WQ0024508_Monitoring - 11-2021_20211213 (2)

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Rev. 06-07-2018

ace Analytical
www.pacelabs.cam
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2 Lab ID: 92574016001 Collected: 11/23/21 10:15 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids Analytical Method: SM 2540C-2015
Pace Analytical Services - Eden
Total Dissolved Solids 82.0 mg/L 25.0 1 11/30/21 13:42
350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia ND mg/L 0.10 1 11/23/21 14:56 7664-41-7
353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate 0.55 mg/L 0.040 1
11/23/21 17:03 14797-55-8
MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms ND CFU/100 mL 1.0 1 11/23/21 14:18 11/24/21 12:35
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone ND ug/L 25.0 1 12/03/21 10:05 67-64-1
Benzene ND ug/L 1.0 1 12/03/21 10:05 71-43-2
Bromobenzene ND ug/L 1.0 1 12/03/21 10:05 108-86-1
Bromochloromethane ND ug/L 1.0 1 12/03/21 10:05 74-97-5
Bromodichloromethane ND ug/L 1.0 1 12/03/21 10:05 75-27-4
Bromoform ND ug/L 1.0 1 12/03/21 10:05 75-25-2
Bromomethane ND ug/L 2.0 1 12/03/21 10:05 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 12/03/21 10:05 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 12/03/21 10:05 56-23-5
Chlorobenzene ND ug/L 1.0 1 12/03/21 10:05 108-90-7
Chloroethane ND ug/L 1.0 1 12/03/21 10:05 75-00-3
Chloroform ND ug/L 1.0 1 12/03/21 10:05 67-66-3
Chloromethane ND ug/L 1.0 1 12/03/21 10:05 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 12/03/21 10:05 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 12/03/21 10:05 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 12/03/21 10:05 96-12-8
Dibromochloromethane ND ug/L 1.0 1 12/03/21 10:05 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 12/03/21 10:05 106-93-4
Dibromomethane ND ug/L 1.0 1 12/03/21 10:05 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:05 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:05 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:05 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 12/03/21 10:05 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 12/03/21 10:05 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 12/03/21 10:05 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 12/03/21 10:05 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 12/03/21 10:05 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 12/03/21 10:05 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 12/03/21 10:05 78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 34

ace Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2
Parameters
Lab ID: 92574016001
Results
Collected: 11/23/21 10:15 Received: 11/23/21 12:40 Matrix: Water
Units Report Limit DF
Prepared
Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
300.0 IC Anions 28 Days
Chloride
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
98
100
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ova
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
2.0 1
5.0 1
1.0 1
5.0 1
5.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
2.0 1
1.0 1
1.0 1
2.0 1
1.0 1
70-130 1
70-130 1
70-130 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
3.5 mg/L
1.0 1
12/03/21 10:05 142-28-9
12/03/21 10:05 594-20-7
12/03/21 10:05 563-58-6
12/03/21 10:05 10061-01-5
12/03/21 10:05 10061-02-6
12/03/21 10:05 108-20-3
12/03/21 10:05 100-41-4
12/03/21 10:05 87-68-3
12/03/21 10:05 591-78-6
12/03/21 10:05 99-87-6
12/03/21 10:05 75-09-2
12/03/21 10:05 108-10-1
12/03/21 10:05 1634-04-4
12/03/21 10:05 91-20-3
12/03/21 10:05 100-42-5
12/03/21 10:05 630-20-6
12/03/21 10:05 79-34-5
12/03/21 10:05 127-18-4
12/03/21 10:05 108-88-3
12/03/21 10:05 87-61-6
12/03/21 10:05 120-82-1
12/03/21 10:05 71-55-6
12/03/21 10:05 79-00-5
12/03/21 10:05 79-01-6
12/03/21 10:05 75-69-4
12/03/21 10:05 96-18-4
12/03/21 10:05 108-05-4
12/03/21 10:05 75-01-4
12/03/21 10:05 1330-20-7
12/03/21 10:05 179601-23-1
12/03/21 10:05 95-47-6
12/03/21 10:05 460-00-4
12/03/21 10:05 17060-07-0
12/03/21 10:05 2037-26-5
11/26/21 17:43 16887-00-6
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
1.6 mg/L
0.050 1 12/06/21 22:17 12/07/21 17:27 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 34

(1r
ace Analytical®
www.pacelabs.com
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2 Lab ID: 92574016001 Collected: 11/23/21 10:15 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310E TOC Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
Total Organic Carbon ND mg/L 1.0 1 12/05/21 16:14 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 34

aceAnalyticalm
(r
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ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3 Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids Analytical Method: SM 2540C-2015
Pace Analytical Services - Eden
Total Dissolved Solids 69.2 mg/L 38.5 1 11/30/21 13:42
350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia ND mg/L 0.10 1 11/23/21 14:58 7664-41-7
353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate ND mg/L 0.20 5 11/23/21 17:17 14797-55-8
MBIO 9222D Fecal Coliform EDN
Fecal Coliforms
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
ND CFU/100 mL 1.0 1 11/23/21 14:18 11/24/21 12:35
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone ND ug/L 25.0 1 12/03/21 10:23 67-64-1
Benzene ND ug/L 1.0 1 12/03/21 10:23 71-43-2
Bromobenzene ND ug/L 1.0 1 12/03/21 10:23 108-86-1
Bromochloromethane ND ug/L 1.0 1 12/03/21 10:23 74-97-5
Bromodichloromethane ND ug/L 1.0 1 12/03/21 10:23 75-27-4
Bromoform ND ug/L 1.0 1 12/03/21 10:23 75-25-2
Bromomethane ND ug/L 2.0 1 12/03/21 10:23 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 12/03/21 10:23 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 12/03/21 10:23 56-23-5
Chlorobenzene ND ug/L 1.0 1 12/03/21 10:23 108-90-7
Chloroethane ND ug/L 1.0 1 12/03/21 10:23 75-00-3
Chloroform ND ug/L 1.0 1 12/03/21 10:23 67-66-3
Chloromethane ND ug/L 1.0 1 12/03/21 10:23 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 12/03/21 10:23 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 12/03/21 10:23 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 12/03/21 10:23 96-12-8
Dibromochloromethane ND ug/L 1.0 1 12/03/21 10:23 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 12/03/21 10:23 106-93-4
Dibromomethane ND ug/L 1.0 1 12/03/21 10:23 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:23 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:23 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 12/03/21 10:23 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 12/03/21 10:23 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 12/03/21 10:23 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 12/03/21 10:23 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 12/03/21 10:23 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 12/03/21 10:23 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 12/03/21 10:23 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 12/03/21 10:23 78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 34

ace Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3
Parameters
Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Results
Units Report Limit DF
Prepared
Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofluorom ethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
300.0 IC Anions 28 Days
Chloride
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
97
99
101
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
2.0 1
5.0 1
1.0 1
5.0 1
5.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
1.0 1
2.0 1
1.0 1
1.0 1
2.0 1
1.0 1
70-130 1
70-130 1
70-130 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
4.0 mg/L
1.0 1
12/03/21 10:23 142-28-9
12/03/21 10:23 594-20-7
12/03/21 10:23 563-58-6
12/03/21 10:23 10061-01-5
12/03/21 10:23 10061-02-6
12/03/21 10:23 108-20-3
12/03/21 10:23 100-41-4
12/03/21 10:23 87-68-3
12/03/21 10:23 591-78-6
12/03/21 10:23 99-87-6
12/03/21 10:23 75-09-2
12/03/21 10:23 108-10-1
12/03/21 10:23 1634-04-4
12/03/21 10:23 91-20-3
12/03/21 10:23 100-42-5
12/03/21 10:23 630-20-6
12/03/21 10:23 79-34-5
12/03/21 10:23 127-18-4
12/03/21 10:23 108-88-3
12/03/21 10:23 87-61-6
12/03/21 10:23 120-82-1
12/03/21 10:23 71-55-6
12/03/21 10:23 79-00-5
12/03/21 10:23 79-01-6
12/03/21 10:23 75-69-4
12/03/21 10:23 96-18-4
12/03/21 10:23 108-05-4
12/03/21 10:23 75-01-4
12/03/21 10:23 1330-20-7
12/03/21 10:23 179601-23-1
12/03/21 10:23 95-47-6
12/03/21 10:23 460-00-4
12/03/21 10:23 17060-07-0
12/03/21 10:23 2037-26-5
11 /26/21 17:59 16887-00-6
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
2.1 mg/L
0.050 1 12/06/21 22:17 12/07/21 17:28 7723-14-0
REPORT OF LABORATORY ANALYSIS
Date: 12/09/2021 04:33 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 34

ace Analytical
www.pacelabs.cam
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3 Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
Total Organic Carbon 1.1 mg/L 1.0 1 12/05/21 16:29 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 34