ug/L
NO
0.50
10/06/21 15:17
1,2-Dichloropropane
ug/L
ND
0.50
10/06/21 15:17
1,3,5-Trimethylbenzene
ug/L
ND
0.50
10/06/21 15:17
1,3-Dichlorobenzene
ug/L
ND
0.50
10/06/21 15:17
1,3-Dichloropropane
ug/L
ND
0.50
10/06/21 15:17
1,4-Dichlorobenzene
ug/L
ND
0.50
10106/2115:17
2,2-Dichloropropane
ug/L
NO
0.50
10/06/21 15:17
2-Chiorotoluene
ug/L
NO
0.50
10/06/21 15:17
4-Chiorotoluene
ug/L
NO
0.50
10/06/21 15:17
Benzene
ug/L
ND
0.60
10/06/21 15:17
Bromobenzene
ug/L
ND
0.50
10/06/21 15:17
Bromochloromethane
ug/L
ND
0.50
10/06/21 15:17
Bromodichloromethane
ug/L
ND
0.50
10/06/21 15:17
Bromoform
ug/L
ND
0.50
10/06/21 15:17
Bromomethane
ug/L
ND
5.0
10/06/21 15:17
Carbon tetrachloride
ug/L
NO
0.50
10/06/21 15:17
Chlorobenzene
ug/L
NO
0.50
10/06/21 15:17
Chloroethane
ug/L
NO
1.0
10/06/21 15:17
Chloroform
ug/L
NO
0.50
10/0612115:17
Chloromethane
ug/L
NO
1.0
10/06/21 15:17
cis-1,2-Dichloroethene
ug/L
ND
0.50
10/06/21 15:17
cis-1,3-Dichloropropene
ug/L
NO
0.50
10/06/21 15:17
Dibromochloromethane
ug/L
ND
0.50
10/06/21 15:17
Dibromomethane
ug/L
ND
0.50
10/06/21 15:17
Dichlorodifluoromethane
ug/L
ND
0.50
10/06/21 15:17
Diisopropyl ether
ug/L
ND
0.50
10/06/21 15:17
Qualifiers
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, L-C.

aceAnalytical w
wwmpacslabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct2021 MW 10/1
Pace Project No.: 92564509
METHOD BLANK: 3415467 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit
Analyzed
Ethylbenzene
ug/L
NO
0.50
10/06/21 15:17
Hexachloro-1,3-butadiene
ug/L
NO
2.0
10/06/21 15:17
Isopropylbenzene (Cumene)
ug/L
NO
0.50
10/06/21 15:17
m&p-Xylene
ug/L
ND
1.0
10/06/21 15:17
Methyl-tert-butyl ether
ug/L
NO
0.50
10/06/21 15:17
Methylene Chloride
ug/L
NO
2.0
10/06/21 15:17
n-Bulylbenzene
ug/L
NO
0.50
10/06/21 15:17
n-Propylbenzene
ug/L
NO
0.50
10/06/21 15:17
Naphthalene
ug/L
ND
2.0
10/06/21 15:17
o-Xylene
ug/L
NO
0.50
10/06/21 15:17
sec-Bulylbenzene
ug/L
NO
0.50
10/06/21 15:17
Styrene
ug/L
NO
0.50
10106/2115:17
tert-Buylbenzene
ug/L
NO
0.50
10/06/21 15:17
Tetrachloroethene
ug/L
NO
0.50
10106/2115:17
Toluene
ug/L
NO
0.50
10/06/21 15:17
trans-1,2-Dichloroethene
ug/L
NO
0.50
10/06/21 15:17
trans-1,3-Dichloropropene
ug/L
NO
0.50
10/0612115:17
Trichloroethene
ug/L
NO
0.50
10/06/21 15:17
Trichlorofluoromethane
ug/L
NO
1.0
10/06/21 15:17
Vinyl chloride
ug/L
NO
1.0
10/06/21 15:17
1,2-Dichloroethene-d4 (S)
%
96
70-130
10/06/21 15:17
4-Bromofluorobenzene (S)
%
96
70.130
10/06/21 15:17
Toluene-d8 (S)
%
98
70.130
10/06/21 15:17
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3415468
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rao
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.7
109
60-140
1,1,1-Trichloroethane
ug/L
50
49.5
99
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
50.3
101
60-140
1,1,2-Trichloroethane
ug/L
50
50.4
101
60.140
111-Dichloroethane
ug/L
50
48.1
96
60.140
1,1-Dichloroethene
ug/L
50
47.3
95
60-140
1,1-Dichloropropene
ug/L
50
51.8
104
60.140
1,2,3-Trichlorobenzene
ug/L
50
58.2
116
60.140
1,2,3-Trichloropropane
ug/L
50
52.6
105
60.140
1,2,4-Trichlorobenzene
ug/L
50
55.3
111
60-140
1,2,4-Trimethylbenzene
ug/L
50
53.1
106
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.6
107
60.140
1,2-Dibromoelhane (EDB)
ug/L
50
52.3
105
60.140
1,2-Dichlorobenzene
ug/L
50
52.3
105
60-140
1,2-Dichloroethane
ug/L
50
46.9
94
60-140
1,2-Dichloropropane
ug/L
50
50.8
102
60-140
1,3,5-Trimethylbenzene
ug/L
50
54.6
109
60-140
Qualifiers
Results presented on this page are In the units Ind lcated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacelahs.cum
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QUALITY
CONTROL
DATA
LABORATORY CONTROL SAMPLE:
3415468
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
%Rec
Limits
1,3-Dichlorobenzene
ug/L
50
53.5
1,3-Dichloropropane
ug/L
50
107
60-140
1,4-Dichlorobenzene
ug/L
50
52.5
105
60-140
2,2-Dichloropropane
ug/L
50
52.5
105
60-140
2-Chlorotoluene
ug/L
50
48.7
97
60.140
4-Chlorotoluene
ug/L
50
52.2
104
60-140
Benzene
ug/L
50
51.1
50.4
102
60-140
Bromobenzene
ug/L
50
53.0
101
60-140
Bromochloromethane
ug/L
50
48.1
106
60-140
Bromodichloromethane
ug/L
50
50.0
96
60-140
Bromoform
ug/L
50
54.1
100
60-140
Bromomethane
ug/L
50
46.6
108
60.140
Carbon tetrachloride
ug/L
50
53.1
93
60.140
Chlorobenzene
ug/L
50
106
60-140
Chloroethane
ug/L
5o
51.9
104
60.140
Chloroform
ug/L
50
55.4
111
60-140
Chloromethane
ug/L
50
47.9
96
60-140
cis-1,2-Dichloroethene
ug/L
50
41.9
45.5
84
60-140
cis-1,3-Dichloropropene
ug/L
50
51.7
91
60-140
Dibromochloromethane
ug/L
50
55.0
103
60.140
Dibromomethane
ug/L
50
50.8
110
60.140
Dichlorodifluoromethane
ug/L
50
47.2
102
60-140
Diisopropyl ether
ug/L
50
49.5
94
60.140
Ethylbenzene
ug/L
50
51.8
99
60-140
Hexachloro-1,3-butadiene
ug/L
50
55.2
104
60-140
Isopropylbenzene (Cumene)
ug/L
50
56.1
110
60.140
m&p-Xylene
ug/L
100
106
112
106
60.140
60-140
Methyl-tert-butyl ether
ug/L
50
52.0
104
60.140
Methylene Chloride
ug/L
50
48.8
98
60-140
n-Butylbenzene
ug/L
50
55.0
110
60-140
n-Propylbenzene
ug/L
50
52.9
106
60-140
Naphthalene
ug/L
50
54.5
109
60-140
o-Xylene
ug/L
50
54.6
109
60-140
sec-Butylbenzene
ug/L
50
54.3
109
60-140
Styrene
ug/L
50
54.3
109
60-140
tert-Butylbenzene
ug/L
50
45.0
90
60-140
Tetrachloroethene
ug/L
50
55.0
110
60-140
Toluene
ug/L
50
47.6
95
60-140
trans-1,2-Dichloroethene
ug/L
50
48.1
96
60-140
trans-1.3-Dichloropropene
ug/L
50
60.9
102
60-140
Trichloroethene
ug/L
50
47.7
95
60-140
Trichlorofluoromethane
ug/L
50
44.8
90
Vinyl chloride
ug/L
50
44.0
88
60-140
1,2-Dichloroethane-d4 (S)
%
60-140
4-Bromoflucrobenzene (S)
%
100
70.130
Toluene-d8 (S)
%
98
70-130
94
70-130
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical services, LLC.

_ ace Analytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3415469
3415470
MS
MSD
92564595005
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
NO
200
200
291
244
145
122
60-140
17 M1
1,1,1-Trichloroethane
ug/L
NO
200
200
292
237
146
119
60-140
20 M1
1,1,2,2-Tetrachloroethane
ug/L
NO
200
200
262
221
131
111
60-140
17
1,1,2-Trichloroethane
ug/L
ND
200
200
268
221
134
110
60-140
19
1,1-Dichloroethane
ug/L
ND
200
200
272
223
136
111
60-140
20
1,1-Dichloroethane
ug/L
NO
200
200
273
227
137
113
60.140
19
1,1-Dichloropropane
ug/L
NO
200
200
291
244
145
122
60.140
17 Mt
1,2,3-Trichlorobenzene
ug/L
NO
200
200
297
251
148
126
60-140
17 M1
1,2,3-Tiichloropropane
ug/L
NO
200
200
251
208
125
104
60-140
19
1,2,4-Trichlorobenzene
ug/L
NO
200
200
274
245
137
123
60.140
11
1,2,4-Trimethylbenzene
ug/L
65.0
200
200
365
317
160
126
60-140
14 Mt
1,2-Dibromo-3-chloropropane
ug/L
NO
200
200
268
233
134
117
60-140
14
1,2-Dibromoethane (EDB)
ug/L
NO
200
200
283
239
142
120
60.140
17 M1
1,2-Dichlorobenzene
ug/L
NO
200
200
276
240
138
120
60.140
14
1,2-Dichloroethane
ug/L
61.4
200
200
331
267
135
103
60-140
21
1,2-Dichloropropane
ug/L
NO
200
200
287
231
143
116
60-140
21 Ml
1,3,5-Trimethylbenzene
ug/L
19.1
200
200
308
270
144
126
60.140
13 M1
1,3-Dichlorobenzene
ug/L
NO
200
200
287
254
144
127
60-140
12 M7
1,3-Dichloropropane
ug/L
NO
200
200
278
237
139
119
60-140
16
1,4-Dichlorobenzene
ug/L
NO
200
200
277
234
139
117
60-140
17
2,2-Dichloropropane
ug/L
NO
200
200
274
225
137
112
60-140
20
2-Chlorotoluene
ug/L
NO
200
200
294
256
147
128
60-140
14 MI
4-Chlorotoluene
ug/L
NO
200
200
273
233
136
117
60-140
16
Benzene
ug/L
136
200
200
425
375
145
120
60.140
13 MI
Bromobenzene
ug/L
NO
200
200
289
248
144
124
60.140
15 M1
Bromochloromethane
ug/L
NO
200
200
275
219
137
110
60-140
23
Bromodichloromethane
ug/L
NO
200
200
270
225
135
112
60-140
18
Bromoform
ug/L
NO
200
200
263
218
132
109
60-140
19
Bromomethane
ug/L
NO
200
200
250
223
125
111
60-140
12
Carbon tetrachloride
ug/L
NO
200
200
297
245
148
123
60.140
19 M1
Chlorobenzens
ug/L
NO
200
200
287
240
143
120
60-140
18 Mt
Chloroethane
ug/L
NO
200
200
346
277
173
139
60-140
22 M1
Chloroform
ug/L
NO
200
200
274
216
137
107
60.140
24
Chloromelhane
ug/L
NO
200
200
233
197
116
99
60.140
16
cis-1,2-Dichloroethene
ug/L
NO
200
200
259
213
130
107
60-140
19
cis-1,3-Dichloropropene
ug/L
NO
200
200
264
220
132
110
60-140
18
Dibromochloromethane
ug/L
NO
200
200
282
237
141
119
60.140
17 M1
Dibromomethane
ug/L
NO
200
200
282
226
141
113
60.140
22 M1
Dichlorodi8uoromethane
ug/L
NO
200
200
248
217
124
108
60.140
14
Diisopropyl ether
ug/L
432
200
200
730
673
149
121
60-140
8 MI
Ethylbenzene
ug/L
52.2
200
200
346
298
147
123
60-140
15 MI
Hexachloro-1,3-butadiene
ug/L
NO
200
200
288
251
144
126
60-140
14 M1
Isopropylbenzene (Cumene)
ug/L
NO
200
200
310
267
155
133
60-140
15 M1
m&p-Xylene
ug/L
189
400
400
788
694
150
126
60.140
13 M1
Methyl-tert-butyl ether
ug/L
1540
200
200
1980
1890
217
172
60-140
5 Mt
Methylene Chloride
ug/L
NO
200
200
273
222
137
Ill
60-140
21
Results presented on this page are in the unite Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/202109:52 AM without the written consent of Pace Analytical Services,LLC.

ace Analytical
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[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3415469
3415470
MS
MSD
92564595005
Spike
Spike
MS
MSD
MS
MSD
% Rao
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Dual
n-Butylbenzene
ug/L
5.3
200
200
288
258
141
126
60-140
11 Ml
n-Propylbenzene
ug/L
11.6
200
200
299
256
144
122
60-140
16 M1
Naphthalene
ug/L
ND
200
200
290
256
141
124
60-140
12 MI
o-Xylene
ug/L
73.6
200
200
371
327
149
127
60-140
13 M1
sec-Butylbenzene
ug/L
ND
200
200
299
256
150
128
60-140
16 M1
Styrene
ug/L
ND
200
200
291
248
145
124
60-140
16 M1
tert-Butylbenzene
ug/L
NO
200
200
250
212
125
106
60.140
16
Tetrachloroethene
ug/L
NO
200
200
299
260
150
130
60-140
14 M1
Toluene
ug/L
362
200
200
618
574
128
106
60-140
7
trans-1,2-Dichloroethene
ug/L
ND
200
200
275
228
137
114
60-140
18
trans-1,3-Dichloropropene
ug/L
ND
200
200
257
216
128
108
60-140
17
Trichloroethene
ug/L
NO
200
200
263
220
132
110
60-140
18
Trichlorofluoromethane
ug/L
NO
200
200
243
201
122
100
60-140
19
Vinyl chloride
ug/L
ND
200
200
254
209
127
104
60-140
19
1,2-Dichloroethane-d4 (S)
%
99
98
70-130
4-Bromofluorobenzene (S)
%
98
99
70-130
Toluene-d8 (S)
%
94
93
70.130
Results presented on this page are In the units Ind caled by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

PaceAnalytical �
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 650950 Analysis Method: SM 254OC-2011
QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001,92564509002,92564509003,92564509004
METHOD BLANK: 3413727 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 10/05/21 17:37
LABORATORY CONTROL SAMPLE: 3413728
Spike LCS LCS % Rao
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Dissolved Solids mg/L 251 236 94 90-110
SAMPLE DUPLICATE: 3413729
35666709002 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 557 558 0
SAMPLE DUPLICATE: 3413730
92564509004 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 194 192 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 650529 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3412029 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L NO 1.0 10102/2120:27
LABORATORY CONTROL SAMPLE: 3412030
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Sulfate mg/L
50
49.1
98
90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3412031
3412032
MS
MSD
92564509004
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Cone.
Cone. Result
Result
%Rec %Rec Limits RPD Qual
Sulfate mg/L 39.3
50
50 89.3
89.7
100 101 90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 653228 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3425221 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 10/16/21 12:27
IrusvKAWKYCONTROLSAMPLE: 3425222
Spike
LCS
LCS
% Rae
Parameter
Units
Cone.
Result
% Rae
Limits Qualifiers
Nitrogen, Ammonia
mg/L
5
5.0
100
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3425223
3425224
MS
MSD
92565568001
Spike
Spike MS
MSD
MS MSD %Rec
Parameter
Units Result
Cone.
Cone. Result
Result
% Rae % Rae Limits RPD Qual
Nitrogen, Ammonia
mg/L 7.5
5
5 12.0
11.9
90 87 90-110 1 M1
MAI KIA SPIKE & MATRIX SPIKE DUPLICATE: 3425225 3425226
MS MSD
92565570001 Spike Spike MS MSD MS MSD % Rae
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 6.1 5 5 10.7 10.8 92 94 90-110 1
Results presented on this page are in the units Indicated by the "Units" column except where an allemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 650483 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3411908 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L NO 0.040 10/02/21 00:05
LABORATORY CONTROL SAMPLE: 3411909
Spike
LCS
LCS
% Rae
Parameter Units
Cone.
Result
% Rea
Limits
Qualifiers
Nitrogen, Nitrate mg/L
1.5
1.5
100
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3411912
3411913
MS
MSD
92564446002
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter Units Result
Cone.
Cone.
Result
Result
% Rae
% Rae
Limits RPD 4ual
Nitrogen, Nitrate mg/L 36.4
1.5
1.5
32.0
35.4
-293
-69
90-110 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3411930
3411931
MS
MSD
92564446001
Spike
Spike
MS
MSD
MS
MSD
% Rea
Parameter Units Result
Cone.
Conc.
Result
Result
%Rec
%Rec
Limits RPD Qua[
Nitrogen, Nitrate mg/L 1.7
1.5
1.5
3.1
3.2
96
97
90-110 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

aceAnalXical w
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 650974 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3413897 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 1.0 10/05/2118:32
LABORATORY CONTROL SAMPLE: 3413898
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rae Limits Qualifiers
Chloride mg/L 20 20.5 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3413899
3413900
MS
MSD
92564484001 Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter Units Result Cone.
Cone.
Result
Result
%Rec
%Rec
Limits RPD Qual
Chloride mg/L 245 10
10
257
258
121
127
90.110 0 Ml
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3413901
3413902
MS
MSD
92564526001 Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter Units Result Cone.
Cone.
Result
Result
%Rec
%Rec
Limits RPD Qual
Chloride mg/L 13.5 10
10
23.7
22.7
102
92
90.110 4
Results presented on this page are in the units Ind lcated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

��aceAnalj4icale
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, INC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 651195
Analysis Method:
QC Batch Method: SM 53108.2011
Analysis Description:
Laboratory:
Associated Lab Samples: 92564509001, 92564509002, 92564509004
METHOD BLANK: 3415106
Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509004
Blank Reporting
Parameter Units
Result Limit
Total Organic Carbon mg/L
NO
SM 531OB-2011
5310B TOC
Pace Analytical Services -Asheville
Analyzed
1.0 10/07/21 05:09
Qualifiers
LABORATORY CONTROL SAMPLE: 3415107
Spike LCS LCS %Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 26.1 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3415108 3415109
MS MSD
92564526001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone, Result Result %Rec %Rec Limits RPD Qual
Total Organic Carbon mg/L 7.3 25 25 33.7 34.2 105 107 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3415110 3415111
MS MSD
92564681001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result %Rae %Rec Limits RPD Qual
Total Organic Carbon mg/L 1060 25 25 1070 1020 25 -167 90-110 5 M1
Results presented on this page are in the unite Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project:
Oct 2021 MW 10/1
Pace Project No.:
92564509
QC Batch:
653343
Analysis Method: SM 531OB-2011
QC Batch Method:
SM 531OB-2011
Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509003
METHOD BLANK: 3426942 Matrix: Water
Associated Lab Samples: 92564509003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 10/20/21 01:30
LABORATORY CONTROL SAMPLE: 3425943
Spike
LCS
LCS
% Rae
Parameter Units
Cone.
Result
%Rec
Limits Qualifiers
Total Organic Carbon mg/L
25
26.4
106
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3426944
3425945
MS
MSD
92564521009
Spike
Spike MS
MSD
MS MSD %Rec
Parameter Units Result
Cone.
Cone. Result
Result
%Rec %Rec Limits RPD Qual
Total Organic Carbon mg/L ND
25
25 ND
ND
3 4 90-110 D3,M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3425954 3425955
MS MSD
92565900003 Spike Spike MS MSD MS MSO % Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Total Organic Carbon mg/L 4.3 25 25 29.3 29.3 100 100 90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

aceAnaljftal m
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
QC Batch: 650850 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
METHOD BLANK: 3413092 Matrix: Water
Associated Lab Samples: 92564509001, 92564509002, 92564509003, 92564509004
Parameter Blank Reporting
Units Result Limit Analyzed
Mercury y Qualifiers
ug/L ND 0.20 10107/2113:16
LABORATORY CONTROL SAMPLE: 3413093
Spike LCS
Parameter Units Cone. Result
Mercury ug/L 2.5 2.3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3413094 3413095
MS MSD
92564018003 Spike Spike MS
Parameter Units Result Cone. Cone. Result
Mercury ug/L ND 2.5 2.5 ND
LCS % Rae
%Rec Limits Qualifiers
93 85-115
MSD MS MSD %Rec
Result %Rec %Rec Limits RPD Qual
ND 0 -1 70-130 MI
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is Presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2021 09:52 AM without the written consent of Pace Analytical Services, I.I.C.

PaceAnalXical
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Pace Analytical Services, LLC
2225 Riverside Dr,
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[phone]
QUALIFIERS
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazlne decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4.5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
MI Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date: 10/25/2021 09:52 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, I.I.C.

aceAnalytical
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Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oct 2021 MW 10/1
Pace Project No.: 92564509
Lab ID
92564509001
92564509002
92564509003
92564609004
92564609001
92564509002
92564609003
92564509004
92564509001
92564509002
92564509003
92564509004
92564509001
92564609002
92564609003
92564509004
92564609001
92564509002
92664509003
92564509004
92564509001
92664509002
92564609003
92564509004
92564509001
92664509002
92664509003
92564509004
92664509001
92564509002
92564509003
92564609004
92564509001
92564509002
92664509003
92664509004
92564509001
92564509002
92564509003
92664509004
Sample ID
MW-06
MW-06R
M W-07
MW-08R
MW-05
M W-06 R
MW-07
MW-08R
MW-OS
MW-06R
MW-07
MW-08R
MW-06
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
MW-05
MW-06R
MW-07
MW-08R
Date: 10/25/2021 09:52 AM
QC Batch Method
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 254OC-2011
SM 254OC-2011
SM 254OC-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
SM 4500-CI-E-2011
SM 4500-CI-E-2011
SM 4500-CI-E-2011
SM 4500-CI-E-2011
SM 531OB-2011
SM 531OB-2011
SM 531OB-2011
SM 531OB-2011
QC Batch Analytical Method
652167
652167
652167
652167
650850
650850
650850
650850
651254
651254
651254
651254
650950
650950
650950
650950
650529
650529
650529
650529
653228
653228
653228
653228
650483
650483
650483
650483
650974
650974
650974
650974
651195
651195
653343
651195
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4A 1994
EPA 200.7 Rev 4.4 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
Analytical
Batch
652185
652185
652185
652185
651178
651178
651178
651178

Document Name:
Document Revised: October 29, 2020
F�-CeAp2Uy(IC2il r
Sample Condition Upon Receipt(sCUR)
Page 1 of 2
Document No.:
Issuing Authority!
F-CAR-CS-033�Rev.O?
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville] Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mecfianicsville❑ Atlanta❑ ❑ Kernersville
Client Name:
�/j WO# : 92564509
/ ' fl Pro;aetq:
Courier: ❑Fed'Ex UUP§ ❑USPS ❑Client IIIII' I IIIII III I III III
❑ Commercial ❑Pace []Other:—
,,..--,,//
Custody Sea[Present? ❑yes Y)N0 Seals Intact? ❑Yes 0IN10, 92564509
Date/Initials Person Examining Contents: IC7)ZA`
Packing Material: ;21�ubble Wrap ❑Bubble Bags Elmore ❑ Other
Thernsomet5e- 2Net ❑Blue
IRGun IDr 11- jp2 Type of Ice;
Correction factor:
Cooler Temp: Add/Subtract('C), O
Cooler Temp Corrected I'C :- i., fir A. 11
USDA Regulated Soft ( NIA, watersample)
Did samples originate in aquarantine zone within th (United:States: CA, NY, or SC(checkmaps)?
11Voc MN,,
Biological Tissue Fro n?
❑Yes []NO/A
[]None
Temp should be above freezing to VC
[]samples out of temp criteria. Samples on ice; cooling process
hasbcgun
Did samplesc riginate from a foreign source (internationally;
Includfna Hawaii and Puerto Ricol? ❑Yes ❑No
Cam ments/Discrepancy:
Chat In of Custody Present?
es
I]No
N/A
1.
Samples Arrived wfthin Hold Time?
Ves
I]No
❑N/A
2.
Short Hold Time Analysis (<72 ha)?
es
ONO
[]N/A
3. No
Rush Turn Around Time Requested?
[]yes
CK.,
i]N/A
d.
Sufficient Volume?
%
Elmo
❑N7A
5.
Correct Containers Used?
- Pace Con tainerS Used?
es
Yes
E]No
I]No
❑N/.A
N/A
G.
Containers Intact?
16Yes
Olt.
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
QV
❑No-
8.
Sample Labefs Match CDC?
-Includes Datet`Tme/ID/Analysis Marrix:
es
V _
Elmo
❑N/A
9.
Readspace In VOA Vials (>5-Gmm)?
[]Yes
rlo-
!A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Dyes
QYes
❑No
I]No
/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split can tainerm
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/1-1me:
Field Data Required? ❑yes I]No
Project Manager SCURF Review: Date:
Project Manager SRF Review: — Date: l I I

*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project # WO# : 92564509
PM: UP Due Date: 10/15/21
CLIENT: 93—MSO
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lot a
adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certificatimi Office (i.e.
Out of hold, incorrect preservative, out of temp. incorrect containers.

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Domment Name: Field data Sheet Date Issued: November
t -"." ""-�'�Jk7EytlG81
Page: 1of1
Decument Number: F-CAR-FLD-001-rev.02 Issui ng Authority: Pace Hunte
/� S ni
OH ce
Field Data Sheet
Client: Location: f�a Nj
yam' `' ` c Project #: J
Name and Affiliation (Sampler(s): �9h S 0 k
----�---
,rC�G h/ ield Data Sheet Review:
Name and Affiliation (Inspector):-__�l%��__
Well Information
Date: By:
Well ID: M W , ✓ i
Well Locked: (YES NO)
r
Well Diameter:
Construction: (PVC Steel/Stainless Steel)
t�
Total Well Depth: / ft
/�
Static Water Level: b r a�
Muni Factor*: Q • I � 3 .
[ (Radius/12)2 x3.14 x 7.481
ft.
Casing Volume: 0.14
its
gauo
e
Height of Water Colun: S' / ft
Cal. 3 Volumes: a .$a
gallons
Pump Intake: /S ft
Purge Information r /
Date Purged:/ 0I Start: Finish: 0 Purge Rate: I I
Purging Method: A121 X yc —r r Total Volume Purged: r% 8� (gall"� mlS)
Sampling Information
Date Collectedjo-�(J-9—L Time Collected: I SSS ( /�
am
Sampling Equipment Used:-e.c, t 244, L Instrument ID: i' t Z 0, 011 k�aa Y S
Bottle Type Preservation Anal sis Required
�IaSc bn
s�
IN.S• .L /\
V
- iNh 0,1.E .
Me-I� IS
— Lo(
lldMe
1,
sureme �
Field Measurements/Ob//servations
VQC (p'D0U -
Sample Temp (°C): 110 Time:_. S
Turbidity (ntu): s' 3 3 Time: I S S a
Diss Oxy (mg/L): T- a Time: I S oZ
r �r—�—_
Specific Cond. (u5): 3") Time: I S $ a
Sl P
Res_CI (MO - (!1g/T)' Tia P.
Sample pH (s.u.): S s ] Time; 'SS-2
Odor: /w /fie I S S a T me:
ReDox (mV): 15 (rl Time: I S i ")i
Appearance: G Time: I SS l-2
ReDox (EH value):YSI ProPlus 4-200mV :� .�
General/Weather Observations: ��i' IiN l SG G
(/ is,r ni
Wind-3_(mph)
Sampler Signature:
)/Mn °/��yl
Date: J
161
Stabilization Test
Time
Purged
Tem .
P
(°C)
Diss Ox .
y
(mg/L)
Spec'
Cond.
P H() su.
ReDox
(mV)
Turbidity
(ntu)
Volume
remove
Water er(ftOther
(US)
(gallons uds
level
30-1
•.Sy
153,
Sao
I to
Any
I71
.�-OI
3 08
3
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t il.2
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mac 4if,a "
Document Name: Field data Sheet
Date Issued: November 27, 2018
page; lot}
Document Number: F-CAR-FLD-001-rev.02
Issuing Authority: Pace Huntersville Quality
Office
-5>f
Field Data Sheet
Name and Affiliation (Sampler(s):DoA-1 Ae 5cttalP-
Name and Affiliation (impector):9 14__
Well Information
Well ID: Alta - 0 6 k
Well Diameter: ;L f/
Total Well Depth: 1 % ft
Stack Water Level: q 6t 1 ft
m Height of Water Colun4-S I ft
Project #: i�
Id Data Sheet Review:
Date: By:
Well Locked: YES /zm
Construction: (PV /Steel/Stainless Steel)
Multi Factor*: 01 / � 3 [•(Radius/12)2 x 3.14 x 7.48]
Casing Volume: gallons
Cal. 3 Volumes: 3J ' I gallops
Pump Intake: ft
Purge Information
Date Purged; I1 O /! �__/Sta t:) G S Finish: Iy �7OPurgeRate: ICO
Purging Method: Ad-7 4q5,10
]]
"I c r c Total Volume Purged: -1 5oy (gallons/lJ
Sampling Information .D MS
Date Collected:1 D / 01 / /t101) Time Collected: W�o G0�10 4 �1
Sampling Equipment Used: IL R re ? 9t Instrument ID: ki'> 69 it
Bottle Type Preservation Analysis Re uired
�lgs C lVbA-e liv cG r suI
PIu�F� �+a sa + nh(nfe
lgs k� 41A3 ` h44)s
(; lass Ttie6 Itor Ar-; 1 •-jbC
C�asS .' dA- �c VoL 490D
Field MeasuremeriWObservations
Sample Temp (°C): a Time� Turbidity (ntu): Time:
Diss Oxy (mg/L): 0.0 I Time: IOU U Fed I etn'; Xi
Specific Cond. (uS): n Time: R - e:
Sample pH(s.u.): S'1 1 Time: Odor:— �N �t Tima:
ReDox(mV): Ie"S•j Time: Appearance: CItu1 Time:_-Da�
ReDox (EH value):YSI ProPlus +200mV ASS: �✓ Oth07. Time:
Genera]/Weather Observations: A�q / }, 0 Ul6t)
Sampler
(rainy) Tempje (CF) Wind. -(mph)
-/ - a,
Time
Purged
Temp,
(aC)
Diss Oxy.
(mg/L)
Cond.
(u5)
Hsu.
P ( )
ReDox
(mV)
Turbidity
(ntu)
Volume
� 0 2f
(gallons
Water
level (ft)
Other
160
,U
10ot
`'.L
0 it
1 .S
S. I'(
ISS.S
3.0
100
Io.
lolo
13
6.
ill 15-m
10 5
9J)
s00
ia15
L.�
$Y�
S IS
5
IoDJ
10• D
1qS .
S•ll,
JJVIo
0•,60
1 1Sna
(j,

Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-OO1.rev.02
Client: ' 1
Location:
Project:
Well ID:
Reviewed Date and
Stabilization Test
Document
Pageaof 9L
Issueing Authority:
Pace Huntersville Quality Office
i•4ell Bisxxizt.�Mlulliphcalt,�n
F`,-t,,e
1s1
21.Er25.,46

ce,�!raryricat'
Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-rev.02
Page: 1 of J
ity: Pace Hum
Office
-Y QK1
Name and Affiliation
Name and Affiliation
Well Information
Well ID: M/V - 0 ?
WeII Diameter:
Total Well Depth: ``�� ft
Static Water Level: I 1 ft.
Height of Water Column: •7H ft
G 1vl Field Data Sheet Review:
Date:
Well Locked: ( YES NO
Construction: (PV /Steel/Stainless Steel)
Muhl Factor*: Ot % 3 [ (Radius/12)2 x 3.14 x 7.48]
Casing Volume: D % Jr gallons
Cal. 3 Volumes: gallons
-47
By:
Pump Intake: ft
Purge Information
Date Purged:
_W / 61 / O) Start: I jSa Finish: 100 r+L
Purge Rate: h't • n
Purging Method: Pit _, a ii�pc r• < Total Volume Purged: ©b 1) allons/ tl s (g
Sampling Information
Date Collected; L/' L /__L Time Collected:
Sampling Equipment Used: &a, , k, Instrument ID: y S - 6211
Battle Type
`�9p Preservation lc An+ alysi's Required
) /
field Mvo t
Meld easureme W0bservations
Sample Temp (eC): d d ° 5 Time:�_1 �l Turbidity (ntu): S 3
Time:
Diss Oxy (mg/L):_ o . '7 a Time:. _;1
30, /7 12 T me:
Specific COnd. (uS): 3 Time: -
Odor- ( 1)A_Q L) - Time: _
Sample pH(s.u.): 5��� Time: e) I� Odor: /vJ�-R ) Ia
T me:
ReDox (mV): 13D Time: R K Appearance: C
ReDox(EH value):YSIPrOPlus+200mV 370' ���
Oth .
GeneraWeatherObservations: ----- tee'
Sampler
1.,-.,,,.,ILk,
cant
A%\6AjtA MT
A I-- 1)fi `t AtT41

Document Name: Field data Sheet
Name and Affiliation
Name and Affiliation
Well Information
Well ID: /1't /✓ - 0
Well Diameter: ; t
Total Well Depth: / i q It
Static Water Level: 1©, �I�1 ft
ti
Height of Water Cf
olumnTo ��t
b.')I
Documeat Number: F-CAR-FLD-001-rev.02
(cr
Page: 1 of=
wity: Pace Hun
Office
M 6,/ ' y
Data Sheet Review:
Date:
Well Locked: (YFS / p
Construction: PV /Steel/Stainless Steel)
Multi Factor*: 12�[»(Radius/12)2 x 3.14 x 7.48]
Casing Volume -J -- I, v i
3 gall
Cal. 3 Volumes:- �-� $a Ions
Pump Intake: s LJl ft
a
:PlLts /0--)-a l
tils��at�ed 4A l' m l
Analysis Required /_
'@s CIS lord & +, ,l/r}� 4e
_,/iMMan�a
�C-I"Q Jc
I17�
V OC. Iv a o 0
Sample Temp (eC): J )' 3 Time: ) 3S (o Turbidity (ntu): I D Time: (3S
Diss Oxy (mg/L):_ O. y 3 Time: 3Scv + mg
Specific Cond. (uS):Time: / 35 119 Res-, e L
Sample pH s.u.: ��) Time: _
-.... -P (_ ) Time: 1�5I Odor: kll!IZ Time:
( V): i3Sla
ReDox m n>S(t - - 13� Time: Appearance: Time:
ReDox (EH value):YSI ProPlus +200mVve`�. �j nttm --
Purge Information —--u----
Date Purged: ) & / 1 /� Start :133 tJ I 1 I� Purge Rate: q l� M I
n
Purging Method_Y L 2r 1 �� Finish: Pur - r Total Volume Purged: tysUD allons ss )
(gallons/9
g /F�) /
Sampling Information
Date Collected: 10 /v I /� Time Collected: NO
(amjo
Sampling Equipment Used:f"AuAny C InstrumentlD: YgOg(/ WI- �2ayS
Preservation
u Pilo e
General/Weather Observations: M as %1h t ju/I Sze
h
sum /cloudy/rainy) Temp. 3 (gip) Wind S !m
P)
Sampler Signature: Date: j d / 1' .�
IM
A

Document Name:
Document Issued: November 27, 2018
Field Data Sheet
Page2of _)- -
. Document Number:
F-CAR-FLD-OO1.rev.02
Issueing Authority:
Pace Huntersville Quality Office
Client: _ _ ✓
iIVd11 Dismeberistitil xlrcati�n ;; at orv. .
LU
Location: _ I `�
7 0 0918
Project: Lis
1..625 O-1fp30
WeII MIS-p-
09
t y
ID:
a O 3,67O
Reviewed Date and By:
4 0-6-530
Stabilization Test
a 1-0